2005 obp biennial peer review selective harvest kevin l. kenney, christopher t. wright biomass...

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2005 OBP Biennial Peer Review Selective Harvest Kevin L. Kenney, Christopher T. Wright Biomass Feedstock Interface Platform November 14, 2005

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  • 2005 OBP Biennial Peer ReviewSelective Harvest

    Kevin L. Kenney, Christopher T. WrightBiomass Feedstock Interface PlatformNovember 14, 2005

  • OverviewWork ObjectiveObjective Decrease 2005 cost to $35/dry ton by 2015 for the purpose reducing sugar cost by almost 2 cents per lb, for all Billion Ton Vision FeedstocksBudget About $2M per year from 2004 -2006Current Partners National Laboratories, Universities, Equipment IndustryDeveloping Partners Agribusiness Commodity Companies, Regional Feedstock Centers Partnerships, Feedstock Interface to Biorefining PartnersNote: Sugar conversion cost estimate reductions based on the 2005 post-enzyme subcontract conversion case.

    Cost Chart 1

    1028.51103.5

    12.515.51112.251.75

    12.515.510.259.251.75

    12.515.510.2581.75

    1315.510.2561.75

    1314.251061.75

    152315020

    1012.582.7511.75

    912.552.755.75

    $53.00

    $53.00

    $49.25

    $46.00

    $39.50

    $35.00

    $45.00

    $73.00

    $35.00

    Production

    Harvest & Collection

    Transportation & Handling

    Preprocessing

    Storage

    Cost ($/dry ton)

    Cost Chart 2

    12.515.51112.251.75

    152315020

    912.552.755.75

    $53.00

    $73.00

    $35.00

    Production

    Harvest & Collection

    Transportation & Handling

    Preprocessing

    Storage

    Cost ($/dry ton)

    Chart Data

    2005 Dry2005 Wet2015 Multifeed

    Production$12.50$15.00$9.00

    Harvest & Collection$15.50$23.00$12.50

    Preprocessing$12.25-$2.75

    Transportation & Handling$11.00$15.00$5.00

    Storage$1.75$20.00$5.75

    Total$53.00$73.00$35.00

    Chris Wright:Don MacRea: $6.00 wet ton bagged %70 moisture 9-9-05

    Chris Wright:Don MacRea: $7.50 wet ton cop, haul, minus $2.00 for packing %70 moisture 9-9-05

  • PathwayAgriculture Residue PathwayEnergy Crops PathwayPathway Impact:B-Level Milestone Agriculture residue and energy crop feedstocks available to a biorefinery at $35/dry ton by 2015C-Level Milestones Production($10.00), Harvest/Collect($12.50), Storage($1.75), Transport($8.00), Preprocessing ($2.75), System IntegrationCost and Quality Improvements (dry biomass first, wet second)

  • Approach1. DOE Multi-Year Technical Plan Barriers for Feedstock Supply can be grouped into:Cost - $35 / try ton (Operational and Capital Costs)Quality dockage, composition, conversion efficiency (selective harvest, fractional milling, in-storage fractional conversion)Quantity biomass types (Billion Ton Study)2. Develop preprocessing based feedstock supply systems that interface biorefining conversion processes to feedstock resources:Corn StoverCereal StrawSwitchgrass

  • Interim Stage Gate OverviewFeedstock Interface Core R&DAg Residue Processing R&DEnergy Crop Processing R&DFeedstock Supply Chain AnalysisHarvest & CollectionPreprocessingStorageFeedstock Harvest & Collection Assembly System Classification of Biomass Physical Properties in Preprocessing Multi-Component Harvesting Equipment for Sugars Biomass Structure Task Post-Harvest Physiology of Biomass Storage Collection, Commercial Processing, and Utilization of Corn Stover Native Grass Utilization Project Biomass Power for Rural Development Chariton Valley Switchgrass Project UT Switchgrass Project Biomass Supply Systems & LogisticsSupply Forecast & Analysis Harvesting CollectionSystems IntegrationVirtual Engineering Tools for Airstream Separation

  • Summarized Reviewer CommentsThis project was categorized by the reviewers as engineering tool development rather than an R&D project subject to Stage-Gate decision-making. It was observed that the modeling tool(s) were general and that increased focus on biomass and biomass-related applications would be of greater benefit.Recommendation: It is important to identify biomass feedstock characteristics that are important to a biorefinery and show how these tools can help provide feedstock with these characteristics more cheaply/efficiently. The question of where processing is most effectively done needs to be answered. What are the trade-offs on where you effect the separations? These questions need to be answered and the tool tied directly to real-world equipment development.

  • DOE ResponseProject focused on the relevance to a specific biomass application selective harvestIdentified necessary approachIdentified theoretical targetsIdentified practical targetsDeveloped and applied a computational engineering tool to achieve practical targetsField tested functionality of engineered solutionAnalyzed residue fractions to establish the value of selective harvest not according to theoretical separation targets, but according to actual separations accomplished with a grain combine

  • DOE ResponsePractical Quality TargetsOptimize Engineering Design AnalysisResultsTesting

    Chart9

    35.627912811121.562655816818.14145835037.1945276143

    39.405872118120.44591824720.30439569712.8403940336

    32.569296349422.065732436815.963070614811.2683631814

    Glucan

    Xylan

    Acid insoluble lignin

    Ash

    Composition (%)

    UK

    Wheat

    GlucoseGlucanXyloseXylanAcid insoluble ligninAcid soluble ligninAsh

    DistributionAvgSEAvgAvgSEAvgAvgSEAvgSEAvgSE

    Chaff0.2437.00633756930.365658642233.305703812325.51322421180.676539667122.451637306414.89983931510.20413702373.38228253040.071724925512.16950573920.5288970172

    Internodes0.3345.4944604770.549405843940.945014429322.82289723060.352495302120.084149562920.31832504060.23121523242.90022526580.05992828632.83045646850.1048276757

    Leaves0.1835.09713303580.501724850731.587419732224.4899916030.41329317821.551192610617.38071234780.08244138943.45161900780.044900840210.06683977090.2698258306

    Nodes0.1339.4431317320.34777013535.498818558824.27756151970.380677561721.364254137420.26903659450.16625295273.28419965810.05180703492.86562016030.1419525939

    Whole Stover40.15884550640.444806316435.627912811124.194805270.460014946421.562655816818.14145835030.17212229343.20385995750.05696006587.19452761430.3528588043

    StrawInternode + Nodes43.78430235340.492421839239.405872118123.2339980080.360459853720.44591824720.30439569710.21285632723.0087397680.057633152.84039403360.1153195004

    ChaffChaff + Leaves36.18810705490.423972731632.569296349425.07469595090.563719743222.065732436815.96307061480.15198175193.41199816360.060228888911.26836318140.4178665086

    Straw No BaffleCH-S-NB39.405872118138.191156796723.4720794292

    Chaff No BaffleCH-C-NB36.594411936523.9803994085

    Straw BaffleCH-S-B40.979214528622.3308704179

    Chaff BaffleCH-C-B32.343326205223.5034692963

    Control37.621.7

    Corn

    Cob0.1541.33059006911.260045892737.197531062232.1627802130.235046418328.303246587517.74286544620.31893024464.81604854310.09822280570.28441654440.0385015976

    Husk0.0842.96724627780.867372405338.670521650133.55660217880.465702265929.529809917412.24882096890.07747620884.14618199740.12352538160.70638608830.0199683918

    Leaves0.2841.83315678710.537545680837.649841108422.92610958121.195613912620.174976431517.47830884030.13937813845.46761499520.16825804692.2073705330.0634454118

    Bottom0.443.31184314711.724444184138.980658832421.02774728550.28772873518.504417611220.56675561680.18627618054.63591202140.16445890940.4269152130.0726178421

    Top0.0841.22018061310.944950326337.098162551823.45193019890.630593376620.63769857518.28445690650.10644957934.35440425330.0495419291.18360313840.0211357303

    Whole Stover42.39656951611.186144612838.156912564524.46011032230.578610104721.524897083718.40880885760.17786863714.83611231190.14290365920.99261763060.0564398197

    Cob/Stalk42.5745082831.514889815338.317057454723.98677835250.318723693521.108364950219.6045851050.20772377024.64305465130.13409577610.48907431420.0579575157

    Chaff42.0851766740.610840508437.876659006625.28844126961.033411324522.253828317216.31620042450.12562215415.17396321790.15831745461.87381843420.0537838518

    UK

    39.405872118138.1911567967

    20.44591824723.4720794292

    20.304395697118.3398887335

    2.84039403365.391659488

    Target

    No Baffle

    INL

    39.405872118120.445918247

    38.191156796723.4720794292

    40.979214528622.3308704179

    32.569296349422.0657324368

    36.594411936523.9803994085

    32.343326205223.5034692963

    Glucan

    Xylan

    Composition (%)

    Sheet1

    000

    000

    000

    000

    Whole Stover

    Straw

    Chaff

    Compositon ((%)

    0000

    0000

    0000

    Glucan

    Xylan

    Acid insoluble lignin

    Ash

    Composition (%)

    0000

    0000

    0000

    Glucan

    Xylan

    Acid insoluble lignin

    Ash

    Composition (%)

    srm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjdirect measurementdirect measurementtheoretical ehtanol yield

    SampleStarting WeightFinal VolumeGlucanXylanGalactanArabinanMannan% Lignin% RecoveryGlucanXylanGalactanArabinanMannan% LigninGlucanXylanGalactanArabinanMannanacid insoluble ligninacid insoluble ash

    CH-S-NB aCH-S-NB0.50362000.30697874570.17351846780.00746750620.01829772870.00295975030.2384829230.747705121538.17%23.45%0.75%1.83%0.30%17.81%CH-S-NB aStraw No Baffle38.238.1923.523.470.750.761.831.830.300.2718.3918.345.465.39112.5

    CH-S-NB b0.50142000.31042213210.17460103770.00792367980.0186925750.00265444710.23693657760.751230449338.59%23.60%0.79%1.87%0.27%17.69%CH-S-NB b38.623.60.791.870.2718.355.35

    CH-S-NB c0.5012000.30412876030.17288301750.00750625970.01790297910.00240173140.23652694610.741349694237.81%23.37%0.75%1.79%0.24%17.66%CH-S-NB c37.823.40.751.790.2418.285.37

    CH-C-NB aCH-C-NB0.50432000.2891111530.17451962040.00865992230.01945383850.00479110610.24727344830.743809088635.95%23.59%0.87%1.95%0.48%18.46%CH-C-NB aChaff No Baffle35.936.5923.623.980.870.851.951.970.480.4817.7317.647.006.93111.4111.95

    CH-C-NB b0.50582000.300875860.1793445480.00803463320.01998514840.00496621010.24337682880.756583228337.41%24.24%0.80%2.00%0.50%18.17%CH-C-NB b37.424.20.802.000.5017.406.94

    CH-C-NB c0.50272000.29301413230.17842137680.00892880720.01965519980.00467936860.2464690670.751167951736.43%24.11%0.89%1.97%0.47%18.40%CH-C-NB c36.424.10.891.970.4717.806.84

    CH-S-B aCH-S-B0.50342000.32398993150.16174946910.00759096620.01833981070.00321454620.22050059590.735385319840.28%21.86%0.76%1.83%0.32%16.47%CH-S-B aStraw Baffle40.340.9821.922.330.760.801.831.890.320.3517.6417.714.414.48115.6

    CH-S-B b0.50182000.33176940490.16800690720.00834043450.01916660170.00373365340.22359505780.754612059541.25%22.71%0.83%1.92%0.37%16.70%CH-S-B b41.222.70.831.920.3717.864.50

    CH-S-B c0.50092000.33304445750.16591508150.00811323110.01913106740.0034854760.2216011180.751290431541.41%22.42%0.81%1.91%0.35%16.55%CH-S-B c41.422.40.811.910.3517.654.51

    CH-C-B aCH-C-B0.50312000.26021161540.17333521140.01115216150.02214755770.00778434690.2770820910.75171298432.35%23.43%1.12%2.21%0.78%20.69%CH-C-B aChaff Baffle32.432.3423.423.501.121.082.212.210.780.7816.5016.6911.211.25104.6

    CH-C-B b0.5012000.26059266280.17277585860.01041194940.02192557960.00775326710.27984031940.753299636832.40%23.35%1.04%2.19%0.78%20.90%CH-C-B b32.423.41.042.190.7816.6511.3110.21

    CH-C-B c0.50492000.25962072570.17558820420.01075199770.02213801820.00788302850.28118439290.757166367232.28%23.73%1.08%2.21%0.79%21.00%CH-C-B c32.323.71.082.210.7916.9111.2

    Control aControl0.50042000.29918003730.15864226670.00709100550.01792444550.00151161910.21502797760.699377351637.20%21.44%0.71%1.79%0.15%16.06%Control aControl37.237.6021.421.700.710.721.791.810.150.1617.1117.084.404.22108.1

    Control b0.50142000.29919995130.15886123550.00719783690.01792364790.00169957810.21400079780.698883047437.20%21.47%0.72%1.79%0.17%15.98%Control b37.221.50.721.790.1717.234.17

    Control c0.5039200.50.30888539170.16416471920.00730070610.01854174080.0014413720.2097638420.710097771838.40%22.19%0.73%1.85%0.14%15.66%Control c38.422.20.731.850.1416.894.09

    NISTnist data0.3760.2170.080.0250.0030.15937.60%21.70%8.00%2.50%0.30%NIST

    mean controlsour data0.30242179340.16055607380.00719651620.01812994470.00155085640.212930872537.60%21.70%0.72%1.81%0.16%15.90%mean controls17.07544584250.5%

    multiplierdivisors0.80431328040.73988974081111.33918787723.3%

    University of Kentucky Data

    GlucoseGlucanXyloseXylanAcid insoluble ligninAsh

    DistributionAvgAvgAvgAvgAvgAvg

    Chaff0.2437.006337569333.305703812325.513224211822.451637306414.899839315112.1695057392

    Internodes0.3345.49446047740.945014429322.822897230620.084149562920.31832504062.8304564685

    Leaves0.1835.097133035831.587419732224.48999160321.551192610617.380712347810.0668397709

    Nodes0.1339.44313173235.498818558824.277561519721.364254137420.26903659452.8656201603

    Whole StoverWhole Plant40.1636.1424.1121.220.942.040.5618.236.86106.1

    Chaff TargetChaff + Leaves36.188107054932.569296349425.074695950922.065732436815.963070614811.2683631814

    Straw TargetInternode + Nodes43.784302353439.405872118123.23399800820.44591824720.30439569712.8403940336

    Theoretical Straw w/Baffle7% straw, 93% chaff36.719840725833.047856653224.945847094921.952345443516.2669633706010.678405341

    0%

    0000

    0000

    0000

    0000

    0000

    0000

    Glucan

    Xylan

    Acid Insoluble Lignin

    Acid Insoluble Ash

    Composition (%)

    0

    0

    0

    0

    Theoretical Ethanol Yield (gal/dry ton)

    0000

    0000

    0000

    Glucan

    Xylan

    acid insoluble lignin

    acid insoluble ash

    Composition (%)

    GlucanXylanAcid Insoluble LigninAshGlucanXylanAcid Insoluble LigninAsh

    Whole Stover36.121.218.26.9Whole Wheat Stover36.121.218.26.9

    Straw Target39.420.420.32.8Straw Target39.43.39.0%21.0%20.4-0.8-3.6%-7.3%20.32.111.4%27.2%2.8-4.0-58.6%-74.8%

    Chaff Target32.622.116.011.3Chaff Target32.6-3.6-9.9%22.10.84.0%16.0-2.3-12.4%11.34.464.2%

    Straw - No Baffle38.2b23.5a18.3a5.4cStraw - No Baffle38.2b2.05.7%4.4%23.5a2.310.6%-2.1%18.3a0.10.6%3.9%5.4c-1.5-21.4%-22.2%

    Chaff - No Baffle36.6c24.0a17.6b6.9bChaff - No Baffle36.6c0.51.2%24.0a2.813.0%17.6b-0.6-3.2%6.9b0.10.9%

    Straw - Baffle41.0a22.3b17.7b4.5dStraw - Baffle41.0a4.813.4%26.7%22.3b1.15.2%-5.0%17.7b-0.5-2.8%6.2%4.5d-2.4-34.8%-60.2%

    Chaff - Baffle32.3d23.5a16.7c11.3aChaff - Baffle32.3d-3.8-10.5%23.5a2.310.8%16.7c-1.5-8.5%11.3a4.463.9%

    0000

    0000

    0000

    Glucan

    Xylan

    Acid Insoluble Lignin

    Ash

    % Difference

    Straw Compared to Whole Stover

    0000

    0000

    0000

    0000

    0000

    0000

    0000

    b

    a

    a

    c

    c

    a

    b

    b

    a

    b

    b

    d

    d

    a

    c

    a

    Glucan

    Xylan

    Acid Insoluble Lignin

    Ash

    Composition (%)

    0000

    0000

    0000

    Glucan

    Xylan

    Acid Insoluble Lignin

    Ash

    % Difference

    Straw Compared to Chaff

    0000

    0000

    0000

    Glucan

    Xylan

    Acid Insoluble Lignin

    Ash

    % Difference

    Chaff Compared to Whole Stover

  • Ongoing Tasks: Feedstock Conversion Interface (Quality)Anatomical Plant Parts Theoretical Quality TargetsCompositionPretreatment SeverityTechno-economic analysis Identifies differential product yield potential and conversion efficiency for plant partsMotivation for selective harvest

    Chart3

    000000000

    26.321031155811.07484904497.76101608688.32535305629.26238967967.28028571597.56012289516.78191336547.6218530933

    20.031546694846.247221864738.171560979870.490076230324.166210314538.534393108121.283782778817.164867306248.9981657189

    14.983750896357.245165292144.077056827959.820047845218.821460797132.225781082318.233906746625.004042022253.854255202

    16.447094415671.331262898377.696458074387.096575481316.066648694540.875108476417.16630684522.154845806591.4423750422

    Wheat Chaff

    Wheat Chaff Pretreated

    Wheat Leaves

    Wheat Leaves Pretreated

    Wheat Nodes

    Wheat Nodes Pretreated

    Wheat Internodes

    Wheat Internodes Pretreated

    NREL Pretreated Control

    Time (days)

    [ETOH] (% of theoretical glucose conversion)

    Sheet1

    Experiment #5

    Kentucky corn and Holm

    start 9-15-5 for pretreatment

    SSF start 9-22-5

    1st draft 9-19-5 DB

    rawrawrawraw% th% th% th% th

    Sample nameSample #empty panwet + pandry + panwater (g)% moisturemass to addamt addedDMC-6PT MultiplierC-6 final13571357Sample name01357

    6 Stalk corn5010.98840.988438.980658832438.98065883240.26089085470.30227464530.25098694570.378071525637.283974986739.474161109230.223406939546.56164496556 Stalk corn034.630077175440.655878093539.161436646347.9750232898

    51 Stalk corn5020.98950.989538.980658832438.98065883240.19201885770.26283248440.342182850.367771107627.628117721933.924222442942.920596311845.071963411351 Stalk corn6.12275468347.39368342877.77304159693.81162916

    106 Stalk corn5030.98890.988938.980658832438.98065883240.273154450.36752991680.35216022410.41926022538.978138817548.569250728344.340306687652.2914614928106 Stalk corn

    6 leaves corn5041.00771.007737.649841108437.64984110840.08883745070.33785297530.18686632690.336529316913.444329425445.136067032221.592262178341.38841137916 leaves corn013.883548768728.473719440231.690606268439.7889375195

    51 leaves corn5050.980.9837.649841108437.64984110840.04410589710.17814786260.2691992460.27623197997.296494801623.105488114534.217724518933.758851869751 leaves corn6.817283558314.73106915819.1018223655.4106640261

    106 leaves corn5060.98580.985837.649841108437.64984110840.13823820480.13823790120.3053558860.349706457520.909822079117.17960317439.26183210844.2195493097106 leaves corn

    6 tops corn5070.97760.977637.098162551837.09816255180.26270073520.30259642880.40629614290.587394441839.877402786141.983216732255.166252620980.542488256 tops corn038.491403787354.398732808362.186590291485.2362548137

    51 tops corn5080.99150.991537.098162551837.09816255180.24923591590.36062674930.42906856240.518181210837.347292754449.8894787757.726433340469.281495882951 tops corn1.282281768615.181012068410.024467511918.7476316129

    106 tops corn5090.99140.991437.098162551837.09816255180.25537287430.50699879180.53791238730.768154454438.249515821471.323502922773.6670849131105.8847803081106 tops corn

    6 cobs corn5100.99570.995737.197531062237.19753106220.10282319510.1857531860.25445972560.226516571215.80504350224.123346535631.944882363726.40298638556 cobs corn010.459413662422.764065247632.945429288629.8466708653

    51 cobs corn5111.10661.106637.197531062237.19753106220.09524155010.19641757790.35491027130.229696533313.229358201623.100786522241.883377453124.172931536451 cobs corn7.14530960251.55522530998.48205016437.9742616485

    106 cobs corn5121.00911.009137.197531062237.19753106220.01044642910.16668751180.20905915140.31652587922.343839283521.06806268525.008028048938.964094674106 cobs corn

    6 husk corn5131.10411.104138.670521650138.67052165010.06671331520.43480999590.24889623360.3322353149.156502259552.335323210327.009585858536.23618790666 husk corn033.576889837844.46485958239.37075880157.1680450976

    51 husk corn5141.02521.025238.670521650138.67052165010.27265234630.27265234630.44044350150.508490515237.831352685134.33920562155.103764344762.963518219351 husk corn22.59557814989.207577023814.347392011218.7195122381

    106 husk corn5151.01641.016438.670521650138.67052165010.38640889580.3608574620.2975030360.572696238253.742814568946.720049914635.998926199772.3044291669106 husk corn

    Holm 24 chaff5161.03921.039233.305703812333.30570381230.4585642990.15420807860.13080762910.15382986872.255808098420.906935879614.94764333416.9459638431Holm 24 chaff026.321031155820.031546694814.983750896316.4470944156

    Holm 31 chaff5171.04511.045133.305703812333.30570381230.02309768260.19183884110.13757201260.15262988224.484600022926.610094035715.909655487116.66466877Holm 31 chaff39.79675695427.05708017070.90838918390.6362000464

    Holm 48 chaff5181.05211.052133.305703812333.30570381230.00857188830.10167114940.12644474690.14727308112.222685346312.57761016914.093953867915.7306506336Holm 48 chaff

    Holm 24 leaves5191.03361.033631.587419732231.58741973220.04888286470.27204035040.31027835770.61677138979.033703396741.596780013745.444801939994.3137777918Holm 24 leaves07.761016086838.171560979844.077056827977.6964580743

    Holm 31 leaves5201.05311.053131.587419732231.58741973220.05365011810.17194260110.26779858160.5055554159.638094526724.623914042837.727192540774.5650782612Holm 31 leaves2.744465406712.20111490025.788480570715.2939764162

    Holm 48 leaves5211.03831.038331.587419732231.58741973220.02219456370.31398028010.33354668740.43601137724.611250336948.29398888349.059176003264.2105181698Holm 48 leaves

    Holm 24 nodes5221.01561.015635.498818558835.49881855880.05359456490.13933712590.13665542420.16133010318.884499563417.850124653815.223440117.3886653406Holm 24 nodes09.262389679624.166210314518.821460797116.0666486945

    Holm 31 nodes5231.01871.018735.498818558835.49881855880.04415477180.1883987930.16743763790.13866496727.451910306425.100919387519.76048002913.9609888216Holm 31 nodes2.02603029625.90448275063.23247574211.8433160634

    Holm 48 nodes5241.02421.024235.498818558835.49881855880.07142653320.21933433310.17976804930.158680729211.450759168929.547586902321.480462262316.8502919211Holm 48 nodes

    Holm 24 internodes5251.01851.018540.945014429340.94501442930.04492462370.16941781470.20190761980.189523936.561383120519.315694694221.586109598518.6731287374Holm 24 internodes07.560122895121.283782778818.233906746617.166306845

    Holm 31 internodes5261.02171.021740.945014429340.94501442930.04691877090.19469239320.12943626850.16576615856.797504176222.508349764312.190537176415.5567232639Holm 31 internodes1.52994316731.72130163475.24413758541.5607420486

    Holm 48 internodes5271.02251.022540.945014429340.94501442930.06658490530.19108902480.1974244230.17917486399.321481388622.027303877920.925073464917.2690685337Holm 48 internodes

    PTPT6 Stalk corn5280.97591.11510.99770.11740.84339080466.38532110096.39241.001108620738.980658832448.72582354050.05332681670.19806110240.31948368990.33067857576.536872783519.674978119931.432704432131.54504859036 Stalk corn06.516856947825.366391188110.441689515231.668549517

    PTPT51 Stalk corn5290.98071.09790.9960.10190.86945392497.6601307197.67821.002358873738.980658832448.72582354050.04720746540.27114907080.04981000440.34853566075.854085802127.70808704331.663076642333.474372728951 Stalk corn0.65299334374.954610357918.25964833861.7473491671

    PTPT106 Stalk corn5300.97661.08630.99850.08780.80036463085.00913242015.06541.011232999138.980658832448.72582354050.05962436330.28259849310.01852117340.31930400837.159612257828.7161084011-1.770712528929.9862272317106 Stalk corn

    PTPT6 leaves corn5310.9771.18821.00080.18740.88731060618.87394957988.89231.002067897737.649841108447.06230138550.09994414320.37694967430.37368441520.485583760612.084031509240.775705234938.701028508550.31525916076 leaves corn010.078879622538.309314005548.845086051764.704384914

    PTPT51 leaves corn5320.97761.10160.99580.10580.85322580656.81318681326.810.999532258137.649841108447.06230138550.07712301240.37263898920.58318954760.79928597619.502452413440.385721012862.780334660586.351009075651 leaves corn1.78803755843.9390079712.479306609819.0826434317

    PTPT106 leaves corn5330.98031.07740.99610.08130.83728115356.14556962036.24271.015804943437.649841108447.06230138550.07090742960.31961452760.43473489940.55494293588.65015494533.766515768745.053894986157.4468865057106 leaves corn

    PTPT6 tops corn5340.98031.06960.99480.07480.83762597986.15862068976.11250.992511198237.098162551846.37270318980.05529819620.20329585260.29601812330.45729977277.158706026721.464848162730.568584170348.2462355186 tops corn07.302930944130.307523935542.800812747764.672330656

    PTPT51 tops corn5350.98291.08810.9970.09110.86596958177.46099290787.47071.001301045637.098162551846.37270318980.06552332320.3598769330.42990822840.81134745428.281595886939.433965413845.826481100288.878989344451 tops corn0.91511640058.987918887511.035008747721.4046267837

    PTPT106 tops corn5360.98251.08340.99860.08480.84043607536.26708074536.30341.005795242837.098162551846.37270318980.05013842760.27989035070.48522193390.53770854626.468490918830.023758230152.007372972656.8917671056106 tops corn

    PTPT6 cobs corn5370.9821.09711.01020.08690.7549956564.08156028374.10121.004811815837.197531062246.49691382780.02132331960.29922377310.59063101750.61415088043.136621135832.201011759764.067466971965.60520032316 cobs corn06.239773153145.584191508165.21792383880.0889571877

    PTPT51 cobs corn5380.98241.10331.00840.09490.78494623664.654.75451.022473118337.197531062246.49691382780.06868833750.46076821260.58173281150.62283618258.446909184349.941000212761.953028795565.455673687151 cobs corn2.766210996111.82299996793.967267517825.2162074721

    PTPT106 cobs corn5390.9831.06270.9940.06870.86198243415.5556.01010.829499372637.197531062246.49691382780.04522090740.4109949790.53350836710.82714510427.135789139254.610562551869.6332757465109.2059975529106 cobs corn

    PTPT6 husk corn5400.98291.09240.99920.09320.85114155256.7177914118.12611.209638630138.670521650148.33815206260.08173848110.49064550990.57242040780.74729416198.069717462843.357069720649.51487421864.68132440996 husk corn07.036755121745.86174090655.35104301976.5546428171

    PTPT51 husk corn5410.97711.06850.98840.08010.87636761498.08849557528.17041.010126039438.670521650148.33815206260.04451055510.37722592240.38268123970.68887431615.558257338539.413226324338.371089336971.014417255551 husk corn1.31367209068.000507903920.529918880415.4094338447

    PTPT106 husk corn5420.97951.11470.99720.11750.86908284027.63841807917.64171.000429659838.670521650148.33815206260.06130674470.5121200070.73675545150.888843837.482290563754.814926673278.167165501993.968186786106 husk corn

    PTPTHolm 24 chaff5430.97971.09181.00920.08260.73684210533.83.84531.011921052633.305703812341.63212976540.09064459920.46860940940.44023499380.559840174912.338580542557.360509900951.828827672565.8149830703Holm 24 chaff011.074849044946.247221864757.245165292171.3312628983

    PTPTHolm 31 chaff5440.97971.05450.99590.05860.78342245994.61728395064.6891.015532085633.305703812341.63212976540.06846824970.25761412690.42437713970.56969627399.470394767130.284831851649.624926616266.8362005918Holm 31 chaff1.464135041714.174217013411.3436562058.6850992975

    PTPTHolm 48 chaff5450.981.07761.00150.07610.77971311484.53953488374.56851.006380635233.305703812341.63212976540.08293393720.41740939970.58160038090.67784417711.415571825151.096323841570.281741587581.3426050329Holm 48 chaff

    PTPTHolm 24 leaves5460.98221.11761.0040.11360.83899556876.21100917436.70011.078745790331.587419732239.48427466530.04640331010.53780501130.60783290080.82905210866.61105737365.481629630972.449960646599.1290320725Holm 24 leaves08.325353056270.490076230359.820047845287.0965754813

    PTPTHolm 31 leaves5470.98091.10460.99740.10720.86661277287.4969696977.54571.006531.587419732239.48427466530.05513882230.39350634760.47892725620.51866120518.269167772350.630836205560.184947507164.1895992258Holm 31 leaves1.74306760222.780208402712.816259206319.8464700982

    PTPTHolm 48 leaves5480.97981.11350.99760.11590.86686611827.51123595518.24871.09818145131.587419732239.48427466530.0754081490.78772760110.41180469030.833855294710.095834023395.357762854546.82523538297.9710951456Holm 48 leaves

    PTPTHolm 24 nodes5490.98121.07490.9990.07590.81003201715.26404494385.4221.030006403435.498818558844.37352319850.06342353390.26419095730.40240775650.44297778088.166135683728.789361687843.316616473646.8971951825Holm 24 nodes07.280285715938.534393108132.225781082340.8751084764

    PTPTHolm 31 nodes5500.97931.10120.99780.10340.84823625926.58918918926.66581.011626743235.498818558844.37352319850.06576466090.34713005520.36393809010.36973973288.595319946739.26097416239.489169656238.9643300704Holm 31 nodes1.91806366539.402818843816.01001218945.3300777832

    PTPTHolm 48 nodes5510.97841.08040.99710.08330.81666666675.45454545455.54761.0170635.498818558844.37352319850.03668059040.41838689310.15099032690.3530404725.079401517547.552843474513.871557117336.7638001764Holm 48 nodes

    PTPTHolm 24 internodes5520.98111.06640.99370.07270.85228604926.76984126986.84771.011500820640.945014429351.18126803660.05643475990.2113714050.27701800210.35309884966.482576919619.922999261725.200478208332.0550067876Holm 24 internodes06.781913365417.164867306225.004042022222.1548458065

    PTPTHolm 31 internodes5530.98011.09430.99810.09620.84238178636.34444444446.37131.004232924740.945014429351.18126803660.06512018310.19811574490.27796981150.10818857297.439386201818.678511680225.48257310336.6299641624Holm 31 internodes0.57014669713.75143200550.601315217913.6138278976

    PTPTHolm 48 internodes5540.97911.07910.99750.08160.8165.43478260875.491.0101640.945014429351.18126803660.055787550.14361715050.26832971260.31163804546.42377697512.893090976824.32907475527.7795664695Holm 48 internodes

    PTPTcontrol NREL5550.86.20511598213.510.70260.3960.390.05307333630.38918351980.50335083110.71764154167.489371262446.913483381259.520852627185.445609592control NREL07.621853093348.998165718953.85425520291.4423750422

    PTPTcontrol NREL5560.83.48523.49410.6988260.3960.390.05376517090.32809625580.40887994750.75188653977.611722610939.332877636747.738221356990.2037307214control NREL0.137826583310.85876371945.90415910476.7024842473

    PTPTcontrol NREL5570.83.48523.51220.7024460.3960.390.05527755350.49840777870.46254249750.8223094867.764465406760.748136138854.303691622198.6777848131control NREL

    water558-0.0023420377-0.01433606340.03532970980.0466244401

    water559-0.00100026110.03360968260.03362868160.0436170164

    water560-0.01433606340.04018408450.03521615770.0444644658

    Sheet1

    00000000000

    00000000000

    00000000000

    00000000000

    00000000000

    Corn Stalk Bottoms

    Corn Stalk Bottoms Pretreated

    Corn Leaves

    Corn Leaves Pretreated

    Corn Tops

    Corn Tops Pretreated

    Corn Cobs

    Corn Cobs Pretreated

    Corn Husks

    Corn Husks Pretreated

    NREL Pretreated Control

    Time (days)

    [ETOH] (% of theoretical glucose conversion)

    Sheet2

    000000000

    000000000

    000000000

    000000000

    000000000

    Wheat Chaff

    Wheat Chaff Pretreated

    Wheat Leaves

    Wheat Leaves Pretreated

    Wheat Nodes

    Wheat Nodes Pretreated

    Wheat Internodes

    Wheat Internodes Pretreated

    NREL Pretreated Control

    Time (days)

    [ETOH] (% of theoretical glucose conversion)

    Sheet3

  • Ongoing Tasks: Feedstock Conversion Interface (Quality)Residue Fractions:Chaff (hulls, awns, leaves)Straw (internodal stem, nodes)Practical Quality TargetsHand Fractionation vs. Combine FractionationAnatomical Fractions:Chaff (hulls, awns, etc.)LeavesInternodal StemNodes

    Chart9

    35.627912811121.562655816818.14145835037.1945276143

    39.405872118120.44591824720.30439569712.8403940336

    32.569296349422.065732436815.963070614811.2683631814

    Glucan

    Xylan

    Acid insoluble lignin

    Ash

    Composition (%)

    UK

    Wheat

    GlucoseGlucanXyloseXylanAcid insoluble ligninAcid soluble ligninAsh

    DistributionAvgSEAvgAvgSEAvgAvgSEAvgSEAvgSE

    Chaff0.2437.00633756930.365658642233.305703812325.51322421180.676539667122.451637306414.89983931510.20413702373.38228253040.071724925512.16950573920.5288970172

    Internodes0.3345.4944604770.549405843940.945014429322.82289723060.352495302120.084149562920.31832504060.23121523242.90022526580.05992828632.83045646850.1048276757

    Leaves0.1835.09713303580.501724850731.587419732224.4899916030.41329317821.551192610617.38071234780.08244138943.45161900780.044900840210.06683977090.2698258306

    Nodes0.1339.4431317320.34777013535.498818558824.27756151970.380677561721.364254137420.26903659450.16625295273.28419965810.05180703492.86562016030.1419525939

    Whole Stover40.15884550640.444806316435.627912811124.194805270.460014946421.562655816818.14145835030.17212229343.20385995750.05696006587.19452761430.3528588043

    StrawInternode + Nodes43.78430235340.492421839239.405872118123.2339980080.360459853720.44591824720.30439569710.21285632723.0087397680.057633152.84039403360.1153195004

    ChaffChaff + Leaves36.18810705490.423972731632.569296349425.07469595090.563719743222.065732436815.96307061480.15198175193.41199816360.060228888911.26836318140.4178665086

    Straw No BaffleCH-S-NB39.405872118138.191156796723.4720794292

    Chaff No BaffleCH-C-NB36.594411936523.9803994085

    Straw BaffleCH-S-B40.979214528622.3308704179

    Chaff BaffleCH-C-B32.343326205223.5034692963

    Control37.621.7

    Corn

    Cob0.1541.33059006911.260045892737.197531062232.1627802130.235046418328.303246587517.74286544620.31893024464.81604854310.09822280570.28441654440.0385015976

    Husk0.0842.96724627780.867372405338.670521650133.55660217880.465702265929.529809917412.24882096890.07747620884.14618199740.12352538160.70638608830.0199683918

    Leaves0.2841.83315678710.537545680837.649841108422.92610958121.195613912620.174976431517.47830884030.13937813845.46761499520.16825804692.2073705330.0634454118

    Bottom0.443.31184314711.724444184138.980658832421.02774728550.28772873518.504417611220.56675561680.18627618054.63591202140.16445890940.4269152130.0726178421

    Top0.0841.22018061310.944950326337.098162551823.45193019890.630593376620.63769857518.28445690650.10644957934.35440425330.0495419291.18360313840.0211357303

    Whole Stover42.39656951611.186144612838.156912564524.46011032230.578610104721.524897083718.40880885760.17786863714.83611231190.14290365920.99261763060.0564398197

    Cob/Stalk42.5745082831.514889815338.317057454723.98677835250.318723693521.108364950219.6045851050.20772377024.64305465130.13409577610.48907431420.0579575157

    Chaff42.0851766740.610840508437.876659006625.28844126961.033411324522.253828317216.31620042450.12562215415.17396321790.15831745461.87381843420.0537838518

    UK

    39.405872118138.1911567967

    20.44591824723.4720794292

    20.304395697118.3398887335

    2.84039403365.391659488

    Target

    No Baffle

    INL

    39.405872118120.445918247

    38.191156796723.4720794292

    40.979214528622.3308704179

    32.569296349422.0657324368

    36.594411936523.9803994085

    32.343326205223.5034692963

    Glucan

    Xylan

    Composition (%)

    Sheet1

    000

    000

    000

    000

    Whole Stover

    Straw

    Chaff

    Compositon ((%)

    0000

    0000

    0000

    Glucan

    Xylan

    Acid insoluble lignin

    Ash

    Composition (%)

    0000

    0000

    0000

    Glucan

    Xylan

    Acid insoluble lignin

    Ash

    Composition (%)

    srm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjdirect measurementdirect measurementtheoretical ehtanol yield

    SampleStarting WeightFinal VolumeGlucanXylanGalactanArabinanMannan% Lignin% RecoveryGlucanXylanGalactanArabinanMannan% LigninGlucanXylanGalactanArabinanMannanacid insoluble ligninacid insoluble ash

    CH-S-NB aCH-S-NB0.50362000.30697874570.17351846780.00746750620.01829772870.00295975030.2384829230.747705121538.17%23.45%0.75%1.83%0.30%17.81%CH-S-NB aStraw No Baffle38.238.1923.523.470.750.761.831.830.300.2718.3918.345.465.39112.5

    CH-S-NB b0.50142000.31042213210.17460103770.00792367980.0186925750.00265444710.23693657760.751230449338.59%23.60%0.79%1.87%0.27%17.69%CH-S-NB b38.623.60.791.870.2718.355.35

    CH-S-NB c0.5012000.30412876030.17288301750.00750625970.01790297910.00240173140.23652694610.741349694237.81%23.37%0.75%1.79%0.24%17.66%CH-S-NB c37.823.40.751.790.2418.285.37

    CH-C-NB aCH-C-NB0.50432000.2891111530.17451962040.00865992230.01945383850.00479110610.24727344830.743809088635.95%23.59%0.87%1.95%0.48%18.46%CH-C-NB aChaff No Baffle35.936.5923.623.980.870.851.951.970.480.4817.7317.647.006.93111.4111.95

    CH-C-NB b0.50582000.300875860.1793445480.00803463320.01998514840.00496621010.24337682880.756583228337.41%24.24%0.80%2.00%0.50%18.17%CH-C-NB b37.424.20.802.000.5017.406.94

    CH-C-NB c0.50272000.29301413230.17842137680.00892880720.01965519980.00467936860.2464690670.751167951736.43%24.11%0.89%1.97%0.47%18.40%CH-C-NB c36.424.10.891.970.4717.806.84

    CH-S-B aCH-S-B0.50342000.32398993150.16174946910.00759096620.01833981070.00321454620.22050059590.735385319840.28%21.86%0.76%1.83%0.32%16.47%CH-S-B aStraw Baffle40.340.9821.922.330.760.801.831.890.320.3517.6417.714.414.48115.6

    CH-S-B b0.50182000.33176940490.16800690720.00834043450.01916660170.00373365340.22359505780.754612059541.25%22.71%0.83%1.92%0.37%16.70%CH-S-B b41.222.70.831.920.3717.864.50

    CH-S-B c0.50092000.33304445750.16591508150.00811323110.01913106740.0034854760.2216011180.751290431541.41%22.42%0.81%1.91%0.35%16.55%CH-S-B c41.422.40.811.910.3517.654.51

    CH-C-B aCH-C-B0.50312000.26021161540.17333521140.01115216150.02214755770.00778434690.2770820910.75171298432.35%23.43%1.12%2.21%0.78%20.69%CH-C-B aChaff Baffle32.432.3423.423.501.121.082.212.210.780.7816.5016.6911.211.25104.6

    CH-C-B b0.5012000.26059266280.17277585860.01041194940.02192557960.00775326710.27984031940.753299636832.40%23.35%1.04%2.19%0.78%20.90%CH-C-B b32.423.41.042.190.7816.6511.3110.21

    CH-C-B c0.50492000.25962072570.17558820420.01075199770.02213801820.00788302850.28118439290.757166367232.28%23.73%1.08%2.21%0.79%21.00%CH-C-B c32.323.71.082.210.7916.9111.2

    Control aControl0.50042000.29918003730.15864226670.00709100550.01792444550.00151161910.21502797760.699377351637.20%21.44%0.71%1.79%0.15%16.06%Control aControl37.237.6021.421.700.710.721.791.810.150.1617.1117.084.404.22108.1

    Control b0.50142000.29919995130.15886123550.00719783690.01792364790.00169957810.21400079780.698883047437.20%21.47%0.72%1.79%0.17%15.98%Control b37.221.50.721.790.1717.234.17

    Control c0.5039200.50.30888539170.16416471920.00730070610.01854174080.0014413720.2097638420.710097771838.40%22.19%0.73%1.85%0.14%15.66%Control c38.422.20.731.850.1416.894.09

    NISTnist data0.3760.2170.080.0250.0030.15937.60%21.70%8.00%2.50%0.30%NIST

    mean controlsour data0.30242179340.16055607380.00719651620.01812994470.00155085640.212930872537.60%21.70%0.72%1.81%0.16%15.90%mean controls17.07544584250.5%

    multiplierdivisors0.80431328040.73988974081111.33918787723.3%

    University of Kentucky Data

    GlucoseGlucanXyloseXylanAcid insoluble ligninAsh

    DistributionAvgAvgAvgAvgAvgAvg

    Chaff0.2437.006337569333.305703812325.513224211822.451637306414.899839315112.1695057392

    Internodes0.3345.49446047740.945014429322.822897230620.084149562920.31832504062.8304564685

    Leaves0.1835.097133035831.587419732224.48999160321.551192610617.380712347810.0668397709

    Nodes0.1339.44313173235.498818558824.277561519721.364254137420.26903659452.8656201603

    Whole StoverWhole Plant40.1636.1424.1121.220.942.040.5618.236.86106.1

    Chaff TargetChaff + Leaves36.188107054932.569296349425.074695950922.065732436815.963070614811.2683631814

    Straw TargetInternode + Nodes43.784302353439.405872118123.23399800820.44591824720.30439569712.8403940336

    Theoretical Straw w/Baffle7% straw, 93% chaff36.719840725833.047856653224.945847094921.952345443516.2669633706010.678405341

    0%

    0000

    0000

    0000

    0000

    0000

    0000

    Glucan

    Xylan

    Acid Insoluble Lignin

    Acid Insoluble Ash

    Composition (%)

    0

    0

    0

    0

    Theoretical Ethanol Yield (gal/dry ton)

    0000

    0000

    0000

    Glucan

    Xylan

    acid insoluble lignin

    acid insoluble ash

    Composition (%)

    GlucanXylanAcid Insoluble LigninAshGlucanXylanAcid Insoluble LigninAsh

    Whole Stover36.121.218.26.9Whole Wheat Stover36.121.218.26.9

    Straw Target39.420.420.32.8Straw Target39.43.39.0%21.0%20.4-0.8-3.6%-7.3%20.32.111.4%27.2%2.8-4.0-58.6%-74.8%

    Chaff Target32.622.116.011.3Chaff Target32.6-3.6-9.9%22.10.84.0%16.0-2.3-12.4%11.34.464.2%

    Straw - No Baffle38.2b23.5a18.3a5.4cStraw - No Baffle38.2b2.05.7%4.4%23.5a2.310.6%-2.1%18.3a0.10.6%3.9%5.4c-1.5-21.4%-22.2%

    Chaff - No Baffle36.6c24.0a17.6b6.9bChaff - No Baffle36.6c0.51.2%24.0a2.813.0%17.6b-0.6-3.2%6.9b0.10.9%

    Straw - Baffle41.0a22.3b17.7b4.5dStraw - Baffle41.0a4.813.4%26.7%22.3b1.15.2%-5.0%17.7b-0.5-2.8%6.2%4.5d-2.4-34.8%-60.2%

    Chaff - Baffle32.3d23.5a16.7c11.3aChaff - Baffle32.3d-3.8-10.5%23.5a2.310.8%16.7c-1.5-8.5%11.3a4.463.9%

    0000

    0000

    0000

    Glucan

    Xylan

    Acid Insoluble Lignin

    Ash

    % Difference

    Straw Compared to Whole Stover

    0000

    0000

    0000

    0000

    0000

    0000

    0000

    b

    a

    a

    c

    c

    a

    b

    b

    a

    b

    b

    d

    d

    a

    c

    a

    Glucan

    Xylan

    Acid Insoluble Lignin

    Ash

    Composition (%)

    0000

    0000

    0000

    Glucan

    Xylan

    Acid Insoluble Lignin

    Ash

    % Difference

    Straw Compared to Chaff

    0000

    0000

    0000

    Glucan

    Xylan

    Acid Insoluble Lignin

    Ash

    % Difference

    Chaff Compared to Whole Stover

  • Ongoing TasksObjective: Design a baffle to accomplish high-fidelity residue separation

    Approach: Develop virtual engineering model to design baffle separator by simulating baffle performance to (1) determine the effect of the baffle on the airflow of the combine cleaning system and (2) predict the effectiveness of the baffle in separating the residue streams. Model Components:Combine geometryBaffle design canvas (CAD tool)Embedded, interactive CFD model of the single-phase air flow of the combine cleaning systemComputational Engineering Approach

  • Ongoing TasksBaffle increased the chaff stream purity from 64% to 93%The 7% straw is result if spearing through the concavesShows that chaff mixing with the straw is not a problemTesting

    Chart7

    0.40828640390.4145562886

    0.59171359610.5854437114

    No Baffle

    Baffle

    Mass Fraction

    Straw Wagon Sample

    Sheet1

    Container Wts (kg)23456PanSample Size (gm)

    2.5542.5872.5872.6252.5972.61625

    Sample IDSieve Time (min)Sieve #2Sieve #3Sieve #4Sieve #5Sieve #6PanSumSample IDSieve #2Sieve #3Sieve #4Sieve #5Sieve #6PanSum

    WB_S_NB3Gross3.1503.3463.3273.2483.4003.240WB_S_NB3.594.584.463.764.843.7625.00

    Net0.5960.7590.7400.6230.8030.6244.145

    14%18%18%15%19%15%100%

    33%67%100%

    0.603

    WB_S_B_12.5Gross6.2833.6753.5613.2843.5322.989WB_S_B_15.645.234.683.174.491.7925.00

    Net1.1751.0880.9740.6590.9350.3735.204

    23%21%19%13%18%7%100%

    43%57%100%

    1.161

    WB_S_B_25Gross3.0493.6863.8293.4173.6493.188WB_S_B_22.365.235.913.775.012.7225.00

    Net0.4951.0991.2420.7921.0520.5725.252

    9%21%24%15%20%11%100%

    30%70%100%

    WB_C_NB5Gross3.0103.3123.5264.2854.2153.856WB_C_NB1.722.733.546.256.094.6725.00

    Net0.4560.7250.9391.6601.6181.2406.638

    7%11%14%25%24%19%100%

    18%82%100%

    0.476

    WB_C_B_12.5Gross2.7203.1204.0385.6744.9823.907WB_C_B_10.471.504.098.596.723.6425.00

    Net0.1660.5331.4513.0492.3851.2918.875

    2%6%16%34%27%15%100%

    8%92%100%

    WB_C_B_25Gross2.6783.1533.1154.7634.6313.836WB_C_B_20.472.142.008.097.694.6125.00

    Net0.1240.5660.5282.1382.0341.2206.610

    2%9%8%32%31%18%100%

    10%90%100%

    CH_S_NB2.5Gross6.2083.5173.5013.3283.3983.140CH_S_NB5.534.684.603.534.032.6325.00

    Net1.1000.9300.9140.7030.8010.5244.972

    22%19%18%14%16%11%100%

    41%59%100%

    CH_S_B2.5Gross6.1273.5163.4503.2363.4773.013CH_S_B5.424.944.593.254.682.1125.00

    Net1.0190.9290.8630.6110.8800.3974.699

    22%20%18%13%19%8%100%

    41%59%100%

    CH_C_NB2.5Gross6.1253.7073.5163.5773.8953.179CH_C_NB4.324.763.954.055.522.3925.00

    Net1.0171.1200.9290.9521.2980.5635.879

    17%19%16%16%22%10%100%

    36%64%100%

    CH_C_B_2.52.5Gross2.6683.0593.8825.0115.1773.936CH_C_B_2.50.351.443.967.307.904.0425.00

    Net0.1140.4721.2952.3862.5801.3208.167

    1%6%16%29%32%16%100%

    7%93%100%

    CH_C_B_33Gross2.6753.3253.3834.8405.4394.100CH_C_B0.372.252.436.768.674.5325.00

    Net0.1210.7380.7962.2152.8421.4848.196

    1%9%10%27%35%18%100%

    10%90%100%

    Sheet1

    000

    000

    WB_S_NB

    WB_S_B_1

    WB_S_B_2

    Mass Fraction

    Westbred 936 - Straw Wagon

    Sheet2

    000

    000

    WB_C_NB

    WB_C_B_1

    WB_C_B_2

    Mass Fraction

    Westbred 936 - Chaff Wagon

    Sheet4

    000

    000

    CH_C_NB

    CH_C_B_2.5

    CH_C_B_3

    Mass Fraction

    Challis - Chaff Wagon

    Sheet3

    kennkl:2 sample weights

    kennkl:2 samples - so subtract 2 container wts.

    kennkl:2 sample weights

    kennkl:2 samples - so subtract 2 container wts.

    kennkl:2 sample weights

    kennkl:2 samples - so subtract 2 container wts.

    CH_S_NB

    CH_S_B

    Mass Fraction

    Challis - Straw Wagon

    Straw

    Straw

    Chaff

    Chaff

    0

    0

    0

    0

    kennkl:2 sample weights

    kennkl:2 samples - so subtract 2 container wts.

    kennkl:re-weigh sample - this weight includes baggie weight of sub-samples and some of the sample may have been removed for compositional analysis

    kennkl:re-weigh sample - this weight includes baggie weight of sub-samples and some of the sample may have been removed for compositional analysis

    kennkl:re-weigh sample - this weight includes baggie weight of sub-samples and some of the sample may have been removed for compositional analysis

    Sheet3

    0.1437876960.22578785550.0942498096

    0.18311218340.20906994620.2092536177

    0.17852834740.18716372020.2364813404

    0.15030156820.1266333590.1507996954

    0.19372738240.1796694850.2003046458

    0.15054282270.07167563410.1089108911

    WB_S_NB

    WB_S_B_1

    WB_S_B_2

    Mass Fraction

    Westbred 936 - Straw

    0.06869539020.01870422540.0187594554

    0.10921964450.0600563380.0856278366

    0.14145827060.16349295770.0798789713

    0.25007532390.34354929580.3234493192

    0.24374811690.26873239440.3077155825

    0.1868032540.14546478870.1845688351

    WB_C_NB

    WB_C_B_1

    WB_C_B_2

    Mass Fraction

    Westbred 936 - Chaff

    0.40828640390.4145562886

    0.59171359610.5854437114

    No Baffle

    Baffle

    Mass Fraction

    Straw Wagon Sample

    0.36349719340.0717521734

    0.63650280660.9282478266

    No Baffle

    Baffle

    Mass Fraction

    Chaff Wagon Sample

    0.32689987940.43485780170.3035034273

    0.67310012060.56514219830.6964965727

    WB_S_NB

    WB_S_B_1

    WB_S_B_2

    Mass Fraction

    Westbred 936 - Straw

    0.17791503460.07876056340.104387292

    0.82208496540.92123943660.895612708

    WB_C_NB

    WB_C_B_1

    WB_C_B_2

    Mass Fraction

    Westbred 936 - Chaff

    0.36349719340.07175217340.104807223

    0.63650280660.92824782660.895192777

    CH_C_NB

    CH_C_B_2.5

    CH_C_B_3

    Mass Fraction

    Challis - Chaff

    0.40828640390.4145562886

    0.59171359610.5854437114

    CH_S_NB

    CH_S_B

    Mass Fraction

    Challis - Straw

    Chart7

    0.36349719340.0717521734

    0.63650280660.9282478266

    No Baffle

    Baffle

    Mass Fraction

    Chaff Wagon Sample

    Sheet1

    Container Wts (kg)23456PanSample Size (gm)

    2.5542.5872.5872.6252.5972.61625

    Sample IDSieve Time (min)Sieve #2Sieve #3Sieve #4Sieve #5Sieve #6PanSumSample IDSieve #2Sieve #3Sieve #4Sieve #5Sieve #6PanSum

    WB_S_NB3Gross3.1503.3463.3273.2483.4003.240WB_S_NB3.594.584.463.764.843.7625.00

    Net0.5960.7590.7400.6230.8030.6244.145

    14%18%18%15%19%15%100%

    33%67%100%

    0.603

    WB_S_B_12.5Gross6.2833.6753.5613.2843.5322.989WB_S_B_15.645.234.683.174.491.7925.00

    Net1.1751.0880.9740.6590.9350.3735.204

    23%21%19%13%18%7%100%

    43%57%100%

    1.161

    WB_S_B_25Gross3.0493.6863.8293.4173.6493.188WB_S_B_22.365.235.913.775.012.7225.00

    Net0.4951.0991.2420.7921.0520.5725.252

    9%21%24%15%20%11%100%

    30%70%100%

    WB_C_NB5Gross3.0103.3123.5264.2854.2153.856WB_C_NB1.722.733.546.256.094.6725.00

    Net0.4560.7250.9391.6601.6181.2406.638

    7%11%14%25%24%19%100%

    18%82%100%

    0.476

    WB_C_B_12.5Gross2.7203.1204.0385.6744.9823.907WB_C_B_10.471.504.098.596.723.6425.00

    Net0.1660.5331.4513.0492.3851.2918.875

    2%6%16%34%27%15%100%

    8%92%100%

    WB_C_B_25Gross2.6783.1533.1154.7634.6313.836WB_C_B_20.472.142.008.097.694.6125.00

    Net0.1240.5660.5282.1382.0341.2206.610

    2%9%8%32%31%18%100%

    10%90%100%

    CH_S_NB2.5Gross6.2083.5173.5013.3283.3983.140CH_S_NB5.534.684.603.534.032.6325.00

    Net1.1000.9300.9140.7030.8010.5244.972

    22%19%18%14%16%11%100%

    41%59%100%

    CH_S_B2.5Gross6.1273.5163.4503.2363.4773.013CH_S_B5.424.944.593.254.682.1125.00

    Net1.0190.9290.8630.6110.8800.3974.699

    22%20%18%13%19%8%100%

    41%59%100%

    CH_C_NB2.5Gross6.1253.7073.5163.5773.8953.179CH_C_NB4.324.763.954.055.522.3925.00

    Net1.0171.1200.9290.9521.2980.5635.879

    17%19%16%16%22%10%100%

    36%64%100%

    CH_C_B_2.52.5Gross2.6683.0593.8825.0115.1773.936CH_C_B_2.50.351.443.967.307.904.0425.00

    Net0.1140.4721.2952.3862.5801.3208.167

    1%6%16%29%32%16%100%

    7%93%100%

    CH_C_B_33Gross2.6753.3253.3834.8405.4394.100CH_C_B0.372.252.436.768.674.5325.00

    Net0.1210.7380.7962.2152.8421.4848.196

    1%9%10%27%35%18%100%

    10%90%100%

    Sheet1

    000

    000

    WB_S_NB

    WB_S_B_1

    WB_S_B_2

    Mass Fraction

    Westbred 936 - Straw Wagon

    Sheet2

    000

    000

    WB_C_NB

    WB_C_B_1

    WB_C_B_2

    Mass Fraction

    Westbred 936 - Chaff Wagon

    Sheet4

    000

    000

    CH_C_NB

    CH_C_B_2.5

    CH_C_B_3

    Mass Fraction

    Challis - Chaff Wagon

    Sheet3

    kennkl:2 sample weights

    kennkl:2 samples - so subtract 2 container wts.

    kennkl:2 sample weights

    kennkl:2 samples - so subtract 2 container wts.

    kennkl:2 sample weights

    kennkl:2 samples - so subtract 2 container wts.

    CH_S_NB

    CH_S_B

    Mass Fraction

    Challis - Straw Wagon

    Straw

    Straw

    Chaff

    Chaff

    0

    0

    0

    0

    kennkl:2 sample weights

    kennkl:2 samples - so subtract 2 container wts.

    kennkl:re-weigh sample - this weight includes baggie weight of sub-samples and some of the sample may have been removed for compositional analysis

    kennkl:re-weigh sample - this weight includes baggie weight of sub-samples and some of the sample may have been removed for compositional analysis

    kennkl:re-weigh sample - this weight includes baggie weight of sub-samples and some of the sample may have been removed for compositional analysis

    Sheet3

    0.1437876960.22578785550.0942498096

    0.18311218340.20906994620.2092536177

    0.17852834740.18716372020.2364813404

    0.15030156820.1266333590.1507996954

    0.19372738240.1796694850.2003046458

    0.15054282270.07167563410.1089108911

    WB_S_NB

    WB_S_B_1

    WB_S_B_2

    Mass Fraction

    Westbred 936 - Straw

    0.06869539020.01870422540.0187594554

    0.10921964450.0600563380.0856278366

    0.14145827060.16349295770.0798789713

    0.25007532390.34354929580.3234493192

    0.24374811690.26873239440.3077155825

    0.1868032540.14546478870.1845688351

    WB_C_NB

    WB_C_B_1

    WB_C_B_2

    Mass Fraction

    Westbred 936 - Chaff

    0.40828640390.4145562886

    0.59171359610.5854437114

    No Baffle

    Baffle

    Mass Fraction

    Straw Wagon Sample

    0.36349719340.0717521734

    0.63650280660.9282478266

    No Baffle

    Baffle

    Mass Fraction

    Chaff Wagon Sample

    0.32689987940.43485780170.3035034273

    0.67310012060.56514219830.6964965727

    WB_S_NB

    WB_S_B_1

    WB_S_B_2

    Mass Fraction

    Westbred 936 - Straw

    0.17791503460.07876056340.104387292

    0.82208496540.92123943660.895612708

    WB_C_NB

    WB_C_B_1

    WB_C_B_2

    Mass Fraction

    Westbred 936 - Chaff

    0.36349719340.07175217340.104807223

    0.63650280660.92824782660.895192777

    CH_C_NB

    CH_C_B_2.5

    CH_C_B_3

    Mass Fraction

    Challis - Chaff

    0.40828640390.4145562886

    0.59171359610.5854437114

    CH_S_NB

    CH_S_B

    Mass Fraction

    Challis - Straw

  • Ongoing TasksFractionation of residue stream has statistically significant effect on the composition of the the straw and chaff residue streamsHigh-fidelity separation has largest effect on glucan and ash contentCompositional Analysis

    Chart3

    39.405872118120.44591824720.30439569712.8403940336

    32.569296349422.065732436815.963070614811.2683631814

    38.191156796723.472079429218.33988873355.391659488

    36.594411936523.980399408517.6431944636.9274503427

    40.979214528622.330870417917.71466675544.4752256355

    32.343326205223.503469296316.686220400911.250673044

    b

    a

    a

    c

    c

    a

    b

    b

    a

    b

    b

    d

    d

    a

    c

    a

    Glucan

    Xylan

    Acid Insoluble Lignin

    Acid Insoluble Ash

    Composition (%)

    UK

    Wheat

    GlucoseGlucanXyloseXylanAcid insoluble ligninAcid soluble ligninAsh

    DistributionAvgSEAvgAvgSEAvgAvgSEAvgSEAvgSE

    Chaff0.2437.00633756930.365658642233.305703812325.51322421180.676539667122.451637306414.89983931510.20413702373.38228253040.071724925512.16950573920.5288970172

    Internodes0.3345.4944604770.549405843940.945014429322.82289723060.352495302120.084149562920.31832504060.23121523242.90022526580.05992828632.83045646850.1048276757

    Leaves0.1835.09713303580.501724850731.587419732224.4899916030.41329317821.551192610617.38071234780.08244138943.45161900780.044900840210.06683977090.2698258306

    Nodes0.1339.4431317320.34777013535.498818558824.27756151970.380677561721.364254137420.26903659450.16625295273.28419965810.05180703492.86562016030.1419525939

    Whole Plant40.15884550640.444806316435.627912811124.194805270.460014946421.562655816818.14145835030.17212229343.20385995750.05696006587.19452761430.3528588043

    Chaff TargetChaff + Leaves36.18810705490.423972731632.569296349425.07469595090.563719743222.065732436815.96307061480.15198175193.41199816360.060228888911.26836318140.4178665086

    Straw TargetInternode + Nodes43.78430235340.492421839239.405872118123.2339980080.360459853720.44591824720.30439569710.21285632723.0087397680.057633152.84039403360.1153195004

    Straw No BaffleCH-S-NB39.405872118138.191156796723.4720794292

    Chaff No BaffleCH-C-NB36.594411936523.9803994085

    Straw BaffleCH-S-B40.979214528622.3308704179

    Chaff BaffleCH-C-B32.343326205223.5034692963

    Control37.621.7

    Corn

    Cob41.33059006911.260045892732.1627802130.235046418317.74286544620.31893024464.81604854310.09822280570.28441654440.0385015976

    Husk42.96724627780.867372405333.55660217880.465702265912.24882096890.07747620884.14618199740.12352538160.70638608830.0199683918

    Leaves41.83315678710.537545680822.92610958121.195613912617.47830884030.13937813845.46761499520.16825804692.2073705330.0634454118

    Bottom43.31184314711.724444184121.02774728550.28772873520.56675561680.18627618054.63591202140.16445890940.4269152130.0726178421

    Top41.22018061310.944950326323.45193019890.630593376618.28445690650.10644957934.35440425330.0495419291.18360313840.0211357303

    6.83657576868.6358883234

    1.5967448602

    UK

    038.1911567967

    023.4720794292

    018.3398887335

    05.391659488

    Target

    No Baffle

    INL

    00

    00

    00

    00

    00

    00

    Glucan

    Xylan

    Composition (%)

    Sheet1

    srm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjdirect measurementdirect measurement

    SampleStarting WeightFinal VolumeGlucanXylanGalactanArabinanMannan% Lignin% RecoveryGlucanXylanGalactanArabinanMannan% LigninGlucanXylanGalactanArabinanMannanacid insoluble ligninacid insoluble ash

    CH-S-NB aCH-S-NB0.50362000.30697874570.17351846780.00746750620.01829772870.00295975030.2384829230.747705121538.17%23.45%0.75%1.83%0.30%17.81%CH-S-NB aStraw No Baffle38.238.223.523.50.750.81.831.80.300.318.3918.35.465.4

    CH-S-NB b0.50142000.31042213210.17460103770.00792367980.0186925750.00265444710.23693657760.751230449338.59%23.60%0.79%1.87%0.27%17.69%CH-S-NB b38.623.60.791.870.2718.355.35

    CH-S-NB c0.5012000.30412876030.17288301750.00750625970.01790297910.00240173140.23652694610.741349694237.81%23.37%0.75%1.79%0.24%17.66%CH-S-NB c37.823.40.751.790.2418.285.37

    CH-C-NB aCH-C-NB0.50432000.2891111530.17451962040.00865992230.01945383850.00479110610.24727344830.743809088635.95%23.59%0.87%1.95%0.48%18.46%CH-C-NB aChaff No Baffle35.936.623.624.00.870.91.952.00.480.517.7317.67.006.9

    CH-C-NB b0.50582000.300875860.1793445480.00803463320.01998514840.00496621010.24337682880.756583228337.41%24.24%0.80%2.00%0.50%18.17%CH-C-NB b37.424.20.802.000.5017.406.94

    CH-C-NB c0.50272000.29301413230.17842137680.00892880720.01965519980.00467936860.2464690670.751167951736.43%24.11%0.89%1.97%0.47%18.40%CH-C-NB c36.424.10.891.970.4717.806.84

    CH-S-B aCH-S-B0.50342000.32398993150.16174946910.00759096620.01833981070.00321454620.22050059590.735385319840.28%21.86%0.76%1.83%0.32%16.47%CH-S-B aStraw Baffle40.341.021.922.30.760.81.831.90.320.317.6417.74.414.5

    CH-S-B b0.50182000.33176940490.16800690720.00834043450.01916660170.00373365340.22359505780.754612059541.25%22.71%0.83%1.92%0.37%16.70%CH-S-B b41.222.70.831.920.3717.864.50

    CH-S-B c0.50092000.33304445750.16591508150.00811323110.01913106740.0034854760.2216011180.751290431541.41%22.42%0.81%1.91%0.35%16.55%CH-S-B c41.422.40.811.910.3517.654.51

    CH-C-B aCH-C-B0.50312000.26021161540.17333521140.01115216150.02214755770.00778434690.2770820910.75171298432.35%23.43%1.12%2.21%0.78%20.69%CH-C-B aChaff Baffle32.432.323.423.51.121.12.212.20.780.816.5016.711.211.3

    CH-C-B b0.5012000.26059266280.17277585860.01041194940.02192557960.00775326710.27984031940.753299636832.40%23.35%1.04%2.19%0.78%20.90%CH-C-B b32.423.41.042.190.7816.6511.3

    CH-C-B c0.50492000.25962072570.17558820420.01075199770.02213801820.00788302850.28118439290.757166367232.28%23.73%1.08%2.21%0.79%21.00%CH-C-B c32.323.71.082.210.7916.9111.2

    Control aControl0.50042000.29918003730.15864226670.00709100550.01792444550.00151161910.21502797760.699377351637.20%21.44%0.71%1.79%0.15%16.06%Control a37.237.621.421.70.710.71.791.80.150.217.1117.14.404.2

    Control b0.50142000.29919995130.15886123550.00719783690.01792364790.00169957810.21400079780.698883047437.20%21.47%0.72%1.79%0.17%15.98%Control b37.221.50.721.790.1717.234.17

    Control c0.5039200.50.30888539170.16416471920.00730070610.01854174080.0014413720.2097638420.710097771838.40%22.19%0.73%1.85%0.14%15.66%Control c38.422.20.731.850.1416.894.09

    NISTnist data0.3760.2170.080.0250.0030.15937.60%21.70%8.00%2.50%0.30%NIST

    mean controlsour data0.30242179340.16055607380.00719651620.01812994470.00155085640.212930872537.60%21.70%0.72%1.81%0.16%15.90%mean controls17.0754458425

    multiplierdivisors0.80431328040.73988974081111.3391878772

    University of Kentucky Data

    GlucoseGlucanXyloseXylanAcid insoluble ligninAsh

    DistributionAvgAvgAvgAvgAvgAvg

    Chaff0.2437.006337569333.305703812325.513224211822.451637306414.899839315112.1695057392

    Internodes0.3345.49446047740.945014429322.822897230620.084149562920.31832504062.8304564685

    Leaves0.1835.097133035831.587419732224.48999160321.551192610617.380712347810.0668397709

    Nodes0.1339.44313173235.498818558824.277561519721.364254137420.26903659452.8656201603

    Whole Plant40.158845506436.142960955824.112512935321.21901138318.23239963516.8628338541

    Chaff TargetChaff + Leaves36.188107054932.569296349425.074695950922.065732436815.963070614811.2683631814

    Straw TargetInternode + Nodes43.784302353439.405872118123.23399800820.44591824720.30439569712.8403940336

    0%

    36.142960955821.219011383

    Sheet1

    0000

    0000

    0000

    0000

    0000

    0000

    Glucan

    Xylan

    Acid Insoluble Lignin

    Acid Insoluble Ash

    Composition (%)

    GlucanXylanAcid Insoluble LigninAcid Insoluble AshGlucanXylanAcid Insoluble LigninAsh

    Whole Stover36.121.218.26.9Whole Wheat Stover36.121.218.26.9

    Straw Target39.420.420.32.8Straw Target39.43.39.0%21.0%20.4-0.8-3.6%-7.3%20.32.111.4%27.2%2.8-4.0-58.6%-74.8%

    Chaff Target32.622.116.011.3Chaff Target32.6-3.6-9.9%22.10.84.0%16.0-2.3-12.4%11.34.464.2%

    Straw - No Baffle38.2b23.5a18.3a5.4cStraw - No Baffle38.2b2.05.7%4.4%23.5a2.310.6%-2.1%18.3a0.10.6%3.9%5.4c-1.5-21.4%-22.2%

    Chaff - No Baffle36.6c24.0a17.6b6.9bChaff - No Baffle36.6c0.51.2%24.0a2.813.0%17.6b-0.6-3.2%6.9b0.10.9%

    Straw - Baffle41.0a22.3b17.7b4.5dStraw - Baffle41.0a4.813.4%26.7%22.3b1.15.2%-5.0%17.7b-0.5-2.8%6.2%4.5d-2.4-34.8%-60.2%

    Chaff - Baffle32.3d23.5a16.7c11.3aChaff - Baffle32.3d-3.8-10.5%23.5a2.310.8%16.7c-1.5-8.5%11.3a4.463.9%

    0000

    0000

    Glucan

    Xylan

    Acid Insoluble Lignin

    Ash

    0000

    0000

    0000

    Glucan

    Xylan

    Acid Insoluble Lignin

    Ash

    0000

    0000

    0000

    0000

    0000

    0000

    0000

    b

    a

    a

    c

    c

    a

    b

    b

    a

    b

    b

    d

    d

    a

    c

    a

    Glucan

    Xylan

    Acid Insoluble Lignin

    Ash

    Composition (%)

    Chart6

    0.2099086113-0.07340858480.2719605261-0.7479319766

    0.0436335707-0.02119731080.0394879891-0.2216964076

    0.267006809-0.04989045930.0616344702-0.602225963

    Glucan

    Xylan

    Acid Insoluble Lignin

    Acid Insoluble Ash

    % Difference

    Straw Compared to Chaff

    UK

    Wheat

    GlucoseGlucanXyloseXylanAcid insoluble ligninAcid soluble ligninAsh

    DistributionAvgSEAvgAvgSEAvgAvgSEAvgSEAvgSE

    Chaff0.2437.00633756930.365658642233.305703812325.51322421180.676539667122.451637306414.89983931510.20413702373.38228253040.071724925512.16950573920.5288970172

    Internodes0.3345.4944604770.549405843940.945014429322.82289723060.352495302120.084149562920.31832504060.23121523242.90022526580.05992828632.83045646850.1048276757

    Leaves0.1835.09713303580.501724850731.587419732224.4899916030.41329317821.551192610617.38071234780.08244138943.45161900780.044900840210.06683977090.2698258306

    Nodes0.1339.4431317320.34777013535.498818558824.27756151970.380677561721.364254137420.26903659450.16625295273.28419965810.05180703492.86562016030.1419525939

    Whole Plant40.15884550640.444806316435.627912811124.194805270.460014946421.562655816818.14145835030.17212229343.20385995750.05696006587.19452761430.3528588043

    Chaff TargetChaff + Leaves36.18810705490.423972731632.569296349425.07469595090.563719743222.065732436815.96307061480.15198175193.41199816360.060228888911.26836318140.4178665086

    Straw TargetInternode + Nodes43.78430235340.492421839239.405872118123.2339980080.360459853720.44591824720.30439569710.21285632723.0087397680.057633152.84039403360.1153195004

    Straw No BaffleCH-S-NB39.405872118138.191156796723.4720794292

    Chaff No BaffleCH-C-NB36.594411936523.9803994085

    Straw BaffleCH-S-B40.979214528622.3308704179

    Chaff BaffleCH-C-B32.343326205223.5034692963

    Control37.621.7

    Corn

    Cob41.33059006911.260045892732.1627802130.235046418317.74286544620.31893024464.81604854310.09822280570.28441654440.0385015976

    Husk42.96724627780.867372405333.55660217880.465702265912.24882096890.07747620884.14618199740.12352538160.70638608830.0199683918

    Leaves41.83315678710.537545680822.92610958121.195613912617.47830884030.13937813845.46761499520.16825804692.2073705330.0634454118

    Bottom43.31184314711.724444184121.02774728550.28772873520.56675561680.18627618054.63591202140.16445890940.4269152130.0726178421

    Top41.22018061310.944950326323.45193019890.630593376618.28445690650.10644957934.35440425330.0495419291.18360313840.0211357303

    6.83657576868.6358883234

    1.5967448602

    UK

    038.1911567967

    023.4720794292

    018.3398887335

    05.391659488

    Target

    No Baffle

    INL

    00

    00

    00

    00

    00

    00

    Glucan

    Xylan

    Composition (%)

    Sheet1

    srm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjsrm adjdirect measurementdirect measurement

    SampleStarting WeightFinal VolumeGlucanXylanGalactanArabinanMannan% Lignin% RecoveryGlucanXylanGalactanArabinanMannan% LigninGlucanXylanGalactanArabinanMannanacid insoluble ligninacid insoluble ash

    CH-S-NB aCH-S-NB0.50362000.30697874570.17351846780.00746750620.01829772870.00295975030.2384829230.747705121538.17%23.45%0.75%1.83%0.30%17.81%CH-S-NB aStraw No Baffle38.238.223.523.50.750.81.831.80.300.318.3918.35.465.4

    CH-S-NB b0.50142000.31042213210.17460103770.00792367980.0186925750.00265444710.23693657760.751230449338.59%23.60%0.79%1.87%0.27%17.69%CH-S-NB b38.623.60.791.870.2718.355.35

    CH-S-NB c0.5012000.30412876030.17288301750.00750625970.01790297910.00240173140.23652694610.741349694237.81%23.37%0.75%1.79%0.24%17.66%CH-S-NB c37.823.40.751.790.2418.285.37

    CH-C-NB aCH-C-NB0.50432000.2891111530.17451962040.00865992230.01945383850.00479110610.24727344830.743809088635.95%23.59%0.87%1.95%0.48%18.46%CH-C-NB aChaff No Baffle35.936.623.624.00.870.91.952.00.480.517.7317.67.006.9

    CH-C-NB b0.50582000.300875860.1793445480.00803463320.01998514840.00496621010.24337682880.756583228337.41%24.24%0.80%2.00%0.50%18.17%CH-C-NB b37.424.20.802.000.5017.406.94

    CH-C-NB c0.50272000.29301413230.17842137680.00892880720.01965519980.00467936860.2464690670.751167951736.43%24.11%0.89%1.97%0.47%18.40%CH-C-NB c36.424.10.891.970.4717.806.84

    CH-S-B aCH-S-B0.50342000.32398993150.16174946910.00759096620.01833981070.00321454620.22050059590.735385319840.28%21.86%0.76%1.83%0.32%16.47%CH-S-B aStraw Baffle40.341.021.922.30.760.81.831.90.320.317.6417.74.414.5

    CH-S-B b0.50182000.33176940490.16800690720.00834043450.01916660170.00373365340.22359505780.754612059541.25%22.71%0.83%1.92%0.37%16.70%CH-S-B b41.222.70.831.920.3717.864.50

    CH-S-B c0.50092000.33304445750.16591508150.00811323110.01913106740.0034854760.2216011180.751290431541.41%22.42%0.81%1.91%0.35%16.55%CH-S-B c41.422.40.811.910.3517.654.51

    CH-C-B aCH-C-B0.50312000.26021161540.17333521140.01115216150.02214755770.00778434690.2770820910.75171298432.35%23.43%1.12%2.21%0.78%20.69%CH-C-B aChaff Baffle32.432.323.423.51.121.12.212.20.780.816.5016.711.211.3

    CH-C-B b0.5012000.26059266280.17277585860.01041194940.02192557960.00775326710.27984031940.753299636832.40%23.35%1.04%2.19%0.78%20.90%CH-C-B b32.423.41.042.190.7816.6511.3

    CH-C-B c0.50492000.25962072570.17558820420.01075199770.02213801820.00788302850.28118439290.757166367232.28%23.73%1.08%2.21%0.79%21.00%CH-C-B c32.323.71.082.210.7916.9111.2

    Control aControl0.50042000.29918003730.15864226670.00709100550.01792444550.00151161910.21502797760.699377351637.20%21.44%0.71%1.79%0.15%16.06%Control a37.237.621.421.70.710.71.791.80.150.217.1117.14.404.2

    Control b0.50142000.29919995130.15886123550.00719783690.01792364790.00169957810.21400079780.698883047437.20%21.47%0.72%1.79%0.17%15.98%Control b37.221.50.721.790.1717.234.17

    Control c0.5039200.50.30888539170.16416471920.00730070610.01854174080.0014413720.2097638420.710097771838.40%22.19%0.73%1.85%0.14%15.66%Control c38.422.20.731.850.1416.894.09

    NISTnist data0.3760.2170.080.0250.0030.15937.60%21.70%8.00%2.50%0.30%NIST

    mean controlsour data0.30242179340.16055607380.00719651620.01812994470.00155085640.212930872537.60%21.70%0.72%1.81%0.16%15.90%mean controls17.0754458425

    multiplierdivisors0.80431328040.73988974081111.3391878772

    University of Kentucky Data

    GlucoseGlucanXyloseXylanAcid insoluble ligninAsh

    DistributionAvgAvgAvgAvgAvgAvg

    Chaff0.2437.006337569333.305703812325.513224211822.451637306414.899839315112.1695057392

    Internodes0.3345.49446047740.945014429322.822897230620.084149562920.31832504062.8304564685

    Leaves0.1835.097133035831.587419732224.48999160321.551192610617.380712347810.0668397709

    Nodes0.1339.44313173235.498818558824.277561519721.364254137420.26903659452.8656201603

    Whole Plant40.158845506436.142960955824.112512935321.21901138318.23239963516.8628338541

    Chaff TargetChaff + Leaves36.188107054932.569296349425.074695950922.065732436815.963070614811.2683631814

    Straw TargetInternode + Nodes43.784302353439.405872118123.23399800820.44591824720.30439569712.8403940336

    0%

    36.142960955821.219011383

    Sheet1

    0000

    0000

    0000

    0000

    0000

    0000

    Glucan

    Xylan

    Acid Insoluble Lignin

    Acid Insoluble Ash

    Composition (%)

    GlucanXylanAcid Insoluble LigninAshGlucanXylanAcid Insoluble LigninAsh

    Whole Stover36.121.218.26.9Whole Wheat Stover36.121.218.26.9

    Straw Target39.420.420.32.8Straw Target39.43.39.0%21.0%20.4-0.8-3.6%-7.3%20.32.111.4%27.2%2.8-4.0-58.6%-74.8%

    Chaff Target32.622.116.011.3Chaff Target32.6-3.6-9.9%22.10.84.0%16.0-2.3-12.4%11.34.464.2%

    Straw - No Baffle38.2b23.5a18.3a5.4cStraw - No Baffle38.2b2.05.7%4.4%23.5a2.310.6%-2.1%18.3a0.10.6%3.9%5.4c-1.5-21.4%-22.2%

    Chaff - No Baffle36.6c24.0a17.6b6.9bChaff - No Baffle36.6c0.51.2%24.0a2.813.0%17.6b-0.6-3.2%6.9b0.10.9%

    Straw - Baffle41.0a22.3b17.7b4.5dStraw - Baffle41.0a4.813.4%26.7%22.3b1.15.2%-5.0%17.7b-0.5-2.8%6.2%4.5d-2.4-34.8%-60.2%

    Chaff - Baffle32.3d23.5a16.7c11.3aChaff - Baffle32.3d-3.8-10.5%23.5a2.310.8%16.7c-1.5-8.5%11.3a4.463.9%

    0000

    0000

    0000

    Glucan

    Xylan

    Acid Insoluble Lignin

    Ash

    % Difference

    Straw Compared to Whole Stover

    0000

    0000

    0000

    0000

    0000

    0000

    0000

    b

    a

    a

    c

    c

    a

    b

    b

    a

    b

    b

    d

    d

    a

    c

    a

    Glucan

    Xylan

    Acid Insoluble Lignin

    Ash

    Composition (%)

    0000

    0000

    0000

    Glucan

    Xylan

    Acid Insoluble Lignin

    Ash

    % Difference

    Straw Compared to Chaff

    0000

    0000

    0000

    Glucan

    Xylan

    Acid Insoluble Lignin

    Ash

    % Difference

    Chaff Compared to Whole Stover

  • Ongoing TasksStraw fraction has highest theoretical ethanol yieldNo Baffle: no value of selective harvest at this level of fractionationBaffle: 11 gallons of ethanol per dry ton difference between chaff and straw streams significant differential value of selective harvestWhole stover ethanol yield approximated by dashed line. 0.5% increase for no-baffle straw, 3.3% increase for baffle strawBaffle: Do not loose higher value straw in chaff streamResults

  • Summary and Future Work

    Platform Level Technical Outcomes Is the Platform performing well?Is the Platform managed in a way that facilitates reaching its end goals?Do the Platform goals support the Programs goals?Are there any outlying projects that do not seem to support the Programs goals?

    The purpose of this slide is to provide some context for evaluating the current work in this barrier element focusing on accomplishments. The information in the left column describes the magnitude and timing of the investment this area. The information in the right column describes the players.Please indicate the degree to which the work on this barrier supports the Platforms goals and objectives of the Multi-Year RD&D plan.Please indicate the relevance to Platform Objectives

    Recommended time for this slide: 1 min(General)Purpose: Describe how the program has addressed the comments received in past reviews.

    Purpose: Describe how the program has addressed the comments received in past reviews.

    Tasks to accomplish/overcome the barriers issuesPurpose: Describe the most important technical accomplishments and results obtained in the last year. Whenever possible, describe the significance of the accomplishments by relating the results to the appropriate DOE targets and milestones from the MYPP. Include sufficient slides to explain what was done leading to the technical accomplishments Please limit your slides to the time you have available you will not be allowed to go over your allotted timeTo assist the reviewers evaluating your work, please include bullet comments of the key points on each slideThough your presentation will be in color, it is best to choose colors and data symbols so that they can be easily distinguished in black and white for those reviewers with hardcopiesTasks to accomplish/overcome the barriers issuesPurpose: Describe the most important technical accomplishments and results obtained in the last year. Whenever possible, describe the significance of the accomplishments by relating the results to the appropriate DOE targets and milestones from the MYPP. Include sufficient slides to explain what was done leading to the technical accomplishments Please limit your slides to the time you have available you will not be allowed to go over your allotted timeTo assist the reviewers evaluating your work, please include bullet comments of the key points on each slideThough your presentation will be in color, it is best to choose colors and data symbols so that they can be easily distinguished in black and white for those reviewers with hardcopiesRecommended time for this slide: 1 minPurpose: Describe what will be done in the remainder of this year and in the coming year.