2014 - · pdf fileformulation guide 2014 ... body wash cream 17 back to basic clear body...

Formulation Guide

2014

Amino acid Based ingredients for personal care

New applicationsFacial wipe for oily skin 6“Diverse” Cleansing Wipe 7Facial wash powder 8Toothpaste 9Foaming Shower Cream 10

Glycinate conceptTransparent Hair Shampoo 13Facial Cream Cleanser 14Facial Wash Cream 15Foaming Make Up Remover 16Body Wash Cream 17

Back to basicClear Body Wash 20Sulfate Free “Natural” Shampoo 21Transparent Hair Shampoo for Oily Hair 22Transparent Hair Shampoo 23Transparent Hand Soap 24

Facial washClear Facial Wash Gel 27“Natural” Facial Skin Toner 28Facial Skin Toner 29Humectant-Rich Anti-Aging Toner 30

Eye Shadow 34Transparent Lipstick 35Solid Fragrance Clear Gel 36BB Balm 37“Natural” Skin Care Cream 38

Formulation finder 40Contact 43

Solutions,inspired from Nature

Amino acids are called the source of LIFE for good reasons. Our bodies’ muscles, organs, SKIN and HAIR are all made up of proteins, which are unique combinations of 20 types of AMINO ACIDS.

To bring the blessings of the earth and the very essence of life to more people, AJINOMOTO develops amino acid based PERSONAL CARE ingredients, FRIENDLY to people and to earth.

The aim of this formulary is to INSPIRE you in your existing or future product developments.

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NewapplicationsNewS

Newapplications

Our laboratories constantly develop new ideas to sup-port you in your growth platform

“Diverse” Cleansing wipeThis rinse-free cleansing wipe is appropriate to use on a variety of skin areas, including face, hands, and baby’s bottom. The wipe contains AMISOFT ECS-22SB as an economic, mild acyl-glutamate surfactant that selectively cleanses the skin by removing the dirt while leaving the skin undamaged. The after-feel is clean, non-sticky, soft, and conditioned to the touch. AJIDEW NL-50 performs its role as the skin-identical component of the natural moisturizing factor.

PArT INGrEDIENTS % W/W FuNCTION TrADE NAME / SuPPLIEr

A POLYSORBATE-20 0.60 Solubilizing agent LIPOSORB L-20

LIPO CHEMICALS, INC

LAURYL LACTATE 0.25 Emollient /

Spreadability, feel,

moisturization

SCHERCEMOL LL ESTER

LUBRIzOL CORP.

FRAGRANCE 0.10

PHENOxYETHANOL, CAPRYLYL

GLYCOL, HExYLENE GLYCOL

0.80 Preservative DIOCIDE / DIOW, DIST. BY

CENTERCHEM, INC

B BIS PEG-8 DIMETHICONE 0.50 Silicone / After-feel GRANSIL Vx-409

GRANT INDUSTRIES

C AMISOFT ECS-22SB (30%) 2.50 Gentle surfactant /

Cleansing

AJINOMOTO CO. INC

WATER 94.75

AJIDEW NL-50 0.50 Humectant /

Moisturization

AJINOMOTO CO. INC

D CITRIC ACID q.s. to pH

5.5

100.0

PrOCEDurE:

1 Combine part A with mixing at room temperature, add part B, then part C.

2 Mix well and adjust the pH with citric acid (part D).

3 Saturate the wipe cloth and store in an air-tight container.

TECHNICAL INFOrMATION:

Appearance clear solutionFinal pH 5.50Stability > 1 month @ 45, 25, 3°C

Facial wipe for Oily SkinAJIDEW ZN-100 is a multifunctional active ingredient that has anti-sebum oil-reducing properties while also providing anti-aging benefits by reducing collagenase activity via inhibition of Activator Protein-1.


A WATER 83.20 Diluent

B AJIDEW ZN-100 1.00 Active ingredient /

Anti-aging, sebum

appearance

reduction

AJINOMOTO CO. INC

HYDROxYPROPYLTRIMONIUM

HYALURONATE

0.05 Cationic active

ingredient

Conditioned skin

feel

HYALOVEIL-P / KEWPIE

CORP

C WITCH HAzEL (HAMAMELIS

VIRGINIANA) ExTRACT, WATER,

ETHANOL

15.00 Active natural

extract /

Astringency, oil

reduction

WITCH HAzEL DISTILLATE

D PHENYLETHANOL, ETHYLHExYL

GLYCERIN

0.75 Preservative SENSIVA PA-20

SCHüLKE & MYER

100.0

PrOCEDurE:

1 Dissolve part B in part A with thorough mixing at room temperature.

2 Add parts C and D, mix well.

3 Saturate the wipe cloth with the solution and store in an air-tight container.


pH 4.90Stability > 1 month at 45, 25, 3°C

7 Newapplications

ASC

26-119-1ASC

26-

94-3

ToothpasteA SDS-free mild toothpaste.


A CELLULOSE GUM 1.00 Binder CEKOL 3000 / CP KELCO

WATER 49.00

B DIPOTASSIUM GLYCYRRHIzATE 0.10 Active/ anti-

inflammatry

DIPOTASSIUM

GLYCYRRHIzATE

JUNSEI CHEMICAL

SODIUM MONOFLUOROPHOSPHATE 0.10 Active/ anti-caries SODIUM

FLUOROPHOSPHATE

WAKO

SODIUM SACCHARIN 0.15 Flavor SODIUM SACCHARIN

DIHYDRATE / WAKO

WATER Balance

C GLYCERIN 10.00 Humectant

SORBITOL 10.00 Humectant

D SILICA 6.50 Abrasive SYLOPURE 25 / FUJI SILYSIA

SILICA 15.00 Abrasive SYLOPURE 35 / FUJI SILYSIA

E AMISOFT MS-11 2.00 Foaming agent AJINOMOTO CO. INC

F FRAGRANCE q.s.

100.00

PrOCEDurE:

1 Disperse part A at room temperature.

2 Dissolve part B at room temperature.

3 Add part B and C to part A with stirring.

4 Add part D to part A and disperse well at 85°C.

5 Add part E with stirring and cool down to 40°C.

6 Add part F with stirring and cool to room temperature.


pH 6.6Stability 0, 25, 45°C, Cycle, for 1 month

Facial wash § PowderFacial wash in a powder format using mild surfactants Amisoft LS-11 and Amisoft MS-11. Product has to be emulsified in the hands and then applied on the face for a mild cleansing. Amihope LL imports soft sensory feeling.


A AMISOFT LS-11 15.0 Cleansing

surfactant

AJINOMOTO CO. INC

AMISOFT MS-11 15.0 Cleansing

surfactant

AJINOMOTO CO. INC

MANNITOL 10.0 Humectant MARINE CRYSTAL

TOWA CHEMICAL

INDUSTRY

TALC 20.0 Dispersing agent MICROACE P-3

NIPPON TALC

zEA MAYS (CORN) STRACH 23.5 Vehicle ST STARCH C(W)

NIPPON STARCH

CHEMICALS

GLUCOSE 15.0 Vehicle

AMIHOPE LL 1.0 Sensory

improvement

AJINOMOTO CO. INC

AGAR 0.5 Foam stabilizer

100.0

PrOCEDurE:

1 Mix all ingredients and mill.


pH 5.5 (1% aq.)

9

TSIL-P-3-MSPW

T-31

0

Newapplications

Notes

Foaming Shower CreamA sulfate-free, DEA-free, PEG-free cold-process mild shower cream based on a combination of vegetable origin surfactants. AMILITE ACS12 provides rich foam and vegetable origin emollient nourishes the skin.


A WATER Balance

B ACRYLATES COPOLYMER (30%) 8.00 Thickening polymer SYNTHALEN W400

3V SIGMA

C ETHYLHExYL GLYCERIN,

PHENOxYETHANOL, TOCOPHEROL

0.30 Preservatives EUxYL PE9010

SCHULKE & MAYR

AMISOFT ECS-22SB (30%) 15.00 Primary foaming

surfactant

AJINOMOTO CO. INC

AMIILTE ACS-12 (30%) 5.00 Foam booster AJINOMOTO CO. INC

COCAMIDOPROPYL BETAINE (30%) 10.00 Secondary foaming

surfactant

SOFTAzOLIN CPB

KAWAKEN FINE

CHEMICALS

LAURYL GLUCOSIDE (50%) 4.70 Thickening PLANTACARE 1200UP

BASF

PRUNUS AMYGDALUS DULCIS (SWEET

ALMOND) OIL

5.00 Emollient NIKKOL SWEET ALMOND

OIL

NIKKO CHEMICALS

D CITRIC ACID (40% Aq.) 0.30 pH adjustment

E FRAGRANCE q.s.

100.0

PrOCEDurE:

1 Disperse part B in part A at room temperature.

2 Add part C in the listed order to part A and mix well.

3 While stirring gradually add part D to adjust the pH to 5.6 ~ 6.0 (The level of citric acid is presented as a rough guide).

4 Add part E.


pH 6.0 ~ 6.5Viscosity 1,000 ~ 2,000 mPa.s (B-type, Rotor No.3, 12rpm, 30sec., 25°C)Stability -5°C, 0°C, 25°C, 45°C, cycle(-5 n 40°C) for 3 months

KN

S-09

7E-4

Newapplications

11

Mild cleansing with abundant foam providing nourish-ing and refreshing feeling

Glycinate concept

Transparent Hair ShampooA cleansing shampoo which refreshes the hair and scalp. Amilite GCS-12K improves volume and smoothness of the foam while viscosity is controlled by the use of Ajidew NL-50.


A SODIUM LAURETH SULFATE (27%) 27.00 Cleansing

surfactant

EMAL E-27C

KAO

COCAMIDOPROPYL BETAINE (30%) 14.00 Co-surfactant AMPHITOL 55AB / KAO

AMILITE GCS-12K (30%) 12.00 Foam booster AJINOMOTO CO. INC

AJIDEW NL-50 (50%) 1.00 Viscosity modifier AJINOMOTO CO. INC

GLYCERIN 3.00 Moisturizer

PRESERVATIVE q.s.

POLYqUATERNIUM-10 (2%Aq.) 10.00 Hair conditioning

agent

LEOGARD GP

AKzO NOBEL SURFACE

CHEMISTRY AB

WATER Balance

B PEG-150 DISTEARATE 0.40 Thickening polymer EMANON 3299V / KAO

C CITRIC ACID (20%Aq.) 0.81

D AMODIMETHICONE 0.30 Hair conditioning

agent

Fz-4671

DOW CORNING TORAY

E FRAGRANCE q.s.

100.0

PrOCEDurE:

1 Dissolve part A at 60-70°C with stirring.

2 Add part B to part A.

3 Add part C to adjust pH to 6.9. The level of citric acid is presented as a rough guide.

4 Cool down to 45°C, and add part D and part E.

5 Cool down to room temperature with stirring.


pH 6.9Viscosity 4,800-5,200 mPa.s (B type, Rotor No.3, 12rpm, 30sec., 25°C)Stability -5, 25, 45°C, Cycle, for one month

Glycinate concept

13

CC

S-112

Facial Cleanser § CreamAmilite GCS-12K provides creamy foam to this facial cleanser, using an economical production process without vacuum.


A AMILITE GCS-12K(30% ) 29.20 Cleansing

surfactant

AJINOMOTO CO. INC

SODIUM LAURETH SULFATE(27%) 23.00 Cleansing

surfactant

EMAL E-27C / KAO

LAURAMIDOPROPYL BETAINE(30%) 21.00 Cleansing

surfactant

SOFTAzOLINE LPB

KAWAKEN / FINE

CHEMICALS

DISODIUM LAURETH

SULFOSUCCINATE(32%)

2.00 Emulsifier TExAPON SB-3

COGNIS

BUTYLENE GLYCOL 0.20 Humectant

WATER Balance

PRESERVATIVE q.s.

POLYqUATERNIUM-7(10%) 1.00 Film forming agent LIPOFLOW MN / LION

B ALUMINUM MAGNESIUM SILICATE 1.00 Viscosity builder VEEGUM HV GRUNULES

R.T.VANDERBILT

WATER 19.00

C TITANIUM DIOxIDE 0.20 Pigment TIPEqUE CR-50

ISHIHARA SANGYO

D CITRIC ACID (20%Aq.) 3.00

E FRAGRANCE q.s.

100.0

PrOCEDurE:

1 Thoroughly disperse part B at room temperature.

2 Dissolve part A and add part B with stirring at 70-80°C.

3 Add part C with stirring well.

4 Adjust pH to 5.7 with part D. The level of citric acid is presented as a rough guide.

5 Cool to 50°C and add part E.



pH 5.7 Stability -5, 25, 50°C, Cycle for one month

Facial wash § CreamThis good foaming cream-type facial wash formulation employs Amilite GCS-12K (liquid type) in a simple production process.


A AMILITE GCS-12K (30%) 55.00 Cleansing

surfactant

AJINOMOTO CO. INC

WATER Balance

GLYCERIN 28.00 Humectant PRICERINE 9091

UNIqUEMA

SODIUM LAUROAMPHOACETATE

(30%)

8.00 Cleansing

surfactant

SOFTAzOLIN LHL

KAWAKEN FINE

CHEMICALS

POLYqUATERNIUM-39 (10%) 1.00 Film forming agent MERqUAT PLUS 3330

ONDEO NALCO

DISODIUM EDTA 0.05 Chelating agent

CITRIC ACID 1.20 pH adjuster

PRESERVATIVE q.s

B HYDROxYPROPYL METHYLCELLULOSE 0.04 Viscosifier METROSE 60SH-4000

SHIN-ETSU SILICONES

WATER 1.96

100.0

PrOCEDurE:

1 Dissolve part A at 60°C with stirring. The level of citric acid is presented as a rough guide.

2 Start reducing the pressure to 400mmHg.

3 Cool down to the crystallizing temperature (about 49°C) with gentle stirring.

4 When the crystallization started add part B and mix well.



pH 6.9 (1% aqueous solution)Stability 0, 25, 50°C, Cycle(-5 n 40°C) for one month

Glycinate concept

15

SKPE

G-1

12 FC-109H

Bodywash § CreamA sulfate-free, easy-to-prepare creamy body wash with luxurious pearly appearance. Improvement of moisturizing feel is achieved by addition of AMILITE GCS-12K.


A AMILITE GCS-12K(30%) 8.0 Cleansing agent AJINOMOTO CO. INC

COCAMIDOPROPYL

BETAINE(30%)

30.0 Foam stabilizer DEHYTON K / BASF

SODIUM

COCOAMPHOACETATE(32%)

20.0 Foam stabilizer MIRANOL ULTRA C-32

SOLVAY

WATER Balance

B ACRYLATES/BEHENETH-25

METHACRYLATE COPOLYMER

5.0 Thickening agent NOVETHIx L-10

LUBRIzOL

WATER 10.0

C GLYCOL STEARATE 3.0 Pearlesing agent CITHROL EDGS-

PA-(SG) / CRODA

D PRESERVATIVE q.s.

100.0

PrOCEDurE:

1 Mix part A until uniform at room temperature.

2 Mix part B at room temperature.

3 Add part B to part A with stirring.

4 Add part C to the mixture and heat it up about 60 ~ 70°C.

5 Keep stirring until uniform.

6 Cool down to room temperature and add part D.

7 Keep stirring until uniform.


pH 7.3Viscosity 8,000 ~ 12,000 mPa.s (64, 30rpm, 30sec., 24°C)Stability 1, 25, 45°C, Cycle(-5 n 40°C), for 3 months

Foaming Make-up RemoverEasy-to-use self-foaming type make-up remover.Amilite GCS-12K is used for its foamability and fresh skin afterfeel. The stability of the foam is improved by the use of Amisafe AL-01.


A HYDROGENATED POLYISOBUTENE 1.10 Make up cleansing PERLEAM Ex / NOF

PEG-20 GLYCERYL TRIISOSTEARATE 2.70 Emulsifier EMALEx GWIS-320Ex

NIHON EMULSION

FRAGRANCE q.s.

B WATER Balance

ISOPENTYLDIOL 10.00 Solubilizer ISOPRENE GLYCOL-S

KURARAY


AMILITE GCS-12K (30%) 10.00 Cleansing

surfactant

AJINOMOTO CO. INC

LAURAMIDOPROPLY

HYDROxYSULTAINE (30%)

14.00 Cleansing

surfactant

SOFTAzOLINE LSB

KAWAKEN FINE CHEMICAL

LAURYL GLUCOSIDE (50%) 2.00 Foam booster PLANTACARE 1200 UP

BASF-COGNIS

AMISAFE AL-01 0.02 Foam stabilizer AJINOMOTO CO. INC

C DISODIUM EDTA 0.10 Chelating agent

PRESERVATIVES q.s.

100.0

PrOCEDurE:

1 Mix part A until uniform at room temperature.

2 Dissolve part B with stirring at 80°C.

3 Add part C to B and dissolve at 80°C.

4 Cool to 50°C with stirring, add part A to B, stir until uniform.

5 Cool to room temperature with stirring.


pH 7.3Stability -5, 25°C, 45°C 1 month

Glycinate concept

17

AC

AC

-PNS-4D

MS-

14S-

5

Because mild cleansing products always will have a strong value in Cosmetic and Toiletry industries

CleaNSiNG

Back to basic

Sulfate Free “Natural” ShampooThis nature-inspired Sulfate free shampoo is kind to the hair and leaves the hair soft and smooth with good luster.


A AMISOFT ECS-22SB (30%) 10.00 Natural surfactant AJINOMOTO CO. INC.

COCAMIDOPORPYL BETAINE (30%) 33.00 Primary Surfactant LONzAINE C / LONzA

LAURYL GLUCOSIDE (50%) 10.00 Foam stabilizer,

viscosity control

PLANTAREN 1200 N

BASF

GLYCERYL LAURATE 2.00 Viscosity Control MONOMULS 90-L12 / BASF

WATER 43.00 Diluent

B AJIDEW NL-50 (50%) 1.00 Humectant /

moisturizer

AJINOMOTO CO. INC

PrODEW 500 (50%) 1.00 Moisturizer, hair

nourishment

AJINOMOTO CO. INC

C PRESERVATIVE qS per

supplier

Micro-organism

control

D CITRIC ACID To pH 5.5

+/-0.2

pH Adjustment

100.0

PrOCEDurE:

1 Combine ingredients in part A and heat with mixing to 65°C. When clear, cool.

2 At 55°C add ingredients of part B.

3 At 50°C add part C.

4 Cool to room temperature and adjust pH (part D).


Viscosity 2200 mPa.s (Brookfield LV-D spindle #3 @ 30 rpm @ 25°C 30 sec)Stability 4 weeks @ 3°C, 25°C, 40°C, 45°C

Clear BodywashAn extremely mild sulphate-free shower gel, using Amisoft ECS-22SB and Ajidew NL 50 which leave a pleasant soft and moisturized feel to the skin.


A AMISOFT ECS-22SB (30%) 7.5 Secondary

surfactant

AJINOMOTO CO. INC

COCAMIDOPROPYL BETAINE(30%) 26.3 Primary surfactant MIRATAINE BET C30 NP

SOLVAY

DECYL GLUCOSIDE (50%) 4.5 Co-surfactant PLANTACARE 2000UP

BASF

COCAMIDE MEA 1.0 Viscosity modifier NINOL COMF / STEPHAN

PEG-120 METHYL GLUCOSE

TRIOLEATE AND PROPANEDIOL

2.53 Thickening polymer GLUCAMATE VLT

THICKENER / LUBRIzOL

AJIDEW NL-50 (30%) 2.0 Moisturizer AJINOMOTO CO. INC

WATER Balance

B POLYSORBATE 20 1.5 Solubilizer for

fragrance

POLYSORBATE 20

NOF

FRAGRANCE

C 10% CITRIC ACID q.S. TO 5.80 2.32 pH adjustment

D PRESERVATIVE q.s.

100.0

PrOCEDurE:

1 Heat part A about 60-70°C.

2 Add part B to part A.

3 Cool down to room temperature.

4 Add part C (The level of citric acid is presented as a rough guide) and part D to mixture with gentle stirring.


pH 5.88Viscosity 1,000 ~ 1,600 mPa.sStability 1, 25, 45°C, Cycle(-5 n 40°C), for

3 months

21 Back tobasic

ASC

27-15-3A

CA

C-B

SB-2

1

Back tobasic

Transparent Hair ShampooAjidew NL-50 and Ajidew ZN-100 are combined in this shampoo formulation to improve hair condition and sebum control as well as bringing anti-bacterial activity. On top, Amilite ET-CS-12 is boosting foam quality and quantity.


A POLYqUATERNIUM-10 0.2 Conditioning agent UCARE POLYMER JR400 DOW

B WATER 10.0 EMAL E27-C / KAO

C SODIUM LAURETH SULFATE (27%) 40.0 Cleansing surfactant DEHYTON K / BASF

COCAMIDOPROPYL BETAINE (30%) 10.0 Cleansing surfactant

AMILITE ET-CS-12 (25%) 7.0 Foam booster AJINOMOTO CO. INC

GLYCERYL CAPRATE 2.0 Viscosity modifier SANSOFT NO.760 KAWAKEN FINE CHEMICAL

PEG-7 POLYGLYCERYL COCOATE 2.0 Emollient CETIOL HE / BASF


SODIUM CHLORIDE 0.8 Viscosity modifier

PRESERVATIVE q.s

WATER Balance

D FRAGRANCE q.s

E CITRIC ACID 0.1 pH adjuster

WATER q.s.

F AJIDEW ZN-100 0.5 Sebum control, Anti-bacterial

AJINOMOTO CO. INC

WATER 5.0

100.0

PrOCEDurE:1 Thoroughly disperse part A in part B at room temperature.2 Add part B to part C and heat to 80°C. Mix until uniform. 3 Cool to 50°C and add part D.4 Cool to room temperature with stirring.5 Adjust pH with part E (The level of citric acid is presented as a rough guide).

Stir until homogeneous. 6 Add part F and stir until homogeneous. Readjust pH to 5.5 with part E.


pH 5.5Viscosity 3,900 ~ 4,000 mPa.s (B type, rotor No.4, 30rpm, 30sec., 25°C)Stability 45°C, 25°C, 0°C, cycle (-5°C n 40°C) for 1 month

Transparent Hair Shampoo for oily hairThis sulphate-free hair shampoo is formulated for normal to oily hair and scalp. Ajidew ZN-100 is a multifunctional ingredient that has sebum control and antibacterial properties. Amisafe AL-01 is used for its conditioning properties without any greasy feeling after use.


A SODIUM LAURYL SULFOACETATE 4.00 Co-surfactant NIKKOL LSA-F NIKKO CHEMICALS

LAURYL GLUCOSIDE(50%) 9.00 Co-surfactant PLANTACARE 1200UP / BASF

AMISOFT CS-22 (25%) 20.00 Primary cleansingsurfactant

AJINOMOTO CO. INC

PRESERVATIVES q.s.

WATER 45.00

B GLYCERYL CAPRATE 3.00 Viscosity modifier SUNSOFT NO.760 / TAIYO KAGAKU

C AMISAFE AL-01 0.40 Conditioning Agent AJINOMOTO CO. INC

D FRAGRANCE q.s.

E MAGNESIUM CHLORIDE 1.50 Viscosity modifier

F CITRIC ACID 0.50 pH Adjuster

WATER Balance

G AJIDEW ZN-100 0.50 Sebum control,Anti-bacterial

AJINOMOTO CO. INC

WATER 5.00

100.0

PrOCEDurE:

1 Dissolve part A at 80°C with stirring.

2 Mix until uniform and add part B.

3 Mix until uniform and add part C.

4 Cool down to 45°C with stirring, add part D and part E.

5 Cool down to room temperature with stirring, add part F to adjust the pH to 6.0 (The level of citric acid is presented as a rough guide).

6 Add part G with stirring.


pH 5.5Viscosity 1,800 ~ 2,500 mPa.s (B type, rotor No.3, 30rpm, 30sec., 25°C)Stability 0°C, 25°C, 45°C, Cycle(-5 n 40°C) for 1 month 23

CG

-ZN19

NSA

I-ZN

02

Notes

Transparent HandsoapThis clear hand soap contains Ajidew ZN-100, an ingredient with anti-bacterial properties. Amisoft ECS-22SB and Ajidew NL-50 impart moisturized skinfeel to hands after washing.


A SODIUM LAURETH SULFATE (27%) 35.00 Primary cleansing

surfactant

EMAL E-27C/KAO

COCAMIDEPROPYL BETAINE (30%) 15.00 Co-surfactant AMPHITOL 55AB/KAO

AMISOFT ECS-22SB (30%) 1.00 Moisturizing mild

sufractant

AJINOMOTO CO. INC


PRESERVATIVE q.s.

WATER Balance

B CITRIC ACID 0.27 pH adjuster

WATER q.s.

C AJIDEW ZN-100 0.50 Anti-bacterial AJINOMOTO CO. INC

WATER 5.00

100.0

PrOCEDurE:

1 Mix part A with stirring at 80°C.

2 Adjust pH to about 6.0 by part B (The level of citric acid is presented as a rough guide), and add part C.


pH 5.5Viscosity 2,800 ~ 4,000 mPa.s (B type, rotor No.3, 30rpm, 30sec., 25°C)Stability 0°C, 25°C, 45°C, Cycle(-5 n 40°C) for 1 month

HA

N -

ZN

02

25 Back tobasic

Mild and moisturizing ingredients to clean and nourish your face

Clear Facial wash § GelA SLES-free facial cleansing gel which imparts soft and moisturized feel to the skin.


A AMISOFT ECS-22SB (30%) 15.0 Secondary

surfactant

AJINOMOTO CO. INC

COCAMIDOPROPYL BETAINE(30%) 52.5 Primary surfactant MIRATAINE BET C30 NP

SOLVAY

DECYL GLUCOSIDE(50%) 9.0 Foam stabilizer PLANTACARE 2000UP

BASF

COCAMIDE MEA 2.0 Viscosity modifier NINOL COMF / STEPHAN

PEG-120 METHYL GLUCOSE

TRIOLEATE AND PROPANEDIOL

1.0 Thickening polymer GLUCAMATE VLT

THICKENER / LUBRIzOL


WATER Balance

B 10% CITRIC ACID q.S. TO 5.80 4.24 pH adjustment

C PRESERVATIVE q.s.

100.0

PrOCEDurE:

1 Heat part A at around 60-70°C.

2 Add part B (The level of citric acid is presented as a rough guide) to part A.


4 Add part C to mixture with gentle stirring.


pH 5.86Viscosity 6,000 ~ 12,000 mPa.sStability 1, 25, 45°C, Cycle(-5 n 40°C), for 3 months

Facial wash

27

AC

AC

-FSB-6

Faciallwash

Facial Skin TonerA hazy facial skin toner enriched with pseudo-ceramide ELDEW PS-203 r.


A ELDEW PS-203 r 0.35 Emolient AJINOMOTO CO. INC

CETYL ETHYLHExANOATE 0.15 Emolient EMALEx CC168

NIHON EMULSION

PPG-8-CETETH-20 0.50 Emulsifier NIKKOL PBC-44

NIKKO CHEMICALS

PPG-6-DECYLTETRADECETH-30 0.50 Emulsifier NIKKOL PEN-4630

NIKKO CHEMICALS


B WATER 5.00

C DIPROPYLENE GLYCOL 2.00 Moisturizer

BUTYLENE GLYCOL 3.00 Moisturizer

SODIUM CITRATE 0.20 pH Adjuster

PrODEW P-DS-12(30%) 3.33 Moisturizer AJINOMOTO CO. INC

WATER Balance

D CITRIC ACID (20% Aq.) 0.58 pH Adjuster

100.0

PrOCEDurE:

1 Dissolve part A with stirring at 70°C.

2 Add part B slowly at 70°C with stirring.

3 Cool down to 40°C with gentle stirring.

4 Dissolve part C in a separate vessel.

5 Add part C gradually (The level of citric acid is presented as a rough guide) to part A with stirring and cool to room temperature.

6 Adjust the pH with part D.


pH 5.5Stability 0, 25, 45°C, Cycle (-5°C n 40°C), for 1 month

“Natural” Facial Skin TonerAn alcohol-free skin toner formulated only with natural ingredients such as Ajidew NL-50 and Prodew P-DS-12 which bring good nourishing properties.


A SODIUM HYALURONATE 0.10 Moisturizer FCH-120

KIKKOMAN BIOCHEMIFA

B WATER Balance

C SORBITOL 5.00 Moisturizer SORBITOL / KAO



PROPANEDIOL 3.00 zEMEA PROPANEDIOL

DUPONT

PrODEW P-DS-12 (30%) 1.67 Moisturizer AJINOMOTO CO. INC

SODIUM CITRATE (20% Aq.) 0.20 pH adjuster

D CITRIC ACID 0.05 pH adjuster

100.0

PrOCEDurE:

1 Add part A to part B with stirring.

2 After confirmation of dissolution, add part C (The level of citric acid is presented as a rough guide) to part A with stirring.

3 Add part D to part A to adjust the pH.


pH 5.5Stability -5, 25, 45°C, Cycle (-5°C n 40°C),

for 3 months

29

SSPB-CP-2

NTO

N-C

P-3

Faciallwash

Notes

Humectant-Rich anti-aging TonerThis moisturizing toner contains Prodew 500 which is an optimized mix of humectant ingredients and amino acids, as well as anti-aging compounds. Ajidew ZN-100 is a multifunctional active ingredient that has anti-sebum oil-reducing properties while also providing anti-aging benefits by reducing collagenase activity via inhibition of Activator Protein-1.

PArT INGrEDIENTS %W/W FuNCTION TrADE NAME / SuPPLIEr

A TREHALOSE 0.25 Humectant / Moisturization

TREHALOSE / HYASHIBARA

C12-13 ALKYL GLYCERYL HYDROLYzED HYALURONATE

0.05 Active ingredient / Skin barrier repair, moisturization

HYALOREPAIR / KEWPIE CORP.

AJIDEW ZN-100 1.00 Active ingredient / Anti-aging, sebum appearance reduction

AJINOMOTO CO. INC.

B WATER 89.50 Diluent

GLYCERIN 3.00 Humectant / Moisturization

C PrODEW 500 (50%) 1.50 Humectant / Moisturization

AJINOMOTO CO. INC.

SACCHARIDE ISOMERATE 2.00 Humectant / Moisturization

PENTAVITIN / DSM NUTRITIONAL PRODUCTS

PROPYLENE GLYCOL, WATER, ECHINACEA ANGUSTIFOLIA ExTRACT, CENTELLA ASIATICA ExTRACT, FUCUS VESICULOSUS ExTRACT, TRIGONELLA FOENUM-GRAECUM SEED ExTRACT

1.00 Active natural extract / Anti-aging, moisturization, skin firming

POLYPLANT FIRMING PROVITAL GROUP

WATER, BUTYLENE GLYCOL, SAKURA (PRUNUS LANNESIANA) FLOWER ExTRACT, ASCORBIC ACID, MALIC ACID

0.20 Active natural extract / Anti-aging, moisturization

SAKURA ExTRACT LC ORYzA OIL & FAT CORP

PROPANEDIOL, WATER, BRESENIA SCHREBERI LEAF ExTRACT

0.50 Active natural extract / Antioxidant, moisturization

WATERSHIELD ExTRACT LC ORYzA OIL & FAT CORP.

PHENOxYETHANOL, ETHYLHExYL GLYCERIN 1.00 Preservative EUxYL PE9010 SCHüLKE & MAYR

100.0

PrOCEDurE:

1 Combine part B and add part A ingredients in sequential order with thorough mixing until dissolved.

2 Add part C.


pH 4.50Stability > 1 month @ 45 °C

ASC

26-

86-1

B

31 Faciallwash

Ideas to make your life more beautifulBeauTyeNHaNCeMeNT

Transparent lipstickThis formulation has excellent transparency and imparts non sticky feeling.

PArT INGrED IENTS % W/W FuNCTION TrADE NAME / SuPPLIEr

A GELATINIZATION AGENT EB-21 2.0 Oil gelling agent AJINOMOTO CO. INC

GELATINIZATION AGENT GP-1 3.0 Oil gelling agent AJINOMOTO CO. INC

OCTYLDODECANOL 20.0 Initial solvent RISONOL 20SP / KOKYU

ALCOHOL KOGYO

B DIISOSTEARYL MALATE 17.0 Emollient HAIMALATE DIS / KOKYU

ALCOHOL KOGYO

ELDEW PS-203r 5.0 Solubilizing agent,

emollient

AJINOMOTO CO. INC

CYCLOPENTASILOxANE 2.0 Emollient SH245 FLUID / DOW

CORNING

TOCOPHEROL q.s.

PRESERVATIVE q.s.

C HYDROGENATED POLYISOBUTENE Balance PARLEAM V / NOF

D PEARLESCENT PIGMENTS q.s. Pigment REFLECKS RAYS OF RED

ENGELHARD

100.0

PrOCEDurE:

1 Dissolve part A at 110°C with stirring.

2 Add part B to part A at 95°C, and mix with stirring.

3 Add part C at 95°C, and mix with stirring.

4 Add part D at 95°C, and mix with stirring.



Stability 40°C, 25°C, 5°C for one month

eye ShadowA unique color balm formulated with an amino acid derived gelling agent, Gelatinization Agent GP-1 providing good spreadability. Thanks to Amihope LL, our functional powder, the smooth oil gel turns into powder on the skin, leaving non-oily silky soft feel.


A TRIETHYLHExANOIN 39.42 Emollient NIKKOL TRIFAT S-308 NIKKO CHEMICALS

CYCLOPENTASILOxANE 5.19 Emollient SILICONE STV-5 DOW CORNING

SILICA, METHICONE 4,67 Texturizer SI-5 SILDEx H-52 / DAITO

MICA, DEA-C8-18 PERFLUOROALKYLETHYL PHOSPHATE

1.85 Extender PF-5 MICA NO.5500 DAITO

POLYMETHYLSILSESqUIOxANE 5.93 Texturizer TOSPEARL 2000B MOMENTIVE

AMIHOPE LL 1.00 Sensory improver AJINOMOTO CO. INC

B MICA AND TITANIUM DIOxIDE AND CAMINE

12.76 Pigment COLORONA MAGENTA MERCK

MICA AND TITANIUM DIOxIDE 5.0 Pigment KC219 WENzHOU KUNCAI PEARLESCENT PIGMENT CO., LTD

C OCTYLDODECANOL*8 18.75 Emollient, solubilizer for GP-1

EUTANOL G BASF


100.0

PrOCEDurE:

1 Mix part B until uniform at room temperature.

2 Mix part A at room temperature.

3 Dissolve part C at 120°C with stirring.

4 Heat part A around 80°C.

5 Add part B to part A while heating around 80°C.

6 Add part C and continue to mix at 80°C.

7 Pour into a jar quickly.

8 Cool down to room temperature without mixing.


Stability 1, 25, 45°C, Cycle(-5, 40°C), for 1 months

35

LGS-S1

AC

AC

-ESH

-9

BB Balm with UV protectionA highly concealing foundation formulation using our pseudo-ceramide ingredient Eldew PS-203r. Amihope LL, our functional powder and our amino acid derived Gelatinization Agent GP-1 provide good spreadability, turning the smooth oil gel into powder, leaving a non-oily silky soft feel on the skin.


A TRIETHYLHExANOIN 38.92 Emollient NIKKOL TRIFAT S-308 NIKKO CHEMICALS

CYCLOPENTASILOxANE 5.20 Emollient SILICONE STV-5 DOW CORNING

TITANIUM DIOxIDE 7.42 UV filter TTO-D2 ISHIHARA SANGYO

SILICA, METHICONE 4.67 Texturizer SI-5 SILDEx H-52 DAITO KASEI

MICA, DEA-C8-18 PERFLUOROALKYLETHYL PHOSPHATE

1.85 Extender PF-5 MICA NO.5500 DAITO KASEI

POLYMETHYLSILSESqUIOxANE 5.93 Texturizer TOSPEARL 2000B MOMENTIVE

AMIHOPE LL 1.00 Sensory improver AJINOMOTO CO. INC

ELDEW PS-203r 0.50 Pseudo-ceramide AJINOMOTO CO. INC

B PIGMENT DISPERSION (WHITE) 10.72 Pigment DIDW 50 DF/KOBO

PIGMENT DISPERSION (YELLOW) 1.03 Pigment DIDW 45 DYF/KOBO

PIGMENT DISPERSION (RED) 0.33 Pigment DIDW 40 DRF/KOBO

PIGMENT DISPERSION (BLACK) 0.17 Pigment DIDW 55 DBF/KOBO

C OCTYLDODECANOL 18.75 Solubilizer for GP-1 EUTANOL G/BASF


100.0

PrOCEDurE:

1 Mix part B until uniform at room temperature.

2 Mix part A at room temperature.

3 Dissolve part C at 120°C with stirring.

4 Heat part A around 80 - 90°C.

5 Add part B to part A while heating around 80-90°C.

6 Add part C to mixer and mix at 80°C.

7 Pour into a jar quickly. Cool down to room temperature without mixing.


Stability 1, 25, 45°C, Cycle(-5 n 40°C), for 3 months

Solid Fragrance Clear Gel This transparent solid fragrance has both an enticing scent and appearance. A hard gel is produced by using low molecular weight amino acid-derived Gelatinization Agent GP-1 and EB-21 which, combined, form a network in the chosen oils. The resulting clear solid gel traps the fragrance and releases it upon contact with the skin. Eldew SL-205 and Eldew PS-203r are used to improve stability and moisturizing properties of the formulation.


A GELATINIZATION AGENT GP-1 2.4 Oil gelling agent AJINOMOTO CO. INC

GELATINIZATION AGENT EB-21 1.6 Oil gelling agent AJINOMOTO CO. INC

OCTYLDODECANOL 16.0 Initial solvent RISONOL 20SP / KOKYU ALCOHOL KOGYO CO., LTD.

B HYDROGENATED POLYISOBUTENE

5.00 High viscosity oil PANALANE H300E LIPO CHEMICALS, INC

HYDROGENATED POLYISOBUTENE

9.00 Low viscosity oil PANALANE L14 E LIPO CHEMICALS, INC

ELDEW SL-205 10.00 Light ester Moisturization

AJINOMOTO CO. INC

DIISOSTEARYL MALATE 9.00 High MW ester, stability Moisturization

SCHERCEMOL DISM ESTER LUBRIzOL - NOVEON

C12-15 ALKYL BENzOATE 11.00 Light emollient, clarity improvement Moisturization

LIPONATE NEB LIPO CHEMICALS, INC

C ISOSTEARYL ISOSTEARATE 10.00 Light ester, fragrance incorporation

SCHERCEMOL 1818 ESTER LUBRIzOL - NOVEON

ELDEW PS-203r 7.00 Stabilizing agent, emollient

AJINOMOTO CO. INC

FRAGRANCE 10.00 Scent CHERRY BLOSSOM FRAGRANCE / FIRMINECH

FRAGRANCE 2.00 Scent GINGER FRAGRANCE / BELL

CLEMENTINE ESSENTIAL OIL 2.00 Scent CLEMENTINE CO2 ESSENTIAL OIL

100.0

PrOCEDurE:1 Heat part A to 115°C, mix until fully dissolved, cool to 85°C and add to the

heated to 85°C part B, mix thoroughly while maintaining temperature. 2 Upon cooling to 80°C, slowly add mixed part C.

3 Maintain temperature at 75°C and pour into molds, then let cool to room temperature.


Appearance Transparent fragrant gelSolidification point ~ 70°CStability > 4 months at 45, 40, 25, and 3°C

37

AC

AC

-BB-08ASC

21-

43-1

“Natural” Skin Care § CreamAn Oil in Water emulsion for a night cream concept using natural ingredients. Amisoft HS-11 P improves emulsion sta-bility while Eldew PS-203r is used as a damage prevention or damage care compound. Additionally Prodew P-DS-12 imparts good nourishing properties.


A SqUALANE 5.00 Emolient

SIMMONDSIA CHINENSIS (JOJOBA) SEED OIL 5.00 Emolient

MACADAMIA TERNIFOLIA SEED OIL 5.00 Emolient

CAPRYLIC / CAPRIC TRIGLYCERIDE 5.00 Emolient TCG-M/ KOKYU ALCOHOL

KOGYO

ELDEW PS-203r 1.00 Emolient AJINOMOTO CO. INC

ISOSTEARYL HYDROxYSTEARATE 2.00 Emolient SCHERCEMOL SHS ESTER

LUBRIzOL

BUTYROSPERMUM PARKII (SHEA BUTTER) 2.00 Emolient

STEARYL ALCOHOL 3.80 Emulsion stabilizer KALCOL 8688 / KAO

COPERNICIA CFRIFERA (CARNAUBA) WAx 0.10 Viscosity modifier

GLYCERYL STEARATE 2.90 Emulsifier NIKKOL MGS-BV2

NIKKO CHEMICALS

B xANTHAN GUM 0.20 Emulsion stabilizer KELTROL CG T / CP KELCO

PROPANEDIOL 5.00 Moisturizer zEMEA PROPAEDIOL

DUPONT TATE&LYLE

BIOPRODUCTS

WATER Balance

C SUCROSE PALMITATE 0.40 Co-emulsifier SURFHOPE SE COSME

C-1615 / MITSUBISHI

KAGAKU FOODS

AMISOFT HS-11P 0.20 Co-emulsifier AJINOMOTO CO. INC

D SODIUM CITRATE 0.20 pH Adjuster

CITRIC ACID (20% AW.) q.s. pH Adjuster

E PrODEW P-DS-12 (30%) 1.67 Moisturizer AJINOMOTO CO. INC

WATER 5.0

F FRAGRANCE q.s.

100.0

PrOCEDurE:

1 Aqueous phase preparation: thoroughly disperse part B at room temperature.

2 Add part C and part D (The level of citric acid is presented as a rough guide) to part B, dissolve at 85°C.

3 Oil phase preparation: mix part A well at 85°C.

4 Add the aqueous phase to the oil phase with stirring by homogenizer at 85°C.(3000rpm/3min.)

5 Cool down to 40°C with stirring by a mechanical stirrer (50rpm).

6 Add part E and part F with stirring by a mechanical stirrer (100rpm).

7 Cool down to room temperature with stirring by a mechanical stirrer (50rpm).


pH 4.8Viscosity 15,000 ~ 25,000 mPa.s (B type, Rotor No.4, 12rpm, 30sec., 25°C)Stability 0, 25, 45°C, Cycle, for 1 month

39

ECJ-C

P-2ECJ-

CP-

2

39

PrODuCT CATEGOry

PrODuCTFOrMuLATION rEF.

APPLICATION PAGE

ANIONIC SURFACTANT

Amisoft CS-22 NSAI-zN02Transparent hair shampoo for oily hair

22

Amisoft ECS-22 SB

ASC 26-119-1 “Diverse” cleansing wipes 7

KNS-097E-4 Foaming shower cream 10

ACAC-BSB-21 Clear body wash 20

ASC 27-15-3Sulfate free “natural” shampoo

21

HAN-zN02 Transparent hand soap 24

ACAC-FSB-6 Clear facial wash gel 27

Amisoft MS-11PWT-310 Facial wash powder 8

TSIL-P-3-MS Toothpaste 9

Amisoft LS-11 PWT-310 Facial wash powder 8

Amisoft HS-11 P ECJ-CP-2 “Natural” skin care cream 38

Amilite ACS-12 KNS-097E-4 Foaming shower cream 10

Amilite GCS-12 K

CCS-112 Transparent hair shampoo 13

SKPEG-112 Facial cream cleanser 14

FC-109H Facial wash cream 15

DMS-14S-5 Foaming make up remover 16

ACAC-PNS-4 Body wash cream 17

Amilite ET-CS-12 CG-zN19 Transparent hair shampoo 23

AMPHOTERIC SURFACTANT

Amisafe AL-01DMS-14S-5 Foaming make up remover 16

NSAI-zN02Transparent hair shampoo for oily hair

22

PrODuCT CATEGOry

PrODuCTFOrMuLATION rEF.

APPLICATION PAGE

HUMECTANT

Ajidew NL-50

ASC 26-119-1 “Diverse” cleansing wipes 7

CCS-112 Transparent hair shampoo 13

ACAC-BSB-21 Clear body wash 20

ASC 27-15-3 Sulfate free “natural” shampoo 21

CG-zN19 Transparent hair shampoo 23


ACAC-FSB-6 Clear facial wash gel 27

NTON-CP3 “Natural” facial skin toner 28

Ajidew zN-100

ASC 26-94-3 Facial wipes for oily skin 6

NSAI-zN02 Transparent hair shampoo for oily hair 22

CG-zN19 Transparent hair shampoo 23


ASC 26-86-1B Humectant-rich anti aging toner 30

Prodew 500ASC 27-15-3 Sulfate free “natural”

shampoo 21

ASC 26-86-1B Humectant-rich anti aging toner 30

Prodew P-DS-12

NTON-CP3 “Natural” facial skin toner 28

SSPB-CP-2 Facial skin toner 29

ECJ-CP-2 “Natural” skin care cream 38

EMOLLIENTEldew PS-203 R

SSPB-CP-2 Facial skin toner 29

LGS-S1 Transparent lipstick 35

ASC 21-43-1 Solid Fragrance Clear Gel 36

ACAC-BB-08 BB balm 37

ECJ-CP-2 “Natural” skin care cream 38

Eldew SL-205 ASC 21-43-1 Solid Fragrance Clear Gel 36

FUNCTIONAL POWDER

Amihope LL

PWT-310 Facial wash powder 8

ACAC-ESH-9 Eye Shadow 34


GELLING AGENT

GP-1

ACAC-ESH-9 Eye shadow 34

LGS-S1 Transparent lipstick 35



EB-21LGS-S1 Transparent lipstick 35


Formulation Finder

Notes

Contact

DisclaimerThis information is presented in good faith and we believe that it is correct, but no warranty as to accuracy of results or fitness for particular use is given, not is freedom from patent infringement to be inferred. It is offered solely for information.Before using any Ajinomoto product, or any product mentioned in this literature: read, understand and follow the information contained in the most recent Material Safety Data Sheet.

S.A. Ajinomoto OmniChem N.V.

Industrial Research Park Fleming B-1348 Louvain-la-Neuve

Belgium

Phone : +32 10 48 32 22Fax: +32 10 45 06 93

[email protected]

43

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