longhornaap.comlonghornaap.com/system/assets/adminrecord/2018/2018... · 2019. 6. 20. · form 2 -...
TRANSCRIPT
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LONGHORN ARMY AMMUNITION PLANT
KARNACK, TEXAS
ADMINISTRATIVE RECORD
Volume 48
2018
Bate Stamp Numbers 00909876 – 00911340
Prepared for
Department of the Army Longhorn Army Ammunition Plant
1976 – 2018
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LONGHORN ARMY AMMUNITION PLANT KARNACK, TEXAS
ADMINISTRATIVE RECORD – CHRONOLOGICAL INDEX
VOLUME 48 2018 A. Title: Report (cont’d) – Draft Final Fourth Annual Remedial Action Operation Report, LHAAP-50 Former Sump Water Tank, Lab Data, Longhorn Army Ammunition Plant, Karnack, Texas, December 2018 Author(s): Department of the Army
Recipient: Environmental Protection Agency Date: December 5, 2018
Bate Stamp: 00909876 – 00910711 B. Title: Public Meeting – Transcript of December 6, 2018 Public Meeting for LHAAP-29 Final Revised Proposed Plan, Longhorn Army Ammunition Plant, Karnack, Texas, December 2018 Author(s): U.S. Army
Recipient: Public Date: December 6, 2018 Bate Stamp: 00910712 – 00910732
C. Title: Minutes – Final Minutes, Monthly Managers' Meeting (MMM), Longhorn Army Ammunition Plant (LHAAP), November 15, 2018 Author(s): Department of the Army
Recipient: All Parties Date: December 13, 2018 Bate Stamp: 00910733 – 00910754
D. Title: Report – Draft Final Fourth Annual Remedial Action Operation Report, LHAAP-67 (Above Ground Storage Tank Farm), Longhorn Army Ammunition Plant, Karnack, Texas, December 2018 Author(s): Department of the Army
Recipient: Environmental Protection Agency Date: December 18, 2018 Bate Stamp: 00910755 – 00910930
E. Title: Report – Draft Final Fourth Annual Remedial Action Operation Report, LHAAP-67 (Above Ground Storage Tank Farm), Lab Data, Longhorn Army Ammunition Plant (LHAAP), December 2018 Author(s): Department of the Army
Recipient: Environmental Protection Agency Date: December 18, 2018 Bate Stamp: 00910931 – 00911340
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Metals Raw Data
Aptim Environmental & Infrastucture, Inc. Project: Longhorn Army Ammunition Plant
ALS WO# HS17110741
147 of 828
00909936
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Form 2 - Initial and Continuing Calibration Verification
HS17110741Longhorn Army Ammunition Plant Aptim Environmental & Infrastucture, Inc.
WorkOrder:Project:Client:
ICPMS05Instrument:Method: SW6020
Run ID: ICPMS05_305808
Analyte Found
Seq: 4318338ICV ICV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 09:56
Iron 10000 9224.699 92 90-110
Analyte Found
Seq: 4318401CCV1 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 10:18
Iron 10000 9917.393 99 90-110
Analyte Found
Seq: 4318415CCV2 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 10:47
Iron 10000 9579.08 96 90-110
Analyte Found
Seq: 4319164CCV3 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 11:07
Iron 10000 9789.292 98 90-110
Analyte Found
Seq: 4319181CCV4 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 11:31
Iron 10000 9648.514 97 90-110
Analyte Found
Seq: 4319210CCV5 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 12:02
Iron 10000 9725.55 97 90-110
Analyte Found
Seq: 4319229CCV6 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 12:23
Iron 10000 10051.694 101 90-110
Analyte Found
Seq: 4319241CCV7 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 12:47
Iron 10000 9760.49 98 90-110
Analyte Found
Seq: 4319673CCV8 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 13:09
Iron 10000 9976.173 100 90-110
Analyte Found
Seq: 4319280CCV9 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 13:33
Iron 10000 9785.242 98 90-110
Analyte Found
Seq: 4319292CCV10 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 13:58
Iron 10000 9856.469 99 90-110
Analyte Found
Seq: 4319374CCV11 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 14:22
Iron 10000 9908.065 99 90-110
Analyte Found
Seq: 4319386CCV12 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 14:46
Iron 10000 9844.218 98 90-110
Analyte Found
Seq: 4319540CCV13 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 15:10
Iron 10000 9982.962 100 90-110
Analyte Found
Seq: 4319692CCV14 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 15:35
Iron 10000 10089.722 101 90-110
01-Dec-17Date: ALS Group USA, Corp
148 of 828
00909937
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Form 2 - Initial and Continuing Calibration Verification
HS17110741Longhorn Army Ammunition Plant Aptim Environmental & Infrastucture, Inc.
WorkOrder:Project:Client:
ICPMS05Instrument:Method: SW6020
Run ID: ICPMS05_305808
Analyte Found
Seq: 4320409CCV15 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 15:59
Iron 10000 9874.634 99 90-110
Analyte Found
Seq: 4320577CCV16 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 16:23
Iron 10000 9879.277 99 90-110
Analyte Found
Seq: 4320589CCV17 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 16:48
Iron 10000 9778.145 98 90-110
Analyte Found
Seq: 4320445CCV18 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 17:12
Iron 10000 9548.464 96 90-110
Analyte Found
Seq: 4320471CCV19 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 18:05
Iron 10000 9960.165 100 90-110
Analyte Found
Seq: 4320483CCV20 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 18:29
Iron 10000 9492.895 95 90-110
Analyte Found
Seq: 4320495CCV21 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 18:53
Iron 10000 9637.185 96 90-110
Analyte Found
Seq: 4320507CCV22 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 19:17
Iron 10000 9694.474 97 90-110
Analyte Found
Seq: 4320519CCV23 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 19:41
Iron 10000 9540.444 95 90-110
Analyte Found
Seq: 4320526CCV24 CCV Units: ug/L
True %R Control Limits Flag
Date: 21-Nov-2017 19:55
Iron 10000 9629.624 96 90-110
01-Dec-17Date: ALS Group USA, Corp
149 of 828
00909938
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ICPMS05_305808Run ID:
Form 3 - BLANKS
SW6020Method:Instrument: ICPMS05
Client:Project:WorkOrder:
Aptim Environmental & Infrastucture, Inc.Longhorn Army Ammunition Plant HS17110741
Analyte Result Qual
Seq: 4318341ICB 21-Nov-2017 10:02 ICB Units: ug/L
Report LimitMDL
Date:
Iron U20012200
Analyte Result Qual
Seq: 4318402CCB1 21-Nov-2017 10:20 CCB Units: ug/L
Report LimitMDL
Date:
Iron U20012200
Analyte Result Qual
Seq: 4318413CCB2 21-Nov-2017 10:42 CCB Units: ug/L
Report LimitMDL
Date:
Iron U20012200
Analyte Result Qual
Seq: 4319165CCB3 21-Nov-2017 11:09 CCB Units: ug/L
Report LimitMDL
Date:
Iron U20012200
Analyte Result Qual
Seq: 4319182CCB4 21-Nov-2017 11:33 CCB Units: ug/L
Report LimitMDL
Date:
Iron U20012200
Analyte Result Qual
Seq: 4319208CCB5 21-Nov-2017 11:57 CCB Units: ug/L
Report LimitMDL
Date:
Iron U20012200
Analyte Result Qual
Seq: 4319230CCB6 21-Nov-2017 12:25 CCB Units: ug/L
Report LimitMDL
Date:
Iron U20012200
Analyte Result Qual
Seq: 4319242CCB7 21-Nov-2017 12:49 CCB Units: ug/L
Report LimitMDL
Date:
Iron U20012200
Analyte Result Qual
Seq: 4319674CCB8 21-Nov-2017 13:11 CCB Units: ug/L
Report LimitMDL
Date:
Iron U20012200
Analyte Result Qual
Seq: 4319281CCB9 21-Nov-2017 13:35 CCB Units: ug/L
Report LimitMDL
Date:
Iron U20012200
Analyte Result Qual
Seq: 4319293CCB10 21-Nov-2017 14:00 CCB Units: ug/L
Report LimitMDL
Date:
Iron U20012200
Analyte Result Qual
Seq: 4319375CCB11 21-Nov-2017 14:24 CCB Units: ug/L
Report LimitMDL
Date:
Iron U20012200
Analyte Result Qual
Seq: 4319387CCB12 21-Nov-2017 14:48 CCB Units: ug/L
Report LimitMDL
Date:
Iron U20012200
Analyte Result Qual
Seq: 4319541CCB13 21-Nov-2017 15:12 CCB Units: ug/L
Report LimitMDL
Date:
Iron U20012200
Analyte Result Qual
Seq: 4319693CCB14 21-Nov-2017 15:37 CCB Units: ug/L
Report LimitMDL
Date:
Iron U20012200
01-Dec-17Date: ALS Group USA, Corp
150 of 828
00909939
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ICPMS05_305808Run ID:
Form 3 - BLANKS
SW6020Method:Instrument: ICPMS05
Client:Project:WorkOrder:
Aptim Environmental & Infrastucture, Inc.Longhorn Army Ammunition Plant HS17110741
Analyte Result Qual
Seq: 4320410CCB15 21-Nov-2017 16:01 CCB Units: ug/L
Report LimitMDL
Date:
Iron U20012200
Analyte Result Qual
Seq: 4320575MBLK-122338 21-Nov-2017 16:19 MBLK Units: ug/L
Report LimitMDL
Date:
Iron U20012200
Analyte Result Qual
Seq: 4320578CCB16 21-Nov-2017 16:25 CCB Units: ug/L
Report LimitMDL
Date:
Iron U20012200
Analyte Result Qual
Seq: 4320590CCB17 21-Nov-2017 16:50 CCB Units: ug/L
Report LimitMDL
Date:
Iron U20012200
Analyte Result Qual
Seq: 4320446CCB18 21-Nov-2017 17:14 CCB Units: ug/L
Report LimitMDL
Date:
Iron U20012200
Analyte Result Qual
Seq: 4320472CCB19 21-Nov-2017 18:07 CCB Units: ug/L
Report LimitMDL
Date:
Iron J2001226.03
Analyte Result Qual
Seq: 4320484CCB20 21-Nov-2017 18:31 CCB Units: ug/L
Report LimitMDL
Date:
Iron J2001227.25
Analyte Result Qual
Seq: 4320496CCB21 21-Nov-2017 18:55 CCB Units: ug/L
Report LimitMDL
Date:
Iron J2001219.16
Analyte Result Qual
Seq: 4320508CCB22 21-Nov-2017 19:19 CCB Units: ug/L
Report LimitMDL
Date:
Iron J2001232.71
Analyte Result Qual
Seq: 4320520CCB23 21-Nov-2017 19:43 CCB Units: ug/L
Report LimitMDL
Date:
Iron J2001233.44
Analyte Result Qual
Seq: 4320527CCB24 21-Nov-2017 19:57 CCB Units: ug/L
Report LimitMDL
Date:
Iron J2001218.3
01-Dec-17Date: ALS Group USA, Corp
151 of 828
00909940
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Form 4 - ICP Interference Check Sample
HS17110741Longhorn Army Ammunition Plant Aptim Environmental & Infrastucture, Inc.
WorkOrder:Project:Client:
ICPMS05Instrument:Method:SW6020
Run ID:ICPMS05_305808
Analyte Found
ICSA
True %R
Date: 21-Nov-2017 10:04 Units: ug/LICSASeq: 4318342
Iron 100000 96520 96.5
Analyte Found
ICSAB
True %R
Date: 21-Nov-2017 10:06 Units: ug/LICSABSeq: 4318343
Iron 110000 106200 96.5
Analyte Found
ICSA
True %R
Date: 21-Nov-2017 20:03 Units: ug/LICSASeq: 4320530
Iron 100000 93330 93.3
Analyte Found
ICSAB
True %R
Date: 21-Nov-2017 20:05 Units: ug/LICSABSeq: 4320531
Iron 110000 105300 95.8
01-Dec-17Date: ALS Group USA, Corp
152 of 828
00909941
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Form 5A - Matrix Spike/Matrix Spike Duplicate Recovery
HS17110741Longhorn Army Ammunition Plant Aptim Environmental & Infrastucture, Inc.
WorkOrder:Project:Client: Date Analyzed: 21-Nov-2017 16:42
20-Nov-2017 09:34Date Extracted:ug/LUnits:
Matrix Spike: HS17110677-07MSClient Sample ID:
% Rec Limits
RPD Limit
MSD Result
Spike Amount % Rec% Rec
Spike Amount
MS Result
Sample Result RPDAnalyte
Analysis Method: SW6020
Iron 200.0 4221 5000 84.3 4315 5000 86.2 80-120 2.22 20Manganese 37.08 78.67 50.00 83.2 81.56 50.00 89.0 80-120 3.61 20
01-Dec-17Date: ALS Group USA, Corp
153 of 828
00909942
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Form 5B - Post Digest Sample Recovery
HS17110741Longhorn Army Ammunition Plant Aptim Environmental & Infrastucture, Inc.
WorkOrder:Project:Client: Date Analyzed: 21-Nov-2017 16:44
20-Nov-2017 09:34Date Extracted:ug/LUnits:
Lab Sample ID: HS17110677-07PDSClient Sample ID:
% Rec Limits% Rec
Spike Amount
PDS Result
Sample ResultAnalyte
Analysis Method: SW6020
Iron 0 8457 10000 85 75-125Manganese 37.08 122.5 100 85 75-125
01-Dec-17Date: ALS Group USA, Corp
154 of 828
00909943
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Form 7 - Laboratory Control Sample
HS17110741Longhorn Army Ammunition Plant Aptim Environmental & Infrastucture, Inc.
WorkOrder:Project:Client: Date Analyzed: 21-Nov-2017 16:21
20-Nov-2017 09:34Date Extracted:ug/LUnits:
Lab Sample ID: LCS-122338
% Rec Limits% Rec
Spike Amount
LCS ResultAnalyte
Analysis Method: SW6020
Iron 4491 90 80-1205000Manganese 44.71 89 80-12050
01-Dec-17Date: ALS Group USA, Corp
155 of 828
00909944
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Form 8 - ICP Serial Dilutions
HS17110741Longhorn Army Ammunition Plant Aptim Environmental & Infrastucture, Inc.
WorkOrder:Project:Client: Date Analyzed: 21-Nov-2017 16:37
20-Nov-2017 09:34Date Extracted:ug/LUnits:
Lab Sample ID: HS17110677-07SDClient Sample ID:
SD ResultSample Result RPDAnalyte
Analysis Method: SW6020
C C QIron 0 0 0U UManganese 37.08 38.74 4
01-Dec-17Date: ALS Group USA, Corp
156 of 828
00909945
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Form 11 - INTERNAL STANDARD ASSOCIATION
Instrument:ICPMS05
HS17110741Longhorn Army Ammunition Plant Aptim Environmental & Infrastucture, Inc.
WorkOrder:Project:Client:
AnalyteMass Assoc Int Standard 1 Assoc Int Standard 2 Mode
9 Beryllium Lithium Ar9 Beryllium Lithium Ar
11 Boron Lithium Ar11 Boron Lithium Ar23 Sodium Germanium Ar23 Sodium Germanium Ar24 Magnesium Germanium Ar24 Magnesium Germanium Ar27 Aluminum Germanium Ar27 Aluminum Germanium Ar39 Potassium Germanium Ar39 Potassium Germanium Ar44 Calcium Germanium Ar44 Calcium Germanium Ar47 Titanium Germanium Ar47 Titanium Germanium Ar51 Vanadium Germanium ArHe51 Vanadium Germanium ArHe52 Chromium Germanium ArHe52 Chromium Germanium ArHe55 Manganese Germanium ArHe55 Manganese Germanium ArHe56 Iron Germanium ArHe56 Iron Germanium ArHe59 Cobalt Germanium ArHe59 Cobalt Germanium ArHe60 Nickel Germanium ArHe60 Nickel Germanium ArHe63 Copper Germanium ArHe63 Copper Germanium ArHe66 Zinc Germanium ArHe66 Zinc Germanium ArHe75 Arsenic Germanium ArHe75 Arsenic Germanium ArHe78 Selenium Germanium ArHe78 Selenium Germanium ArHe88 Strontium Germanium Ar88 Strontium Germanium Ar95 Molybdenum Germanium Ar95 Molybdenum Germanium Ar
105 Palladium Germanium Ar105 Palladium Germanium Ar107 Silver Germanium Ar107 Silver Germanium Ar114 Cadmium Indium Ar114 Cadmium Indium Ar118 Tin Germanium Ar118 Tin Germanium Ar121 Antimony Germanium ArHe121 Antimony Germanium ArHe137 Barium Indium Ar137 Barium Indium Ar205 Thallium Bismuth Ar205 Thallium Bismuth Ar208 Lead Bismuth Ar208 Lead Bismuth Ar
01-Dec-17Date: ALS Group USA, Corp
157 of 828
00909946
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FORM 12 - PREPARATION LOG
Batch ID:Prep Code:
End Date:Start Date: Technician:Method:
122338
SW3010A20-Nov-2017 12:00 20-Nov-2017 16:30
3010AClient:Project:WorkOrder:
Aptim Environmental & Infrastucture, Inc.Longhorn Army Ammunition Plant HS17110741
PrepFacFinalVol(mL)Init VolMatrixSampID Init WtClientID
HS17110677-07MS 10 10 1HS17110677-07MSD 10 10 1HS17110677-07PDS 10 10 1HS17110677-07SD 10 10 1HS17110741-02 Groundwater 10 10 150WW23-111417HS17110741-03 Groundwater 10 10 150WW12-111417HS17110741-04 Groundwater 10 10 150WW16-111417LCS-122338 10 10 1MBLK-122338 10 10 1
01-Dec-17Date: ALS Group USA, Corp
158 of 828
00909947
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ICPMS05_305808Run ID:
FORM 13 - ANALYSIS RUN LOG
Method: Instrument:
Sample No. D/F Time Analytes
HS17110741Longhorn Army Ammunition Plant Aptim Environmental & Infrastucture, Inc.
WorkOrder:Project:Client:
ICPMS05
Start Date: End Date:21-Nov-2017 21-Nov-2017
FileIDICPMS05_305808_Tune 1 21-Nov-2017 00:00 ICPMS05_305808_Tune_1CAL BLK 1 21-Nov-2017 09:42 004CALB.d_4318331 FE2/10/200 1 21-Nov-2017 09:44 005CALS.d_4318332 FE5/25/500 1 21-Nov-2017 09:46 006CALS.d_4318333 FE10/50/1000 1 21-Nov-2017 09:48 007CALS.d_4318334 FE100/500/10K 1 21-Nov-2017 09:50 008CALS.d_4318335 FE200/1000/20K 1 21-Nov-2017 09:52 009CALS.d_4318336 FEICV 1 21-Nov-2017 09:56 011_ICV.d_4318338 FELLICV2 1 21-Nov-2017 09:58 012SMPL.d_4318339 FELLICV5 1 21-Nov-2017 10:00 013LICV.d_4318340 FEICB 1 21-Nov-2017 10:02 014_ICB.d_4318341 FEICSA 1 21-Nov-2017 10:04 015ICSA.d_4318342 FEICSAB 1 21-Nov-2017 10:06 016ICSB.d_4318343 FECCV 1 1 21-Nov-2017 10:18 022_CCV.d_4318401 FECCB 1 1 21-Nov-2017 10:20 023_CCB.d_4318402 FECCB 2 1 21-Nov-2017 10:42 034_CCB.d_4318413 FECCV 2 1 21-Nov-2017 10:47 036_CCV.d_4318415 FECCV 3 1 21-Nov-2017 11:07 046_CCV.d_4319164 FECCB 3 1 21-Nov-2017 11:09 047_CCB.d_4319165 FECCV 4 1 21-Nov-2017 11:31 058_CCV.d_4319181 FECCB 4 1 21-Nov-2017 11:33 059_CCB.d_4319182 FECCB 5 1 21-Nov-2017 11:57 071_CCB.d_4319208 FECCV 5 1 21-Nov-2017 12:02 073_CCV.d_4319210 FECCV 6 1 21-Nov-2017 12:23 083_CCV.d_4319229 FECCB 6 1 21-Nov-2017 12:25 084_CCB.d_4319230 FECCV 7 1 21-Nov-2017 12:47 095_CCV.d_4319241 FECCB 7 1 21-Nov-2017 12:49 096_CCB.d_4319242 FECCV 8 1 21-Nov-2017 13:09 106_CCV.d_4319673 FECCB 8 1 21-Nov-2017 13:11 107_CCB.d_4319674 FECCV 9 1 21-Nov-2017 13:33 118_CCV.d_4319280 FECCB 9 1 21-Nov-2017 13:35 119_CCB.d_4319281 FECCV 10 1 21-Nov-2017 13:58 130_CCV.d_4319292 FECCB 10 1 21-Nov-2017 14:00 131_CCB.d_4319293 FECCV 11 1 21-Nov-2017 14:22 142_CCV.d_4319374 FECCB 11 1 21-Nov-2017 14:24 143_CCB.d_4319375 FECCV 12 1 21-Nov-2017 14:46 154_CCV.d_4319386 FECCB 12 1 21-Nov-2017 14:48 155_CCB.d_4319387 FECCV 13 1 21-Nov-2017 15:10 166_CCV.d_4319540 FECCB 13 1 21-Nov-2017 15:12 167_CCB.d_4319541 FECCV 14 1 21-Nov-2017 15:35 178_CCV.d_4319692 FECCB 14 1 21-Nov-2017 15:37 179_CCB.d_4319693 FECCV 15 1 21-Nov-2017 15:59 190_CCV.d_4320409 FECCB 15 1 21-Nov-2017 16:01 191_CCB.d_4320410 FEMBLK-122338 1 21-Nov-2017 16:19 200SMPL.d_4320575 FELCS-122338 1 21-Nov-2017 16:21 201SMPL.d_4320576 FECCV 16 1 21-Nov-2017 16:23 202_CCV.d_4320577 FECCB 16 1 21-Nov-2017 16:25 203_CCB.d_4320578 FEZZZZZZSD 5 21-Nov-2017 16:37 209SMPL.d_4320584 FEZZZZZZMS 1 21-Nov-2017 16:39 210SMPL.d_4320585 FEZZZZZZMSD 1 21-Nov-2017 16:42 211SMPL.d_4320586 FEZZZZZZPDS 1 21-Nov-2017 16:44 212SMPL.d_4320587 FECCV 17 1 21-Nov-2017 16:48 214_CCV.d_4320589 FECCB 17 1 21-Nov-2017 16:50 215_CCB.d_4320590 FE50WW23-111417 1 21-Nov-2017 17:04 222SMPL.d_4320597 FE
01-Dec-17Date: ALS Group USA, Corp
159 of 828
00909948
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ICPMS05_305808Run ID:
FORM 13 - ANALYSIS RUN LOG
Method: Instrument:
Sample No. D/F Time Analytes
HS17110741Longhorn Army Ammunition Plant Aptim Environmental & Infrastucture, Inc.
WorkOrder:Project:Client:
ICPMS05
Start Date: End Date:21-Nov-2017 21-Nov-2017
FileID50WW12-111417 1 21-Nov-2017 17:06 223SMPL.d_4320598 FE50WW16-111417 1 21-Nov-2017 17:08 224SMPL.d_4320599 FECCV 18 1 21-Nov-2017 17:12 226_CCV.d_4320445 FECCB 18 1 21-Nov-2017 17:14 227_CCB.d_4320446 FECCV 19 1 21-Nov-2017 18:05 238_CCV.d_4320471 FECCB 19 1 21-Nov-2017 18:07 239_CCB.d_4320472 FECCV 20 1 21-Nov-2017 18:29 250_CCV.d_4320483 FECCB 20 1 21-Nov-2017 18:31 251_CCB.d_4320484 FECCV 21 1 21-Nov-2017 18:53 262_CCV.d_4320495 FECCB 21 1 21-Nov-2017 18:55 263_CCB.d_4320496 FECCV 22 1 21-Nov-2017 19:17 274_CCV.d_4320507 FECCB 22 1 21-Nov-2017 19:19 275_CCB.d_4320508 FECCV 23 1 21-Nov-2017 19:41 286_CCV.d_4320519 FECCB 23 1 21-Nov-2017 19:43 287_CCB.d_4320520 FECCV 24 1 21-Nov-2017 19:55 293_CCV.d_4320526 FECCB 24 1 21-Nov-2017 19:57 294_CCB.d_4320527 FELLCCV5 1 21-Nov-2017 19:59 295LICV.d_4320528 FELLCCV2 1 21-Nov-2017 20:01 296SMPL.d_4320529 FEICSA 1 21-Nov-2017 20:03 297ICSA.d_4320530 FEICSAB 1 21-Nov-2017 20:05 298ICSB.d_4320531 FE
01-Dec-17Date: ALS Group USA, Corp
160 of 828
00909949
-
Tune Report
Resp Ratio
(Flag)
Resp Ratio
(Actual)
NaN
NaN
NaN
Resp Ratio
(Required)
-
-
-
Response
(Required)
[cps/ug/l]
Response
(Flag)
Count
(Actual)
59
468
8793
Response
(Actual)
[cps/ug/l]
Mass
9
24
59
Range
V
[He]
Energy Discrimination 5.00.0
0.0
0
mL/min
mL/min
%
V
V
He Flow
H2 Flow
3rd Gas Flow
OctP Bias
OctP RF
Use Gas
-8.0
190
true
V
V
## Cell Parameters ##
Deflect
Plate Bias
15.6
-50
8.0
-38
-58
V
V
V
V
V
V
Omega Lens
Cell Entrance
Cell Exit
Extract 1
Extract 2
Omega Bias
0.0
-200.0
-100
℃
L/min
## Lenses Parameters ##
S/C Temp
Makeup/Dilution Gas
Gas Switch
2
0.50
Dilution Gas
0.0
0.10
L/min
%
rps
V
mm
Carrier Gas
Option Gas
Nebulizer Pump
RF Matching
Smpl Depth
1600
1.70
8.0
Y Axis Linear
Tune Parameters
## Plasma Paramters ##
RF Power W 0.35
X = 5 Integration Time [sec] 0.1 Acquisition Time [sec] 168.5
W-X%
(Flag)
W-X%
(Required)
0.750
0.750
0.750
0.750
0.750
W-X%
(Actual)
0.479
0.466
0.442
0.443
0.515
W-50%
0.37
0.37
0.35
0.32
0.33
Axis
(Flag)
115.00
208.00
Axis
(Required)
8.9 - 9.1
23.9 - 24.1
58.9 - 59.1
114.9 - 115.1
207.9 - 208.1
115
208
Peak
Height
1570.24
5733.70
9820.59
13035.51
8531.48
Integration Time [sec] 0.1
Mass
9
24
59
Axis
(Actual)
8.95
23.95
58.95
28759
Replicate 5
Count
5790
21042
33885
42298
28885
Replicate 4
Count
5772
20553
33802
42150
28861
Replicate 3
Count
5810
20381
33543
41553
29078
Replicate 2
Count
5447
20375
33282
41779
208
Replicate 1
Count
5512
20759
34115
41822
28672
Mass
9
24
59
115
Background
(Flag)
Background
(Required)
Background
(Actual)
RSD%
(Flag)
RSD%
(Required)
5.005.005.005.005.00
RSD%
(Actual)
3.051.370.950.720.53
Mass
92459
115208
Resp Ratio
(Flag)
Resp Ratio
(Required)
-
-
-
-
-
Resp Ratio
(Actual)
NaN
NaN
NaN
NaN
NaN
Response
(Flag)
Response
(Required)
[cps/ug/l]
Response
(Actual)
[cps/ug/l]
Count
(Actual)
5666
20622
33726
41920
28851208
RangeMass
9
24
59
115
Batch Folder C:\Agilent\ICPMH\1\DATA\112117A.b
Report Comment
Instrument Name G3281A JP11080910
[nogas]
Page 1 of 2 Generated at: 09:04 on:2017-11-21
161 of 828
00909950
-
Tune Report
VEnergy Discrimination 5.05.5
0.0
0
mL/min
mL/min
%
V
V
He Flow
H2 Flow
3rd Gas Flow
OctP Bias
OctP RF
Use Gas
-18.0
190
true
V
V
## Cell Parameters ##
Deflect
Plate Bias
2.0
-60
8.0
-32
-70
V
V
V
V
V
V
Omega Lens
Cell Entrance
Cell Exit
Extract 1
Extract 2
Omega Bias
0.0
-200.0
-100
℃
L/min
## Lenses Parameters ##
S/C Temp
Makeup/Dilution Gas
Gas Switch
2
0.50
Dilution Gas
0.0
0.10
L/min
%
rps
V
mm
Carrier Gas
Option Gas
Nebulizer Pump
RF Matching
Smpl Depth
1600
1.70
8.0
Y Axis LinearTune Parameters
## Plasma Paramters ##RF Power W 0.35
W-X%
(Flag)
X = 5 Integration Time [sec] 0.1 Acquisition Time [sec] 100.6
W-X%
(Actual)
0.492
0.459
0.438
W-X%
(Required)
0.750
0.750
0.750
Axis
(Flag)
W-50%
0.40
0.38
0.33
Axis
(Actual)
8.90
23.90
58.95
Axis
(Required)
8.9 - 9.1
23.9 - 24.1
58.9 - 59.1
Integration Time [sec] 0.1
Mass
9
24
59
Peak
Height
15.08
126.69
2666.56
57
461
9026
Replicate 5
Count
50
486
9021
56
466
8728
Replicate 3
Count
68
484
8894
9
24
59
Replicate 1
Count
64
442
8297
Background
(Flag)
Mass
Replicate 2
Count
Replicate 4
Count
Background
(Required)
5.00
5.00
RSD%
(Flag)
[F]
24
59
RSD%
(Actual)
12.15
3.82
3.44
Mass
9
RSD%
(Required)
5.00
Background
(Actual)
Page 2 of 2 Generated at: 09:04 on:2017-11-21
162 of 828
00909951
-
Calibration Blank Report
106.25
2749.55
0.01
0.00
1.30
0.00
6.82
0.07
57.58
4.30
5.04
81.35
23.62
0.01
5196.15
1.89
0.38
0.92
32.41
6.27
20.30
41.34
0.00
6.22
3.39
0.00
3.56
2.29
500.00
0.22
0.00
0.02
0.05
0.41
1.33
0.23
%RSD
549.91
0.00
0.57
0.08
0.00
15.47
3
37584
710570
887
206353
5888
63
267
470
43
26
11917
3
230
1453
1323
310
390
107
80
52209
247
117
195288
393
340
20
4697
143
33912
9302
373
743
1963
373
1696710
3634
9819
3945604
230
1684487
nogas
nogas
He
He
He
He
nogas
nogas
He
He
He
He
He
He
He
He
He
He
He
He
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
Tune Mode
nogas
nogas
nogas
nogas
1
2
2
2
1
1
1
2
2
2
2
2
2
2
2
2
2
2
2
1
1
1
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
Tune Step
1
1
1
1
1
75
78
11
28
43
44
55
56
59
60
63
66
27
39
43
44
51
52
205
208
206
207
23
24
66
75
88
107
111
121
51
52
55
59
60
63
Mass
9
23
24
27
39
47
Se
B
Si
Ca
Ca
Fe
Co
Ni
Cu
Zn
As
K
Ca
Ca
V
Cr
Mn
Pb
[Pb]
[Pb]
Na
Mg
Al
As
Sr
Ag
Cd
Sb
Tl
Cr
Mn
Co
Ni
Cu
Zn
Na
Mg
Al
K
Ti
V
Dilution 1
Comment
QC Analyte Table
Name
Be
CPS
17
Acq Date Time 2017-11-21T09:42:07-06:00
Sample Type CalBlk
Level 1
Sample Table
Sample Name CAL BLK
Data File Name 004CALB.d
Data Path Name C:\Agilent\ICPMH\1\DATA\112
Page 1 of 2 Printed at: 09:43 on:2017-11-21163 of 828
00909952
-
Calibration Blank Report
Mass Tune Step Tune Mode CPS %RSD
106835
%RSD
5.76
2.89
4.80
3.77
0.71
nogas
nogas
nogas
nogas
He
CPS
210265
1178367
1181392
1190813
72
Tune Step
1
1
1
1
2
Li
Ge
In
Bi
Ge
Mass
6
72
115
209
3.09
0.03
0.00
70.83
QC ISTD Table
Name Tune Mode
0.00
0.01
11.98
0.29
1.74
13.50
20945
71037
77
64839
317
3547
800
140
453
1054680
nogas
nogas
He
nogas
nogas
nogas
nogas
nogas
nogas
nogas
1
2
1
1
1
1
1
1
1
1
121
7
31
139
56
77
82
95
118
137
Li
P
La
Se
Se
Mo
Sn
Ba
Sb
Fe
Name
Page 2 of 2 Printed at: 09:43 on:2017-11-21164 of 828
00909953
-
Calibration Standard Report
0.02
1.95
1.57
240.56
0.00
0.00
0.04
0.15
0.53
0.00
0.02
0.60
0.00
0.00
19.75
0.01
51.90
1.00
0.19
0.01
0.01
0.01
0.03
0.01
0.13
0.05
0.07
0.00
0.01
0.03
0.00
0.82
0.00
0.01
0.01
0.01
%RSD
0.19
0.00
0.00
0.02
4724
737
450
12
46060
1108861
3468
4344
1553
250423
5584
1743
94252
20285
197
21916
63
797
3424
18604
24622
39306
9766
8522
5494
13805
4491
192946
25853
16325
5324661
1660
1640848
51208
33678
21326
CPS
3410
3415320
1217950
23182
He
He
He
He
nogas
nogas
He
He
He
He
He
He
He
He
He
He
He
He
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
Tune Mode
nogas
nogas
nogas
nogas
2
2
2
2
1
1
2
2
2
2
2
2
2
2
2
2
2
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Tune Step
1
1
1
1
63
66
75
78
11
28
51
52
55
56
59
60
23
24
27
39
43
44
111
121
205
208
206
207
60
63
66
75
88
107
39
47
51
52
55
59
Mass
9
23
24
27
Cu
Zn
As
Se
B
Si
V
Cr
Mn
Fe
Co
Ni
Na
Mg
Al
K
Ca
Ca
Cd
Sb
Tl
Pb
[Pb]
[Pb]
Ni
Cu
Zn
As
Sr
Ag
K
Ti
V
Cr
Mn
Co
QC Analyte Table
Name
Be
Na
Mg
Al
Dilution 1
Comment
ISTD Ref File Name 004CALB.d
ISTD Pass/Fail Pass
Acq Date Time 2017-11-21T09:44:07-06:00
Sample Type CalStd
Level 2
Sample Table
Sample Name 2/10/200
Data File Name 005CALS.d
Data Path Name C:\Agilent\ICPMH\1\DATA\112
Page 1 of 2 Printed at: 09:45 on:2017-11-21165 of 828
00909954
-
Calibration Standard Report
QC Flag%QC High
125
125
125
125
125
%QC Low
70
70
70
70
70
%Rec
100.04
100.81
99.88
99.78
104.04
Ref CPS
210265
1178367
1181392
1190813
106835
%RSD
1.48
0.63
0.45
3.99
3.91
CPS
210360
1187950
1179929
1188207
111154
Tune Mode
nogas
nogas
nogas
nogas
He
Tune Step
1
1
1
1
2
Mass
6
72
115
209
72
Name
Li
Ge
In
Bi
Ge
0.03
0.02
0.37
0.00
48.11
QC ISTD Table
0.18
0.00
0.00
0.01
3.74
0.05
%RSD
9513
4484
2380
75808
60
3724
250016
3115173
63394
570
8039
CPS
nogas
nogas
He
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
Tune Mode
1
1
2
1
1
1
1
1
1
1
1
Tune Step
118
137
121
31
139
43
44
56
77
82
95
Mass
Sn
Ba
Sb
P
La
Ca
Ca
Fe
Se
Se
Mo
Name
Page 2 of 2 Printed at: 09:45 on:2017-11-21166 of 828
00909955
-
Calibration Standard Report
0.04
0.63
0.40
65.22
0.01
0.00
0.01
0.05
0.18
0.00
0.04
0.28
0.00
0.01
1.55
0.00
123.92
0.84
0.07
0.00
0.00
0.00
0.01
0.02
0.01
0.01
0.02
0.00
0.00
0.00
0.00
0.17
0.00
0.00
0.00
0.01
%RSD
0.00
0.00
0.00
0.01
10793
1587
1077
45
58123
1634320
6783
8769
2947
587063
13128
3700
152345
48630
273
38063
67
1707
7899
37200
62481
92997
22476
20527
12811
30877
10473
209965
63036
38814
7219822
3784
1776010
80403
67271
52617
CPS
8899
5798618
2818163
45509
He
He
He
He
nogas
nogas
He
He
He
He
He
He
He
He
He
He
He
He
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
Tune Mode
nogas
nogas
nogas
nogas
2
2
2
2
1
1
2
2
2
2
2
2
2
2
2
2
2
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Tune Step
1
1
1
1
63
66
75
78
11
28
51
52
55
56
59
60
23
24
27
39
43
44
111
121
205
208
206
207
60
63
66
75
88
107
39
47
51
52
55
59
Mass
9
23
24
27
Cu
Zn
As
Se
B
Si
V
Cr
Mn
Fe
Co
Ni
Na
Mg
Al
K
Ca
Ca
Cd
Sb
Tl
Pb
[Pb]
[Pb]
Ni
Cu
Zn
As
Sr
Ag
K
Ti
V
Cr
Mn
Co
QC Analyte Table
Name
Be
Na
Mg
Al
Dilution 1
Comment
ISTD Ref File Name 004CALB.d
ISTD Pass/Fail Pass
Acq Date Time 2017-11-21T09:46:08-06:00
Sample Type CalStd
Level 3
Sample Table
Sample Name 5/25/500
Data File Name 006CALS.d
Data Path Name C:\Agilent\ICPMH\1\DATA\112
Page 1 of 2 Printed at: 09:47 on:2017-11-21167 of 828
00909956
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Calibration Standard Report
QC Flag%QC High
125
125
125
125
125
%QC Low
70
70
70
70
70
%Rec
99.43
98.66
101.70
99.76
99.67
Ref CPS
210265
1178367
1181392
1190813
106835
%RSD
4.83
1.90
5.68
2.81
1.92
CPS
209061
1162587
1201488
1187967
106487
Tune Mode
nogas
nogas
nogas
nogas
He
Tune Step
1
1
1
1
2
Mass
6
72
115
209
72
Name
Li
Ge
In
Bi
Ge
0.00
0.04
0.06
0.00
27.06
QC ISTD Table
0.05
0.00
0.00
0.01
1.58
0.03
%RSD
22118
10704
4977
84224
80
7742
311295
6042067
66572
890
15360
CPS
nogas
nogas
He
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
Tune Mode
1
1
2
1
1
1
1
1
1
1
1
Tune Step
118
137
121
31
139
43
44
56
77
82
95
Mass
Sn
Ba
Sb
P
La
Ca
Ca
Fe
Se
Se
Mo
Name
Page 2 of 2 Printed at: 09:47 on:2017-11-21168 of 828
00909957
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Calibration Standard Report
0.01
0.38
0.23
17.60
0.01
0.00
0.02
0.01
0.07
0.00
0.01
0.02
0.00
0.00
3.62
0.00
31.82
0.26
0.03
0.00
0.00
0.00
0.01
0.00
0.01
0.01
0.01
0.00
0.00
0.00
0.00
0.02
0.00
0.00
0.00
0.00
%RSD
0.02
0.00
0.00
0.00
21340
3034
2205
83
80636
2424770
12217
16801
6225
1152905
26196
7308
250732
95093
463
64341
120
3257
15711
72776
124251
184231
44522
40615
24303
60672
18927
236370
124138
77452
10470832
7215
1883920
124573
125300
103214
CPS
17292
9914735
5495232
78934
He
He
He
He
nogas
nogas
He
He
He
He
He
He
He
He
He
He
He
He
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
Tune Mode
nogas
nogas
nogas
nogas
2
2
2
2
1
1
2
2
2
2
2
2
2
2
2
2
2
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Tune Step
1
1
1
1
63
66
75
78
11
28
51
52
55
56
59
60
23
24
27
39
43
44
111
121
205
208
206
207
60
63
66
75
88
107
39
47
51
52
55
59
Mass
9
23
24
27
Cu
Zn
As
Se
B
Si
V
Cr
Mn
Fe
Co
Ni
Na
Mg
Al
K
Ca
Ca
Cd
Sb
Tl
Pb
[Pb]
[Pb]
Ni
Cu
Zn
As
Sr
Ag
K
Ti
V
Cr
Mn
Co
QC Analyte Table
Name
Be
Na
Mg
Al
Dilution 1
Comment
ISTD Ref File Name 004CALB.d
ISTD Pass/Fail Pass
Acq Date Time 2017-11-21T09:48:10-06:00
Sample Type CalStd
Level 4
Sample Table
Sample Name 10/50/1000
Data File Name 007CALS.d
Data Path Name C:\Agilent\ICPMH\1\DATA\112
Page 1 of 2 Printed at: 09:49 on:2017-11-21169 of 828
00909958
-
Calibration Standard Report
QC Flag%QC High
125
125
125
125
125
%QC Low
70
70
70
70
70
%Rec
98.23
97.07
99.72
95.20
98.80
Ref CPS
210265
1178367
1181392
1190813
106835
%RSD
5.51
2.65
4.54
1.42
2.51
CPS
206551
1143783
1178029
1133682
105554
Tune Mode
nogas
nogas
nogas
nogas
He
Tune Step
1
1
1
1
2
Mass
6
72
115
209
72
Name
Li
Ge
In
Bi
Ge
0.00
0.02
0.02
0.00
30.11
QC ISTD Table
0.02
0.00
0.00
0.00
1.12
0.02
%RSD
42265
20045
9156
96653
103
14756
422766
11193548
72351
1420
28911
CPS
nogas
nogas
He
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
Tune Mode
1
1
2
1
1
1
1
1
1
1
1
Tune Step
118
137
121
31
139
43
44
56
77
82
95
Mass
Sn
Ba
Sb
P
La
Ca
Ca
Fe
Se
Se
Mo
Name
Page 2 of 2 Printed at: 09:49 on:2017-11-21170 of 828
00909959
-
Calibration Standard Report
0.00
0.02
0.01
0.77
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.24
0.00
0.43
0.02
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
%RSD
0.00
0.00
0.00
0.00
184694
27858
19627
766
539833
15437736
100742
135997
54181
9863914
225712
65897
1839577
870788
2864
492988
1747
26743
141196
641325
1146983
1702085
419744
379478
213762
531312
172197
407649
1132164
687796
64068393
64448
2752843
885810
1060918
925909
CPS
163444
79003827
52444990
705023
He
He
He
He
nogas
nogas
He
He
He
He
He
He
He
He
He
He
He
He
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
Tune Mode
nogas
nogas
nogas
nogas
2
2
2
2
1
1
2
2
2
2
2
2
2
2
2
2
2
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Tune Step
1
1
1
1
63
66
75
78
11
28
51
52
55
56
59
60
23
24
27
39
43
44
111
121
205
208
206
207
60
63
66
75
88
107
39
47
51
52
55
59
Mass
9
23
24
27
Cu
Zn
As
Se
B
Si
V
Cr
Mn
Fe
Co
Ni
Na
Mg
Al
K
Ca
Ca
Cd
Sb
Tl
Pb
[Pb]
[Pb]
Ni
Cu
Zn
As
Sr
Ag
K
Ti
V
Cr
Mn
Co
QC Analyte Table
Name
Be
Na
Mg
Al
Dilution 1
Comment
ISTD Ref File Name 004CALB.d
ISTD Pass/Fail Pass
Acq Date Time 2017-11-21T09:50:11-06:00
Sample Type CalStd
Level 5
Sample Table
Sample Name 100/500/10K
Data File Name 008CALS.d
Data Path Name C:\Agilent\ICPMH\1\DATA\112
Page 1 of 2 Printed at: 09:51 on:2017-11-21171 of 828
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-
Calibration Standard Report
QC Flag%QC High
125
125
125
125
125
%QC Low
70
70
70
70
70
%Rec
87.43
96.73
98.24
92.19
95.26
Ref CPS
210265
1178367
1181392
1190813
106835
%RSD
1.15
2.23
1.13
3.17
1.23
CPS
183829
1139784
1160616
1097772
101772
Tune Mode
nogas
nogas
nogas
nogas
He
Tune Step
1
1
1
1
2
Mass
6
72
115
209
72
Name
Li
Ge
In
Bi
Ge
0.00
0.00
0.00
0.00
9.18
QC ISTD Table
0.00
0.00
0.00
0.00
0.03
0.00
%RSD
396138
190578
82770
307559
277
123731
2134105
89314448
80199
10276
250552
CPS
nogas
nogas
He
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
Tune Mode
1
1
2
1
1
1
1
1
1
1
1
Tune Step
118
137
121
31
139
43
44
56
77
82
95
Mass
Sn
Ba
Sb
P
La
Ca
Ca
Fe
Se
Se
Mo
Name
Page 2 of 2 Printed at: 09:51 on:2017-11-21172 of 828
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-
Calibration Standard Report
0.00
0.00
0.00
0.25
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.25
0.00
0.22
0.01
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
%RSD
0.00
0.00
0.00
0.00
372908
55786
38826
1492
1109923
28411012
199774
269505
106959
19543489
447879
128825
3594676
1628054
4871
957133
3334
54437
285951
1250833
2143890
3225217
818287
751035
419714
1024641
345248
609480
2238306
1286918
128244920
126433
3423341
1586374
2017806
1799711
CPS
333867
155734453
103072813
1260655
He
He
He
He
nogas
nogas
He
He
He
He
He
He
He
He
He
He
He
He
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
Tune Mode
nogas
nogas
nogas
nogas
2
2
2
2
1
1
2
2
2
2
2
2
2
2
2
2
2
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Tune Step
1
1
1
1
63
66
75
78
11
28
51
52
55
56
59
60
23
24
27
39
43
44
111
121
205
208
206
207
60
63
66
75
88
107
39
47
51
52
55
59
Mass
9
23
24
27
Cu
Zn
As
Se
B
Si
V
Cr
Mn
Fe
Co
Ni
Na
Mg
Al
K
Ca
Ca
Cd
Sb
Tl
Pb
[Pb]
[Pb]
Ni
Cu
Zn
As
Sr
Ag
K
Ti
V
Cr
Mn
Co
QC Analyte Table
Name
Be
Na
Mg
Al
Dilution 1
Comment
ISTD Ref File Name 004CALB.d
ISTD Pass/Fail Pass
Acq Date Time 2017-11-21T09:52:11-06:00
Sample Type CalStd
Level 6
Sample Table
Sample Name 200/1000/20K
Data File Name 009CALS.d
Data Path Name C:\Agilent\ICPMH\1\DATA\112
Page 1 of 2 Printed at: 09:53 on:2017-11-21173 of 828
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-
Calibration Standard Report
QC Flag%QC High
125
125
125
125
125
%QC Low
70
70
70
70
70
%Rec
76.24
93.28
95.41
87.94
91.65
Ref CPS
210265
1178367
1181392
1190813
106835
%RSD
1.14
0.84
2.74
1.57
2.92
CPS
160297
1099169
1127131
1047197
97916
Tune Mode
nogas
nogas
nogas
nogas
He
Tune Step
1
1
1
1
2
Mass
6
72
115
209
72
Name
Li
Ge
In
Bi
Ge
0.00
0.00
0.00
0.00
2.85
QC ISTD Table
0.00
0.00
0.00
0.00
0.01
0.00
%RSD
797030
375985
164800
548372
447
261984
4174667
180758192
92109
20752
499094
CPS
nogas
nogas
He
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
Tune Mode
1
1
2
1
1
1
1
1
1
1
1
Tune Step
118
137
121
31
139
43
44
56
77
82
95
Mass
Sn
Ba
Sb
P
La
Ca
Ca
Fe
Se
Se
Mo
Name
Page 2 of 2 Printed at: 09:53 on:2017-11-21174 of 828
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-
Initial Calibration Verification (ICV) Report
QC Flag%QC High
125
125
125
125
%QC Low
70
70
70
70
%Rec
83.10
96.95
97.47
93.58
Ref CPS
210265
1178367
1181392
1190813
174727
1142378
1151541
1114380
%RSD
2.51
4.52
1.51
4.73
1
1
Tune Mode
nogas
nogas
nogas
nogas
In
Bi
Mass
6
72
115
209
ICV Main CR1 Failed
QC ISTD Table
Name
Li
Ge
Tune Step
1
1
CPS
ICV Main CR1 Failed
ICV Main CR1 Failed
ICV Main CR1 Failed
ICV Main CR1 Failed
ICV Main CR1 Failed
ICV Main CR1 Failed
ICV Main CR1 Failed
ICV Main CR1 Failed
ICV Main CR1 Failed
ICV Main CR1 Failed
110
110
110
110
110
QC Flag
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
90
90
%High
110
110
110
110
110
110
110
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
98.1
87.1
89.1
104.9
268.5
%Low
90
90
90
90
91.6
34.3
90.8
94.3
92.3
98.4
98.1
94.6
89.2
99.1
88.5
89.3
96.3
92.2
99.6
98.9
96.6
94.2
86.6
92.7
87.4
93.5
94.0
95.8
99.1
94.5
101.2
91.4
95.4
96.3
84.6
93.9
97.7
97.8
99.6
105.3
98.0
98.4
100.2
99.0
98.5
96.2
100
100
%Rec
90.7
95.1
95.3
93.1
90.3
94.1
78.4
100
100
100
100
100
500
5000
10000
10000
10000
100
100
100
100
100
100
100
500
10000
100
100
100
10000
100
100
10000
10000
100
10000
10000
100
100
100
100
100
100
100
100
100
100
100
100
10000
100
100
100
100
100
1.93
2.67
1.64
45.19
21.65
Exp Value
100
10000
10000
100
0.83
2.45
2.64
2.68
0.81
2.86
1.58
11.44
0.97
2.48
2.28
0.10
1.31
2.23
2.42
1.67
1.46
0.93
15.50
1.92
8.97
1.73
1.31
4.50
0.22
2.63
1.69
0.69
3.91
2.63
1.98
0.96
3.04
1.21
1.02
2.51
0.37
0.64
2.41
1.81
1.86
3.57
277
27
CPS %RSD
0.65
1.36
2.30
4.49
2.20
3.93
1.58
244002
373573
188593
83480
363435
289780
15040492
118503
2023019
85597873
68465
9843
65993
185088
27020
19655
731
537073
26219
97263
133769
53248
9300010
229987
362258
1794252
818134
2324
451683
1513
141788
646673
1204544
1701918
1544312
438315
215270
524893
171309
378872
1085283
657399
61389203
61644
2412059
832758
1037817
934451
2.232
1.691
7.666
61.753
32.664
CPS
160107
75659037
49701068
622551
3.931
81.069
2.471
6.853
1.234
2.842
1.655
11.220
3.214
4.925
6.430
5.096
1.578
1.986
2.423
1.383
1.627
1.130
16.642
1.974
8.963
2.029
1.276
4.439
4.762
7.033
6.038
4.394
4.274
2.878
11.816
5.435
4.408
2.458
5.492
6.899
5.056
3.935
6.621
5.657
4.291
2.500
104.928
268.463
Conc %RSD
2.326
2.061
3.703
7.559
5.774
6.002
17.817
94.298
92.322
98.394
98.109
87.129
445.749
4955.026
8847.297
8932.439
9158.270
34.252
90.828
98.915
96.594
94.196
98.068
94.630
445.942
9349.566
93.970
95.817
96.261
9224.699
99.559
91.393
9537.316
9628.368
86.623
9269.427
8744.181
97.835
99.585
105.294
99.133
94.490
101.238
98.988
98.535
96.201
84.646
93.882
97.739
9026.322
94.100
78.446
97.999
98.439
100.206
He
nogas
nogas
nogas
nogas
Conc
90.695
9514.950
9525.423
93.102
nogas
nogas
nogas
nogas
nogas
nogas
He
He
nogas
nogas
nogas
nogas
He
He
He
He
He
He
He
He
He
He
He
He
nogas
nogas
nogas
nogas
He
He
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
1
1
Tune Mode
nogas
nogas
nogas
nogas
nogas
nogas
nogas
1
1
1
2
1
1
1
1
1
1
1
1
2
2
2
2
2
1
2
2
2
2
2
2
1
2
2
2
2
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
121
7
31
139
197
Tune Step
1
1
1
1
56
77
82
95
118
137
75
78
11
28
43
44
55
56
59
60
63
66
27
39
43
44
51
52
208
238
206
207
23
24
75
88
107
111
121
205
52
55
59
60
63
66
La
Au
Mass
9
23
24
27
39
47
51
Mo
Sn
Ba
Sb
Li
P
Si
Ca
Ca
Fe
Se
Se
Ni
Cu
Zn
As
Se
B
Ca
V
Cr
Mn
Fe
Co
[Pb]
Na
Mg
Al
K
Ca
Cd
Sb
Tl
Pb
U
[Pb]
Ni
Cu
Zn
As
Sr
Ag
K
Ti
V
Cr
Mn
Co
QC Analyte Table
Name
Be
Na
Mg
Al
Comment
ISTD Ref File Name 004CALB.d
Sample QC Pass/Fail Fail
ISTD Pass/Fail Pass
Acq Date Time 2017-11-21T09:56:15-06:00
Sample Type ICV
Dilution 1
Sample Table
Sample Name ICV
Data File Name 011_ICV.d
Data Path Name C:\Agilent\ICPMH\1\DATA\112
Page 1 of 2 Printed at: 09:57 on:2017-11-21
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Initial Calibration Verification (ICV) Report
Mass Tune Step Tune Mode CPS %RSD Ref CPS QC Flag
125
%QC High
70
%QC Low
95.04
%Rec
0.30 1068351015352 HeGe 72
Name
Page 2 of 2 Printed at: 09:57 on:2017-11-21
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-
Sample Report
QC Flag
200000
2000
2000
2000
2000
2000
2000
2000
2000
2000
200000
2000
2000
200000
200000
2000
200000
200000
200000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
2000
LDR
2000
200000
200000
2000
200000
0.02
6.16
0.14
0.05
0.37
0.47
12.59
0.04
25.89
0.07
0.05
0.14
0.10
0.04
0.02
0.23
1.16
-0.95
0.98
532.59
0.07
0.01
0.01
0.01
0.01
0.02
0.04
0.02
0.06
0.00
0.01
0.01
0.00
0.13
0.00
0.00
0.01
0.01
%RSD
0.06
0.01
0.02
0.01
4181
4364
727
438
22
59297
1190144
3530
4107
1207
234653
4964
1663
87329
18443
137
22253
43
790
15010
45653
38869
39239
9563
8626
13242
4171
200816
24724
15387
3147
1383
1731176
48056
32152
21707
5561
CPS
3554
3231751
1142034
23211
5080071
9.59
8.88
3.97
3.99
7.08
7.53
21.60
12.57
22.80
3.32
14.37
19.72
2.69
5.27
1.64
4.56
5.50
-160.85
9.17
11.39
0.39
2.33
18.14
2.77
2.13
1.51
3.51
4.03
8.12
91.60
3.55
5.37
3.47
23.59
58.15
17.52
5.51
3.68
Conc %RSD
13.25
5.03
6.63
9.09
257.422
2.367
2.681
2.056
2.769
24.227
183.628
2.487
2.050
1.642
226.220
2.112
2.261
203.770
213.355
-1.295
217.866
230.787
204.531
1.680
3.920
2.216
2.352
2.160
2.132
2.200
2.298
5.432
2.159
2.298
2.143
1.839
14.508
2.017
2.292
2.345
2.148
FinalConc
2.100
218.858
220.394
2.166
217.015
2.681
2.056
2.769
24.227
183.628
257.422
2.050
1.642
226.220
2.112
2.261
2.367
213.355
-1.295
217.866
230.787
204.531
2.487
3.920
2.216
2.352
2.160
2.132
203.770
2.298
5.432
2.159
2.298
2.143
1.680
14.508
2.017
2.292
2.345
2.148
2.200
Conc
2.100
218.858
220.394
2.166
217.015
1.839
He
He
nogas
nogas
nogas
He
He
He
He
He
He
He
He
He
He
He
He
nogas
nogas
nogas
nogas
He
He
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
Tune Mode
nogas
nogas
nogas
nogas
nogas
nogas
nogas
2
1
1
1
2
2
2
2
2
2
2
2
2
2
2
2
1
1
1
2
2
2
1
1
1
1
1
1
1
1
1
1
1
1
Tune Step
1
1
1
1
1
1
1
1
11
28
43
59
60
63
66
75
78
43
44
51
52
55
56
206
207
23
24
27
39
107
111
121
205
208
238
59
60
63
66
75
88
27
39
47
51
52
55
Si
Ca
Ni
Cu
Zn
As
Se
B
Ca
V
Cr
Mn
Fe
Co
[Pb]
Na
Mg
Al
K
Ca
Cd
Sb
Tl
Pb
U
[Pb]
Ni
Cu
Zn
As
Sr
Ag
K
Ti
V
Cr
Mn
Co
QC Analyte Table
Name
Be
Na
Mg
Al
Mass
9
23
24
Comment
ISTD Ref FileName 004CALB.d
Sample QC Pass/Fail Pass
ISTD Pass/Fail Pass
Acq Date Time 2017-11-21T09:58:14-06:00
Sample Type Sample
Dilution 1
Sample Table
Sample Name LLICV2
Data File Name 012SMPL.d
Data Path Name C:\Agilent\ICPMH\1\DATA\112
Page 1 of 2 Printed at: 09:59 on:2017-11-21
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Sample Report
Tune Step Tune Mode Conc FinalConc Conc %RSD CPS
QC Flag%QC High
125
125
125
125
125
%QC Low
70
70
70
70
70
%Rec
90.25
94.48
98.15
94.54
95.54
Ref CPS
210265
1178367
1181392
1190813
106835
%RSD
1.97
2.47
0.41
2.61
2.70
CPS
189771
1113349
1159550
1125819
102070
Tune Mode
nogas
nogas
nogas
nogas
He
Tune Step
1
1
1
1
2Ge
Mass
6
72
115
209
72
QC ISTD Table
Name
Li
Ge
In
Bi
QC Flag
2000
2000
2000
2000
2000
200000
200000
2000
2000
2000
LDR
0.02
0.02
0.05
0.09
-16.51
#DIV/0!
0.09
0.01
0.04
0.52
%RSD
9486
4221
1927
57
0
235418
2863942
65130
643
677127.85
5.49
4.79
6.71
-157.14
0.00
9.92
5.72
105.99
24.37
2.140
2.117
1.753
-9.353
-149.434
202.957
207.182
23.972
3.366
1.369
2.117
1.753
-9.353
-149.434
202.957
207.182
23.972
3.366
1.369
2.140
He
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
1
1
1
1
1
1
1
2
1
1
197
82
95
118
137
121
139
44
56
77
Mass
Mo
Sn
Ba
Sb
La
Au
Ca
Fe
Se
Se
Name
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Low Level Initial Calibration Verification (LLICV) Report
QC Flag%QC High
125
125
%QC Low
70
70
%Rec
90.66
96.92
Ref CPS
210265
1178367
190626
1142132
%RSD
2.84
1.32
Tune Mode
nogas
nogas
Mass
6
72
LLICV Main CR1 Failed
LLICV Main CR1 Failed
QC ISTD Table
Name
Li
Ge
Tune Step
1
1
CPS
LLICV Main CR1 Failed
LLICV Main CR1 Failed
LLICV Main CR1 Failed
LLICV Main CR1 Failed
LLICV Main CR1 Failed
LLICV Main CR1 Failed
130
130
130
130
130
QC Flag
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
70
70
%High
130
130
130
130
130
130
130
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
70
97.9
94.3
100.8
-126.4
-977.4
%Low
70
70
70
70
100.3
1305.0
111.3
83.7
101.9
102.5
102.7
101.9
124.4
1304.6
99.8
95.9
93.0
108.0
98.8
96.7
106.0
108.5
44.4
104.0
44.8
101.0
110.0
104.1
103.3
109.0
98.8
101.5
103.2
104.7
355.4
104.7
108.7
110.2
98.1
103.0
114.0
105.0
107.5
103.0
104.3
106.7
5
5
%Rec
102.8
104.0
104.5
106.8
97.1
97.8
818.5
5
5
5
5
5
25
25
500
500
500
5
5
5
5
5
5
5
25
500
5
5
5
500
5
5
500
500
5
500
500
5
5
5
5
5
5
5
5
5
5
5
5
500
5
5
5
5
5
4.88
3.41
2.28
71.20
86.60
Exp Value
5
500
500
5
3.21
3.15
9.99
2.15
3.39
2.21
4.60
11.17
1.40
0.99
4.19
1.09
5.35
1.77
4.18
8.79
2.86
3.52
17.84
3.54
26.65
6.30
1.06
5.43
0.32
1.73
1.80
2.06
0.64
2.39
3.46
1.65
0.69
4.30
0.79
0.61
0.98
2.06
3.80
0.64
0.51
4.39
63
7
CPS %RSD
10.25
1.34
1.28
1.10
2.32
4.85
2.72
14146
21367
9960
4737
37187
81381
1634481
7512
298046
5657063
73779
890
3484
10327
1567
1091
41
66732
1680
6842
8762
2957
569797
11881
20947
149244
46301
233
36586
43
8005
36221
61276
92295
92777
22282
12214
29598
9683
232971
60928
36883
6926537
3417
2040313
79418
63926
50534
9.107
1.177
20.568
-353.055
-178.246
CPS
8736
5584754
2719613
44761
5.268
29.625
13.323
1.541
7.197
6.962
4.890
7.951
8.479
3.349
3.349
3.936
7.446
5.194
6.500
13.283
6.161
4.399
59.211
5.243
29.972
11.167
3.355
7.684
1.710
1.173
3.181
0.514
6.281
6.025
28.543
2.862
2.032
9.340
1.945
1.112
2.416
3.939
4.950
0.893
1.881
5.737
-6.320
-48.872
Conc %RSD
7.756
3.776
2.670
0.459
7.118
3.798
19.848
4.186
5.093
5.124
4.895
4.713
25.205
326.139
499.229
479.479
501.485
65.251
5.563
4.837
5.299
5.427
5.136
5.097
31.106
505.000
5.500
5.204
4.651
540.214
4.939
5.077
515.861
523.343
2.219
519.969
224.114
5.510
4.906
5.150
5.163
5.451
4.939
5.151
5.213
5.337
17.768
5.233
5.434
485.726
4.888
40.925
5.698
5.250
5.375
He
nogas
nogas
nogas
nogas
Conc
5.142
519.982
522.690
5.342
nogas
nogas
nogas
nogas
nogas
nogas
He
He
nogas
nogas
nogas
nogas
He
He
He
He
He
He
He
He
He
He
He
He
nogas
nogas
nogas
nogas
He
He
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
1
1
Tune Mode
nogas
nogas
nogas
nogas
nogas
nogas
nogas
1
1
1
2
1
1
1
1
1
1
1
1
2
2
2
2
2
1
2
2
2
2
2
2
1
2
2
2
2
2
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
121
7
31
139
197
Tune Step
1
1
1
1
56
77
82
95
118
137
75
78
11
28
43
44
55
56
59
60
63
66
27
39
43
44
51
52
208
238
206
207
23
24
75
88
107
111
121
205
52
55
59
60
63
66
La
Au
Mass
9
23
24
27
39
47
51
Mo
Sn
Ba
Sb
Li
P
Si
Ca
Ca
Fe
Se
Se
Ni
Cu
Zn
As
Se
B
Ca
V
Cr
Mn
Fe
Co
[Pb]
Na
Mg
Al
K
Ca
Cd
Sb
Tl
Pb
U
[Pb]
Ni
Cu
Zn
As
Sr
Ag
K
Ti
V
Cr
Mn
Co
QC Analyte Table
Name
Be
Na
Mg
Al
Comment
ISTD Ref File Name 004CALB.d
Sample QC Pass/Fail Fail
ISTD Pass/Fail Pass
Acq Date Time 2017-11-21T10:00:16-06:00
Sample Type LLICV
Dilution 1
Sample Table
Sample Name LLICV5
Data File Name 013LICV.d
Data Path Name C:\Agilent\ICPMH\1\DATA\112
Page 1 of 2 Printed at: 10:01 on:2017-11-21
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Low Level Initial Calibration Verification (LLICV) Report
Mass Tune Step Tune Mode CPS %RSD Ref CPS QC Flag
125
125
125
%QC High
70
70
70
%QC Low
97.77
96.93
98.60
%Rec
3.74
1181392
1190813
106835
1154988
1154210
105343
4.78
1.54
1
1
2
nogas
nogas
He
In
Bi
Ge
115
209
72
Name
Page 2 of 2 Printed at: 10:01 on:2017-11-21
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Initial Calibration Blank (ICB) Report
ICB Main CR1 Failed
ICB Main CR1 Failed
QC Flag
100
100
2.5
2.5
2.5
10
5
100
2.5
2.5
100
2.5
2.5
2.5
100
5
100
100
100
2.5
1
2.5
2.5
2.5
2.5
100
2.5
2.5
2.5
2.5
1
2.5
2.5
2.5
2.5
2.5
2.5
2.5
Upper Limit
1
100
100
5
100
2.5
57.7
2.0
0.9
9.1
1.2
0.5
2.0
46.6
22.8
22.2
22.9
40.0
3.2
173.2
18.5
2.2
20.3
21.1
9.9
21.1
11.5
2.9
15.2
33.8
3.3
20.0
28.6
2.3
29.9
13.9
3.0
19.2
15.1
7.3
3.9
3.9
CPS %RSD
20.0
2.8
17.6
4.3
0.7
17.0
3.9
3.1
701500
1207
187280
947186
217
567
67
33
6
41733
173
1675
1360
213
9226
87
133
49528
537
123
11544
7
70
1770
2874
863
863
213
500
1580
653
218565
810
550
3800140
223
1996313
34192
9829
580
CPS
150
1631805
25656
11717
-9.7
-5.3
13.8
163.9
62.2
20.4
98.5
29.8
523.8
-46.0
8.9
165.1
83.9
18.0
24.8
-73.1
-99.8
343.8
-59.4
2.5
30.5
22.4
13.7
38.4
29.6
-16.3
5.6
27.5
7.7
51.7
38.3
-1.9
16.9
56.4
45.9
53.1
-13.0
-39.2
Conc %RSD
21.7
45.9
19.5
18.0
-215.5
2315.2
0.689
4.455
4.401
25.983
-62.296
-8.203
3.240
0.010
0.090
0.387
0.391
0.038
-7.875
18.613
-18.766
0.629
0.033
-0.163
0.033
0.025
0.014
-11.394
3.299
-2.057
0.037
0.033
0.034
-0.430
0.232
0.027
0.078
0.023
-0.254
-0.061
0.259
11.167
Conc
0.074
9.661
4.279
0.333
-3.795
0.002
36.503
0.165
nogas
nogas
nogas
nogas
He
He
He
He
He
nogas
He
He
He
He
He
He
nogas
He
He
He
He
He
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
nogas
Tune Mode
nogas
nogas
nogas
nogas
1
1
2
2
2
1
1
1
2
2
2
2
2
2
2
2
2
2
2
2
1
1
1
1
1
2
1
1
1
1
1
1
1
1
1
1
1
1
Tune Step
1
1
1
1
1
1
78
11
28
43
44
56
56
59
60
63
66
75
39
43
44
51
52
55
238
206
207
23
24
27
88
107
111
121
205
208
55
59
60
63
66
75
Mass
9
23
24
27
39
47
51
52
Si
Ca
Ca
Fe
Ni
Cu
Zn
As
Se
B
Ca
V
Cr
Mn
Fe
Co
[Pb]
Na
Mg
Al
K
Ca
Cd
Sb
Tl
Pb
U
[Pb]
Ni
Cu
Zn
As
Sr
Ag
K
Ti
V
Cr
Mn
Co
QC Analyte Table
Name
Be
Na
Mg
Al
Comment
ISTD Ref File Name 004CALB.d
Sample QC Pass/Fail Fail
ISTD Pass/Fail Pass
Acq Date Time 2017-11-21T10:02:18-06:00
Sample Type ICB
Dilution 1
Sample Table
Sample Name ICB
Data File Name 014_ICB.d
Data Path Name C:\Agilent\ICPMH\1\DATA\112
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Initial Calibration Blank (ICB) Report
CPS CPS %RSD Upper Limit QC FlagName Mass Tune Step Tune Mode Conc Conc %RSD
QC Flag%QC High
125
125
125
125
125
%QC Low
70
70
70
70
70
%Rec
97.39
96.88
100.60
96.14
99.01
Ref CPS
210265
1178367
1181392
1190813
106835
%RSD
0.62
0.90
4.18
1.36
2.19
CPS
204772
1141634
1188483
1144870
105772
1
2
Tune Mode
nogas
nogas
nogas
nogas
He
Bi
Ge
Mass
6
72
115
209
72
ICB Main CR1 Failed
QC ISTD Table
Name
Li
Ge
In
Tune Step
1
1
1
ICB Main CR1 Failed
ICB Main CR1 Failed
2.5
2.5
10
2.5
2.5
2.5
2.5
2.5
5
2.4
13.1
66.7
3.1
17.3
8.8
6.7
40.8
0.0
30
1243
957
197
150
67099
117
70573
367
133.8
-1.1
-124.8
33.0
100.0
20.5
104.7
-4.7
25.3
-3.509
19.989
311.301
46.168
0.590
-0.862
0.037
0.028
-0.339
nogas
nogas
nogas
nogas
He
nogas
nogas
nogas
nogas
1
2
1
1
1
1
1
1
1
31
139
197
77
82
95
118
137
121
Au
Mo
Sn
Ba
Sb
P
La
Se
Se
Page 2 of 2 Printed at: 10:03 on:2017-11-21
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Interference Check Solution A (ICS-A) Report
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
ICSA Main CR1 Failed
0
0
0
QC Flag
ICSA Main CR1 Failed
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
14.1
27.4
12.6
Upper Limit
0
0
0
0
1.6
3.0
2.5
2.5
18.8
1.2
8.9
6.2
38.9
65.5
4.0
0.5
5.2
2.3
26.9
2.7
37.7
16.7
1.0
1.5
0.8
0.9
1.7
2.9
8.1
10.7
17.4
10.6
16.6
14.1
14.7
2.4
10.6
3.1
4.8
18.7
0.5
2.3
2.0
2.2
0.6
1.9
1083
243
243
CPS %RSD
28.6
1.8
1.9
1.3
1286451
19846699
906142187
57020
373
4916431
1523
93
54
5
47581
919502
681
3154
260
95149635
77
240
18200696
8261254
2178244
4593318
14776
261306
1500
2314
637
2053
547
483
1520
6405
2870
171889
10970
433
608871580
1331121
913827
40515
9579
1307
51.0
60.7
-15.4
CPS
53
790898668
525752128
626429191
2.4