25 funston road kansas city, kansas 66115 octkm991 · united states environmental protection age...

UNITED STATES ENVIRONMENTAL PROTECTION AGE

rttUblVEO

OCTKM991SECTION

REGION 725 FUNSTON ROAD

KANSAS CITY, KANSAS 66115

OCTDate:

MEMORANDUM

SUBJECT: Data 'Transmittal for Activity #:Site -Desciption: K^ /s ^ v

FROM: Andrea JirkaChief, Laboratory Branch, ENSV

TO:

ATTN:

Robert MorbyChief, Superfund Branch, WSTM

Attached is the data transmittal for the above referenced

site. This should be considered a Partial or

Complete data transmittal (completes transmittal of/

). If you have have any questions or

comments, please contact Dee Simmons at 551-5129.

Attachments

cc: Data Files

NOTE: Please see Mary Gerken, SPFD-WSTM, if you want-an -- ..._—.„ ^electronic copy of the data. • :• hltaa~?>f)i-J>.- *•••£ I

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ENVIRONMENTAL SERVICES ASSISTANCE TEAM - ZONE H

ICF Technology Incorporated

NSI Technology Services Corp.

The Bionetics Corp.

ESAT Region VIINSI Technology Services25 Funston RoadKansas City, KS 66115(913) 236-3881

TO: Larry Marchin/Barry EvansData Review Task Monitor

THRU: Harold Brown, Ph.D.ESAT Deputy Project Officer, EPJ

FROM: Kevin LudwikoskiESAT Data Reviewer

THRU: . Ronald A. RossESAT Team Manager

DATE: September 17, 1991SUBJECT: Review of inorganic data for Mississippi River Pool # 15

TID# 07-9103-535ASSIGNMENT/ 955ICF ACCT# 302-26-535-02ManTech S.O.# 1073-535ESAT Document No. ESAT-VII-535-0209

These data were reviewed primarily according to the"Laboratory Data Validation Functional Guidelines for EvaluatingInorganic Analyses," July 1988 revision with changes given in theRegion VII Inorganic Data Review Training Manual and EPAmemorandums.

The following comments and attached data sheets are a resultof the'ESAT review, according to EPA policies, of the followingdata from the contract laboratory.

CASE NO.: 16873SITE: Mississippi River PoolREVIEWER: Kevin Ludwikoski

LABORATORY: AAT8METHOD NO.: CS0390IEPA ACTIVITY NO.: ISXP8MATRIX: SOIL/WATER

TOTAL METALS(SOIL)

SMO Sample No. EPA Sample No.

TOTAL METALS(WATER)

SMO Sample No. EPA Sample No,

MGH299MGH300MGJ031MGJ032MGJ033MGJ034

ISXP8101ISXP8102ISXP8103ISXP8103DISXP8104ISXP8105

MGH297MGH298MGJ026MGJ027MGJ028MGJ029MGJ030MGJ298MGJ299

ISXP8001ISXP8001DISXP8002ISXP8003ISXP8004ISXP8005ISXP8008FISXP8109FISXP8929P

GENERAL

This data review assignment covers NINE WATER samples analyzedfor TOTAL METALS and SIX SOIL samples analyzed for TOTAL METALSfor case number 16873. There was one PE sample, one field blank,one rinsate blank and one field duplicate for Total Metals inwater. There was one field duplicate for Total Metals in soilincluded with this assignment. Sample ISXP8001D was used as alaboratory duplicate sample for the analysis. As a result, thissample is refered to in this document and reported in the datasheets as ISXP8001L.

1. Technical Holding Times / Preservation

A. Technical holding times were observed for a1!! analytes.

B. Technical holding times are not specified for soil samples.

2. Initial and Continuing Calibration

A. All percent recoveries were within control limits for watersamples.

B. All percent recoveries were with control limits for soilsamples.

3. Blanks

Several analytes were detected in the blanks. Correspondingsample results were qualified according to the blank rule usingfive times the highest blank value. Sample results requiringmodification are reported as non-detect on the attached datasheets.

A. , TOTAL METALS(WATER)

5 x HighestAnalyte Blank fua/L) Qualified Samples

As 14 None qualifiedCu 65 None qualifiedPb 8 ISXP8001, -001D, -001L, -004Hg 2.95 ISXP8004S, -929P

Fe, Mg, and Pb were found in the rinsate blank (ISXP8109F) ;however, no data were qualified due to this sample. Due to the highconcentration of these analytes, the user is encouraged to usecareful judgement in utilizing associated data.

B. TOTAL METALS(SOIL)

5 x HighestAnalvte Blank (mq/kq) Qualified Samples

Pb 1.4 None qualified

4. ICP interference Check

Recoveries of solution AB analytes were within control limitsfor Total Metals. Sb, K, and Na were found but not present in theICS solution. All absolute values for these analytes were below theCRDL; therefore, no data were qualified by the ICP interferencecheck sample.

5. Laboratory control Standard (LCS)

A. LCS results were within established control limits forTotal Metals in water samples.

B. LCS results were within established control limits forTotal Metals in soil samples.

6. Duplicates

A. The RPD for all analytes were within control limits forTotal Metals in water samples.

B. The RPD for Cu and Fe exceeded control limits for TotalMetals in soil. The sample results that were coded J are listedbelow.

TOTAL METALS(SOIL)

Analyte Samples Qualified Code

Cu ISXP8101, -102, -103, -103D, -104, J-104S, -105, -901C

Fe ISXP8101, -102, -103, -103D, -104, J-105, -901C

Note: All samples listed above with the exception of ISXP8104Swere also "J" coded for Cu due to the spike rule.

7. Matrix Spike Sample

A. Cd, Pb, and Tl were out of range for matrix spike recoveryfor Total Metals in water. The samples that had data qualified arelisted below.

TOTAL METALS(WATER)

Analyte % Rec Sample No. Code

Cd 128.9 ISXP8929P, -900C JPb 54.1 ISXP8929P, -900C JCr 66.9 ISXP8900C J

Note: Samples ISXP8001, -001D, -001L and 004 were qualified for Pb;however, these samples had been previously "U" coded according tothe blank rule.

(CONT.)

B. Sb, Cd, Cr and Cu were out of range for matrix spikerecovery for Total Metals in soil. The samples that had dataqualified are listed below.

TOTAL METALS(SOIL)

Analyte % Rec Sample No. Code

Sb 20.9 ISXP8901C JISXP8101, -102, -103, -103D, -104, I-104L, -105, -901M

Cd 137.0 ISXP8901C JCr 167.3 ISXP8101, -102, -103, -103D, -104 J

-104L, -105, -901CCU 419.2.- ISXP8101, -102, -103, -103D, -104 J

-104L, -105, -901CNote: Cu in samples ISXP8101, -102, -103, -103D, -104, -105 and901C were previously "J" coded due to the duplicate rule.

s. ICP Serial Dilution

A. The ICP serial dilution results for Total metals in waterwere within control limits.

B. The ICP serial dilution results for Total Metals in soilwere within control limits with the exception of Cu (13.9 %RPD).Samples ISXP8101, -102, -103, -103D, -104, -104L, -104S, -105, and-901C were qualified by ICP serial dilution rules. These sampleshad been previously "J" coded due to either the spike or duplicaterules.

9. Furnace Atomic Absorption/

A. No MSA's were performed on Total Metals in water.

B. The analytical scheme was followed for Furnace AA analysisfor Total Metals in soil. MSA correlation coefficients wereacceptable for As in samples ISXP8104 and ISXP8104L (cc=.9949 and.9981 respect ively).

10. PE Sample

All analytes present in the PE Sample were found at acceptablelevels with the exception of Al and Hg (160% and 149% recoveries,respectively).

11. summary

A. Two analytes had samples that were qualified by the blankrule and three by the spike rule for Total Metals in water.

B. Four analytes were qualified by the spike rule, two by theduplicate rule and one by serial dilution outliers for Total Metalsin soil. '«'

ENVIRONMENTAL SERVICES ASSISTANCE TEAM - ZONE H

ICF Technology Incorporated

NSI Technology services Corp.

The Bionetics Corp.

ESAT Region VIINSI Tech. Serv. Corp.25 Funston RoadKansas City, KS 66115(913) 551-5000

TO:

THRU:

FROM:

THRU:

Barry EvansData Review Task MonitorHarold Brown, Ph.D.ESAT Deputy Project Officer, EPA

David J. HickeyESAT Data ReviewerRonald A. "RossESAT Team Manager

DATE: September 27, 1991SUBJECT: Review of organic data for Mississippi River Pool #15

TID# 07-9103-535ASSIGNMENT/ 957ICF ACCT# 26-535-02NSI S.0.# 1073-535ESAT Document No. ESAT-VII-535-0223

These data were reviewed primarily according to the "LaboratoryData Validation Functional Guidelines for Evaluating OrganicAnalyses," February 1990.

The following comments and attached data sheets are a result ofthe ESAT review, according to EPA policies, of the following datafrom the contract laboratory.

CASE NO.: 16873SITE: Mississippi River PoolREVIEWER: David J. Hickev

LABORATORY: PNELIMETHOD NO.: CS03900EPA ACTIVITY NO.: ISXP8MATRIX: WATER/SOIL

GL339GL340GL362GL363GL364GL365

VOLATILES(WATER)


ISXP8001ISXP8001DISXP8002ISXP8003ISXP8004ISXP8005


GL361GL366GL343GL344GL347

ISXP8006FISXP8008FISXP8009FISXP8109FISXP8926P

SMO Sample No.

GL341GL342GL368GL369

SMO Sample No.

GL339GL340GL362GL363GL364GL365

SMO Sample No.

GL341GL342GL368

t

SMO Sample No.

GL339GL340GL362GL363GL364

SMO Sample No.

GL341GL342GL368GL369

VOLATILES(SOIL)

EPA Sample No. SMO Sample

ISXP8101 GL370ISXP8102 GL371ISXP8103 GL367ISXP8103D

SEMIVOLATILES(WATER)


ISXP8001 GL366•'•••• ISXP8001D GL344.. ISXP8002 GL345ISXP8003ISXP8004ISXP8005

SEMIVOLATILES(SOIL)


ISXP8101 GL369ISXP8102 GL370ISXP8103 GL371

PESTICIDES /PCBs(WATER)


ISXP8001 GL365ISXP8001D GL366ISXP8002 GL344ISXP8003 GL346ISXP8004

PESTICIDES /PCBs(SOIL)


ISXP8101 GL370ISXP8102 GL371ISXP8103ISXP8103D

No. EPA Sample

ISXP8104ISXP8105ISXP8108F

No. EPA Sample

ISXP8008FISXP8109FISXP8927P

No. EPA Sample

ISXP8103DISXP8104ISXP8105

No. EPA Sample

ISXP8005ISXP8008FISXP8109FISXP8928P

No. EPA Sample

ISXP8104ISXP8105

No

No

No

No

No,

GENERAL

This data review assignment covers 11 WATER and 7 SOIL samplesanalyzed for VOLATILES; 9 WATER and 6 SOIL samples analyzed forSEMIVOLATILES: and 9 WATER and 6 SOIL samples analyzed forPESTICIDES/PCBs for Case number 16873. For the volatiles, therewere five field blanks (including trip and rinsate), six methodblanks, two field duplicates, and one performance evaluation sampleincluded with this assignment. For the semivolatiles, there weretwo field blanks, five method blanks, two field duplicates, and oneperformance evaluation sample included with this assignment. Forthe pesticides/PCBs, there was two field blanks, two fieldduplicates, one performance evaluation sample, four method blanks,and six instrument blanks included with this assignment.

1. Holding Times and Preservation

Volatiles;

Several water samples exceeded the specified Aromatic holdingtimes for volatiles by 2 days or less but no qualification wasrequired. No holding times have been established for soil samples.

Semivolatiles;

Two water samples exceeded extraction holding times by two daysor less but no qualification was required. Analysis of the watersfor semivolatiles was completed within the specified time limit. Noholding times have been established for soil samples.

Pesticides/"PCBs:

Two water samples exceeded extraction holding times by two daysor less but no qualification was required. Analysis of the waterswas completed within the specified time limit. No holding timeshave been 'established for soil samples.

2. GC/MS Tuning

All relative ion abundances were within the established controllimits.

3. initial and Continuing Calibration

Volatiles;

All %RSD's were within control limits on the initialcalibration. All RRF values were within control limits on both theinitial and continuing calibrations. %D was out of control forChloromethane, Chloroethane, Acetone, 2-Butanone,Dibromochloromethane, and Bromoform. Since associated data wereeither non-detect or qualified by other rules, no data werequalified by the volatile continuing calibrations.

Semivolatiles;

All %RSD's were withiofi' control limits on the initial

calibrations. All RRF values were within control limits on both theinitial and continuing calibrations.%D was out of control forHexachlorocyclopentadiene, 2-Methylphenol, 2,2'-Oxybis(l-Chloropropane), N-Nitroso-Dipropylamine, 4-Nitrophenol, Carbazole,3-Nitroaniline, 2,4-Dinitrophenol, 4-Nitroaniline, 4,6-Dinitro-2-Methylphenol, N-Nitrosodiphenylamine, and Bis(2-Ethylhexyl)Phthalate. As a result, the following samples were J-coded: ISXP8102S, ISXP8102W, ISXP8104S, and ISXP8104W for N-Nitroso-Dipropylamine; ISXP8102S, ISXP8102W, ISXP8104S, andISXP8104W for 4-Nitrophenol; ISXP8103, ISXP8103D, ISXP8104,ISXP8104S, and ISXP8104W for Carbazole.

Pesticides/PCBs;

All samples were within quality control limit requirements forretention time windows and percent relative standard deviation onthe initial calibration. All samples were within quality controllimit requirements 'for analytical sequence and relative percentdifference on the continuing calibration. Almost every sample hadcompounds that did not meet quality control limit requirements forpercent difference between the concentrations between columns(quantitation column within 25% of confirmation column). Since allcompounds were less than the contract required quantitation limit(CRQL), no data were qualified.

4. GC/ECD Instrument Performance

The pesticide resolution check mixture was within qualitycontrol limit requirements. The pesticide performance evaluationcheck was within quality control limit requirements for retentiontime windows, relative percent difference of the performanceevaluation mixtures and individual mixes, and percent breakdown ofEndrin and 4,4'-DDT.

5. Internal Standard Response

Volatiles;

Sample ISXP8102 and its reanalysis were outside of controllimits (high) for Chlorobenzene. Since all compounds quantitatedfrom Chlorobenzene were non-detect for this sample, no qualificationwas necessary.

Semivolatiles;

Sample ISXP8103 and the diluted analysis were outside ofcontrol limits (low) for Acenaphthene-dlO and Phenanthrene-dlO(original analyses only), Crysene-dl2 and Perylene-12. As a result,all positive compound results quantitated from Crysene-dl2 andPerylene-dl2 were J-coded for that sample. Sample ISXP8103D and thediluted analysis were outside of control limits for Acenaphthene-dlOand Phenanthrene-dlO (original analyses only), Crysene-dl2 andPerylene-12. As a result, all positive compound results quantitatedfrom Acenaphthene-dlO, Phenanthrene-dlO, Crysene-dl2, and Perylene-d!2 were J-coded for that sample. Samples ISXP8104, ISXP8104S, andISXP8104W were outside of control limits (low) for Acenaphthene-dlO,Phenanthrene-dlO, Crysene-di2, and Perylene-dl2. These samples were

not reanalyzed. As a result, all positive compound resultsquantitated from Acenaphthene-dlO, Phenanthrene-dlO, Crysene-dl2,and Perylene-dl2 were J-coded for those samples. Samples ISXP8102,ISXP8102S, and ISXP8102W were outside of control limits (low) forPerylene-dl2. These samples were not reanalyzed. As a result, allpositive compound results quantitated from Perylene were J-coded forthose samples.

5. Pesticide Clean-up Checks

The percent recoveries for the florisil cartridge were withinquality control limit requirements with the exception of Endrin. Nodata were qualified.

6. Blanks

Volatiles:

Methylene Chloride was found in two of the water method blanksat levels below the CRQL. No samples were qualified as a result ofmethod blank contamination. Methylene Chloride, Acetone, andToluene were found in the water field blanks, qualifying samplesISXP8006F, ISXP8009F, and ISXP8926P with a U-code for Acetone.Acetone in the soil field blank (ISXP8108F) qualified samplesISXP8101, ISXP8102, ISXP8103D, ISXP8104, ISXP8105, ISXP8104S, andISXP8104W with a U-code.

Semivolatiles:

Bis(2-Ethylhexyl)Phthalate was found in two of the soil methodblanks, qualifying samples ISXP8103D and ISXP8104 with a U-code forthat compound. Diethylphthalate, Bis(2-Ethylhexyl)Phthalate, andDi-N-Butylphthalate were found in the water field blanks, qualifyingsample ISXP8001D with a U-code for Bis(2-Ethylhexyl)Phthalate.

Pesticides/PCBs;

All four method blanks were free of contamination. Allinstrument blanks were free of contamination.

7. Surrogate Recovery

Volatiles;

Surrogate compound recoveries were outside control limits (low)for l,2-Dichloroethane-d4 in sample ISXP8102. Upon reanalysis ofthe sample, all surrogate compound recoveries were within controllimits. There was no qualification of sample data based on thereanalysis results.

Semivolatilesi

Surrogate compound recoveries for 2-Fluorobiphenyl and 2,4,6-Tribromophenol were above control limits in several samples.However, no samples were qualified.

Pesticides/PCBs^*

Surrogate compound recoveries for both Tetrachloro-m-Xylene andDecachlorobiphenyl were below control limits in several samples.Surrogate compound recoveries for Tetrachloro-m-Xylene was abovecontrol limits in the dilution of one sample. Surrogate compoundrecoveries for Decachlorobiphenyl were 0% recovery in severalsamples. As a result of these outliers, all positive results forsamples ISXP8001, ISXP8001D, ISXP8004, ISXP8005, ISXP8109F,ISXP8101, ISXP8102, ISXP8104, ISXP8104S, ISXP8104W, and ISXP8105were J-coded; the high concentrations of some analytes seen in manysoil samples should be seen as lower estimates of the trueconcentrations. All non-detect values for these samples should beviewed as estimated detection limits.

8. Matrix spike/Matrix Splice Duplicate Recovery

Volatiles:

The Matrix spike/Matrix spike duplicate recoveries for bothmatrices were within control limits. All RPDs for both matriceswere within control limits. Contamination of Acetone in the waterMS/MSD; and Methylene Chloride, Acetone, and 2-Butanone in the soilMS/MSD did not result in the gualification of any sample data. Notethat for LAST purposes, the MS and MSD are listed as ISXP8001S andISXP8001W, even though they originated from sample ISXP8001D.

Semivolatiles;

The Matrix spike/Matrix spike duplicate recoveries were out ofcontrol for one compound in the water matrix. The MS/MSD recoverieswere out of control for two compounds in the medium-level soilmatrix, and out of control for one compound in the low-level soilmatrix. The RPD for the water matrix was within control limits,while both level soil matrix MSD's each had one RPD out of controllimits. Ho samples were qualified based on MS/MSD recoveries orRPD's. Note that for LAST purposes, the MS and MSD for the watermatrix are listed as ISXP8001S and ISXP8001W, even though theyoriginated from sample ISXP8001D.

Pesticides/PCBs:

The Matrix spike/Matrix spike duplicate recoveries were out ofcontrol for three compounds in the water matrix. The Matrixspike/Matrix spike duplicate recoveries were out of control for tencompounds in the soil matrix. The RPDs for both the water and soilmatrices were within control limits. No samples were qualifiedbased on MS/MSD recoveries. Note that for LAST purposes, the MS andMSD for the water matrix are listed as ISXP8001S and ISXP8001W, eventhough they originated from sample ISXP8001D.

9. Performance Evaluation Sample

Volatiles;

Recovery of spiked analytes was very good. Acetone, which wasalso present in one of the/.field blanks, was the only additional

compound found in the performance sample. No data were qualifiedbased on performance evaluation sample recoveries.

Semivolatiles;

Recovery of spiked analytes was very poor. None of the targetanalytes were recovered from the performance sample. The reason forno recovery is thought to exist in the performance spiking solution,as similar results (no recovery) were obtained from two otherperformance samples unrelated to this project. As a result, thespiking solution is no longer being used in performance evaluation.

Pesticides/PCBs:

Recovery of spiked analytes was very poor. None of the targetanalytes were recovered from the performance sample. The reason forno recovery is unknown.

10. Duplicates

Volatiles;

Good agreement existed between the duplicates in both matricesand their respective original samples.

Semivolatiles;

Good agreement existed between the duplicates in both matricesand their respective original samples. However, two phthalates weredetected in sample ISXP8001D that were not detected in the originalsample. Additionally, a phthalate was reported in sample ISXP8103which was not present in the duplicate.

Pesticides/PCBs;

Good 'agreement existed between the duplicates in both matricesand their respective original samples. Note that Endrin wasdetected in the duplicate of ISXP8003, but just below the CRQL.

11. Compound Identification and Quantitation

Due to the requested review level, results listed on thesummary forms were used for the review. These results were notchecked against the raw data for accuracy, and calculations were notverified. All positive results found below the CRQL were raised tothe CRQL and coded U. Samples ISXP8104S and ISXP8104W in theSemivolatiles, which exceeded the calibration range of theinstrument for Fluoranthene, were not diluted and reanalyzed. Hadthe samples not been qualified for other QC outliers, they wouldhave been J-coded.

12. summary

Volatiles:

The lab was instructed to analyze the water and soil samplesfor VOA analytes. Calibration outliers were found for many

compounds, however, sample results were either non-detect or werequalified by other rules. Methylene Chloride was found in two ofthe three water method blanks, but since samples were non-detect forthis compound, no coding was necessary. All soil method blanks werefree of contamination. Field blank contamination resulted in thequalification of three water samples for one compound, and sevensoil samples for one compound. Poor internal standard compoundrecovery in a sample and its reanalysis did not result in any sampledata qualification since no quantitated compounds were affected.All other QC was acceptable.

Semivolatiles;

The lab was instructed to analyze the water and soil samplesfor Semivolatiles analytes. Calibration outliers were found formany compounds, resulting in data for seven soil samples being J-coded. One common laboratory contaminant was found in two of thethree soil method blanks and three common laboratory contaminantswere found in both vof the water field blanks, qualifying threesamples with a U-code for Bis(2-Ethylhexyl)Phthalate. All watermethod blanks were free of contamination. Poor surrogate compoundrecovery did not result in the qualification of any positive sampledata. Poor internal standard compound recovery in eight samples(six of which were not reanalyzed) resulted in the qualification ofall positive sample data which were quantitated from those internalstandard compounds that were out of control with a J-code. Allother QC was acceptable.

Pesticides/PCBs:

All quality-control limit requirements were met for bothinitial and continuing calibrations. All instrument performancechecks met quality control limit requirements except for onecompound in the clean-up check, but that outlier did not result inthe qualification of any sample data. All blanks were free ofcontaminafion. Severe surrogate recovery outliers led to thequalification of all positive results with a J-code for twelvesamples. All other QC was acceptable.

S P F D

ANALYSIS REQUEST REPORT

FOR ACTIVITY: ISXP8

10/10/91 16:08:b2

PRELIMINARY DATASUBJECT TO REVISION

ALL REAL SAMPLES AND FIELD .Q.C.

* LABO APPROVED

FY: 91 ACTIVITY: ISXP8

LABO DUE DATE IS 10/ 1/91.

INSPECTION DATE: 8/ 1/91

DESCRIPTION: MISSISSIPPI RIVfR POOL #15 LOCATION: DAVENPORT

STATUS: ACTIVE TYPE: SAMPLING - CONTRACT LAB ANALYSIS ' PROJECT:

REPORT DUE DATE IS 10/15/91.

ALL SAMPLES RECEIVED DATE: 08/02/91

IOWA

A41

..ALL DATA APPROVED BY LABO DATE: .10/10/91^ •»

"EXPECTED LABO TURNAROUND TIME IS 60 DAYS

ACTUAL LABO 1URWAROUMD TIME IS 69 DAYS

FINAL REPORT TRANSMITTED DATE: 00/00/00

EXPECTED REPORT TURNAROUND TIME IS 75 DAYS

ACTUAL REPORT TURNAROUND TIME IS 0 DAYS

SAMP.NO.

001001on 900300400500600800910110210.?i fi.'i1041 Ob108109

QCC

D

FFF

D

FF

M

WWWWWWWWWSSss5SSW

DESCRIPTION

MISS.MISS.MISS.MISS.MISS.MISS.MISS.MISS.MISS.MISS.MISSMISS|,Jt T £. C.

MISS.MISS.MISS.MISS.

RIVER POOLRIVER POOLPTI/FP POOL

RIVER POOLRIVER POOLRIVER POOLRIVER POOLRIVER POOLRIVER POOLRIVER POOLRIVER POOLRIVER POOLD j ii PD nnf'iRIVER POOLRIVER POOLRIVER POOLRIVER POOL

015-OUTFALL 001ii 15-OUTFALL 001//15-OUTFALL 002,#15-OUTFALL 003015-OUTFALL 004/H5-OUTFALL 005//15-VOA TRIP BLANK//15-FIELD BLANK415-WATER TRIP BLANK015-OUTFALL 001«15-OUTFALL 002H15-OUTFALL 003//15-OUTFALL 003«lF.-riUTFAI 1. 00')//15-OUTFALL 005//15-SOIL TRIP BLA/ /15-WATER RIMSATE

SAMPLESTATUS

11

IAIJS 1111

; 11WK. 1

1i1•,11

OK 1BLK 1

aCONT. CITY

4444441415£555514

RIVERDALERIVERDALERIVERDALtRIVERDALERIVERDALERIVERDALERIVERDALERIVERDALERIVERDALERIVERDALERIVERDALERIVFRDALERIVERDALERIVERDALERIVERDALERIVERDALERIVERDALE

STATE

IOWAIOWAIOWAIOWAIOWAIOWAIOWAIOWAIOWAIOWAIOWAIOWAIOWAIOWAIOWAIOWAIOWA

AIRS/STORETLOC NO

BEG.DATE

07/31/9107/31/9108/01/9108/01/91OS/01/9108/01/9108/01/9108/01/9107/31/9107/31/9107/31/9107/31/9107/31/9107/31/9107/31/9108/01/9107/31/91

BEG.TIME

10:501 0 : B509 '. 0509:2011: 1010:1014:101 1 : 3018:151 3 : 5015: 'IS1 5 ' A 515: '151 6 : 3017:1014:0016:45

END.DATE

END.TIME

EXPLANATION! OF CODES AND INFORMATION ON ANALYSIS REQUEST DETAIL REPORT

SAMPLE INFORMATION:

SAMP. NO. = SAMPLE IDENTIFICATION NUMBER (A 3-DIGIT NUMBERWHICH IN COMBINATION WITH THE ACTIVITY NUMBERAND QCC, PROVIDES AN UNIQUE NUMBER FOR EACH SAMPLEFOR IDENTIFICATION PURPOSES)

QCC = QUALITY CONTROL CODE I A ONE-LETTER CODE USED TODESIGNATE SPECIFIC QC SAMPLES. THIS FIELD WILL BEBLANK FOR ALL NON-QC OR ACTUAL SAMPLES):A = TRUE VALUE FOR CALIBRATION STANDARDB = CONCENTRATION RESULTING FROM DUPLICATE LAB SPIKEC = MEASURED VALUE FOR CALIBRATION STANDARDD = MEASURED VALUE FOR FILED DUPLICATEF = MEASURED VALUE FOR FIELD BLANK ;

G = MEASURED VALUE FOR METHOD STANDARDH = TRUE VALUE FOR METHOD STANDARDK = CONCENTRATION RESULTING FROM DUPLICATE FIELD

SPIKEL = MEASURED VALUE FOR LAB DUPLICATEM = MEASURED VALUE FOR LAB BLANKN = MEASURED VALUE FOR DUPLICATE FIELD SPIKEP = MEASURED VALUE FOR PERFORMANCE STANDARDR = CONCENTRATION RESULTING FROM LAB SPIKES = MEASURED VALUE FOR LAB SPIKET = TRUE VALUE OF PERFORMANCE STANDARDW = MEASURED VALUE FOR DUPLICATE LAB SPIKEY = MEASURED VALUE FOR.FIELD SPIKEZ = CONCENTRATION RESULTING FROM FIELD SPIKE

M = MEDIA CODE (A ONE-LETTER CODE DESIGNATING THEMEDIA OF THE SAMPLE):A = AIRH = OTHER (DOES NOT FIT ANY OTHER CATEGORY)S = SOLID (SOIL. SEDIMENT. SLUDGE)T = TISSUE (PLANT & ANIMAL)W = WATER (GROUND WATER. SURFACE WATER. WASTE

WATER, DRINKING WATER)DESCRIPTION = A SHORT DESCRIPTION OF THE LOCATION WHERE SAMPLE

WAS COLLECTEDAIRS/STORET LOC. NO. = THE SPECIFIC LOCATION IDENTIFICATION

NUMBER FOR EITHER OF THESE NATIONALDATABASE SYSTEMS, AS APPROPRIATE

DATE/TIME INFORMATION = SPECIFIC INFORMATION REGARDING WHEN THESAMPLE WAS COLLECTEDBEG DATE = DATE SAMPLING WAS STARTEDBEG. TIME = TIME SAMPLING WAS STARTEDEND DATE - DATE SAMPLING WAS COMPLETEDEND TIME = TIME SAMPLING WAS COMPLETEDNOTE: A GRAB SAMPLE WILL CONTAIN ONLY

BEG. DATE/TIMEA TIMED COMPOSITE SAMPLE WILLCONTAIN BOTH BEG AND END DATE/TIMETO DESIGNATE DURATION OF SAMPLECOLLECTION

ANALYTICAL RESULTS/MEASUREMENTS INFORMATION:

COMPOUND = MGP (MEDIA-GROUP-PARAMETER) CODE AND NAME OFTHE MEASURED CONSTITUENT OR CHARACTERISTICOF EACH SAMPLE

UNITS = SPECIFIC UNITS IN WHICH RESULTS ARE REPORTED:C = CCtJTIGRADC (CELSIUS) DEGRtcSCFS = CUBIC FEET PER SECONDGPM = GALLONS PER MINUTEIN = INCHESI.D. = SPECIES IDENTIFICATIONKG -•• = KILOGRAML = LITERLB = POUNDSMG =.MILLIGRAMS (1 X 10-3 GRAMS)MGD ; = MILLION GALLONS PER DAYMPH = MILES PER HOURMV = MILLIVOLTM/F = MALE/FEMALEM2 = SQUARE METERM3 = CUBIC METERNA = NOT APPLICABLENG = NANOGRAMS (1 X 10-9 GRAMS)NTU = NEPHELOMETRTC. TURBIDITY UNITSPC/L = PICO (1 X 10-12.) TUPRIES PER LITE1?PG = PICOGRAMS (1 X 10-12 GRAMS)P/CM2 = PICOGRAMS PER SQUARE CENTIMETERSCM = STANDARD CUBIC METER (1 ATM, 25 C)SQ FT = SQUARE FEETSU = STANDARD UNITS (PH)UG = MICROGRAMS (1 X 10-6 GRAMS)UMHOS = MICROMHOS/CM (CONDUCTIVITY UNITS)U/CC2 = MICROGRAMS PER 100 SQUARE

CENTIMETERSU/CM2 = MICROGRAMS PER SQUARF CENTIMETER1000G = 1000 GALLONS+/- = POSITIVE/NEGATIVE# = NUMBER

DATA QUALIFIERS = SPECIFIC CODES USED IN CONJUNCTIONWITH DATA VALUES TO PROVIDE ADDITIONALINFORMATION ON THE REPORTED RESULTS. OR USEDTO EXPLAIN THE ABSENCE OF A SPCIFIC VALUE:BLANK = IF FIELD IS BLANK. NO REMARKS OR

QUALIFIERS ARE PERTINENT. FOR FIN A LREPORTED DATA. THIS MEAMS THAT THEvALUEs HAVE BEEN REVIEWED AND FOUNDTO BE ACCEPTABLE FOR USE.

I = INVALID SAMPLE/DATA - VALUE WOT REPORTEDj = DATA REPORTED BUT NOT VALID BY APPROVED

QC PROCEDURESK = ACTUAL VALUE OF SAMPLE IS < VALUE REPORTEDL = ACTUAL VALUE OF SAMPLE IS > VALUE REPORTEDM = DETECTED BUT BELOW THE LEVEL OF REPORTED

VALUE FOR ACCURATE QUANTIFICATION0 = PARAMETER NOT ANALYZEDU = ACTUAL VALUE OF SAMPLE IS < THE

MEASUREMENT DETECTION LIMIT (REPORTEDVALUE)

ANALYSIS REQUEST DETAIL REPORT ACTIVITY: 1-ISXP8 PRELIMINARY DATASUBJECT TO REVISION

COMPOUND UNITS 001 0010 002 003 004

WM01 SILVER BY ICAP

WM02 ALUMINUM, TOTAL. BY ICAP

WM03 ARSENIC. TOTAL, BY ICAP

WM04 BARIUM, TOTAL, BY ICAP

WM05 BERYLLIUM. TOTAL, BY ICAP

WM06 CADMIUM. TOTAL. BY ICAP

WM07 COBALT, TOTAL, BY ICAP

WM08 CHROMIUM, TOTAL. BY ICAP

WMO9 COPPER. TOTAL, BY ICAP

WM10 IRON. TOTAL, BY ICAP

WM11 MANGANESE, TOTAL. BY ICAP

WM12 MOLYBDENUM BY ICAP

WM13 NICKEL BY ICAP

WM14 LEAD. TOTAL. BY ICAP

WM15 ANTIMONY, TOTAL. BY ICAP

WM16 SELENIUM BY ICAP

WM17 TITANIUM BY ICAP

WM18 THALLIUM BY ICAP

WM19 VANADIUM BY ICAP

l\'M?0 I?UJO BY ICAP

WK21 CALCIUM. TOTAL BY Ii'.AP

WM22 MAGNESIUM. TOTAL BY ICAP

WM23 SODIUM. TOTAL BY ICAP

WM24 POTASSIUM, TOTAL BY ICAP

WM34 MERCURY BY COLD VAPOR AA

WP17 PCB-1016

:. UG/l.

••UG/L

:UG/L

:UG/L:.UG/L

:UG/L

:UG/L

•UG/L

:UG/L

•UG/L

•UG/L

: UG/L

•'UG/L

•UG/L

!UG/L

:UG/L

: UG/L

:UG/L

:UG/L

•UG/L

•MG/L

!MG/L:MG/L

:MG/L

:UG/L

;UG/L

• 10

•420

: 10

:200

Is.o\5.0

•so!lO

:25

M200

:430

':N/A

:40

\4.8

•60

:5.0

•N/A

: 10

^50

: 32

^53

: 15

•41

•5.0

•0.20

:1 .0

u

U

U

uuuuu

0

uuuu0

uu

uuu

:'10

•420

: 10

:200

':5.0

•5.0:.50

: 10

:25

: 1200

•430

:N/A

•40

^5.2

•60

•5.0

•N/A

: 10

•50

•33

•53

: 15

•40:5.0

•0.20

•1.0

U

U

U

U

U

U

U

u

0

uuuu0

uu

uuu

•1C

.:230

MO

:200

:5.0

'•5.0'

•50

: 10

:25

:370

•250

iN/A

':40:3 0

:60

•5.0

:N/A

: 10

•50

^20

'.73

•32

^20

•5.0

: 0 . 20

':1.0

u

U

U

uuuuu

0

uuuu0

uuu

uuu

" C

1200

10

200

5.0

5.0

50

10

25

250

60

N/A

40

3.0

60

5.0

N/A

10

50

29

60

23

19

5.0

0.20

1 .0

u

U

U

U

U

U

uu

0

uuII

u0

uu

uuu

i 0

: 1 3000

: 10

•200

•5.0:.5.0

:50

•12

^25

: 2600

•500

•N/A

•40:.6.9:60

!5.0

:N/A

•10

•50

••11;67

:22

: 16

'.5.0

•0.20

:1 .0

U

U

U

U

U

u

u

0

uuuu0

uu

uuu


COMPOUND UNITS 001 00 ID 002 003 004

WP18 PCB-1221 -UO/L

WP19 PCB-1232 :UG/L

WP20 PCB-1242 :UG/L

WP21 PCB-1248 :UG/L

WP22 PCB-1254 : UG/L

WP23 PCB-1260 :UG/L

WS01 PHENOL :UG/L

WS03 ETHER, BIS(2-CHLOROETHYL) . BY GC/MS \ UG/L

W-S04 2-CHLOROPHENOL : UG/L

WS05 1 ,3-DICHLOROBENZENE : UG/L

W50G 1 ,4-DICHLOROBENZENE :UG/L

WS07 BENZYL ALCOHOL : UG/L

WS08 1 .2-DICHLOROBENZENE : UG/L

WS09 2-METHYLPHENOL (0-CRESOL) :UG/L

WS10 ETHER. BIS(2-CHLOROISOPROPYL). BY GC/MS':UG/L

WS11 4-METHYLPHENOL IP-CRESOL) :UG/L

WS12 N-NITROSO-DIPROPYLAMINE : UG/L

WS13 HEXACHLOROETHANE.BY GC/MS :UG/L

WS14 NITROBENZENE ': UG/L

Wf,15 rc.OPHORON/E.BV GC/MS :UG./L

V.'SIG 2-NITROPHENOL : UG/L

WS17 2 .4-D1METHYLPHENOL : UG/L

WS18 BENZOIC ACID. BY GC/MS : UG/L

WS19 METHANE, BISC2-CHLOROETHYOXY) . BY GC/MS^UG/L

WS20 2.4-DICHLOROPHENOL :UG/L

WS21 1 ,2.4-TRICHLOROBENZENE :.UG/L

1.0 U

2.0 U

1 .0 U

1.0 ,- U

1 .0 U

1 .0 U

10 U

10 U

10 U

10 U

10 U

N/A 0

10 U

10 U

N/A 0

10 U

10 U

10 U

10 U

10 IJ

10 U

10 U

N/A 0

10 U

10 U

10 U

1.0 U

2.0 U

1.0 U

1.0 U

1.0 U

1 .0 U

10 U

10 U

10 U

10 U

10 U

N/A 0

10 U

10 U

': N/A 0

: 10 U

: 10 U

•10 U

• 10 U

•1C U

•10 U

: 10 U

•N/A 0

MO U

• 10 U

•10 U

1 . G U '.

2.0 U

1.0 U

1 .0 U

1.0 U

1 .0 U

10 U

10 U

10 U

10 U

10 U

N/A 0

10 U

10 U

N/A 0

10 U

10 U

10 U

10 U

'.W iJ

10 U

10 U

N/A 0

10 U

10 U

10 U

" . 0 u .

2.0 U

1.0 U

1.0 U

1 .0 U

1 .0 U

10 U

10 U

10 U

10 U

10 LI

N/A 0

10 U

10 U

N/A 0

10 U

10 U

10 U

10 IJ

10 U

1 0 U

10 U

N/A 0

10 U

10 U

10 U

1.0 u

2.0 U

1 .0 U

1 .0 U

1 .0 U

1.0 U

10 U

10 U

10 U

10 U

10 U

N/A 0

10 U

10 U

M/A ij

10 U

10 U

10 U

10 U

i 0 i '

iG i.i

1 0 U

N/A 0

10 U

10 U

10 U


COMPOUND UNITS 001 0010 002 003 004

W522 NAPHTHALENE

WS23 4-CHLOROANILINE

WS24 HEXACHLOROBUTADIENE.BY GC/MS

WS25 4-CHLORO-3-METHYLPHENOL

WS26 2-METHYLNAPHTHALENE

WS27 HEXACHLOROCYCLOPENTADIENE.BY GC/MS

WS28 2.4.6-TRICHLOROPHENOL

WS29 2.4.5-TRICHLOROPHENOL

MJG/L

••UG/L

•UG/L

•UG/L

•UG/L

:UG/L

iUG/L

:UG/L

W530 2-CHLORONAPHTHALENE \ UG/L

WS31 2-NITROANILINE (ORTHO NITROANILINE )

WS32 PHTHALATE. DIMETHYL. BY GC/MS

WS33 ACENAPHTHYLENE. BY GC/MS

WS34 3-N1TROANILINE

WS35 ACENAPHTHENE. BY GC/MS

WS36 2,4-DIUITROPHENOL

WS37 4-WITROPHENOL

•UG/L

•UG/L

•UG/L

:UG/L

•.UG/L

: UG/L

•UG/L

WS38 DIBENZOFURAN • UG/L

WS39 2.4-DINITROTOLUENE !UG/L

WS40 2,6-DINITROTOLUENE ! UG/L

WS-11 PHTHALATE. DIETHYL. BY GC/MS

WS42 4-CHLOROPHENYL PHEWYL ETHER

WS'13 FLUORENE.BY GC/MS

WS-14 4-NITROAN1LINE

WS45 4.6-DIWITRO-2-METHYLPHENOL

•UG/L

•UG/L

• UG/L

•UG/L

•UG/L

WS46 N-WITROSODIPHENYLAMINE :UG/L

WS47 4-BROMOPHENYL PHENYL ETHER •UG/L

10

10

10

10

10

10

10

25

10

25

10

10

25

10

25

25

10

10

10

10

10

10

25

25

10

10

ij

U

uuuuuuuuuuuuuuuuuuuuuuuu

i o: 10: 10

•10

•10

• 10

ho':25

ho

;25: 10

•10:.25

': 10

•25

:25

• 10

': 10

: 10

: 10

: 10

•10

25

25

10

10

1 1

U

U

uuuuuuuuuuuuuuuuIJuuuuuu

10

10

10

10

10

10

10

25

10

25

10

10

25

10

25

25

10

10

10

10

10

10

25

25

10

10

U

U

uuuuuIJuuuuuuuuuuuu

uuuuuu

. 1 0

: 10

ho•10

: 10

': 10:10

:25

:10

:25 .: 10

•10

:25

•10

•25

:25

! 10: 10

: 10

: 10

: 10: 10

^25

^25

•10

': 10

L'

U

uuuuuuuIJ

Vuuu11

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i 0

10

10

10

10

10

10

25

10

25

10

10

25

10

25

25

10

10

10

(1 : 'i 0

J : i 0

U '. 1 0

U :25

U :25

U -10

U : 10

u

U

U

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I.I

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-I.I

uuuuu


COMPOUND UNITS 001 001D 002 003 004

WS-18 HEXACHLORGBEMZENE.BY iif./MS

WS49 PENTACHLOROPHENOL

WS50 PHENANTHRENE

WS51 ANTHRACENE, BY GC/MS

WS52 PHTHALATE. DI-N-BUTYL-. BY GC/MS

WS53 FLUORAMTHENE.BY GC/MS

WS54 PYRENE

WS55 PHTHALATE, BUTYL BEN2YL

US66 3.3'-DICHLOROBENZIDINE

WS57 ANTHRACENE. BEWZOiAi. BY GC/MS

WS58 PHTHALATE. BISi 2-ETHYLHEXYL J . BY GC/MS

WS59 CHRYSENE, BY GC/MS

WS60 PHTHALATE, DI-N-OCTYL-. BY GC/MS

WS61 FLUORANTHENE. BENZO(B), BY GC/MS

WS62 FLUORAMTHEME. BENZSGi K.) . BY GC/MS

WSG3 PYRENE, BENZGiA;, BY GC/MS

WS64 INDENOl 1 . 2 . 3-CD JPYRENE

WS65 ANTHRACENE. DI BENZOI A . H) . BY GC/MS

WS66 PERYLENE. BENZOI G.H. I ). BY GC/MS

Wf,r,7 riRRATvii.r

WV03 CiiLCRGWETHrtl-jC . BV i'v-.-MS.

WVO'i BROMGMt THANE . BY GC/MS

WVOb V J N Y L CHLORIDE

WV06 CHLOROETHANE, BY GC/MS

WV07 METHYLENE CHLORIDE

WV08 1 . 1-DICHLOROETHENE

• i if;/!. ^

:UG/L

: UG/L

•UG/L

: UG/L

:UG/L

: UG/L

:UG/L

•UG/L

:UG/L

•UG/L

•UG/L

: UG/L

•UG/L: UG/L

: UG/L

•UG/L

10

25

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

'UG/L -10

•UG/L ho

JJC/L : 10

in1, /i. •. in

•HG/L :10

•UG/L -10

•UG/L :10

•UG/L :10

•UG/L -10

M

uuuuuuuuuuuuuuuuuuij

IJ

uuuuu

• 10:25

: 10

MO

:10

:10

•10

': 15

: 10

: 10

• 1 1

•10

•!io•10

: 10

•10

: 10:. 10:10: 10

•1C

•10:. 10

•10

: 10

•10

uuuuuuu

uuu

uuuuuuuIJuuuuuuu

10

25

10 .

10

10 , v10

10

10

10

10

10

10

10

1.0

10

10

10

10

10

10

10

10

uuuuuuuuuuuuuuuuuuuLI

uIJ

240

10

10

10

uuu

1C

25

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

10

uuuuuu0

uuuuIJuuI)uuuuuuu

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':10

•25

ho;. 10:. 10:. 10:. 10

•10

ho

: 10

•10

•10

ho

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: 10

•10

•TO

•10

:10

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; 10•10

•10

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• 10

•10

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WV09 1 . 1-DICHLOROETHANE . mVU

WV10 1 .2-DICHLOROETHENE. TOTAL i UG/L

WV11 CHLOROFORM, BY GC/MS : UG/L

WV12 1 ,2-DICHLOROETHANE :UG/L

WV13 1 ,1 .1-TRICHLOROETHANE • : UG/L

WV14 CARBON TETRACHLORIDE . BY GC/MS : UG/L

WV15 BROMODICHLOROMETHANE. BY GC/MS !uG/L

WV16 1 .2-DICHLOROPROPANE '.UG/L

•ti\n7 BENZENE, BY GC/MS ': UG/L

WV19 TRICHLOROETHENE :UG/L

WV20 DICHLORGPROPENE. CIS-1.3-, BY GC/MS :UG/L

WV21 DIBROMOCHLOROMETHANE. BY GC/MS : UG/L

WV22 1 , 1 .2-TRICHLOROETHANE : UG/L

WV24 BROMOFORM, BY GC/MS ': UG/L

WV25 TETRACHLOROETHEME :LUVL

WV26 TOLUENE ;. UG/L

WV27 1 . 1 ,2,2-TETRACHLOROETHANE ': UG/L

WV28 CHLOROBEN2ENE. BY GC/MS : UG/L

WV29 ETHYL BEN2ENE . BY GC/MS ': UG/L

WV30 ACETONE. BY GC/MS :l.i:.-.."_

WV31 CARBON DISULfTRE. BY dr. /MS :U '.>/!.

WV32 2-BUTANONE : llf./L

WV33 VINYL ACETATE : UG/L

WV34 2-HEXANONE • UG/L

WV35 4-METHYL-2-PENTANONE : UG/L

WV36 STYRENE ! UG/L

in i.i

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

. •> M j ;I ','

1 0 '-'

•"10 i.i

: M/A 0

: 10 U

•10 U

: 10 U

10 I1

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

U

1C 'J

; 10 I!

; N/A 0

: 10 U

•10 U

•10 U

10 U

1600

10 U

10 U

10 • U

10 U

10 U

10 U

10 U

190

10 U

10 U

10 U

10 U

2800

10 U

10 U

: 10 U

: 10 U

: 10 U

:o u': 1 0 'J

: N/A 0

,: 1 o . u: 10 U

: 10 U

10 U

86

44

10 U

10 U

10 U

10 U

10 U

10 U

4R

10 U

10 U

10 U

10 U

160

10 U

10 U

: 10 U

: 10 U

•10 U

.'iO U

: 1 0 U

•N/A 0

: 10 U

•10 U

: 10 U

10 U

30

71

10 U

10 U

10 U

10 U

10 U

10 U

12

10 U

10 U

10 U

10 U

35

10 U

10 U

10 U

10 U

10 U

10 U

10 U

N/A 0

10 U

10 U

10 U



WV37

WV40

Z201

2202

XYLENES. TOTAL

TRANS-1 ,3-DICHLOROPROPENE

SAMPLE NUMBER

ACTIVITY CODE

• iif.;/i_ .

•UG/L

:NA

:NA

j 1(?

•10

•001

:ISXP8

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•002

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•004

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COMPOUND UNITS 005 006 F 008F. 009F 101

SM01 SILVER BY I CAP

SM02 ALUMINUM. TOTAL. BY ICAP

SM03 ARSENIC. TOTAL. BY JCAP

SM04 BARIUM. TOTAL, BY ICAP

SM05 BERYLLIUM, TOTAL, BY ICAP

SM06 CADMIUM. TOTAL. BY ICAP

SM07 COBALT. TOTAL. BY ICAP

SM08 CHROMIUM, TOTAL. BY ICAP

S&S9 COPPER, TOTAL. BY ICAP

SM10 IRON, TOTAL, BY 1C.AP

SM11 MANGANESE. TOTAL BY ICAP

SMI 2 MOLYBDENUM BY ICAP

SMI 3 NICKEL BY ICAP

SMI 4 LEAD, TOTAL. BY ICAP

SM15 ANTIMONY, TOTAL. BY ICAP

SM1G SELENIUM BY ICAP

SM17 TITANIUM BY ICAP

SM18 THALLIUM BY ICAP

SMI 9 VANADIUM BY ICAP

SM20 2Ifir BY I CAP

SM21 CALCIUM. TOTAL. BY KAP

SM22 MAGNESIUM. TOTAL. BY ICAP

SM23 SODIUM BY ICAP

SM24 POTASSIUM BY ICAP

SM34 MERCURY BY COLD VAPOR AA

SP17 PCB-1016

•Mr, /krv

: MG/KG:

:MG/KG.

:MG/KG: :.

:MG/KG:

: MG/KG:

: MG/KG:

.MG/KG:

: MG/KG:

: MG/KG:

: MG/KG:

: MG/KG:

: MG/KG:

: MG/KG:

:Mfj/Mj:

: MG/KG:

:MG/KG:

: MG/KG:

: MG/KG:: M'.,. •>->,:

• MI , / 1: i : •

•MG/Kf, !

•MG/KG:

•MG/KG:

: MG/KG ':;UG/KG:

i.: 2. 6

•8300

•2.8

•72

•1.4

•1.4

: 14

: 18

•53

: 1 3000

':260

:N/A

: 18

•39: M/A

•1.4

:N/A

•2.8

•21

'. 110

: 36000

: 1 3000

: 1 400

• 1400

•0.14

•51

U

U

U

U

U

J

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U

U

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COMPOUND UNITS 005 006 F 008 F 009F 101

SP18 PCB-1221

SP19 PC6-1232 :

SP20 PCB-1242

SP21 PCB-1248 !

SP22 PCB-1254 :

SP23 PCB-1260 :

SS01 PHENOL

SS02 CARBAZOLE

•SSO3 ETHER, BIS(2-CHLOROETHYL) , BY GC/MS

SS04 2-CHLOROPHENOL

SS05 1 ,3-DICHLOROBENZENE


SS07 BENZYL ALCOHOL

SS08 1 .2-DICHLOROBENZENE

SSOQ 2-METHYLPHENOL (0-CRESOLJ

SS10 WTHER. BIS(2-CHLOR01SOPROPYL). BY GC/MS

SS11 4-METHYLPHENOL IP-CRESOL)

SS12 N-NITROSO-DIPROPYLAM1WE

SSI 3 HEXACHLOROETHANE.BY GC/MS

SSI 4 NITROBENZENE

SSI 5 1SOPHORONE. BY GC/MS

SSI 6 2-N1TROPHENOL

SSI 7 2.4-D1METHYLPHENOL

SS18 BEMZ01C ACID, BY GC/MS

SS19 METHANE. BIS(2-CHLOROETHYOXY) . BY GC/MS

SS20 2,4-DICHLOROPHENOL

UC-./KG:

UG/KG:

UG/KG:

UG/KG: ;•

UG/KG:

UG/KG:

UG/KG:

UG/KG:

UG/KG:

UG/KG:

UG/KG:

UG/KG:

UG/KG:

UG/KG:

UG/KG :

UG/KG:

UG/KG:

UG/KG:

UG/KG:

UG/I--0:

UG/CG:

•UG/KG:; UG/KG :

: UG/KG :

•UG/KG:

: UG/KG :

'5',

; 100

!51

•940

151

151

•5100

•5500

^5100

: c' 1 00

:5100

•5100

•N/A:.5100

: T-1 GO

IN/ A:5100

•5100

:5100

I-': C'O

: b 'i 00

• :51CO

': ':5100

• !N/A• :5100

: ! 5 1 00

U :

U

U

J

U

U

U

U

U

1,1

U

0

U

i l

0

U

U

U

1 1

I I

U

U

0

U

U



SS21 1 . 2.4-TR1CHLGROBENZENE

SS22 NAPHTHALENE

SS23 4-CHLOROANILINE

SS24 HEXACHLOROBUTADIENE.BY GC/MS

SS25 4-CHLORO-3-METHYLPHENOL

SS26 2-METHYLNAPHTHALENE

SS27 HEXACHLOROCYCLOPENTADIENE.BY GC/MS

SS28 2.4.6-TRICHLOROPHENOL

S£29 2.4,5-TRICHLOROPHENOL

SS3G 2-CHLOROMAPHTHALENE

SS31 2-NITROANILINE

SS32 PHTHALATE. DIMETHYL. BY GC/MS

SS33 ACENAPHTHYLENE, BY GC/MS

SS34 3-NITROANILINE

SS35 ACEKAF-HTHENE . BY GC/MS

3336 2.4-DlNlTRGPH£NuL

SS37 4-NITRGPHENOL

5S38 DIBENZOFURAN

SS39 2.4-DIN1TROTOLUENE

S''-1C) 2 fi-niM!TROTOH''!:''!F

SS-II PiiTiiALATE. DIETV-iVi . 6 1 i-.i'..-'M~,

SS-12 .-i-ilhLORuF'HE'N/L PHENYL El HER

SS43 HLUOREME .(JL/MS

SS44 4-N1TROANILINE

SS45 /1.6-DINITRO-2-METHYLPHENOL

SS46 N-NITROSODIPHENYLAMINE

•MO/KG^

•-UG/KG:

:UG/KG:

: UG/KG.

:UG/KG:

:UG/K.G:

:UG/KG:

:UG/K.G:

:UG/KG:

: uG/K-C:

• UG/KG:

:UG/KG:

:UG/KG:

!UG/KG:

• UG/MJ-

:UG/KG:

:UG/KG.:

•UG/KG:

:UG/KG:

ll'.i.-t-!;-

• I I I - /" I. .

•UG/KG': UG/KG:

: UG/KG :

: UG/KG:

•UG/KG:

: o i 00

^5100

:5100

^5100

15100:.5100

:5100

^5100

: 1 2000

•5100

: 1 2000

•5100

•5100

: 1 2000

:5100

: 1 2000

': 1 2000

^5100:.5100

; 5 1 oo:.5100

•5100

•5100

: 1 2000

: : 1 2000

: :5100

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U


COMPOUND UNITS 005 006 F 008 F' 009 F 101

SS47 4-BRGMOPHEWYL PHENYL ETHER

SS48 HEXACHLOROBENZENE.BY GC/MS

SS49 PENTACHLOROPHENOL

SS50 PHENANTHRENE

SS51 ANTHRACENE, BY GC/MS

SS52 PHTHALATE. DI-N-BUTYL-. BY GC/MS

SS53 FLUORANTHENE.BY GC/MS

SS54 PYRENE

S555 PHTHALATE. BUTYL BENZYL

3556 3.3'-DICHLOROBEN2IDINE

SS57 ANTRACENE. BENZO(A) , BY GC/MS

SS58 PHTHALATE. BIS12-ETHYLHEXYL) , BY GC/MS

SS59 CHRYSENE. BY GC/MS

SS60 PHTHALATE, DI-N-OCTYL-. BY GC/MS

SS61 FLUORANTHEME. BEMZO(B) . BY GC/MS

SS62 FLUORAMTHENE. BENZOvK) . BY GC/MS

SS63 PYRENE, BENZO(AJ. BY GC/MS

SS64 INDEWOl 1 . 2 . 3-CD) PYRENE

SS65 ANTHRACENE. DIBEWZO( A , H) . BY GC/MS

SSee PERYLEME. BEMZOf.G H I>. BY GC/MS

GVG3 CliLOROMETHAME . BY Gf./MS

SV04 BROMOME THANE . BY GC/MS

iVOB VINYL CHLORIDE

SV06 CHLOROETHANE. BY GC/MS

SV07 METHYLENE CHLORIDE

SV08 1 . 1-DICHLOROETHYLENE

•UG/KG.:

•UG/KG:

: UG/KG:

•.UG/KG:

:' UG/KG :

: UG/KG:

: UG/KG :

•UG/KG:

:UG/KG:-

:UG/KG:

: UG/KG :

: UG/KG:

•UG/KG:

: UG/KG:

: UG/KG:

: UG/KU:

•UG/KG:

•UG/KG:

: UG/KG:

: IJG/T-.G:

: UG/KG;

• UG/KG :

•UG/KG:

: UG/KG :

•UG/KG:

: UG/KG :

•: D i 00

^5100

: 1 2000

: 1 9000

':5100

^5100

: 28000

: 26000

•5100

: 5100

: 1 5000

•5100

: 1 9000

•5100: 1 8000

:5100: 1 3000

• 5400

: 5 1 00

. 5500: 15

. 15

880

15

15

15

0

U

U

U

U

U

U

U

U

U

U

l l

II\ I

U

U

U



SV03 1 . 1-D1CHLOROETHANE -iir;/KG :

SV10 TRANS-1 ,2-DICHLOROETHYLENE : UG/KG :

SV11 CHLOROFORM. BY GC/MS : UG/KG:

SV12 1 ,2-DICHLOROETHANE :UG/KG:

SV13 1 .1 .1-TRICHLOROETHANE :UG/KG:

SV14 CARBON TETRACHLORIDE . BY GC/MS \ UG/KG :

SV15 BROMODICHLOROMETHANE , BY GC/MS : UG/KG:

SV16 1 ,2-DICHLOROPROPANE :UG/KG:

"SV17 BENZENE, BY GC/MS : UG/KG:

SV18 TRAMS-i . 3-DICHLOROPROPEWE :UG/KG:

SV1S TRICHLOROETHYLENE -UG/K.G:

SV20 DICHLOROPROPENE. CIS-1,3-. BY GC/MS : UG/KG :

SV21 DIBROMOCHLOROMETHANE, BY GC/MS -UG/K.G:

SV22 1 , 1 ,2-TRICHLOROETHANE : UG/KG :

SV24 BROMOFORM, BY GC/MS iiJG/KG:

SV25 1 . 1 .2,2-TETRACHLGFtOETHENE : UG/KG:

SV26 TOLUENE ': UG/KG .:

SV27 1 . 1 . 2.2-TETRACHLOROETHANE -UG/K.G:

SV28 CHLOROBENZENE, BY GC/MS : UG/KG:

SV29 ETHYL BEMZEME.BY G-"/M? '•.>.'<,"<:'

SV30 ACETOWE. BY GC/MS : '>."'.-. 'f- •: :

SV31 CARBON DISULFIOE. BY bC/MS . : UC,./MV

SV32 2-BUTANONE : UG/KG.

SV33 V7NYL ACETATE : UG/KG:

SV34 2-HEXANONE : UG/KG :

SV35 4-METHYL-2-PENTANONE :' UG/KG :

15 u

15 U

15 U

15 U

15 U

15 U

15 U

15 U

15 U

15 U

15 U

15 U

15 U

15 U

15 U

15 U

15 U

15 U

15 U

1 5 . 1 )

1 7 I I

15 U

15 U

N/A 0

15 U

15 U


COMPOUND UNITS 005 006 F 008 F' 009 F 101

SV36 STYRENE

SV37 XYLENES. TOTAL

WM01 SILVER BY ICAP

WM02 ALUMINIUM. TOTAL, BY ICAP

WM03 ARSENIC. TOTAL, BY ICAP

WM04 BARIUM. TOTAL. BY ICAP

WM05 BERYLLIUM. TOTAL. BY ICAP

WM06 CADMIUM. TOTAL. BY ICAP

Wto€>7 COBALT. TOTAL. BY ICAP

WMCS CHROMIUM. TOTAL. BY ICAP

WM09 COPPER. TOTAL. BY ICAP

WM10 IRON. TOTAL. BY ICAP

WM11 MANGANESE, TOTAL. BY ICAP

WM12 MOLYBDENUM BY ICAP

WM13 NICKEL BY ICAP

WM14 LEAD. TOTAL. BY ICAP

WM15 ANTIMONY, TOTAL, BY ICAP

WM16 SELENIUM BY ICAP

WM17 TITANIUM BY ICAP

WM1S THALLIUM BY ICAP

WM13 VANADIUM BY ICAP

WM20 ZINC BY ICAP

WM^1 CALCIUM. TOTAL BY ICAP

WM22 MAGNESIUM, TOTAL BY ICAP

WM23 SODIUM. TOTAL BY ICAP

WM24 POTASSIUM, TOTAL BY ICAP

• I.IG/KGJ•-UG/K.G:

:UG/L :10

:UG/L :370

:UG/L :10

:UG/L :200

:UG/L :5.0

!UG/L 5.0

:UG/L :50

:UG/L :10

:UG/L :25

:UG/L :320

:UG/L .400

:UG/L :N/A

:UG/L :40

:UG/L .;15

:UG/L ':60

:UG/L :5.0

:UG/L :N/A

•UG/L -10

:U'J/L :50

• UG/I. -20

:MC/L : 120

:MG/L :48

:MG/L :820

•MG/L :7.1

U

/

U

U

U

U

U

U

U

0

U

U

U

U

0

U

U

U

:10

•200

= 10 . •

•200

'•.5.0

'•s.o:.50

• 10•25

•100

•15

:N/A

:40

:3.0

^60

!s.o!N/A: !0

:'SC:.20

!s.o!s.o!s.o:5.0

U

U

U

U

U

U

U

I)

U

U

U

0

U

U

U

U

0

U

U

U

U

U

U

U

15 U :

IB U :.

-



WM34 MERCURY BY C.OLD VAPOR AA :"«VU

WP1 7 PCB-1016 :UG/L

WP18 PCB-1221 :UG/L

WP19 PCB-1232 ':UG/L

WP20 PCB-1242 !UG/L

WP21 PCB-1248 :'UG/L

WP22 PCB-1254 ': UG/L

WP23 PCB-1260 :UG/L

•WSrOI PHENOL :UG/L

WS03 ETHER. BIS( 2-CHLOROETHVL ) , BY fit /MS : UG/L

WS04 2-CHLOROPHENGL :UG/L

WS05 1 ,3-DlCHLOROBENZENE : UG/L

WS06 1 ,4-DICHLOROBENZENE :UG/L

WS07 BEN2YL ALCOHOL : UG/L

WS08 1 .2-DICHLOROBENZENE :Ub/L

WS09 2-METHYLPHENOL lO-CRESOL.) : UG/L

WS10 ETHER. BIS(2-CHLOROISOPROPYL) . BY GC/MS:UG/L

WS11 1-METHYLPHENOL (P-CRESOL.) : UG/L

WS12 N-NITROSO-DIPROPYLAMIME : UG/L

v,'c. n nrxAr.ni nRnFTMii.]r pv r,r ..•(,'. c. :'i,.-^

W31-1 NITRGBEUZEIJE :i.M.-.'L

WS15 1SOPHORONE .BY L)C/MS : UG/L

WS16 '^-WITROPHEWOL :l)G/L

W517 2.4-DIMETHYLPHENOL : UG/L

WS18 BENZOIC ACID, BY GC/MS : UG/L

WS19 METHANE. BIS( 2-CHLOROETHYOXY ) . BY GC/MS: UG/L

0 20 '.' :

1.0 U

1 .0 U

2.0 ,r U

1 .0 U

1 .0 U

1 .0 U

1 .0 U

10 U

10 U

10 U

10 U

10 U

N/A 0

10 U

10 U

N/A 0

10 U

10 U

• '0 U

• 1 0 U

'•10 U

:10 U:. 10 U

: N/A 0

: 10 U

0.52

1.0 U

1.0 U

2.0 U

1.0 • .. U

1.0 U

1 .0 U

1.0 U

10 U

10 U

10 U

10 U

10 U

N/A 0

10 U

10 U

N/A 0

10 U

10 U

10 • U

10 U

10 U

10 U

10 U

N/A 0

10 U

.


COMPOUND UNITS 005 006 F 008 F 009 F 101

WS20 2.4-DICHLOROPHENOL :n<VU

WS21 1 ,2.4-TRICHLOROBENZENE ' : UG/L

WS22 NAPHTHALENE : UG/L

WS23 4-CHLOROANILINE : UG/L

WS24 HEXACHLOROBUTADIENE.BY GC/MS : UG/L

WS25 4-CHLORO-3-METHYLPHENOL : UG/L

WS26 2-METHYLUAPHTHALENE : UG/L

WS27 HEXACHLOROCYCLOPENTADIEUE.BY GC/MS : UG/L

-tf928 2.4.6-TRICHLOROPHENOL :. UG/L

WS29 2.4.5-TRICHLOROPHENOL :UG/L

WS30 2-CHLORONAPHTHALENE ! UG/L

WS31 2-NITROANILINE (ORTHO NITROANILINE ) : UG/L

WS32 PHTHALATE. DIMETHYL. BY GC/MS : UG/L

WS33 ACENAPHTHYLENE, BY GC/MS : UG/L

WS34 3-NITROANILINE : UG/L

WS35 ACENAPHTHENE. BY GC/MS • UG/L

WS36 2.4-DINITROPHENOL ! UG/L

WS37 4-NITROPHENOL . !uG/L

WS38 DIBENZOFURAN • UG/L

WS39 2.4-DINITROTOLUENE :UG/L

WS-10 2.C-DINITROTOLUEWE : 00/L

WS41 PHTHALATE. DIETHYL. BY GC/MS : UG/L

W542 4-CHLOROPHENYL PHENYL ETHER : UG/L

WS43 FLUORENE.BY GC/MS ': UG/L

WS44 4-N1TROANILINE : UG/L

WS45 4.6-DINITRO-2-METHYLPHENOL :. UG/L

i n i i -

10 U \

10 U

10 / U

10 U

10 U

10 U

10 U

10 U

25 11

10 U

25 U

10 U

10 , U

25 U

10 U

25 U

25 U

10 U

1 G U

10 U

10 U

10 U

10 U

25 U

25 U

10 U .

10 U

10 U

10 U

10 . •.., U

10 U

10 U

10 LI

10 U

25 U

10 U

25 U

10 U

10 U

25 |!

10 U

25 U

25 U

10 U

} 0 :.:

'.',0 U

• 10 '.'

: 10 U

•10 U

•25 U

':2S U


COMPOUND UNITS 005 006 F 008 F. 009F 101

WS4G Ki-KilTROSGDlf'HENVLAMINE 'iiG/L^:

WS47 4-BROMOPHENYL PHENYL ETHER 'iuG/L :

WS48 HEXACHLOROBENZENE.BY GC/MS ' : UG/L :

WS49 PENTACHLOROPHENOL : UG/L :

WS50 PHENANTHRENE : UG/L :

WS51 ANTHRACENE. BY GC/MS : UG/L

WS52 PHTHALATE, DI-N-BUTYL-, BY GC/MS : UG/L

WS53 FLUORAMTHENE.BY GC/MS : UG/L

W554 PYRENE : UG/L

WS55 PH1HALATE, BUTYL BENZYL : UG/L

WS5G 3.3'-DICHLOROBENZIDINE : UG/L

WS57 ANTHRACENE. BENZO(A), BY GC/MS : UG/L

WS58 PHTHALATE. BISC2-ETHYLHEXYL) , BY GC/MS ': UG/L

WS59 CHRYSENE. BY GC/MS : UG/L

WS6C PHTHALATE. DI-M-OCTYL-. BY GC/MS -UG/L

WS61 FLUGRANTHElML, BENZOL), BY GC/MS :UG/L

WS62 FLUORANTHENE. BENZSO(K). BY GC/MS ! UG/L

WS63 PYRENE. BEN?0<A). BY GC/MS : UG/L

WS64 INDENOU . 2 . 3-CD) PYRENE : UG/L

V,'c-,(rtr. iMTHR.-.r.nii: D J BEfv.TO' A . M? . fiV GC/MS :ijG/L

V.'CCC rCR','LEi-iL . arw.'i'i G.H. j 'i B'v i,f /MS :!'0/L

WS67 CAFiBA.20Lfc : UG/L

WV03 '.'.HLOROMEThAHE. BY GC/MS : UG/L

WU04 BROMOMETHANE. BY GC/MS : UG/L

WV05 VINYL CHLORIDE : UG/L

WV06 CHLOROETHANE. BY GC/MS : UG/L

10 U :

10 U

10 U

25 .. U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

25 U

10 . U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

1C U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U


COMPOUND UNITS 005 006 F 008F' 009F 101

WV07 METHYLENE CHLORIDE U^/L^

WV08 1 ,1-DICHLOROETHENE ':UG/L

WV09 1 . 1-DICHLOROETHANE : UG/L

WV10 1 ,2-DICHLOROETHENE. TOTAL \ UG/L

WV11 CHLOROFORM, BY GC/MS :UG/L

WV12 1 .2-DICHLOROETHANE \ UG/L

WV13 1 .1 ,1-TRICHLOROETHANE ! UG/L

WV14 CARBON TETRACHLORIDE, BY GC/MS • UG/L

tfV-15 BROMODICHLOROMETHANE, BY GC/MS : UG/L

WV16 1 ,2-DICHLOROPROPANE :. UG/L

WV17 BENZENE. BY GC/MS ! UG/L

WV19 TRICHLOROETHENE • UG/L

WV20 DICHLOROPROPENE, CIS-1,3-, BY GC/MS : UG/L

WV21 DIBROMOCHLOROMETHANE. BY GC/MS : UG/L

WV22 1 , 1 ,2-TRICHLOROETHAME : UG/L

WV24 BROMOFORM. BY GC/MS : Uli/L

WV25 TETRACHLOROETHENE : UG/L

WV26 TOLUENE : UG/L

WV27 1 , 1 ,2.2-TETRACHLOROETHANE : UG/L

WV78 r.HLOROBENZEME . BY GC/MS :UG/L

WV29 ETKYL BENZENE. BY GC/MS : UG/L

WV30 ACETONE. BY GC/MS. : UG/L

WV31 CARBON DISULFIDE. BY GC/MS :UG/L

WV32 2-BUTANONE :UG/L

WV33 VINYL ACETATE . :. UG/L

WV34 2-HEXANONE :UG/L

in ii •

10 U

10 U

10 :• U

16

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 Li

10 'J

10 U

10 U

10 U

N/A O

10 U

in M

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

TO U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

-0 ij

10 C

31 L;10 U

10 U

N/A 0

•10 U

1C L!

10 • u10 U

10 U

10 , ;... U

10 U

10 U

10 U

10 U

10 i.l

10 U

10 U

10 U

10 U

10 U

10 U

10 U

16

10 U

: 0 U

;c u1 0 U

10 U

10 U

N/A 0

•10 U

;o u10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

. ; 0 U

.1C U

.' 38 i.l

•10 U

: 10 U

: N/A 0

:-\0 U


COMPOUND

WV35 4-METHYL-2-PENTANONE

WV36 STYRENE

WV37 XYLENES. TOTAL

WV40 TRAMS-1 ,3-DICHLOROPROPENE

2201 SAMPLE NUMBER

2202 ACTIVITY CODE

UNITS

• UC'/l.

' :UG/L

:UG/L

!UG/L

:NA

:NA

005

10

10

10

10

005

ISXP8

006 F

n -; 10

U : 10

U :. 10

U : 10

:006

: ISXP8

008 F'

11 .10,

U :10

U : 10

U : 10

• 008

^isxpe

009F

u . ' U U

U :. 10 U

U : 10 U

U : 10 U

:009

: ISXP8

101

101

ISXP8


COMPOUND UNITS 102 103 103D. 104 105

SM01 SILVER BY ICAP

SM02 ALUMINUM, TOTAL, BY ICAP

SM03 ARSENIC. TOTAL, BY ICAP

SM04 BARIUM, TOTAL, BY ICAP

SM05 BERYLLIUM, TOTAL. BY ICAP

SM06 CADMIUM. TOTAL, BY ICAP

SM07 COBALT. TOTAL, BY ICAP

SM08 CHROMIUM, TOTAL, BY ICAP

'SM09 COPPER. TOTAL, BY ICAP

SM10 IRON. TOTAL. BY ICAP

5M11 MANGANESE. TOTAL BY ICAP

SMI 2 MOLYBDENUM BY ICAP

SM13 NICKEL BY ICAP

SM14 LEAD. TOTAL, BY ICAP

SM15 ANTIMONY. TOTAL, BY ICAP

SM16 SELENIUM BY ICAP

SM17 TITANIUM BY ICAP

SM18 THALLIUM BY ICAP

SM19 VANADIUM BY ICAP

SM20 riNC BY ICAP

SM21 CALCIUM. TOTAL. BY Tf.AP

SM22 MAGNESIUM. TOTAL. BY ICAP

SM23 SODIUM BY ICAP

SM24 POTASSIUM BY ICAP

SM34 MERCURY BY COLD VAPOR AA

SP17 PCB-1016

•MG/KG,-' : MG/KG:

: MG/KG.

: MG/KG

: MG/KG

: MG/KG

: MG/KG

: MG/KG

: MG/KG

: MG/KG

: MG/KG

•MG/KG

: MG/KG

: MG/KG

•MG/KG

:MG/KG

': MG/KG

: MG/KG

: MG/KG

': MO/K.G

•MG/KG

•MG/KG

: MG/KG

: MG/KG

•MG/KG

•UG/KG

3. 7

23000

4.6

130 ;.

1 .9

1 .9

19

40

160

19000

530

N/A

24

68

N/A

1 .9

•N/A

:3.7

:31

: 240

: 35000:. 1 3000

: 1 900

•1900

:0. 19

•660

ij

U

U

uJJJ

0

0

u0

u

uuuu

•l° G

: 1 1 000

•3.6

^96

•1.8

:1 .8

•18

-.20

':68

': 1 3000

i270

!N/A•16:. 19

: N/A

:1 .8

!N/A!3.6

:23

;.S9

1-1000

3900

1800

1800

0. 18

720

n

U

U

uJJ,1

0

0

u0

u

uuuu

. -I A

•11000:3.6

: 110

•1.7:. 1 . 7

•1.7

•21

:71

: 14000

•340

•N/A

: 14

:21

: N/A

•1.7

:N/A

:34.3

:22

:76

: 1 300C

: 4600

: 1700

: 1700

:0. 17

:620

'J

U

U

uJJ.1

0

Iu0

uu-uu

.3.3

: 2 1 000

.:9.6

: 100

•1.7

•1.7

• 17

:28

^200

29OOO

^530

!N/A:22

•35

;N/A:1 .7

•N/A

':3.3

•37

'. 1 ; 0

: i SOOO

: G80G

: 1 700

: 1700

:0.17

'.580

Li .3.2

U

U

U

J

J

.1

0

T

U

0

u

u

12000

3.4

64

1 .6

1 .6

16

16

47

U

U

U

U

J

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'0000 .!

190

N/A 0

15

18

M/A

1 .6

N/A

3.2

o

u0

u1 7

h 1

; fcooo: 2500

U :1600

U -1600

U :0. 16

U ^53

uuuu


COMPOUND UNITS 102 103 103D. 104 105

SP18 PCS- 1221

SP19 PCB-1232

SP20 PCB-1242

SP21 PCB-1248

SP22 PCB-1254

SP23 PCB-1260

SS01 PHENOL

SS02 CARBAZOLE

S"S03 ETHER, BIS( 2-CHLOROETHYL) , BY

SS04 2-CHLOROPHENOL

SS05 1 , 3-DICHLOROBEN2ENE


SS07 BENZYL ALCOHOL


SS09 2-METHYLPHEMCL (0-CRESOL)

SS10 WTHER. BIS(2-CHLCROISOPROPYL)

SS11 4-METHYLPHENOL IP-CRESOL)

SS12 N-NITROSO-DIPROPYLAMINE

SS13 HEXACHLOROETHANE.BY GC/MS

SS1-1 NITROBENZENE

S515 ISOPHORONE. BY GC/MS

SS16 2-NITRGPHENOL

SSI 7 2.4-DIMETHYLPHENOL

SS18 BENZOIC ACID, BY GC/MS

SS19 METHANE. BISC2-CHLOROETHYOXY )

SS20 2,4-DICHLOROPHENOL

• nr; iv(±

' : UG/KG:

': UG/KG:

\ UG/KG:

•UG/KG

: UG/KG

: UG/KG

: UG/KG

GC/MS i UG/KG

•UL./K.G

: UG/KG

660

1300

660

24000

660

660

20000

20000

20000

20000

20000

•UG/KG -20000

•UG/KG

: UG/KG

: Li i.i / <t- b

. BY GC/MS: UG/KG

: UG/KG

: UG/KG

: UG/KG

: l''../f !:.

1 1 ' 1.- ' k I.-

: UG/KG

: UG/KG

: UG/KG

, BY GC/MS: UG/KG

•UG/KG

N/A

20000

20000

N/A

20000

20000

20000

;:OX'0

• .-Vir.ri

• 20000

: 20000

: N/A

: 20000

• 20000

1 1 "7On

U 1500

U

J

U

U

U

U

U

!J

U

U

0

U

I.I

0

720

1 1ij

U

U

17000

720

720

720

1100

720

720

720

720

N/A

720

•'20

N/A

U : 720

U :. 720

II : 720

; : ' - •" .".

II . T~\.'\

U :720

U : 720

0 :M/A

U :. 720

U :720

U

U

U

JU

U

U

U

G20

1300

620

19000

620

620'

620

890

620

620

620

620

0 :N/A

U :620

U ;620

0 :N/A

U :620

U '.620

U '620; , . ,t 7.1",

I i f r, s\•^ • O*LW

'J :620

U :620

0 -N/A

U :620

U :620

U

U

U

U

U

U

JU

U

U

U

0

U

U

0

U

U

U

1.1

\J

IJU

0

U

U

. oSG

. 1200

^580

: 1 5000

:580

:580

^580

: 1100

•580

: 580

':580

•580:N/A

^580

: 580

:N/A

'.580

•580

•580[' •"' •'"'J O-_.

.580

: 580

:580

:N/A

•580

•580

u

U

U

J

U

U

U

J

U

U

U

u0

uII

0

uuuuuuu0

uu

: bo: 1 10

^53

^3700

•53

:53

•5300

: 1 1 000

•5300

^5300

': 5300

•5300

•N/A:. 5300

': 5300

•N/A

.: 5300

: 5300

•5300

: 5300: 5300

': 5300

15300

': N/A

': 5300

': 5300

U

U

U

J

U

U

u

uuuu0

uu0

uuuuuuu0

uu


COMPOUND UNITS 102 103 103D 104 105

SS21 1 . 2.4-TRICHLOROBENZENE

SS22 NAPHTHALENE

SS23 4-CHLOROANILINE

SS24 HEXACHLOROBUTADIENE.BY GC/MS

SS25 4-CHLORO-3-METHYLPHENOL

SS26 2-METHYLNAPHTHALENE

SS27 HEXACHLOROCYCLOPENTADIENE.BY GC/MS

SS28 2.4 .6-TRICHLOROPHENOL

'5S29 2,4.5-TRICHLOROPHENOL

S530 2-CHLOROMAPHTHALENE

SS31 2-NITROANILINE

SS32 PHTHALATE. DIMETHYL. BY GC/MS

SS33 ACENAPHTHYLENE, BY GC/MS

SS34 3-NITROANILINE

SS35 ACENAPHTHENE , BY GC/MS

SS36 2,4-DINITROPHENOL

SS37 4-NITROPHENOL

SS38 DIBENZOFURAN

SS39 2.4-D1NITROTOLUENE

Sr,40 ? G-DIMITROTOLUEWE

SS41 PHTHALATE . DIETHYL. BY C.f./MS

SS42 4-CHLOROPHENYL PHENYL ETHER

SS43 FLUORENE .GC/MS

SS44 4-NITROANILINE

SS45 4.6-DINITRO-2-METHYLPHENOL

SS46 N-NITROSODIPHENYLAMINE

•UG/KC- 20000' : UG/KG -20000

: UG/KG •. 20000

: UG/KG : 20000

: UG/KG : 20000

: UG/KG: 20000

: UG/KG : 20000

: UG/KG: 20000

: UG/KG: 50000

: UG/KG: 20000

•UG/KG: 50000

:' UG/KG : 20000

: UG/KG: 20000

: UG/KG: 50000

: UG/KG -20000

•UG/KG -50000

•UG/KG; 50000: UG/KG: 20000

: UG/KG : 20000: UG/KG: 20000

: UG/ KG : 20000: UG/KG: : 20000

•UG/KG: 20000

•UG/KG :50000

: UG/KG -50000

: UG/KG -20000

n

U

uU

uuuuuuuuuuLi

uuuuuuuuuuu

•?or\

720

720

720

720

720

720

720

1700

720

1700

720

720

1700

720

1700

1700

720

720

720

720

720

720

1700

1700

720

it . (T *-»rtvj . \j ^_w

U :620

U :620

U :620

U :620

U :620

U ^620

U ":620

U : 1 500

U : 620

U : 1 500

U :620

U :620

U : 1 500

U :620

U i 1 500

U : 1 500

U ;.620

U .:620

U -650

U ^620

U ^620

U :620

U ! 1 500

U : 1 500

U :620

U

U

uuuuuuu1.1

uuuuuuuuuuIj1!

uuuu

CSC

580

580

580

580

580

580

580

1400

580

1400

580

580

1400

580

1400

1400

580

580

t&O

5SO

580

580

1400

1400

580

u . o300

U :5300

U : 5300

U ^5300

U :. 5300

U : 5300

U : 5300

U 15300

U ': 1 3000

ii • .300

U : 1 3000

U ^5300

U I5300

U : 1 3000

1! MOO

U : 1 3000

U : 1 3000

U ;5300

U : 5300

I: . 'x-GO

l.i ; ,s\)'. 'f

i i 5500

U :5700

U ! 1 3000

U '. 1 3000

U 15300

u

U

U

uuuuuuuI.I

uuu

uuuLI

i'

LI

u

uuu


COMPOUND UNITS 102 103 103D 104 105

SS47 4-BROMOPHEMYL PHENYL ETHER

SS48 HEXACHLOROBENZENE.BY GC/MS

SS49 PENTACHLOROPHENOL

SS50 PHENANTHRENE

SS51 ANTHRACENE, BY GC/MS

SS52 PHTHALATE. DI-N-BUTYL-. BY GC/MS

SS53 FLUORANTHENE.BY GC/MS

SS54 PYRE ME

•-SS55 PHTHALATE. BUTYL BENZYL

SS56 3.3'-DICHLOROBENZIDIME

SS57 AMTRACEME, BEN20(Al. BY GC/MS

SS58 PHTHALATE. BISC2-ETHYLHEXYL) . BY GC/MS

SS59 CHRYSENE, BY GC/MS

SS60 PHTHALATE, DI-N-OCTYL-. BY GC/MS

SS61 FLUORANTIIEME. OEMZOCB). BY GC/MS

SS62 FLUGRANTHENE, BENZGlM, BY GC/MS

SS63 PYRENE. BENZOlA). BY GC/MS

SS64 IMDENQf 1 .2. 3-CD) PYRENE

SS65 ANTHRACENE. DIBENZO( A . H ) . BY GC/MS

Sf.f.P. PF.RYLF.Mti. BEwrO'G.H. T i EV ;;-C/M5

C.V03 CHLCROUCTHAUE . a'. iV./Wf

SVG'l 6ROMOMETHANE . BY UC/MS

S\/Ob VINYL CHLORIDE

SV06 CHLOROETHANE, BY GC/MS



"0/KJj

: UG/KG:

•UG/KG:

:UG/KG:

: UG/KG-

: UG/KG

: UG/KG

: UG/KG

: UG/KG

: UG/K.G

: UG/KG

: UG/KG

: UG/KG

: UG/KG

. UG/Mj

: UG/KG

: UG/KG

: UG/KG

: UG/KG

• LI c /i (;

'-'C.i /v; !j

: U C./ KG

.UG/KG

: UG/KG

: UG/KG

: UG/KG

20000

20000

50000

62000

20000

20000

1 20000

1 30000

20000

20000

63000

20000

63000

20000

84000

23000

48000

45000

20000

.'•< 1 000

- ori

.20

:20

:20

:20

:20

1 1

U

u

U

u

uu

u

u,1

JJJu,!

uuuuuu

7or*

720

1700

3200

720

720

5300

7100

720

720

2700

1200

2600

720

3900

1200

2100

3400

720

:i • oo22

22

22

22

22

22

U

U

U

J

uuJJuuJJJuJJJJuJuuuu1.1u

C20

620

1500

2400

620 ;,

620

5500

6300

620

620

3000

870

2700

620

4400

1300

2000

3900

750

1400

19

19

19

19

19

19

U

U

U

J

U

U

J

U

U

J

U

J

U

JJJJJJuuuuuu

580

580

1400

3600

610

580

5700

5400

580

580

2700

640

2700

580

3400

1000

1500

2400

580

580

IS

18

18

18

18

18

U

U

uJJuJJuuJuJuJJJJuuuVJ

uuuu

•5300

•5300

: 1 3000

•31000

• 7600

': 5300

: 38000

: 40000

•5300

^5300

: 25000

: 5300

: 30000

•5300; 27000

: 5300

• 20000

•8200

• 5300

': 5300

: 16

\ 16

': 16

: 16

': 16

: 16

U

U

U

U

U

U

U

U

U

U

uuuuuuu


COMPOUND UNITS 102 103 1030 104 105

SV09 1 .1-DICHLOROET.HANE

SV10 TRANS-1 .2-DICHLOROETHYLENE

SV11 CHLOROFORM. BY GC/MS

SV12 1 ,2-DICHLOROETHANE

SV13 1 . 1 .1-TRICHLOROETHANE

SV14 CARBON TETRACHLORIDE , BY GC/MS

SV15 BROMODICHLOROMETHANE. BY GC/MS

SV16 1 ,2-DICHLOROPROPANE

•£\M7 BENZENE, BY GC/MS

SV18 TRANS-1 ,3-DICHLOROPROPENE

SV19 TRICHLOROETHYLENE

SV20 DICHLOROPROPENE. CIS-1.3-. BY GC/MS

SV21 DIBROMOCHLOROMETHANE, BY GC/MS

SV22 1 .1 ,2-TRICHLOROETHANE

SV24 BROMOFORM. BY GC/MS

SV25 1 , 1 .2,2-TETRACHLOROETHENE

SV26 TOLUENE

SV27 1 . 1 ,2.2-TETRACHLOROETHANE

SV28 CHLOROBENZENE. BY GC/MS

SV?9 ETHYL BENZENE . BY GC/MS

SV30 ACETONE. BY GC/MS

SV31 CARBON DISULFIDE. BY GC/MS

SV32 2-BUTANONE

SV33 VINYL ACETATE

SV34 2-HEXANONE

SV35 4-METHYL-2-PENTANONE

:..r,/K£:

•UG/KG:

•UG/KG:

: UG/KG:

•UG/KG:

•UG/KG:

: UG/KG :

•UG/KG

: UG/KG

i UG/KG,

•UG/KG

•UG/KG

•UG/KG

: UG/KG

: UG/'Nb

: UG/KG;. UG/KG

: UG/KG

•UG/KG

: Lit./ KG:L'G/^

: UG/KG

: UG/KG

•UG/KG

• UG/KG

•UG/KG

90

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

2C

66:20

:20

•N/A

•20

':20

n

U

U

uuuuuuLi

U

U

uuuuuuuI I

uuu0

uu

!22

•22

•22

•22

\22

•22

•22

•22

:22

22

•22

•22

:22

•22:22

:22

':22

'.22

•22

'.22

': 22

• 22

:22

•N/A

•22

•22

U

U

U

U

U

U

U

U

U

U

U

U

uuuuuuuI1

uu

12 U

19

19

19

19

19

19

19

19

19

19

19

19

19

1 Q

19

19

19

19

; -.

2Z

1 O

U • 19

0 N/A

U 19

U 19

U

U

U

uuuuuuuuuuuuuu

"i 8

18

18

18

18

18

18

18

18

IP

18

18

18

18

18

18

18

18

U : 18

U :\B

L: :2G

U : 1 8

U : 18

0 : N/A

U : 18

U : 18

iJ

U

U

U

uuuuuuuuuuuuuuuuu

16 U

16

16

16

16

16

16

16

16

16

16

16

16

16

U

U

U

U

U

U

U

U

U

U

U

uu

• R U

16

16

16

16

16

uuuuu

25 U

U 16

U 16

0 N/A

U 16

U 16

uu0

uu


COMPOUND UNITS 102 103 103D- 104 105

SV36

SV37

Z201

ZZ02

STYRENE

XYLENES, TOTAL

• 1 1 f ; / K Q

' luG/KG:

SAMPLE NUMBER • MA

ACTIVITY CODE •MA

20

:20

:102

•ISXP8

n .'22

U ^22

•103

•ISXP8

U -.5

U : 19

: 103

: ISXP8

U

U

. IS

• 18

: 104

•ISXP8

U

U

. 16:16

: 105

: ISXP8

U

U


COMPOUND UNITS 108F 109F

SV03 CHLOROMETHANE . BY GC/MS

SV04 BROMOMETHANE , BY GC/MS

SV05 VINYL CHLORIDE

SV06 CHLOROETHANE, BY GC/MS



SV09 1 . 1-DICHLOROETHANE

SV10 TRANS-1 , 2-DICHLOROETHYLENIE

SV11 CHLOROFORM. BY GC/MS

SV12 1 ,2-DICHLOROETHANE

SV13 1 .1 ,1-TRICHLOROETHANE

SV14 CARBON TETRACHLORIDE . BY GC/MS

SV15 BROMODICHLOROMETHANE, BY GC/MS

SV16 1.2-DICHLOROPROPANE

SV17 BENZENE, BY GC/MS

SV1S TRANS-1 .3-DICHLORGPROPENE

SV19 TRICHLOROETHYLENE

SV20 DICHLOROPROPENE. CIS-1.3-. BY GC/MS

SV21 DIBROMOCHLOROMETHANE. BY GC/MS

SV22 1 , 1 , 2-TRICHLOROETHAME

SV2-1 BROMOFORM. BY GC./M5

SV25 1 . 1 ,2.2-TETRACHLOROETHENE

SV26 TOLUENE

SV27 1 ,1 ,2.2-TETRACHLOROETHANE

SV28 CHLOROBENZENE. BY GC/MS

SV29 ETHYL BENZENE . BY GC/MS

• IIG/KCV 10

•UG/KG: 10

: UG/KG: 10

•UG/KG: 10

i UG/KG:' 10

•UG/KG: 10

: UG/KG: 10

! UG/KG: 10

: UG/KG: 10

:Ub/KG: 10

•UG/KG: 10

•UG/KG :10

•UG/KG': 10•UG/KG !lO

: UG/Kb: 10

•UG/KG: 10

•UG/KG: 10

•UG/KG: 10

•UG/KG: 10

• UC/t-.G: 10

1 Uf.i/f t ' 10

•UG/KG: 10

:UG/KG: 10

•UG/KG: 10

•UG/KG: 10

: UG/KG .: 10

n

. U

u/ u

u-uuuuuuuuuI I

uuuu(1

1 1

uuuuu



SV30 ALETONiE . BY GC/MS : UG/KG,: 1 ?

SV31 CARBON DISULFIDE . BY GC/MS : UG/KG: 10 U

SV32 2-BUTANONE : UG/KG: 10 U

SV33 VINYL ACETATE : UG/KG :N/A •• 0

SV34 2-HEXANONE : UG/KG: 10 U

SV35 4-METHYL-2-PENTANONE : UG/KG : 10 U

SV36 STYRENE " : UG/KG: 10 U

SV37 XYLENES. TOTAL : UG/KG: 10 U

WM01 SILVER BY ICAP :. UG/L :.

WM02 ALUMINUM. TOTAL, BY ICAP : UG/L :

WM03 ARSENIC, TOTAL. BY ICAP i UG/L :.

WM04 BARIUM, TOTAL, BY ICAP : UG/L :

WM05 BERYLLIUM, TOTAL, BY ICAP ! UG/L :

WM06 CADMIUM, TOTAL. BY ICAP : UG/L :

WM07 COBALT. TOTAL. BY ICAP : UG/L :

WM08 CHROMIUM, TOTAL. BY ICAP :UG/L :

WM09 COPPER, TOTAL, BY ICAP : UG/L :

WM10 IRON. TOTAL. BY ICAP !uG/L :

WM11 MANGANESE. TOTAL. BY ICAP : UG/L :

WM1? MOLVBHENUM BY ICAP : UG/L :

WMT3 MICHEL rTV I CAP : UG/L :

WMi'i LEAD, TOTAL, BY ICAP : UG/L :

WM16 ANTIMONY. TOTAL. BY ICAP : UG/L :

WM16 SELENIUM BY ICAP : UG/L :

WM17 TITANIUM BY ICAP . : UG/L :

WM18 THALLIUM BY ICAP : UG/L :

10 U

200 U

10 U

200 U

5.0 U

5.0 U

50 U

10 U

25 U

100 U

15 U

IO/A 0

40 U

3.0 U

50 U

5.0 U

N/A 0

10 U



WM19 VANADIUM BY ICAP lirVL%.

WM20 ZINC BY ICAP :. UG/L

WM21 CALCIUM, TOTAL BY ICAP :MG/L

WM22 MAGNESIUM, TOTAL BY ICAP :MG/L

WM23 SODIUM, TOTAL BY ICAP :MG/L

WM24 POTASSIUM. TOTAL BY ICAP :MG/L

WM34 MERCURY BY COLD VAPOR AA : UG/L

WP17 PCB-1016 .UG/L

W>18 PCB-1221 -UG/L


WP20 PCB-1242 :UG/L

WP21 PCB-1248 .;UG/L


WP23 PCB-1260 !UG/L

WS01 PHENOL :Ub/L

WS03 ETHER, BIS1.2-CHLORGE1 HYL ) . BY GC/MS : UG/L

WS04 2-CHLOROPHENOL : UG/L

WS05 1 .3-DICHLOROBEN2EME : UG/L

WS06 1 ,4-DICHLOROBENZENE : UG/L

WS07 BENZVL ALCOHOL '•••••.. .-L

WSOS 1 . 2-DICHLOROBtN.II:KiE ; '.."...• L

W509 2-METHYLPHENOL lO-CRESOD HG/I-

WS1G ETHER. BI5(2-CHLOROISOPKOPYL.) . BY CC/MS: UG/L

WS11 4-METHYLPHENOL (P-CRESOL) : UG/L

WS12 N-NITROSO-DIPROPYLAMINE : UG/L

WS13 HEXACHLOROETHANE.BY GC/MS : UG/L

;•

50 U

20 U

5.0 U

5.0 U

5.0 U

5.0 U

0.20 U

1.0 U

1 .0 U

2.0 U

1.0 U

1 .0 U

1 .0 U

1.0 U

10 U

10 U

10 U

10 U

10 U

?J/A 0

10 U

10 U

N/A 0

10 U

10 U

10 U



WS14 NITROBENZENE :|-lri/L^

WS15 ISOPHORONE .BY GC/MS :UG/L

WS16 2-NITROPHENOL : UG/L

WS17 2.4-DIMETHYLPHENOL :UG/L

WS18 BENZOIC ACID, BY GC/MS : UG/L

WS19 METHANE. BIS(2-CHLOROETHYOXY) . BY GC/MS: UG/L

WS20 2.4-DICHLOROPHENOL : UG/L

WS21 1 . 2.4-TRICHLOROBENZENE : UG/L

1lte22 NAPHTHALENE : UG/L

WS23 4-CHLOROANILINE : UG/L

WS24 HEXACHLOROBUTADIENE.BY GC/MS : UG/L

WS25 4-CHLORO-3-METHYLPHENOL : UG/L

WS26 2-METHYLNAPHTHALENE : UG/L

WS27 HEXACHLOROCYCLOPENTADIENE.BY GC/MS : UG/L

WS2S 2.4,6-TRICHLOROPHENOL :UG/L

WS29 2.4.5-TRICHLOROPHENOL. :UG/L

WS30 2-CHLORONAPHTHALENE : UG/L

WS31 2-NITROANILINE (ORTHO NITROANILINE) : UG/L

WS32 PH1HALATE. DIMETHYL. BY GC/MS : UG/L

Wf-. ? AP.ENAPHTHYLENE. BY GC/MS : UG/L

WS34 3-NITROANILINE :UG/L

WS35 ACENAPHTHENE. BY GC/MS : UG/L

WS36 2.4-DINITROPHENOL : UG/L

WS37 4-NITROPHENOL • UG/L

WS38 D1BENZOFURAN ': UG/L

WS39 2,4-DINITROTOLUENE : UG/L

TO I1

10 U

10 U

10 U

N/A 0

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

25 U

10 U

25 U

•10 U

10 U

:25 U

•10 U

.25 U

:25 U

: 10 U

: 10 U



WS40 2.6-DINITRGTOLUENE ''.''Vl '

WS41 PHTHALATE, DIETHYL. BY GC/MS ' ': UG/L

WS42 4-CHLOROPHENYL PHENYL ETHER '• UG/L

WS43 FLUORENE.BY GC/MS •. UG/L

WS44 4-NITROANILINE : UG/L

WS45 4.6-DINITRO-2-METHYLPHENOL : UG/L

WS46 N-NITROSODIPHENYLAMINE : UG/L

WS47 4-BROMOPHENYL PHENYL ETHER :UG/L

•V?S48 HEXACHLOROBEN2ENE.BY GC/MS ': UG/L

WS49 PENTACHLOROPHEMOL : UG/L

WS50 PHEMANTHRENE : UG/L

WS51 ANTHRACENE. BY GC/MS : UG/L

WS52 PHTHALATE. DI-N-BUTYL-, BY GC/MS : UG/L

WS53 FLUORANTHENE.BY GC/MS !UG/L

WS54 PYREME ilJb/L

WS55 PHTHAuATE. BUTYL BENZYL : UG/L

WS56 3.3'-DICHLOROBEN2IDINE :UG/L

WS57 ANTHRACENE. BEN20(A). BY GC/MS :UG/L

WS58 PHTHALATE. BIS( 2-ETHYLHEXYL ) . BY GC/MS : UG/L

W7.F.P Cl-lR'.'Sr'JE . BV TjC/fv'?. :l)'.,/t.

V.'SGC PHTr-'iALATE . OI-l-j-Cn".7Vi. - nv I.,I../MX :'..'b,'!.

WS61 FLUORANTHEME. BENZOlBj. OY GC/MS : UG/L

WS62 FLUORANTHENE. BEH2SOIK). BY GC/MS .UG/L

WS63 PYRENE, BENZO(A) . BY GC/MS : UG/L

WS64 INDENOd . 2. 3-CD)PYRENE : UG/L

WS65 ANTHRACENE, DIBENZO( A . H) . BY GC/MS :UG/L

10 U

10 U

10 U

10 U

25 U

25 U

10 U

10 U

10 U

25 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

to u120

10 U

10 U

10 U

10 U

10 U

10 U

10 U



WSG6 PERYLENE . BENZOI G.H . I > . BY Gf./MS '• UC./L

WS67 CARBAZOLE ' : UG/L

WV03 CHLOROMETHANE . BY GC/MS : UG/L

WV04 BROMOMETHANE . BY GC/MS :.UG/L

WV05 VINYL CHLORIDE : UG/L

VA/06 CHLOROETHANE . BY GC/MS ':UG/L

WV07 METHYLENE CHLORIDE : UG/L

WV08 1 ,1-DICHLOROETHENE : UG/L

'V?y09 1 ,1-DICHLOROETHANE ":UG/L

WV10 1 .2-DICHLOROETHENE. TOTAL : UG/L

WV11 CHLOROFORM. BY GC/MS :UG/L

WV12 1 ,2-DICHLOROETHANE : UG/L

WV13 1 . 1 , 1-TRI CHLOROETHANE • UG/L

WV14 CARBON TETRACHLORIDE . BY GC/MS : UG/L

WV15 BROMODICHLOROMETHANE, BY GC/MS • UG/L

WV16 1 .2-DICHLOROPROPANE -UG/L

WV17 BENZENE. BY GC/MS : UG/L

WV19 TRICHLOROETHENE -UG/L

WV20 DICHLOROPROPENE. CIS-1,3-. BY GC/MS : UG/L

WV21 DIBRQMOCHLOROMETHAWE. BY GC/MS : UC/L

WV22 1 , 1 ,2-TR I CHLOROETHANE :UG/L

WV2'1 BROMOFORM. BY. GC/MS : UG/L

WV2b TETRACHLOROETHENE :UG/L

WV26 TOLUENE : UG/L

WV27 1 , 1 ,2,2-TETRACHLOROETHANE : UG/L

WV28 CHLOROBENZENE, BY GC/MS ' : UG/L

10 'J :

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

10 U

•10 U

•1C U

•10 II

• 10 U

: 18

: 10 U

•10 U



WV29 ETHYL BENZENE. BY GC/MS :HG/L^.

WV30 ACETONE, BY GC/MS :UG/L

WV31 CARBON DISULFIDE. BY GC/MS ! UG/L

WV32 2-BUTANONE :. UG/L

WV33 VINYL ACETATE : UG/L

WV34 2-HEXANONE :UG/L

WV35 4-METHYL-2-PENTANONE : UG/L

WV36 STYRENE ! UG/L

fotfB? XYLENES.. TOTAL :UG/L

WV40 TRAWS-1 ,3-DICHLOROPROPENE : UG/L

2201 SAMPLE NUMBER ': MA

2202 ACTIVITY CODE : NA

. 'i r\ M

: 10 U

: 10 U

•10 U

IN/A o•10 U

:10 U

: 10 U

:10 U:. 1 0 U

108 :109

ISXP8 :ISXP8

PRELIMINARY DATASUBJECT TO REVISION

ACTIVITY ISXP8 MISSISSIPPI RIVER POOL #15

THE PROJECT LEADER SHOULD CIRCLE ONE - STORET, AIRS, OR ARCHIVE.

CIRCLE ONE: STORET AIRS ARCHIVE

•s

DATA APPROVED BY LABO FOR TRANSMISSION TO PROJECT LEADER ON) 10/10/91 16:08:52 BY

SITE: MISSISSIPPI RIVER POOL # 15

ACTIVITY: isxpSLAB: AATSCASE: 16873

ANALYSIS TYPE: METALS,TOTAL METHOD: CS0390IMATRIX: WATER DATA COMPLETED: 10/10/91

PARAMETERS

SILVERALUMINUMARSENICBARIUMBERYLLIUMCADMIUMCOBALTCHROMIUMCOPPERIRONMANGANESEMOLYBDENUMNICKELLEADANTIMONYSELENIUMTITANIUM •THALLIUMVANADIUMZINCCALCIUMMAGNESIUMSODIUM,,POTASSIUMMERCURY BY COLD VAPOR AA

EPA #SAMPLEDID #SMO #

UNITS

UG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LMG/LMG/LMG/LMG/LUG/L

IS07o#MG

10420102005.05.05010251200430

404.8605.0

1050325315415.00.20

uuuuuuuu

NUUuuNUU

UU

10420102005.05.05010251200430

405.2605.0

1050335315405.00.20

U

UUUUUUU

NUUUUNUU

UU

10230102005.05.0501025370250

403.0605.0

1050207332205.00.20

U

UUUUUUU

NUUUUNUUU

UU

* DATA QUALIFIER CODES *

U: LESS THAN DETECTION LIMITI: INVALID - NO VALUE REPORTEDJ: DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURESN: PARAMETER NOT ANALYZEDM: DETECTED BUT BELOW LEVEL FOR ACCURATE QUANTIFICATION




PARAMETERS UNITS

SILVER UG/L 10ALUMINUM UG/L 1200ARSENIC UG/L 10BARIUM . UG/L 200BERYLLIUM UG/L 5.0CADMIUM ' UG/L 5.0COBALT UG/L 50CHROMIUM UG/L 10COPPER UG/L 25IRON UG/L 250MANGANESE UG/L 60MOLYBDENUM UG/LNICKEL UG/L 40LEAD UG/L 3.0ANTIMONY UG/L 60SELENIUM UG/L 5.0TITANIUM - UG/LTHALLIUM . UG/L 10VANADIUM ' UG/L 50ZINC UG/L 29CALCIUM MG/L 60MAGNESIUM MG/L 23SODIUM MG/L 19POTASSIUM MG/L 5.0MERCURY BY COLD VAPOR AA UG/L 0.20

J ISXP8004 ISXPL 08/01/91 08/0) 0#1 T#17

U

uUuuuuu

NUUUUNUU

UU

MGJ028

1013000102005.05.05012252600500

406.9605.0

1050415722165.00.20

U

UUUUU

U

NUUUUNUU

UU

0#1MGJO

10370102005.05.0501025320400

4015605.0

105020120488207.10.20

U

uuuuuuu

NUUuuNUUU

U






PARAMETERS

SILVERALUMINUMARSENICBARIUMBERYLLIUMCADMIUMCOBALTCHROMIUMCOPPERIRONMANGANESEMOLYBDENUMNICKELLEADANTIMONYSELENIUMTITANIUMTHALLIUMVANADIUMZINCCALCIUMMAGNESIUMSODIUMPOTASS JCUMMERCURY BY COLD VAPOR AA


UNITS

ISXP8008F08/01/91FIELD BLKMGJ030

UG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LMG/LMG/LMG/LMG/LUG/L

10200102005.05.050102510015

403.0605.0

1050205.05.05.05.00.59

ISXP8109F07/31/91RINSATEMGJ298

UUUUUUUUUUUNUUUUNUUUUUUUU

UUUUUUUUUUUNUUUUNUUUUUUU

10200102005.05.050102510015

403.0605.0

1050205.05.05.05.00.20




ACTIVITY: ISXP8LAB: PNELICASE: 16873

ANALYSIS TYPE: PCBSMATRIX: WATER

METHOD: CS03900DATA COMPLETED: 10/10/91

PARAMETERS

PCB-PCB-PCB-PCB-PCB-PCB-PCB-

10161221123212421248•12541260

PARAMETERS

PCB-1016PCB-1221 -PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260

PARAMETERS

PCB-PCB-PCB-PCB-PCB-PCB-PCB-

•101612211232•1242124812541260


UNITS

UG/LUG/LUG/LUG/LUG/LUG/LUG/L


UNITS

UG/LUG/LUG/LUG/LUG/LUG/L .UG/L


UNITS


ISXP800107/31/910#1 A#41GL339

1.0 U1.0 U2.0 U1.0 U1.0 U1.0 U1.0 U

ISXP800308/01/910#1 T#20GL363

1.0 U1.0 U2.0 U1.0 U1.0 U1.0 U1.0 U

ISXP8008F08/01/91FIELD BLKGL366

1.0 U1.0 U2.0 U1.0 U1.0 U1.0 U1.0 U

ISXP8001D07/31/910#1 A#41GL340

1.0 U1.0 U2.0 U1.0 U1.0 U1.0 U1.0 U

ISXP800408/01/910#1 T#17GL364

1.0 U1.0 U2.0 U1.0 U1.0 U1.0 U1.0 U

ISXP8109F07/31/91RINSATEGL344

1.0 U1.0 U2.0 U1.0 U1.0 U1.0 U1.0 U

ISXP800208/01/910#1 T#14GL362

1.0 U1.0 U2.0 U1.0 U1.0 U1.0 U1.0 U

ISXP800508/01/910#1 T#lGL365

1.0 11.0 12.0 11.0 11.0 \1.0 11.0 \





ANALYSIS TYPE: SEMIVOLATILES-1 METHOD: CS0390OMATRIX: WATER DATA COMPLETED: 10/10/91

PARAMETERS

PHENOLBIS(2-CHLOROETHYL) ETHER2-CHLOROPHENOL1,3-DICHLOROBENZENE1,4-DICHLOROBENZENEBENZYL ALCOHOL1,2-DICHLOROBENZENE2-METHYLPHENOL (0-CRESOLBIS(2-CHLOROISOPROPYL) ET4-METHYLPHENOL (P-CRESOLN-NITROSO-DIPROPYLAMINEHEXACHLOROETHANENITROBENZENEISOPHORONE2-NITROPHENOL2,4-DIMETHYLPHENOLBENZOIC ACIDBIS(2-CHLOROETHYOXY) METH2,4-DICHLOROPHENOL1,2,4-TRICHLOROBENZENENAPHTHALENE4-CHLOROANILINEHEXACHLOROBUTADIENE4-CHLORO-3-METHYLPHENOL2-METHYLNAPHTHALENEHEXACHLOROCYCLOPENTADIENE2,4,6-TRICHLOROPHENOL2,4,5-TRICHLOROPHENOL2-CHLORONAPHTHALENE2-NITROANILINE (ORTHO NITDIMETHYLPHTHALATEACENAPHTHYLENE3-NITROANILINE


UNITS


L UG/LT UG/LL UG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/L

H UG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/L

E UG/LUG/LUG/LUG/L

r UG/LUG/LUG/LUG/L

i

1010101010

1010

10101010101010

10101010101010101010251025101025

UUUUUNUUNUUUUUUUNUUUUUUUUUUUUUUUU

1010101010

1010

10101010101010

10101010101010101010251025101025


1010101010

1010

10101010101010

10101010101010101010251025101025







PARAMETERS

ACENAPHTHENE2,4-DINITROPHENOL4-NITROPHENOLDIBENZOFURAN2,4-DINITROTOLUENE2,6-DINITROTOLUENEDIETHYLPHTHALATE4-CHLOROPHENYL PHENYL ETHFLUORENE4-NITROANILINE4,6-DINITRO-2-METHYLPHENON-NITROSODIPHENYLAMINE4-BRQMOPHENYL PHENYL ETHEHEXACHLOROBEN Z ENEPENTAGHLOROPHENOLPHENANTHRENEANTHRACENEDI-N-BUTYL PHTHALATEFLUORANTHENEPYRENEBUTYL BENZYL PHTHALATE3,3'-DICHLOROBENZIDINEBENZO(A)ANTHRACENEBIS(2-ETHYLHEXYL)PHTHALATCHRYSENEDI-N-OCTYL PHTHALATEBENZO(B)FLUORANTHENEBENZO(K)FLUORANTHENEBENZO(A)PYRENEINDENO(1,2,3-CD)PYRENEDIBENZO(A,H)ANTHRACENEBENZO(G,H,I)PERYLENECARBAZOLE


UNITS


H UG/LUG/LUG/L

0 UG/LUG/L

E UG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/L

r UG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/L

102525101010101010252510101025101010101010101010101010101010101010

uuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu

102525101010101010252510101025101010101015101011101010101010101010

uuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu

102525101010101010252510101025101010101010101010101010101010101010








ISXP800308/01/910#1 T#20GL363

ISXP800408/01/910#1 T#17GL364

ISXP800508/01/910#1 T#lGL365

PARAMETERS UNITS

PHENOLBIS(2-CHLOROETHYL) ETHER2-CHLOROPHENOL1,3-DICHLOROBENZENE1,4-DICHLOROBENZENEBENZYL ALCOHOL1,2-DICHLOROBENZENE2-METHYLPHENOL (O-CRESOLBIS(2-CHLOROISOPROPYL) ET4-METHYLPHENOL (P-CRESOLN-NITROSO-DIPROPYLAMINEHEXACHLOROETHANENITROBENZENEISOPHORONE2-NITROPHENOL2,4-DIMETHYLPHENOLBENZOIC ACIDBIS(2-CHLOROETHYOXY) METH2,4-DICHLOROPHENOL1,2,4-TRICHLOROBENZENENAPHTHALENE4-CHLOROANILINEHEXACHLOROBUTADIENE4-CHLORO-3-METHYLPHENOL2-METHYLNAPHTHALENEHEXACHLOROCYCLOPENTADIENE2,4,6-TRICHLOROPHENOL2,4,5-TRICHLOROPHENOL2-CHLORONAPHTHALENE2-NITROANILINE (ORTHO NITDIMETHYLPHTHALATEACENAPHTHYLENE3-NITROANILINE

UG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/L

1010101010

1010

10101010101010

10101010101010101010251025101025


1010101010

1010

10101010101010

10101010101010101010251025101025


1010101010

1010

10101010101010

10101010101010101010251025101025






ANALYSIS TYPE: SEMIVOLATILES-2 METHOD: CS03900MATRIX: WATER DATA COMPLETED: 10/10/91


ISXP800308/01/910#1 T#20GL363

ISXP800408/01/910#1 T#17GL364

ISXP800508/01/910#1 T#lGL365

PARAMETERS UNITS

ACENAPHTHENE2,4-DINITROPHENOL4-NITROPHENOLDIBENZOFURAN2,4-DINITROTOLUENE2,6-DINITROTOLUENEDIETHYLPHTHALATE4-CHLOROPHENYL PHENYL ETHFLUORENE4-NITROANILINE4,6-DINITRO-2-METHYLPHENON-NITROSODIPHENYLAMINE4-BROMOPHENYL PHENYL ETHEHEXACHLOROBEN Z ENEPENTACHLOROPHENOLPHENANTHRENEANTHRACENEDI-N-BUTYL PHTHALATEFLUORANTHENEPYRENEBUTYL BENZYL PHTHALATE3,3'-DICHLOROBENZIDINEBENZO(A)ANTHRACENEBIS(2-ETHYLHEXYL)PHTHALATCHRYSENEDI-N-OCTYL PHTHALATEBENZO(B)FLUORANTHENEBENZO(K)FLUORANTHENEBENZO(A)PYRENEINDENO(1,2,3-CD)PYRENEDIBENZO(A,H)ANTHRACENEBENZO(G,H,I)PERYLENECARBAZOLE


102525101010101010252510101025101010101010101010101010101010101010

UuUuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu

102525101010101010252510101025101010101010101010101010101010101010


102525101010101010252510101025101010101010101010101010101010101010









PARAMETERS UNITS

PHENOLBIS(2-CHLOROETHYL) ETHER2-CHLOROPHENOL1,3-DICHLOROBENZENE1,4-DICHLOROBENZENEBENZYL ALCOHOL1,2-DICHLOROBENZENE2-METHYLPHENOL (0-CRESOLBIS(2-CHLOROISOPROPYL) ET4-METHYLPHENOL (P-CRESOLN-NITROSO-DIPROPYLAMINEHEXACHLOROETHANENITROBENZENEISOPHORONE2-NITROPHENOL2,4-DIMETHYLPHENOLBENZOIC ACIDBIS(2-CHLOROETHYOXY) METH2,4-DICHLOROPHENOL1,2,4-TRICHLOROBENZENENAPHTHALENE4-CHLOROANILINEHEXACHLOROBUTADIENE4-CHLORO-3-METHYLPHENOL2-METHYLNAPHTHALENEHEXACHLOROCYCLOPENTADIENE2,4,6-TRICHLOROPHENOL2,4,5-TRICHLOROPHENOL2-CHLORONAPHTHALENE2-NITROANILINE (ORTHO NITDIMETHYLPHTHALATEACENAPHTHYLENE3-NITROANILINE


1010101010

1010

10101010101010

10101010101010101010251025101025


1010101010

1010

10101010101010

10101010101010101010251025101025











PARAMETERS UNITS

ACENAPHTHENE2,4-DlNlTROPHENOL4-NITROPHENOLDIBENZOFURAN ;.2,4-DINITROTOLUENE2,6-DINITROTOLUENEDIETHYLPHTHALATE4-CHLOROPHENYL PHENYL ETHFLUORENE4-NITROANILINE4, 6-DINITRO-2-METHYLPHENON-NITROSODIPHENYLAMINE4-BROMOPHENYL PHENYL ETHEHEXACHLOROBENZENEPENTACHLOROPHENOLPHENANTHRENEANTHRACENEDI-N-BUTYL PHTHALATEFLUORANTHENE ""PYRENEBUTYL BENZYL PHTHALATE3,3'-DICHLOROBENZIDINEBENZO(A)ANTHRACENEBIS(2-ETHYLHEXYL)PHTHALATCHRYSENEDI-N-OCTYL PHTHALATEBENZO(B)FLUORANTHENEBENZO(K)FLUORANTHENEBENZO(A)PYRENEINDENO(1,2,3-CD)PYRENEDIBENZO(A,H)ANTHRACENEBENZO ( G, H, I) PERYLENECARBAZOLE


102525101010101010252510101025101010101010101010101010101010101010

UuUuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu

1025251010101010102525101010251010101010101010120101010101010101010

uuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu





ANALYSIS TYPE: VOLATILES METHOD: CS0390OMATRIX: WATER DATA COMPLETED: 10/10/91

PARAMETERS

CHLOROMETHANEBROMOMETHANEVINYL CHLORIDECHLOROETHANEMETHYLENE CHLORIDE1,1-DICHLOROETHENE1,1-DICHLOROETHANE1, 2-DICHLOROETHENE, TOTALCHLOROFORM1,2-DICHLOROETHANE1,1,1-TRICHLOROETHANECARBON TETRACHLORIDEBROMODICHLOROMETHANE1,2-DICHLOROPROPANEBENZENETRICHLOROETHENECIS-1,3-DICHLOROPROPENEDIBROMOCHLORQMETHANE1,1,2-TRICHLOROETHANEBROMOFORMTETRACHLOROETHENETOLUENE1,1,2,2-TETRACHLOROETHANECHLOROBENZENEETHYL BENZENEACETONECARBON DISULFIDE2-BUTANONEVINYL ACETATE2-HEXANONE4-METHYL-2-PENTANONESTYRENEXYLENES, TOTALTRANS-1,3-DICHLOROPROPENE


UNITS


L UG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/L

E UG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/L

E UG/L

10101010101010101010101010101010101010101010101010101010

1010101010

)01 ISXP8001D ISXP8002'91 07/31/91 08/01/91Hi 0#1 A#41 0#1 T#14

GL340

UUUUUUUUUUUUUUUUUUUUUUUUUUUUNUUUUU

10101010101010101010101010101010101010101010101010101010

1010101010

UUUUUUUUUUUUUUUUUUUUUUUUUUUUNUUUUU

GL362

10102401010101016001010101010101019010101010280010101010101010

1010101010

UU

UUUU

UUUUUUU

UUUU

UUUUUUUNUUUUU





ANALYSIS TYPE: VOLATILES METHOD: CS03900MATRIX: WATER DATA COMPLETED: 10/10/91


ISXP800308/01/910#1 T#20GL363

ISXP800408/01/910#1 T#17GL364

ISXP800508/01/910#1.T#1GL365

PARAMETERS UNITS

CHLOROMETHANEBROMOMETHANEVINYL CHLORIDECHLOROETHANEMETHYLENE CHLORIDE1,1-DICHLOROETHENE1,1-DICHLOROETHANE1,2-DICHLOROETHENE, TOTALCHLOROFORM1,2-DICHLOROETHANE1,1,1-TRICHLOROETHANECARBON TETRACHLORIDEBROMODICHLOROMETHANE1,2-DICHLOROPROPANEBENZENETRICHLOROETHENECIS-1,3-DICHLOROPROPENEDIBROMOCHLORQMETHANE1,1,2-TRICHLOROETHANEBROMOFORMTETRACHLOROETHENETOLUENE1,1,2,2-TETRACHLOROETHANECHLOROfeENZENEETHYL BENZENEACETONECARBON DISULFIDE2-BUTANONEVINYL ACETATE2-HEXANONE4-METHYL-2-PENTANONESTYRENEXYLENES, TOTALTRANS-1,3-DICHLOROPROPENE

UG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/L

101010101010108644101010101010451010101016010101010101010

1010101010

Uu

Uuuu

uuuuuu

uuuuuuuuuuuNuuuuu

10101010101010307110101010101012101010103510101010101010

1010101010

Uuuuuuu

uuuuuu

uuuuuuuuuuuNuuuuu

10101010101010101610101010101010101010101010101010101010

1010101010

uuuuuuuuuuuuuuuuuuuuuuuuuuuNuuuuu







PARAMETERS UNITS

CHLOROMETHANEBROMOMETHANEVINYL CHLORIDECHLOROETHANEMETHYLENE CHLORI-DE1,1-DICHLOROETHENE1,1-DICHLOROETHANE1,2-DICHLOROETHENE, TOTALCHLOROFORM1,2-DICHLOROETHANE1,1,1-TRICHLOROETHANECARBON TETRACHLORIDEBROMODICHLOROMETHANE1,2-DICHLOROPROPANEBENZENETRICHLOROETHENECIS-1,3-DICHLOROPROPENEDIBROMOCHLOROMETHANE1,1,2-TRICHLOROETHANEBROMOFORMTETRACHLOROETHENETOLUENE1,1,2,2-TETRACHLOROETHANECHLOROBENZENEETHYL BENZENEACETONECARBON DISULFIDE2-BUTANONEVINYL ACETATE2-HEXANONE4-METHYL-2-PENTANONESTYRENEXYLENES, TOTALTRANS-1,3-DICHLOROPROPENE

ISXP8006F08/01/91TRIP BLK.GL361



10101010101010101010101010101010101010101010101010311010

10

uuuuuuuuuuuuuuuuuuuuuuuuuuuuNu

10 U10 U10 U10 U

10101010101010101010101010101010101010101016101010101010

1010101010


uuuuuuuuuuuuuuuuuuuuuuuuuuuNuuuuu

10101010101010101010101010101010101010101010101010381010

10

uuuuuuuuuuuuuuuuuuuuuuuuuuuuNu

10 U10 U10 U10 U







PARAMETERS UNITS

CHLOROMETHANEBROMOMETHANEVINYL CHLORIDE .CHLOROETHANEMETHYLENE CHLORIDE1,1-DICHLOROETHENE1,1-DICHLOROETHANE1,2-DICHLOROETHENE, TOTALCHLOROFORM1,2-DICHLOROETHANE1,1,1-TRICHLOROETHANECARBON TETRACHLORIDEBROMODICHLOROMETHANE1, 2-DI.CHLOROPROPANEBENZENETRICHLOROETHENECIS-1,3-DICHLOROPROPENEDIBROMOCHLOROMETHANE1,1,2-TRICHLOROETHANEBROMOFORMTETRACHLOROETHENETOLUENE1,1,2, 2"-TETRACHLOROETHANECHLOROBENZENEETHYL BENZENEACETONECARBON DISULFIDE2-BUTANONEVINYL ACETATE2-HEXANONE4-METHYL-2-PENTANONESTYRENEXYLENES, TOTALTRANS-1,3-DICHLOROPROPENE


10101010101010101010101010101010101010101018101010101010

1010101010


UUUUUUUUUUUUUUUUUUUUU

UUUUUUNUUUUU




ACTIVITY: ISXP8LAB: AATSCASE: 16873

ANALYSIS TYPE: METALS,TOTAL METHOD: CS0390IMATRIX: SEDIMENT DATA COMPLETED: 10/10/91

PARAMETERS

SILVERALUMINUMARSENICBARIUMBERYLLIUMCADMIUMCOBALTCHROMIUMCOPPERIRONMANGANESEMOLYBDENUMNICKELLEADANTIMONYSELENIUM .TITANIUMTHALLIUMVANADIUMZINCCALCIUMMAGNESIUMSODIUM 'POTASSIUMMERCURY


ISXP8101 ISXP810207/31/91 07/31/910#1 A#43A 0#2 A#7MGH299 MGH300

ISXP810307/31/910#3 A#2MGJ031

UNITS

BY I CAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY COLD VA

MG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KG

2.883002.8721.41.414185313000260

1839

1.4

2.8211403600013000140014000.14

U

U

UUUJJJ

N

NUNU

UUU

3.7230004.61301.91.9:.9'1016019000530

2468

1.9

3.7312403500013000190019000.19

U

UUUJJJ

N

NUNU

UUU

3.6110003.6961.81.818206813000270

1619

1.8

3.62369140003900180018000.18

U

UUUJJJ

N

NUNU

UUU




ACTIVITY: ISXP8LAB: AATSCASE: 16873

ANALYSIS TYPE: METALS,TOTAL METHOD: CS0390IMATRIX: SEDIMENT DATA COMPLETED: 10/10/91

PARAMETERS

SILVERALUMINUMARSENICBARIUMBERYLLIUMCADMIUMCOBALTCHROMIUMCOPPERIRONMANGANESEMOLYBDENUMNICKELLEADANTIMONYSELENIUMTITANIUMTHALLIUMVANADIUMZINCCALCIUMMAGNESIUMSODIUM/POTASSIUMMERCURY

BY I CAPBY I CAPBY ICAPSY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY ICAPBY COLD


UNITS

MG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KGMG/KG

VA MG/KG

ISXP8103D07/31/910#3 A#2MGJ032

3.4110003.61101.71.71.7217114000340

1421

1.7

34.32276190004600170017000.17

U

UUUJJJ

N

IUN

UUU

ISXP810407/31/910#4 A#17MGJ033

3.3210009.61001.71.7172820029000530

2235

1.7

3.337110180006800170017000.17

U

UUUJJJ

N

IUNU

UUU

ISXP810507/31/910#5 A#lMGJ034

3.2120003.4641.61.616164710000190

1518

1.6

3.2178166002800160016000.16

U

UUUUJJJ

N

NUNU

UUU





ANALYSIS TYPE: PCBSMATRIX: SEDIMENT

METHOD: CS03900DATA COMPLETED: 10/10/91

PARAMETERS

PCB-1016

PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260

PARAMETERS

PCB-1016PCB-1221PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260


UNITS

UG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KG


UNITS


ISXP810107/31/910#1 A#43AGL341

51 U51 U100 U51 U940 J51 U51 U

ISXP8103D07/31/910#3 A#2GL369

620 U620 U1300 U620 U19000620 U620 U

ISXP810207/31/910#2 A#7GL342

660 U660 U1300 U660 U24000 J660 U«;eo u

ISXP810407/31/910#4 A#17GL370

580 U580 U1200 U580 U15000 J580 U580 U

ISXP810307/31/910#3 A#2GL368

720 U720 U1500 U720 U17000720 U720 U

ISXP810507/31/910#5 A#lGL371

53 l53 i11053 l370053 153 1





ANALYSIS TYPE: SEMIVOLATILES-1 METHOD: CS0390OMATRIX: SEDIMENT DATA COMPLETED: 10/10/91

PARAMETERS

PHENOLCARBAZOLEBIS(2-CHLOROETHYL) ETHER2-CHLOROPHENOL1,3-DICHLOROBENZENE1,4-DICHLOROBENZENEBENZYL ALCOHOL1,2-DICHLOROBENZENE2-METHYLPHENOL (0-CRESOLBIS(2-CHLOROISOPROPYL) ET4-METHYLPHENOL (P-CRESOLN-NITROSO-DIPROPYLAMINEHEXACHLOROETHANENITROBENZENEISOPHORONE2-NITROPHENOL2,4-DIMETHYLPHENOLBENZOIC ACIDBIS(2-CHLOROETHYOXY) METH2,4-DICHLOROPHENOL1,2,4-TRICHLOROBENZENENAPHTHALENE4-CHLOROANILINEHEXACHLOROBUTADIENE4-CHLORO-3-METHYLPHENOL2-METHYLNAPHTHALENEHEXACHLOROCYCLOPENTADIENE2,4,6-TRICHLOROPHENOL2,4,5-TRICHLOROPHENOL2-CHLORONAPHTHALENE2-NITROANILINEDIMETHYLPHTHALATEACENAPHTHYLENE3-NITROANILINE


UNITS

UG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KG

L UG/KGT UG/KGL UG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KG

H UG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KG

E UG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KG

ISXP810107/31/910#1GL34

510055005100510051005100

51005100

5100510051005100510051005100

5100510051005100510051005100510051005100120005100120005100510012000

A#43A1

U

uUuuNUUNUUUUUUUNUUUUUuuuuuuuuuuu

ISXP810207/31/91O#2 A#7GL342

2000020000200002000020000,?0000

2000020000

20000200002000020000200002000020000

20000200002000020000200002000020000200002000020000500002000050000200002000050000

UUUUUUNUUNUUUUUUUNUUUUUUUUUUUUuuuu

7201100720720720720

720720

720720720720720720720

720720720720720720720720720720170072017007207201700

UJUUUUNUUNUUUUUUUNUUUUUuuuuuuuuuuu





ANALYSIS TYPE: SEMIVOLATILES-2 METHOD: CS03900MATRIX: SEDIMENT DATA COMPLETED: 10/10/91

PARAMETERS

ACENAPHTHENE2,4-DINITROPHENOL4-NITROPHENOLDIBENZOFURAN2,4-DINITROTOLUENE2,6-DINITROTOLUENEDIETHYLPHTHALATE4-CHLOROPHENYL PHENYL ETHFLUORENE4-NITROANILINE4,6-DINITRO-2-METHYLPHENON-NITROSODIPHENYLAMINE4-BROMOPHENYL PHENYL ETHEHEXACHLOROBENZENEPENTACHLOROPHENOLPHENANTHRENEANTHRACENEDI-N-BUTYL PHTHALATEFLUORANTHENEPYRENEBUTYL BENZYL PHTHALATE3,3'-DICHLOROBENZIDINEBENZO ( A') ANTHRACENEBIS(2-ETHYLHEXYL)PHTHALATCHRYSENEDI-N-OCTYL PHTHALATEBENZO(B)FLUORANTHENEBENZO(K)FLUORANTHENEBENZO(A)PYRENEINDENO(1,2,3-CD)PYRENEDIBENZO(A,H)ANTHRACENEBENZO( G, H, I)PERYLENE


UNITS


H UG/KGUG/KGUG/KG

0 UG/KGUG/KG

E UG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KG

r UG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KG

ISXP810107/31/910#1 A#43AGL341

51001200012000510051005100510051005100120001200051005100510012000190005100510028000260005100510015000510019000510018000510013000540051005100

UUUUUUUUUUUUUUU

UU

UU

U

U

U

UU

ISXP8102 IS07/31/91 070#2 A#7 o#GL342 GL

200005000050000200002000020000;,'0000;>oooo20000500005000020000200002000050000620002000020000120000130000200002000063000200006300020000840002300048000450002000031000

UUUUUUUUUUUUUUU

UU

UU

U

UJJJJUJ

7201700170072072072072072072017001700720720720170032007207205300710072072027001200260072039001200210034007202100

UUUUUUUUUUUUUUUJUUJJUUJJJUJJJJUJ





ANALYSIS TYPE: SEMIVOLATILES-1 METHOD: CS0390OMATRIX: SEDIMENT DATA COMPLETED: 10/10/91


ISXP8103D07/31/910#3 A#2GL369

ISXP810407/31/910#4 A#17GL370

ISXP810507/31/910#5 A#lGL371

PARAMETERS UNITS

PHENOLCARBAZOLEBIS(2-CHLOROETHYL) ETHER2-CHLOROPHENOL1,3-DICHLORQBENZENE1,4-DICHLOROBENZENEBENZYL ALCOHOL1,2-DICHLOROBENZENE2-METHYLPHENOL (O-CRESOLBIS(2-CHLOROISOPROPYL) ET4-METHYLPHENOL (P-CRESOLN-NITROSO-DIPROPYLAMINEHEXACHLOROETHANENITROBENZENEISOPHORONE2-NITROPHENOL2,4-DIMETHYLPHENOLBENZOIC ACID '-BIS(2-CHLOROETHYOXY) METH2,4-DICHLOROPHENOL1,2,4-TRICHLOROBENZENENAPHTHALENE4-CHLOROANILINEHEXACHLOROBUTADIENE4-CHLORO-3-METHYLPHENOL2 -METHYLNAPHTHALENEHEXACHLOROCYCLOPENTADIENE2,4,6-TRICHLOROPHENOL2,4,5-TRICHLOROPHENOL2-CHLORONAPHTHALENE2-NITROANILINEDIMETHYLPHTHALATEACENAPHTHYLENE3-NITROANILINE

UG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KG

620890620620620620

620620

620620620620620620620

620620620620620620620620620620150062015006206201500

UJUUUUNUUNUUUUUUUNUUUUUUUUUUUUUUUU

5801100580580580580

580580

580580580580580580580

580580580580580580580580580580140058014005805801400

UJUUUUNUUNUUUUUUUNUUUUUUUUUUUUUUUU

5300110005300530053005300

53005300

5300530053005300530053005300

5300530053005300530053005300530053005300130005300130005300530013000

U

UUUUNUUNUUUUUUUNUUUUUUUUUUUUUUUU



SITE: MISSISSIPPI RIVER POOL #15


ANALYSIS TYPE: SEMIVOLATILES-2 METHOD: CS03900MATRIX: SEDIMENT DATA COMPLETED: 10/10/91


PARAMETERS

ACENAPHTHENE2,4-DINITROPHENOL4-NITROPHENOLDIBENZOFURAN2,4-DINITROTOLUENE2,6-DINITROTOLUENEDIETHYLPHTHALATE4-CHLOROPHENYL PHENYL ETHFLUORENE4-NITROANILINE4,6-DINITRO-2-METHYLPHENON-NITROSODIPHENYLAMINE4-BROMOPHENYL PHENYL ETHEHEXACHLOROBEN Z ENEPENTACHLOROPHENOLPHENANTHRENEANTHRACENEDI-N-BUTYL PHTHALATEFLUORANTHENEPYRENEBUTYL BENZYL PHTHALATE3,3'-DICHLOROBENZIDINEBENZO(A)ANTHRACENEBIS(2-ETHYLHEXYL)PHTHALATCHRYSENEDI-N-OCTYL PHTHALATEBENZO(B)FLUORANTHENEBENZO(K)FLUORANTHENEBENZO(A)PYRENEINDENO(1,2,3-CD)PYRENEDIBENZO(A,H)ANTHRACENEBENZO( G, H, I)PERYLENE

UNITS

UG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KG

ISXP8103D07/31/910#3 A#2GL369

620150015006206206206206206201500150062062062015002400620620550063006206203000870270062044001300200039007501400

ISXP810407/31/910#4 A#17GL370

UUUUUUUUUUUUUUUJUU

JUUJUJUJJJJJJ

58014001400580580580580580580140014005805805801400360061058057005400580580270064027005803400100015002400580580

UUUUUUUUUUUUUUUJJUJJUUJUJUJJJJUU

ISXP810507/31/910#5 A#lGL371

54001300013000530053005300530053005700130001300053005300530013000310007600530038000400005300530025000530030000530027000530020000820053005300

UUUUUUU

UUUUUU

U

UU

U

U

U

UU





ANALYSIS TYPE: VOLATILES METHOD: CS0390OMATRIX: SEDIMENT DATA COMPLETED: 10/10/91

PARAMETERS

CHLOROMETHANEBROMOMETHANEVINYL CHLORIDE .-CHLOROETHANEMETHYLENE CHLORfDE1,1-DICHLOROETHYLENE1,1-DICHLOROETHANETRANS-1,2-DICHLOROETHYLENCHLOROFORM1,2-DICHLOROETHANE1,1,1-TRICHLOROETHANECARBON TETRACHLORIDEBROMODICHLOROMETHANE1,2-DICHLOROPROPANEBENZENETRANS-1,3-DICHLOROPROPENETRICHLOROETHYLENECIS-1, 3-DICHLOROPROPENEDIBROMOCHLOROMETHANE1,1,2-TRICHLOROETHANEBROMOFORM1,1,2,2-TETRACHLOROETHENETOLUENE1,1,2,2-TETRACHLOROETHANECHLOROBENZENEETHYL BENZENEACETONECARBON BISULFIDE2-BUTANONEVINYL ACETATE2-HEXANONE4-METHYL-2-PENTANONESTYRENEXYLENES, TOTAL


UNITS


N UG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KG

E UG/KGUG/KGUG/KGUG/KGUG/KGUG/KG

E UG/KGUG/KG

E UG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KGUG/KG

1515

ISXP810107/31/910#1 A#43AGL341

UU

8801515151515151515151515151515151515151515151515171515

15151515

UUUUUUUUUUUUUUUUUUUUUUUUUUNUUUU

202020202020;iO;>o202020202020202020202020202020202020662020

20202020

ISXP810207/31/910#2 A#7GL342

UUUUUUUUUUUUUUUUUUUUUUUUUUUUUNUUUU

2222222222222222222222222222222222222222222222222222222222

22222222






ANALYSIS TYPE: VOLATILES METHOD: CS03900MATRIX: SEDIMENT DATA COMPLETED: 10/10/91


ISXP8103D07/31/910#3 A#2GL369

ISXP810407/31/910#4 A#17GL370

ISXP810507/31/910#5 A#lGL371

PARAMETERS UNITS

CHLOROMETHANEBROMOMETHANEVINYL CHLORIDE .CHLOROETHANEMETHY-LENE CHLORIDE1,1-DICHLOROETHYLENE1,1-DICHLOROETHANETRANS-1,2-DICHLOROETHYLENCHLOROFORM1,2-DICHLOROETHANE1,1,1-TRICHLOROETHANECARBON TETRACHLORIDEBROMODICHLOROMETHANE1,2-DICHLOROPROPANEBENZENETRANS-1,3-DICHLOROPROPENETRICHLOROETHYLENECIS-1,3-DICHLOROPROPENEDIBROMOCHLOROMETHANE1,1,2-TRICHLOROETHANEBROMOFORM1,1,2,2-TETRACHLOROETHENETOLUENE71,1,2,2-TETRACHLOROETHANECHLOROBENZENEETHYL BENZENEACETONECARBON BISULFIDE2-BUTANONEVINYL ACETATE2-HEXANONE4-METHYL-2-PENTANONESTYRENEXYLENES, TOTAL


1919191919191919191919191919191919191919191919191919251919

19191919


1818181818181818181818181818181818181818181818181818251818

18181818


1616161616161616161616161616161616161616161616161616251616

16161616






ANALYSIS TYPE: VOLATILES METHOD: CS0390OMATRIX: SEDIMENT DATA COMPLETED: 10/10/91


PARAMETERS UNITS

CHLOROMETHANEBROMOMETHANEVINYL CHLORIDECHLOROETHANEMETHYLENE CHLORIDE1,1-DICHLOROETHYLENE1,1-DICHLOROETHANETRANS-1,2-DICHLOROETHYLENCHLOROFORM1,2-DICHLOROETHANE1,1,1-TRICHLOROETHANECARBON TETRACHLORIDEBROMODICHLOROMETHANE1,2-DICHLOROPROPANEBENZENETRANS-1,3-DICHLOROPROPENETRICHLOROETHYLENECIS-1,3-DICHLOROPROPENEDIBROMOCHLOROMETHANE1,1,2-TRICHLOROETHANEBROMOFORM1,1,2,2-TETRACHLOROETHENETOLUENE,1,1,2,2-TETRACHLOROETHANECHLOROBENZENEETHYL BENZENEACETONECARBON DISULFIDE2-BUTANONEVINYL ACETATE2-HEXANONE4-METHYL-2-PENTANONESTYRENEXYLENES, TOTAL



1010101010101010101010101010101010101010101010101010171010

uuuuuuuuuuuuuuuuuuuuuuuuuu

uuN

10 U10 U10 U10 U



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