平成30年3月29日（公印省...

032 9

30 29

2018

1998 10

178 1998

2018

1998

30

2 2

10

11

12

13

14

15

16

17

18

19

20

21

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23

24

25

30 29 31 9 30

2018

Japanese Pharmaceutical Excipients

5

1993 1993206

6 1994 92 6 1 297 8 l996 99 1 396

10 1998 42 32 2 436 14 488

14 3 29 0329001

6

14 8 22 0822008

42

15 6 4 0604001

1998

44 31 1

18 3 31 0331005

2

18 3 31 0331023

1998

5 21

19 9 28 0928001

1

24 9 28 0928 7

2

24 12 4 1204 1

1998

12 43 2

26 2 28 0228 1

1

28 3 7 0307 3

3

29 12 1 1201 3

1

2018 5

25 8 4 489

2018 2018Japanese Pharmaceutical Excipients 2018JPE2018

6

2 2 2

300 1000 2 NL L L L E

DL dl 5 SBR 55vol 70vol 50 2 21,3

201 LD D 5 L L L L

95vol 99vol NL DL- NN

30

n N ,N DL L

45 55 60 1000

E d 20E.O.

2,2,2

50vol 95vol 99.5vol N 2910 400 dl 95vol 99vol 1,3

2910 A 1,2,6 -33,5t4

317 2020 4267 5439 1055 12040 16030

19667 204 208 5 10 20 40 50 60 100 5E.O. 7E.O. 5E.O. 35 20 40 60 65 2000 d

200 300 600 1000 1540 D D

D

D n L LD S

DL N2 2 6E. O. 6E.O.

NL- 95vol 5 DL DL

- 1 -

6 8 11 14 47

- 2 -

C3H4O272.0699.0 1g 20mL 1mol/L

2 1mol/L 1mL=72.06mg C3H4O2

1000 21,3

0.1g 9510mL 2 L 21,3 2 21,399.0

21,3 4,4 4,4

3 99 4,4

99.0

2.1g 25mL 10L

2

C38H60O18

20mg 10mL

1mL 100mL 20L

- 3 -

1mL 10mL 20L 713

3 0.67kPa 50 12

C20H30O3

10mg 10mL

1mL 100mL 20L

1mL 10mL 20L 713

3 0.67kPa 50 12

A C38H60O17

20mg 10mL

5mL 100mL 20L A A

- 4 -

2mL 10mL 1mL 10mL 20L A A 713

A 4 0.67kPa 50 12

3A 24

0.67kPa 8991

99.5

2 105 2 0.10g 5mL 1mL

200mL 10L 110080401 10cm 105 10

C8H10O99.0 0.175g 99.5100 mL

1L

1.0

95vol

3

- 5 -

95vol99vol

0.10g 5mL 1 100mL 5mL 1 0.5g 2L 2

99.0 3mm 2m

180250m 15

185 25

C32H50O13

20mg 10mL

1mL 100mL 20L

mL 10mL 20L 713

6 0.67kPa 50 12

- 6 -

A C44H70O23

20mg 10mL

1mL 100mL 20L A A

mL 10mL 20L A A 713

3 0.67kPa 50 12

C C44H70O22

20mg 10mL

5mL 100mL 20L

C C

2mL 10mL 1mL 10mL 20L C C 713

C 3 0.67kPa 50 12

- 7 -

C3H4O2

1114 98.0 1.5g 50mL 1molL

2 1molL 1mL72.07mg C3H4O2

300

CH2CHCOOC2H5

LD 2 C11H20O2

95

n 25D 1.43 d 2020 0.881 213 99.0 2

n C7H12O2

n 20D1.4171.419 d 20200.8990.902 10g 25mL

3 0.1mol/L 0.28mL

98.5 1g 0.5mol/L 50mL

2 0.5mol/L 3

0.5mol/L 1mL=64.09mg C7H12O2 n

CH2CHCOOCH3

- 8 -

95 n 25D 1.40 d 2020 0.957 76.5 80 99.0 2

p C7H9NO

5760

p p 1.23g 1.66g

100mL

p p 0.5g 100g

21,3 Bacillus subtilis var. Biotecus

1g 77008500

95

1

C6H5COOC4H9 95

237 1250002L 2

22 2 2

- 9 -

2 2

180mL n 1mL

1mL 5.0mL 280400nm 0.01

300mL 75mL

150mL 10

0.2g 20mL 1mL 100mL 10L

3

1mL 10mL 10L 713

1132005mL 5mL 10L 1 2.0

10L 6 1.0

0.350.40

1220mL

- 10 -

n CH3(CH2)18CH3 3637

95

1g 10mL

1g 10 1.3kPa408

99.5

35

C4H10O4

D

D

FeCl24H2O JIS K 8137

1g 2mL 20mL

10 g 20mL 95 200mL 0.5mol/L 150mL 1.5mL 30

7g

- 11 -

0.02g 100mL

0.5g

21510mL D

LaCl37H2O .99.5

0.51g18 . 95.0. 1.0g100mL

. 10mL 40mL 1g 111111 pH5.56.5 0.01mol/L 0.3mL10

0.01mol/L 1mL =3.714g LaCl37H2O

88.30g 2750500mL

1000mL

C14H14ClN3HCl 1

100 1mL 30mL 1mL 110120

(CH3)2NHHCl

0.1mol/L 1000mL HCl36.463.646g

9.0mL 1000mL 500650 4050

0.15g 30mL 3

- 12 -

0.1mol/L

0.1mol/L 1mL=5.299mg Na2CO3

10001055

95vol99vol

0.127g 50mL A

8 2.5g 100350100mL B

A B

1,2,6 3.5g 100mL

n d 20200.8710.876

11g 200mL (100)800mL

HIO42H2O1

21.9g 1003g 100mL

D 10.6g 100mL

D

- 13 -

pH10.0 2.47g 600mL 2.7mL1002.3mL 1000mLII 1000mL 0.2mol/L800mL

0.2mL 100mL

15mol/L 1000mL HCOOH46.03690.45g

705g 1000mL 10mL 1000mL 10mL

0.1mol/L 3

0.1mol/L 1mL=4.603mg HCOOH

HCOONa JIS K8267

5g6g100mL

8 8 2.5g 100350100mL

Cl Cl 75

150m

Cl 20g

15mm 300mm25mL 2

OH

3001000m

- 14 -

OHC(CH2)3CHO100.12

187189

121mL pH10.0

100mL 25mL pH10.0 100mL 30

HOOC(CH2)3COOH132.12

96100 98.0 0.13g 40mL 0.1mol/L

2 0.1mol/L 1mL=6.606mg C5H8O4

p CH3C6H4(OH) JIS K 8306

0.1g 0.3g

(95)100mL 400mL d

95 n 20D1.4701.480 d 20200.8660.886 95vol99vol

10

- 15 -

HOOC(CH2)2COOH JIS K 8344

0.1mol/L 1000.6g 100mL

2mol/L 1006g 50mL

6 g 1001000mL

110

CuO79.55 28

95 98.0 0.2g 10mL 3mL

250mL 25mL 75mL 6mL 0.2mL 0.05g 0.01mol/L

0.01mol/L 1mL=0.7955mgCuO

21,3

C23H24N4O2H2O JIS K 9565

2910 400 1g 6mol/L 60mL

100mL 2910 400

- 16 -

C6H15NO2

45 2970cm-12830cm-11456cm-11374cm-11161cm-11030cm-1 929cm-1

3

R f 0.7

C4H11NO2

3300cm-12920cm-11455cm-11125cm-11065cm-1 941cm-1 3R f

0.5

0.30 g 10mL 0.5mL

435025mL

2,25 C10H6N4O4S2

153 0.101g 2

300mL 75mL

150mL 10

1mol/L 63mL 1000mL

15g 50mL 99.5400mL

- 17 -

0.5mol/L 35g 20mL

1000mL

10mol/L 420g 1000mL

0.1mol/L 4.5g 50mL

1000mL

0.5g 15 100mL

200g

150100mL 2 100mL 2 50g 1

CH3(CH2)15N(CH3)3Br

245 95

C21H38ClNH2O358.01

8084 4.55.5 0.201g 99.0102.0 0.2g 75mL 10mL

120000.4mL 2150005mL 0.02mol/L 1

- 18 -

0.02mol/L 1mL=6.800mg C21H38ClN

600800m2/g

2910 0.011m 500550m2/g

19667 0.01g 10080mL 32mL

1g 1g

100mL

2910 0.2mol/L 0.1mol/L

50g 0.2mol/L 1mL7.133mg KIO3

0.5g5mL95100mL

45

- 19 -

3

810 0.1mol/L

(C6H10O5)nxH2O JIS K8646

4,4 0.25g

1g 500mL

4,4 C17H22N2

95 9091

28325mL 35g 2mol/L

500mL DD

D

C9H21NO3

3360cm-12970cm-12820cm-11455cm-11375cm-11136cm-11060cm-1 965cm-1

3

R f 0.8

2,4,6 2,4,6 10g

800mL 282810mL 1000mL

- 20 -

1,3,5 C6H3(NO2)3 N ,N

95 123

1,3,5 0.1g N ,N

310100mL

C18H15OP

156158 1g 10mL C18H15OP98

24 10mg

100mL 1mL 6733 100mL 20L

2

100

6.5 g 14mL

2814.5mL 32mL 40mL 48 5mL 2mL

- 21 -

N 1 C10H7HNCH2CH2NH22HC1 JIS K 8197 5

0.04g 13100

100mL N L DL

C10H6(OH)2

95 122124 L10002 100001mL 90 1

58 C9H6O2N2

245 0.052g. 20mg A20mL 1mL

20mL 10L 58 58

254nm 2.1mm 100mm 3m

25 A 1.0g 1L B 1.0g 1L A B

Avol Bvol

02 0 100 26 95 5 69 95 5

910 0 100

- 22 -

0.4mL58 5

58 2

5g 3g

100mL

2g 50mL

32.8g 10010mL 100mL 25mL 100mL

d d

d

1.12g 300mL

250mL 27g 400mL 100mL 34

2g 5mL

95 20mL 10mL 5g 95 50mL 20mL

0.5g 80mL 1mL 100mL

1.5g 6.0g 500mL

110300mL 1000mL

- 23 -

CH3COCOOH

95

98.0 2g 100mL 1mol/L

2 1mol/L 1mL=88.06mg C3H4O3

dl dl

dl dl C5H7NO3

95 0.1g 50mL 1mL

100mL 10L

dl dl

210nm 4mm 15cm 5m

40 1500 dl 5 4mg L 25mg 50mL 10LLdl

10L dl 10

dl 3 dl

- 24 -

1 10g 10mL 25301 100mL 2,2,2

4tert41,1 C1114O2

3g 50mL

2 30 0.1mol/L 0.1mol/L

1g 9550mL

N N 0.2g 100mL

N L DL 0.05mol/L 3mL

0.1g 25mL

C16H34O .

4555 95.0 0.1g 99.599.5

10mL . 0.5L

195.0

0.25mm 2030m

595 0.250.53m

50 325 10 1 20

- 25 -

1.0 mL 99.5 100mL 0.5L 1 515

1 3

n 1mL 25mL

280400nm 0.00

53,62 C13H14N2O4

10g 300mL 320 pH78 7080 2 502mol/L pH3.0 250mL 320 pH7 1g 2mol/L pH3.0

0.025g 50mL 20L 4

4 53,6298.0

0.1g 10mL 100mL 2000

Li2B4O7

95 1.01g9801 98.0

- 26 -

2g 50mL 1mol/L 40mL 1mol/L 2

1mol/L 1mL=84.5mg Li2B4O7

400 400

400 2910 400

C12H24O11

0.51g0.67kPa 803 1g 10mL

10L 99.0

8mm 3050cm 510m

50 15 1g 10mL

7 10L 515mm

2

- 27 -

n

C3H4O4 99.5

: 135 0.1%2g 97.0% 0.2g 50mL 0.1mol/L

0.1mol/L =5.203mg C3H4O4

30 C4H6O2

n 25D1.4301.432 d 20201.0141.017 98.5 0.3g 50mL 0.1mol/L

3 0.1mol/L 1mL=8.609mg C4H6O2

n CH2C(CH3)COOC2H5

2 C12H22O2

95

n 25D 1.44 d 2020 0.884 229 1.0L

298.5

3mm 3m

- 28 -

20M 150180m 10

80 1 4 200 2 20 1.0L 2 70

2 2 2 2

CH2C(CH3)COOCH2CH2N(CH3)2

E

C16H30O2

95

n 25D 1.44 d 2020 0.873 1651.3kPa 1.0L

98.5

3mm 3m 150180m 5

120 1 4 220 21 1.0L 70

2 2 2

- 29 -

CH2C(CH3)COOC4H9 E

C5H8O2

98.0 1L

98.0

0.25mm 30m 20M 0.25m

50 150 10 200 250 3 1120 3

1L 20000 0.62.0

1L 6 8

E

LS LiBO22H2O

1 1.0g 40mL 2 0.9g 0.01mol/L 0.25mL

0.010 95.0

- 30 -

0.2g 50mL 150.1mol/L FF 34

0.1mol/L 1mL=8.578mg LiBO22H2O

4 C4H6N2

95 262264 4648

0.1g 95100mL

0.01g 100mL

N N 500mL 12g

0.03g 50g 1000mL

C3H6N6 2,4,6S

25095

C7H8O2124.14

95 5253 1.0g 20mL 3.01g0.67kPa24 97.0 3mg

0.01mol/L 1mL=0.2069mg C7H8O2

- 31 -

10mL 100mL

10001055

1 C18H37I

95.0 0.5g 10mL 1L

1-

100

0.25mm 30m 0.25m

250 250 250 1 5 1100 1 4

1g 80mL

20mL L

0.005molL 0.5molL 10mL 1000mL

- 32 -

0.4g 20mL 1530mL

MnSO445H2O JIS K8997

0.025 mol/LpH2.0 0.851g 250mL

pH2.0 E

0.0625mol/LpH2.0 8.9g

8.5g 1000mL pH2.0 E

0.125mol/LpH2.0 17.8g

17.0g 1000mL pH2.0 LS

pH2 1L 85pH2

LD 1g 300mL

30 5 C

2.0g4mL 2 200mL

0.1mol/L 2 1000mL HCl36.4613.6461g

9.0mL 2 1000mL 1mol/L 0.15g

- 33 -

30mL 0.1mol/L 1mL=5.299mg Na2CO3

0.01mol/L 1000mL [Zn(CH3COO)22H2O219.50]2.195g

0.05mol/L 5

0.01mol/L 0.1mol/L

10

0.25mol/L 1000mL NaOH39.9979.999g

11g 1mol/L

1mol/L 0.7g

0.25mol/L 1mL=24.275mg HOSO2NH2 1mol/L

0.025mol/L 5mL

100mL

0.05mol/L 1000mL NH4SCN

76.123.806g 0.1mol/L 2

112mol/L 1000mL K2Cr2O7294.1824.515g

100110 34

24.515g 1000mL

- 34 -

16mol/L 1000mL K2Cr2O7294.1849.03g

100110 34

49.03g 1000mL

DD

D

0.004mol/L

C19H42BrN364.45 1.45g 1000mL

0.01mol/L

C21H38ClNH2O358.013.400g 1000mL

0.004mol/L 1000mL C27H42ClNO2448.09

1.7924g 1.79g

1000mL 0.004mol/L 10mL 100mL

25mL 15mL 20mL 1 0.04mol/L 1 1g 1000mL 10mL 100mL25mL 15mL 20mL0.004mol/L 1mL 2 1 amL

- 35 -

30mL 100mL 25mL 15mL 1 bmL0.004mol/L

mL=a 1010b

0.004mol/L 1mL=0.004mg

0.01mol/L 1000mL KIO3214.002.140g

0.05mol/L 5 201

0.1mg/mL 1g

100mL 1mL 5 100mL5 14 mg/mL 35

500600 1.65g

1000mL 10mL 1000mL 1mL Cl 0.01mg

0.05mol/L 30mL9540mL

3mL 0.02mol/L 0.1mol/L 100mL 200mL

1.631g 1000mL

10mL 100mL 1mL NO3 0.1mg

- 36 -

1.67g 5g 1540mL 1000mL 1mL Ti1.00mg 2910 400

10mL 100mL

1mL Na0.1mg

105 2

450 3 4.952g 92001000mL 1mL Mg1.00 mg

JIS K8160MnCl24H2O3.60g 50mL

10mL 1000mL 10mL 100mL 1mL Mn0.01mg

6.107g 0.01mol/L

1000mL 1mL Li1.00mg

750 1.81g

1000mL 10mL 1000mL 1mL SO4 0.01mg

100m JIS Z 8801-1 3 JIS B 7503 0.01mm 5mm

- 37 -

110560

Acrylic AcidOctyl Acrylate Copolymer

1734cm-11461cm-11381cm-11257cm-1 1163cm-1

150.0g 300mL

500mL 300mL 30 301 No.5 10 1 9000mPas

mPas=400 5.0g 80mL 30

100mL pH 3.55.5 25mL 1

2.0mL 16ppm 10mL 1 4ppm 5mL

0.002mol/L 10mL 1mL 3 0.1g 5 0.01mol/L 5mL 0.002mol/L 1.0mL

0.51g

- 38 -

A E B F C G D H

65mm

130mm

80mm

- 39 -

109602 2 2-Ethylhexyl AcrylateVinylpyrrolidone Copolymer Solution

2N2

16 N14.012.53.1

d 2020 0.94

1730cm-11690cm-11460cm-11420cm-11270cm-1 1170cm-1

500mL 85mm 120mm

250.5

2 15851 5000mPas

1.0g 2

2.0mL 20ppm 2.0g 3 1ppm

1.0g 150mL

100mL 121 1

pH 20mL pH 1.0

5mL 0.002mol/L

20.0mL 1mL 3 0.10g 10 0.01mol/L 5 5.0mL 0.002mol/L 2.0mL

- 40 -

A E B F C G D H

2 1.0g

8mL 20mL 2 0.20g 2.00g 100mL 1mL 100mL 10mL 8mL 20mL 1L

65mm

130mm

80mm

- 41 -

2Q Ta Q Tb 2 Q Sa Q SbQ Ta Q SaQ Tb Q Sb

n 340000

3mm 2m 20M 180250m 10

140 2 5 1L 2

61.568.51g1053 0.55g 0.08g

0.005mol/L 1mL=0.1401mg N

- 42 -

122111 2

2

2-Ethylhexyl Acrylate2-Ethylhexyl Methacrylate Dodecyl Methacrylate Copolymer Solution

2 2

181

d 2020 0.94

2930cm-12860cm-11730cm-11465m-1 1178cm-1 0.050.15g

20mL 50mL 1.0m 350.1 1 1.1

1.0g 4

2.0mL 20ppm 2 2

1g 10mL 6 1mL 1mL 2 2 0.1g 100mL 5mL 100mL 1mL 1mL 2L 2 2 Q TaQ TbQ Tc2 2 Q SaQ Sb Q Sc 2 2 0.2 2 2

- 43 -

= M aQ TaQ SaM bQ TbQ SbM c

Q TcQ Sc

1MT

12

M a 2g M b 2g M cg M T g

125000

0.22mm 25m

1486 0.25m

50 1 10 220220 3

18 15

2 2

0.1g 100mL 5mL 100mL 2mL 20mL 1mL 1mL 2L

713 2L 2

2 5

2 L 6 5.0

1g 105 2 30.070.0

0.105g

- 44 -

120032

Ethyl AcrylateMethyl Methacrylate Copolymer Dispersion

100E.O.

95

pH 5.58.6

3mL 105 1.5 10mL

0.5mL 1mL 3

1 105 1.5 2980cm-11730cm-11447cm-11380cm-1 1160cm-1

47mm2/s 1 20 d 20201.0351.050

1.0mL 25mL 3 0.1mol/L 0.70mL

1.0g 4 2.0mL20ppm

1.0g 3 2ppm 10.0g

50mL 10mL 5mL 5mL 10mL 0.10g 0.10g 100mL 5mL 50mL 5mL 50mL 10mL 5mL 5mL 10mL 20L

- 45 -

205nm 4mm 15cm 5m

40 41 12 20L

20L 20mm

1g 105 3 28.531.5

0.34g 105 1 1mL

- 46 -

109097

Silkfibroin Acrylate Copolymer

800

95

1g 100mL 10mL 10mL 1mL

0.5g 1220mL 3

14 5mL 23

120 pH 0.20g 100mL pH 6.0

8.0

0.10g 50mL 3mL 20 30mL 100mL 2

1.0g 2 2.0mL20ppm

1.0g 3 2ppm 5.0g 10mL

60 0.050g 50mL 1mL 10mL 3.0L

4mm 2m 180250m

- 47 -

5 1

140 3

15.01g1054 45651g

- 48 -

110680 300

Starch Grafted Acrylate 300

14.2

230250

0.5g 100mL 10

10g 10g 5

5.0g 9550mL 10 G4

1.0g 200mL 25mL 3 25mL 1

1.0g 2 2.0mL20ppm

2.0g 3 1ppm 365nm 5.0g 10mL

4 0.010g 200mL 5.0L

3mm 3m 20M 180250m 10

130 20

- 49 -

5.0L 510mm

10.02g1053 40501g 1.0g 200mL 30

No.22 2.78.0kPa 1g 5070mL

- 50 -

109099 1000

Starch Grafted Acrylate 1000

111

95 230250

0.1g 100mL 10

10g 3 10g 5

5g 9550mL 10 G4

0.20g 200mL 25mL 3 25mL 1

1.0g 2 2.0mL20ppm

365nm 5.0g 10mL 4

0.010g 200mL 5L

H T H SH T H S

3mm 3m 20M 180250m 10

130 20 5L 510mm

- 51 -

10.02g1053 40.055.01g 1.0g 200mL 30

No.2 22.78.0kPa 1g 6080mL

- 52 -

111960 2

Emulsion of Methyl Acrylate and 2-Ethylhexyl Acrylate Copolymer

230E.O.

d 2020 1.02 pH 2.03.0

0.5g 952mL

5mL 5mL

0.5mm 20mm 5 2950cm-11740cm-11460cm-1 1160cm-1

A E B F C G D H

300mL 251 H G F 12 1 C 2 100500mPas

5

- 53 -

0.5g 15mL 25mL 5mL 0.005mol/L 0.40mL 0.192

1.0g 2 2.0mL20ppm

2.0g 3 1ppm 2 10.0g

10mL 15

- 54 -

0.100g 2 0.500g 100mL 1mL 10mL 2.0L

2 2

4mm 2m 4000 150180m 30

100 150 1 5

2 17 2 L 2

1g 105 3 5761

0.52g

- 55 -

100297 Adipic Acid

C6H10O4146.14

C6H10O499.0

95

1205mL pH 7 23

0.05g 0.05g 1mL 13010 25 10mL

1690cm-11410cm-11280cm-11195cm-1 926cm-1 151.5154

2.0g 2mL 0.4mL 1mL 15mL 1 1001202mL 10mL 50mL 2.0mL1001202mL 50mL 10ppm

1.0g 3 2ppm 0.8g 50mL 1mL

200mL 20L

210nm 4mm 25cm 510m

25

- 56 -

0.05mol/L 15 pH 2.5 850mL 150mL

15 0.08g 0.08g 100mL 20L 3

20L 515mm

2 0.201g 0.5g 75mL 0.5mol/L

2 0.5mol/L 1mL=36.536mg C6H10O4

- 57 -

110681

Diisobutyl Adipate

C14H26O4258.35

95

5g 50mL

1 50mL 2 6mol/L 100mL 20mL 5g 105 30 144154

5g 1mol/L 25mL 1 2

n 25D1.4271.433 d 20200.9500.957 0.5 420440

1.0g 2 2.0mL20ppm

1.0g 3 2ppm 3.01g1053

- 58 -

101861

Diisopropyl Adipate

C12H22O4230.30

2

95

2980cm-12940cm-11731cm-11374cm-11180cm-1 1110cm-1

n 25D1.4201.430 d 20200.9500.975 1.0 470495 1.0g 2

2.0mL 20ppm 0.101g

- 59 -

101915

Dioctyl Adipate

2C22H42O4370.57

95

0.5g 10mL 10mL

n 25D1.4441.446 d 25250.9180.924 1 298308 0.5

1.0g 2 2.0mL20ppm

1.0g 3 2ppm 0.102g

- 60 -

504017 NL

Sodium N -Acyl-L-glutamate

L N 1117

N14.013.64.0

95

3320cm-12920cm-12850cm-11717cm-11649cm-115851545cm-1 1416cm-1

11001

pH 1.0g 40 100mL pH 5.06.5 105140 1.0g 3

2.0mL 20ppm 5.02g1052 0.07g

0.005mol/L 1mL=0.1401mg N

- 61 -

103749 L

L-Ascorbyl Stearate C

C24H42O7442.59

LC24H42O795.0

95

95110010mL 2,6 12

0.1g 100mL 5mL 110001 1 50 5

1141191g601

2.0g 2 2.0mL10ppm

1.0g 3 2ppm 0.102g 0.2g 9530mL

1515mL 10mL 0.05mol/L 10mL 10 10mL 100mL 5 0.1mol/L 10mL

0.1mol/L 1mL=22.130mg C24H42O7

- 62 -

108638 L

Sodium L-Ascorbate C

C6H7NaO6198.11

LC6H7NaO699.0

(99.5)

110010mL 2,6 12

0.1g 150100mL 5mL 110001 1 50 5

110

20D1031081g10mL100mm

pH 1.0g 10mL pH 6.58.0

1.0g 10mL J

1.0g 2 2.0mL20ppm

0.5g 1 4ppm 0.51g24 0.2g 15050mL

0.05mol/L 1mL 0.05mol/L 1mL9.905mg C6H7NaO6

- 63 -

890033 L

Sodium L-Aspartate L

C4H6NNaO4H2O173.10

L

C4H6NNaO4H2O98.0

95

11005mL 1mL 3

110

20D18.021.0 2g6mol/L 25mL100mm

pH 1.0g 10mL pH 6.07.5

1.0g 10mL 0.30g 0.01mol/L 0.35mL

0.041 1.0g 1 2.0mL

20ppm 1.0g 1 2ppm 0.25g 25mL 1mL

100mL 5L 1100211 10cm 80 30 1120080 10

0.301g5 0.1g 3mL 10050mL 0.1mol/L

- 64 -

0.1mol/L 1mL=8.655mg C4H6NNaO4H2O

- 65 -

109295

Aspartame -L--L-

C14H18N2O5294.30

C14H18N2O598.0102.0

95

160

3330cm-11737cm-11666cm-11379cm-11227cm-1 699cm-1

20D14.516.5 2 g15mol/L 50mL100mm

30 pH 1. 0g 125mL pH 4.56.0

0.10g 16010mL 2.0g 2 2.0mL

10ppm 1.0g 20mL 122.5mL

2 ppm 0.05g 100mL

53,6 2 0.075g 100mL 1mL 100mL 20L 53,62 A T A s A T A s

2.0

- 66 -

210nm 4mm 15cm 5m

40 15.6g 1900mL pH

4.5 2000mL 500mL 0.45m

53,62 4

0.075g53,62 0.075g100mL 2mL 100mL 20L 53,62 10

20L 53,62 5090

2 4.51g1054 0.201g 0.3g 3mL 10050mL 0.1mol/L

0.1mo1/L 1mL=29.431mg C14H18N2O5

- 67 -

100210 Acesulfame Potassium

C4H4KNO4S201.24

C4H4KNO4S99.0101.0

100

99.5

1100000 225229nm

1.0g 100mL pH 5.57.5

1.0g 5mL 2.0g 10mL 1

2020mL 1

14010mL 1415mL 11025 pH 5.45.6 100mL 50mL

3.0ppm 110 2

2.210g 200mL 1000mL 3mL 1000mL 2mL

- 68 -

14010mL 1415mL

2.0g 2 1.0mL5ppm

10.0g

450550 4mL 1150 20mL 1.0mL 1150 20mL 1.0ppm

283.3nm

1.0g 5mL 2mL 2mL 23mL 15mL 23mL 10mL 2ppm

1.0g 100mL 20L

2mL 100mL 2mL 100mL 5mL 100mL 20L

20ppm

227nm 4.6mm 25cm 5m

40 17500032

7 3

- 69 -

2mL 20mL

20L 713

10mg 20mg 100mL 2mL 20mL 20L

4 20L 6

2.0 1.0 1g1053 0.15g 10050mL 0.1mol/L

0.1mol/L 1mL20.12mg C4H4KNO4S

- 70 -

100261

Acetylglycerin Fatty Acid Ester

95

2930cm-1

1749cm-11458cm-11369cm-1 1223cm-1 6.0

2.0g 2 2.0mL10ppm

1.0g 3 2ppm 1.0g

25mL 1 310020mL

15mL 10mL

1.51 g

- 71 -

107780

Sodium Acetyl Tryptophan

C13H13N2NaO3268.24

C13H13N2NaO3

95.0

95

150010mL 4 5mL 3mL

120

0.20g 10mL 0.5g 6mL 50mL

0.01mo1/L 0.30mL 0.021 0.10g 2 2.0mL

200ppm 0.1g 1 A

3.0mL 300ppm 1.0g 1 2ppm 0.10g 25mL 1mL

50mL 5mL 20mL

10L 31 10cm 15080 10

0.51g1053

- 72 -

0.02g 0.005mol/L 1mL=1.3413mg C13H13N2NaO3

- 73 -

001018 Acetone

C3H6O58.08

C3H6O99.0

95 55.557

12001mL 1mL

3 3010cm-1

1719cm-11423cm-11365cm-11224cm-11092cm-1 899cm-1 d 20200.7900.795

30mL 0.02mol/L 0.10mL 15

3.0mL 601503 23 2253mL

125.0mL 105 2 2.0mg

1 g 20mL 100mL 10mL 100mL 10mL 25mL 5 0.05mol/L 25mL 10 310030mL 0.1mol/L 1mL

0.05mol/L 1mL=0.9680mg C3H6O

- 74 -

100694

Azodicarbonamide

C2H4N4O2116.08

C2H4N4O298.6

N14.0147.248.7

95

200 pH 2.0g 100mL 5 pH 5.07.0

1.0g 3 3.0mL30ppm

0.40g 1.0g 0.6g 1.0g 1 10mL 5 10mL 5mL 10ppm

0.51.5g502 450550

1.5g

80025 15 0.15

0.15g 250mL

3mL 75050mL 5mL 60 5 5 0.1mol/L 1mL

0.1mol/L 1mL=5.804mg C2H4N4O2 5mg

- 75 -

0.005mol/L 1mL=0.1401mg N

- 76 -

109215 E

Aminoalkyl Methacrylate Copolymer E

N14.014.06.0

95

0.1g 1mol/L 10mL

232

2960cm-12820cm-12770cm-11730cm-11457cm-1 1147cm-1

10.00g 80mL 100mL 200.1 1 2.55.5mm2/s

0.5g 1mol/L 20mL

1.0g 2

2.0mL 20ppm 1.0g 3 2ppm

1g pH2.0

0.0625mol/L 32 50mL 10mg 20mg 1 3mL pH2.0 0.0625mol/L 32 50mL 1mL pH2.0 0.0625mol/L 3250mL 50L

A T1A T2

- 77 -

A S1 A S2 500ppm 1000ppm

ppm20M S1M T A T1A S1

ppm20M S2M T A T2A S2

M S1mg M S2mg M Tg

205nm 4.6mm 12.5cm 7m

20 pH2.0 0.0625mol/L 119

8

2mL pH2.0 0.0625mol/L 32 10mL 50L

1822 50L 10

50L 6

3.0 1g

50mL 15mg 50mL 5mL 50mL50L

A T A S 1000ppm

ppm100M SM TA TA S

- 78 -

M Smg M Tg

215nm 4.6mm 12.5cm 7m

20 pH2.0 0.025 mol/L 31

2

2mL 20mL 50L

812 50L 1500 2.0

50L 6 2.0

2.01g1054 0.21g 0.2g

0.005mol/L 1mL0.1401mg N

- 79 -

120034

Maltose Syrup Powder

C12H22O11342.3083.0

95 12023 5mL

25D130140 5g

0.6mL 50mL 100mm

pH 1.0g 10mL pH 4.05.5

30.0g 50 100mL 1 420nm 720nm 720nm 0.200 0.100

2.0g 0.01mol/L 1.0mL 0.018

2.0g 0.005mol/L 1.0mL 0.024

5.0g 2 2.5mL5ppm

1.5g 5mL 5mL 1mL 5 5mL 1.3ppm

1.0g 10mL 1 1

7.00.5g 0.052g 1.0g 10mL 10L

- 80 -

C12H22O11= A 2A 1A 2A 3100

A 1 A 2 A 3

8mm 30cm

50 1020 0.5g

100mL 10L

1.6 4.1

- 81 -

101962 DL

DL-Alanine

C3H7NO289.09

DLC3H7NO298.5102.0

95

6mol/L 110

110005mL 1mL 3

0.2g 10mL 0.1g

1622cm-11598cm-11412cm-1 1358cm-1 pH 1.0g 20mL pH 5.57.0

1.0g 20mL 0.5g 0.01mo1/L 0.30mL

0.021 1.0g 1 2.0mL

20ppm 1.0g 1 2ppm 0.20g 10mL 1mL

10mL 1mL 20mL

5L 1100521 10cm 15080 5

0.301g1053

- 82 -

0.201g 0.2g 3mL 10050mL

0.1mol/L 0.1mol/L 1mL=8.909mg C3H7NO2

- 83 -

111961 dl

Allantoin Sodium-dl -Pyrrolidonecarboxylate

C9H12N5NaO6309.21

C4H6N4O3 dl C5H6NNaO3

dl

C9H12N5NaO697.0103.0

95 207

0.02g 50mL

0.02g 50mL dl 0.04g 50mL

5L 1100411 10cm

3g 3mL 30 95 2 1 1 R f

1200 pH 4.0g 100mL pH 5.07.0

0.5g 50mL

0.25g 10mL 50mL 0.01mol/L 0.50mL 0.070

- 84 -

0.8g 5mL 50mL 0.005mol/L 0.50 mL 0.030

1.0g 2mL 50mL 2.0mL 20ppm

1.0g 5mL 2mL 2mL 23mL 15mL 25mL 2ppm

6.00.2g 0.1g

0.05mol/L 1mL=6.184mg C9H12N5NaO6

- 85 -

890034

Sodium Sulfite

Na2SO37H2O252.15

Na2SO37H2O95.0

95 120

1.0g 10mL 2.0g 15mL 5mL

10mL 2mL 2mL 50mL 7mL 2mL 2.0mL 50mL 10ppm

0.5g 10mL 1mL 2mL 5mL 4ppm

49.051.01g1054 0.5g 0.05mol/L 50mL

5 1mL 0.1mol/L 1mL

0.05mol/L 1mL=12.608mg Na2SO37H2O

- 86 -

120035

Alkyl Dimethylamine Oxide Solution

C2H6NOR 250

29.532.0

95100 0.2g 80

2920cm-12850cm-1l467 cm-1967cm-1928cm-1

n 20D1.3771.382 pH 7.68.6 d 20200.9630.973

1.0g 2 2.0mL20ppm

5g 0.25mol/L 75mL 210mL 0.1mol/L 1,10 2 0.5

0.1mol/L 1mL=1.7mg 10g 100mL

15 10050mL 0.1mol/L 1.0

0.1mol/L 1mL=23.4mg 1.01g 2g 100100mL 0.1mol/L

0.1mol/L 0.1mol/L

0.1mol/L 1mL25.000mg 1mg0.1mol/L 0.043mL

- 87 -

100364 Alginic Acid

Phaeophyceae1,4D

1.4L Glycuronoglycan

95

1g 150mL

5mL 1mL

5mL 1mL

5mg 5mL9511001mL 5mL 3 15 5mL 15mL

pH 3.0g 100mL pH 1.53.5 230

1g 50mL1125030mL 1 0.1mol/L 5

0.1mol/LmL

g 5.611

2.0g 800mL pH7

3mL 1 G4105 0.2

1.0g 0.01mol/L 1000mL 5mL 1

1.0g 2 2.0mL20ppm

1.0g 3 2ppm

- 88 -

15.05g1054 4.0

- 89 -

001039

Sodium Alginate

Phaeophyceae

90.0105.0

95

11005mL 1mL

110010mL 1mL

1.0g 100mL pH 6.08.0

0.10g 20mL 1mL 10 50mL 10mL 50mL 0.005mol/L 0.40mL 141mL 50mL 0.960

1.0g 4 2.0mL20ppm

1.0g 3 2ppm l5.01g1054 33.037.01g

A B C D E F G H I20 25g J K L M N

3525 mm

- 90 -

0.25g D 112025mL F

M B 5cm M 12

1 30006000mL E 2 15 G 23mL J 0.25mol/L 25mL 1 5 J

1 2000mL G D E 2

J 0.25mo1/L M K J 15mL 3

- 91 -

K K 11010mL 2

2 0.1mol/L

0.25mol/L 1mL27.75mg

- 92 -

003018

Propylene Glycol Alginate

1,2

95

110010 mL 1mL 56

1mL

3420cm-11745cm-11625cm-1 1035cm-1

75.0

100abc ab c

a b c

0.5g 200mL 0.02mol/L 20 2

0.02mol/LmL0.00352

g 100

1g 300400 2

50mL 0.05mol/L 20mL 1

0.1mol/L 3

0.05mol/LmL0.0198

g 100

- 93 -

1.5 1.0g 2 2.0mL

20ppm 0.5g 3 4ppm

20.01g1054

- 94 -

100418 Pregelatinized Starch

95

1g 50mL 1

4.0g 160mL

pH 4.07.0 1.0g 142mL

1mL 550600 2mL 3 10mL 2

1 2mL 10mL 50mL 142mL 1mL 2mL 3 2.0mL 50mL 20ppm

1.0g 4 10mL 2ppm

2.0mL 20g 12200mL

100mL 3mL 0.01mol/L 0.5mL 0.003

5.0g 20mL 311mL 0.5mL 5

131g1053 0.52g

- 95 -

- 96 -

109280

-Thioglycerol

C3H8O2S108.16

C3H8O2S98.0

95

23 0.5g

11005mL 2mL 1mL

n 20D1.5211.526 pH 1.0g 10mL pH 3.57.0 d 25251.2411.250

1.0g 10mL 1.0g 2 2.0mL

20ppm 1.0g 1 2ppm

5.00.5g 0.101g 0.4g 50mL 0.05mol/L

3mL 0.05mol/L 1mL10.816mg C3H8O2S

- 97 -

100405 Almond Oil

Prunus amygdalus Batsch(Rosaceae )

95

d 20200.9110.918 5.0 188200 1.5 92105 10mL 10mL 0.1mL

15 10mL

1.0g 2 2.0mL20ppm

- 98 -

109100

Ammonioalkyl Methacrylate Copolymer RS

A B

C9H18ClNO2207.708.8511.96 4.486.77

95

232

2950cm-11733cm-11448cm-1 1146cm-12820cm-12770cm-1

10.00g 80mL 100mL 200.1 1 1.04.0mm2/s

2.0g 100mL

25mL 105 4 4.0mg

1.0g 2 2.0mL20ppm

1.0g 3 2ppm 5g

50mL 10mL 72005mL 70mg 20mg 1 5mL 50mL 5mL 50mL 5mL 50mL 10mL 72005mL

- 99 -

20L

AT1 AT2 A S1 A S2 100ppm 50ppm

ppm10M S1M TA T1A S1

ppm10M S2M TA T2A S2

M S1mg M S2mg M Tg

202nm 4.6mm 12.5cm 7m 20 pH2.0 41 8

2mL 10mL 72005mL 20L 1822

20L 1.5

20L 6

2.0 5.01g1054 0.201g A 1g B

2g 5010075mL 30 25mL 0.1mol/L

0.1mol/L 1mL20.77mg C9H18ClNO2

- 100 -

- 101 -

109220 Ammonioalkyl Methacrylate Copolymer Dispersion

A B C9H18ClNO2207.7010.1813.736.118.26C6H8O2112.130.100.30

2.0g 100mL 5mL 100mL 253258nm

1 60 15 2950cm-11735cm-11455cm-1 1145cm-12820cm-1 2770cm-1

150mm2/s 1 20 pH 4.06.0 d 20201.0401.060 3g 105 4 2832

0.52g

A 2g B 4g 90 30 5010075mL 30 25mL0.1mol/L

0.1mol/L 1mL20.77mg C9H18ClNO2 1g 50mL

5mL 50mL 10mL 72005mL 20mg

- 102 -

100mL 1mL 50mL 10mL 72005mL 50L A T A S

C6H8O2(mg)M S A TA S110

M Smg

262nm 4.6mm 15cm 5m

pH2 11 5

50L 1.5 3000

50L 6 2.0

- 103 -

111544 Isoamyl Isovalerate

C10H20O2172.26

C10H20O298.0

95

2960cm-12870cm-11738cm-11468cm-11188cm-1 1169cm-1

n 20D1.4111.414 d 20200.8550.858 1.0

1.0g 3510mL 1.0g 2 2.0mL

20ppm 1.0g 3 2ppm

1g 0.5mol/L 25mL 1 0.5mol/L 3

0.5mol/L 1mL86.13mg C10H20O2

- 104 -

108599 Isocyanuric Acid

C3H3N3O3129.07

C3H3N3O399.0

95

11000 pH 4.35.1 11000011000011

20g 100mL

7 0.1mol/L A1220mL 3 B A B 0.1mol/L 0.05

0.0018fV

S 100

f0.1mol/L V0.1mol/L mL Sg

2.0g 3 20mL 10ppm

2.0g 3 1ppm 0.205g1052 0.01520g700800 2.5g 1235mL

1 9 250m

- 105 -

2g 500mL 50mL 150mL 1430mL 0.25mol/L 20mL 400mL 3 0.1mol/L 0.25mol/L 20mL 200mL 3 0.1mol/L

C3H3N3O3=BA 0.004303f50050 100S

A 0.1mol/L mL B 0.1mol/L mL f0.1mol/L Sg 0.0043030.1mol/L 1mL g

- 106 -

108522

Isostearyl Alcohol

C18H38O270.49

95 d 20200.8300.866 1.0 3.0 180215 12

1.0g 2mL 1mL 500600 2mL 0.5mL 2mL 50mL 2.0mL 2mL 50mL 20ppm

1.0g 3 2ppm 0.101g

- 107 -

103139

Isostearic Acid

C18H36O2284.48

95

d 20200.8620.905 15

A

9.512.5mm

B C 6mm

A D 5mm

B A

E F1 G

120 B 5157mm F B B l4 C 03 E A B A E 25mm 1 B A 3 10 B 17152 73533 3 B

( mm )

- 108 -

175215 12 15

1.0g 0.5g 30mL

0.01mol/L 0.7mL 6mL 30mL 1mL

1.0g 2 2.0mL20ppm

0.105g

- 109 -

111545

Hexadecyl Isostearate

C34H68O2508.90

95

1735cm-1

1185cm-1 d 25250.8300.870 0.5 100120 3.5 1.0g 2

2.0mL 20ppm 0.52g

- 110 -

001062

Inositol

C6H12O6180.16

C6H12O697.0

(99.5) 110 110

3380cm-13220 cm-11446cm-11147 cm-11114cm-1 1049cm-1

223227

1.0g 10mL 2.0g 0.01mol/L 0.30mL

0.005 4.0g 0.005mol/L 0.50mL

(0.006) 0.8 g 1 2.0mL

25ppm 2.0 g 40mL 2mL 0.04 g

2mL 1.0mL 40mL

1.0 g 10mL 1mL 1

1.0g 1 2ppm 5.0g 15mL 4.0mL

3 2 50mL 10mL 10mL 40mL 3

- 111 -

G4

20mL 800.02mol/L 1.0mL

0.51g1054 0.101g 0.2g 30mL

5mL 50mL 10L Q TQ S

(C6H12O6)mgmgQ TQ S

1325

8mm 30cm 8m

Na 65 9

10L

2.0 10L 6

1.0

- 112 -

520128 5

Disodium 5-Inosinate

C10H11N4Na2O8P392.17

5C10H11N4Na2O8P

97.0102.0

95

0.01mol/L

3100003mL 951100.2mL 0.01mol/L 110003mL 10

1205mL 2mL 7mL 10

0.01mol/L 150000

248252nm 110

pH 1.0g 20mL pH 7.08.5

1.0g 20mL 2.0g 1 2.0mL

10ppm 1.0g 1 2ppm 0.10g 20mL 1mL

100mL

- 113 -

5L 1652 10cm 254nm

0.020g 0.01mol/L 100mL 10mL 0.01mol/L 100mL 250nm260nm 280nm A 1A 2 A 3A 1/A 2 1.551.65A 3/A 2 0.200.30

29.00.15g 0.5g 0.01mol/L 250mL

10mL 0.01mol/L 100mL 10mL 0.01mol/L 100mL 250nm A

5C10H11N4Na2O8Pmg A310250000

- 114 -

103095

Powdered Iris Root

Iris germanica Linn Iris pallida Lamarck Iris florentina Linn(Iridaceae )

10g0.5mL

1 1501 5 1101

7

0.8g 3 2.0mL

25ppm 10.01g1052 5.01g 0.5

- 115 -

LPG DME

mm 354366 -132 -1040

mm 9.0

mm 1922 0.5 1

MPa 1.4 1.0 1.5 5 5

g/cm3 0.5000.600 0.5000.650 0.6000.700 5 10

15 mm 5070 5070

g/cm3 0.001 0.2 1.0

g/cm3 0.005

g/cm3 0.01

mm 125145

g/cm3 0.001

LPG DME

003600

Liquefied Petroleum Gas

C3H844.10C4H1058.12C4H1058.12 95.0

d 20200.490.59

LPG

200.5 200.5200.5

98kPa

- 116 -

15g 100mL

80g

1051 0.002

0.005315g 15mL

3 95.0

A Pf P+A IBf IB+A Bf B

A Pf P+A IBf IB+A Bf B+A af a+ 100

- 117 -

A f PIBBa

f

f

0.89 0.80 0.99 0.90 1.04 1.03 1.00 1.00 1.06 1.12 1.01 1.04

3mm 610m n ,

2535 180250m

40 6

1mL

1.5 1mL 6

2.0

40

- 118 -

122112

Liquid Polyisoprene Rubber

1,4

95 2960cm-1

1644cm -11448cm-11375cm-1888cm-1 837cm-1 5.00g 10mL 250.l

2 20 2401790mPas

d 20200.8760.893 220232 20.0g 2

2.0mL 1ppm 0.10g/dL 1g 10mL 0.101g

- 119 -

109939

Liquid Lanolin

95

1501mL 2mL

250.1 2 20 16502200mPas

d 20200.9380.946 1020

A

9.512.5mm

B C 6mm

D 5mm

B A

E F1 G

120 B 5157mm F B B 14 C 03 E A B A E 25mm 1 B A 3 10 B l7l5

( mm )

- 120 -

2 73533 3 B

3.0 2040 0.8g 500mL

20mL 25mL 2030 1 11020mL 100mL 0.1mol/L 1mL

ab1.269g

a 0.1mol/L mL b 0.1mol/L mL

5g 25mL 10

2.0g 40mL 10

20mL 6mL 50mL 0.01mol/L 1.0mL 0.036

10mL 1mL

5mL 0.002mol/L 0.5mL 10

1.0g 20mL 0.020g 20mL 5L

10cm 12110 10 365nm

110 60 1.0g 2 2.0mL

20ppm 0.51g1051 0.301g

- 121 -

- 122 -

110635

Liquid Sugar

100g 66.568.5g

95

1.5g

0.15g 2mL 4mL

3mL d 20201.328 1 2

20 66.568.5 1 2 1974

10.0g 100mL 20mL

6mL 50mL 0.01mol/L 0.30mL 0.005

40mL 1mL 50mL 0.005mol/L 0.50mL 0.006

10mL 1mL

6.0g 1 3.0mL5ppm

1.0g 1 2ppm 7.5g 100mL

100mL 300mL 50.0mL 5 50mL 10 5 G49510mL 10mL 105 30 0.12g

- 123 -

1

0.

0 0.

1 0.

2 0.

3 0.

4 0.

5 0.

6 0.

7 0.

8 0.

9

56

57

58

59

60 61

62

63

64

65 66

67

68

69

70 71

72

73

74

75 76

77

78

79

80 81

82

83

84

85

1.43

2993

1.

4352

01

1.43

7427

1.

4396

69

1.44

1928

1.44

4204

1.

4464

97

1.44

8807

1.

4511

34

1.45

3478

1.45

5839

1.

4582

17

1.46

0613

1.

4630

26

1.46

5456

1.46

7903

1.

4703

68

1.47

2850

1.

4753

49

1.47

7866

1.48

0400

1.

4829

51

1.48

5520

1.

4881

05

1.49

0708

1.49

3328

1.

4959

66

1.49

8620

1.

5012

92

1.50

3980

4332

13

4354

23

4376

50

4398

94

4421

55

44

4432

44

6727

44

9039

45

1367

45

3713

4560

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56

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54

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46

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47

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47

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47

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54

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65

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45

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19

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13

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46

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47

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88

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52

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47

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4819

29

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69

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37

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28

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80

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44

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44

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44

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84

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12

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47

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47

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47

7614

48

0146

4826

95

4852

62

4878

46

4904

77

4930

66

49

5701

49

8354

50

1024

50

3711

- 124 -

20

0

5 10

15

20

25

30

35

40

45

50

55

60

65

70

75

80

85

15

16

17

18

19

0.29

0.

24

0.18

0.

12

0.06

0.31

0.

25

0.19

0.

13

0.06

0.32

0.

26

0.20

0.

13

0.07

0.33

0.

27

0.20

0.

14

0.37

0.34

0.

28

0.21

0.

14

0.07

0.35

0.

28

0.21

0.

14

0.07

0.36

0.

29

0.22

0.

15

0.07

0.37

0.

30

0.22

0.

15

0.08

0.37

0.

30

0.23

0.

15

0.08

0.38

0.

30

0.23

0.

15

0.08

0.38

0.

31

0.23

0.

15

0.08

0.38

0.

31

0.23

0.

15

0.08

0.38

0.

31

0.23

0.

15

0.08

0.38

0.

31

0.23

0.

15

0.08

0.38

0.

31

0.23

0.

15

0.08

0.38

0.

30

0.23

0.

15

0.08

0.37

0.

30

0.23

0.

15

0.08

0.37

0.

30

0.22

0.

15

0.07

21

22

23

24

25

26

27

28

29

30 31

32

33

34

35 36

37

38

39

40

0.06

0.

13

0.20

0.

27

0.34

0.42

0.

50

0.58

0.

66

0.74

0.83

0.

91

1.00

1.

10

1.19

1.29

1.

38

1.48

1.

59

0.69

0.07

0.

14

0.21

0.

28

0.35

0.43

0.

51

0.59

0.

67

0.75

0.84

0.

93

1.02

1.

11

1.20

1.30

1.

40

1.50

1.

60

0.70

0.07

0.

14

0.21

0.

29

0.36

0.44

0.

52

0.60

0.

68

0.77

0.85

0.

94

1.03

1.

12

1.22

1.31

1.

41

1.51

1.

61

1.71

0.07

0.

14

0.22

0.

29

0.37

0.45

0.

53

0.61

0.

69

0.78

0.87

0.

95

1.04

1.

13

1.23

1.32

1.

42

1.52

1.

62

1.72

0.07

0.

15

0.22

0.

30

0.38

0.46

0.

54

0.62

0.

70

0.79

0.88

0.

96

1.05

1.

15

1.24

1.33

1.

43

1.53

1.

62

1.72

0.07

0.

15

0.23

0.

30

0.38

0.46

0.

55

0.63

0.

71

0.80

0.89

0.

97

1.06

1.

15

1.25

1.34

1.

44

1.53

1.

63

1.73

0.08

0.

15

0.23

0.

31

0.39

0.47

0.

55

0.64

0.

72

0.81

0.89

0.

98

1.07

1.

16

1.25

1.35

1.

44

1.54

1.

63

1.73

0.08

0.

15

0.23

0.

31

0.39

0.47

0.

56

0.64

0.

73

0.81

0.90

0.

99

1.08

1.

17

1.26

1.35

1.

44

1.54

1.

63

1.73

0.08

0.

16

0.23

0.

31

0.40

0.48

0.

56

0.64

0.

73

0.81

0.90

0.

99

1.08

1.

17

1.26

1.35

1.

44

1.54

1.

63

1.72

0.08

0.

16

0.24

0.

32

0.40

0.48

0.

56

0.65

0.

73

0.82

0.90

0.

99

1.08

1.

17

1.25

1.35

1.

44

1.53

1.

62

1.71

0.08

0.

16

0.24

0.

32

0.40

0.48

0.

56

0.65

0.

73

0.81

0.90

0.

99

1.07

1.

16

1.25

1.34

1.

43

1.52

1.

61

1.70

0.08

0.

16

0.24

0.

32

0.40

0.48

0.

56

0.64

0.

73

0.81

0.90

0.

98

1.07

1.

15

1.24

1.33

1.

42

1.51

1.

60

1.69

0.08

0.

16

0.24

0.

32

0.40

0.48

0.

56

0.64

0.

72

0.81

0.89

0.

97

1.06

1.

14

1.23

1.32

1.

40

1.49

1.

58

1.67

0.08

0.

16

0.23

0.

31

0.39

0.47

0.

55

0.64

0.

72

0.80

0.88

0.

96

1.05

1.

13

1.21

1.30

1.

38

1.47

1.

56

1.64

0.08

0.

15

0.23

0.

31

0.39

0.47

0.

55

0.63

0.

71

0.79

0.87

0.

95

1.03

1.

12

1.20

1.28

1.

36

1.45

1.

53

1.62

0.08

0.

15

0.23

0.

31

0.39

0.46

0.

54

0.62

0.

70

0.78

0.86

0.

94

1.02

1.

10

1.18

1.26

1.

34

1.42

1.

50

1.59

0.08

0.

15

0.23

0.

30

0.38

0.46

0.

53

0.61

0.

69

0.77

0.84

0.

92

1.00

1.

08

1.16

1.24

1.

32

1.39

1.

47

1.55

0.07

0.

15

0.22

0.

30

0.37

0.45

0.

52

0.60

0.

68

0.75

0.83

0.

90

0.98

1.

06

1.13

1.21

1.

29

1.36

1.

44

1.52

- 125 -

100mL 100mL 50mL 50mL 100mL

23

0.103g 30g 100mL 200mm

20D 65.5

20D2.8880026

g

2.88800 26 26g 100mL 100

1

- 126 -

102199 Ester Gum

95

1g 5mL 5mL

0.1g 10mL 1

8.0 0.102g

- 127 -

108634 SBR

Styrene Butadiene Rubber Latex

C8H8104.152530C4H654.097075

95

pH 251pH

7.88.2

70 1mm 5cm5cm 1mm 2.3g2 300mL 200mL 60 60

5mL 5 60 10mL 151mL

200mL 510mL 190mL 200mL 5mL 15mm 5mL 10 5mL 15mm 5mL 10

31125

20mL 50mL 2.0mL3112520mL 50 mL 2 5

1ppm 100mL 105

105 2 A mg 20ppm

ppmA B1000

mL

- 128 -

B125mg v 100mL135mL

0.002mol/L 5mL 5 100mL 135mL 0.002mol/L 10mL 5 0.005mol/L 10mL 0.002mol/L

5ppm

ppmA Bf1000

100 0.316

A 0.002mol/L mL B 0.002mol/L mL f0.002mol/L

0.5g 3 4ppm 1g 25mL

0.1g 200mL 1mL 100mL 1mL 25mL 10L H T H SH T H S

3mm 2m 20M 180250m 20

90 9 10L

10L 812mm

2g 2 1mL 10548.052.0

- 129 -

gg 100

- 130 -

110749 55vol 55vol Ethanol

C2H6O46.07

52.957.2vol15

1mL 2mL 1mL

1mL 1001mL 3

d 15150.9200.929

- 131 -

109570 70vol

70volEthanol

C2H6O46.0768.172.2vol15

1mL 2mL 1mL

1mL 1001mL 3

d 15150.8850.895

- 132 -

110566 50

Ethanol 50 50w/w

C2H6O46.0749.051.015

2mL 2mL 1mL

50mL 5mL 1mL 1001mL

3 d 15150.9160.921

20mL 20mL 510 30

20mL 3 0.1mol/L 0.10mL

20mL 2 2 5

30mL 1 3.0mL1.1ppm

20mL 1mL 0.4mL 10mL 5mL

20mL 15 0.02mol/L 0.30mL 15 20 20mL 5mL 5

2mL 80mL 105 1

1.0mg

- 133 -

102258

Ethylcellulose

-OC2H545.0646.551.0 mPas

95 1 g 100mL

100mL

10mg lmL 2mL

5g 9541 95g

5.000g 9541 100mL 9541 100.0g250.1 2

0.20g 20mL 5mL

12 10mL 50mL 0.01mol/L 0.45mL 0.080

1.0g 2 4.0mL40ppm

1.0g 3 2ppm 2.01g1051 0.401g 15mg

1g 100mL 15g 10091150mL

145mL 5mL

- 134 -

E1/2 J20mL 15mg A 6mL A C 1 D G B E 1 2 A 2030 150 60 G J 1510mL 500mL 200mL 1mL 3g 15mL 5 0.1mol/L lmL

0.1mol/L 1mL0.7510mg C2H5O

- 135 -

120313

Ethylcellulose Aqueous Dispersion

0.10.3m

2832 24.529.5C16H34O242.441.73.3C12H25NaO4S288.380.91.7

H2O234.01 50ppm

30mg 1mL 2mL

20mL

252 330 109030 150mPas

- 136 -

pH 4.07.0 5mL

110 3 10g 5mL 60

6872 0.1g 1g 100mL 15g 10091150mL

145mL 5mL

- 137 -

E 12 J 20mL 0.1g A 6mL A C 1 D G B E 1 2 A 2030 150 60 G J 1510mL 500mL 200mL 1mL 3g 15mL 5 0.1mol/L lmL

0.1mol/L 1mL0.7510mg C2H5O

10g 1 6mL

- 138 -

100mL 0.15g16mL100mL 10mL 25mL 15mL 0.004mol/L 1mL

1

0.004mol/L mg

0.004mol/LmLAB

C100K

Amg BmL C 0.004mol/L mL

DK10

EF

D 0.004mol/L mL EmL F g

40mg 20mL 23 4mL 5mL 10mL 2L

0.25g 5mL 10mL 2L

n 11000

3mm 2m 150180m 10

220 1012 2L

- 139 -

4

- 140 -

109317 Ethylurea

C3H8N2O88.11

C3H8N2O97.0

95

0.5g 10mL 2mL 1

0.1g 1mL 1mL 9193

1.0g 20mL 2.0g 0.01mol/L 0.40mL

0.007 2.0g 0.005mol/L 0.40mL

0.010 1.0g 2 2.0mL

20ppm 3.01g853 0.101g 0.4g 200mL

5mL 0.005mol/L 1mL0.8811mg C3H8N2O

- 141 -

102255 Ethyl Vanillin

C9H10O3:166.17

C9H10O398.0

95

1g 5mL

5mL 6070 5

3300cm-11678cm-11583cm-11287cm-11264cm-1 1168cm-1

7678

1.0g 3510mL 2.0g 2 2.0mL

10ppm 0.5g 3 4ppm

0.51g4 0.052g 1g 75mL

15 0.5mol/L

0.5mol/L 1mL83.09mg C9H10O3

- 142 -

- 143 -

122113 2

Cetyl 2-Ethylhexanoate

C24H48O2:368.64

2

95

2920cm-1

2850cm-11736cm-11465cm-11172cm-11145cm-1 722cm-1 2.0 1351654 3.0 1.0g 2

2.0mL 20ppm 0.101g

- 144 -

109236 21,3

2-Ethyl-1,3-hexanediol

C8H18O2146.23

21,3C8H18O298.0

95

0.2mL 5mL 1mL

0.1g 100mL 21,3 0.1g 100mL 10L HPTLC Fertigplatten kieselgel 60F254118cm p 105 10 R f

d 20200.9400.944

APHA 20

15.0g 15mL 2 10mL 2 0.1mol/L 0.85mL

2.0g 2 2.0mL10ppm

1.0g 3 2ppm 0.1010g 21,3 0.1g

95 10mL 2L

- 145 -

21,3 H T H S 21,3C8H18O2mg

21,3mgH TH S

3mm 2m

150180m 3

120 21,3 5 0.1g 9510mL

2L 5

5 21,3 0.8

- 146 -

102242

Ethylmaltol

C7H8O3140.14

C7H8O399.0

95 0.1g 9510mL 3

0.1g 5mL 1mL

5

8993 0.10g 955mL 1.0g 2 2.0mL

20ppm 1.0g 3 2ppm 0.51g 0.051g 0.2g 0.1mol/L

500mL 5mL 0.1mol/L 200mL 0.1mol/L

276nm A T A s C7H8O3mg

mgA TA s

- 147 -

109101 Ethylene Carbonate

C3H4O388.06

C3H4O398.0

95 3438

0.2g 4.5mL 0.5mL

0.1mL

3000cm-11802cm-11165cm-1 1075cm-1 pH 1.0g 0.01mol/L 0.01mol/L pH7.0

10mL pH 5.76.9

1.0g 10mL 2.0g 1 2.0mL

10ppm 1.0g 1 2ppm

0.055g 75g 1000mL

50mL 0.6g 10 0.5mol/L 6


- 148 -

102265

Ethylene Glycol

C2H6O262.07

95

5mL 71003mL 151mL 0.2mL 2mL

1mL 0.5g d 20201.1141.117

5mL 20mL 20.0g 50mL

5 0.05mol/L 0.33mL 2.0g 0.01mol/L 0.40mL

0.007 10.0g 0.005mol/L 0.40mL

0.002 2.0g 3 A

1.0mL 5ppm 0.2010g 20g

0.2mL 0.005

19519895vol

- 149 -

890035

Tetrasodium Edetate Dihydrate

C10H12N2Na4O82H2O416.20

C10H12N2Na4O8

380.1798.5

95

0.01g 5mL 12002mL 2mL 2

12010mL 1mL 2mL

120 pH 1g 20mL pH 10.012.0

1.0g 100mL 10mL 0.5mol/L 15mL 100mL 100mL 20mL 1 pH6.8 5mL 151.0mL23 5mL 2030 50

1.0mL 0.5mol/L 15 mL 1000mL 20mL

2.0g 2 3.0mL15ppm

1.0g 1 2ppm 8.010.01g1955

- 150 -

1g 50mL pH10.7 2mL T 0.04g 0.1mol/L

0.1mol/L 1mL=38.017mg C10H12N2Na4O8

- 151 -

120316

Erythritol

C4H10O4122.12

C4H10O498.0

99.5

3250cm-12970cm-12910cm-11416cm-11256cm-11081cm-1 1055cm-1

119122

2.0g 10mL 2.0g 0.01mol/L 0.30mL

0.005 4.0g 0.005mol/L 0.50mL

0.006 4.0g 1 2.0mL

5ppm 1.0g 1 2ppm 2g N14.01

0.01 5.0g 15mL 4mL

3 2 50mL 10mL 10mL 40mL 3 G4

20mL 800.02mol/L 1.0mL

0.52g1054 0.101g

- 152 -

0.2g 100mL 10mL 50mL 15 2.5g 5 0.1mol/L 3mL


- 153 -

102189 Erythorbic Acid

C6H8O6176.12

C6H8O699.0

95

110010mL 1mL

0.1g 150100mL 5mL

110001 1 50 5

20D16.218.21g10mL100mm

166172

1.0g 10mL J

1.0g 1 2.0mL20ppm

0.5g 1 4ppm 0.401g3 0.301g 0.4g 150

100mL 50mL 0.05mol/L 1mL


- 154 -

890036

Sodium Erythorbate

C6H7NaO6H2O216.12

C6H7NaO6H2O

98.0

95 200

1g 10mL 11002mL 0.1mol/L 4mL

56 2

0.1g 150100mL 5mL 110001 1 5060 5

110010mL 1mL

1100 pH 1.0g 50mL pH 6.58.0

1.0g 10mL J

1.0g 1 2.0mL20ppm

0.5g 1 B 4ppm

0.31g24 1g 150

250mL 50mL 0.05mol/L

- 155 -

1mL 0.05mol/L 1mL10.806mg C6H7NaO6H2O

- 156 -

890037

Aluminum Chloride

AlCl36H2O241.43

AlCl36H2O97.0

95

120 pH 1.0g 20mL pH 2.23.7

1.0g 20mL 2.0g 30mL 50mL 3

40mL 0.1mol/L 0.60mL

1.0g 30mL 953mL 1mL 50mL 30 0.005mol/L 0.20mL 953mL 0.010

2.0g 1 2.0mL10ppm

10.0g 50mL 1210mL301mL 5 100mL 10mL 121mL11001mL 5mL 50mL 5 5.0mL 121mL301mL11001mL 5mL 50mL 5

480nmA TA SA T A S50ppm

1.0g 1 2ppm 1g 250mL 25mL

0.01mol/L 50mL pH4.8 10mL 3 9585mL

- 157 -

0.01mol/L 3mL 0.01mol/L 1mL2.4143mg AlCl36H2O

- 158 -

890038

Stannous Chloride

SnCl22H2O225.65

SnCl22H2O96.0

95

1100

1.0g 10mL 0.5g 100mL 0.5g 1mL 5mL

50mL 0.005mol/L 0.50mL 1mL 50mL 0.048

0.10g 1.0mL0.01

2.0g 2mL 10mL 5mL 1mL 40mL 5mL 15mL 1mL 40mL 20mL 20mL 152mL 50mL 6mol/L 0.3mL 2.5mL

200ppm 4mL 5mL

1.0mL 4mL 143mL 6mol/L pH5 1100.5mL 10 20mL 2,2951200.1mL 15

50ppm 1.0g 3mL 2mL

2ppm

- 159 -

0.1g 3mol/L 1mL 10mL 155mL 0.6g 0.05mol/L 1mL

0.05mol/L 1mL11.282mg SnCl22H2O

- 160 -

890039

Ferric Chloride

FeCl36H2O270.30

FeCl36H2O99.0

95

110

2.0g 10mL 230.3mL

2.0g 5mL 25

5.0g 100mL 5

5.0g 9535mL 15mL

1.2mL 20mL 131mL1500.2mL 1mL 15

10.0g 50mL 50mL 50mL 200mL A A 40mL 5mL 10mL233mL 230.3mL 30mL 953mL 1102mL 30 0.005

10mL 5mL 233mL 10mL230.3mL 30mL

A 10mL 0.1mL 10mL 10

0.5g 10mL 231mL 1201 1

0.5g 20mL 231mL

- 161 -

100mL 10mL 231mL 100mL 10mL 2.5mL 231mL 100mL

12 500ppm

279.5nm

1.0g 20mL 231mL 100mL 1.0g 20mL 231mL 5.0mL 100mL

12 500ppm

589.0nm

10 1.0g 20mL 231mL 100mL 1.0g 20mL 231mL 2.0mL 100mL

12 50ppm

213.9nm

11 1.0g20mL231mL100mL 1.0g 20mL 231 mL 5.0mL 100mL

12 50ppm

324.7nm

12 1.0g20mL231mL100mL 1.0g 20mL 231mL

- 162 -

5.0mL 100mL

l2 50ppm

283.3nm

13 0.5g 3mL 10mL 2mL 10mL 10mL 10mL 25mL 20mL 5ppm

3mL 10mL 2mL 10mL 10mL 10mL 25mL 20mL 2.0mL

0.6g 50mL 3mL 3g 15 0.1mol/L 1mL

0.1mol/L 1mL27.030mg FeCl36H20

- 163 -

109059

Yellow Ferric Oxide

Fe2O398.0

10.013.02g9002

- 164 -

890040 4,4

4,4-Oxybis(benzenesulfonylhydrazide) 4,4

C12H14N4O5S2358.39

4,4C12H14N4O5S2

95.0

95

150159

1100000 258262nm

3370cm-13260cm-11578cm-11237cm-11159cm-1 704cm-1

0.1g 100mL 10mL 100mL 10mL 100mL 4,4 0.05g 100mL 2mL 100mL 260nm A T A s

4,4C12H14N4O5S2mg

4,4mgA TA S

- 165 -

890041 8-Hydroxyquinoline Sulfate

(C9H7NO)2H2SO4H2O406.41

(C9H7NO)2H2SO4388.3999.0

10095

110

150005mL 1

5mL 1 3 1mL

1105mL 1.5mL

4 7376

150 176178

1.0g 10mL 1.5g 45mL 5mL

20mL 2 20mL 0.01mol/L 0.30mL 0.018

1.5g 20mL 4mL 30mL 20mL 2 20mL 2mL 50mL 4mL3.0mL 2mL 50mL 30ppm

- 166 -

0.20g 1 10ppm 3.55.50.5g 0.10.5g 0.5g 10010mL 40mL 0.1mol/L

0.1mol/L 1mL38.840mg (C9H7NO)2H2SO4

- 167 -

108980

Oxybenzone 2--4-

C14H12O3228.24

C14H12O397.0

9599.5

240244nm286290nm 322327nm 262266nm 308313nm

6265

1.0g 99.520mL

1.0g 2 2.0mL20ppm

0.51g24 0.101g 0.025g 95 100mL

2mL 95 100mL 288nm A

C14H12O3mg A64950000

- 168 -

( mm )

003805

2-Octyldodecanol

2 C20H42O298.55

95 3330cm-1

2920cm-12850cm-11466cm-11378cm-11039cm-1 721cm-1 n 20D1.4521.457 d 20200.8300.850 1.0 5.0 170l90 10 1.0g 2

2.0mL 20ppm 20

A

9.512.5mm

B C6mm

D 5mm

B A

E

FJIS B 7410

1 AP39

G

120

- 169 -

B 5157mm F B B 14 C 03 E A B A E 25mm 1 B A 3 10B 1715 2 73533 3 B

1g 4505500.10

- 170 -

104831

Oleyl Alcohol

C18H36O268.48

9599.5

3330cm-1

3005cm-12920cm-12850cm-1l466cm-11057cm-1 722cm-1 n 20D1.4591.462 d 20200.8450.855 0.5 2.0 200220 8094 6

A

9.512.5mm

B C 6mm

D 5mm

B A

E F1 G

120 B 5157mm F B B 14 C 03 E A B A E 25mm 1 B

- 171 -

A 3 10 B 17152 73533 3 B

3.0g 99.525mL

2 1.0g 2 2.0mL

20ppm 0.101g

- 172 -

002062 Oleic Acid

C18H34O2282.46

95

2930cm-1

1711cm-11465cm-11413cm-11285cm-1 938cm-1 10 d 20200.8660.906 195204 3.0 8095

1.0mL 0.5g 50mL


1.0g 2 2.0mL20ppm

1.0g 3 2ppm 0.01g 5mL

15 30mL 20mL 3 g 5mL 2L

70.0

3mm 3m

150l80m

- 173 -

l5 210 10 2L 30

2

0.105g

- 174 -

102246

Ethyl Oleate

C20H38O2310.51

95 2930cm-1

2850cm-11740cm-11460cm-1 1180cm-11 177185 7085

1.0g 2 2.0mL20ppm

1.0g 3 2ppm 1g

12 0.10

- 175 -

104830

Oleyl Oleate

C36H68O2532.92

95

0.5g 1mL 5

2930cm-12850cm-11740cm-11460cm-1 1180cm-1

n 20D1.4641.468 d 20200.8600.884 3.0 90125 10 70120

2.0g 10mL 1.0g 2 2.0mL

20ppm 1.0g 3 2ppm

0.102g

- 176 -

101696

Decyl Oleate

C28H54O2422.73

95

2920cm-12850cm-11738cm-11460cm-1 1168cm-1

n 20D1.4531.457 d 20200.8600.870 1.0 130150 5.0 5565 10

A

9.512.5mm

B C 6mm

D 5mm

B A

E F1 G

120

B 5157mm F B B 14 C 03 E A B A E 25mm 1 B

- 177 -

A 3 10 B 17152 73533 3 B

1.0g 2 2.0mL 20ppm

- 178 -

106709

Sodium Oleate

C18H34O2282.46

95

12550mL 5mL

23 1mL 13 311434mL 1001101 1mL

0.5g 20mL 5g 100mL

400.05mol/L a mL 10mL 5 0.05mol/L b mL 3 0.50

0.0040a +0.0053b

g 100

0.5g 2 2.0mL40ppm


5.0mL 30mL 6 mL 50mL 20mL

22.025.01g

- 179 -

110156

Orange Essence

9575

n 20D1.3551.371 d 20200.9000.916

10.0g 1 2.0mL2ppm

2.0g 3 1ppm

- 180 -

111963

Powdered Cacao

Theobroma cacao Linn(Sterculiaceae )

15m 23

6.01053 8.0 0.4 10.0

- 181 -

520287

Powdered Hydrolyzed Gelatin

N14.0112.018.0

95 0.5g 2mL 0.1mL

pH 1.0g 100mL pH 5.07.0

1.0g 3 5.0mL50ppm

1.0g 3 2ppm 8.01g1053 2.52g 0.2g 100mL

10mL 0.005mol/L 1mL0.1401mg N

- 182 -

101267 Casein

N14.0113.816.0

95

0.1g 11010mL 6mol/L 8mL

0.1g 11010mL 1

0.1g 450550

5mL 1mL

4

0.10g 30mL 10 2mL 60 1 100mL

15.0mL 10mL131mL1500.2mL 1mL 50mL 15

1.0g 50mL 10 pH 3.76.5

1.0g 30mL 10 20mL100 10.0mg

1.0g 2 2.0mL20ppm

1.0g 4 2ppm 100 30

2.5g 2315mL 20

- 183 -

9510mL 25mL 1 25mL 30 A 15mL 15mL 2

98100 4 1.5

12.01g1003 2.51g 0.015g

0.005mol/L 1mL0.1401mg N

- 184 -

106628 Sodium Caseinate

N14.0114.515.8

95

1.0g 50mL pH 6.07.5 20ppm 1.0g 3 2ppm 1.5

15.01g1003 6.01g 0.015g

0.005mol/L 1mL0.1401mg N

- 185 -

110715

Fructose Glucose Syrup

C6H12O6180.1653.058.0

C6H12O6180.1637.042.0

95 110

12023 5mL

12010mL 0.1g 1mL 3

pH 1.0g 2mL pH 3.85.8

25.0g 50mL

5.0g 50mL 3 0.01mol/L 0.60mL

2.0g 0.01mol/L 1.0mL 0.018

2.0g 0.005mol/L 1.0mL 0.024

5.0g 2 2.0mL4ppm

2.0g 5mL 5mL 1mL 5 5mL 1ppm

1.0g 10mL 1

A T1 A T2 A T3A T3A T1+A T2+A T3 6.0

25.02g2.7kPa 903.5 0.52g

- 186 -

5g 25mL 2.1g 105 6 1.5g 25mL 10L A T1A T2A S1 A S2

C6H12O6mgmgA T1A S1

C6H12O6mgmgA T2A S2

A T1A S1 A T2A S2

8mm 3050cm

50 8 10L

1.5 6

1.0

- 187 -

106623

Sodium Caprylate

C8H15NaO2166.20

C8H15NaO298.0

95

0.5g 25mL 0.5g 25mL

2 0.1mol/L 0.35mL 0.1mol/L 1.25mL

0.1mol/L 1mL14.421mg C8H16O2 0.1mol/L 1mL4.000mg NaOH

1.0 1.0g

2mL 20mL 2mL 2 15mL 50mL 2mL 2mL 2.0mL 50mL 20ppm

1.0g 125mL 20mL 3 2ppm

1.01g1053 0.2g 1000.1mol/L

0.1mol/L 1mL16.620mg C8H15NaO2

- 188 -

511014 Capric Acid

2920cm-12840cm-11710cm-11470cm-1920cm-1 720cm-1 2834 2 3213330.5g 0.5

1.0g 2 2.0mL20ppm

1.0g 3 2ppm 0.15g

- 189 -

101233

Carbon Black

C12.01

95

1.0g 20mL 5mL 5 50mL 1mol/L 1mL 20mL 5mL 10mL

1410mL 2 2510mL N ,N1205mL 42 10.0mL 42 0.50mL 50mL 0.5mL1410mL 2

5ppm

283.3nm

1.0g 20mL 5mL 5mL

1110mL l15mL 10mL 3 50mL 20mL 5ppm

5.0g 70mL 5 100mL 10mL 40mL

- 190 -

105 1 10mg 5.01g1053 0.51g

- 191 -

109190 Carrageenan

Phodophyceae

99.5

1g 100mL

5mL 1mL 25mL 25mL 1

510mL 1 10mL

pH 1.0g 100mL pH 7.510.5

1.0g 2 2.0mL

20ppm 2.5g 20mL

5mL 5mL

15mL 25mL 10mL 2ppm

10mL 2mL

2g 150mL 1.5mL 300 mL 6

105 3 0.5g 105 3 (G3) 105 3 2.0

M 1M 2M 3

M 4 100

M 1g

- 192 -

M 2g M 3g M 4g

6.011.51g1052 15.542.01g

- 193 -

101214 Caramel

95

1g 100mL 10g 100mL 150

20mL 1204mL 1504mL

2.0g

140mL 2.0g 12520mL 60mL

0.05mol/L

0.05mol/L 1mL1.401mg N N 0.5

1.00g 1000mL 555nm A

A

0.130

A 180mL 1425mL D1D2 10mL

A3 10.0g AA60 EGE

- 194 -

D1D2GF1mol/L 4 2mL 56 56

9520mL 20mL BaSO4SO2 0.1

SO2BaSO4g0.2745

g 100

A1L B C D E300mm F G

1.0g 20mL 2mL 23mL 1mL 100mL 1mL 3mL 5 2mL1102mL 25mL 30 1mL 650nm 2.0mL

2.0g 1mL 550600 1mL 0.2mL 1mL 15mL 1

- 195 -

2mL 10mL 50mL

1mL 1mL 0.2mL 1mL 15mL 3.0mL 50mL 15ppm

1.0g 100mL 5mL 5mL 23mL 15mL 23mL 10mL 5mL

28 5mL

1mL 2ppm 4 10.0g

1510mL 1510mL 250mL 9541100mL 2 15 300mL 9541100mL 10g 30 34 10 250mL 954110mL 0.25mol/L 15mL 2 0.25mol/L 15mL 2 pH 9 250mL 5mL 3 9541100mL 2 15 9541100mL 405mL 4 0.10g 250mL 2L 22512 0.2mm 120 2 411 15cm 12001110

- 196 -

- 197 -

120060

Powdered Karaya Gum

Sterculia urens Roxburgh Sterculiaceae

95

0.5g 40mL 0.5mL 151mL 3mL

1.0g 25mL 25mL

25mL 50mL 0.01mol/L 0.40mL 12mL 50mL 0.028

10mL 5 5

1.0g 2 4.0mL40ppm

0.5g 2 4ppm 1.0g 100mL 1

5g 25mL 25mL

G4105 5 3.0

C2H4O260.05 1g 100mL 5mL 2 80mL 0.1mol/L 2

0.1mol/L 1mL6.005mg C2H4O2 10.0

20.01g105 7.01g

- 198 -

2.0

- 199 -

105513

Potassium Persulfate K2S2O8270.32

K2S2O895.0

95

0.1g 11023 5mL 2mL

130

1.0g 30mL 1.0g 1g

30mL pH 4 13 6mL 50mL 0.01mol/L 0.25mL 6mL 50mL 0.009

1.0g 30mL 3mL 5mL 10mL 1 2mL 50mL

5.0mL 2mL 50mL 50ppm 2g 250mL 50mL

0.1mol/L 50mL 5mL 0.02mol/L

0.1mol/L 1mL13.516mg K2S2O8

- 200 -

103410

Light Gravel Granule 1260

95 0.5g 133mL

20mL

5.0g 100mL 15 100mL

50mL 7002 0.040g

10.0g 20mL 10mL 0.01mol/L 0.30mL

0.021 3mL 10 30mL

50mL 2.0mL 1mL 50mL 0.005mol/L 1.0mL 0.480

1.5g 50mL 5mL 20 10mL 2 28

0.5g 0.5g 8mL 150mL 50mL 2.5mL 0.15g 0.15g 2mL 50mL 50ppm


2.01g1053

- 201 -

101243

Carboxyvinyl Polymer

COOH45.0258.063.0

95 N ,N

0.5g 100mL 2

10mL 1mL

10mL 1mL

2960cm-11720cm-11455cm-11415cm-11250cm-11175cm-1 800cm-1

A F B G C H D I4 E J6

0.40g 200mL 200mL

pH7.07.5 10 I J E G 20 200.130 C F D 3 150050000mPas

- 202 -

10,000mPas I4 100 10,000mPas J6 500

pH 0.20g 100mL pH 2.54.0

2.0g 9512020mL 1mL 500600

3mL 10mL 1 2mL 10mL 50mL 9512020mL 2.0mL50mL10ppm

- 203 -

2.5g 20mL 5mL 23mL

15mL 25mL 10mL 2ppm

1.0g 100mL 24 0.05mol/L 10mL 1220mL 20 20mL0.1mol/L1mL 1.0

C3H4O2ab0.3603g


7.02g1053 2.51g 0.1g N ,N310

100mL 0.1mol/L

0.1mol/L 1mL4.502mg COOH

- 204 -

101246

Carboxymethylethylcellulose

-CH2COOH59.048.914.9

-OC2H545.0632.543.0

95 11

0.01g 1mL 2mL

0.01g 251102

125 56

1g 20mL 1mL

1g 1150mL 0.5mL 2980cm-12880cm-11760cm-1 1112cm-1

10.0g 50 90.0g 40 200.l 1 2070mm2/s

1.0g 1110mL


10 1.0g 0.2mol/L 40mL

1 20mL 20mL

- 205 -

3 200mL 50mL 0.01mol/L 0.50mL 0.2mol/L 10mL 7mL 50mL 0071

0.5g 30mL 10

100mL 40mL 1mL 50mL 0.005mol/L 0.40mL 1mL 50mL 0.096

2.0g 2 2.0mL10ppm

1.0g 9511010mL 3mL 2ppm

5.01g1051 0.51g

1g 0.1mol/L 50mL 0.05mol/L 2

0.1mol/L 1mL5.904mg C2H3O2 25mg

1g 100mL 15g 10091150mL

145mL 5mL E 12 J

20mL 25mg A 6mL A C 1 D G B E 1 2 A 2030 150 60 G J 151mL 500mL 200mL 1mL 3g 15mL 5 0.1mol/L

- 206 -

lmL 0.1mol/L 1mL0.7510mg C2H5O

- 207 -

101254 Carmine

Coccus cacti Linn(Coccidae )

C22H20O13492.3950.0

99.5

0.1g 30mL

3mL

0.5 g 500 20mL 10

0.25g 2.5mL

100mL G42811000105 2.5mg

1.0g 450550 20mL 30 20mL 2mL 50mL 2.0mL 2mL 50mL 20ppm

1.0g 4 2ppm 25

0.005mol/L 1mL0.8754mg

20.01g1353 15.01g

0.10 g 2mol/L 30mL 1000mL 494nm A

- 208 -

C22H20O13mg A13910000

- 209 -

111964 Carmellose Potassium

CMC

K39.1010.012.5

95100

0.2g 20mL

1mL 5mL 1 0.5mL 10

10mL 1mL

3g 20mL 2mL 5 20mL

pH 1.0g 100mL pH 6.08.0

250mm 25mm 2mm 2mm

300mm 15mm 2 mm 2mm 1.0g 100mL 1mm 1mm 15

3

0.005mol/L 5.50mL 1mL955mL 50mL 2mL 10

0.5g 50mL 10mL 10mL

10mL 3 200mL 50mL 0.01mol/L

- 210 -

0.45mL 0.640 10mL 1mL

10mL 3 50mL 10mL 50mL 0.005mol/L 0.40mL 0.960

1.0g 2 2.0mL20ppm

1.0g 20mL 5mL 5mL

15mL 25mL 5mL

5mL 2mL 10ppm

10.01g1054 0.5g 10080mL

130 2 0.1mol/L

0.1mol/L 1mL3.910mg K

- 211 -

122101 -Carotene

C40H56536.87

C40H5698.0

95

1400

3030cm-12950cm-12920cm-11442cm-11367cm-1 966cm-1 176183

1.0g 2 2.0mL20ppm

0.5g 3 4ppm 0.04g

100mL 5mL 100mL 10mL 100mL 340nm 362nm A 1 A 2 434nm455nm 483nm A 3A 4 A 5A 2A 1 1.00 A 410A 1 15.0 A 4A 3 1.301.60A 4A 5 1.51.25

1.01g4 0.101g

455nm A

C40H56mg A2450200000

- 212 -

- 213 -

103319

Hydrogenated Maltose Starch Syrup

D C12H24O11344.31

75.080.0

153mL 1mL 1.5mL

110002mL 150

2mL 4mL 80 15

5.0g 50mL

1 0.01mol/L 0.5mL 30

5.0g 1 2.5mL5ppm

1.0g 1 2ppm 1105mL 3

3 5 1.0g 25mL 40mL

3 G4 20mL 800.02mo1/L 1.7mL

25.00.1g 0.025g 1g 10mL

100mL 0.67kPa 803 1g 10mL 100mL

- 214 -

10L Q T Q S

C12H24O11mgmgQ TQ S

5g 50mL

8mm 3050cm 510m

50 17 10L

1.5

- 215 -

120016

Hydrogenated Starch Syrup

153mL 1mL 1.5mL

11002mL 5mL 80

15

5.0g 1 2.5mL

5ppm 0.5g 5mL 3 5

1.0g 25mL

40mL 3 G4

20mL 800.02mol/L 2.0mL

1g 30 100 902.67kPa 23 2.67kPa 5

2832 0.105g

- 216 -

109974

LanolinHydrogenated

99.595100

1505mL 1mL 2

3555 1.0 10 20 100

11

5g 25mL 10 pH 5.08.0

2.0g 40mL 10 20mL 6mL 50mL 0.01mol/L 1.0mL 0.036

10mL 1mL

5mL 0.002mol/L 0.5mL 10

0.5g 99.540mL

0.01mol/L 0.70mL 6mL 50mL 1mL 5

30

- 217 -

110452 201

Photosensitizer 201

C23H39IN2S2534.60

201 C23H39IN2S297.0

95

0.1g 10mL 3 5mL

1200000

409413nm 224228

1.0g 30mL 2g pH 5.07.0

5.0g 10mL 10mL 23mL 15mL 50mL 20mL 1 28 2mL 50mL 10mL 10mL 2.0mL 50mL 1 5 10ppm

0.51g903 0.201g 0.5g 500mL 12

50mL 115100mL 20 25mL

- 218 -

1151100250mL 2 3 250mL100mL500mL 100mL 10mL 0.01mol/L 5

0.01mol/L 1mL10.692mg C23H39IN2S2

- 219 -

106575

Hydrated Silicon Dioxide

SiO260.0895.0

95

0.1g 20mL 12mL

11000010mL

0.8g 60mL 2mL 10 100mL 20mL 100mL 10mL 1mL 50mL 0.005mol/L 0.50mL 1mL 50mL 1.5

0.5g 20mL 3115mL 10mL 50mL 20mL 1 31 1.5mL 2mL 50mL 30ppm

0.5g 40mL 50mL 5mL 318.5mL 2mL 50mL 30 520nm

0.176g 1000mL 25mL 5mL318.5mL 2mL 50mL

0.05g 20mL

- 220 -

1 7mL 50mL 0.05g 5mL 5

2.5mL 20mL 1 7mL 50mL 0.05g 5mL

1.0g 30mL 20mL 1 5mL 100mL 25mL 1mL 9550mL 10

180 4 0.250g 3mL 100mL 1mL 5mL 100mL 25mL 1mL 95 50mL

0.40g 10mL 5mL 5mL5ppm

15.01g1054 21.01g850950 1g 20mL

110120 2 5mL 2025mL 30 ag6mL 3 5 bg

SiO2gab

- 221 -

120320 LD

Dried Methacrylic Acid Copolymer LD

LD C4H6O286.0946.051.0

99.5 2

200mg 7mL 0.5mL 5mL 1mL

2331

2980cm-11734cm-11700cm-11473cm-11449cm-11383cm-1 1178cm-1

1g 20mL 5mL 3mL 10mL

5g 1130mL 2 0.1mL 0.1mL 2mL 2mL

10.00g 80mL 100mL 200.1 1 1545mm2/s

1.0g 2 2.0mL

20ppm 1.0g 3 2ppm 1g

50mL 5mL 5mL

0.01g 0.011 5mL 100mL 1mL 100mL 5mL 5mL

- 222 -

20L

200nm 4.6mm 12cm 7m

20 pH2 41 3 8

2mL 10mL 20L 1822

20L 6

20L 6 2.0

5.01g1052 0.401g 0.5g 232100mL

0.5mol/L


- 223 -

109973

Dried Egg White

Gallus gallus domesticus Brisson

2.0g 20mL

0.1g 100mL 10mL 11010mL

1.0g 2 2.0mL

20ppm 1.0g 3 2ppm

10.01g1054 10.02g

- 224 -

103947

Dried Magnesium Sulfate

MgSO47H2O 35

MgSO4120.3799.0

95

140 pH 1.0g 20mL pH 6.07.0

1.0g 0.01mol/L 0.40mL 0.014

2.0g 1 2.0mL10ppm

2.0g 20mL 311mL 5

30.045.01g4503 0.5g 2mL

100mL 25mL 50mL pH10.7 5mL 0.05mol/L T 0.04g

0.05mol/L 1mL6.018mg MgSO4

- 225 -

120257

Kanbaiko

Oryza sativa Linn var. glutinosa Matsum.(Gramineae )

99.5

1g 50mL 120

1.0g 4 2.0mL

20ppm 1.0g 4 2ppm

15.06 1.0

- 226 -

109058 Xanthan Gum

Xanthomonas Campestris

DDD

99.5

1g 100mL 1.5g 1.5g 80

300mL 60 30 2

A E B F C G3 D

- 227 -

3.00g 3.00g 294g 500mL 2 250.5G E 60 30 D

3 20 600mPas 650.5

25 65 V 1 V 2V 1V 2 1.021.45

pH 1.0g 100mL pH 5.08.0

0.5g 100mL 1.0g 2 2.0mL

20ppm 2.5g 20mL

5mL 5mL 15mL 25mL 5mL 5.0mL 20mL 2ppm

15.02g1053 5.516.0 0.6g 100mL 10mL

1mol/L 20mL 3 2mL2,4 2mol/L 12001mL 5 5mL 2 1105mL 3 110 100mL 0.30g 100mL 1mL 100mL 2mL 2,4 2mol/L 12001mL 375nm

- 228 -

101651 D

D-Xylose

C5H10O5150.13

DC5H10O598.0

9595

1g 25mL

1g 3mL 3mol/L

95140523mL 5

12023 5mL

0.5g 20mL 30mL 10mL 2 160163

4.0g 20mL 1.0g 10mL

1 0.2mol/L 1 4.0g 0.005mol/L 0.40mL

0.005 2.0g 1 2.0mL

10ppm 1.0g 1 2ppm 0.20g 10mL 1mL

50mL 10L 1100311 10cm 0.93g 1.66g 1 100mL100125 5

- 229 -

1.01g1053 0.052g 0.2g 100mL

10mL 50mL 15 2.5g 5 0.1mol/L 3mL

0.1mol/L 1mL1.8766mg C5H10O5

- 230 -

110457

Adsorption Refined Lanolin

Ovis aries Linn(Bovidae )

1501mL 2mL

3038 3 0.5 10g 1836

0.8g 500mL 20mL 25mL 2030 30 11020mL 100mL 0.1mol/L 1mL

ab1.269g


5 5g 80110

1.5g 200mL 0.5mol/L 25mL2 20mL 750mm 6mm 3

1.0g 2

2.0mL 20ppm 1.0g 3 2ppm

0.55g1051 0.13g

30

- 231 -

122102

Fish Scale Flake

Trichiurus lepturus

95

0.5g 1525mL 20

5g 9530mL 4000 10

9530mL 2 105 1 3300cm-13080cm-11666cm-11369cm-1 940cm-1

2.0g 4 2.0mL

10ppm 1.0g 5mL 5mL

2mL 15mL 10mL 2ppm

1.01g

- 232 -

103518

Gold Leaf

Au196.9794.0

0.01g 5415mL

2mL 4 20mL 495130001mL

0.40g 5mL 5mL 5ppm

0.025g 2mL 200mL 2mL 25mL 5mL10mL 15mL 25mL

242.8nm

- 233 -

102495

Silver Leaf

Ag107.8797.0

99.5

0.6g 136mL 30mL

5.0g 1340mL

250mL 23 300mL 150mL 230.1mL 10mL 1 450550 2.5mg

231mL 131mL 231mL 50mL 20mL 15mL 142mL312mL1102mL 0.5mL 5mL 50.005

138.4mL 23 15 23 1mL 5.0mL 15mL

10mL 232.8mL 25mL 0.03g 1102mL 5 0.005

134.2mL 23 110 0.2mL 233mL 2.5mL 25mL

0.3 g 1315mL 50mL 10mL 0.1mol/L 5mL

0.1mol/L 1mL10.787mg Ag

- 234 -

- 235 -

520357 Guar Gum

Cyamopsis tetragonolobus Linn(Leguminosae )

95 1g 100mL

130030mL 0.01g

0.15g

6.25 10.0

2.0g 2 2.0mL10ppm

0.5g 2 4ppm 1.0g 10mL 1

1.5g 150mL 1.5mL 6

G3105 3 0.105g

15.01g1055 1.51g

- 236 -

890042

Guanidine Nitrate

CH5N3HNO3122.08

CH5N3HNO394.0

95

1100

1501mL 0.5mL

1mL 150

209216

5g 250mL 25mL2812 4550 2,4,6 150mL 3 G4 2,4,6 100mL 1mol/L 1mol/L 0.5mL 1 G4 105 2.0

C3H6N612

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平成30年3月29日（公印省...