3334 victor court , santa clara, ca 95054 phone: (408) 588

Entech Analytical Labs, Inc. 3334 Victor Court , Santa Clara, CA 95054 Phone: (408) 588-0200 Fax: (408) 588-0201

PES Environmental, Inc.1682 Novato Boulevard, Suite 100

On June 30, 2006, samples were received under chain of custody for analysis.

TestMatrix

Novato, CA 94947

Jim Dunn

Comments

Certificate of Analysis - Final Report

Lab Certificate Number: 50220

Project Name: BaxterProject Number: 285.002.01

Issued: 07/19/2006

Entech analyzes samples "as received" unless otherwise noted. The following results are included:

Liquid pH - EPA 9040C for Groundwater and Water - EPA 150.1 for WastewaterEPA 7470A Mercury for Water and Groundwater / EPA 245.1 Mercury for WastewaterICP Metals: EPA 3010A / EPA 6010B for Groundwater and Water - EPA 200.7 for WastewaterChromium-VI: EPA 7196A for Water and Groundwater / Std. Methods (18th Ed.) 3500-Cr-D for WastewaterTPH-Extractable: EPA 3510C / EPA 8015BVOCs: EPA 5030C / EPA 8260B for Groundwater and Water - EPA 624 for WastewaterCyanide, Total: EPA 9010C/9014 for Groundwater and Water - EPA 335.2 for WastewaterTPH-Purgeable: GC/MS

Solid EPA 6010B Metals by ICPChromium VI: EPA 7196AEPA 7471B / EPA 245.5 MercuryTPH-Extractable: EPA 8015BEPA 8260BCyanide, Total: EPA 9010C/9014pH - EPA 9045DTPH-Purgeable: GC/MS

Entech Analytical Labs, Inc. is certified for environmental analyses by the State of California (#2346). If you have any questions regarding this report, please call us at 408-588-0200 ext. 225.

Sincerely,

Erin CunniffeOperations Manager

Environmental Analysis Since 1983

Original signed by Erin Cunniffe

PES Environmental, Inc.1682 Novato Boulevard, Suite 100Novato, CA 94947

Certificate of Analysis - Data Report

Entech Analytical Labs, Inc. __ 3334 Victor Court , Santa Clara, CA 95054 Phone: (408) 588-0200 Fax: (408) 588-0201

Sample Collected by: Client

Attn: Jim Dunn

Project Name: Baxter

Samples Received: 06/30/2006

Project Number: 285.002.01

Lab # : 50220-001 Sample ID: 06QC-07-1 Matrix: Solid Sample Date: 6/29/2006 1:50 PM

Parameter Result UnitsDetection LimitD/P-F QC BatchQual Prep Date Analysis DatePrep BatchChromium VI: EPA 7196A

Chromium (VI) ND mg/Kg0.101.0 SCR60607117/11/2006SCR60607117/11/2006

Reviewed by: JISIDERIO

Analyzed by: Rlazaro

Parameter Result UnitsDetection LimitD/P-F QC BatchQual Prep Date Analysis DatePrep BatchEPA 7471B / EPA 245.5 Mercury

Mercury 0.090 mg/Kg0.0501.0 SHG060718A7/18/2006SHG060718A7/18/2006

Reviewed by: HDINH

Analyzed by: RWipfler

Parameter Result UnitsDetection LimitD/P-F QC BatchQual Prep Date Analysis DatePrep BatchEPA 6010B Metals by ICP

Antimony ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Arsenic 8.2 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Barium 110 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Beryllium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cadmium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Chromium 45 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cobalt 24 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Copper 100 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Lead 27 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Molybdenum ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Nickel 75 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Selenium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Silver ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Thallium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Vanadium 54 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Zinc 100 mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006

Reviewed by: HDINH

Analyzed by: Equeja

Parameter Result UnitsDetection LimitD/P-F QC BatchQual Prep Date Analysis DatePrep BatchpH - EPA 9045D

pH 7.4 pH Units1.01.0 SPH0607057/5/2006SPH0607057/5/2006

Reviewed by: HDINH

Analyzed by: Jisiderio

D/P-F = Dilution and/or Prep Factor includes sample volume adjustments.ND = Not Detected at or above the Detection Limit.

7/19/2006 6:58:05 PM - ECunniffeQual = Data QualifierDetection Limit = Detection Limit for Reporting.





Attn: Jim Dunn















Attn: Jim Dunn





Parameter Result UnitsDetection LimitD/P-F QC BatchQual Prep Date Analysis DatePrep BatchEPA 8260B

1,1,1,2-Tetrachloroethane ND g/Kg4.40.88 SM60607137/13/2006N/AN/A1,1,1-Trichloroethane ND g/Kg5.01.0 SM60607137/13/2006N/AN/A1,1,2,2-Tetrachloroethane ND g/Kg4.40.88 SM60607137/13/2006N/AN/A1,1,2-Trichloroethane ND g/Kg4.40.88 SM60607137/13/2006N/AN/A1,1-Dichloroethane ND g/Kg4.40.88 SM60607137/13/2006N/AN/A1,1-Dichloroethene ND g/Kg4.40.88 SM60607137/13/2006N/AN/A1,1-Dichloropropene ND g/Kg4.40.88 SM60607137/13/2006N/AN/A1,2,3-Trichlorobenzene ND g/Kg4.40.88 SM60607137/13/2006N/AN/A1,2,3-Trichloropropane ND g/Kg4.40.88 SM60607137/13/2006N/AN/A1,2,4-Trichlorobenzene ND g/Kg4.40.88 SM60607137/13/2006N/AN/A1,2,4-Trimethylbenzene ND g/Kg4.40.88 SM60607137/13/2006N/AN/A1,2-Dibromo-3-Chloropropane ND g/Kg4.40.88 SM60607137/13/2006N/AN/A1,2-Dibromoethane (EDB) ND g/Kg4.40.88 SM60607137/13/2006N/AN/A1,2-Dichlorobenzene ND g/Kg4.40.88 SM60607137/13/2006N/AN/A1,2-Dichloroethane ND g/Kg4.40.88 SM60607137/13/2006N/AN/A1,2-Dichloropropane ND g/Kg4.40.88 SM60607137/13/2006N/AN/A1,3,5-Trimethylbenzene ND g/Kg4.40.88 SM60607137/13/2006N/AN/A1,3-Dichlorobenzene ND g/Kg4.40.88 SM60607137/13/2006N/AN/A1,3-Dichloropropane ND g/Kg4.40.88 SM60607137/13/2006N/AN/A1,4-Dichlorobenzene ND g/Kg4.40.88 SM60607137/13/2006N/AN/A1,4-Dioxane ND g/Kg1800.88 SM60607137/13/2006N/AN/A2,2-Dichloropropane ND g/Kg4.40.88 SM60607137/13/2006N/AN/A2-Butanone (MEK) ND g/Kg350.88 SM60607137/13/2006N/AN/A2-Chloroethyl-vinyl Ether ND g/Kg4.40.88 SM60607137/13/2006N/AN/A2-Chlorotoluene ND g/Kg4.40.88 SM60607137/13/2006N/AN/A2-Hexanone ND g/Kg350.88 SM60607137/13/2006N/AN/A4-Chlorotoluene ND g/Kg4.40.88 SM60607137/13/2006N/AN/A4-Methyl-2-Pentanone(MIBK) ND g/Kg350.88 SM60607137/13/2006N/AN/AAcetone ND g/Kg880.88 SM60607137/13/2006N/AN/AAcetonitrile ND g/Kg350.88 SM60607137/13/2006N/AN/AAcrolein ND g/Kg4.40.88 SM60607137/13/2006N/AN/AAcrylonitrile ND g/Kg4.40.88 SM60607137/13/2006N/AN/ABenzene ND g/Kg4.40.88 SM60607137/13/2006N/AN/ABenzyl Chloride ND g/Kg4.40.88 SM60607137/13/2006N/AN/ABromobenzene ND g/Kg4.40.88 SM60607137/13/2006N/AN/ABromochloromethane ND g/Kg4.40.88 SM60607137/13/2006N/AN/ABromodichloromethane ND g/Kg4.40.88 SM60607137/13/2006N/AN/ABromoform ND g/Kg4.40.88 SM60607137/13/2006N/AN/ABromomethane ND g/Kg4.40.88 SM60607137/13/2006N/AN/ACarbon Disulfide ND g/Kg4.40.88 SM60607137/13/2006N/AN/ACarbon Tetrachloride ND g/Kg4.40.88 SM60607137/13/2006N/AN/AChlorobenzene ND g/Kg4.40.88 SM60607137/13/2006N/AN/AChloroethane ND g/Kg4.40.88 SM60607137/13/2006N/AN/AChloroform ND g/Kg4.40.88 SM60607137/13/2006N/AN/AChloromethane ND g/Kg4.40.88 SM60607137/13/2006N/AN/A







Attn: Jim Dunn






cis-1,2-Dichloroethene ND g/Kg4.40.88 SM60607137/13/2006N/AN/Acis-1,3-Dichloropropene ND g/Kg4.40.88 SM60607137/13/2006N/AN/ACyclohexanone ND g/Kg350.88 SM60607137/13/2006N/AN/ADibromochloromethane ND g/Kg4.40.88 SM60607137/13/2006N/AN/ADibromomethane ND g/Kg4.40.88 SM60607137/13/2006N/AN/ADichlorodifluoromethane ND g/Kg4.40.88 SM60607137/13/2006N/AN/ADiisopropyl Ether ND g/Kg4.40.88 SM60607137/13/2006N/AN/AEthyl Benzene ND g/Kg4.40.88 SM60607137/13/2006N/AN/AFreon 113 ND g/Kg8.80.88 SM60607137/13/2006N/AN/AHexachlorobutadiene ND g/Kg4.40.88 SM60607137/13/2006N/AN/AIodomethane ND g/Kg350.88 SM60607137/13/2006N/AN/AIsopropanol ND g/Kg880.88 SM60607137/13/2006N/AN/AIsopropylbenzene ND g/Kg4.40.88 SM60607137/13/2006N/AN/AMethyl-t-butyl Ether ND g/Kg4.40.88 SM60607137/13/2006N/AN/AMethylene Chloride ND g/Kg220.88 SM60607137/13/2006N/AN/An-Butylbenzene ND g/Kg4.40.88 SM60607137/13/2006N/AN/An-Propylbenzene ND g/Kg4.40.88 SM60607137/13/2006N/AN/ANaphthalene ND g/Kg4.40.88 SM60607137/13/2006N/AN/Ap-Isopropyltoluene ND g/Kg4.40.88 SM60607137/13/2006N/AN/APentachloroethane ND g/Kg4.40.88 SM60607137/13/2006N/AN/Asec-Butylbenzene ND g/Kg4.40.88 SM60607137/13/2006N/AN/AStyrene ND g/Kg4.40.88 SM60607137/13/2006N/AN/Atert-Amyl Methyl Ether ND g/Kg4.40.88 SM60607137/13/2006N/AN/Atert-Butanol (TBA) ND g/Kg350.88 SM60607137/13/2006N/AN/Atert-Butyl Ethyl Ether ND g/Kg4.40.88 SM60607137/13/2006N/AN/Atert-Butylbenzene ND g/Kg4.40.88 SM60607137/13/2006N/AN/ATetrachloroethene ND g/Kg4.40.88 SM60607137/13/2006N/AN/ATetrahydrofuran ND g/Kg350.88 SM60607137/13/2006N/AN/AToluene ND g/Kg4.40.88 SM60607137/13/2006N/AN/Atrans-1,2-Dichloroethene ND g/Kg4.40.88 SM60607137/13/2006N/AN/Atrans-1,3-Dichloropropene ND g/Kg4.40.88 SM60607137/13/2006N/AN/Atrans-1,4-Dichloro-2-butene ND g/Kg350.88 SM60607137/13/2006N/AN/ATrichloroethene ND g/Kg4.40.88 SM60607137/13/2006N/AN/ATrichlorofluoromethane ND g/Kg4.40.88 SM60607137/13/2006N/AN/AVinyl Acetate ND g/Kg4.40.88 SM60607137/13/2006N/AN/AVinyl Chloride ND g/Kg4.40.88 SM60607137/13/2006N/AN/AXylenes, Total ND g/Kg8.80.88 SM60607137/13/2006N/AN/A

Reviewed by: MaiChiTu

Analyzed by: AtamSurrogate Surrogate Recovery Control Limits (%)4-Bromofluorobenzene 86.8 60 130-Dibromofluoromethane 85.9 60 130-Toluene-d8 96.6 60 130-







Attn: Jim Dunn






Mercury ND mg/Kg0.0501.0 SHG060718A7/18/2006SHG060718A7/18/2006

Reviewed by: HDINH



Antimony ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Arsenic 7.3 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Barium 80 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Beryllium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cadmium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Chromium 79 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cobalt 8.5 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Copper 180 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Lead 6.5 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Molybdenum ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Nickel 570 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Selenium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Silver ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Thallium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Vanadium 67 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Zinc 66 mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006

Reviewed by: HDINH

Analyzed by: Equeja



Reviewed by: HDINH


Parameter Result UnitsDetection LimitD/P-F QC BatchQual Prep Date Analysis DatePrep BatchTPH-Purgeable: GC/MS

TPH as Gasoline ND g/Kg930.93 SM60607127/12/2006N/AN/A


Analyzed by: AtamSurrogate Surrogate Recovery Control Limits (%)4-Bromofluorobenzene 90.5 60 130-Dibromofluoromethane 130 60 130-Toluene-d8 91.9 60 130-







Attn: Jim Dunn





Parameter Result UnitsDetection LimitD/P-F QC BatchQual Prep Date Analysis DatePrep BatchTPH-Extractable: EPA 8015B

TPH as Diesel ND mg/Kg2.51.0 SD060713B7/16/2006SD060713B7/13/2006

Reviewed by: dba

Analyzed by: JHsiangSurrogate Surrogate Recovery Control Limits (%)o-Terphenyl 65.2 41 137-







Attn: Jim Dunn















Attn: Jim Dunn






Mercury ND mg/Kg0.0501.0 SHG060718A7/18/2006SHG060718A7/18/2006

Reviewed by: HDINH



Antimony 1.7 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Arsenic 14 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Barium 110 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Beryllium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cadmium 1.2 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Chromium 56 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cobalt 12 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Copper 400 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Lead 13 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Molybdenum ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Nickel 1400 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Selenium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Silver ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Thallium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Vanadium 16 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Zinc 230 mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006

Reviewed by: HDINH

Analyzed by: Equeja



Reviewed by: HDINH












Attn: Jim Dunn







Reviewed by: dba








Attn: Jim Dunn






Chromium (VI) 1.1 mg/Kg0.101.0 SCR60607117/11/2006SCR60607117/11/2006



Parameter Result UnitsDetection LimitD/P-F QC BatchQual Prep Date Analysis DatePrep BatchCyanide, Total: EPA 9010C/9014

Cyanide, total ND mg/Kg1.01.0 SCN0607057/7/2006SCN0607057/6/2006

Reviewed by: HDINH








Attn: Jim Dunn













Attn: Jim Dunn







Reviewed by: HDINH



Antimony 2.4 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Arsenic 13 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Barium 110 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Beryllium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cadmium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Chromium 79 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cobalt 15 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Copper 31 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Lead 8.6 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Molybdenum ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Nickel 2300 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Selenium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Silver ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Thallium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Vanadium 14 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Zinc 65 mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006

Reviewed by: HDINH

Analyzed by: Equeja



Reviewed by: HDINH












Attn: Jim Dunn






TPH as Diesel ND mg/Kg2.51.0 SD060715A7/18/2006 SD060715A7/15/2006

Reviewed by: ECunniffe








Attn: Jim Dunn















Attn: Jim Dunn







Reviewed by: HDINH



Antimony 1.4 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Arsenic 26 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Barium 85 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Beryllium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cadmium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Chromium 36 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cobalt 8.3 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Copper 21 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Lead 8.5 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Molybdenum ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Nickel 230 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Selenium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Silver ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Thallium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Vanadium 11 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Zinc 59 mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006

Reviewed by: HDINH

Analyzed by: Equeja



Reviewed by: HDINH












Attn: Jim Dunn















Attn: Jim Dunn











Reviewed by: HDINH



Antimony 23 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Arsenic 16 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Barium 63 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Beryllium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cadmium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Chromium 250 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cobalt 34 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Copper 48 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Lead 7.0 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Molybdenum ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Nickel 500 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Selenium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Silver ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Thallium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Vanadium 55 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Zinc 61 mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006

Reviewed by: HDINH

Analyzed by: Equeja



Reviewed by: HDINH








Attn: Jim Dunn









Parameter Result UnitsDetection LimitD/P-F QC BatchQual Prep Date Analysis DatePrep BatchCyanide, Total: EPA 9010C/9014

Cyanide, total ND mg/Kg1.01.0 SCN0607057/7/2006SCN0607057/6/2006

Reviewed by: HDINH








Attn: Jim Dunn













Attn: Jim Dunn







Reviewed by: HDINH




Reviewed by: HDINH

Analyzed by: Equeja



Reviewed by: HDINH












Attn: Jim Dunn















Attn: Jim Dunn











Reviewed by: HDINH




Reviewed by: HDINH

Analyzed by: Equeja



Reviewed by: HDINH








Attn: Jim Dunn











Reviewed by: HDINH



Antimony ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Arsenic 6.5 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Barium 110 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Beryllium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cadmium 3.3 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Chromium 48 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cobalt 240 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Copper 180 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Lead 67 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Molybdenum ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Nickel 420 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Selenium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Silver 35 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Thallium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Vanadium 48 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Zinc 190 mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006

Reviewed by: HDINH

Analyzed by: Equeja



Reviewed by: HDINH








Attn: Jim Dunn











Reviewed by: HDINH



Antimony ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Arsenic ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Barium 110 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Beryllium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cadmium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Chromium 15 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cobalt 11 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Copper 18 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Lead 13 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Molybdenum ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Nickel 22 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Selenium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Silver ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Thallium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Vanadium 25 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Zinc 200 mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006

Reviewed by: HDINH

Analyzed by: Equeja



Reviewed by: HDINH








Attn: Jim Dunn











Reviewed by: HDINH



Antimony ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Arsenic ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Barium 150 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Beryllium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cadmium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Chromium 430 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cobalt 34 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Copper 30 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Lead 6.1 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Molybdenum ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Nickel 520 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Selenium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Silver ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Thallium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Vanadium 55 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Zinc 45 mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006

Reviewed by: HDINH

Analyzed by: Equeja



Reviewed by: HDINH








Attn: Jim Dunn











Reviewed by: HDINH



Antimony 1.7 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Arsenic 11 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Barium 220 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Beryllium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cadmium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Chromium 24 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cobalt 13 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Copper 40 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Lead 14 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Molybdenum ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Nickel 97 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Selenium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Silver ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Thallium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Vanadium 20 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Zinc 81 mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006

Reviewed by: HDINH

Analyzed by: Equeja



Reviewed by: HDINH








Attn: Jim Dunn















Attn: Jim Dunn






cis-1,2-Dichloroethene ND g/Kg5.01.0 SM30607147/14/2006N/AN/Acis-1,3-Dichloropropene ND g/Kg5.01.0 SM30607147/14/2006N/AN/ACyclohexanone ND g/Kg401.0 SM30607147/14/2006N/AN/ADibromochloromethane ND g/Kg5.01.0 SM30607147/14/2006N/AN/ADibromomethane ND g/Kg5.01.0 SM30607147/14/2006N/AN/ADichlorodifluoromethane ND g/Kg5.01.0 SM30607147/14/2006N/AN/ADiisopropyl Ether ND g/Kg5.01.0 SM30607147/14/2006N/AN/AEthyl Benzene ND g/Kg5.01.0 SM30607147/14/2006N/AN/AFreon 113 ND g/Kg101.0 SM30607147/14/2006N/AN/AHexachlorobutadiene ND g/Kg5.01.0 SM30607147/14/2006N/AN/AIodomethane ND g/Kg401.0 SM30607147/14/2006N/AN/AIsopropanol ND g/Kg1001.0 SM30607147/14/2006N/AN/AIsopropylbenzene ND g/Kg5.01.0 SM30607147/14/2006N/AN/AMethyl-t-butyl Ether ND g/Kg5.01.0 SM30607147/14/2006N/AN/AMethylene Chloride ND g/Kg251.0 SM30607147/14/2006N/AN/An-Butylbenzene ND g/Kg5.01.0 SM30607147/14/2006N/AN/An-Propylbenzene ND g/Kg5.01.0 SM30607147/14/2006N/AN/ANaphthalene ND g/Kg5.01.0 SM30607147/14/2006N/AN/Ap-Isopropyltoluene ND g/Kg5.01.0 SM30607147/14/2006N/AN/APentachloroethane ND g/Kg5.01.0 SM30607147/14/2006N/AN/Asec-Butylbenzene ND g/Kg5.01.0 SM30607147/14/2006N/AN/AStyrene ND g/Kg5.01.0 SM30607147/14/2006N/AN/Atert-Amyl Methyl Ether ND g/Kg5.01.0 SM30607147/14/2006N/AN/Atert-Butanol (TBA) ND g/Kg401.0 SM30607147/14/2006N/AN/Atert-Butyl Ethyl Ether ND g/Kg5.01.0 SM30607147/14/2006N/AN/Atert-Butylbenzene ND g/Kg5.01.0 SM30607147/14/2006N/AN/ATetrachloroethene ND g/Kg5.01.0 SM30607147/14/2006N/AN/ATetrahydrofuran ND g/Kg401.0 SM30607147/14/2006N/AN/AToluene ND g/Kg5.01.0 SM30607147/14/2006N/AN/Atrans-1,2-Dichloroethene ND g/Kg5.01.0 SM30607147/14/2006N/AN/Atrans-1,3-Dichloropropene ND g/Kg5.01.0 SM30607147/14/2006N/AN/Atrans-1,4-Dichloro-2-butene ND g/Kg401.0 SM30607147/14/2006N/AN/ATrichloroethene ND g/Kg5.01.0 SM30607147/14/2006N/AN/ATrichlorofluoromethane ND g/Kg5.01.0 SM30607147/14/2006N/AN/AVinyl Acetate ND g/Kg5.01.0 SM30607147/14/2006N/AN/AVinyl Chloride ND g/Kg5.01.0 SM30607147/14/2006N/AN/AXylenes, Total ND g/Kg101.0 SM30607147/14/2006N/AN/A


Analyzed by: MfelixSurrogate Surrogate Recovery Control Limits (%)4-Bromofluorobenzene 77.6 60 130-Dibromofluoromethane 83.6 60 130-Toluene-d8 89.8 60 130-







Attn: Jim Dunn







Reviewed by: HDINH



Antimony 2.4 mg/Kg1.01.0 SM0607167/18/2006SM0607167/16/2006Arsenic 8.0 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Barium 76 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Beryllium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cadmium 11 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Chromium 180 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cobalt 35 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Copper 170 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Lead 11 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Molybdenum ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Nickel 2200 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Selenium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Silver 1.5 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Thallium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Vanadium 44 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Zinc 360 mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006

Reviewed by: HDINH

Analyzed by: Equeja



Reviewed by: HDINH





Analyzed by: MfelixSurrogate Surrogate Recovery Control Limits (%)4-Bromofluorobenzene 80.8 60 130-Dibromofluoromethane 77.8 60 130-Toluene-d8 90.0 60 130-







Attn: Jim Dunn






TPH as Diesel ND mg/Kg2.51.0 SD060715A7/18/2006 SD060715A42 mg/Kg Motor Oil. No Diesel pattern present.

7/15/2006









Attn: Jim Dunn















Attn: Jim Dunn







Reviewed by: HDINH



Antimony ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Arsenic 7.2 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Barium 190 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Beryllium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cadmium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Chromium 44 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cobalt 17 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Copper 41 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Lead 10 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Molybdenum ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Nickel 56 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Selenium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Silver ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Thallium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Vanadium 41 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Zinc 55 mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006

Reviewed by: HDINH

Analyzed by: Equeja



Reviewed by: HDINH












Attn: Jim Dunn






TPH as Diesel 370 mg/Kg2510 SD060715A7/18/2006 SD060715AAtypical pattern (C12-C28).

7/15/2006









Attn: Jim Dunn















Attn: Jim Dunn






1,1,1,2-Tetrachloroethane ND g/Kg18037 7/13/2006N/AN/A1,1,1-Trichloroethane ND g/Kg18037 7/13/2006N/AN/A1,1,2,2-Tetrachloroethane ND g/Kg18037 7/13/2006N/AN/A1,1,2-Trichloroethane ND g/Kg18037 7/13/2006N/AN/A1,1-Dichloroethane ND g/Kg18037 7/13/2006N/AN/A1,1-Dichloroethene ND g/Kg18037 7/13/2006N/AN/A1,1-Dichloropropene ND g/Kg18037 7/13/2006N/AN/A1,2,3-Trichlorobenzene ND g/Kg18037 7/13/2006N/AN/A1,2,3-Trichloropropane ND g/Kg18037 7/13/2006N/AN/A1,2,4-Trichlorobenzene ND g/Kg18037 7/13/2006N/AN/A1,2,4-Trimethylbenzene 200 g/Kg18037 7/13/2006N/AN/A1,2-Dibromo-3-Chloropropane ND g/Kg18037 7/13/2006N/AN/A1,2-Dibromoethane (EDB) ND g/Kg18037 7/13/2006N/AN/A1,2-Dichlorobenzene ND g/Kg18037 7/13/2006N/AN/A1,2-Dichloroethane ND g/Kg18037 7/13/2006N/AN/A1,2-Dichloropropane ND g/Kg18037 7/13/2006N/AN/A1,3,5-Trimethylbenzene 460 g/Kg18037 7/13/2006N/AN/A1,3-Dichlorobenzene ND g/Kg18037 7/13/2006N/AN/A1,3-Dichloropropane ND g/Kg18037 7/13/2006N/AN/A1,4-Dichlorobenzene ND g/Kg18037 7/13/2006N/AN/A1,4-Dioxane ND g/Kg740037 7/13/2006N/AN/A2,2-Dichloropropane ND g/Kg18037 7/13/2006N/AN/A2-Butanone (MEK) ND g/Kg150037 7/13/2006N/AN/A2-Chloroethyl-vinyl Ether ND g/Kg18037 7/13/2006N/AN/A2-Chlorotoluene ND g/Kg18037 7/13/2006N/AN/A2-Hexanone ND g/Kg150037 7/13/2006N/AN/A4-Chlorotoluene ND g/Kg18037 7/13/2006N/AN/A4-Methyl-2-Pentanone(MIBK) ND g/Kg150037 7/13/2006N/AN/AAcetone ND g/Kg370037 7/13/2006N/AN/AAcetonitrile ND g/Kg150037 7/13/2006N/AN/AAcrolein ND g/Kg18037 7/13/2006N/AN/AAcrylonitrile ND g/Kg18037 7/13/2006N/AN/ABenzene ND g/Kg18037 7/13/2006N/AN/ABenzyl Chloride ND g/Kg18037 7/13/2006N/AN/ABromobenzene ND g/Kg18037 7/13/2006N/AN/ABromochloromethane ND g/Kg18037 7/13/2006N/AN/ABromodichloromethane ND g/Kg18037 7/13/2006N/AN/ABromoform ND g/Kg18037 7/13/2006N/AN/ABromomethane ND g/Kg18037 7/13/2006N/AN/ACarbon Disulfide ND g/Kg18037 7/13/2006N/AN/ACarbon Tetrachloride ND g/Kg18037 7/13/2006N/AN/AChlorobenzene ND g/Kg18037 7/13/2006N/AN/AChloroethane ND g/Kg18037 7/13/2006N/AN/AChloroform ND g/Kg18037 7/13/2006N/AN/AChloromethane ND g/Kg18037 7/13/2006N/AN/A







Attn: Jim Dunn






cis-1,2-Dichloroethene ND g/Kg18037 7/13/2006N/AN/Acis-1,3-Dichloropropene ND g/Kg18037 7/13/2006N/AN/ACyclohexanone ND g/Kg150037 7/13/2006N/AN/ADibromochloromethane ND g/Kg18037 7/13/2006N/AN/ADibromomethane ND g/Kg18037 7/13/2006N/AN/ADichlorodifluoromethane ND g/Kg18037 7/13/2006N/AN/ADiisopropyl Ether ND g/Kg18037 7/13/2006N/AN/AEthyl Benzene ND g/Kg18037 7/13/2006N/AN/AFreon 113 ND g/Kg37037 7/13/2006N/AN/AHexachlorobutadiene ND g/Kg18037 7/13/2006N/AN/AIodomethane ND g/Kg150037 7/13/2006N/AN/AIsopropanol ND g/Kg370037 7/13/2006N/AN/AIsopropylbenzene ND g/Kg18037 7/13/2006N/AN/AMethyl-t-butyl Ether ND g/Kg18037 7/13/2006N/AN/AMethylene Chloride ND g/Kg92037 7/13/2006N/AN/An-Butylbenzene ND g/Kg18037 7/13/2006N/AN/An-Propylbenzene ND g/Kg18037 7/13/2006N/AN/ANaphthalene ND g/Kg18037 7/13/2006N/AN/Ap-Isopropyltoluene ND g/Kg18037 7/13/2006N/AN/APentachloroethane ND g/Kg18037 7/13/2006N/AN/Asec-Butylbenzene ND g/Kg18037 7/13/2006N/AN/AStyrene ND g/Kg18037 7/13/2006N/AN/Atert-Amyl Methyl Ether ND g/Kg18037 7/13/2006N/AN/Atert-Butanol (TBA) ND g/Kg150037 7/13/2006N/AN/Atert-Butyl Ethyl Ether ND g/Kg18037 7/13/2006N/AN/Atert-Butylbenzene ND g/Kg18037 7/13/2006N/AN/ATetrachloroethene ND g/Kg18037 7/13/2006N/AN/ATetrahydrofuran ND g/Kg150037 7/13/2006N/AN/AToluene ND g/Kg18037 7/13/2006N/AN/Atrans-1,2-Dichloroethene ND g/Kg18037 7/13/2006N/AN/Atrans-1,3-Dichloropropene ND g/Kg18037 7/13/2006N/AN/Atrans-1,4-Dichloro-2-butene ND g/Kg150037 7/13/2006N/AN/ATrichloroethene ND g/Kg18037 7/13/2006N/AN/ATrichlorofluoromethane ND g/Kg18037 7/13/2006N/AN/AVinyl Acetate ND g/Kg18037 7/13/2006N/AN/AVinyl Chloride ND g/Kg18037 7/13/2006N/AN/AXylenes, Total 530 g/Kg37037 7/13/2006N/AN/A









Attn: Jim Dunn







Reviewed by: HDINH



Antimony ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Arsenic ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Barium 85 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Beryllium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cadmium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Chromium 410 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cobalt 31 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Copper 36 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Lead 6.5 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Molybdenum ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Nickel 460 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Selenium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Silver ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Thallium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Vanadium 61 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Zinc 54 mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006

Reviewed by: HDINH

Analyzed by: Equeja



Reviewed by: HDINH



TPH as Gasoline 56000 g/Kg370037 7/13/2006N/AAtypical pattern. No indication of gasoline.

N/A









Attn: Jim Dunn






TPH as Diesel 170 mg/Kg125.0 SD060715A7/17/2006 SD060715A110 mg/Kg Motor Oil.

7/15/2006









Attn: Jim Dunn















Attn: Jim Dunn







Reviewed by: HDINH



Antimony 1.9 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Arsenic 8.9 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Barium 150 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Beryllium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cadmium 2.6 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Chromium 530 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cobalt 22 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Copper 510 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Lead 150 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Molybdenum ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Nickel 1500 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Selenium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Silver ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Thallium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Vanadium 47 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Zinc 350 mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006

Reviewed by: HDINH

Analyzed by: Equeja



Reviewed by: HDINH












Attn: Jim Dunn






TPH as Diesel ND mg/Kg12050 SD060715A7/18/2006 SD060715A930 mg/Kg Motor Oil. No Diesel pattern present.

7/15/2006


Analyzed by: JHsiangSurrogate Surrogate Recovery Control Limits (%)o-Terphenyl 106 41 137-







Attn: Jim Dunn






Chromium (VI) 11 mg/Kg1.010 SCR60607117/11/2006SCR60607117/11/2006









Attn: Jim Dunn













Attn: Jim Dunn








Analyzed by: AtamSurrogate Surrogate Recovery Control Limits (%)4-Bromofluorobenzene 91.0 60 130-Dibromofluoromethane 104 60 130-Toluene-d8 106 60 130-







Attn: Jim Dunn







Reviewed by: HDINH



Antimony 8.3 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Arsenic 9.1 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Barium 73 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Beryllium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cadmium 5.4 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Chromium 2500 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cobalt 13 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Copper 1400 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Lead 100 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Molybdenum ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Nickel 5700 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Selenium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Silver ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Thallium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Vanadium 23 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Zinc 330 mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006

Reviewed by: HDINH

Analyzed by: Equeja



Reviewed by: HDINH












Attn: Jim Dunn















Attn: Jim Dunn




Lab # : 50220-018 Sample ID: 06UST-01-4 Matrix: Solid Sample Date: 6/29/2006 4:10 PM







Attn: Jim Dunn













Attn: Jim Dunn







Reviewed by: HDINH



Antimony ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Arsenic 13 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Barium 82 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Beryllium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cadmium ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Chromium 110 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Cobalt 23 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Copper 81 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Lead 52 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Molybdenum ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Nickel 62 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Selenium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Silver ND mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Thallium ND mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006Vanadium 83 mg/Kg1.01.0 SM0607167/17/2006SM0607167/16/2006Zinc 100 mg/Kg2.01.0 SM0607167/17/2006SM0607167/16/2006

Reviewed by: HDINH

Analyzed by: Equeja



Reviewed by: HDINH












Attn: Jim Dunn






TPH as Diesel ND mg/Kg2.51.0 SD060715B7/18/2006SD060715B55 mg/Kg Motor Oil. No Diesel pattern present.

7/15/2006









Attn: Jim Dunn




Lab # : 50220-020 Sample ID: Equip-1 Matrix: Liquid Sample Date: 6/29/2006 2:00 PM

Parameter Result UnitsDetection LimitD/P-F QC BatchQual Prep Date Analysis DatePrep BatchChromium-VI: EPA 7196A for Water and Groundwater / Std. Methods (18th Ed.) 3500-Cr-D for Wastewater

Chromium (VI) ND mg/L0.0101.0 WCR60606306/30/2006N/AN/A


Analyzed by: RLazaro

Parameter Result UnitsDetection LimitD/P-F QC BatchQual Prep Date Analysis DatePrep BatchCyanide, Total: EPA 9010C/9014 for Groundwater and Water - EPA 335.2 for Wastewater

Cyanide, total ND mg/L0.0201.0 WCN0607057/5/2006WCN0607057/5/2006

Reviewed by: hdinh








Attn: Jim Dunn





Parameter Result UnitsDetection LimitD/P-F QC BatchQual Prep Date Analysis DatePrep BatchVOCs: EPA 5030C / EPA 8260B for Groundwater and Water - EPA 624 for Wastewater

1,1,1,2-Tetrachloroethane ND g/L0.501.0 WM20607117/12/2006N/AN/A1,1,1-Trichloroethane ND g/L0.501.0 WM20607117/12/2006N/AN/A1,1,2,2-Tetrachloroethane ND g/L0.501.0 WM20607117/12/2006N/AN/A1,1,2-Trichloroethane ND g/L0.501.0 WM20607117/12/2006N/AN/A1,1-Dichloroethane ND g/L0.501.0 WM20607117/12/2006N/AN/A1,1-Dichloroethene ND g/L0.501.0 WM20607117/12/2006N/AN/A1,1-Dichloropropene ND g/L0.501.0 WM20607117/12/2006N/AN/A1,2,3-Trichlorobenzene ND g/L5.01.0 WM20607117/12/2006N/AN/A1,2,3-Trichloropropane ND g/L0.501.0 WM20607117/12/2006N/AN/A1,2,4-Trichlorobenzene ND g/L5.01.0 WM20607117/12/2006N/AN/A1,2,4-Trimethylbenzene ND g/L5.01.0 WM20607117/12/2006N/AN/A1,2-Dibromo-3-Chloropropane ND g/L5.01.0 WM20607117/12/2006N/AN/A1,2-Dibromoethane (EDB) ND g/L0.501.0 WM20607117/12/2006N/AN/A1,2-Dichlorobenzene ND g/L0.501.0 WM20607117/12/2006N/AN/A1,2-Dichloroethane ND g/L0.501.0 WM20607117/12/2006N/AN/A1,2-Dichloropropane ND g/L0.501.0 WM20607117/12/2006N/AN/A1,3,5-Trimethylbenzene ND g/L5.01.0 WM20607117/12/2006N/AN/A1,3-Dichlorobenzene ND g/L0.501.0 WM20607117/12/2006N/AN/A1,3-Dichloropropane ND g/L0.501.0 WM20607117/12/2006N/AN/A1,4-Dichlorobenzene ND g/L0.501.0 WM20607117/12/2006N/AN/A1,4-Dioxane ND g/L501.0 WM20607117/12/2006N/AN/A2,2-Dichloropropane ND g/L0.501.0 WM20607117/12/2006N/AN/A2-Butanone (MEK) ND g/L201.0 WM20607117/12/2006N/AN/A2-Chloroethyl-vinyl Ether ND g/L5.01.0 WM20607117/12/2006N/AN/A2-Chlorotoluene ND g/L5.01.0 WM20607117/12/2006N/AN/A2-Hexanone ND g/L201.0 WM20607117/12/2006N/AN/A4-Chlorotoluene ND g/L5.01.0 WM20607117/12/2006N/AN/A4-Methyl-2-Pentanone(MIBK) ND g/L201.0 WM20607117/12/2006N/AN/AAcetone ND g/L201.0 WM20607117/12/2006N/AN/AAcetonitrile ND g/L5.01.0 WM20607117/12/2006N/AN/AAcrolein ND g/L5.01.0 WM20607117/12/2006N/AN/AAcrylonitrile ND g/L5.01.0 WM20607117/12/2006N/AN/ABenzene ND g/L0.501.0 WM20607117/12/2006N/AN/ABenzyl Chloride ND g/L5.01.0 WM20607117/12/2006N/AN/ABromobenzene ND g/L0.501.0 WM20607117/12/2006N/AN/ABromochloromethane ND g/L0.501.0 WM20607117/12/2006N/AN/ABromodichloromethane ND g/L0.501.0 WM20607117/12/2006N/AN/ABromoform ND g/L0.501.0 WM20607117/12/2006N/AN/ABromomethane ND g/L0.501.0 WM20607117/12/2006N/AN/ACarbon Disulfide ND g/L0.501.0 WM20607117/12/2006N/AN/ACarbon Tetrachloride ND g/L0.501.0 WM20607117/12/2006N/AN/AChlorobenzene ND g/L0.501.0 WM20607117/12/2006N/AN/AChloroethane ND g/L0.501.0 WM20607117/12/2006N/AN/AChloroform ND g/L0.501.0 WM20607117/12/2006N/AN/AChloromethane ND g/L0.501.0 WM20607117/12/2006N/AN/A







Attn: Jim Dunn






cis-1,2-Dichloroethene ND g/L0.501.0 WM20607117/12/2006N/AN/Acis-1,3-Dichloropropene ND g/L0.501.0 WM20607117/12/2006N/AN/ACyclohexanone ND g/L201.0 WM20607117/12/2006N/AN/ADibromochloromethane ND g/L0.501.0 WM20607117/12/2006N/AN/ADibromomethane ND g/L0.501.0 WM20607117/12/2006N/AN/ADichlorodifluoromethane ND g/L0.501.0 WM20607117/12/2006N/AN/ADiisopropyl Ether ND g/L5.01.0 WM20607117/12/2006N/AN/AEthyl Benzene ND g/L0.501.0 WM20607117/12/2006N/AN/AFreon 113 ND g/L5.01.0 WM20607117/12/2006N/AN/AHexachlorobutadiene ND g/L5.01.0 WM20607117/12/2006N/AN/AIodomethane ND g/L5.01.0 WM20607117/12/2006N/AN/AIsopropanol ND g/L201.0 WM20607117/12/2006N/AN/AIsopropylbenzene ND g/L1.01.0 WM20607117/12/2006N/AN/AMethyl-t-butyl Ether ND g/L1.01.0 WM20607117/12/2006N/AN/AMethylene Chloride ND g/L201.0 WM20607117/12/2006N/AN/An-Butylbenzene ND g/L5.01.0 WM20607117/12/2006N/AN/An-Propylbenzene ND g/L5.01.0 WM20607117/12/2006N/AN/ANaphthalene ND g/L5.01.0 WM20607117/12/2006N/AN/Ap-Isopropyltoluene ND g/L5.01.0 WM20607117/12/2006N/AN/APentachloroethane ND g/L0.501.0 WM20607117/12/2006N/AN/Asec-Butylbenzene ND g/L5.01.0 WM20607117/12/2006N/AN/AStyrene ND g/L0.501.0 WM20607117/12/2006N/AN/Atert-Amyl Methyl Ether ND g/L5.01.0 WM20607117/12/2006N/AN/Atert-Butanol (TBA) ND g/L101.0 WM20607117/12/2006N/AN/Atert-Butyl Ethyl Ether ND g/L5.01.0 WM20607117/12/2006N/AN/Atert-Butylbenzene ND g/L5.01.0 WM20607117/12/2006N/AN/ATetrachloroethene ND g/L0.501.0 WM20607117/12/2006N/AN/ATetrahydrofuran ND g/L201.0 WM20607117/12/2006N/AN/AToluene ND g/L0.501.0 WM20607117/12/2006N/AN/Atrans-1,2-Dichloroethene ND g/L0.501.0 WM20607117/12/2006N/AN/Atrans-1,3-Dichloropropene ND g/L0.501.0 WM20607117/12/2006N/AN/Atrans-1,4-Dichloro-2-butene ND g/L1.01.0 WM20607117/12/2006N/AN/ATrichloroethene ND g/L0.501.0 WM20607117/12/2006N/AN/ATrichlorofluoromethane ND g/L0.501.0 WM20607117/12/2006N/AN/AVinyl Acetate ND g/L5.01.0 WM20607117/12/2006N/AN/AVinyl Chloride ND g/L0.501.0 WM20607117/12/2006N/AN/AXylenes, Total ND g/L0.501.0 WM20607117/12/2006N/AN/A


Analyzed by: TAFSurrogate Surrogate Recovery Control Limits (%)4-Bromofluorobenzene 94.9 60 130-Dibromofluoromethane 110 60 130-Toluene-d8 77.4 60 130-







Attn: Jim Dunn





Parameter Result UnitsDetection LimitD/P-F QC BatchQual Prep Date Analysis DatePrep BatchEPA 7470A Mercury for Water and Groundwater / EPA 245.1 Mercury for Wastewater

Mercury ND mg/L0.00021.0 WHG0607077/7/2006WHG0607077/7/2006



Parameter Result UnitsDetection LimitD/P-F QC BatchQual Prep Date Analysis DatePrep BatchICP Metals: EPA 3010A / EPA 6010B for Groundwater and Water - EPA 200.7 for Wastewater

Antimony ND mg/L0.0101.0 WM0606306/30/2006WM0606306/30/2006Arsenic ND mg/L0.0101.0 WM0606306/30/2006WM0606306/30/2006Barium ND mg/L0.00501.0 WM0606306/30/2006WM0606306/30/2006Beryllium ND mg/L0.00501.0 WM0606306/30/2006WM0606306/30/2006Cadmium ND mg/L0.00201.0 WM0606306/30/2006WM0606306/30/2006Chromium ND mg/L0.00501.0 WM0606306/30/2006WM0606306/30/2006Cobalt ND mg/L0.00501.0 WM0606306/30/2006WM0606306/30/2006Copper ND mg/L0.00501.0 WM0606306/30/2006WM0606306/30/2006Lead ND mg/L0.00501.0 WM0606306/30/2006WM0606306/30/2006Molybdenum ND mg/L0.00501.0 WM0606306/30/2006WM0606306/30/2006Nickel ND mg/L0.00501.0 WM0606306/30/2006WM0606306/30/2006Selenium ND mg/L0.0201.0 WM0606306/30/2006WM0606306/30/2006Silver ND mg/L0.00501.0 WM0606306/30/2006WM0606306/30/2006Thallium ND mg/L0.0201.0 WM0606306/30/2006WM0606306/30/2006Vanadium ND mg/L0.00501.0 WM0606306/30/2006WM0606306/30/2006Zinc ND mg/L0.0101.0 WM0606306/30/2006WM0606306/30/2006

Reviewed by: EQUEJA

Analyzed by: Hdinh

Parameter Result UnitsDetection LimitD/P-F QC BatchQual Prep Date Analysis DatePrep BatchpH - EPA 9040C for Groundwater and Water - EPA 150.1 for Wastewater

pH 6.7 pH Units1.01.0 WPH0606306/30/2006N/AN/A

Reviewed by: RLAZARO



TPH as Gasoline ND g/L251.0 WM20607117/12/2006N/AN/A


Analyzed by: TAFSurrogate Surrogate Recovery Control Limits (%)4-Bromofluorobenzene 108 60 130-Dibromofluoromethane 99.8 60 130-Toluene-d8 76.2 60 130-







Attn: Jim Dunn





Parameter Result UnitsDetection LimitD/P-F QC BatchQual Prep Date Analysis DatePrep BatchTPH-Extractable: EPA 3510C / EPA 8015B

TPH as Diesel ND g/L501.0 WD060714A7/16/2006WD060714A7/14/2006

Reviewed by: dba




Entech Analytical Labs, Inc. _ 3334 Victor Court , Santa Clara, CA 95054 Phone: (408) 588-0200 Fax: (408) 588-0201

ParameterSample Result

Replicate Result QC TypeRPD

RPD LimitsUnits

Validated by: HDINH - 07/06/06QC/Prep Batch ID: SPH060705QC/Prep Date: 7/5/2006

Replicate - Solid - pH - EPA 9045D

Replicate6.461 6.454 0.1 30.0pH 50220-019 pH Units

ParameterSample Result

Replicate Result QC TypeRPD

RPD LimitsUnits

Validated by: RLAZARO - 07/05/06QC Batch ID: WPH060630QC Batch Analysis Date: 6/30/2006

Replicate - Liquid - pH - EPA 9040C for Groundwater and Water - EPA 150.1 for Wastewater

Replicate6.670 6.641 0.4 25.0pH 50220-020 pH Units

QC-Replicate - ECunniffe - 7/19/2006 6:58:47 PM


Validated by: dba - 07/17/06QC/Prep Batch ID: SD060713BQC/Prep Date: 7/13/2006Parameter Result DF UnitsPQLR

Method Blank - Solid - TPH-Extractable: EPA 8015B

TPH as Diesel ND 1 mg/Kg2.5

Surrogate for Blank % Recovery Control Limitso-Terphenyl 84.9 41 137-

Reviewed by: dba - 07/17/06QC Batch ID: SD060713BQC/Prep Date: 7/13/2006

LCS / LCSD - Solid - TPH-Extractable: EPA 8015B

Parameter Method Blank Spike Amt SpikeResult % Recovery Recovery LimitsLCS

Units<2.5 50 49.9TPH as Diesel 45 - 14099.8mg/Kg<10 50 43.0TPH as Motor Oil 45 - 14086.0mg/Kg

Surrogate % Recovery Control Limitso-Terphenyl 87.4 41 137-

Parameter Method Blank Spike Amt SpikeResult % Recovery Recovery LimitsLCSD

RPD RPD LimitsUnits<2.5 50 48.9 30.0TPH as Diesel 45 - 1402.097.8mg/Kg<10 50 43.5 30.0TPH as Motor Oil 45 - 1401.287.0mg/Kg


QCReport - ECunniffe - 7/19/2006 6:53:25 PM


Validated by: dba - 07/17/06QC/Prep Batch ID: SD060715AQC/Prep Date: 7/15/2006Parameter Result DF UnitsPQLR




Reviewed by: dba - 07/17/06Prep/QC Batch ID: SD060715A /SD060715AQC/Prep Date: 7/15/2006






RPD RPD LimitsUnits<2.5 50 36.0 30.0TPH as Diesel 45 - 1401.172.0mg/Kg<10 50 34.9 30.0TPH as Motor Oil 45 - 1404.169.8mg/Kg


Reviewed by: ECunniffe - 07/18/06QC/Prep Batch ID: SD060715AQC/Prep Date: 7/15/2006

MS / MSD - Solid - TPH-Extractable: EPA 8015B

Parameter Sample Result

Spike Amount

Spike Result Units % Recovery

Recovery Limits

AnalysisDate

Sample Spiked: 50415-005MS

ND 50 42.3TPH as Diesel 45 - 1407/16/2006mg/Kg 84.6



Spike Amount


Recovery Limits

AnalysisDate

Sample Spiked: 50415-005

RPD RPD Limits

MSD

ND 50 40.9 30.0TPH as Diesel 45 - 1407/16/2006mg/Kg 3.481.8




Validated by: ECunniffe - 07/18/06QC/Prep Batch ID: SD060715BQC/Prep Date: 7/15/2006Parameter Result DF UnitsPQLR




Reviewed by: ECunniffe - 07/18/06QC Batch ID: SD060715BQC/Prep Date: 7/15/2006






RPD RPD LimitsUnits<2.5 50 36.7 30.0TPH as Diesel 45 - 1401173.4mg/Kg<10 50 33.5 30.0TPH as Motor Oil 45 - 1400.6067.0mg/Kg




Validated by: dba - 07/17/06QC/Prep Batch ID: WD060714AQC/Prep Date: 7/14/2006Parameter Result DF UnitsPQLR

Method Blank - Liquid - TPH-Extractable: EPA 3510C / EPA 8015B

TPH as Diesel ND 1 g/L50


Reviewed by: dba - 07/17/06QC Batch ID: WD060714AQC/Prep Date: 7/14/2006

LCS / LCSD - Liquid - TPH-Extractable: EPA 3510C / EPA 8015B


Units<50 1000 574TPH as Diesel 40 - 13857.4g/L<200 1000 729TPH as Motor Oil 40 - 13872.9g/L



RPD RPD LimitsUnits<50 1000 716 25.0TPH as Diesel 40 - 1382271.6g/L<200 1000 761 25.0TPH as Motor Oil 40 - 1384.276.1g/L




Validated by: MaiChiTu - 07/14/06QC Batch ID: SM3060714QC Batch Analysis Date: 7/14/2006Parameter Result DF UnitsPQLR

Method Blank - Solid - EPA 8260B

1,1,1,2-Tetrachloroethane ND 1 g/Kg5.01,1,1-Trichloroethane ND 1 g/Kg5.01,1,2,2-Tetrachloroethane ND 1 g/Kg5.01,1,2-Trichloroethane ND 1 g/Kg5.01,1-Dichloroethane ND 1 g/Kg5.01,1-Dichloroethene ND 1 g/Kg5.01,1-Dichloropropene ND 1 g/Kg5.01,2,3-Trichlorobenzene ND 1 g/Kg5.01,2,3-Trichloropropane ND 1 g/Kg5.01,2,4-Trichlorobenzene ND 1 g/Kg5.01,2,4-Trimethylbenzene ND 1 g/Kg5.01,2-Dibromo-3-Chloropropane ND 1 g/Kg5.01,2-Dibromoethane (EDB) ND 1 g/Kg5.01,2-Dichlorobenzene ND 1 g/Kg5.01,2-Dichloroethane ND 1 g/Kg5.01,2-Dichloropropane ND 1 g/Kg5.01,3,5-Trimethylbenzene ND 1 g/Kg5.01,3-Dichlorobenzene ND 1 g/Kg5.01,3-Dichloropropane ND 1 g/Kg5.01,4-Dichlorobenzene ND 1 g/Kg5.01,4-Dioxane ND 1 g/Kg2002,2-Dichloropropane ND 1 g/Kg5.02-Butanone (MEK) ND 1 g/Kg402-Chloroethyl-vinyl Ether ND 1 g/Kg5.02-Chlorotoluene ND 1 g/Kg5.02-Hexanone ND 1 g/Kg404-Chlorotoluene ND 1 g/Kg5.04-Methyl-2-Pentanone(MIBK) ND 1 g/Kg40Acetone ND 1 g/Kg100Acetonitrile ND 1 g/Kg40Acrolein ND 1 g/Kg5.0Acrylonitrile ND 1 g/Kg5.0Benzene ND 1 g/Kg5.0Benzyl Chloride ND 1 g/Kg5.0Bromobenzene ND 1 g/Kg5.0Bromochloromethane ND 1 g/Kg5.0Bromodichloromethane ND 1 g/Kg5.0Bromoform ND 1 g/Kg5.0Bromomethane ND 1 g/Kg5.0Carbon Disulfide ND 1 g/Kg5.0Carbon Tetrachloride ND 1 g/Kg5.0Chlorobenzene ND 1 g/Kg5.0Chloroethane ND 1 g/Kg5.0Chloroform ND 1 g/Kg5.0Chloromethane ND 1 g/Kg5.0cis-1,2-Dichloroethene ND 1 g/Kg5.0cis-1,3-Dichloropropene ND 1 g/Kg5.0Cyclohexanone ND 1 g/Kg40Dibromochloromethane ND 1 g/Kg5.0Dibromomethane ND 1 g/Kg5.0





Dichlorodifluoromethane ND 1 g/Kg5.0Diisopropyl Ether ND 1 g/Kg5.0Ethyl Benzene ND 1 g/Kg5.0Freon 113 ND 1 g/Kg10Hexachlorobutadiene ND 1 g/Kg5.0Iodomethane ND 1 g/Kg40Isopropanol ND 1 g/Kg100Isopropylbenzene ND 1 g/Kg5.0Methylene Chloride ND 1 g/Kg25Methyl-t-butyl Ether ND 1 g/Kg5.0Naphthalene ND 1 g/Kg5.0n-Butylbenzene ND 1 g/Kg5.0n-Propylbenzene ND 1 g/Kg5.0Pentachloroethane ND 1 g/Kg5.0p-Isopropyltoluene ND 1 g/Kg5.0sec-Butylbenzene ND 1 g/Kg5.0Styrene ND 1 g/Kg5.0tert-Amyl Methyl Ether ND 1 g/Kg5.0tert-Butanol (TBA) ND 1 g/Kg40tert-Butyl Ethyl Ether ND 1 g/Kg5.0tert-Butylbenzene ND 1 g/Kg5.0Tetrachloroethene ND 1 g/Kg5.0Tetrahydrofuran ND 1 g/Kg40Toluene ND 1 g/Kg5.0trans-1,2-Dichloroethene ND 1 g/Kg5.0trans-1,3-Dichloropropene ND 1 g/Kg5.0trans-1,4-Dichloro-2-butene ND 1 g/Kg40Trichloroethene ND 1 g/Kg5.0Trichlorofluoromethane ND 1 g/Kg5.0Vinyl Acetate ND 1 g/Kg5.0Vinyl Chloride ND 1 g/Kg5.0Xylenes, Total ND 1 g/Kg10

Surrogate for Blank % Recovery Control Limits4-Bromofluorobenzene 92.1 60 130-Dibromofluoromethane 89.4 60 130-Toluene-d8 92.7 60 130-


Method Blank - Solid - TPH-Purgeable: GC/MS

TPH as Gasoline ND 1 g/Kg100




Reviewed by: MaiChiTu - 07/14/06QC Batch ID: SM3060714QC Batch ID Analysis Date: 7/14/2006

LCS / LCSD - Solid - EPA 8260B


Units<5.0 40 33.81,1-Dichloroethene 70 - 13584.5g/Kg<5.0 40 41.5Benzene 70 - 135104g/Kg<5.0 40 44.5Chlorobenzene 70 - 135111g/Kg<5.0 40 30.5Methyl-t-butyl Ether 70 - 13576.2g/Kg<5.0 40 41.1Toluene 70 - 135103g/Kg<5.0 40 45.8Trichloroethene 70 - 135114g/Kg

Surrogate % Recovery Control Limits4-Bromofluorobenzene 97.5 60 130-Dibromofluoromethane 96.7 60 130-Toluene-d8 93.6 60 130-


RPD RPD LimitsUnits<5.0 40 39.3 30.01,1-Dichloroethene 70 - 1351598.2g/Kg<5.0 40 46.3 30.0Benzene 70 - 13511116g/Kg<5.0 40 44.7 30.0Chlorobenzene 70 - 1350.45112g/Kg<5.0 40 32.2 30.0Methyl-t-butyl Ether 70 - 1355.480.5g/Kg<5.0 40 46.2 30.0Toluene 70 - 13512116g/Kg<5.0 40 43.1 30.0Trichloroethene 70 - 1356.1108g/Kg



LCS / LCSD - Solid - TPH-Purgeable: GC/MS


Units<100 250 203TPH as Gasoline 70 - 13081.2g/Kg



RPD RPD LimitsUnits<100 250 185 30.0TPH as Gasoline 70 - 1309.374.0g/Kg







Surrogate for Blank % Recovery Control Limits4-Bromofluorobenzene 87.0 60 130-Dibromofluoromethane 121 60 130-Toluene-d8 105 60 130-




Surrogate for Blank % Recovery Control Limits4-Bromofluorobenzene 90.8 60 130-Dibromofluoromethane 108 60 130-Toluene-d8 98.1 60 130-






Units<5.0 40 34.31,1-Dichloroethene 70 - 13585.8g/Kg<5.0 40 39.5Benzene 70 - 13598.8g/Kg<5.0 40 40.9Chlorobenzene 70 - 135102g/Kg<5.0 40 34.6Methyl-t-butyl Ether 70 - 13586.5g/Kg<5.0 40 39.4Toluene 70 - 13598.5g/Kg<5.0 40 43.7Trichloroethene 70 - 135109g/Kg



RPD RPD LimitsUnits<5.0 40 31.5 30.01,1-Dichloroethene 70 - 1358.578.8g/Kg<5.0 40 39.9 30.0Benzene 70 - 1351.099.8g/Kg<5.0 40 40.3 30.0Chlorobenzene 70 - 1351.5101g/Kg<5.0 40 31.2 30.0Methyl-t-butyl Ether 70 - 1351078.0g/Kg<5.0 40 37.0 30.0Toluene 70 - 1356.392.5g/Kg<5.0 40 42.9 30.0Trichloroethene 70 - 1351.8107g/Kg








RPD RPD LimitsUnits<100 250 205 30.0TPH as Gasoline 70 - 1308.482.0g/Kg







Units<5.0 40 43.21,1-Dichloroethene 70 - 135108g/Kg<5.0 40 46.2Benzene 70 - 135116g/Kg<5.0 40 47.6Chlorobenzene 70 - 135119g/Kg<5.0 40 35.8Methyl-t-butyl Ether 70 - 13589.5g/Kg<5.0 40 46.1Toluene 70 - 135115g/Kg<5.0 40 45.8Trichloroethene 70 - 135114g/Kg



RPD RPD LimitsUnits<5.0 40 38.8 30.01,1-Dichloroethene 70 - 1351197.0g/Kg<5.0 40 43.3 30.0Benzene 70 - 1356.5108g/Kg<5.0 40 44.9 30.0Chlorobenzene 70 - 1355.8112g/Kg<5.0 40 32.6 30.0Methyl-t-butyl Ether 70 - 1359.481.5g/Kg<5.0 40 44.0 30.0Toluene 70 - 1354.7110g/Kg<5.0 40 43.6 30.0Trichloroethene 70 - 1354.9109g/Kg








RPD RPD LimitsUnits<100 250 265 30.0TPH as Gasoline 70 - 13020106g/Kg




Validated by: MaiChiTu - 07/11/06QC Batch ID: WM2060711QC Batch Analysis Date: 7/11/2006Parameter Result DF UnitsPQLR

Method Blank - Liquid - VOCs: EPA 5030C / EPA 8260B for Groundwater and Water - EPA 624 for Wastewater

1,1,1,2-Tetrachloroethane ND 1 g/L0.501,1,1-Trichloroethane ND 1 g/L0.501,1,2,2-Tetrachloroethane ND 1 g/L0.501,1,2-Trichloroethane ND 1 g/L0.501,1-Dichloroethane ND 1 g/L0.501,1-Dichloroethene ND 1 g/L0.501,1-Dichloropropene ND 1 g/L0.501,2,3-Trichlorobenzene ND 1 g/L5.01,2,3-Trichloropropane ND 1 g/L0.501,2,4-Trichlorobenzene ND 1 g/L5.01,2,4-Trimethylbenzene ND 1 g/L5.01,2-Dibromo-3-Chloropropane ND 1 g/L5.01,2-Dibromoethane (EDB) ND 1 g/L0.501,2-Dichlorobenzene ND 1 g/L0.501,2-Dichloroethane ND 1 g/L0.501,2-Dichloropropane ND 1 g/L0.501,3,5-Trimethylbenzene ND 1 g/L5.01,3-Dichlorobenzene ND 1 g/L0.501,3-Dichloropropane ND 1 g/L0.501,4-Dichlorobenzene ND 1 g/L0.501,4-Dioxane ND 1 g/L502,2-Dichloropropane ND 1 g/L0.502-Butanone (MEK) ND 1 g/L202-Chloroethyl-vinyl Ether ND 1 g/L5.02-Chlorotoluene ND 1 g/L5.02-Hexanone ND 1 g/L204-Chlorotoluene ND 1 g/L5.04-Methyl-2-Pentanone(MIBK) ND 1 g/L20Acetone ND 1 g/L20Acetonitrile ND 1 g/L5.0Acrolein ND 1 g/L5.0Acrylonitrile ND 1 g/L5.0Benzene ND 1 g/L0.50Benzyl Chloride ND 1 g/L5.0Bromobenzene ND 1 g/L0.50Bromochloromethane ND 1 g/L0.50Bromodichloromethane ND 1 g/L0.50Bromoform ND 1 g/L0.50Bromomethane ND 1 g/L0.50Carbon Disulfide ND 1 g/L0.50Carbon Tetrachloride ND 1 g/L0.50Chlorobenzene ND 1 g/L0.50Chloroethane ND 1 g/L0.50Chloroform ND 1 g/L0.50Chloromethane ND 1 g/L0.50cis-1,2-Dichloroethene ND 1 g/L0.50cis-1,3-Dichloropropene ND 1 g/L0.50Cyclohexanone ND 1 g/L20Dibromochloromethane ND 1 g/L0.50





Dibromomethane ND 1 g/L0.50Dichlorodifluoromethane ND 1 g/L0.50Diisopropyl Ether ND 1 g/L5.0Ethyl Benzene ND 1 g/L0.50Freon 113 ND 1 g/L5.0Hexachlorobutadiene ND 1 g/L5.0Iodomethane ND 1 g/L5.0Isopropanol ND 1 g/L20Isopropylbenzene ND 1 g/L1.0Methylene Chloride ND 1 g/L20Methyl-t-butyl Ether ND 1 g/L1.0Naphthalene ND 1 g/L5.0n-Butylbenzene ND 1 g/L5.0n-Propylbenzene ND 1 g/L5.0Pentachloroethane ND 1 g/L0.50p-Isopropyltoluene ND 1 g/L5.0sec-Butylbenzene ND 1 g/L5.0Styrene ND 1 g/L0.50tert-Amyl Methyl Ether ND 1 g/L5.0tert-Butanol (TBA) ND 1 g/L10tert-Butyl Ethyl Ether ND 1 g/L5.0tert-Butylbenzene ND 1 g/L5.0Tetrachloroethene ND 1 g/L0.50Tetrahydrofuran ND 1 g/L20Toluene ND 1 g/L0.50trans-1,2-Dichloroethene ND 1 g/L0.50trans-1,3-Dichloropropene ND 1 g/L0.50trans-1,4-Dichloro-2-butene ND 1 g/L1.0Trichloroethene ND 1 g/L0.50Trichlorofluoromethane ND 1 g/L0.50Vinyl Acetate ND 1 g/L5.0Vinyl Chloride ND 1 g/L0.50Xylenes, Total ND 1 g/L0.50

Surrogate for Blank % Recovery Control Limits4-Bromofluorobenzene 95.8 70 125-Dibromofluoromethane 105 70 125-Toluene-d8 77.8 70 125-


Method Blank - Liquid - TPH-Purgeable: GC/MS

TPH as Gasoline ND 1 g/L25

Surrogate for Blank % Recovery Control Limits4-Bromofluorobenzene 110 60 130-Dibromofluoromethane 94.9 60 130-Toluene-d8 76.6 60 130-



Reviewed by: MaiChiTu - 07/11/06QC Batch ID: WM2060711QC Batch ID Analysis Date: 7/11/2006

LCS / LCSD - Liquid - VOCs: EPA 5030C / EPA 8260B for Groundwater and Water - EPA 624 for Wastewater


Units<0.50 20 21.41,1-Dichloroethene 70 - 130107g/L<0.50 20 22.0Benzene 70 - 130110g/L<0.50 20 22.1Chlorobenzene 70 - 130110g/L<1.0 20 18.2Methyl-t-butyl Ether 70 - 13091.2g/L

<0.50 20 20.8Toluene 70 - 130104g/L<0.50 20 21.8Trichloroethene 70 - 130109g/L



RPD RPD LimitsUnits<0.50 20 21.4 25.01,1-Dichloroethene 70 - 1300.22107g/L<0.50 20 21.9 25.0Benzene 70 - 1300.67109g/L<0.50 20 21.9 25.0Chlorobenzene 70 - 1300.61110g/L<1.0 20 19.1 25.0Methyl-t-butyl Ether 70 - 1304.595.4g/L

<0.50 20 20.7 25.0Toluene 70 - 1300.32104g/L<0.50 20 21.7 25.0Trichloroethene 70 - 1300.77108g/L



LCS / LCSD - Liquid - TPH-Purgeable: GC/MS


Units<25 250 239TPH as Gasoline 65 - 13595.7g/L



RPD RPD LimitsUnits<25 250 242 25.0TPH as Gasoline 65 - 1351.096.7g/L




Reviewed by: HDINH - 07/10/06QC Batch ID: SCN060705QC/Prep Date: 7/6/2006

LCS / LCSD - Solid - Cyanide, Total: EPA 9010C/9014


Units<1.0 5.0 5.27Cyanide, total 70 - 130105mg/Kg


RPD RPD LimitsUnits<1.0 5.0 4.94 30.0Cyanide, total 70 - 1306.498.8mg/Kg



Reviewed by: hdinh - 07/05/06QC Batch ID: WCN060705QC/Prep Date: 7/5/2006

LCS / LCSD - Liquid - Cyanide, Total: EPA 9010C/9014 for Groundwater and Water - EPA 335.2 for Wastewater


Units<0.020 0.10 0.101Cyanide, total 75 - 125101mg/L


RPD RPD LimitsUnits<0.020 0.10 0.0932 25.0Cyanide, total 75 - 1258.393.2mg/L



Reviewed by: hdinh - 07/05/06QC/Prep Batch ID: WCN060705QC/Prep Date: 7/5/2006

MS / MSD - Liquid - Cyanide, Total: EPA 9010C/9014 for Groundwater and Water - EPA 335.2 for Wastewater


Spike Amount


Recovery Limits

AnalysisDate


ND 0.10 0.0846Cyanide, total 75 - 1257/5/2006mg/L 84.6


Spike Amount


Recovery Limits

AnalysisDate


RPD RPD Limits

MSD

ND 0.10 0.0825 25.0Cyanide, total 75 - 1257/5/2006mg/L 2.582.5



Reviewed by: JISIDERIO - 07/11/06QC Batch ID: SCR6060711QC/Prep Date: 7/11/2006

LCS / LCSD - Solid - Chromium VI: EPA 7196A


Units<0.10 1.0 1.02Chromium (VI) 75 - 125102mg/Kg


RPD RPD LimitsUnits<0.10 1.0 0.994 30.0Chromium (VI) 75 - 1252.799.4mg/Kg



Reviewed by: JISIDERIO - 07/11/06QC/Prep Batch ID: SCR6060711QC/Prep Date: 7/11/2006

MS / MSD - Solid - Chromium VI: EPA 7196A


Spike Amount


Recovery Limits

AnalysisDate


1.00 1.0 1.94Chromium (VI) 75 - 1257/11/2006mg/Kg 93.4


Spike Amount


Recovery Limits

AnalysisDate


RPD RPD Limits

MSD

1.00 1.0 1.97 30.0Chromium (VI) 75 - 1257/11/2006mg/Kg 1.496.1



Reviewed by: JISIDERIO - 06/30/06QC Batch ID: WCR6060630QC Batch ID Analysis Date: 6/30/2006

LCS / LCSD - Liquid - Chromium-VI: EPA 7196A for Water and Groundwater / Std. Methods (18th Ed.) 3500-Cr-D for Wastewater


Units<0.010 0.10 0.0923Chromium (VI) 75 - 12592.3mg/L


RPD RPD LimitsUnits<0.010 0.10 0.0906 25.0Chromium (VI) 75 - 1251.890.6mg/L



Reviewed by: JISIDERIO - 06/30/06QC Batch ID: WCR6060630QC Batch ID Analysis Date: 6/30/2006

MS / MSD - Liquid - Chromium-VI: EPA 7196A for Water and Groundwater / Std. Methods (18th Ed.) 3500-Cr-D for Wastewater


Spike Amount


Recovery Limits

AnalysisDate


ND 0.10 0.0990Chromium (VI) 75 - 1256/30/2006mg/L 99.0


Spike Amount


Recovery Limits

AnalysisDate


RPD RPD Limits

MSD

ND 0.10 0.0962 25.0Chromium (VI) 75 - 1256/30/2006mg/L 2.996.2



Reviewed by: JISIDERIO - 07/07/06QC Batch ID: WHG060707QC/Prep Date: 7/7/2006

LCS / LCSD - Liquid - EPA 7470A Mercury for Water and Groundwater / EPA 245.1 Mercury for Wastewater


Units<0.0002 0.0020 0.00211Mercury 75 - 125106mg/L


RPD RPD LimitsUnits<0.0002 0.0020 0.00208 25.0Mercury 75 - 1251.4104mg/L



Reviewed by: HDINH - 07/18/06QC/Prep Batch ID: SHG060718AQC/Prep Date: 7/18/2006

MS / MSD - Solid - EPA 7471B / EPA 245.5 Mercury


Spike Amount


Recovery Limits

AnalysisDate


ND 0.40 0.326Mercury 75 - 1257/18/2006mg/Kg 81.5


Spike Amount


Recovery Limits

AnalysisDate


RPD RPD Limits

MSD

ND 0.40 0.368 30.0Mercury 75 - 1257/18/2006mg/Kg 1292.0



Reviewed by: HDINH - 07/18/06QC Batch ID: SM060716QC/Prep Date: 7/16/2006

LCS / LCSD - Solid - EPA 6010B Metals by ICP


Units<1.0 50 45.4Antimony 75 - 12590.7mg/Kg<1.0 50 46.4Arsenic 75 - 12592.8mg/Kg<1.0 50 46.7Barium 75 - 12593.4mg/Kg<1.0 50 46.0Beryllium 75 - 12592.0mg/Kg<1.0 50 45.8Cadmium 75 - 12591.7mg/Kg<1.0 50 48.0Chromium 75 - 12596.0mg/Kg<1.0 50 47.1Cobalt 75 - 12594.3mg/Kg<1.0 50 46.9Copper 75 - 12593.9mg/Kg<1.0 50 48.1Lead 75 - 12596.2mg/Kg<1.0 50 47.5Molybdenum 75 - 12594.9mg/Kg<1.0 50 49.1Nickel 75 - 12598.2mg/Kg<2.0 50 42.7Selenium 75 - 12585.4mg/Kg<1.0 50 46.1Silver 75 - 12592.2mg/Kg<2.0 50 43.8Thallium 75 - 12587.6mg/Kg<1.0 50 46.9Vanadium 75 - 12593.7mg/Kg<2.0 50 47.2Zinc 75 - 12594.3mg/Kg


RPD RPD LimitsUnits<1.0 50 44.8 25.0Antimony 75 - 1251.489.5mg/Kg<1.0 50 45.7 25.0Arsenic 75 - 1251.691.3mg/Kg<1.0 50 45.2 25.0Barium 75 - 1253.390.4mg/Kg<1.0 50 45.3 25.0Beryllium 75 - 1251.490.7mg/Kg<1.0 50 45.2 25.0Cadmium 75 - 1251.490.4mg/Kg<1.0 50 47.3 25.0Chromium 75 - 1251.694.5mg/Kg<1.0 50 46.5 25.0Cobalt 75 - 1251.493.0mg/Kg<1.0 50 46.0 25.0Copper 75 - 1251.992.1mg/Kg<1.0 50 47.2 25.0Lead 75 - 1252.094.3mg/Kg<1.0 50 46.4 25.0Molybdenum 75 - 1252.292.9mg/Kg<1.0 50 48.3 25.0Nickel 75 - 1251.596.7mg/Kg<2.0 50 42.0 25.0Selenium 75 - 1251.684.1mg/Kg<1.0 50 44.8 25.0Silver 75 - 1252.889.6mg/Kg<2.0 50 42.5 25.0Thallium 75 - 1253.184.9mg/Kg<1.0 50 46.1 25.0Vanadium 75 - 1251.792.1mg/Kg<2.0 50 46.3 25.0Zinc 75 - 1251.892.6mg/Kg



Reviewed by: DQueja - 06/30/06QC Batch ID: WM060630QC/Prep Date: 6/30/2006

LCS / LCSD - Liquid - ICP Metals: EPA 3010A / EPA 6010B for Groundwater and Water - EPA 200.7 for Wastewater


Units<0.010 0.50 0.485Antimony 75 - 12597.0mg/L<0.010 0.50 0.471Arsenic 75 - 12594.2mg/L

<0.0050 0.50 0.490Barium 75 - 12598.0mg/L<0.0050 0.50 0.476Beryllium 75 - 12595.2mg/L<0.0020 0.50 0.474Cadmium 75 - 12594.8mg/L<0.0050 0.50 0.477Chromium 75 - 12595.4mg/L<0.0050 0.50 0.488Cobalt 75 - 12597.6mg/L<0.0050 0.50 0.492Copper 75 - 12598.4mg/L<0.0050 0.50 0.492Lead 75 - 12598.4mg/L<0.0050 0.50 0.494Molybdenum 75 - 12598.8mg/L<0.0050 0.50 0.482Nickel 75 - 12596.4mg/L<0.020 0.50 0.455Selenium 75 - 12591.0mg/L

<0.0050 0.50 0.489Silver 75 - 12597.8mg/L<0.020 0.50 0.444Thallium 75 - 12588.8mg/L<0.050 1.0 0.985Tin 75 - 12598.5mg/L

<0.0020 0.50 0.503Titanium 75 - 125101mg/L<0.0050 0.50 0.492Vanadium 75 - 12598.4mg/L<0.010 0.50 0.480Zinc 75 - 12596.0mg/L


RPD RPD LimitsUnits<0.010 0.50 0.481 25.0Antimony 75 - 1250.8396.2mg/L<0.010 0.50 0.466 25.0Arsenic 75 - 1251.193.2mg/L

<0.0050 0.50 0.492 25.0Barium 75 - 1250.4198.4mg/L<0.0050 0.50 0.467 25.0Beryllium 75 - 1251.993.4mg/L<0.0020 0.50 0.473 25.0Cadmium 75 - 1250.2194.6mg/L<0.0050 0.50 0.474 25.0Chromium 75 - 1250.6394.8mg/L<0.0050 0.50 0.483 25.0Cobalt 75 - 1251.096.6mg/L<0.0050 0.50 0.486 25.0Copper 75 - 1251.297.2mg/L<0.0050 0.50 0.481 25.0Lead 75 - 1252.396.2mg/L<0.0050 0.50 0.485 25.0Molybdenum 75 - 1251.897.0mg/L<0.0050 0.50 0.475 25.0Nickel 75 - 1251.595.0mg/L<0.020 0.50 0.441 25.0Selenium 75 - 1253.188.2mg/L

<0.0050 0.50 0.485 25.0Silver 75 - 1250.8297.0mg/L<0.020 0.50 0.439 25.0Thallium 75 - 1251.187.8mg/L<0.050 1.0 0.972 25.0Tin 75 - 1251.397.2mg/L

<0.0020 0.50 0.492 25.0Titanium 75 - 1252.298.4mg/L<0.0050 0.50 0.488 25.0Vanadium 75 - 1250.8297.6mg/L<0.010 0.50 0.476 25.0Zinc 75 - 1250.8495.2mg/L



Reviewed by: HDINH - 07/18/06QC/Prep Batch ID: SM060716QC/Prep Date: 7/16/2006

MS / MSD - Solid - EPA 6010B Metals by ICP


Spike Amount


Recovery Limits

AnalysisDate


ND 50 15.9Antimony 75 - 1257/16/2006mg/Kg 31.7 ***7.34 50 46.1Arsenic 75 - 1257/16/2006mg/Kg 77.680.1 50 135Barium 75 - 1257/16/2006mg/Kg 109ND 50 42.3Beryllium 77 - 1257/16/2006mg/Kg 84.6ND 50 44.0Cadmium 75 - 1257/16/2006mg/Kg 88.078.8 50 123Chromium 75 - 1257/16/2006mg/Kg 87.78.51 50 51.9Cobalt 75 - 1257/16/2006mg/Kg 86.9180 50 211Copper 75 - 1257/16/2006mg/Kg 61.0 ***6.55 50 50.2Lead 75 - 1257/16/2006mg/Kg 87.4ND 50 41.2Molybdenum 75 - 1257/16/2006mg/Kg 82.5565 50 596Nickel 75 - 1257/16/2006mg/Kg 61.2 ***ND 50 21.7Selenium 75 - 1257/16/2006mg/Kg 43.4 ***ND 50 44.1Silver 75 - 1257/16/2006mg/Kg 88.3ND 50 36.3Thallium 75 - 1257/16/2006mg/Kg 72.7 ***65.6 50 107Zinc 75 - 1257/16/2006

***All MS/MSD recoveries that do not fall within the control limit are out due to the nature of the sample matrix. The batch was accepted by the LCS/LCSD recoveries.mg/Kg 83.6


Spike Amount


Recovery Limits

AnalysisDate


RPD RPD Limits

MSD

ND 50 16.0 25.0Antimony 75 - 1257/16/2006mg/Kg 0.6931.9 ***7.34 50 46.9 25.0Arsenic 75 - 1257/16/2006mg/Kg 1.979.180.1 50 130 25.0Barium 75 - 1257/16/2006mg/Kg 7.8101ND 50 43.2 25.0Beryllium 75 - 1257/16/2006mg/Kg 2.286.5ND 50 45.1 25.0Cadmium 75 - 1257/16/2006mg/Kg 2.490.278.8 50 127 25.0Chromium 75 - 1257/16/2006mg/Kg 1097.18.51 50 52.8 25.0Cobalt 75 - 1257/16/2006mg/Kg 2.088.6180 50 219 25.0Copper 75 - 1257/16/2006mg/Kg 2376.86.55 50 51.1 25.0Lead 75 - 1257/16/2006mg/Kg 2.089.2ND 50 41.8 25.0Molybdenum 75 - 1257/16/2006mg/Kg 1.483.7565 50 605 25.0Nickel 75 - 1257/16/2006mg/Kg 2679.2 ***ND 50 22.8 25.0Selenium 75 - 1257/16/2006mg/Kg 4.845.6 ***ND 50 45.4 25.0Silver 75 - 1257/16/2006mg/Kg 2.790.7ND 50 37.5 25.0Thallium 75 - 1257/16/2006mg/Kg 3.175.0 ***67.4 50 114 25.0Vanadium 75 - 1257/16/2006mg/Kg 0.092.265.6 50 111 25.0Zinc 75 - 1257/16/2006

***All MS/MSD recoveries that do not fall within the control limit are out due to the nature of the sample matrix. The batch was accepted by the LCS/LCSD recoveries.mg/Kg 8.390.8




On July 12, 2006, samples were received under chain of custody for analysis.

TestMatrix

Novato, CA 94947

Jim Dunn

Comments




Issued: 07/19/2006

P.O. Number: 285.002.01.005


Liquid EPA 7470A Dissolved Mercury for Water and Groundwater / EPA 245.1 Dissolved Mercury for WastewaterDissolved Metals by ICP: EPA 3005A / EPA 6010B for Groundwater and Water - EPA 200.7 for WastewaterChromium-VI: EPA 7196A for Water and Groundwater / Std. Methods (18th Ed.) 3500-Cr-D for WastewaterTPH-Extractable: EPA 3510C / EPA 8015BVOCs: EPA 5030C / EPA 8260B for Groundwater and Water - EPA 624 for WastewaterTPH-Purgeable: GC/MS


Sincerely,







P.O. Number: 285.002.01.005


Attn: Jim Dunn




Lab # : 50355-001 Sample ID: 06UST-01-GW Matrix: Liquid Sample Date: 7/11/2006 1:45 PM


1,1,1,2-Tetrachloroethane ND g/L0.501.0 WM10607177/18/2006N/AN/A1,1,1-Trichloroethane ND g/L0.501.0 WM10607177/18/2006N/AN/A1,1,2,2-Tetrachloroethane ND g/L0.501.0 WM10607177/18/2006N/AN/A1,1,2-Trichloroethane ND g/L0.501.0 WM10607177/18/2006N/AN/A1,1-Dichloroethane ND g/L0.501.0 WM10607177/18/2006N/AN/A1,1-Dichloroethene ND g/L0.501.0 WM10607177/18/2006N/AN/A1,1-Dichloropropene ND g/L0.501.0 WM10607177/18/2006N/AN/A1,2,3-Trichlorobenzene ND g/L5.01.0 WM10607177/18/2006N/AN/A1,2,3-Trichloropropane ND g/L0.501.0 WM10607177/18/2006N/AN/A1,2,4-Trichlorobenzene ND g/L5.01.0 WM10607177/18/2006N/AN/A1,2,4-Trimethylbenzene ND g/L5.01.0 WM10607177/18/2006N/AN/A1,2-Dibromo-3-Chloropropane ND g/L5.01.0 WM10607177/18/2006N/AN/A1,2-Dibromoethane (EDB) ND g/L0.501.0 WM10607177/18/2006N/AN/A1,2-Dichlorobenzene ND g/L0.501.0 WM10607177/18/2006N/AN/A1,2-Dichloroethane ND g/L0.501.0 WM10607177/18/2006N/AN/A1,2-Dichloropropane ND g/L0.501.0 WM10607177/18/2006N/AN/A1,3,5-Trimethylbenzene ND g/L5.01.0 WM10607177/18/2006N/AN/A1,3-Dichlorobenzene ND g/L0.501.0 WM10607177/18/2006N/AN/A1,3-Dichloropropane ND g/L0.501.0 WM10607177/18/2006N/AN/A1,4-Dichlorobenzene ND g/L0.501.0 WM10607177/18/2006N/AN/A1,4-Dioxane ND g/L501.0 WM10607177/18/2006N/AN/A2,2-Dichloropropane ND g/L0.501.0 WM10607177/18/2006N/AN/A2-Butanone (MEK) ND g/L201.0 WM10607177/18/2006N/AN/A2-Chloroethyl-vinyl Ether ND g/L5.01.0 WM10607177/18/2006N/AN/A2-Chlorotoluene ND g/L5.01.0 WM10607177/18/2006N/AN/A2-Hexanone ND g/L201.0 WM10607177/18/2006N/AN/A4-Chlorotoluene ND g/L5.01.0 WM10607177/18/2006N/AN/A4-Methyl-2-Pentanone(MIBK) ND g/L201.0 WM10607177/18/2006N/AN/AAcetone ND g/L201.0 WM10607177/18/2006N/AN/AAcetonitrile ND g/L5.01.0 WM10607177/18/2006N/AN/AAcrolein ND g/L5.01.0 WM10607177/18/2006N/AN/AAcrylonitrile ND g/L5.01.0 WM10607177/18/2006N/AN/ABenzene ND g/L0.501.0 WM10607177/18/2006N/AN/ABenzyl Chloride ND g/L5.01.0 WM10607177/18/2006N/AN/ABromobenzene ND g/L0.501.0 WM10607177/18/2006N/AN/ABromochloromethane ND g/L0.501.0 WM10607177/18/2006N/AN/ABromodichloromethane ND g/L0.501.0 WM10607177/18/2006N/AN/ABromoform ND g/L0.501.0 WM10607177/18/2006N/AN/ABromomethane ND g/L0.501.0 WM10607177/18/2006N/AN/ACarbon Disulfide 1.4 g/L0.501.0 WM10607177/18/2006N/AN/ACarbon Tetrachloride ND g/L0.501.0 WM10607177/18/2006N/AN/AChlorobenzene ND g/L0.501.0 WM10607177/18/2006N/AN/AChloroethane ND g/L0.501.0 WM10607177/18/2006N/AN/AChloroform ND g/L0.501.0 WM10607177/18/2006N/AN/AChloromethane ND g/L0.501.0 WM10607177/18/2006N/AN/A






P.O. Number: 285.002.01.005


Attn: Jim Dunn






cis-1,2-Dichloroethene ND g/L0.501.0 WM10607177/18/2006N/AN/Acis-1,3-Dichloropropene ND g/L0.501.0 WM10607177/18/2006N/AN/ACyclohexanone ND g/L201.0 WM10607177/18/2006N/AN/ADibromochloromethane ND g/L0.501.0 WM10607177/18/2006N/AN/ADibromomethane ND g/L0.501.0 WM10607177/18/2006N/AN/ADichlorodifluoromethane ND g/L0.501.0 WM10607177/18/2006N/AN/ADiisopropyl Ether ND g/L5.01.0 WM10607177/18/2006N/AN/AEthyl Benzene ND g/L0.501.0 WM10607177/18/2006N/AN/AFreon 113 ND g/L5.01.0 WM10607177/18/2006N/AN/AHexachlorobutadiene ND g/L5.01.0 WM10607177/18/2006N/AN/AIodomethane ND g/L5.01.0 WM10607177/18/2006N/AN/AIsopropanol ND g/L201.0 WM10607177/18/2006N/AN/AIsopropylbenzene ND g/L1.01.0 WM10607177/18/2006N/AN/AMethyl-t-butyl Ether 81 g/L1.01.0 WM10607177/18/2006N/AN/AMethylene Chloride ND g/L201.0 WM10607177/18/2006N/AN/An-Butylbenzene ND g/L5.01.0 WM10607177/18/2006N/AN/An-Propylbenzene ND g/L5.01.0 WM10607177/18/2006N/AN/ANaphthalene ND g/L5.01.0 WM10607177/18/2006N/AN/Ap-Isopropyltoluene ND g/L5.01.0 WM10607177/18/2006N/AN/APentachloroethane ND g/L0.501.0 WM10607177/18/2006N/AN/Asec-Butylbenzene ND g/L5.01.0 WM10607177/18/2006N/AN/AStyrene ND g/L0.501.0 WM10607177/18/2006N/AN/Atert-Amyl Methyl Ether ND g/L5.01.0 WM10607177/18/2006N/AN/Atert-Butanol (TBA) ND g/L101.0 WM10607177/18/2006N/AN/Atert-Butyl Ethyl Ether ND g/L5.01.0 WM10607177/18/2006N/AN/Atert-Butylbenzene ND g/L5.01.0 WM10607177/18/2006N/AN/ATetrachloroethene ND g/L0.501.0 WM10607177/18/2006N/AN/ATetrahydrofuran ND g/L201.0 WM10607177/18/2006N/AN/AToluene 0.54 g/L0.501.0 WM10607177/18/2006N/AN/Atrans-1,2-Dichloroethene ND g/L0.501.0 WM10607177/18/2006N/AN/Atrans-1,3-Dichloropropene ND g/L0.501.0 WM10607177/18/2006N/AN/Atrans-1,4-Dichloro-2-butene ND g/L1.01.0 WM10607177/18/2006N/AN/ATrichloroethene ND g/L0.501.0 WM10607177/18/2006N/AN/ATrichlorofluoromethane ND g/L0.501.0 WM10607177/18/2006N/AN/AVinyl Acetate ND g/L5.01.0 WM10607177/18/2006N/AN/AVinyl Chloride ND g/L0.501.0 WM10607177/18/2006N/AN/AXylenes, Total ND g/L0.501.0 WM10607177/18/2006N/AN/A


Analyzed by: XBianSurrogate Surrogate Recovery Control Limits (%)4-Bromofluorobenzene 96.5 60 130-Dibromofluoromethane 99.3 60 130-Toluene-d8 99.1 60 130-






P.O. Number: 285.002.01.005


Attn: Jim Dunn






TPH as Gasoline 83 g/L251.0 WM10607177/18/2006N/AN/A


Analyzed by: XBianSurrogate Surrogate Recovery Control Limits (%)4-Bromofluorobenzene 93.7 60 130-Dibromofluoromethane 107 60 130-Toluene-d8 94.6 60 130-










P.O. Number: 285.002.01.005


Attn: Jim Dunn







Reviewed by: jisiderio







P.O. Number: 285.002.01.005


Attn: Jim Dunn












P.O. Number: 285.002.01.005


Attn: Jim Dunn





Parameter Result UnitsDetection LimitD/P-F QC BatchQual Prep Date Analysis DatePrep BatchEPA 7470A Dissolved Mercury for Water and Groundwater / EPA 245.1 Dissolved Mercury for Wastewater

Mercury, Dissolved ND mg/L0.00021.0 WHGDISS0607137/13/2006WHGDISS0607137/13/2006

Reviewed by: HDINH


Parameter Result UnitsDetection LimitD/P-F QC BatchQual Prep Date Analysis DatePrep BatchDissolved Metals by ICP: EPA 3005A / EPA 6010B for Groundwater and Water - EPA 200.7 for Wastewater

Antimony ND mg/L0.0101.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Arsenic ND mg/L0.0101.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Barium ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Beryllium ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Cadmium ND mg/L0.00201.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Chromium ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Cobalt ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Copper ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Lead ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Molybdenum ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Nickel ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Selenium ND mg/L0.0201.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Silver ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Thallium ND mg/L0.0201.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Vanadium ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Zinc ND mg/L0.0101.0 WM060717DISS7/18/2006WM060717DISS7/17/2006

Reviewed by: HDINH

Analyzed by: Equeja














P.O. Number: 285.002.01.005


Attn: Jim Dunn




Lab # : 50355-003 Sample ID: Trip-1 Matrix: Liquid Sample Date: 7/11/2006 2:35 PM










P.O. Number: 285.002.01.005


Attn: Jim Dunn












P.O. Number: 285.002.01.005


Attn: Jim Dunn







Reviewed by: HDINH



Antimony ND mg/L0.0101.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Arsenic ND mg/L0.0101.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Barium ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Beryllium ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Cadmium ND mg/L0.00201.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Chromium ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Cobalt ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Copper ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Lead ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Molybdenum ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Nickel ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Selenium ND mg/L0.0201.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Silver ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Thallium ND mg/L0.0201.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Vanadium ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Zinc 0.010 mg/L0.0101.0 WM060717DISS7/18/2006WM060717DISS7/17/2006

Reviewed by: HDINH

Analyzed by: Equeja














P.O. Number: 285.002.01.005


Attn: Jim Dunn




Lab # : 50355-004 Sample ID: 06QC-05-GW Matrix: Liquid Sample Date: 7/11/2006 3:40 PM










P.O. Number: 285.002.01.005


Attn: Jim Dunn












P.O. Number: 285.002.01.005


Attn: Jim Dunn






cis-1,2-Dichloroethene ND g/L0.501.0 WM10607177/18/2006N/AN/Acis-1,3-Dichloropropene ND g/L0.501.0 WM10607177/18/2006N/AN/ACyclohexanone ND g/L201.0 WM10607177/18/2006N/AN/ADibromochloromethane ND g/L0.501.0 WM10607177/18/2006N/AN/ADibromomethane ND g/L0.501.0 WM10607177/18/2006N/AN/ADichlorodifluoromethane ND g/L0.501.0 WM10607177/18/2006N/AN/ADiisopropyl Ether ND g/L5.01.0 WM10607177/18/2006N/AN/AEthyl Benzene ND g/L0.501.0 WM10607177/18/2006N/AN/AFreon 113 ND g/L5.01.0 WM10607177/18/2006N/AN/AHexachlorobutadiene ND g/L5.01.0 WM10607177/18/2006N/AN/AIodomethane ND g/L5.01.0 WM10607177/18/2006N/AN/AIsopropanol ND g/L201.0 WM10607177/18/2006N/AN/AIsopropylbenzene ND g/L1.01.0 WM10607177/18/2006N/AN/AMethyl-t-butyl Ether 8.4 g/L1.01.0 WM10607177/18/2006N/AN/AMethylene Chloride ND g/L201.0 WM10607177/18/2006N/AN/An-Butylbenzene ND g/L5.01.0 WM10607177/18/2006N/AN/An-Propylbenzene ND g/L5.01.0 WM10607177/18/2006N/AN/ANaphthalene ND g/L5.01.0 WM10607177/18/2006N/AN/Ap-Isopropyltoluene ND g/L5.01.0 WM10607177/18/2006N/AN/APentachloroethane ND g/L0.501.0 WM10607177/18/2006N/AN/Asec-Butylbenzene ND g/L5.01.0 WM10607177/18/2006N/AN/AStyrene ND g/L0.501.0 WM10607177/18/2006N/AN/Atert-Amyl Methyl Ether ND g/L5.01.0 WM10607177/18/2006N/AN/Atert-Butanol (TBA) ND g/L101.0 WM10607177/18/2006N/AN/Atert-Butyl Ethyl Ether ND g/L5.01.0 WM10607177/18/2006N/AN/Atert-Butylbenzene ND g/L5.01.0 WM10607177/18/2006N/AN/ATetrachloroethene ND g/L0.501.0 WM10607177/18/2006N/AN/ATetrahydrofuran ND g/L201.0 WM10607177/18/2006N/AN/AToluene 0.70 g/L0.501.0 WM10607177/18/2006N/AN/Atrans-1,2-Dichloroethene ND g/L0.501.0 WM10607177/18/2006N/AN/Atrans-1,3-Dichloropropene ND g/L0.501.0 WM10607177/18/2006N/AN/Atrans-1,4-Dichloro-2-butene ND g/L1.01.0 WM10607177/18/2006N/AN/ATrichloroethene ND g/L0.501.0 WM10607177/18/2006N/AN/ATrichlorofluoromethane ND g/L0.501.0 WM10607177/18/2006N/AN/AVinyl Acetate ND g/L5.01.0 WM10607177/18/2006N/AN/AVinyl Chloride ND g/L0.501.0 WM10607177/18/2006N/AN/AXylenes, Total ND g/L0.501.0 WM10607177/18/2006N/AN/A


Analyzed by: XBianSurrogate Surrogate Recovery Control Limits (%)4-Bromofluorobenzene 109 60 130-Dibromofluoromethane 90.5 60 130-Toluene-d8 96.2 60 130-






P.O. Number: 285.002.01.005


Attn: Jim Dunn







Reviewed by: HDINH



Antimony ND mg/L0.0101.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Arsenic 0.011 mg/L0.0101.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Barium 0.26 mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Beryllium ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Cadmium ND mg/L0.00201.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Chromium ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Cobalt 0.0060 mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Copper 0.15 mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Lead 0.0080 mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Molybdenum 0.037 mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Nickel 0.38 mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Selenium ND mg/L0.0201.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Silver ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Thallium ND mg/L0.0201.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Vanadium 0.0050 mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Zinc ND mg/L0.0101.0 WM060717DISS7/18/2006WM060717DISS7/17/2006

Reviewed by: HDINH

Analyzed by: Equeja














P.O. Number: 285.002.01.005


Attn: Jim Dunn














P.O. Number: 285.002.01.005


Attn: Jim Dunn






cis-1,2-Dichloroethene ND g/L0.501.0 WM10607177/18/2006N/AN/Acis-1,3-Dichloropropene ND g/L0.501.0 WM10607177/18/2006N/AN/ACyclohexanone ND g/L201.0 WM10607177/18/2006N/AN/ADibromochloromethane ND g/L0.501.0 WM10607177/18/2006N/AN/ADibromomethane ND g/L0.501.0 WM10607177/18/2006N/AN/ADichlorodifluoromethane ND g/L0.501.0 WM10607177/18/2006N/AN/ADiisopropyl Ether ND g/L5.01.0 WM10607177/18/2006N/AN/AEthyl Benzene ND g/L0.501.0 WM10607177/18/2006N/AN/AFreon 113 ND g/L5.01.0 WM10607177/18/2006N/AN/AHexachlorobutadiene ND g/L5.01.0 WM10607177/18/2006N/AN/AIodomethane ND g/L5.01.0 WM10607177/18/2006N/AN/AIsopropanol ND g/L201.0 WM10607177/18/2006N/AN/AIsopropylbenzene ND g/L1.01.0 WM10607177/18/2006N/AN/AMethyl-t-butyl Ether 8.7 g/L1.01.0 WM10607177/18/2006N/AN/AMethylene Chloride ND g/L201.0 WM10607177/18/2006N/AN/An-Butylbenzene ND g/L5.01.0 WM10607177/18/2006N/AN/An-Propylbenzene ND g/L5.01.0 WM10607177/18/2006N/AN/ANaphthalene ND g/L5.01.0 WM10607177/18/2006N/AN/Ap-Isopropyltoluene ND g/L5.01.0 WM10607177/18/2006N/AN/APentachloroethane ND g/L0.501.0 WM10607177/18/2006N/AN/Asec-Butylbenzene ND g/L5.01.0 WM10607177/18/2006N/AN/AStyrene ND g/L0.501.0 WM10607177/18/2006N/AN/Atert-Amyl Methyl Ether ND g/L5.01.0 WM10607177/18/2006N/AN/Atert-Butanol (TBA) ND g/L101.0 WM10607177/18/2006N/AN/Atert-Butyl Ethyl Ether ND g/L5.01.0 WM10607177/18/2006N/AN/Atert-Butylbenzene ND g/L5.01.0 WM10607177/18/2006N/AN/ATetrachloroethene ND g/L0.501.0 WM10607177/18/2006N/AN/ATetrahydrofuran ND g/L201.0 WM10607177/18/2006N/AN/AToluene ND g/L0.501.0 WM10607177/18/2006N/AN/Atrans-1,2-Dichloroethene ND g/L0.501.0 WM10607177/18/2006N/AN/Atrans-1,3-Dichloropropene ND g/L0.501.0 WM10607177/18/2006N/AN/Atrans-1,4-Dichloro-2-butene ND g/L1.01.0 WM10607177/18/2006N/AN/ATrichloroethene ND g/L0.501.0 WM10607177/18/2006N/AN/ATrichlorofluoromethane ND g/L0.501.0 WM10607177/18/2006N/AN/AVinyl Acetate ND g/L5.01.0 WM10607177/18/2006N/AN/AVinyl Chloride ND g/L0.501.0 WM10607177/18/2006N/AN/AXylenes, Total ND g/L0.501.0 WM10607177/18/2006N/AN/A








P.O. Number: 285.002.01.005


Attn: Jim Dunn







Reviewed by: HDINH



Antimony ND mg/L0.0101.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Arsenic 0.016 mg/L0.0101.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Barium 0.15 mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Beryllium ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Cadmium ND mg/L0.00201.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Chromium ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Cobalt 0.0080 mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Copper 0.26 mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Lead 0.0070 mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Molybdenum 0.051 mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Nickel 0.50 mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Selenium ND mg/L0.0201.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Silver ND mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Thallium ND mg/L0.0201.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Vanadium 0.012 mg/L0.00501.0 WM060717DISS7/18/2006WM060717DISS7/17/2006Zinc ND mg/L0.0101.0 WM060717DISS7/18/2006WM060717DISS7/17/2006

Reviewed by: HDINH

Analyzed by: Equeja















Units<0.50 20 17.31,1-Dichloroethene 70 - 13086.5g/L<0.50 20 20.8Benzene 70 - 130104g/L<0.50 20 21.0Chlorobenzene 70 - 130105g/L<1.0 20 16.2Methyl-t-butyl Ether 70 - 13081.0g/L

<0.50 20 19.8Toluene 70 - 13099.0g/L<0.50 20 20.4Trichloroethene 70 - 130102g/L



RPD RPD LimitsUnits<0.50 20 17.1 25.01,1-Dichloroethene 70 - 1301.285.5g/L<0.50 20 20.3 25.0Benzene 70 - 1302.4102g/L<0.50 20 20.5 25.0Chlorobenzene 70 - 1302.4102g/L<1.0 20 15.6 25.0Methyl-t-butyl Ether 70 - 1303.878.0g/L

<0.50 20 18.9 25.0Toluene 70 - 1304.794.5g/L<0.50 20 20.2 25.0Trichloroethene 70 - 1300.99101g/L








RPD RPD LimitsUnits<25 120 127 25.0TPH as Gasoline 65 - 13513102g/L




Validated by: ECunniffe - 07/18/06QC/Prep Batch ID: WD060717AQC/Prep Date: 7/17/2006Parameter Result DF UnitsPQLR




Reviewed by: ECunniffe - 07/18/06QC Batch ID: WD060717AQC/Prep Date: 7/17/2006






RPD RPD LimitsUnits<50 1000 661 25.0TPH as Diesel 40 - 1381766.1g/L<200 1000 674 25.0TPH as Motor Oil 40 - 1385.667.4g/L




Reviewed by: HDINH - 07/13/06QC Batch ID: WHGDISS060713QC/Prep Date: 7/13/2006

LCS / LCSD - Liquid - EPA 7470A Dissolved Mercury for Water and Groundwater / EPA 245.1 Dissolved Mercury for Wastewater


Units<0.0002 0.0020 0.00203Mercury, Dissolved 75 - 125102mg/L


RPD RPD LimitsUnits<0.0002 0.0020 0.00201 25.0Mercury, Dissolved 75 - 1250.99100mg/L

Reviewed by: HDINH - 07/13/06QC/Prep Batch ID: WHGDISS060713QC/Prep Date: 7/13/2006

MS / MSD - Liquid - EPA 7470A Dissolved Mercury for Water and Groundwater / EPA 245.1 Dissolved Mercury for Wastewater


Spike Amount


Recovery Limits

AnalysisDate


ND 0.0040 0.00402Mercury, Dissolved 75 - 1257/13/2006mg/L 100


Spike Amount


Recovery Limits

AnalysisDate


RPD RPD Limits

MSD

ND 0.0040 0.00388 25.0Mercury, Dissolved 75 - 1257/13/2006mg/L 3.597.0



Reviewed by: HDINH - 07/18/06QC Batch ID: WM060717DISSQC/Prep Date: 7/17/2006

LCS / LCSD - Liquid - Dissolved Metals by ICP: EPA 3005A / EPA 6010B for Groundwater and Water - EPA 200.7 for Wastewater


Units<0.010 0.50 0.531Antimony 75 - 125106mg/L<0.010 0.50 0.505Arsenic 75 - 125101mg/L

<0.0050 0.50 0.503Barium 75 - 125101mg/L<0.0050 0.50 0.496Beryllium 75 - 12599.2mg/L<0.0020 0.50 0.500Cadmium 75 - 125100mg/L<0.0050 0.50 0.507Chromium 75 - 125101mg/L<0.0050 0.50 0.519Cobalt 75 - 125104mg/L<0.0050 0.50 0.514Copper 75 - 125103mg/L<0.050 0.50 0.523Iron 75 - 125105mg/L

<0.0050 0.50 0.523Lead 75 - 125105mg/L<0.0020 0.50 0.521Manganese 75 - 125104mg/L<0.0050 0.50 0.517Molybdenum 75 - 125103mg/L<0.0050 0.50 0.518Nickel 75 - 125104mg/L<0.020 0.50 0.479Selenium 75 - 12595.8mg/L

<0.0050 0.50 0.510Silver 75 - 125102mg/L<0.020 0.50 0.477Thallium 75 - 12595.4mg/L

<0.0050 0.50 0.515Vanadium 75 - 125103mg/L<0.010 0.50 0.509Zinc 75 - 125102mg/L


RPD RPD LimitsUnits<0.010 0.50 0.526 25.0Antimony 75 - 1250.95105mg/L<0.010 0.50 0.501 25.0Arsenic 75 - 1250.80100mg/L

<0.0050 0.50 0.493 25.0Barium 75 - 1252.098.6mg/L<0.0050 0.50 0.486 25.0Beryllium 75 - 1252.097.2mg/L<0.0020 0.50 0.494 25.0Cadmium 75 - 1251.298.8mg/L<0.0050 0.50 0.498 25.0Chromium 75 - 1251.899.6mg/L<0.0050 0.50 0.513 25.0Cobalt 75 - 1251.2103mg/L<0.0050 0.50 0.506 25.0Copper 75 - 1251.6101mg/L<0.050 0.50 0.504 25.0Iron 75 - 1253.7101mg/L

<0.0050 0.50 0.513 25.0Lead 75 - 1251.9103mg/L<0.0020 0.50 0.512 25.0Manganese 75 - 1251.7102mg/L<0.0050 0.50 0.508 25.0Molybdenum 75 - 1251.8102mg/L<0.0050 0.50 0.508 25.0Nickel 75 - 1251.9102mg/L<0.020 0.50 0.478 25.0Selenium 75 - 1250.2195.6mg/L

<0.0050 0.50 0.506 25.0Silver 75 - 1250.79101mg/L<0.020 0.50 0.473 25.0Thallium 75 - 1250.8494.6mg/L

<0.0050 0.50 0.508 25.0Vanadium 75 - 1251.4102mg/L<0.010 0.50 0.501 25.0Zinc 75 - 1251.6100mg/L



Reviewed by: jisiderio - 07/12/06QC Batch ID: WCR6060712QC Batch ID Analysis Date: 7/12/2006

LCS / LCSD - Liquid - Chromium-VI: EPA 7196A for Water and Groundwater / Std. Methods (18th Ed.) 3500-Cr-D for Wastewater


Units<0.010 0.10 0.0981Chromium (VI) 75 - 12598.1mg/L




MS / MSD - Liquid - Chromium-VI: EPA 7196A for Water and Groundwater / Std. Methods (18th Ed.) 3500-Cr-D for Wastewater


Spike Amount


Recovery Limits

AnalysisDate


ND 0.10 0.0915Chromium (VI) 75 - 1257/12/2006mg/L 91.5


Spike Amount


Recovery Limits

AnalysisDate


RPD RPD Limits

MSD

ND 0.10 0.0964 25.0Chromium (VI) 75 - 1257/12/2006mg/L 5.296.4


Entech AnalyticalLabs,Inc.3334 Victor Court,Santa Clara,CA 95054 Phone:(408)588-0200 Fax:(408)588-0201

PES Environm ental,Inc.

1682NovatoBoulevard,Suite100

On July13,2006,samples werereceived underchainofcustody foranalysis.

Test/Com m entsM atrix

Novato,CA 94947

Jim Dunn

CertificateofAnalysis-FinalReport

Lab CertificateNum ber: 50376

ProjectNam e: Baxter

ProjectNum ber: 285.002.01

Issued: 07/21/2006

P.O .Num ber: 285.002.01.005

Entech analyzes samples "as received" unless otherwise noted.The followingresultsareincluded:

Liquid Chrom ium VI:EPA 7196A forW aterand Groundwater/Std.M ethods (18thEd.)3500-Cr-D forW astewater

Dissolved M etalsby ICP:EPA 3005A /EPA 6010B forGroundwaterand W ater - EPA 200.7forW astewater

EPA 7470A Dissolved M ercuryforW aterand Groundwater / EPA 245.1Dissolved M ercuryforW astewater

EPA 7470A M ercuryforW aterand Groundwater / EPA 245.1M ercuryforW astewater

TPH-Extractable:EPA 3510C /EPA 8015B

TPH-Purgeable:GC/M S

VOCs:EPA 5030C /EPA 8260B forGroundwaterand W ater - EPA 624forW astewater

Entech AnalyticalLabs,Inc.iscertified forenvironmentalanalyses by the StateofCalifornia(#2346).Ifyou have any questions regarding thisreport,please callus at408-588-0200ext.225.

Sincerely,

LaurieGlantz-M urphyLaboratoryDirector

Environm entalAnalysis Since 1983

Original signed by Laurie Glantz-Murphy

PES Environm ental,Inc.1682NovatoBoulevard,Suite100Novato,CA 94947

CertificateofAnalysis-DataReport

Entech AnalyticalLabs,Inc. __3334 Victor Court,Santa Clara,CA 95054 Phone:(408)588-0200 Fax:(408)588-0201

P.O.Number: 285.002.01.005

SampleCollected by: Client

Attn: Jim Dunn

ProjectName: Baxter


ProjectNumber: 285.002.01

Lab #: 50376-001 Sam pleID: 06QC-12-GW M atrix: Liquid Sam pleDate: 7/12/2006 2:30PM

Param eter Result UnitsDetection Lim itD/P-F Q C BatchQ ual Prep Date AnalysisDatePrep Batch

Chrom ium VI:EPA 7196A for W aterand G roundwater/Std.M ethods (18th Ed.)3500-Cr-D for W astewater

Chrom ium (VI) ND mg/L0.0101.0 W CR60607137/13/2006N/AN/A

Reviewed by:JISIDERIO

Analyzed by:Rlazaro

D/P-F = Dilution and/orPrep Factorincludes sam plevolum e adjustm ents.

ND = NotDetected atorabove the Detection Lim it.7/21/20062:29:48PM -dbaQual= DataQualifier

Detection Lim it= Detection Lim itforReporting.




P.O.Number: 285.002.01.005


Attn: Jim Dunn

ProjectName: Baxter





VO Cs:EPA 5030C /EPA 8260B for Groundwaterand W ater - EPA 624for W astewater

1,1,1,2-Tetrachloroethane ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

1,1,1-Trichloroethane ND µg/L0.501.0 W M 10607177/17/2006N/AN/A



1,1-Dichloroethane ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

1,1-Dichloroethene ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

1,1-Dichloropropene ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

1,2,3-Trichlorobenzene ND µg/L5.01.0 W M 10607177/17/2006N/AN/A

1,2,3-Trichloropropane ND µg/L0.501.0 W M 10607177/17/2006N/AN/A


1,2,4-Trim ethylbenzene ND µg/L5.01.0 W M 10607177/17/2006N/AN/A

1,2-Dibrom o-3-Chloropropane ND µg/L5.01.0 W M 10607177/17/2006N/AN/A

1,2-Dibrom oethane (EDB) ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

1,2-Dichlorobenzene ND µg/L0.501.0 W M 10607177/17/2006N/AN/A


1,2-Dichloropropane ND µg/L0.501.0 W M 10607177/17/2006N/AN/A





1,4-Dioxane ND µg/L501.0 W M 10607177/17/2006N/AN/A


2-Butanone (M EK) ND µg/L201.0 W M 10607177/17/2006N/AN/A

2-Chloroethyl-vinylEther ND µg/L5.01.0 W M 10607177/17/2006N/AN/A

2-Chlorotoluene ND µg/L5.01.0 W M 10607177/17/2006N/AN/A

2-Hexanone ND µg/L201.0 W M 10607177/17/2006N/AN/A


4-M ethyl-2-Pentanone(M IBK) ND µg/L201.0 W M 10607177/17/2006N/AN/A

Acetone ND µg/L201.0 W M 10607177/17/2006N/AN/A

Acetonitrile ND µg/L5.01.0 W M 10607177/17/2006N/AN/A

Acrolein ND µg/L5.01.0 W M 10607177/17/2006N/AN/A

Acrylonitrile ND µg/L5.01.0 W M 10607177/17/2006N/AN/A

Benzene ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

BenzylChloride ND µg/L5.01.0 W M 10607177/17/2006N/AN/A

Brom obenzene ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

Brom ochlorom ethane ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

Brom odichlorom ethane ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

Brom oform ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

Brom om ethane ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

Carbon Disulfide ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

Carbon Tetrachloride ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

Chlorobenzene ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

Chloroethane ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

Chloroform ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

Chlorom ethane ND µg/L0.501.0 W M 10607177/17/2006N/AN/A







P.O.Number: 285.002.01.005


Attn: Jim Dunn

ProjectName: Baxter






cis-1,2-Dichloroethene ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

cis-1,3-Dichloropropene ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

Cyclohexanone ND µg/L201.0 W M 10607177/17/2006N/AN/A

Dibrom ochlorom ethane ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

Dibrom om ethane ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

Dichlorodifluorom ethane ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

DiisopropylEther ND µg/L5.01.0 W M 10607177/17/2006N/AN/A

EthylBenzene ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

Freon 113 ND µg/L5.01.0 W M 10607177/17/2006N/AN/A

Hexachlorobutadiene ND µg/L5.01.0 W M 10607177/17/2006N/AN/A

Iodom ethane ND µg/L5.01.0 W M 10607177/17/2006N/AN/A

Isopropanol ND µg/L201.0 W M 10607177/17/2006N/AN/A

Isopropylbenzene ND µg/L1.01.0 W M 10607177/17/2006N/AN/A

M ethyl-t-butylEther 1.3 µg/L1.01.0 W M 10607177/17/2006N/AN/A

M ethylene Chloride ND µg/L201.0 W M 10607177/17/2006N/AN/A

n-Butylbenzene ND µg/L5.01.0 W M 10607177/17/2006N/AN/A

n-Propylbenzene ND µg/L5.01.0 W M 10607177/17/2006N/AN/A

Naphthalene ND µg/L5.01.0 W M 10607177/17/2006N/AN/A

p-Isopropyltoluene ND µg/L5.01.0 W M 10607177/17/2006N/AN/A

Pentachloroethane ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

sec-Butylbenzene ND µg/L5.01.0 W M 10607177/17/2006N/AN/A

Styrene ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

tert-Am ylM ethylEther ND µg/L5.01.0 W M 10607177/17/2006N/AN/A

tert-Butanol(TBA) ND µg/L101.0 W M 10607177/17/2006N/AN/A

tert-ButylEthylEther ND µg/L5.01.0 W M 10607177/17/2006N/AN/A

tert-Butylbenzene ND µg/L5.01.0 W M 10607177/17/2006N/AN/A

Tetrachloroethene ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

Tetrahydrofuran ND µg/L201.0 W M 10607177/17/2006N/AN/A

Toluene ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

trans-1,2-Dichloroethene ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

trans-1,3-Dichloropropene ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

trans-1,4-Dichloro-2-butene ND µg/L1.01.0 W M 10607177/17/2006N/AN/A

Trichloroethene ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

Trichlorofluorom ethane ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

VinylAcetate ND µg/L5.01.0 W M 10607177/17/2006N/AN/A

VinylChloride ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

Xylenes,Total ND µg/L0.501.0 W M 10607177/17/2006N/AN/A

Reviewed by:M aiChiTu

Analyzed by:XBianSurrogate SurrogateRecovery ControlLim its(% )

4-Brom ofluorobenzene 100 60 130-

Dibrom ofluorom ethane 88.3 60 130-

Toluene-d8 97.6 60 130-







P.O.Number: 285.002.01.005


Attn: Jim Dunn

ProjectName: Baxter





EPA 7470A Dissolved M ercury for W aterand G roundwater / EPA 245.1Dissolved M ercury for W astewater

M ercury,Dissolved ND mg/L0.00021.0 W HGDISS0607197/19/2006W HGDISS060719B7/19/2006

Reviewed by:HDINH

Analyzed by:RW ipfler


Dissolved M etalsby ICP:EPA 3005A /EPA 6010B for G roundwaterand W ater - EPA 200.7for W astewater

Antim ony ND mg/L0.0101.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Arsenic 0.018 m g/L0.0101.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Barium 0.47 m g/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Beryllium ND mg/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Cadm ium ND mg/L0.00201.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Chrom ium 0.012 m g/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Cobalt 0.0090 m g/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Copper ND mg/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Lead 0.015 m g/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

M olybdenum 0.034 m g/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Nickel 0.065 m g/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Selenium ND mg/L0.0201.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Silver ND mg/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Thallium ND mg/L0.0201.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Vanadium ND mg/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Zinc ND mg/L0.0101.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Reviewed by:HDINH

Analyzed by:EQueja


TPH -Purgeable:G C/M S

TPH as Gasoline 120 µg/L251.0 W M 10607177/17/2006N/AN/A



4-Brom ofluorobenzene 97.3 60 130-


Toluene-d8 93.2 60 130-


TPH -Extractable:EPA 3510C /EPA 8015B

TPH as Diesel ND µg/L601.2 W D060717A7/20/2006W D060717A

800ppbhydrocarbons (C8-C38).No Dieselpatternpresent.

7/17/2006

Reviewed by:dba

Analyzed by:JHsiangSurrogate SurrogateRecovery ControlLim its(% )

o-Terphenyl 50.1 22 133-







P.O.Number: 285.002.01.005


Attn: Jim Dunn

ProjectName: Baxter



Lab #: 50376-002 Sam pleID: Trip-2 M atrix: Liquid Sam pleDate: 7/12/2006 3:00PM





Analyzed by:Rlazaro







P.O.Number: 285.002.01.005


Attn: Jim Dunn

ProjectName: Baxter

























































P.O.Number: 285.002.01.005


Attn: Jim Dunn

ProjectName: Baxter



















M ethyl-t-butylEther ND µg/L1.01.0 W M 10607177/17/2006N/AN/A




























Toluene-d8 93.3 60 130-







P.O.Number: 285.002.01.005


Attn: Jim Dunn

ProjectName: Baxter





EPA 7470A M ercury for W aterand G roundwater / EPA 245.1M ercury for W astewater

M ercury 0.0016 m g/L0.00021.0 W HG0607197/19/2006W HG0607197/19/2006

Reviewed by:HDINH





Arsenic ND mg/L0.0101.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Barium ND mg/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006



Chrom ium ND mg/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Cobalt ND mg/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006


Lead ND mg/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

M olybdenum ND mg/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Nickel ND mg/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006






Reviewed by:HDINH

Analyzed by:Equeja



TPH as Diesel ND µg/L531.1 W D060717A7/20/2006W D060717A7/17/2006

Reviewed by:ECunniffe






Entech AnalyticalLabs,Inc. _3334 Victor Court,Santa Clara,CA 95054 Phone:(408)588-0200 Fax:(408)588-0201

Validated by: ECunniffe -07/18/06Q C/Prep Batch ID: W D060717A

Q C/Prep Date: 7/17/2006

Param eter Result DF UnitsPQ LR

M ethod Blank - Liquid - TPH-Extractable:EPA 3510C /EPA 8015B

TPH as Diesel ND 1 µg/L50

Surrogatefor Blank % Recovery ControlLim its


M ethod Blank -dba -7/21/2006 2:30:38 PM


Validated by: M aiChiTu -07/18/06Q C Batch ID: W M 1060717

QC Batch Analysis Date: 7/17/2006


M ethod Blank - Liquid - VO Cs:EPA 5030C /EPA 8260B for Groundw ater and W ater - EPA 624 for W astew ater

1,1,1,2-Tetrachloroethane ND 1 µg/L0.50

1,1,1-Trichloroethane ND 1 µg/L0.50



1,1-Dichloroethane ND 1 µg/L0.50

1,1-Dichloroethene ND 1 µg/L0.50

1,1-Dichloropropene ND 1 µg/L0.50

1,2,3-Trichlorobenzene ND 1 µg/L5.0

1,2,3-Trichloropropane ND 1 µg/L0.50


1,2,4-Trim ethylbenzene ND 1 µg/L5.0

1,2-Dibrom o-3-Chloropropane ND 1 µg/L5.0

1,2-Dibrom oethane (EDB) ND 1 µg/L0.50

1,2-Dichlorobenzene ND 1 µg/L0.50


1,2-Dichloropropane ND 1 µg/L0.50





1,4-Dioxane ND 1 µg/L50


2-Butanone (M EK) ND 1 µg/L20

2-Chloroethyl-vinylEther ND 1 µg/L5.0

2-Chlorotoluene ND 1 µg/L5.0

2-Hexanone ND 1 µg/L20


4-M ethyl-2-Pentanone(M IBK) ND 1 µg/L20

Acetone ND 1 µg/L20

Acetonitrile ND 1 µg/L5.0

Acrolein ND 1 µg/L5.0

Acrylonitrile ND 1 µg/L5.0

Benzene ND 1 µg/L0.50

BenzylChloride ND 1 µg/L5.0

Brom obenzene ND 1 µg/L0.50

Brom ochlorom ethane ND 1 µg/L0.50

Brom odichlorom ethane ND 1 µg/L0.50

Brom oform ND 1 µg/L0.50

Brom om ethane ND 1 µg/L0.50

Carbon Disulfide ND 1 µg/L0.50

Carbon Tetrachloride ND 1 µg/L0.50

Chlorobenzene ND 1 µg/L0.50

Chloroethane ND 1 µg/L0.50

Chloroform ND 1 µg/L0.50

Chlorom ethane ND 1 µg/L0.50

cis-1,2-Dichloroethene ND 1 µg/L0.50

cis-1,3-Dichloropropene ND 1 µg/L0.50

Cyclohexanone ND 1 µg/L20

Dibrom ochlorom ethane ND 1 µg/L0.50

Dibrom om ethane ND 1 µg/L0.50







Dichlorodifluorom ethane ND 1 µg/L0.50

DiisopropylEther ND 1 µg/L5.0

EthylBenzene ND 1 µg/L0.50

Freon 113 ND 1 µg/L5.0

Hexachlorobutadiene ND 1 µg/L5.0

Iodom ethane ND 1 µg/L5.0

Isopropanol ND 1 µg/L20

Isopropylbenzene ND 1 µg/L1.0

M ethylene Chloride ND 1 µg/L20

M ethyl-t-butylEther ND 1 µg/L1.0

Naphthalene ND 1 µg/L5.0

n-Butylbenzene ND 1 µg/L5.0

n-Propylbenzene ND 1 µg/L5.0

Pentachloroethane ND 1 µg/L0.50

p-Isopropyltoluene ND 1 µg/L5.0

sec-Butylbenzene ND 1 µg/L5.0

Styrene ND 1 µg/L0.50

tert-Am ylM ethylEther ND 1 µg/L5.0

tert-Butanol(TBA) ND 1 µg/L10

tert-ButylEthylEther ND 1 µg/L5.0

tert-Butylbenzene ND 1 µg/L5.0

Tetrachloroethene ND 1 µg/L0.50

Tetrahydrofuran ND 1 µg/L20

Toluene ND 1 µg/L0.50

trans-1,2-Dichloroethene ND 1 µg/L0.50

trans-1,3-Dichloropropene ND 1 µg/L0.50

trans-1,4-Dichloro-2-butene ND 1 µg/L1.0

Trichloroethene ND 1 µg/L0.50

Trichlorofluorom ethane ND 1 µg/L0.50

VinylAcetate ND 1 µg/L5.0

VinylChloride ND 1 µg/L0.50

Xylenes,Total ND 1 µg/L0.50




Toluene-d8 95.5 70 125-




M ethod Blank - Liquid - TPH-Purgeable:GC/M S

TPH as G asoline ND 1 µg/L25




Toluene-d8 91.2 60 130-



Reviewed by: JISIDERIO -07/13/06Q C Batch ID: W CR6060713

QC Batch ID Analysis Date: 7/13/2006

LCS /LCSD - Liquid - Chrom ium VI:EPA 7196A for W ater and Groundw ater /Std.M ethods (18th Ed.)3500-Cr-D for W astew ater

Param eter M ethod Blank Spike Am t SpikeResult % Recovery Recovery Lim itsLCS

Units

<0.010 0.10 0.0975Chrom ium (VI) 75 -12597.5m g/L

Param eter M ethod Blank Spike Am t SpikeResult % Recovery Recovery Lim itsLCSD

RPD RPD Lim itsUnits

<0.010 0.10 0.0937 25.0Chrom ium (VI) 75 -1254.093.7m g/L

Laboratory ControlSam ple /Duplicate -dba -7/21/2006 2:30:43 PM


Reviewed by: ECunniffe -07/18/06Q C Batch ID: W D060717A


LCS /LCSD - Liquid - TPH-Extractable:EPA 3510C /EPA 8015B


Units

<50 1000 784TPH as Diesel 40 -13878.4µg/L

<200 1000 714TPH as M otorO il 40 -13871.4µg/L

Surrogate % Recovery ControlLim its




<50 1000 661 25.0TPH as Diesel 40 -1381766.1µg/L

<200 1000 674 25.0TPH as M otorO il 40 -1385.667.4µg/L





Reviewed by: HDINH -07/19/06Q C Batch ID: W HG 060719


LCS /LCSD - Liquid - EPA 7470A M ercury for W ater and Groundw ater / EPA 245.1 M ercury for W astew ater


Units

<0.0002 0.0020 0.00191M ercury 75 -12595.5m g/L



<0.0002 0.0020 0.00198 25.0M ercury 75 -1253.699.0m g/L



Reviewed by: HDINH -07/20/06Prep/Q C Batch ID: W HG DISS060719B /W HG DISS060719


LCS /LCSD - Liquid - EPA 7470A Dissolved M ercury for W ater and Groundw ater / EPA 245.1 Dissolved M ercury for W astew ater


Units

<0.0002 0.0020 0.00200M ercury,Dissolved 75 -125100m g/L



<0.0002 0.0020 0.00187 25.0M ercury,Dissolved 75 -1256.793.5m g/L



Reviewed by: HDINH -07/18/06Q C Batch ID: W M 060717DISS


LCS /LCSD - Liquid - Dissolved M etals by ICP:EPA 3005A /EPA 6010B for G roundw ater and W ater -EPA 200.7 for W astew ater


Units

<0.010 0.50 0.531Antim ony 75 -125106m g/L

<0.010 0.50 0.505Arsenic 75 -125101m g/L

<0.0050 0.50 0.503Barium 75 -125101m g/L

<0.0050 0.50 0.496Beryllium 75 -12599.2m g/L

<0.0020 0.50 0.500Cadm ium 75 -125100m g/L

<0.0050 0.50 0.507Chrom ium 75 -125101m g/L

<0.0050 0.50 0.519Cobalt 75 -125104m g/L

<0.0050 0.50 0.514Copper 75 -125103m g/L

<0.050 0.50 0.523Iron 75 -125105m g/L

<0.0050 0.50 0.523Lead 75 -125105m g/L

<0.0020 0.50 0.521M anganese 75 -125104m g/L

<0.0050 0.50 0.517M olybdenum 75 -125103m g/L

<0.0050 0.50 0.518Nickel 75 -125104m g/L

<0.020 0.50 0.479Selenium 75 -12595.8m g/L

<0.0050 0.50 0.510Silver 75 -125102m g/L

<0.020 0.50 0.477Thallium 75 -12595.4m g/L

<0.0050 0.50 0.515Vanadium 75 -125103m g/L

<0.010 0.50 0.509Zinc 75 -125102m g/L



<0.010 0.50 0.526 25.0Antim ony 75 -1250.95105m g/L

<0.010 0.50 0.501 25.0Arsenic 75 -1250.80100m g/L

<0.0050 0.50 0.493 25.0Barium 75 -1252.098.6m g/L

<0.0050 0.50 0.486 25.0Beryllium 75 -1252.097.2m g/L

<0.0020 0.50 0.494 25.0Cadm ium 75 -1251.298.8m g/L

<0.0050 0.50 0.498 25.0Chrom ium 75 -1251.899.6m g/L

<0.0050 0.50 0.513 25.0Cobalt 75 -1251.2103m g/L

<0.0050 0.50 0.506 25.0Copper 75 -1251.6101m g/L

<0.050 0.50 0.504 25.0Iron 75 -1253.7101m g/L

<0.0050 0.50 0.513 25.0Lead 75 -1251.9103m g/L

<0.0020 0.50 0.512 25.0M anganese 75 -1251.7102m g/L

<0.0050 0.50 0.508 25.0M olybdenum 75 -1251.8102m g/L

<0.0050 0.50 0.508 25.0Nickel 75 -1251.9102m g/L

<0.020 0.50 0.478 25.0Selenium 75 -1250.2195.6m g/L

<0.0050 0.50 0.506 25.0Silver 75 -1250.79101m g/L

<0.020 0.50 0.473 25.0Thallium 75 -1250.8494.6m g/L

<0.0050 0.50 0.508 25.0Vanadium 75 -1251.4102m g/L

<0.010 0.50 0.501 25.0Zinc 75 -1251.6100m g/L



Reviewed by: M aiChiTu -07/18/06Q C Batch ID: W M 1060717


LCS /LCSD - Liquid - VO Cs:EPA 5030C /EPA 8260B for Groundw ater and W ater - EPA 624 for W astew ater


Units

<0.50 20 17.31,1-Dichloroethene 70 -13086.5µg/L

<0.50 20 20.8Benzene 70 -130104µg/L

<0.50 20 21.0Chlorobenzene 70 -130105µg/L

<1.0 20 16.2M ethyl-t-butylEther 70 -13081.0µg/L

<0.50 20 19.8Toluene 70 -13099.0µg/L

<0.50 20 20.4Trichloroethene 70 -130102µg/L




Toluene-d8 98.5 60 130-



<0.50 20 17.1 25.01,1-Dichloroethene 70 -1301.285.5µg/L

<0.50 20 20.3 25.0Benzene 70 -1302.4102µg/L

<0.50 20 20.5 25.0Chlorobenzene 70 -1302.4102µg/L

<1.0 20 15.6 25.0M ethyl-t-butylEther 70 -1303.878.0µg/L

<0.50 20 18.9 25.0Toluene 70 -1304.794.5µg/L

<0.50 20 20.2 25.0Trichloroethene 70 -1300.99101µg/L




Toluene-d8 97.4 60 130-



LCS /LCSD - Liquid - TPH-Purgeable:GC/M S


Units

<25 120 112TPH as Gasoline 65 -13589.4µg/L




Toluene-d8 90.4 60 130-



<25 120 127 25.0TPH as Gasoline 65 -13513102µg/L




Toluene-d8 94.5 60 130-



Reviewed by: JISIDERIO -07/13/06Q C Batch ID: W CR6060713


M S /M SD - Liquid - Chrom ium VI:EPA 7196A for W ater and Groundw ater /Std.M ethods (18th Ed.)3500-Cr-Dfor W astew ater

Param eter

Sam pleResult

SpikeAm ount

SpikeResult Units % Recovery

Recovery Lim its

AnalysisDate

Sam ple Spiked: 50376-002M S

ND 0.10 0.0937Chrom ium (VI) 75 -1257/13/2006m g/L 93.7

Param eter

Sam pleResult

SpikeAm ount


Recovery Lim its

AnalysisDate

Sam ple Spiked: 50376-002

RPD RPD Lim its

M SD

ND 0.10 0.0943 25.0Chrom ium (VI) 75 -1257/13/2006m g/L 0.5794.3

M atrix Spike /M atrixSpike Duplicate -dba -7/21/2006 2:30:49 PM


Reviewed by: HDINH -07/20/06Q C/Prep Batch ID: W HG060719


M S /M SD - Liquid - EPA 7470A M ercury for W ater and Groundw ater / EPA 245.1 M ercury for W astew ater

Param eter

Sam pleResult

SpikeAm ount


Recovery Lim its

AnalysisDate


ND 0.0040 0.00380M ercury 75 -1257/19/2006m g/L 95.0

Param eter

Sam pleResult

SpikeAm ount


Recovery Lim its

AnalysisDate


RPD RPD Lim its

M SD

ND 0.0040 0.00442 25.0M ercury 75 -1257/19/2006m g/L 15110



Reviewed by: HDINH -07/20/06Q C/Prep Batch ID: W HGDISS060719B


M S /M SD - Liquid - EPA 7470A Dissolved M ercury for W ater and Groundw ater / EPA 245.1 Dissolved M ercury for W astew ater

Param eter

Sam pleResult

SpikeAm ount


Recovery Lim its

AnalysisDate


ND 0.0040 0.00398M ercury,Dissolved 75 -1257/20/2006m g/L 99.5

Param eter

Sam pleResult

SpikeAm ount


Recovery Lim its

AnalysisDate


RPD RPD Lim its

M SD

ND 0.0040 0.00399 25.0M ercury,Dissolved 75 -1257/20/2006m g/L 0.2599.8



Reviewed by: HDINH -07/18/06Q C/Prep Batch ID: W M 060717DISS


M S /M SD - Liquid - Dissolved M etals by ICP:EPA 3005A /EPA 6010B for G roundw ater and W ater - EPA 200.7 for W astew ater

Param eter

Sam pleResult

SpikeAm ount


Recovery Lim its

AnalysisDate


ND 0.50 0.550Antim ony 75 -1257/17/2006m g/L 110

ND 0.50 0.526Arsenic 75 -1257/17/2006m g/L 105

ND 0.50 0.508Barium 75 -1257/17/2006m g/L 102

ND 0.50 0.514Beryllium 75 -1257/17/2006m g/L 103

ND 0.50 0.511Cadm ium 75 -1257/17/2006m g/L 102

ND 0.50 0.521Chrom ium 75 -1257/17/2006m g/L 104

ND 0.50 0.532Cobalt 75 -1257/17/2006m g/L 106

ND 0.50 0.521Copper 75 -1257/17/2006m g/L 104

ND 0.50 0.537Lead 75 -1257/17/2006m g/L 107

ND 0.50 0.522M olybdenum 75 -1257/17/2006m g/L 104

ND 0.50 0.531Nickel 75 -1257/17/2006m g/L 106

ND 0.50 0.507Selenium 75 -1257/17/2006m g/L 101

ND 0.50 0.521Silver 75 -1257/17/2006m g/L 104

ND 0.50 0.490Thallium 75 -1257/17/2006m g/L 98.0

ND 0.50 0.524Vanadium 75 -1257/17/2006m g/L 105

0.0100 0.50 0.529Zinc 75 -1257/17/2006m g/L 104

Param eter

Sam pleResult

SpikeAm ount


Recovery Lim its

AnalysisDate


RPD RPD Lim its

M SD

ND 0.50 0.555 25.0Antim ony 75 -1257/17/2006m g/L 0.90111

ND 0.50 0.530 25.0Arsenic 75 -1257/17/2006m g/L 0.76106

ND 0.50 0.516 25.0Barium 75 -1257/17/2006m g/L 1.6103

ND 0.50 0.517 25.0Beryllium 75 -1257/17/2006m g/L 0.58103

ND 0.50 0.519 25.0Cadm ium 75 -1257/17/2006m g/L 1.6104

ND 0.50 0.525 25.0Chrom ium 75 -1257/17/2006m g/L 0.76105

ND 0.50 0.541 25.0Cobalt 75 -1257/17/2006m g/L 1.7108

ND 0.50 0.531 25.0Copper 75 -1257/17/2006m g/L 1.9106

ND 0.50 0.548 25.0Lead 75 -1257/17/2006m g/L 2.0110

ND 0.50 0.531 25.0M olybdenum 75 -1257/17/2006m g/L 1.7106

ND 0.50 0.537 25.0Nickel 75 -1257/17/2006m g/L 1.1107

ND 0.50 0.509 25.0Selenium 75 -1257/17/2006m g/L 0.39102

ND 0.50 0.529 25.0Silver 75 -1257/17/2006m g/L 1.5106

ND 0.50 0.507 25.0Thallium 75 -1257/17/2006m g/L 3.4101

ND 0.50 0.534 25.0Vanadium 75 -1257/17/2006m g/L 1.9107

0.0100 0.50 0.535 25.0Zinc 75 -1257/17/2006m g/L 1.1105


@@ PES Environmental, Inc. Engineering & Enuironmentai Services d

UBWATORY: G ~ { @ L . b( JOB NUMBER: 2 cj* A ufm. ( 3 / . , #f>g -

NAME I LOCATION: &&dt?fi,* ' PROJECT MANAGER: - 3-I .I 4

I /: /E?z~~,I DESIGNATION

CHAIN OF CUSTODY RECORD

SAMPLERS: f l ,5'df1", f f 53%

RECORDER.

1682 NOVATO BOULEVARD, SUTTE 100 NOVATO. CALIFORNIA 94947

(415) 899-1600 FAX (415) 899-1601

I ANALYSIS REQUESTED i

I METKOD OF SHIPMENT:

I t I WWITE-Laboratcfy COPY YELLOW-Pmjed Mca C w PINKqield or M T I Cow




On July14,2006,samples werereceived underchainofcustody foranalysis.


Novato,CA 94947

Jim Dunn





Issued: 07/20/2006


Liquid Chrom ium -VI:EPA 7196A forW aterand Groundwater/Std.M ethods (18thEd.)3500-Cr-D forW astewater

Dissolved M etalsby ICP:EPA 3005A /EPA 6010B forGroundwaterand W ater - EPA 200.7forW astewater

EPA 7470A Dissolved M ercuryforW aterand Groundwater / EPA 245.1Dissolved M ercuryforW astewater

TPH-Extractable:EPA 3510C /EPA 8015B

TPH-Purgeable:GC/M S

VOCs:EPA 5030C /EPA 8260B forGroundwaterand W ater - EPA 624forW astewater

Entech AnalyticalLabs,Inc.iscertified forenvironmentalanalyses by the StateofCalifornia(#2346).Ifyou have any questions regarding thisreport,please callus at408-588-0200ext.225.

Sincerely,








Attn: Jim Dunn

ProjectName: Baxter



Lab #: 50393-001 Sam pleID: 065C16GW M atrix: Liquid Sam pleDate: 7/13/2006 5:00PM


Chrom ium -VI:EPA 7196A for W aterand G roundwater/Std.M ethods (18th Ed.)3500-Cr-D for W astewater


Reviewed by:JIsiderio

Analyzed by:Rlazaro








Attn: Jim Dunn

ProjectName: Baxter


































Acetone 32 µg/L201.0 W M 10607187/18/2006N/AN/A











Carbon Disulfide 0.97 µg/L0.501.0 W M 10607187/18/2006N/AN/A













Attn: Jim Dunn

ProjectName: Baxter






































Trichloroethene 1.3 µg/L0.501.0 W M 10607187/18/2006N/AN/A








Dibrom ofluorom ethane 100 60 130-

Toluene-d8 99.2 60 130-








Attn: Jim Dunn

ProjectName: Baxter







Reviewed by:HDINH





Arsenic 0.018 m g/L0.0101.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Barium 0.18 m g/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006



Chrom ium 0.0080 m g/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Cobalt 0.036 m g/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006


Lead 0.014 m g/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

M olybdenum 0.020 m g/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Nickel 2.2 m g/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006




Vanadium 0.0080 m g/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006


Reviewed by:HDINH

Analyzed by:EQueja



TPH as Gasoline ND µg/L251.0 W M 10607187/18/2006N/AN/A





Toluene-d8 94.8 60 130-



TPH as Diesel ND µg/L501.0 W D060715A7/19/2006W D060715A

420ppbm otoroilrange organics. No Dieselpattern.

7/15/2006











Attn: Jim Dunn

ProjectName: Baxter


































Acetone 28 µg/L201.0 W M 10607187/18/2006N/AN/A











Carbon Disulfide 1.6 µg/L0.501.0 W M 10607187/18/2006N/AN/A













Attn: Jim Dunn

ProjectName: Baxter






































Trichloroethene 1.6 µg/L0.501.0 W M 10607187/18/2006N/AN/A









Toluene-d8 99.7 60 130-








Attn: Jim Dunn

ProjectName: Baxter











Toluene-d8 95.2 60 130-








Attn: Jim Dunn

ProjectName: Baxter



Lab #: 50393-003 Sam pleID: Equip3 M atrix: Liquid Sam pleDate: 7/13/2006 5:10PM


Chrom ium -VI:EPA 7196A for W aterand G roundwater/Std.M ethods (18th Ed.)3500-Cr-D for W astewater


Reviewed by:JIsiderio

Analyzed by:Rlazaro








Attn: Jim Dunn

ProjectName: Baxter










































Brom odichlorom ethane 1.2 µg/L0.501.0 W M 10607187/18/2006N/AN/A







Chloroform 24 µg/L0.501.0 W M 10607187/18/2006N/AN/A









Attn: Jim Dunn

ProjectName: Baxter















































Toluene-d8 97.7 60 130-








Attn: Jim Dunn

ProjectName: Baxter







Reviewed by:HDINH





Arsenic ND mg/L0.0101.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Barium ND mg/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006



Chrom ium ND mg/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Cobalt ND mg/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006


Lead ND mg/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

M olybdenum ND mg/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Nickel ND mg/L0.00501.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006





Zinc 0.010 m g/L0.0101.0 W M 060717DISS7/18/2006W M 060717DISS7/17/2006

Reviewed by:HDINH

Analyzed by:EQueja



TPH as Gasoline 25 µg/L251.0 W M 10607187/18/2006N/AN/A





Toluene-d8 93.3 60 130-



TPH as Diesel ND µg/L501.0 W D060715A7/19/2006W D060715A7/15/2006











Attn: Jim Dunn

ProjectName: Baxter


























































Attn: Jim Dunn

ProjectName: Baxter















































Toluene-d8 97.8 60 130-








Attn: Jim Dunn

ProjectName: Baxter











Toluene-d8 93.4 60 130-





Validated by: dba -07/17/06Q C/Prep Batch ID: W D060715A



M ethod Blank - Liquid - TPH-Extractable:EPA 3510C /EPA 8015B

TPH as Diesel ND 1 µg/L50



Q CReport-dba -7/20/2006 5:21:22 PM











1,1-Dichloroethene ND 1 µg/L0.50

1,1-Dichloropropene ND 1 µg/L0.50


1,2,3-Trichloropropane ND 1 µg/L0.50



1,2-Dibrom o-3-Chloropropane ND 1 µg/L5.0

1,2-Dibrom oethane (EDB) ND 1 µg/L0.50








1,4-Dioxane ND 1 µg/L50


2-Butanone (M EK) ND 1 µg/L20

2-Chloroethyl-vinylEther ND 1 µg/L5.0


2-Hexanone ND 1 µg/L20


4-M ethyl-2-Pentanone(M IBK) ND 1 µg/L20

Acetone ND 1 µg/L20

Acetonitrile ND 1 µg/L5.0

Acrolein ND 1 µg/L5.0

Acrylonitrile ND 1 µg/L5.0

Benzene ND 1 µg/L0.50

BenzylChloride ND 1 µg/L5.0

Brom obenzene ND 1 µg/L0.50

Brom ochlorom ethane ND 1 µg/L0.50

Brom odichlorom ethane ND 1 µg/L0.50

Brom oform ND 1 µg/L0.50

Brom om ethane ND 1 µg/L0.50

Carbon Disulfide ND 1 µg/L0.50

Carbon Tetrachloride ND 1 µg/L0.50

Chlorobenzene ND 1 µg/L0.50

Chloroethane ND 1 µg/L0.50

Chloroform ND 1 µg/L0.50

Chlorom ethane ND 1 µg/L0.50

cis-1,2-Dichloroethene ND 1 µg/L0.50

cis-1,3-Dichloropropene ND 1 µg/L0.50

Cyclohexanone ND 1 µg/L20

Dibrom ochlorom ethane ND 1 µg/L0.50

Q CReport-dba -7/20/2006 5:21:24 PM






Dibrom om ethane ND 1 µg/L0.50

Dichlorodifluorom ethane ND 1 µg/L0.50

DiisopropylEther ND 1 µg/L5.0

EthylBenzene ND 1 µg/L0.50

Freon 113 ND 1 µg/L5.0

Hexachlorobutadiene ND 1 µg/L5.0

Iodom ethane ND 1 µg/L5.0

Isopropanol ND 1 µg/L20

Isopropylbenzene ND 1 µg/L1.0

M ethylene Chloride ND 1 µg/L20

M ethyl-t-butylEther ND 1 µg/L1.0

Naphthalene ND 1 µg/L5.0

n-Butylbenzene ND 1 µg/L5.0

n-Propylbenzene ND 1 µg/L5.0

Pentachloroethane ND 1 µg/L0.50

p-Isopropyltoluene ND 1 µg/L5.0

sec-Butylbenzene ND 1 µg/L5.0

Styrene ND 1 µg/L0.50

tert-Am ylM ethylEther ND 1 µg/L5.0

tert-Butanol(TBA) ND 1 µg/L10

tert-ButylEthylEther ND 1 µg/L5.0

tert-Butylbenzene ND 1 µg/L5.0

Tetrachloroethene ND 1 µg/L0.50

Tetrahydrofuran ND 1 µg/L20

Toluene ND 1 µg/L0.50

trans-1,2-Dichloroethene ND 1 µg/L0.50

trans-1,3-Dichloropropene ND 1 µg/L0.50

trans-1,4-Dichloro-2-butene ND 1 µg/L1.0

Trichloroethene ND 1 µg/L0.50

Trichlorofluorom ethane ND 1 µg/L0.50

VinylAcetate ND 1 µg/L5.0

VinylChloride ND 1 µg/L0.50

Xylenes,Total ND 1 µg/L0.50




Toluene-d8 96.4 70 125-




M ethod Blank - Liquid - TPH-Purgeable:GC/M S

TPH as G asoline ND 1 µg/L25




Toluene-d8 92.1 60 130-

Q CReport-dba -7/20/2006 5:21:24 PM


Reviewed by: JIsiderio -07/14/06Q C Batch ID: W CR6060714


LCS /LCSD - Liquid - Chrom ium -VI:EPA 7196A for W ater and Groundw ater /Std.M ethods (18th Ed.)3500-Cr-D for W astew ater


Units

<0.010 0.10 0.0961Chrom ium (VI) 75 -12596.1m g/L



<0.010 0.10 0.100 25.0Chrom ium (VI) 75 -1254.3100m g/L

Q CReport-dba -7/20/2006 5:21:25 PM


Reviewed by: dba -07/17/06Q C Batch ID: W D060715A


LCS /LCSD - Liquid - TPH-Extractable:EPA 3510C /EPA 8015B


Units

<50 1000 536TPH as Diesel 40 -13853.6µg/L

<200 1000 677TPH as M otorO il 40 -13867.7µg/L





<50 1000 533 25.0TPH as Diesel 40 -1380.5653.3µg/L

<200 1000 699 25.0TPH as M otorO il 40 -1383.269.9µg/L



Q CReport-dba -7/20/2006 5:21:26 PM


Reviewed by: HDINH -07/20/06Prep/Q C Batch ID: W HG DISS060719B /W HG DISS060719


LCS /LCSD - Liquid - EPA 7470A Dissolved M ercury for W ater and Groundw ater / EPA 245.1 Dissolved M ercury for W astew ater


Units

<0.0002 0.0020 0.00200M ercury,Dissolved 75 -125100m g/L



<0.0002 0.0020 0.00187 25.0M ercury,Dissolved 75 -1256.793.5m g/L

Q CReport-dba -7/20/2006 5:21:26 PM


Reviewed by: HDINH -07/18/06Q C Batch ID: W M 060717DISS


LCS /LCSD - Liquid - Dissolved M etals by ICP:EPA 3005A /EPA 6010B for G roundw ater and W ater -EPA 200.7 for W astew ater


Units

<0.010 0.50 0.531Antim ony 75 -125106m g/L

<0.010 0.50 0.505Arsenic 75 -125101m g/L

<0.0050 0.50 0.503Barium 75 -125101m g/L

<0.0050 0.50 0.496Beryllium 75 -12599.2m g/L

<0.0020 0.50 0.500Cadm ium 75 -125100m g/L

<0.0050 0.50 0.507Chrom ium 75 -125101m g/L

<0.0050 0.50 0.519Cobalt 75 -125104m g/L

<0.0050 0.50 0.514Copper 75 -125103m g/L

<0.050 0.50 0.523Iron 75 -125105m g/L

<0.0050 0.50 0.523Lead 75 -125105m g/L

<0.0020 0.50 0.521M anganese 75 -125104m g/L

<0.0050 0.50 0.517M olybdenum 75 -125103m g/L

<0.0050 0.50 0.518Nickel 75 -125104m g/L

<0.020 0.50 0.479Selenium 75 -12595.8m g/L

<0.0050 0.50 0.510Silver 75 -125102m g/L

<0.020 0.50 0.477Thallium 75 -12595.4m g/L

<0.0050 0.50 0.515Vanadium 75 -125103m g/L

<0.010 0.50 0.509Zinc 75 -125102m g/L



<0.010 0.50 0.526 25.0Antim ony 75 -1250.95105m g/L

<0.010 0.50 0.501 25.0Arsenic 75 -1250.80100m g/L

<0.0050 0.50 0.493 25.0Barium 75 -1252.098.6m g/L

<0.0050 0.50 0.486 25.0Beryllium 75 -1252.097.2m g/L

<0.0020 0.50 0.494 25.0Cadm ium 75 -1251.298.8m g/L

<0.0050 0.50 0.498 25.0Chrom ium 75 -1251.899.6m g/L

<0.0050 0.50 0.513 25.0Cobalt 75 -1251.2103m g/L

<0.0050 0.50 0.506 25.0Copper 75 -1251.6101m g/L

<0.050 0.50 0.504 25.0Iron 75 -1253.7101m g/L

<0.0050 0.50 0.513 25.0Lead 75 -1251.9103m g/L

<0.0020 0.50 0.512 25.0M anganese 75 -1251.7102m g/L

<0.0050 0.50 0.508 25.0M olybdenum 75 -1251.8102m g/L

<0.0050 0.50 0.508 25.0Nickel 75 -1251.9102m g/L

<0.020 0.50 0.478 25.0Selenium 75 -1250.2195.6m g/L

<0.0050 0.50 0.506 25.0Silver 75 -1250.79101m g/L

<0.020 0.50 0.473 25.0Thallium 75 -1250.8494.6m g/L

<0.0050 0.50 0.508 25.0Vanadium 75 -1251.4102m g/L

<0.010 0.50 0.501 25.0Zinc 75 -1251.6100m g/L

Q CReport-dba -7/20/2006 5:21:27 PM




LCS /LCSD - Liquid - VO Cs:EPA 5030C /EPA 8260B for Groundw ater and W ater - EPA 624 for W astew ater


Units

<0.50 20 17.61,1-Dichloroethene 70 -13088.0µg/L

<0.50 20 20.4Benzene 70 -130102µg/L

<0.50 20 20.5Chlorobenzene 70 -130102µg/L

<1.0 20 15.7M ethyl-t-butylEther 70 -13078.5µg/L

<0.50 20 19.0Toluene 70 -13095.0µg/L

<0.50 20 20.2Trichloroethene 70 -130101µg/L




Toluene-d8 94.4 60 130-



<0.50 20 17.6 25.01,1-Dichloroethene 70 -1300.088.0µg/L

<0.50 20 20.7 25.0Benzene 70 -1301.5104µg/L

<0.50 20 20.8 25.0Chlorobenzene 70 -1301.5104µg/L

<1.0 20 16.9 25.0M ethyl-t-butylEther 70 -1307.484.5µg/L

<0.50 20 19.1 25.0Toluene 70 -1300.5295.5µg/L

<0.50 20 20.2 25.0Trichloroethene 70 -1300.0101µg/L




Toluene-d8 96.1 60 130-



LCS /LCSD - Liquid - TPH-Purgeable:GC/M S


Units

<25 120 126TPH as Gasoline 65 -135101µg/L




Toluene-d8 94.3 60 130-



<25 120 122 25.0TPH as Gasoline 65 -1353.297.4µg/L




Toluene-d8 91.2 60 130-

Q CReport-dba -7/20/2006 5:21:28 PM


Reviewed by: JIsiderio -07/14/06Q C Batch ID: W CR6060714


M S /M SD - Liquid - Chrom ium -VI:EPA 7196A for W ater and Groundw ater /Std.M ethods (18th Ed.)3500-Cr-Dfor W astew ater

Param eter

Sam pleResult

SpikeAm ount


Recovery Lim its

AnalysisDate


ND 0.10 0.0905Chrom ium (VI) 75 -1257/14/2006m g/L 90.5

Param eter

Sam pleResult

SpikeAm ount


Recovery Lim its

AnalysisDate


RPD RPD Lim its

M SD

ND 0.10 0.0922 25.0Chrom ium (VI) 75 -1257/14/2006m g/L 1.892.2

Q CReport-dba -7/20/2006 5:21:29 PM


Reviewed by: HDINH -07/18/06Q C/Prep Batch ID: W M 060717DISS


M S /M SD - Liquid - Dissolved M etals by ICP:EPA 3005A /EPA 6010B for G roundw ater and W ater - EPA 200.7 for W astew ater

Param eter

Sam pleResult

SpikeAm ount


Recovery Lim its

AnalysisDate


ND 0.50 0.550Antim ony 75 -1257/17/2006m g/L 110

ND 0.50 0.526Arsenic 75 -1257/17/2006m g/L 105

ND 0.50 0.508Barium 75 -1257/17/2006m g/L 102

ND 0.50 0.514Beryllium 75 -1257/17/2006m g/L 103

ND 0.50 0.511Cadm ium 75 -1257/17/2006m g/L 102

ND 0.50 0.521Chrom ium 75 -1257/17/2006m g/L 104

ND 0.50 0.532Cobalt 75 -1257/17/2006m g/L 106

ND 0.50 0.521Copper 75 -1257/17/2006m g/L 104

ND 0.50 0.537Lead 75 -1257/17/2006m g/L 107

ND 0.50 0.522M olybdenum 75 -1257/17/2006m g/L 104

ND 0.50 0.531Nickel 75 -1257/17/2006m g/L 106

ND 0.50 0.507Selenium 75 -1257/17/2006m g/L 101

ND 0.50 0.521Silver 75 -1257/17/2006m g/L 104

ND 0.50 0.490Thallium 75 -1257/17/2006m g/L 98.0

ND 0.50 0.524Vanadium 75 -1257/17/2006m g/L 105

0.0100 0.50 0.529Zinc 75 -1257/17/2006m g/L 104

Param eter

Sam pleResult

SpikeAm ount


Recovery Lim its

AnalysisDate


RPD RPD Lim its

M SD

ND 0.50 0.555 25.0Antim ony 75 -1257/17/2006m g/L 0.90111

ND 0.50 0.530 25.0Arsenic 75 -1257/17/2006m g/L 0.76106

ND 0.50 0.516 25.0Barium 75 -1257/17/2006m g/L 1.6103

ND 0.50 0.517 25.0Beryllium 75 -1257/17/2006m g/L 0.58103

ND 0.50 0.519 25.0Cadm ium 75 -1257/17/2006m g/L 1.6104

ND 0.50 0.525 25.0Chrom ium 75 -1257/17/2006m g/L 0.76105

ND 0.50 0.541 25.0Cobalt 75 -1257/17/2006m g/L 1.7108

ND 0.50 0.531 25.0Copper 75 -1257/17/2006m g/L 1.9106

ND 0.50 0.548 25.0Lead 75 -1257/17/2006m g/L 2.0110

ND 0.50 0.531 25.0M olybdenum 75 -1257/17/2006m g/L 1.7106

ND 0.50 0.537 25.0Nickel 75 -1257/17/2006m g/L 1.1107

ND 0.50 0.509 25.0Selenium 75 -1257/17/2006m g/L 0.39102

ND 0.50 0.529 25.0Silver 75 -1257/17/2006m g/L 1.5106

ND 0.50 0.507 25.0Thallium 75 -1257/17/2006m g/L 3.4101

ND 0.50 0.534 25.0Vanadium 75 -1257/17/2006m g/L 1.9107

0.0100 0.50 0.535 25.0Zinc 75 -1257/17/2006m g/L 1.1105

Q CReport-dba -7/20/2006 5:21:29 PM




TestMatrix

Novato, CA 94947

Jim Dunn

Comments




Issued: 07/24/2006

P.O. Number: 285.002.01.003


Liquid TPH-Extractable: EPA 3510C / EPA 8015BVOCs: EPA 5030C / EPA 8260B for Groundwater and Water - EPA 624 for WastewaterTPH-Purgeable: GC/MS


Sincerely,







P.O. Number: 285.002.01.003


Attn: Jim Dunn




Lab # : 50419-001 Sample ID: 065C-09-GW Matrix: Liquid Sample Date: 7/14/2006 9:30 AM


1,1,1,2-Tetrachloroethane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,1,1-Trichloroethane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,1,2,2-Tetrachloroethane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,1,2-Trichloroethane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,1-Dichloroethane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,1-Dichloroethene ND g/L0.501.0 WM10607197/19/2006N/AN/A1,1-Dichloropropene ND g/L0.501.0 WM10607197/19/2006N/AN/A1,2,3-Trichlorobenzene ND g/L5.01.0 WM10607197/19/2006N/AN/A1,2,3-Trichloropropane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,2,4-Trichlorobenzene ND g/L5.01.0 WM10607197/19/2006N/AN/A1,2,4-Trimethylbenzene ND g/L5.01.0 WM10607197/19/2006N/AN/A1,2-Dibromo-3-Chloropropane ND g/L5.01.0 WM10607197/19/2006N/AN/A1,2-Dibromoethane (EDB) ND g/L0.501.0 WM10607197/19/2006N/AN/A1,2-Dichlorobenzene ND g/L0.501.0 WM10607197/19/2006N/AN/A1,2-Dichloroethane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,2-Dichloropropane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,3,5-Trimethylbenzene ND g/L5.01.0 WM10607197/19/2006N/AN/A1,3-Dichlorobenzene ND g/L0.501.0 WM10607197/19/2006N/AN/A1,3-Dichloropropane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,4-Dichlorobenzene ND g/L0.501.0 WM10607197/19/2006N/AN/A1,4-Dioxane ND g/L501.0 WM10607197/19/2006N/AN/A2,2-Dichloropropane ND g/L0.501.0 WM10607197/19/2006N/AN/A2-Butanone (MEK) ND g/L201.0 WM10607197/19/2006N/AN/A2-Chloroethyl-vinyl Ether ND g/L5.01.0 WM10607197/19/2006N/AN/A2-Chlorotoluene ND g/L5.01.0 WM10607197/19/2006N/AN/A2-Hexanone ND g/L201.0 WM10607197/19/2006N/AN/A4-Chlorotoluene ND g/L5.01.0 WM10607197/19/2006N/AN/A4-Methyl-2-Pentanone(MIBK) ND g/L201.0 WM10607197/19/2006N/AN/AAcetone 75 g/L201.0 WM10607197/19/2006N/AN/AAcetonitrile ND g/L5.01.0 WM10607197/19/2006N/AN/AAcrolein ND g/L5.01.0 WM10607197/19/2006N/AN/AAcrylonitrile ND g/L5.01.0 WM10607197/19/2006N/AN/ABenzene ND g/L0.501.0 WM10607197/19/2006N/AN/ABenzyl Chloride ND g/L5.01.0 WM10607197/19/2006N/AN/ABromobenzene ND g/L0.501.0 WM10607197/19/2006N/AN/ABromochloromethane ND g/L0.501.0 WM10607197/19/2006N/AN/ABromodichloromethane ND g/L0.501.0 WM10607197/19/2006N/AN/ABromoform ND g/L0.501.0 WM10607197/19/2006N/AN/ABromomethane ND g/L0.501.0 WM10607197/19/2006N/AN/ACarbon Disulfide ND g/L0.501.0 WM10607197/19/2006N/AN/ACarbon Tetrachloride ND g/L0.501.0 WM10607197/19/2006N/AN/AChlorobenzene ND g/L0.501.0 WM10607197/19/2006N/AN/AChloroethane ND g/L0.501.0 WM10607197/19/2006N/AN/AChloroform ND g/L0.501.0 WM10607197/19/2006N/AN/AChloromethane ND g/L0.501.0 WM10607197/19/2006N/AN/A






P.O. Number: 285.002.01.003


Attn: Jim Dunn














P.O. Number: 285.002.01.003


Attn: Jim Dunn










TPH as Diesel ND g/L521.0 WD060719A7/23/2006WD060719A200 ppb Hydrocarbon (C10-C36). No Diesel pattern present.

7/19/2006


Analyzed by: EricKumSurrogate Surrogate Recovery Control Limits (%)o-Terphenyl 64.6 22 133-






P.O. Number: 285.002.01.003


Attn: Jim Dunn




Lab # : 50419-002 Sample ID: 065R-05-GW Matrix: Liquid Sample Date: 7/14/2006 10:00 AM


1,1,1,2-Tetrachloroethane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,1,1-Trichloroethane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,1,2,2-Tetrachloroethane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,1,2-Trichloroethane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,1-Dichloroethane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,1-Dichloroethene ND g/L0.501.0 WM10607197/19/2006N/AN/A1,1-Dichloropropene ND g/L0.501.0 WM10607197/19/2006N/AN/A1,2,3-Trichlorobenzene ND g/L5.01.0 WM10607197/19/2006N/AN/A1,2,3-Trichloropropane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,2,4-Trichlorobenzene ND g/L5.01.0 WM10607197/19/2006N/AN/A1,2,4-Trimethylbenzene ND g/L5.01.0 WM10607197/19/2006N/AN/A1,2-Dibromo-3-Chloropropane ND g/L5.01.0 WM10607197/19/2006N/AN/A1,2-Dibromoethane (EDB) ND g/L0.501.0 WM10607197/19/2006N/AN/A1,2-Dichlorobenzene ND g/L0.501.0 WM10607197/19/2006N/AN/A1,2-Dichloroethane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,2-Dichloropropane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,3,5-Trimethylbenzene ND g/L5.01.0 WM10607197/19/2006N/AN/A1,3-Dichlorobenzene ND g/L0.501.0 WM10607197/19/2006N/AN/A1,3-Dichloropropane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,4-Dichlorobenzene ND g/L0.501.0 WM10607197/19/2006N/AN/A1,4-Dioxane ND g/L501.0 WM10607197/19/2006N/AN/A2,2-Dichloropropane ND g/L0.501.0 WM10607197/19/2006N/AN/A2-Butanone (MEK) ND g/L201.0 WM10607197/19/2006N/AN/A2-Chloroethyl-vinyl Ether ND g/L5.01.0 WM10607197/19/2006N/AN/A2-Chlorotoluene ND g/L5.01.0 WM10607197/19/2006N/AN/A2-Hexanone ND g/L201.0 WM10607197/19/2006N/AN/A4-Chlorotoluene ND g/L5.01.0 WM10607197/19/2006N/AN/A4-Methyl-2-Pentanone(MIBK) ND g/L201.0 WM10607197/19/2006N/AN/AAcetone 30 g/L201.0 WM10607197/19/2006N/AN/AAcetonitrile ND g/L5.01.0 WM10607197/19/2006N/AN/AAcrolein ND g/L5.01.0 WM10607197/19/2006N/AN/AAcrylonitrile ND g/L5.01.0 WM10607197/19/2006N/AN/ABenzene ND g/L0.501.0 WM10607197/19/2006N/AN/ABenzyl Chloride ND g/L5.01.0 WM10607197/19/2006N/AN/ABromobenzene ND g/L0.501.0 WM10607197/19/2006N/AN/ABromochloromethane ND g/L0.501.0 WM10607197/19/2006N/AN/ABromodichloromethane ND g/L0.501.0 WM10607197/19/2006N/AN/ABromoform ND g/L0.501.0 WM10607197/19/2006N/AN/ABromomethane ND g/L0.501.0 WM10607197/19/2006N/AN/ACarbon Disulfide 0.55 g/L0.501.0 WM10607197/19/2006N/AN/ACarbon Tetrachloride ND g/L0.501.0 WM10607197/19/2006N/AN/AChlorobenzene ND g/L0.501.0 WM10607197/19/2006N/AN/AChloroethane ND g/L0.501.0 WM10607197/19/2006N/AN/AChloroform ND g/L0.501.0 WM10607197/19/2006N/AN/AChloromethane ND g/L0.501.0 WM10607197/19/2006N/AN/A






P.O. Number: 285.002.01.003


Attn: Jim Dunn














P.O. Number: 285.002.01.003


Attn: Jim Dunn










TPH as Diesel ND g/L581.2 WD060719A7/23/2006WD060719A400 ppb Motor Oil Range Organics (C12-C34). No Diesel pattern present.

7/19/2006


Analyzed by: EricKumSurrogate Surrogate Recovery Control Limits (%)o-Terphenyl 70.8 22 133-






P.O. Number: 285.002.01.003


Attn: Jim Dunn




Lab # : 50419-003 Sample ID: Trip-4 Matrix: Liquid Sample Date: 7/14/2006 10:30 AM


1,1,1,2-Tetrachloroethane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,1,1-Trichloroethane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,1,2,2-Tetrachloroethane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,1,2-Trichloroethane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,1-Dichloroethane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,1-Dichloroethene ND g/L0.501.0 WM10607197/19/2006N/AN/A1,1-Dichloropropene ND g/L0.501.0 WM10607197/19/2006N/AN/A1,2,3-Trichlorobenzene ND g/L5.01.0 WM10607197/19/2006N/AN/A1,2,3-Trichloropropane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,2,4-Trichlorobenzene ND g/L5.01.0 WM10607197/19/2006N/AN/A1,2,4-Trimethylbenzene ND g/L5.01.0 WM10607197/19/2006N/AN/A1,2-Dibromo-3-Chloropropane ND g/L5.01.0 WM10607197/19/2006N/AN/A1,2-Dibromoethane (EDB) ND g/L0.501.0 WM10607197/19/2006N/AN/A1,2-Dichlorobenzene ND g/L0.501.0 WM10607197/19/2006N/AN/A1,2-Dichloroethane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,2-Dichloropropane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,3,5-Trimethylbenzene ND g/L5.01.0 WM10607197/19/2006N/AN/A1,3-Dichlorobenzene ND g/L0.501.0 WM10607197/19/2006N/AN/A1,3-Dichloropropane ND g/L0.501.0 WM10607197/19/2006N/AN/A1,4-Dichlorobenzene ND g/L0.501.0 WM10607197/19/2006N/AN/A1,4-Dioxane ND g/L501.0 WM10607197/19/2006N/AN/A2,2-Dichloropropane ND g/L0.501.0 WM10607197/19/2006N/AN/A2-Butanone (MEK) ND g/L201.0 WM10607197/19/2006N/AN/A2-Chloroethyl-vinyl Ether ND g/L5.01.0 WM10607197/19/2006N/AN/A2-Chlorotoluene ND g/L5.01.0 WM10607197/19/2006N/AN/A2-Hexanone ND g/L201.0 WM10607197/19/2006N/AN/A4-Chlorotoluene ND g/L5.01.0 WM10607197/19/2006N/AN/A4-Methyl-2-Pentanone(MIBK) ND g/L201.0 WM10607197/19/2006N/AN/AAcetone ND g/L201.0 WM10607197/19/2006N/AN/AAcetonitrile ND g/L5.01.0 WM10607197/19/2006N/AN/AAcrolein ND g/L5.01.0 WM10607197/19/2006N/AN/AAcrylonitrile ND g/L5.01.0 WM10607197/19/2006N/AN/ABenzene ND g/L0.501.0 WM10607197/19/2006N/AN/ABenzyl Chloride ND g/L5.01.0 WM10607197/19/2006N/AN/ABromobenzene ND g/L0.501.0 WM10607197/19/2006N/AN/ABromochloromethane ND g/L0.501.0 WM10607197/19/2006N/AN/ABromodichloromethane 1.2 g/L0.501.0 WM10607197/19/2006N/AN/ABromoform ND g/L0.501.0 WM10607197/19/2006N/AN/ABromomethane ND g/L0.501.0 WM10607197/19/2006N/AN/ACarbon Disulfide ND g/L0.501.0 WM10607197/19/2006N/AN/ACarbon Tetrachloride ND g/L0.501.0 WM10607197/19/2006N/AN/AChlorobenzene ND g/L0.501.0 WM10607197/19/2006N/AN/AChloroethane ND g/L0.501.0 WM10607197/19/2006N/AN/AChloroform 24 g/L0.501.0 WM10607197/19/2006N/AN/AChloromethane ND g/L0.501.0 WM10607197/19/2006N/AN/A






P.O. Number: 285.002.01.003


Attn: Jim Dunn














P.O. Number: 285.002.01.003


Attn: Jim Dunn






TPH as Gasoline 35 g/L251.0 WM10607197/19/2006N/AAtypical pattern. No indication of gasoline.

N/A









Units<0.50 20 16.61,1-Dichloroethene 70 - 13083.0g/L<0.50 20 19.9Benzene 70 - 13099.5g/L<0.50 20 19.9Chlorobenzene 70 - 13099.5g/L<1.0 20 15.6Methyl-t-butyl Ether 70 - 13078.0g/L

<0.50 20 18.5Toluene 70 - 13092.5g/L<0.50 20 19.4Trichloroethene 70 - 13097.0g/L



RPD RPD LimitsUnits<0.50 20 17.8 25.01,1-Dichloroethene 70 - 1307.089.0g/L<0.50 20 21.4 25.0Benzene 70 - 1307.3107g/L<0.50 20 20.5 25.0Chlorobenzene 70 - 1303.0102g/L<1.0 20 18.0 25.0Methyl-t-butyl Ether 70 - 1301490.0g/L

<0.50 20 19.0 25.0Toluene 70 - 1302.795.0g/L<0.50 20 20.2 25.0Trichloroethene 70 - 1304.0101g/L








RPD RPD LimitsUnits<25 120 124 25.0TPH as Gasoline 65 - 1350.1698.9g/L














RPD RPD LimitsUnits<50 1000 671 25.0TPH as Diesel 40 - 1387.467.1g/L<200 1000 792 25.0TPH as Motor Oil 40 - 1381.879.2g/L






TestMatrix

Novato, CA 94947

Jim Dunn

Comments




Issued: 07/20/2006


Liquid EPA 7470A Dissolved Mercury for Water and Groundwater / EPA 245.1 Dissolved Mercury for WastewaterDissolved Metals by ICP: EPA 3005A / EPA 6010B for Groundwater and Water - EPA 200.7 for WastewaterChromium-VI: EPA 7196A for Water and Groundwater / Std. Methods (18th Ed.) 3500-Cr-D for WastewaterTPH-Extractable: EPA 3510C / EPA 8015BVOCs: EPA 5030C / EPA 8260B for Groundwater and Water - EPA 624 for WastewaterTPH-Purgeable: GC/MS


Sincerely,








Attn: Jim Dunn




Lab # : 50438-001 Sample ID: 06SR-05-GW Matrix: Liquid Sample Date: 7/17/2006 11:00 AM

Parameter Result UnitsDetection LimitD/P-F QC BatchQual Prep Date Analysis DatePrep BatchChromium VI: EPA 7196A for Water and Groundwater / Std. Methods (18th Ed.) 3500-Cr-D for Wastewater





Mercury, Dissolved ND mg/L0.00021.0 WHGDISS0607197/19/2006WHGDISS060719B7/19/2006

Reviewed by: HDINH



Antimony ND mg/L0.0101.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Arsenic 0.031 mg/L0.0101.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Barium 0.50 mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Beryllium ND mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Cadmium ND mg/L0.00201.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Chromium 0.0090 mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Cobalt 0.017 mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Copper ND mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Lead 0.027 mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Molybdenum 0.020 mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Nickel 0.031 mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Selenium ND mg/L0.0201.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Silver ND mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Thallium ND mg/L0.0201.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Vanadium 0.017 mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Zinc ND mg/L0.0101.0 WM060718DISS7/19/2006WM060718DISS7/18/2006

Reviewed by: HDINH

Analyzed by: Equeja







Attn: Jim Dunn




Lab # : 50438-002 Sample ID: 06SC-09-GW Matrix: Liquid Sample Date: 7/17/2006 11:30 AM







Reviewed by: HDINH



Antimony ND mg/L0.0101.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Arsenic 0.016 mg/L0.0101.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Barium 0.19 mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Beryllium ND mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Cadmium ND mg/L0.00201.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Chromium 0.0080 mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Cobalt 0.0070 mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Copper ND mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Lead 0.019 mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Molybdenum 0.018 mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Nickel 0.013 mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Selenium ND mg/L0.0201.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Silver ND mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Thallium ND mg/L0.0201.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Vanadium ND mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Zinc ND mg/L0.0101.0 WM060718DISS7/19/2006WM060718DISS7/18/2006

Reviewed by: HDINH

Analyzed by: EQueja







Attn: Jim Dunn




Lab # : 50438-003 Sample ID: 06SC-10-GW Matrix: Liquid Sample Date: 7/17/2006 12:00 PM











Attn: Jim Dunn






1,1,1,2-Tetrachloroethane ND g/L0.501.0 WM20607207/20/2006N/AN/A1,1,1-Trichloroethane ND g/L0.501.0 WM20607207/20/2006N/AN/A1,1,2,2-Tetrachloroethane ND g/L0.501.0 WM20607207/20/2006N/AN/A1,1,2-Trichloroethane ND g/L0.501.0 WM20607207/20/2006N/AN/A1,1-Dichloroethane ND g/L0.501.0 WM20607207/20/2006N/AN/A1,1-Dichloroethene ND g/L0.501.0 WM20607207/20/2006N/AN/A1,1-Dichloropropene ND g/L0.501.0 WM20607207/20/2006N/AN/A1,2,3-Trichlorobenzene ND g/L5.01.0 WM20607207/20/2006N/AN/A1,2,3-Trichloropropane ND g/L0.501.0 WM20607207/20/2006N/AN/A1,2,4-Trichlorobenzene ND g/L5.01.0 WM20607207/20/2006N/AN/A1,2,4-Trimethylbenzene ND g/L5.01.0 WM20607207/20/2006N/AN/A1,2-Dibromo-3-Chloropropane ND g/L5.01.0 WM20607207/20/2006N/AN/A1,2-Dibromoethane (EDB) ND g/L0.501.0 WM20607207/20/2006N/AN/A1,2-Dichlorobenzene ND g/L0.501.0 WM20607207/20/2006N/AN/A1,2-Dichloroethane ND g/L0.501.0 WM20607207/20/2006N/AN/A1,2-Dichloropropane ND g/L0.501.0 WM20607207/20/2006N/AN/A1,3,5-Trimethylbenzene ND g/L5.01.0 WM20607207/20/2006N/AN/A1,3-Dichlorobenzene ND g/L0.501.0 WM20607207/20/2006N/AN/A1,3-Dichloropropane ND g/L0.501.0 WM20607207/20/2006N/AN/A1,4-Dichlorobenzene ND g/L0.501.0 WM20607207/20/2006N/AN/A1,4-Dioxane ND g/L501.0 WM20607207/20/2006N/AN/A2,2-Dichloropropane ND g/L0.501.0 WM20607207/20/2006N/AN/A2-Butanone (MEK) ND g/L201.0 WM20607207/20/2006N/AN/A2-Chloroethyl-vinyl Ether ND g/L5.01.0 WM20607207/20/2006N/AN/A2-Chlorotoluene ND g/L5.01.0 WM20607207/20/2006N/AN/A2-Hexanone ND g/L201.0 WM20607207/20/2006N/AN/A4-Chlorotoluene ND g/L5.01.0 WM20607207/20/2006N/AN/A4-Methyl-2-Pentanone(MIBK) ND g/L201.0 WM20607207/20/2006N/AN/AAcetone 25 g/L201.0 WM20607207/20/2006N/AN/AAcetonitrile ND g/L5.01.0 WM20607207/20/2006N/AN/AAcrolein ND g/L5.01.0 WM20607207/20/2006N/AN/AAcrylonitrile ND g/L5.01.0 WM20607207/20/2006N/AN/ABenzene ND g/L0.501.0 WM20607207/20/2006N/AN/ABenzyl Chloride ND g/L5.01.0 WM20607207/20/2006N/AN/ABromobenzene ND g/L0.501.0 WM20607207/20/2006N/AN/ABromochloromethane ND g/L0.501.0 WM20607207/20/2006N/AN/ABromodichloromethane ND g/L0.501.0 WM20607207/20/2006N/AN/ABromoform ND g/L0.501.0 WM20607207/20/2006N/AN/ABromomethane ND g/L0.501.0 WM20607207/20/2006N/AN/ACarbon Disulfide ND g/L0.501.0 WM20607207/20/2006N/AN/ACarbon Tetrachloride ND g/L0.501.0 WM20607207/20/2006N/AN/AChlorobenzene ND g/L0.501.0 WM20607207/20/2006N/AN/AChloroethane ND g/L0.501.0 WM20607207/20/2006N/AN/AChloroform ND g/L0.501.0 WM20607207/20/2006N/AN/AChloromethane ND g/L0.501.0 WM20607207/20/2006N/AN/A







Attn: Jim Dunn








Analyzed by: TAFSurrogate Surrogate Recovery Control Limits (%)4-Bromofluorobenzene 101 60 130-Dibromofluoromethane 104 60 130-Toluene-d8 101 60 130-







Attn: Jim Dunn







Reviewed by: HDINH



Antimony ND mg/L0.0101.0 WM060718DISS7/18/2006WM060718DISS7/18/2006Arsenic 0.010 mg/L0.0101.0 WM060718DISS7/18/2006WM060718DISS7/18/2006Barium ND mg/L0.00501.0 WM060718DISS7/18/2006WM060718DISS7/18/2006Beryllium ND mg/L0.00501.0 WM060718DISS7/18/2006WM060718DISS7/18/2006Cadmium ND mg/L0.00201.0 WM060718DISS7/18/2006WM060718DISS7/18/2006Chromium 0.0050 mg/L0.00501.0 WM060718DISS7/18/2006WM060718DISS7/18/2006Cobalt ND mg/L0.00501.0 WM060718DISS7/18/2006WM060718DISS7/18/2006Copper ND mg/L0.00501.0 WM060718DISS7/18/2006WM060718DISS7/18/2006Lead ND mg/L0.00501.0 WM060718DISS7/18/2006WM060718DISS7/18/2006Molybdenum ND mg/L0.00501.0 WM060718DISS7/18/2006WM060718DISS7/18/2006Nickel ND mg/L0.00501.0 WM060718DISS7/18/2006WM060718DISS7/18/2006Selenium ND mg/L0.0201.0 WM060718DISS7/18/2006WM060718DISS7/18/2006Silver ND mg/L0.00501.0 WM060718DISS7/18/2006WM060718DISS7/18/2006Thallium ND mg/L0.0201.0 WM060718DISS7/18/2006WM060718DISS7/18/2006Vanadium ND mg/L0.00501.0 WM060718DISS7/18/2006WM060718DISS7/18/2006Zinc ND mg/L0.0101.0 WM060718DISS7/18/2006WM060718DISS7/18/2006

Reviewed by: HDINH

Analyzed by: EQueja




Analyzed by: TAFSurrogate Surrogate Recovery Control Limits (%)4-Bromofluorobenzene 115 60 130-Dibromofluoromethane 93.9 60 130-Toluene-d8 99.6 60 130-


TPH as Diesel ND g/L501.0 WD060719A7/20/2006WD060719A260 g/L Hydrocarbon (C12-C36).

7/19/2006









Attn: Jim Dunn






1,1,1,2-Tetrachloroethane ND g/L0.501.0 WM20607197/19/2006N/AN/A1,1,1-Trichloroethane ND g/L0.501.0 WM20607197/19/2006N/AN/A1,1,2,2-Tetrachloroethane ND g/L0.501.0 WM20607197/19/2006N/AN/A1,1,2-Trichloroethane ND g/L0.501.0 WM20607197/19/2006N/AN/A1,1-Dichloroethane ND g/L0.501.0 WM20607197/19/2006N/AN/A1,1-Dichloroethene ND g/L0.501.0 WM20607197/19/2006N/AN/A1,1-Dichloropropene ND g/L0.501.0 WM20607197/19/2006N/AN/A1,2,3-Trichlorobenzene ND g/L5.01.0 WM20607197/19/2006N/AN/A1,2,3-Trichloropropane ND g/L0.501.0 WM20607197/19/2006N/AN/A1,2,4-Trichlorobenzene ND g/L5.01.0 WM20607197/19/2006N/AN/A1,2,4-Trimethylbenzene ND g/L5.01.0 WM20607197/19/2006N/AN/A1,2-Dibromo-3-Chloropropane ND g/L5.01.0 WM20607197/19/2006N/AN/A1,2-Dibromoethane (EDB) ND g/L0.501.0 WM20607197/19/2006N/AN/A1,2-Dichlorobenzene ND g/L0.501.0 WM20607197/19/2006N/AN/A1,2-Dichloroethane ND g/L0.501.0 WM20607197/19/2006N/AN/A1,2-Dichloropropane ND g/L0.501.0 WM20607197/19/2006N/AN/A1,3,5-Trimethylbenzene ND g/L5.01.0 WM20607197/19/2006N/AN/A1,3-Dichlorobenzene ND g/L0.501.0 WM20607197/19/2006N/AN/A1,3-Dichloropropane ND g/L0.501.0 WM20607197/19/2006N/AN/A1,4-Dichlorobenzene ND g/L0.501.0 WM20607197/19/2006N/AN/A1,4-Dioxane ND g/L501.0 WM20607197/19/2006N/AN/A2,2-Dichloropropane ND g/L0.501.0 WM20607197/19/2006N/AN/A2-Butanone (MEK) ND g/L201.0 WM20607197/19/2006N/AN/A2-Chloroethyl-vinyl Ether ND g/L5.01.0 WM20607197/19/2006N/AN/A2-Chlorotoluene ND g/L5.01.0 WM20607197/19/2006N/AN/A2-Hexanone ND g/L201.0 WM20607197/19/2006N/AN/A4-Chlorotoluene ND g/L5.01.0 WM20607197/19/2006N/AN/A4-Methyl-2-Pentanone(MIBK) ND g/L201.0 WM20607197/19/2006N/AN/AAcetone 21 g/L201.0 WM20607197/19/2006N/AN/AAcetonitrile ND g/L5.01.0 WM20607197/19/2006N/AN/AAcrolein ND g/L5.01.0 WM20607197/19/2006N/AN/AAcrylonitrile ND g/L5.01.0 WM20607197/19/2006N/AN/ABenzene ND g/L0.501.0 WM20607197/19/2006N/AN/ABenzyl Chloride ND g/L5.01.0 WM20607197/19/2006N/AN/ABromobenzene ND g/L0.501.0 WM20607197/19/2006N/AN/ABromochloromethane ND g/L0.501.0 WM20607197/19/2006N/AN/ABromodichloromethane 1.1 g/L0.501.0 WM20607197/19/2006N/AN/ABromoform ND g/L0.501.0 WM20607197/19/2006N/AN/ABromomethane ND g/L0.501.0 WM20607197/19/2006N/AN/ACarbon Disulfide ND g/L0.501.0 WM20607197/19/2006N/AN/ACarbon Tetrachloride ND g/L0.501.0 WM20607197/19/2006N/AN/AChlorobenzene ND g/L0.501.0 WM20607197/19/2006N/AN/AChloroethane ND g/L0.501.0 WM20607197/19/2006N/AN/AChloroform 26 g/L0.501.0 WM20607197/19/2006N/AN/AChloromethane ND g/L0.501.0 WM20607197/19/2006N/AN/A







Attn: Jim Dunn















Attn: Jim Dunn






TPH as Gasoline 26 g/L251.0 WM20607197/19/2006N/ATPH as Gasoline reported value is the result of a discrete peak (chloroform) that is not typical of TPH as Gasoline but is within the gasoline quantitation range.

N/A


Analyzed by: TAFSurrogate Surrogate Recovery Control Limits (%)4-Bromofluorobenzene 117 60 130-Dibromofluoromethane 97.2 60 130-Toluene-d8 102 60 130-







Attn: Jim Dunn















Attn: Jim Dunn






1,1,1,2-Tetrachloroethane ND g/L0.501.0 WM20607197/19/2006N/AN/A1,1,1-Trichloroethane ND g/L0.501.0 WM20607197/19/2006N/AN/A1,1,2,2-Tetrachloroethane ND g/L0.501.0 WM20607197/19/2006N/AN/A1,1,2-Trichloroethane ND g/L0.501.0 WM20607197/19/2006N/AN/A1,1-Dichloroethane ND g/L0.501.0 WM20607197/19/2006N/AN/A1,1-Dichloroethene ND g/L0.501.0 WM20607197/19/2006N/AN/A1,1-Dichloropropene ND g/L0.501.0 WM20607197/19/2006N/AN/A1,2,3-Trichlorobenzene ND g/L5.01.0 WM20607197/19/2006N/AN/A1,2,3-Trichloropropane ND g/L0.501.0 WM20607197/19/2006N/AN/A1,2,4-Trichlorobenzene ND g/L5.01.0 WM20607197/19/2006N/AN/A1,2,4-Trimethylbenzene ND g/L5.01.0 WM20607197/19/2006N/AN/A1,2-Dibromo-3-Chloropropane ND g/L5.01.0 WM20607197/19/2006N/AN/A1,2-Dibromoethane (EDB) ND g/L0.501.0 WM20607197/19/2006N/AN/A1,2-Dichlorobenzene ND g/L0.501.0 WM20607197/19/2006N/AN/A1,2-Dichloroethane ND g/L0.501.0 WM20607197/19/2006N/AN/A1,2-Dichloropropane ND g/L0.501.0 WM20607197/19/2006N/AN/A1,3,5-Trimethylbenzene ND g/L5.01.0 WM20607197/19/2006N/AN/A1,3-Dichlorobenzene ND g/L0.501.0 WM20607197/19/2006N/AN/A1,3-Dichloropropane ND g/L0.501.0 WM20607197/19/2006N/AN/A1,4-Dichlorobenzene ND g/L0.501.0 WM20607197/19/2006N/AN/A1,4-Dioxane ND g/L501.0 WM20607197/19/2006N/AN/A2,2-Dichloropropane ND g/L0.501.0 WM20607197/19/2006N/AN/A2-Butanone (MEK) ND g/L201.0 WM20607197/19/2006N/AN/A2-Chloroethyl-vinyl Ether ND g/L5.01.0 WM20607197/19/2006N/AN/A2-Chlorotoluene ND g/L5.01.0 WM20607197/19/2006N/AN/A2-Hexanone ND g/L201.0 WM20607197/19/2006N/AN/A4-Chlorotoluene ND g/L5.01.0 WM20607197/19/2006N/AN/A4-Methyl-2-Pentanone(MIBK) ND g/L201.0 WM20607197/19/2006N/AN/AAcetone ND g/L201.0 WM20607197/19/2006N/AN/AAcetonitrile ND g/L5.01.0 WM20607197/19/2006N/AN/AAcrolein ND g/L5.01.0 WM20607197/19/2006N/AN/AAcrylonitrile ND g/L5.01.0 WM20607197/19/2006N/AN/ABenzene ND g/L0.501.0 WM20607197/19/2006N/AN/ABenzyl Chloride ND g/L5.01.0 WM20607197/19/2006N/AN/ABromobenzene ND g/L0.501.0 WM20607197/19/2006N/AN/ABromochloromethane ND g/L0.501.0 WM20607197/19/2006N/AN/ABromodichloromethane 1.1 g/L0.501.0 WM20607197/19/2006N/AN/ABromoform ND g/L0.501.0 WM20607197/19/2006N/AN/ABromomethane ND g/L0.501.0 WM20607197/19/2006N/AN/ACarbon Disulfide ND g/L0.501.0 WM20607197/19/2006N/AN/ACarbon Tetrachloride ND g/L0.501.0 WM20607197/19/2006N/AN/AChlorobenzene ND g/L0.501.0 WM20607197/19/2006N/AN/AChloroethane ND g/L0.501.0 WM20607197/19/2006N/AN/AChloroform 26 g/L0.501.0 WM20607197/19/2006N/AN/AChloromethane ND g/L0.501.0 WM20607197/19/2006N/AN/A







Attn: Jim Dunn















Attn: Jim Dunn






Mercury, Dissolved 0.00035 mg/L0.00021.0 WHGDISS0607197/19/2006WHGDISS060719B7/19/2006

Reviewed by: HDINH



Antimony ND mg/L0.0101.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Arsenic ND mg/L0.0101.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Barium ND mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Beryllium ND mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Cadmium ND mg/L0.00201.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Chromium ND mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Cobalt ND mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Copper ND mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Lead ND mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Molybdenum ND mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Nickel ND mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Selenium ND mg/L0.0201.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Silver ND mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Thallium ND mg/L0.0201.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Vanadium ND mg/L0.00501.0 WM060718DISS7/19/2006WM060718DISS7/18/2006Zinc ND mg/L0.0101.0 WM060718DISS7/19/2006WM060718DISS7/18/2006

Reviewed by: HDINH

Analyzed by: Equeja


TPH as Gasoline 25 g/L251.0 WM20607197/19/2006N/ATPH as Gasoline reported value is the result of a discrete peak (chloroform) that is not typical of TPH as Gasoline but is within the gasoline quantitation range.

N/A


Analyzed by: TAFSurrogate Surrogate Recovery Control Limits (%)4-Bromofluorobenzene 115 60 130-Dibromofluoromethane 98.6 60 130-Toluene-d8 101 60 130-









LCS / LCSD - Liquid - Chromium VI: EPA 7196A for Water and Groundwater / Std. Methods (18th Ed.) 3500-Cr-D for Wastewater


Units<0.010 0.10 0.104Chromium (VI) 75 - 125104mg/L






MS / MSD - Liquid - Chromium VI: EPA 7196A for Water and Groundwater / Std. Methods (18th Ed.) 3500-Cr-D for Wastewater


Spike Amount


Recovery Limits

AnalysisDate


ND 0.10 0.108Chromium (VI) 75 - 1257/18/2006mg/L 108


Spike Amount


Recovery Limits

AnalysisDate


RPD RPD Limits

MSD

ND 0.10 0.105 25.0Chromium (VI) 75 - 1257/18/2006mg/L 3.1105



Reviewed by: HDINH - 07/20/06Prep/QC Batch ID: WHGDISS060719B /WHGDISS060719QC/Prep Date: 7/19/2006

LCS / LCSD - Liquid - EPA 7470A Dissolved Mercury for Water and Groundwater / EPA 245.1 Dissolved Mercury for Wastewater


Units<0.0002 0.0020 0.00200Mercury, Dissolved 75 - 125100mg/L


RPD RPD LimitsUnits<0.0002 0.0020 0.00187 25.0Mercury, Dissolved 75 - 1256.793.5mg/L



Reviewed by: HDINH - 07/19/06QC Batch ID: WM060718DISSQC/Prep Date: 7/18/2006

LCS / LCSD - Liquid - Dissolved Metals by ICP: EPA 3005A / EPA 6010B for Groundwater and Water - EPA 200.7 for Wastewater


Units<0.010 0.50 0.523Antimony 75 - 125105mg/L<0.010 0.50 0.517Arsenic 75 - 125103mg/L

<0.0050 0.50 0.465Barium 75 - 12593.0mg/L<0.0050 0.50 0.503Beryllium 75 - 125101mg/L<0.0020 0.50 0.508Cadmium 75 - 125102mg/L<0.0050 0.50 0.496Chromium 75 - 12599.2mg/L<0.0050 0.50 0.518Cobalt 75 - 125104mg/L<0.0050 0.50 0.499Copper 75 - 12599.8mg/L<0.0050 0.50 0.531Lead 75 - 125106mg/L<0.0050 0.50 0.510Molybdenum 75 - 125102mg/L<0.0050 0.50 0.521Nickel 75 - 125104mg/L<0.020 0.50 0.513Selenium 75 - 125103mg/L

<0.0050 0.50 0.481Silver 75 - 12596.2mg/L<0.020 0.50 0.491Thallium 75 - 12598.2mg/L

<0.0050 0.50 0.505Vanadium 75 - 125101mg/L<0.010 0.50 0.534Zinc 75 - 125107mg/L


RPD RPD LimitsUnits<0.010 0.50 0.539 25.0Antimony 75 - 1253.0108mg/L<0.010 0.50 0.532 25.0Arsenic 75 - 1252.9106mg/L

<0.0050 0.50 0.467 25.0Barium 75 - 1250.4393.4mg/L<0.0050 0.50 0.511 25.0Beryllium 75 - 1251.6102mg/L<0.0020 0.50 0.519 25.0Cadmium 75 - 1252.1104mg/L<0.0050 0.50 0.503 25.0Chromium 75 - 1251.4101mg/L<0.0050 0.50 0.527 25.0Cobalt 75 - 1251.7105mg/L<0.0050 0.50 0.507 25.0Copper 75 - 1251.6101mg/L<0.0050 0.50 0.543 25.0Lead 75 - 1252.2109mg/L<0.0050 0.50 0.520 25.0Molybdenum 75 - 1251.9104mg/L<0.0050 0.50 0.529 25.0Nickel 75 - 1251.5106mg/L<0.020 0.50 0.523 25.0Selenium 75 - 1251.9105mg/L

<0.0050 0.50 0.488 25.0Silver 75 - 1251.497.6mg/L<0.020 0.50 0.500 25.0Thallium 75 - 1251.8100mg/L

<0.0050 0.50 0.513 25.0Vanadium 75 - 1251.6103mg/L<0.010 0.50 0.549 25.0Zinc 75 - 1252.8110mg/L






Surrogate for Blank % Recovery Control Limits4-Bromofluorobenzene 104 70 125-Dibromofluoromethane 119 70 125-Toluene-d8 106 70 125-










Units<0.50 20 20.81,1-Dichloroethene 70 - 130104g/L<0.50 20 22.8Benzene 70 - 130114g/L<0.50 20 22.4Chlorobenzene 70 - 130112g/L<1.0 20 16.8Methyl-t-butyl Ether 70 - 13084.0g/L




RPD RPD LimitsUnits<0.50 20 20.6 25.01,1-Dichloroethene 70 - 1301.4103g/L<0.50 20 22.3 25.0Benzene 70 - 1302.3111g/L<0.50 20 22.0 25.0Chlorobenzene 70 - 1302.0110g/L<1.0 20 18.2 25.0Methyl-t-butyl Ether 70 - 1307.990.9g/L






Units<25 250 276TPH as Gasoline 65 - 135111g/L



RPD RPD LimitsUnits<25 250 309 25.0TPH as Gasoline 65 - 13511124g/L











Surrogate for Blank % Recovery Control Limits4-Bromofluorobenzene 115 60 130-Dibromofluoromethane 94.1 60 130-Toluene-d8 98.9 60 130-






Units<0.50 20 18.41,1-Dichloroethene 70 - 13091.8g/L<0.50 20 20.7Benzene 70 - 130103g/L<0.50 20 21.9Chlorobenzene 70 - 130110g/L<1.0 20 16.7Methyl-t-butyl Ether 70 - 13083.5g/L




RPD RPD LimitsUnits<0.50 20 18.8 25.01,1-Dichloroethene 70 - 1302.494.1g/L<0.50 20 20.8 25.0Benzene 70 - 1300.45104g/L<0.50 20 21.8 25.0Chlorobenzene 70 - 1300.67109g/L<1.0 20 16.9 25.0Methyl-t-butyl Ether 70 - 1301.484.6g/L






Units<25 250 260TPH as Gasoline 65 - 135104g/L



RPD RPD LimitsUnits<25 250 261 25.0TPH as Gasoline 65 - 1350.73105g/L














RPD RPD LimitsUnits<50 1000 671 25.0TPH as Diesel 40 - 1387.467.1g/L<200 1000 792 25.0TPH as Motor Oil 40 - 1381.879.2g/L






On November01,2006,samples werereceived underchainofcustody foranalysis.

TestM atrix

Novato,CA 94947

Jim Dunn

Comm ents





Issued: 11/03/2006

P.O .Num ber: 285.002.01.014


Solid ICP M etals:EPA 3050B /EPA 6010B

M ercury:EPA 7471B /EPA 245.5

VOCs:EPA 8260B

Entech AnalyticalLabs,Inc.iscertified forenvironmentalanalyses by the StateofCalifornia(#2346).Ifyou have any questions regardingthisreport,please callus at408-588-0200ext.225.

Sincerely,

ErinCunniffeOperations M anager






P.O.Number: 285.002.01.014


Attn: Jim Dunn

ProjectName: Baxter



Lab #: 52235-001 Sam pleID: Q CH 110106N1 M atrix: Solid Sam pleDate: 11/1/2006 11:00AM



M ercury ND mg/Kg0.0501.0 SHG06110211/3/2006SHG06110211/2/2006


Analyzed by:Hdinh


ICP M etals:EPA 3050B /EPA 6010B

Antim ony 5.1 m g/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006

Arsenic ND mg/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006

Barium 62 m g/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006

Beryllium ND mg/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006

Cadm ium 1.9 m g/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006

Chrom ium 270 m g/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006

Cobalt 24 m g/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006

Copper 630 m g/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006

Lead 12 m g/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006

M olybdenum ND mg/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006

Nickel 1600 m g/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006

Selenium ND mg/Kg2.01.0 SM 06110111/2/2006SM 06110111/1/2006

Silver ND mg/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006

Thallium ND mg/Kg2.01.0 SM 06110111/2/2006SM 06110111/1/2006

Vanadium 90 m g/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006

Zinc 320 m g/Kg2.01.0 SM 06110111/2/2006SM 06110111/1/2006

Reviewed by:DQueja

Analyzed by:EQueja


ND = NotDetected atorabove the Detection Lim it.11/3/20065:33:31PM -ECunniffeQual= DataQualifier





P.O.Number: 285.002.01.014


Attn: Jim Dunn

ProjectName: Baxter



Lab #: 52235-002 Sam pleID: Q CH 110106S2 M atrix: Solid Sam pleDate: 11/1/2006 11:10AM



M ercury 0.13 m g/Kg0.0501.0 SHG06110211/3/2006SHG06110211/2/2006


Analyzed by:Hdinh




Arsenic 5.7 m g/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006

Barium 130 m g/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006




Cobalt 17 m g/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006

Copper 210 m g/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006

Lead 18 m g/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006


Nickel 2400 m g/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006





Zinc 130 m g/Kg2.01.0 SM 06110111/2/2006SM 06110111/1/2006

Reviewed by:DQueja

Analyzed by:EQueja







P.O.Number: 285.002.01.014


Attn: Jim Dunn

ProjectName: Baxter



Lab #: 52235-003 Sam pleID: Q CH 110106R M atrix: Solid Sam pleDate: 11/1/2006 11:15AM





Analyzed by:Hdinh




Arsenic 15 m g/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006

Barium 81 m g/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006


Cadm ium ND mg/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006


Cobalt 8.2 m g/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006

Copper 17 m g/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006

Lead 17 m g/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006


Nickel 34 m g/Kg1.01.0 SM 06110111/2/2006SM 06110111/1/2006





Zinc 48 m g/Kg2.01.0 SM 06110111/2/2006SM 06110111/1/2006

Reviewed by:DQueja

Analyzed by:EQueja







P.O.Number: 285.002.01.014


Attn: Jim Dunn

ProjectName: Baxter



Lab #: 52235-004 Sam pleID: SC1101-1 M atrix: Solid Sam pleDate: 11/1/2006 1:57PM


VO Cs:EPA 8260B

1,1,1,2-Tetrachloroethane ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

1,1,1-Trichloroethane ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A



1,1-Dichloroethane ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

1,1-Dichloroethene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

1,1-Dichloropropene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

1,2,3-Trichlorobenzene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

1,2,3-Trichloropropane ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A


1,2,4-Trim ethylbenzene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

1,2-Dibrom o-3-Chloropropane ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

1,2-Dibrom oethane (EDB) ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

1,2-Dichlorobenzene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A


1,2-Dichloropropane ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A





1,4-Dioxane ND µg/Kg1600.82 SM 306110111/1/2006N/AN/A


2-Butanone (M EK) ND µg/Kg330.82 SM 306110111/1/2006N/AN/A

2-Chloroethyl-vinylEther ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

2-Chlorotoluene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

2-Hexanone ND µg/Kg330.82 SM 306110111/1/2006N/AN/A


4-M ethyl-2-Pentanone(M IBK) ND µg/Kg330.82 SM 306110111/1/2006N/AN/A

Acetone ND µg/Kg820.82 SM 306110111/1/2006N/AN/A

Acetonitrile ND µg/Kg330.82 SM 306110111/1/2006N/AN/A

Acrolein ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Acrylonitrile ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Benzene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

BenzylChloride ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Brom obenzene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Brom ochlorom ethane ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Brom odichlorom ethane ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Brom oform ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Brom om ethane ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Carbon Disulfide ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Carbon Tetrachloride ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Chlorobenzene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Chloroethane ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Chloroform ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Chlorom ethane ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A







P.O.Number: 285.002.01.014


Attn: Jim Dunn

ProjectName: Baxter





VO Cs:EPA 8260B

cis-1,2-Dichloroethene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

cis-1,3-Dichloropropene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Cyclohexanone ND µg/Kg330.82 SM 306110111/1/2006N/AN/A

Dibrom ochlorom ethane ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Dibrom om ethane ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Dichlorodifluorom ethane ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

DiisopropylEther ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

EthylBenzene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Freon 113 ND µg/Kg8.20.82 SM 306110111/1/2006N/AN/A

Hexachlorobutadiene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Iodom ethane ND µg/Kg8.20.82 SM 306110111/1/2006N/AN/A

Isopropanol ND µg/Kg820.82 SM 306110111/1/2006N/AN/A

Isopropylbenzene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

M ethyl-t-butylEther ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

M ethylene Chloride ND µg/Kg410.82 SM 306110111/1/2006N/AN/A

n-Butylbenzene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

n-Propylbenzene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Naphthalene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

p-Isopropyltoluene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Pentachloroethane ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

sec-Butylbenzene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Styrene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

tert-Am ylM ethylEther ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

tert-Butanol(TBA) ND µg/Kg330.82 SM 306110111/1/2006N/AN/A

tert-ButylEthylEther ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

tert-Butylbenzene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Tetrachloroethene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Tetrahydrofuran ND µg/Kg330.82 SM 306110111/1/2006N/AN/A

Toluene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

trans-1,2-Dichloroethene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

trans-1,3-Dichloropropene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

trans-1,4-Dichloro-2-butene ND µg/Kg8.20.82 SM 306110111/1/2006N/AN/A

Trichloroethene ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Trichlorofluorom ethane ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

VinylAcetate ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

VinylChloride ND µg/Kg4.10.82 SM 306110111/1/2006N/AN/A

Xylenes,Total ND µg/Kg8.20.82 SM 306110111/1/2006N/AN/A


Analyzed by:M felixSurrogate SurrogateRecovery ControlLim its(% )



Toluene-d8 99.1 60 130-







P.O.Number: 285.002.01.014


Attn: Jim Dunn

ProjectName: Baxter





VO Cs:EPA 8260B




















































P.O.Number: 285.002.01.014


Attn: Jim Dunn

ProjectName: Baxter





VO Cs:EPA 8260B










































Toluene-d8 85.1 60 130-







P.O.Number: 285.002.01.014


Attn: Jim Dunn

ProjectName: Baxter





VO Cs:EPA 8260B




















































P.O.Number: 285.002.01.014


Attn: Jim Dunn

ProjectName: Baxter





VO Cs:EPA 8260B










































Toluene-d8 89.3 60 130-







P.O.Number: 285.002.01.014


Attn: Jim Dunn

ProjectName: Baxter





VO Cs:EPA 8260B

1,1,1,2-Tetrachloroethane ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

1,1,1-Trichloroethane ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006



1,1-Dichloroethane ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

1,1-Dichloroethene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

1,1-Dichloropropene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

1,2,3-Trichlorobenzene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

1,2,3-Trichloropropane ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006


1,2,4-Trim ethylbenzene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

1,2-Dibrom o-3-Chloropropane ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

1,2-Dibrom oethane (EDB) ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

1,2-Dichlorobenzene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006


1,2-Dichloropropane ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006





1,4-Dioxane ND µg/Kg810040 PM 061102P11/2/2006PM 061102P11/2/2006


2-Butanone (M EK) ND µg/Kg160040 PM 061102P11/2/2006PM 061102P11/2/2006

2-Chloroethyl-vinylEther ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

2-Chlorotoluene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

2-Hexanone ND µg/Kg160040 PM 061102P11/2/2006PM 061102P11/2/2006


4-M ethyl-2-Pentanone(M IBK) ND µg/Kg160040 PM 061102P11/2/2006PM 061102P11/2/2006

Acetone ND µg/Kg400040 PM 061102P11/2/2006PM 061102P11/2/2006

Acetonitrile ND µg/Kg160040 PM 061102P11/2/2006PM 061102P11/2/2006

Acrolein ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Acrylonitrile ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Benzene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

BenzylChloride ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Brom obenzene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Brom ochlorom ethane ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Brom odichlorom ethane ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Brom oform ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Brom om ethane ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Carbon Disulfide ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Carbon Tetrachloride ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Chlorobenzene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Chloroethane ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Chloroform ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Chlorom ethane ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006







P.O.Number: 285.002.01.014


Attn: Jim Dunn

ProjectName: Baxter





VO Cs:EPA 8260B

cis-1,2-Dichloroethene 2200 µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

cis-1,3-Dichloropropene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Cyclohexanone ND µg/Kg160040 PM 061102P11/2/2006PM 061102P11/2/2006

Dibrom ochlorom ethane ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Dibrom om ethane ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Dichlorodifluorom ethane ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

DiisopropylEther ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

EthylBenzene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Freon 113 ND µg/Kg40040 PM 061102P11/2/2006PM 061102P11/2/2006

Hexachlorobutadiene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Iodom ethane ND µg/Kg40040 PM 061102P11/2/2006PM 061102P11/2/2006

Isopropanol ND µg/Kg400040 PM 061102P11/2/2006PM 061102P11/2/2006

Isopropylbenzene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

M ethyl-t-butylEther ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

M ethylene Chloride ND µg/Kg200040 PM 061102P11/2/2006PM 061102P11/2/2006

n-Butylbenzene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

n-Propylbenzene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Naphthalene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

p-Isopropyltoluene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Pentachloroethane ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

sec-Butylbenzene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Styrene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

tert-Am ylM ethylEther ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

tert-Butanol(TBA) ND µg/Kg160040 PM 061102P11/2/2006PM 061102P11/2/2006

tert-ButylEthylEther ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

tert-Butylbenzene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Tetrachloroethene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Tetrahydrofuran ND µg/Kg160040 PM 061102P11/2/2006PM 061102P11/2/2006

Toluene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

trans-1,2-Dichloroethene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

trans-1,3-Dichloropropene ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

trans-1,4-Dichloro-2-butene ND µg/Kg40040 PM 061102P11/2/2006PM 061102P11/2/2006

Trichloroethene 530 µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Trichlorofluorom ethane ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

VinylAcetate ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

VinylChloride ND µg/Kg20040 PM 061102P11/2/2006PM 061102P11/2/2006

Xylenes,Total ND µg/Kg40040 PM 061102P11/2/2006PM 061102P11/2/2006





Toluene-d8 103 60 130-







P.O.Number: 285.002.01.014


Attn: Jim Dunn

ProjectName: Baxter





VO Cs:EPA 8260B




















































P.O.Number: 285.002.01.014


Attn: Jim Dunn

ProjectName: Baxter





VO Cs:EPA 8260B










































Toluene-d8 87.9 60 130-





Validated by: M aiChiTu -11/02/06Q C/Prep Batch ID: PM 061102P



M ethod Blank - Solid - VO Cs:EPA 8260B

1,1,1,2-Tetrachloroethane ND 50 µg/Kg250

1,1,1-Trichloroethane ND 50 µg/Kg250



1,1-Dichloroethane ND 50 µg/Kg250

1,1-Dichloroethene ND 50 µg/Kg250

1,1-Dichloropropene ND 50 µg/Kg250

1,2,3-Trichlorobenzene ND 50 µg/Kg250

1,2,3-Trichloropropane ND 50 µg/Kg250


1,2,4-Trim ethylbenzene ND 50 µg/Kg250

1,2-Dibrom o-3-Chloropropane ND 50 µg/Kg250

1,2-Dibrom oethane (EDB) ND 50 µg/Kg250

1,2-Dichlorobenzene ND 50 µg/Kg250


1,2-Dichloropropane ND 50 µg/Kg250





1,4-Dioxane ND 50 µg/Kg10000


2-Butanone (M EK) ND 50 µg/Kg2000

2-Chloroethyl-vinylEther ND 50 µg/Kg250

2-Chlorotoluene ND 50 µg/Kg250

2-Hexanone ND 50 µg/Kg2000


4-M ethyl-2-Pentanone(M IBK) ND 50 µg/Kg2000

Acetone ND 50 µg/Kg5000

Acetonitrile ND 50 µg/Kg2000

Acrolein ND 50 µg/Kg250

Acrylonitrile ND 50 µg/Kg250

Benzene ND 50 µg/Kg250

BenzylChloride ND 50 µg/Kg250

Brom obenzene ND 50 µg/Kg250

Brom ochlorom ethane ND 50 µg/Kg250

Brom odichlorom ethane ND 50 µg/Kg250

Brom oform ND 50 µg/Kg250

Brom om ethane ND 50 µg/Kg250

Carbon Disulfide ND 50 µg/Kg250

Carbon Tetrachloride ND 50 µg/Kg250

Chlorobenzene ND 50 µg/Kg250

Chloroethane ND 50 µg/Kg250

Chloroform ND 50 µg/Kg250

Chlorom ethane ND 50 µg/Kg250

cis-1,2-Dichloroethene ND 50 µg/Kg250

cis-1,3-Dichloropropene ND 50 µg/Kg250

Cyclohexanone ND 50 µg/Kg2000

Dibrom ochlorom ethane ND 50 µg/Kg250

Dibrom om ethane ND 50 µg/Kg250

QCReport-ECunniffe -11/3/2006 5:33:46 PM


Validated by: M aiChiTu -11/02/06Q C/Prep Batch ID: PM 061102P




Dichlorodifluorom ethane ND 50 µg/Kg250

DiisopropylEther ND 50 µg/Kg250

EthylBenzene ND 50 µg/Kg250

Freon 113 ND 50 µg/Kg500

Hexachlorobutadiene ND 50 µg/Kg250

Iodom ethane ND 50 µg/Kg500

Isopropanol ND 50 µg/Kg5000

Isopropylbenzene ND 50 µg/Kg250

M ethylene Chloride ND 50 µg/Kg2500

M ethyl-t-butylEther ND 50 µg/Kg250

Naphthalene ND 50 µg/Kg250

n-Butylbenzene ND 50 µg/Kg250

n-Propylbenzene ND 50 µg/Kg250

Pentachloroethane ND 50 µg/Kg250

p-Isopropyltoluene ND 50 µg/Kg250

sec-Butylbenzene ND 50 µg/Kg250

Styrene ND 50 µg/Kg250

tert-Am ylM ethylEther ND 50 µg/Kg250

tert-Butanol(TBA) ND 50 µg/Kg2000

tert-ButylEthylEther ND 50 µg/Kg250

tert-Butylbenzene ND 50 µg/Kg250

Tetrachloroethene ND 50 µg/Kg250

Tetrahydrofuran ND 50 µg/Kg2000

Toluene ND 50 µg/Kg250

trans-1,2-Dichloroethene ND 50 µg/Kg250

trans-1,3-Dichloropropene ND 50 µg/Kg250

trans-1,4-Dichloro-2-butene ND 50 µg/Kg500

Trichloroethene ND 50 µg/Kg250

Trichlorofluorom ethane ND 50 µg/Kg250

VinylAcetate ND 50 µg/Kg250

VinylChloride ND 50 µg/Kg250

Xylenes,Total ND 50 µg/Kg500




Toluene-d8 102 60 130-



Reviewed by: M aiChiTu -11/02/06Q C Batch ID: PM 061102P


LCS /LCSD - Solid - VOCs:EPA 8260B


Units

<5.0 2000 24901,1-Dichloroethene 70 -135124µg/Kg

<5.0 2000 2420Benzene 70 -135121µg/Kg

<5.0 2000 2260Chlorobenzene 70 -135113µg/Kg

<5.0 2000 1740M ethyl-t-butylEther 70 -13587.0µg/Kg

<5.0 2000 2110Toluene 70 -135106µg/Kg

<5.0 2000 2130Trichloroethene 70 -135106µg/Kg




Toluene-d8 107.0 60 130-



<5.0 2000 2400 30.01,1-Dichloroethene 70 -1353.7120µg/Kg

<5.0 2000 2480 30.0Benzene 70 -1352.4124µg/Kg

<5.0 2000 2240 30.0Chlorobenzene 70 -1350.89112µg/Kg

<5.0 2000 1760 30.0M ethyl-t-butylEther 70 -1351.188.0µg/Kg

<5.0 2000 2140 30.0Toluene 70 -1351.4107µg/Kg

<5.0 2000 2090 30.0Trichloroethene 70 -1351.9104µg/Kg




Toluene-d8 106.0 60 130-



Validated by: M aiChiTu -11/02/06Q C Batch ID: SM 3061101

Q C Batch Analysis Date: 11/1/2006



1,1,1,2-Tetrachloroethane ND 1 µg/Kg5.0

1,1,1-Trichloroethane ND 1 µg/Kg5.0



1,1-Dichloroethane ND 1 µg/Kg5.0

1,1-Dichloroethene ND 1 µg/Kg5.0

1,1-Dichloropropene ND 1 µg/Kg5.0

1,2,3-Trichlorobenzene ND 1 µg/Kg5.0

1,2,3-Trichloropropane ND 1 µg/Kg5.0


1,2,4-Trim ethylbenzene ND 1 µg/Kg5.0

1,2-Dibrom o-3-Chloropropane ND 1 µg/Kg5.0

1,2-Dibrom oethane (EDB) ND 1 µg/Kg5.0

1,2-Dichlorobenzene ND 1 µg/Kg5.0


1,2-Dichloropropane ND 1 µg/Kg5.0








2-Chloroethyl-vinylEther ND 1 µg/Kg5.0

2-Chlorotoluene ND 1 µg/Kg5.0






Acrolein ND 1 µg/Kg5.0

Acrylonitrile ND 1 µg/Kg5.0

Benzene ND 1 µg/Kg5.0

BenzylChloride ND 1 µg/Kg5.0

Brom obenzene ND 1 µg/Kg5.0

Brom ochlorom ethane ND 1 µg/Kg5.0

Brom odichlorom ethane ND 1 µg/Kg5.0

Brom oform ND 1 µg/Kg5.0

Brom om ethane ND 1 µg/Kg5.0

Carbon Disulfide ND 1 µg/Kg5.0

Carbon Tetrachloride ND 1 µg/Kg5.0

Chlorobenzene ND 1 µg/Kg5.0

Chloroethane ND 1 µg/Kg5.0

Chloroform ND 1 µg/Kg5.0

Chlorom ethane ND 1 µg/Kg5.0

cis-1,2-Dichloroethene ND 1 µg/Kg5.0

cis-1,3-Dichloropropene ND 1 µg/Kg5.0


Dibrom ochlorom ethane ND 1 µg/Kg5.0

Dibrom om ethane ND 1 µg/Kg5.0







Dichlorodifluorom ethane ND 1 µg/Kg5.0

DiisopropylEther ND 1 µg/Kg5.0

EthylBenzene ND 1 µg/Kg5.0


Hexachlorobutadiene ND 1 µg/Kg5.0



Isopropylbenzene ND 1 µg/Kg5.0


M ethyl-t-butylEther ND 1 µg/Kg5.0

Naphthalene ND 1 µg/Kg5.0

n-Butylbenzene ND 1 µg/Kg5.0

n-Propylbenzene ND 1 µg/Kg5.0

Pentachloroethane ND 1 µg/Kg5.0

p-Isopropyltoluene ND 1 µg/Kg5.0

sec-Butylbenzene ND 1 µg/Kg5.0

Styrene ND 1 µg/Kg5.0

tert-Am ylM ethylEther ND 1 µg/Kg5.0


tert-ButylEthylEther ND 1 µg/Kg5.0

tert-Butylbenzene ND 1 µg/Kg5.0

Tetrachloroethene ND 1 µg/Kg5.0


Toluene ND 1 µg/Kg5.0

trans-1,2-Dichloroethene ND 1 µg/Kg5.0

trans-1,3-Dichloropropene ND 1 µg/Kg5.0


Trichloroethene ND 1 µg/Kg5.0

Trichlorofluorom ethane ND 1 µg/Kg5.0

VinylAcetate ND 1 µg/Kg5.0

VinylChloride ND 1 µg/Kg5.0





Toluene-d8 106 60 130-



Reviewed by: M aiChiTu -11/02/06Q C Batch ID: SM 3061101




Units

<5.0 40 43.51,1-Dichloroethene 70 -135109µg/Kg

<5.0 40 45.8Benzene 70 -135114µg/Kg

<5.0 40 44.6Chlorobenzene 70 -135112µg/Kg

<5.0 40 32.6M ethyl-t-butylEther 70 -13581.5µg/Kg

<5.0 40 41.2Toluene 70 -135103µg/Kg

<5.0 40 40.8Trichloroethene 70 -135102µg/Kg




Toluene-d8 100.0 60 130-



<5.0 40 44.0 30.01,1-Dichloroethene 70 -1351.1110µg/Kg

<5.0 40 43.9 30.0Benzene 70 -1354.2110µg/Kg

<5.0 40 43.5 30.0Chlorobenzene 70 -1352.5109µg/Kg

<5.0 40 31.4 30.0M ethyl-t-butylEther 70 -1353.878.5µg/Kg

<5.0 40 40.2 30.0Toluene 70 -1352.5100µg/Kg

<5.0 40 39.6 30.0Trichloroethene 70 -1353.099.0µg/Kg




Toluene-d8 91.0 60 130-



Reviewed by: JISIDERIO -11/03/06Q C Batch ID: SHG 061102


LCS /LCSD - Solid - M ercury:EPA 7471B /EPA 245.5


Units

<0.050 0.20 0.218M ercury 75 -125109m g/Kg



<0.050 0.20 0.192 30.0M ercury 75 -1251396.0m g/Kg



Reviewed by: JISIDERIO -11/03/06Q C/Prep Batch ID: SHG 061102


M S /M SD - Solid - M ercury:EPA 7471B /EPA 245.5

Param eter

Sam pleResult

SpikeAm ount


Recovery Lim its

AnalysisDate


0.223 0.40 0.691M ercury 75 -12511/2/2006m g/Kg 117

Param eter

Sam pleResult

SpikeAm ount


Recovery Lim its

AnalysisDate


RPD RPD Lim its

M SD

0.223 0.40 0.658 30.0M ercury 75 -12511/2/2006m g/Kg 4.9109



Reviewed by: DQueja -11/02/06Q C Batch ID: SM 061101


LCS /LCSD - Solid - ICP M etals:EPA 3050B /EPA 6010B


Units

<1.0 50 48.7Antim ony 75 -12597.3m g/Kg

<1.0 50 46.2Arsenic 75 -12592.4m g/Kg

<1.0 50 50.9Barium 75 -125102m g/Kg

<1.0 50 47.9Beryllium 75 -12595.8m g/Kg

<1.0 50 47.3Cadm ium 75 -12594.5m g/Kg

<1.0 50 48.8Chrom ium 75 -12597.5m g/Kg

<1.0 50 49.4Cobalt 75 -12598.8m g/Kg

<1.0 50 49.6Copper 75 -12599.2m g/Kg

<1.0 50 48.9Lead 75 -12597.9m g/Kg

<1.0 50 49.5M olybdenum 75 -12599.0m g/Kg

<1.0 50 48.6Nickel 75 -12597.2m g/Kg

<2.0 50 43.3Selenium 75 -12586.6m g/Kg

<1.0 50 48.3Silver 75 -12596.5m g/Kg

<2.0 50 44.8Thallium 75 -12589.5m g/Kg

<1.0 50 49.9Vanadium 75 -12599.7m g/Kg

<2.0 50 48.1Zinc 75 -12596.3m g/Kg



<1.0 50 48.5 25.0Antim ony 75 -1250.3697.0m g/Kg

<1.0 50 46.3 25.0Arsenic 75 -1250.2192.6m g/Kg

<1.0 50 50.3 25.0Barium 75 -1251.1101m g/Kg

<1.0 50 47.5 25.0Beryllium 75 -1250.8395.0m g/Kg

<1.0 50 46.3 25.0Cadm ium 75 -1252.192.5m g/Kg

<1.0 50 47.6 25.0Chrom ium 75 -1252.395.2m g/Kg

<1.0 50 48.3 25.0Cobalt 75 -1252.396.6m g/Kg

<1.0 50 48.8 25.0Copper 75 -1251.597.7m g/Kg

<1.0 50 48.8 25.0Lead 75 -1250.2597.6m g/Kg

<1.0 50 49.1 25.0M olybdenum 75 -1250.7298.3m g/Kg

<1.0 50 47.4 25.0Nickel 75 -1252.594.8m g/Kg

<2.0 50 43.2 25.0Selenium 75 -1250.2286.4m g/Kg

<1.0 50 47.9 25.0Silver 75 -1250.7295.8m g/Kg

<2.0 50 45.1 25.0Thallium 75 -1250.7290.2m g/Kg

<1.0 50 48.5 25.0Vanadium 75 -1252.797.0m g/Kg

<2.0 50 48.6 25.0Zinc 75 -1250.9197.2m g/Kg


PES ENVIRONMENTAL, inc. CHAIN OF CUSTODY RECORD 1682 NOVATO BOULEVARD, SUITE 100

Engineering & Environmental Services NOVATO, CALIFORNIA 94947 (41 5) 899-1600 FAX 1415) 899-1 601





TestM atrix

Novato,CA 94947

Jim Dunn

Comm ents





Issued: 11/03/2006

P.O .Num ber: 285-002-01-013



VOCs:EPA 8260B

Hold


Sincerely,







P.O.Number: 285-002-01-013

Attn: Jim Dunn

ProjectName: Baxter



Lab #: 52255-001 Sam pleID: SC1102-1 M atrix: Solid Sam pleDate: 11/2/2006 7:50AM


VO Cs:EPA 8260B




















































P.O.Number: 285-002-01-013

Attn: Jim Dunn

ProjectName: Baxter





VO Cs:EPA 8260B

cis-1,2-Dichloroethene 7.2 µg/Kg5.81.2 SM 306110311/3/2006N/AN/A








Freon 113 ND µg/Kg121.2 SM 306110311/3/2006N/AN/A


Iodom ethane ND µg/Kg121.2 SM 306110311/3/2006N/AN/A





















trans-1,4-Dichloro-2-butene ND µg/Kg121.2 SM 306110311/3/2006N/AN/A

Trichloroethene 13 µg/Kg5.81.2 SM 306110311/3/2006N/AN/A




Xylenes,Total ND µg/Kg121.2 SM 306110311/3/2006N/AN/A





Toluene-d8 102 60 130-


