4> gei consultants inc.mr. bob mullin gei consultants/nh suffolk building 53 regional drive concord,...

4> GEI Consultants, Inc.

MANAGEMENT OF MIGRATION WATER QUALITY MONITORING PROGRAM QUARTER 9 REPORT

VOLUME 2.3

APPENDIX F - Q9 NET ANALYTICAL REPORTS

Tinkham Garage Site Londonderry, New Hampshire

Prepared for:

THE CANNONS SITES GROUP

Submitted by:

GEI Consultants, Inc.

Robert A. Mullin, P.E. Project Manager

53 Regional Drive Concord, New Hampshire(800)678-1502

Project 92113 July 31,1996

Analytical Report

NET: FD Case 1855 5 ml. PURGE METHOD 624

Cambridge Division NATIONAL 12 Oak Park Bedford, MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET TESTING, INC. Fax: (617) 275-7411

June 5, 1996

:n&,Mr. Bob Mullin GEI Consultants/NH Suffolk Building 53 Regional Drive Concord, NH 03301

RE: Tinkham Garage

Dear Mr. Mullin:

Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1855, NET job number 96.01770).

This narrative addresses all comments for all samples as listed below:

NET JOB NUMBER: 96.01770

SAMPLE NET DATE TIME DATE ID ID TAKEN TAKEN REC'D MATRIX

92113-NAI-M2-0596 148533 05/20/1996 10:10 05/21/1996 GROUND WATER 92113-NAI-I-0596 148534 05/20/1996 10:45 05/21/1996 GROUND WATER 92113-FU260-0596 148535 05/20/1996 10:50 05/21/1996 GROUND WATER 92113-NAI-K1-0596 148536 05/20/1996 10:45 05/21/1996 GROUND WATER 92113-NAI-C1-0596 148537 05/20/1996 11:00 05/21/1996 GROUND WATER 92113-FU09-0596 148538 05/20/1996 09:15 05/21/1996 GROUND WATER 921 13-NAI-A1 -0596 148539 05/20/1996 10:45 05/21/1996 GROUND WATER 92113-NAI-C3-0596 148540 05/20/1996 13:15 05/21/1996 GROUND WATER

CEAitfN

Cambridge Division NATIONAL 12 Oak Park Bedford, MA 01730 ENVIRONMENTAL Tel (617) 275-3535 NET TESTING, INC. Fax (617) 275-7411

All laboratory comments for the data packages have been summarized in the following tables:

Sample Receipt and Login TABLE 1 Metals and Cyanide Analyses No Analyses Requested Volatile Organics Analyses TABLE 3 Semi-Volatile Organics Analyses No Analyses Requested

Pesticide/PCB Organics Analyses No Analyses Requested

Herbicides Analyses No Analyses Requested

General Chemistry Analyses No Analyses Requested

These narrative tables are also enclosed with each data package section.

Please find enclosed a diskette of the results for this case.

Thank you for this opportunity to be of service to you. Please do not hesitate to call or write if you have any questions or require further information.

Sincerely,

Peter M. Conroy Project Manager

enclosures

TABLE 1 SAMPLE RECEIPT & LOGIN

FD1855

GENERAL COMMENTS: No comments were necessary.

TABLES VOLATILES ORGANICS NARRATIVE SUMMARY

FD 1855

GENERAL COMMENTS: The samples were analyzed using method 624. Data forms were produced using our CLP forms software.

Due to software constraints the "92113's" were dropped from the CLIENT ID'S.

MANUAL INTEGRATIONS: Manual integrations are performed on standards and samples when the integration is not complete due to peak shape and chromatography. This is confirmed by visual inspection by the analysts. The "M" flag indicates that a manual integration has been performed.

Compound Total 1,2-Dichloroethene must be integrated in the initial and continuing calibration standards to include the total area of the cis- and trans- isomers.

SURROGATES: All system monitoring compound recoveries were within the contract required QC limits.

MATRIX SPIKE/MATRIX SPIKE DUPLICATE: No site specific MS/MSD was requested by the Client for this SDG.

BLANKS: A method blank was analyzed for each twelve hour time period on each GC/MS system used for analysis. No blank contained greater than five times the reporting limit of Methylene Chloride, Acetone, and 2-Butanone, or greater than or equal to the reporting limit of any other volatile target compound.

TUNE: All instrument performance check criteria were met prior to the start of sample analysis.

CALIBRATION: All compounds met the minimum RF's and maximum RPD's or %D.

INTERNAL STANDARDS: All internal standard areas and retention times were within the QC limits.

HOLDING TIMES: All samples were analyzed within required holding times.

DILUTIONS: The following dilution was necessary:

CLIENT ID NET ID DILUTION NAIC30596 148540 1:2

ANALYTICAL REPORT

Report To: Mr. Bob Mullin GEI Consultants/NH Suffolk Building 53 Regional Drive Concord, NH 03301

Project: Tinkham Garage

FD Case 1855

Section One

NET Job Number: 96.01770

National Environmental Testing, Inc.

Cambridge Division 12 Oak Park

Bedford, MA 01730

Massachusetts Certification Number H MA023

TABLE OF CONTENTS

Page Number Section 1- Report Front

1A. Table of Contents ..............

IB. Narrative/Cover Letter .........

1C. Main Page/Sample Cross Reference ............

ID. Chain of Custody Forms .........

IE. Sample Receipt Logbook .........

IF. Data Qualifier/Flag Descriptions

1G. Document Inventory Sheets ......

1H. Control Charts .................

Section 2. Metals Analysis Data ................. To Be Submitted

Section 3. Volatiles Analysis Data .............. 30000

Section 4. Semi -Volatiles Analysis Data ......... No Analysis Requested

Section 5. Pesticides/PCBs Analysis Data ........ No Analysis Requested

Section 6. Herbicide Analysis Data .............. No Analysis Requested

Section 1 . General Chemistry Analysis Data ...... No Analysis Requested

10001

Cambridge Division NATIONAL 12 Oak Park Bedford, MA 01730 ENVIRONMENTAL Tel (617)275-3535 TESTING, INC. Fax (617) 275-7411 NET

June 5, 1996

Mr. Bob Mullin 6EI Consultants/NH Suffolk Building 53 Regional Drive

Concord, NH 03301

RE: Tinkham Garage

Dear Mr. Mullin:

Enclosed please find the results of the chemical analyses performed by NET Cambridge Division for the Tinkham Garage project (FD Case 1855, NET job number 96.01770).

This narrative addresses all comments for all samples as listed below:

NET JOB NUMBER: 96.01770


92113-NAI-M2-0596 148533 05/20/1996 10:10 05/21/1996 GROUND WATER 92113-NAI-I-0596 148534 05/20/1996 10:45 05/21/1996 GROUND WATER 921 13- FW2 60- 0596 148535 05/20/1996 10:50 05/21/1996 GROUND WATER 92113-NAI-K1-0596 148536 05/20/1996 10:45 05/21/1996 GROUND WATER 92113-NAI-C1-0596 148537 05/20/1996 11:00 05/21/1996 GROUND WATER 92113-FU09-0596 148538 05/20/1996 09:15 05/21/1996 GROUND WATER 921 13-NAI-A1 -0596 148539 05/20/1996 10:45 05/21/1996 GROUND WATER 92113-NAI-C3-0596 148540 05/20/1996 13:15 05/21/1996 GROUND WATER

10002

Cambridge Division NATIONAL 12 Oak Park Bedford, MA 01730 ENVIRONMENTAL Tel. (617) 275-3535 NET TESTING, INC. Fax: (617) 275-7411

All laboratory comments for the data packages have been summarized in the following tables:

Sample Receipt and Login TABLE 1 Metals and Cyanide Analyses No Analyses Requested Volatile Organics Analyses TABLE 3 Semi-Volatile Organics Analyses No Analyses Requested Pesticide/PCB Organics Analyses No Analyses Requested

Herbicides Analyses No Analyses Requested

General Chemistry Analyses No Analyses Requested

These narrative tables are also enclosed with each data package section.

Please find enclosed a diskette of the results for this case.

Thank you for this opportunity to be of service to you. Please do not hesitate to call or write if you have any questions or require further information.

Sincerely,

Y

Peter M. Conroy^ Project Manager

enclosures

10003

TABLE 1 SAMPLE RECEIPT & LOGIN

FD1855

GENERAL COMMENTS: No comments were necessary.

10004

TABLE 3 VOLATILES ORGANICS NARRATIVE SUMMARY

FD 1855







BLANKS: A method blank was analyzed for each twelve hour time period on each GC/MS system used for analysis. No blank contained greater than five times the reporting limit of Methylene Chloride, Acetone, and 2-Butanone, or greater than or equal to the reporting limit of any other volatile target compound.



-INTERNAL STANDARDS: All internal standard areas and retention times were within the QC limits.

10005




1000S

NET Cambridge Division

ANALYTICAL REPORT

Report To: Reported By:

Mr. Bob Mull in National Environmental Testing GEI Consultants/NH NET Atlantic, Incorporated Suffolk Building Cambridge Division 53 Regional Drive 12 Oak Park Concord, NH 03301 Bedford, MA 01730

Report Date: 06/05/1996 NET Job Number: 96.01770

Project: Tinkham Garage NET Client No: 14755

P.O. No: 8307 Collected By: R.Van Etten Shipped Via: FedEx

Job Description: Tinkham Airbill No:

This report has been approved and certified for release by the following staff. Please feel free to call the NET Project Manager at 617-275-3535 with any questions or comments.

Peter M. Conroy Reporrt prepared NET Project Manager NET Reports Group'

Analytical data for the following samples are included in this data report.


92113-NAI-M2-0596 148533 05/20/1996 10:10 05/21/1996 GROUND WATER 92113-NAI-I-0596 148534 05/20/1996 10:45 05/21/1996 GROUND WATER 92113-FU26D-0596 148535 05/20/1996 10:50 05/21/1996 GROUND WATER 921 13-NAI-K1 -0596 148536 05/20/1996 10:45 05/21/1996 GROUND WATER 92113-NAI-C1-0596 148537 05/20/1996 11:00 05/21/1996 GROUND WATER 92113-FW09-0596 148538 05/20/1996 09:15 05/21/1996 GROUND WATER 921 13-NAI-A1 -0596 148539 05/20/1996 10:45 05/21/1996 GROUND WATER 92113-NAI-C3-0596 148540 05/20/1996 13:15 05/21/1996 GROUND WATER

10007

ORGANIC FLAGS AND SAMPLE SUFFIXES

The following qualifiers have been used for reporting results:

B - The "B" flag indicates that the analyte was found in the associated blank as well as in the sample.

E - The "E" flag indentifies compound concentrations that exceed the calibration range of the GC/MS instrument. For Benzo (b) and Benzo (k) Flouranthene, the calibration range of each peak will be considered separately. Ortho, para, and meta xylene are quantified as two peaks, the calibration range of each peak will be considered separately.

D - If a sample is re-analyzed due to high concentrations and both the original analysis and re-analysis have been reported, the diluted analysis will have the "DL" suffix. All concentration values reported for the diluted analysis will be flagged with a "D".

U - The "U" flag indicates that the compound was analyzed for but not detected. The reported "U" value is the detection limit for the given compound. The value is corrected for dilution and for percent moisture.

J - The "J" flag indicates an estimated value. The flag is used for tentatively identified compounds where a 1:1 response is assumed, or when the mass spectral or chromatographic data indicate the presence of a compound that meets the identification criteria but the quantitated value is less than the method quantitation limit.

P - The "P" flag indicates that the quantitated value of a target pesticide/PCB differs by more than 25% on the two GC columns that were reported.

Y - Compound values that are flagged with a "Y" have been edited on our RTE/MS data system.

X - Compound values that are flagged with a "X" have been edited on our Foremaster data reporting system.

The following sample suffixes have been used:

XXXXX = sample number XXXXXMS = matrix spike sample XXXXXMSD = matrix spike duplicate sample XXXXXRE = re-analyzed sample XXXXXDL = sample analyzed at a secondary dilution

10009

EPA CLP 3/90 Deliverables Inventory

Project Name: GEI Consultants/NH NET Job Numbers: 96.01770 FD Number: FD 1855

ITEM

Tinkham Garage

PAGE

3. GCMS VOLATILE ORGANIC ANALYSIS DATA 0000

3A. 3B. 3C.

PC Summary -Forms II, III, IV, V Sample Data -Forms I, Ib, Raw Data Standards Data -Forms VI, VII, VIII, Raw Data

0001 0013 0095

3D. 3D1. 3D2. 3D4. 3D4.

Raw OC Data BFB Tunes Blank Data -Form I, Matrix Spike Raw Data Matrix Spike Duplicate

Ib, Raw Data

Raw Data

0129 0142

NR NR

10010

ANALYTICAL REPORT

Report To: Mr. Bob Mullin GEI Consultants/NH

Suffolk Building 53 Regional Drive

Concord, NH 03301

Project: Tinkham Garage

FD Case 1855

Section Three Volatiles Analysis

NET Job Number: 96.01770

National Environmental Testing, Inc.

Cambridge Division 12 Oak Park

Bedford, MA 01730

Massachusetts Certification Number M HA023

TABLE 3

VOLATILES ORGANICS NARRATIVE SUMMARY

FD 1855







BLANKS: A method blank was analyzed for each twelve hour time period on each GC/MS system used for analysis. No blank contained greater than five times the reporting limit of Methylene Chloride, Acetone, and 2-Butanone, or greater than or equal to the reporting limit of any other volatile target compound..



INTERNAL STANDARDS: All internal standard areas and retention times were within the QC limits.

EPA CLP 3/90 Deliverables Inventory Project Name; GEI Consultants/NH Tinkhain Garage NET Job Numbers: 96.01770 FD Number: FD 1855

ITEM PAGE

3. GCMS VOLATILE ORGANIC ANALYSIS DATA 0000

3A. QC Summary -Forms II, III, IV, V 0001 3B. Sample Data -Forms I, Ib, Raw Data 0013 3C. Standards Data -Forms VI, VII, VIII, Raw Data 0095

3D. Raw PC Data 3D1. •BFB Tunes 0129 3D2. Blank Data -Form I, Ib, Raw Data 0142 3D4. Matrix Spike Raw Data NR 3D4. Matrix Spike Duplicate Raw Data NR

3. VOLATILES DATA

76.0/770

30000

3A. QC SUMMARY

30001

2A WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY

Lab Name: NET CAMBRIDGE Contract: GEI

Lab Code: CAMBRG Case No.: SAS No.: SDG No.: 1855

EPA SMC1 SMC2 SMC3 OTHER TOT SAMPLE NO. (TOL)# (BFB)# (DCE)# OUT

VBLK0529K 108 106 108 0 02 NAIM20596 98 96 94 0 03 NAII0596 102 102 106 0

VBLK0530K 92 92 92 0 05 FW26D0596 101 103 95 0 06 NAIK10596 104 106 97 0 07 NAIC10596 108 108 103 0 08 FW090596 108 105 87 0 09 NAIA10596 101 105 101 0

NAIC30596 VBLJC0601K .

108 J '108 /

no y 108

106 1 112

0 0

12 NAIC30596DL 98 96 100 0 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30

QC LIMITS SMC1 (TOL) = Toluene-d8 (88-110) SMC2 (BFB) = Bromofluorobenzene (86-115) SMC3 (DCE) = l,2-Dichloroethane-d4 (76-114)

# Column to be used to flag recovery values

* Values outside of contract required QC limits

D System Monitoring Compound diluted out

page 1 of 1 FORM II VOA-1 3/90

3000.2

4A EPA SAMPLE NO. VOLATILE METHOD BLANK SUMMARY

VBLK0529K Lab Name: NET CAMBRIDGE Contract: GEI

Lab Code: CAMBRG Case No.: SAS No. : SDG No.: 1855

Lab File ID: K1296 Lab Sample ID: VBLK0529K

Date Analyzed: 05/29/96 Time Analyzed: 1517

GC Column: CAP ID: 0.53 (mm) Heated Purge: (Y/N) N

Instrument ID: HP5970K

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:

EPA LAB LAB TIME SAMPLE NO. SAMPLE ID FILE ID ANALYZED

01 NAIM20596 148533 K1301 1811 02 NAII0596 148534 K1302 1847 03 04 05 06 07 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30

COMMENTS:

page 1 of 1 FORM .IV VOA 3/90

30Q03


Lab Name: NET CAMBRIDGE

Lab Code: CAMBRG Case No.:

Lab File ID: K1330

Date Analyzed: 05/30/96

GC Column: CAP ID: 0.53 (mm)


VBLK0530K Contract: GEI

SAS No.: SDG No.: 1855

Lab Sample ID: VBLK0530K

Time Analyzed: 1532

Heated Purge: (Y/N) N



01 FW26D0596 148535 K1333 1732 02 NAIK10596 148536 K1334 1807 03 NAIC10596 148537 K1335 1842 04 FW090596 148538 K1336 1917 05 NAIA10596 148539 K1337 1952 06 NAIC30596 148540 K1338 2027 07 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30

COMMENTS:

page 1 of 1 FORM IV VOA 3/90




Lab File ID: K1391




VBLK0601K Contract: GEI


Lab Sample ID: VBLK0601K

Time Analyzed: 1426

Heated Purge: (Y/N) N


01 02 03 04 05 06 07 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30

COMMENTS:


NAIC30596DL 148540DL K1393 1542

page 1 of 1 FORM IV VOA 3/90

30005

5A VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK

BROMOFLUOROBENZENE (BFB)



Lab File ID: K327 BFB Injection Date: 04/20/96

Instrument ID: HP5970K BFB Injection Time: 1035

GC Column: CAP ID: 0.53 (mm) Heated Purge: (Y/N) "N

% RELATIVE m/e ION ABUNDANCE CRITERIA ABUNDANCE

50 8.0 - 40.0% of mass 95 2̂8.2 ' •/ 75 30.0 - 66.0% of mass 95 63T4

L_9J> Base Peak, 100% relative abundance 100.0 i 96 5.0 - 9.0% of mass 95 8.0 173 Less than 2.0% of mass 174 0.3 ( 0.3)1 174 50.0 - 120.0% of mass 95 75.7 175 4.0 - 9.0% of mass 174 5.6 ( 7.4)1 176 93.0 - 101.0% of mass 174 74.3 ( 98.2)1 177 5.0 - 9.0% of mass 176 5.4 ( 7.2)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS:

EPA SAMPLE NO.

01 VSTD050K 02 VSTD200K 03 VSTD100K 04 VSTD020K 05 VSTD010K 06 07 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22

LAB LAB SAMPLE ID FILE ID

VSTD050K K330 VSTD200K K331 VSTD100K K332 VSTD020K K333 VSTD010K K334

DATE ANALYZED

04/20/96 04/20/96 04/20/96 04/20/96 04/20/96

TIME ANALYZED

1323 1358 1433 1507 1542

page 1 of 1 FORM V VOA 3/90





Lab File ID: K1291 BFB Injection Date: OS/29/96


GC Column: CAP ID: 0.53 (mm) Heated Purge: (Y/N), N ,/


50 8.0 - 40.0% of mass 95 19.7 75 30.0 - 66.0% of mass 95 54.7 / 95 Base Peak, 100% relative abundance 100.0 ̂ 96 5.0 - 9.0% of mass 95 ~D'.0 173 Less than 2.0% of mass 174 0.3 ( 0.4)1 J 174 50.0 120.0% of mass 95 90.3 175 4.0 - 9.0% of mass 174 6.2 ( 6.9)1 176 93.0 101.0% of mass 174 85.7 ( 94.9)1 177 5.0 - 9.0% of mass 176 5.8 ( 6.8)2



01 02 03 04 05 06 07 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22

EPA LAB LAB DATE SAMPLE NO. SAMPLE ID FILE ID ANALYZED

VSTD050K VSTD050K K1294 05/29/96 VBLK0529K VBLK0529K K1296 05/29/96 NAIM20596 148533 K1301 05/29/96 NAII0596 148534 K1302 05/29/96

TIME ANALYZED

1346 1517 1811 1847


300Q7





Lab File ID: K1323 BFB Injection Date: 05/30/96


GC Column: CAP ID: 0.53 (mm) Heated Purge: (Y/N).N J


50 8.0 - 40.0% of mass 95 21.4 75 30.0 - 66.0% of mass 95 59.8 95 Base Peak, 100% relative abundance 100.0 96 5.0 - 9.0% of mass 95 -7:0 173 Less than 2.0% of mass 174 0.3 ( 0.3)1 174 50.0 - 120.0% of mass 95 82.0 175 4.0 - 9.0% of mass 174 6.0 ( 7.3)1 176 93.0 - 101.0% of mass 174 82.0 (100.0)1 177 5.0 - 9.0% of mass 176 6.4 ( 7.9)2



EPA LAB LAB DATE TIME SAMPLE NO. SAMPLE ID FILE ID ANALYZED ANALYZED

01 VSTD050K VSTD050K K1326 05/30/96 1233 02 VBLK0530K VBLK0530K K1330 05/30/96 1532 03 FW26D0596 148535 K1333 05/30/96 1732 04 NAIK10596 148536 K1334 05/30/96 1807 05 NAIC10596 148537 K1335 05/30/96 1842 06 FW090596 148538 K1336 05/30/96 1917 07 NAIA10596 148539 K1337 05/30/96 1952 08 NAIC30596 148540 K1338 05/30/96 2027 09 10 11 12 13 14 15 16 17 18 19 20 21 22


30008




Lab Cede: CAMBRG Case No. :

Lab File ID: K1387



m/e ION ABUNDANCE CRITERIA

50 8.0 40.0% of mass 95 75 30.0 - 66.0% of mass 95

Contract: GEI


BFB Injection Date: 06/01/96

BFB Injection Time: 1109

Heated Purge: (Y/N) / N /

95 96 173 174 175 176 177

Base Peak, 100% relative abundance 5.0 - 9.0% of mass 95 Less than 2.0% of mass 174 50.0 - 120.0% of mass 95 4.0 9.0% of mass 174 93.0 101.0% of mass 174 5.0 - 9.0% of mass 176

1-Value is % mass 174 2 -Value is % mass

% RELATIVE ABUNDANCE

24.3 55.3

J.00.0 6.S 0.5 ( 0.6)1 88.3 6.7 ( 7.6)1 86.5 ( 98.1)1 5.7 ( 6.6)2

176


01 02 03 04 05 06 07 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22

EPA LAB SAMPLE NO. SAMPLE ID

VSTD050K VSTD050K VBLK0601K VBLK0601K NAIC30596DL 14854 DDL

LAB FILE ID

K1390 K1391 K1393

DATE TIME ANALYZED ANALYZED

06/01/96 1341 06/01/96 1426 06/01/96 1542


30QOS

8A VOLATILE INTERNAL STANDARD AREA AND RT SUMMARY


Lab Code: CAMBRG Case No. : SAS No.: SDG No.: 1855

Lab File ID (Standard): K1294 Date Analyzed: 05/29/96

Instrument ID: HP5970K Time Analyzed: 1346

GC Column: CAP ID: 0.53 (mm) Heated Purge: (Y/N) N /

IS1 (BCM) IS2 (DFB) IS3(CBZ) AREA # RT # AREA #. RT # AREA % RT #

========== = ==g> 12 HOUR STD ' 431114 . 9.40 1592843 12 .2Q 1336134 19_, 99 UPPER LIMIT 862228 9.90 3185686 12.70 2672268 20.49 LOWER LIMIT 215557 8.90 796422 11.70 668067 19.49

EPA SAMPLE NO.

VBLK0529K 452.767V 9.41 1607038^ ^12^20 / 1295314/, _JL9_^99 1







IS1 (BCM) IS2 (DFB) IS3 (CBZ) AREA # RT # AREA # RT # AREA # RT #

12 HOUR STD 412088 9.42 1645612 12.23 1363170 20.00 UPPER LIMIT 824176 9.92 3291224 12.73 2726340 20.50 LOWER LIMIT 206044 8.92 822806 11.73 681585 19.50

EPA SAMPLE NO.

01 VBLK0530K 428552 9.40 1625945 12.21 1384740 19.99 02 FW26D0596 417648 9.41 1586184 12.20 1322799 19.99 03 NAIK10596 409230 9.41 1571913 12.20 1303825 19.99 04 NAIC10596 395734 9.38 1507175 12.22 1274200 19.99 05 FW090596 379549 9.40 1438279 12.22 1107255 19.99 06 NAIA10596 397867 9.39 1491740 12.20 1278971 19.99 07 NAIC30596 402896 9.37 1515342 12.20 1292356 19.99 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22

151 (BCM) = Brotnochloromethane 152 (DFB) = 1,4-Difluorobenzene 153 (CBZ) = Chlorobenzene-d5

AREA UPPER LIMIT = +100% of internal standard area AREA LOWER LIMIT = - 50% of internal standard area RT UPPER LIMIT = + 0.50 minutes of internal standard RT RT LOWER LIMIT = - 0.50 minutes of internal standard RT

# Column used to flag values outside QC limits with an asterisk. * Values outside of QC limits.

page 1 of 1 FORM VIII VOA 3/90

30011







IS1 (BCM) IS2 (DFB) IS3 (CBZ) AREA # RT # AREA # RT # AREA # RT #

======= 12 HOUR STD 449103 9.33 1797733 12.17 1499228 19.98 UPPER LIMIT 898206 9.83 3595466 12.67 2998456 20.48 LOWER LIMIT 224552 8.83 898866 11.67 749614 19.48

EPA SAMPLE NO.

01 VBLK0601K 407276 9.41 1537357 12.21 1291513 20.00 02 NAIC30596DL 537599 9.39 2073310 12.21 1738765 20.00 03 04 05 06 07 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22

151 (BCM) = Bromochloromethane 152 (DFB) = 1,4-Difluorobenzene 153 (CBZ) = Chlorobenzene-d5

AREA UPPER LIMIT = +100% of internal standard area AREA LOWER LIMIT = - 50% of internal standard area RT UPPER LIMIT = + 0.50 minutes of internal standard RT RT LOWER LIMIT = - 0.50 minutes of internal standard RT

# Column used to flag values outside QC limits with an asterisk * Values outside of QC limits.

page 1 of 1 FORM VIII VGA 3/90

3B. SAMPLE DATA

300J3

1A EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET

FW090596 Lab Name: NET CAMBRIDGE Contract: GEI


Matrix: (soil/water) WATER Lab Sample ID: 148538

Sample wt/vol: 5.000 (g/mL) ML Lab File ID: K1336

Level: (low/med) LOW Date Received: 05/21/96

% Moisture: not dec. Date Analyzed: 05/30/96

GC Column: CAP ID: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: (uL) Soil Aliquot Volume: (UL)

CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L

74-87-3 Chi or ome thane 5 U 74-83-9 Bromomethane 5 U 75-01-4 Vinyl ChloridT" 5 U 75-00-3 Chloroethane 5 U 75-09-2 Methylene Chloride 5 U 67-64-1 Acetone 25 U 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethene 75-34-3 1,1-Dichloroe thane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform \ 107-06-2 1,2-Dichloroe thane

555555

U U U U U U

78-93-3 2 -Butanone 25 U 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27-4 Bromodichlorome thane 78-87-5 1,2-Dichloropropane 10061-01-5 cis-1, 3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochlorome thane 79-00-5 1,1,2 -Trichloroe thane 71-43-2 Benzene 10061-02-6 trans -1,3 -Dichloropropene_ 75-25-2 Bromof orm

55555555555

U U U U U U U U U U U

108-10-1 4-Methyl-2-Pentonone 25 U 591-78-6 2- Hexanone 25 U 127-18-4 Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane_ 108-88-3 Toluene 108 -90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 Styrene__^ 75-69-4 Trichlorofluoromethani

5555555

U U U U U U U

FORM I VOA 3/90


FW090596 Lab Name: NET CAMBRIDGE Contract: GEI







Soil Extract Volume: (uL) Soil Aliquot Volume: (uL)


i r\st nc A±\JQ — \JO~1 V .Lily X M.CC Ca US 5 U i i n TC a-1.-I.U~ /3~ O ~*— n_LOrucuiiyx vmyx cuiicir 5 U

5 Uqc_yi'7 c Ayxene 5 U CAI -Ti _i 5 U i nc A.C. iJ.UO — f±O — / , t -jjicn_L(jiOJ->eiizcJie 5 U qc_cn Ty3 o\J~ ± , z -uicn_Loiroj.jeiizfc;iie 5 U

FORM I VGA 3/90

3

P P P P ^^ ^o OJ n ^y ^yO C P — P P — -I 3 —C *Q ^ W3 (9 — 3 3 (9 it

•O O — —3 — 3 OP C -H "W 3 O(0 (9 " t>•> •• r

— Oo cn -c> co3> • 00•o O cn

COCD-t»

ft ft 19 p

•• T|

CO — O TO

I •• 2

3} V. -< o

I 3" co f>

0 3 ~v

— 3" tO -O » cn — CO

CO

8 cn

8jr

CO

8 cn

8 •-BroMochloronethane (9.372)

CO CO o>

-1,2-Dichlorocthane-d^ (10.919) o m

1,4-Dif luorobenzene (12.201)

•-Toluene-d8 (16.110)

ne-cChlorobenzeiie-d5 (19.991)

o o o -o C 3 3

O-t

P 3

cn co

3 01

3r>

3-•a cn co •sj

IS) ISJ'

Broiiof luorobenzene (23.307)

8

Data File: /chem/hp5970k.i/960530.b/k!336.d Report Date: 31-May-1996 09:56

NET Cambridge

VOLATILE ISTD AND RATIO REPORT Data file /chem/hp5970k.i/960530.b/k!336.d Lab Smp Id 148538 Client Smp ID: fw09 Inj Date 30-MAY-96 19:17 Operator jpt Inst ID: hp5970k.i Smp Info 148538,fw09,960530k,jpt,,1770,GEI Misc Info 1855,0,,,1,0,,,,,,,21-may-1996 Comment Method /chem/hp5970k.i/960530.b/kvoa.m Meth Date 30-May-1996 14:40 jamest Quant Type: ISTD Cal Date 30-MAY-96 12:33 Cal File: k!326.d Als bottle 14 Dil Factor 1.000 Integrator HP RTE Compound Sublist: 8240.sub Target Version: 3.12 Concentration Formula: Uf * 1

Name Value Description

Uf 1.000 ng unit correction factor

CONCENTRATIONS

QUANT SIG ON-COLUMN FINAL

Compounds MASS RT EXP RT REL RT RESPONSE ( ug/L) ( ug/L)

20 Bromochloromethane 128.00 9. 399 9.424 (1 .000) 379549 50 .00

25 l,2-Dichloroethane-d4 65 .00 10. 906 10 .931 (1 .160) 574631 43 .35 43.35 28 1,4-Difluorobenzene 114.00 12. 217 12 .229 (1 .000) 1438279 50 .00

35 Toluene-d8 98 .00 16. 110 16 .123 (0. .806) 1173404 54 .29 54.29

43 Chlorobenzene-dS 117.00 19. 991 20 .003 (I..000) 1107255 50 .00

51 Bromofluorobenzene 95 .00 23. 307 23 .320 (1. .166) 878876 52 .35 52.35

300]


FW26D0596 Lab Name: NET CAMBRIDGE Contract: GEI









74-87-3 Chloromethane 5 U 74-83-9 Bromome thane 5 U 75-01-4 Vinyl Chloride 5 U 75-00-3 Chloroethane 5 U 75-09-2 Methylene Chloride 5 U 67-64-1 Acetone 25 U 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethene 75-34-3 1,1-Dichloroe thane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1,2-Dichloroethane

555555

U U U U U U

78-93-3 2 -Butanone 25 U 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27-4 Bromodichloromethane 78-87-5 1, 2-Dichloropropane 10061-01-5 cis -1,3 -Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochlorome thane 79-00-5 1,1, 2-Trichloroethane 71-43-2 Benzene 10061-02-6 trans -1,3 -Dichloropropene 75-25-2 Bromoform

55555555555


108-10-1 4-Methyl-2-Pentonone 25 U 591-78-6 2-Hexanone 25 U 127-18-4 Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenz ene 100-41-4 Ethylbenzene 100-42-5 Styrene 75-69-4 Trichlorof luoromethane

5555555

U U U U U U U

FORM I VOA 3/90


FW26D0596 Lab Name: NET CAMBRIDGE Contract: GEI









5 U IIO — 7^ — fl 'J-.r'Vil r\-rv-\o^H*7l ̂ ri TT\r1 ot"Vio-r 5 U

5 u Q C A *7 £ /•** YT rl ̂ n^ 5 u

5 u 5 u

nc trn T T O T^T c"»lil j-fcy»

p p p p — . rs> n en oo o i

if i...i...

N>is>r \>rois)LJCJUiJcj^^^Jk^i / i i / i incnina>cncno>o)viv iv iv iv ia>a>cocoao(O O T> U> O

ms = C 10 T> *» 3 (O — 3 3 » «

•o o — — 3 — 3 0 o c -n •• I/I 3 O o w •• -n .. .. c

-» M o en Ji O) 3J • CD O. •o O 01 uin

8 « 3> v> -< O

co e> O) 3

VI T» •• in u 10 ISl VI

o> a. 10 8ai

10 8in 8

•-BroMochloroiiethane (9.398)

o

•-1,2-Dichloroethane-cH (10.932) vl o

to u a.

•-1,4-Difluorobenzene (12.201)

r •-Tolucne-d8 (16.097) o o O TJ — ra c i

3 III

3 O 3 r> C

O 3 Q. T ^» ••

§d> ^ T)

TJin

Chlorobenzeni-d5 (19.991) O • in

s

Brotiof luorobenzcne (23.307)

roa>'

8

M)2


NET Cambridge

VOLATILE ISTD AND RATIO REPORT Data file /chem/hp5970k.i/960530.b/k!333.d Lab Smp Id 148535 Client Smp ID: fw26d Inj Date 30-MAY-96 17:32 Operator jpt Inst ID: hp5970k.i Smp Info 148535,fw26d,96053Ok,jpt,,1770,GEI Misc Info 1855,0,, ,1,0,,,,,,,21-may-1996 Comment Method /chem/hp5970k.i/960530.b/kvoa.m Meth Date 30-May-1996 14:40 Jamest Quant Type: ISTD Cal Date 30-MAY-96 12:33 Cal File: k!326.d Als bottle 11 Dil Factor 1.000 Integrator HP RTE Compound Sublist: 8240.sub Target Version: 3.12 Concentration Formula: Uf * 1



CONCENTRATIONS

QUANT SIG ON- COLUMN FINAL


20 Bromochloromethane 128.00 9.412 9. 424 (1 .000) 417648 50 .00

25 l,2-Dichloroethane-d4 65 .00 10 .919 10. 931 (1 .160) 692810 47 .49 47.49

28 1,4-Difluorobenzene 114.00 12 .204 12. 229 (1 .000) 1586184 50 .00

35 Toluene-d8 98.00 16 .097 16. 123 (0. .805) 1304166 50 .51 50.51

43 Chlorobenzene-d5 117.00 19 .991 20. 003 (1, .000) 1322799 SO .00 51 Bromofluorobenzene 95.00 23 .307 23. 320 (1, .166) 1031998 51 .46 51.46

300?

Data F i l e : /chen/hp5970k.i/960530.b/k1333.d

Date : 30-MRY-1996 17:32

Cllent ID: fu26d0596 Instrument: hp5970k.i

Sanple Info: 118535,fw26d,960530k,jpt,,1770,GEI

Purge Volurie: 5.0 Operator: jpt

Colunn phase: CRP ColUhn dianeter: 0.53

33 4-Methyl-2-Pentonone

16.084 Min) of k1333.d Ion 43.00 .8

Scon 1052 C

.6 11.6 .4

.2 1.4 N

in .Q. 'I1.2 k 0 8 . X '

/^ 2 .70 >• yv 0.4

0.2 ..L 1 I.I.I. I.I.1 1.... JjJ-..Lt.4 ... .I..I 1. ^ 40 60 80 100 120 140 160 180 200 n w.

M/Z

0.0 i \ k1 Scon 1052 (16.084, Min) of k1333.d (Subtracted)

1.6 ^98

J I i1 .4 1.2 Hi'n

3:0016:20 Ion 58.00

in 2.0~ 1.0

< 0.8 ii 1.85 0.6

y42 .70 1.6; >• 0.4

0.2 1.4-; 208 0.0 ^LajLj „

40 60 80 100 120 140 160 180 200 n̂ '-2: '•

M/Z J> 1-0... . _ 33 4-Hethy l-2-Pentonone (Reference Spectruii) 10.0, ^•43 5 0.8-;9.0 i

0.6

7.0 ~ 6.0 o


NAIA10596 Lab Name: NET CAMBRIDGE Contract: GEI









74-87-3 Chlorome thane U 74-83-9 Bromome thane U 75-01-4 Vinyl Chloride U 75-00-3 Chloroethane U 75-09-2 Methylene Chloride U 67-64-1 Acetone 25 U 75-15-0 Carbon Disulfide 5 U 75-35-4 1,1 -Dichloroethene 5 U 75-34-3 1,1 -Di chloroethane 5 U 540-59-0 1,2-Dichloroethene (total) 5 U 67-66-3 Chloroform \ 5 U 107-06-2 1,2 -Dichloroethane 5 U 78-93-3 2-Butanone 25 U 71-55-6 1,1,1-Trichloroe thane 5 U 56-23-5 Carbon Tetrachloride 5 U 75-27-4 Bromodichlorome thane 5 U 78-87-5 1,2-Dichloropropane 5 U 10061-01-5 cis-1,3 -Dichloropropene 5 U 79-01-6 Trichloroethene 5 U 124 -48 -1 Dibromochloromethane 5 U 79-00-5 1,1,2- Tri chloroethane 5 U 71-43-2 Benzene 5 U 10061-02-6 trans-1,3-Dichloropropene 5 U 75-25-2 Bromof orm 5 U 108-10-1 4-Methyl-2-Pentonone 25 U 591-78-6 2-Hexanone 25 U 127-18-4 Tet rachloroethene 5 U 79-34-5 l,l,2,2-Tetrachloroethane_ 5 U 108-88-3 Toluene 5 U 108-90-7 Chlorobenzene 5 U 100-41-4 Ethylbenzene 5 U 100-42-5 Styrene 5 U 75-69-4 Trichlorofluorome thane 5 U

FORM I VOA 3/90

1A EPA SAMPLE NO. VOLATILE ORQANICS ANALYSIS DATA SHEET

NAIA10596 Lab Name: NET CAMBRIDGE Contract: GEI

Lab Code: CAMBRG Case No.: SAS No. : SDG No.: 1855





GC Coluimi: CAP ID: 0.53 (mm) Dilution Factor: 1.0



i no nc A. _J.UO — U D ~ f t — — i i n 1^. ft J..LU — /D — o ~ ~ —

— ~~VUlyx ACcUaUc -(_ii_LOioet.xiyj.vniyj. cuiici.

5 5

U U

QC A.I a173— *± / -O _ _~ ana. p— Ayieiie

— Ay -Lcllc

5 5

U U

CA1 _ T T _ 1DtJ." / J — J. 5 U 1 nfi-4.fi-'7 5 U QCC cn-i 5 U

FORM I VOA 3/90

o o o o • O -O 10 O O O O^ C C — C C

C


NET Cambridge

VOLATILE ISTD AND RATIO REPORT Data file /chem/hp5970k.i/960530.b/k!337.d Lab Smp Id 148539 Client Smp ID: naial Inj Date 30-MAY-96 19:52 Operator jpt Inst ID: hp5970k.i Smp Info 148539,naial,960530k,jpt,,1770,GEI Misc Info 1855,0,,,1,0,,,,,,,21-may-1996 Comment Method /chem/hp5970k.i/960530.b/kvoa.m Meth Date 30-May-1996 14:40 jamest Quant Type: ISTD Cal Date 30-MAY-96 12:33 Cal File: k!326.d Als bottle 15 Dil Factor 1.000 Integrator HP RTE Compound Sublist: 8240.sub Target Version: 3.12 Concentration Formula: Uf



CONCENTRATIONS


— Compounds MASS RT EXP RT REL RT RESPONSE ( ug/L) ( ug/U

10 Methylene Chloride 84.00 5.544 5.570 (0 .591) 12421 1, .44 1.44(aQM)

20 Brotnochloromethane 128.00 9.385 9.424 (1 .000) 397867 50, .00

25 l,2-Dichloroethane-d4 65.00 10 .932 10 .931 (1 .165) 699250 50. .32 50.32

28 1,4-Difluorobenzene 114.00 12 .204 12 .229 (1 .000) 1491740 50. .00

35 Toluene-d8 98.00 16 .110 16 .123

Data F i l e : /chen/hp5970k. i/960530.b/k1337.d

Date : 30-MHY-96 19:52

Cl lent ID: naiat InstruMent: hp5970k.I

Saitple Info: 118539, naiat ,960530k, jpt,, 1770, GEI

Purge Voluite: 5.0 Operator: jpt

Colui-m phase: CRP Colunn dianeter: 0.53

10 Methylene Chloride

Scon 218 (5.511 Min) of k1337.d Ion 81.00 lO--"

3.2

2.8

2.1 1.1-!

K2] 1.6 1.1-i

0.9-i 0.8

0.1

0.0 45 50 55 60 65 70 75 80 85

* M/Z Scan 218 J5.511 Min) of k1337.d (Subtracted)

10 Methylene Chloride (Reference Spect run) hylen

^ 2.0 1.8 1.6

0.0-: 5.20 5.10 5.60

Min 5.8O 6.00

1.1 Ion 19.00 1.2

2 i 0 0.8 0.6 0.1 0.2 0.0

10 15 50 55 60 65 70 75 80 85 M/Z

O

10.0 9.0 8.0

7.0 ; 6.0

5.0 1.0

5.20 5.10 5.60 5. '80 6.00 3.0 nin 2.0 /37 2 Ion 51.00 1.0 / y0.0 , 1 , ,,/.

10 15 50 55 60 65 70 75 80 85 M/z

Scan 218 (5.511 Min) of k1337.d & DIFFERENCE) ICO

60 60

10 " "Vx J52 7 20 0 1 •

-20 -10

-60 -80

-ICC 10 15 50 55 60 65 70 75 80 85 5.40 5.60 5.80 6.00

M/Z n in


NAIC10596 Lab Name: NET CAMBRIDGE Contract: GEI

Lab Code: CAMBRG Case No. : SAS No.: SDG NO.: 1855








74-87-3 Chloromethane 74-83-9 Bromomet hane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1 -Dichloroethene

540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform \ 107-06-2 1,2 -Dichloroe thane 78-93-3 2-Butanone 71-55-6 1,1,1 -Trichloroethane

75-27-4

01-5 cis-1,3 -Dichloropropene_ 6 Trichloroethene -1 Dibromc

1-00-5 1,1,2-'.

02-6 trans -1,3 -Dichloropropene 75-25-2 Bromo form ~ 108-10-1 4-Methyl-2-Pentonone

127-18-4 Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane 108-88-3 Toluene ~ 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 Styrene 75-69-4 Trichlorofluorome thane

5 5 5 5 5 25 5 5

5 5 25 5 5 5 5 5 5 5 5 5 5 5 25 25 39

U U U U U U U U U U U U U U U U U U U U U U U U U U

u~ u u u u u

FORM I VOA 3/90



Lab Code: CAMBRG Case No. :

Matrix: (soil/water) WATER

Sample wt/vol:

Level: (low/med)

% Moisture: not dec.

GC Column: CAP

Soil Extract Volume:

CAS NO.

i n f t -n^-A -| i ("1-7^-8

QR-A7-^

^A1 7"3 -1 1 C\£ AC *7 xuo — *to - / QC CO — 1

5.000 (g/mL) ML

LOW

ID: 0.53 (mm)

(uL)

COMPOUND

NAIC10596 Contract: GEI


Lab Sample ID: 148537

Lab File ID: K1335

Date Received: 05/21/96


Dilution Factor: 1.0

Soil Aliquot Volume: (uL)

CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L

/ *t — iJicij-LQiODeiizeiie

5 u 5 u 5 u 5 u 5 u 5 u 5 u

FORM I VOA 3/90

O O O O — -» — — — roN>rs>Mis>cjcjcococo^AAAAcnoioioicno)cocno)ci>' j ->j 'g^j^jcococococo«o«o ivj -& cn co O is) . o o C C — C C

c O T> 0 R C 3 0 — 3 3 ra« .. -n

° 3 5 8 o C -t, .. I •> 2 O 2 ra •• 3 B >v•• o -< o

— — I 3* cn .& o to o • CO — CO 3O cn .̂

CJ — 3" >l CD T)

..01 3 J> (D

£ M gO 7T

(O

8 (O cn 8 8 cn

•-BroMOChloroi-iethanc (9.381) cj in •

•-1,2-Dichlorocthonc-d1 (10.931) o. o ni

•-1i^-Difluorobcnzcne (12.203)

•-Toluene-d8 (16.096) o o o -o 3

ot c -s— ra 3 S

o a -j

•o cn

8Chlorobezenc-d5 (19.990)

cn CJ

Bronof luorobenzene (23.306)'

ts)CO"

or :

• ' t

CJ O"

30030


NET Cambridge

VOLATILE ISTD AND RATIO REPORT Data file /chem/hp5970k.i/960530.b/k!335.d Lab Smp Id 148537 Client Smp ID: naicl Inj Date 30-MAY-96 18:42 Operator jpt Inst ID: hp5970k.i Smp Info 148537,naicl,96053Ok,jpt,,1770,GEI Misc Info 1855,0,,,1,0,,,,,,,21-may-1996 Comment Method /chem/hp5970k.i/960530.b/kvoa.m Meth Date 30-May-1996 14:40 jamest Quant Type: ISTD Cal Date 30-MAY-96 12:33 Cal File: k!326.d Als bottle 13 Dil Factor 1.000 Integrator HP RTE Compound Sublist: 8240.sub Target Version: 3.12 Concentration Formula: Uf * 1



CONCENTRATIONS


Compounds MASS RT EXP RT REL RT RESPONSE ( ug/L) ( ug/L) 1

* 20 Bromochloromethane 128 .00 9. .384 9.424 (1 .000) 395734 50 .00 $ 25 1,2-Dichloroethane-d4 65 .00 10. .931 10 .931 (1 .165) 714681 51 .71 51. 71

* 28 1,4-Difluorobenzene 114 .00 12, .216 12. .229 (1 .000) 1507175 50, .00 S 35 Toluene-d8 98 .00 16, .096 16 .123 (0 .805) 1336873 53, .75 53. 75

41 Tetrachloroethene 164 .00 17. ,748 17, .774 (0 .888) 560236 39, .36 39. 36 * 43 Chlorobenzene-d5 117 .00 19. ,990 20. .003 (1 .000) 1274200 50. .00 $ 51 Bromofluorobenzene 95 .00 23. .306 23 .320 (1 .166) 1041625 S3 .92 53. 92

30031

Data F i l e : /chei-i/hp5970k. i /960530.b/k1 335.d

Date : 30-nflY-1996 18:12

Cl lent ID: naic10596 Instrunent: hp5970k.i

Sanple Info: 118537,naicl,960530k,jpt,,1770,GEI

Purge Volui-ie: 5.0 Operator: jpt

Colunn phase: CRP Colui-in diaMeter: 0.53 r33 1-Methyl-2-Pentonone

Scan 1053 (1J.OJ96 Min) of k1335.d Ion 43.00 ^>98 2.0 J

1.8 2.0-: 1.6 : fl 1.4 " "

1.6: "> 1.2 in 1.0 1 .4: I1

H °'8 o 1.2: 111 X70 2 1.0:

x : 0.2 i 1 17^ ~ 0.8-; 0.4

, ,/118 x !̂ 0.0 . t il.i• M nil 1.1. ii . tli i>l.lll i1 t.i 1. . i . l-ll e • . \O • O

40 60 80 100 120 140 160 180 200 , 1 i k,M/Z 0.4: Scan 1053 (16.096 \iin) of k1335.d (Subtracted)

1.2-1 0.2: 1IIIO.o: Hill15.6015.80 16.0016.20

Min 0.8 Ion 58. 00

in 12.4: 0.6.

x 2.2-i fl ~ 0.4

2.0: /"2 70

/0.2- .8-; A 1 8 /1 74 ?01 .6-:

k.lj|J.I..,l. J, ,., 0.010 60 80 100 120 140 160 180 200 n •^-.

M/Z o 2 ' _ ._ 33 4-nethyl-2-Pentonone (Reference SpectruiO ~

10.0 ^̂ 13 c .0: 9.0 >• 0.8: 8.0 0.6^ 7.0

~ 6.0 0-"1 I I I

°'2 ̂: I I I ^— M A o o " i " '' 1 x 4.0 8 15.6O15.80 16.0016.20 ~ 3.0 /* flin

2.0 85\ Ion 100. 00 1.31.0

t*

0.0 I i . . .1 r 1 .2-. 40 60 80 1OO 120 140 160 180 200 1 . 1 -i

M/Z Scan 1053 (16.096 M,m) of k1335.d (x DIFFERENCE)

ICO, 0.9-; so 0 8' 60 p 0.7^

/** /70 2 0.6^ 20 X : . . . i ~ 0.5-1

i.i *.ij.l.i.u. .Jj.sl> >..... i .rfll . . .' 1E -20.

0.3; z -10 0.2^ -60

-6O O.l-i

0 0 : J^ j-ICO 40 60 80 100 120 140 160 180 2OO 15.6O15.80 16.0O16.20

M/Z Min

30032

http:16.0O16.20http:15.6O15.80http:16.0016.20http:15.6O15.80http:16.0016.20http:15.6015.80

Data File: /chen/hp5970k.i/960530.b/k1335.d

Date : 30-HRY-96 18:12

Client ID: naicl Instrunent: hp5970k.i

Sartple Info: 118537,naicl,960530k,jpt,,1770,GEI

Purge Volume: 5.0 Operator: jpt

Colunn phase: CRP Colunn dianeter: 0.53

41 Tetrachloroethene Scan 1179 (17.748 Min) of k1335.d Ion 164.00

166"-̂ 8.5- * 1 .1 e.oJ A 1.0 7.5 _0.9 7.0-; 0.8 6.5J

~ 0.7 6.0J


NAIC30596 Lab Name: NET CAMBRIDGE Contract: GEI

Lab Code: CAMBRG Case No. : SAS No.: SDG No.: 1855








74-87-3 Chloromethane 5 U 74-83-9 Bromomethane 5 U 75-01-4 Vinyl Chloride" 6 75-00-3 Chloroethane 5 u~ 75-09-2 Methylene Chloride 14 B 67-64-1 Acetone 320 E 75-15-0 Carbon Disulfide 5 U 75-35-4 1,1-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 9 540-59-0 1,2-Dichloroethene (total) 33 67-66-3 Chloroform \ 5 U 107-06-2 1,2-Dichloroethane 8 78-93-3 2-Butanone 44 71-55-6 1,1,1-Trichloroe thane 5 U 56-23-5 Carbon Tetrachloride 5 U 75-27-4 Bromodi chloromethane 5 U 78-87-5 1,2-Dichloropropane 5 U 10061-01-5 cis-l,3-Dichloropropene 5 U 79-01-6 Trichloroethene 21 124 -48-1 Dibromochlorome thane 5 U 79-00-5 1,1,2-Trichloroethane 5 U 71-43-2 Benzene 5 U 10061-02-6 trans -1,3 -Dichloropropene_ 5 U 75-25-2 Bromoform 5 U 108-10-1 4-Methyl-2-Pentonone 44 591-78-6 2-Hexanone 25 U 127-18-4 Tetrachloroethene 5 U 79-34-5 l,l,2,2-Tetrachloroethane_ 5 U 108-88-3 Toluene 18 108-90-7 Chlorobenzene 5 U 100-41-4 Ethylbenzene 5 U 100-42-5 Styrene 5 U 75-69-4 Trichlorof luoromethane 5 U

FORM I VOA 3/90





Sample wt/vol: 5.000 (g/mL) ML

Level: (low/med) LOW



Soil Extract Volume: (uL)

CAS NO. COMPOUND

CAT *7"3 1DftJ.— / J — X

q^ -^

NAIC30596 Contract: GEI


Lab Sample ID: 148540

Lab File ID: K1338






UUUUUUU

5555555

FORM I VOA 3/90

p p o — — is) tn GO O TS> o TJ tno o o

o c p — c c — -t 3 — < - > < - » c ^ ^ w w p3 W — 33 ro r< " -n •o o — — y — 3- — 3 o O ra p c -t> •• i •• M 3 O 2 ft f> " 3 D -s. . . . . p -< o

— — I 3" o cn j» o to o 3) • CO U O> 3•a O en *-.

is) co O

o CJ

CO s CO UI 8

UI

-BroMochloroHethane (9.385)

O" : toa>

•-1,2-Dichloroethone-d4 (10.918)n o m


•-Toluene-d8 (16.110) o o o *D 3 — (9 M c -i i Z c

o 3 a. "r ft

3

8- 3Chlorobbnzene-dS (19.990) 7f

fs> rsT

Brohof luorobenzene (23.307)

IS) 00'

8

3003$.

Data File: /chem/hp5970k.i/960530.b/k!338.d Report Date: 04-Jun-1996 11:45

NET Cambridge

VOLATILE ISTD AND RATIO REPORT Data file /chem/hp5970k.i/960530.b/k!338.d Lab Smp Id 148540 Client Smp ID: naic30596 Inj Date 30-MAY-96 20:27 Operator jpt Inst ID: hp5970k.i Smp Info 148540,naic3,960530k,jpt,,1770,GEI Misc Info 1855,0,,,1,0,,,,,,,21-may-1996 Comment Method /chem/hp5970k.i/960530.b/kvoa.m Meth Date 04-Jun-1996 11:39 linda Quant Type: ISTD Cal Date 30-MAY-1996 12:33 Cal File: k!326.d Als bottle 16 Dil Factor 1.000 Integrator HP RTE Compound Sublist: 8240.sub Target Version: 3.12 Concentration Formula: Uf



CONCENTRATIONS



2 Vinyl Chloride 62.00 2. .843 2.869 (0 .303) 28395 6 6(aM)

7 AceCone 43.00 4.691 4.718 (0 .501) 544804 320 320 (A)

10 Methylene Chloride 84.00 5. .530 5.570 (0 .590) 119338 14 14

14 1,1-Dichloroethane 63 .00 7, .156 7.221 (0.764) 147116 9 9 (a)

16 2-Butanone 43.00 8.795 8.834 (0 .938) 144692 44 44 (M)

18 1,2-Dichloroethene (cotal) 96.00 8.782 8.794 (0 .937) 335280 33 33


QC Flag Legend

a - Target compound detected but, quantitated amount Below Limit Of Quantitation(BLOQ).

A - Target compound detected but, quantitated amount exceeded maximum amount.

Q - Qualifier signal failed the ratio test. M - Compound response manually integrated.

30038

Data Fi le: /cheM/hp5970k. i/960530.b/M338.d

Date : 30-MflY-96 20:27

Cl lent ID: naic3 InstruMent: hp5970k.I

Scuiple Info: 118510,naic3,960530k,jpt,,1770,GEI


Colunn phase: CflP Colunn dianeter: 0.53

2 Vinyl Chloride Scan 12 (2.813 Min) of k1338.d Ion 62.00

3.2

2.8

"•* /62

2̂.6: A

/ 2.1 2.1^ I

o

2•5

*•

2.0

1.6 1.2

0.8

0.1

0.0 n0

|

60 80 100 120 110 160

4^2

«:S g : :lI -^ -^*" >01

0-8i

\ Ii 1

1 tt

2.8

2.1

Scan 32M/Z

(2.813 Min) of k1338.d (Subtracted) 0.6 H

giLi2. '10 2.60 2.80

|l

li 3.00 3.20

Ion 61.00 < 1.6 o

> 0.8 /'36

60 80 100 120 110 160

M/Z

30039

Data File: /chCH/hp5970k.i/960530.b/k1338.d

Date : 30-HHY-96 20:27

Cllent ID: naic3 Instrument: hp5970k.i

Sai-iple Info: 118510>naic3,960530k,jpt,,1770,GEI

Purge Volune: 5.0 Operator: jpt

Coluhn phase: CflP Colunn diacieter: 0.53

7 flcetone

Scan 183 (1.691 Min) of k1338.d Ion 13.00

7.0 7.OH

6.0 6.5-1 6.OH'

5.0 5.5-j 1.0 5.OH

X

> 2.0 Xs8

1.5H 1.0H:

3.5J

1.0

0.0 , 1 1 1 1 , 1 I ,10

x53r

, i .

50 • i

60

71v ^

.

70

y78 f

80

96-v 68 ^ \ • •

90

3.0^

2.5-i

2.OH

7.0

M/Z

Scan 183 (1.691 nin) of0*2,3' k1338.d (Subtracted) 1.5H:

I.OH: 0.5-i

6.0 0.0^ 1.10 1.60 1.80 5.00 5.20

5.0 nin Ion 58.00

1.0 2.0: o

1.8x

2.0

Data F i l e : /cheii/hp5970k. i/960530.b/kt338.d

Date : 30-ttflY-96 20:27

Client ID: naic3 Instrunent: hp5970k.i

Sanple Info: 148540, naic3, 960530k, jpt, , 1770, GEI


Colunn phase: CflP Colunn dianeter: 0.53

10 Methylene Chloride

2 .2 -1 49-" Scan 217 (5.530 nin) of k1338.d Ion 84.00

2.0 1.8 1.6.

1.0 * 0.8

0.6 0.4 0.2 0.0 I II , I I i

10 50 60 70 80H/Z 90 100 110 120 130 140

S£an 247 (5.530 Min) of k1338.d (Subtracted)

2.0 1.8 1.6

5.20 5.40 5.6OMin

5.80 6.00

1.4 Ion 49.00 2.2:

o 1.0 2.0: x 0.8

0.6 0.4 0.2 0.0 i

43 50 60 70 80 90 100 110 120 130 140 H/z

10.0 10 Methyl ene Chlo r i d e (Reference Spectrun)

9.0 8.0

7.0 . 6.0

5.0 : ^.o

3.0 5.20 5.40 5.60Min 5.80 6.00

2.0 Ion 51.00 1.0 0.0

40 50 60 70 80 90 100 110 120 130 140 h/z

100 Scan 247 (5.530 nin) of k1338.d (x DIFFERENCE)

80 60

40 20 /37 5v

= -20 ! -40

-60 -80

-icoJ 40 50 60 70 80 90 100 110 120 130 140 5.20 5.40 5.60 5.60 6.00

ti/z mm

30041

Data File: /chcM/hp5970k.i/960530.b/k1338.d

Date : 30-MflY-96 20:27

Client ID: naic3 Instrunent: hp5970k.i

Sai-iple Info: 118510,naic3,960530k, jpt,, 1770,GEI


Colurin phase: CRP Colunn dianeter: 0.53

11 1,1-Dichloroethanc

371 (7.156 Min) of k1338.d Ion 63.00 Sss0

1.2 :3J \\ i

^ 1.0 .i-i o 0.8 .0^ x 0.6 r o's^ f >- 0.1 2 0.7^

9N"X 119, «7 0.2 ^ 0.6-! x >• 0.5-1

40 50 60 70 80 90 100 110 120 130 0.4^. M/Z

0.0^ iN In nil 1 ih > , 0.3^ I

Scan 371 J7. 156 Hin) of k1338.d (Subtracted) 0.2i j

1.1- °••. . "Ni ^7 •

<

B

4:

'2~:.0:

/

I

\I I -20 0.8-i z -40 0.6:

-60 0» 4- L J J -6O

-ICO ^•'il 1 1 40 50 60 70 80 90 100 110 120 130 6.80 7.00 7.2O 7.40 7.60

M/Z Min

300/j?

Data File: /cheii/hp5970k. i/960530.b/k1338.d

Date : 30-MRY-1996 20:27

Client ID: naic30596 Instrunent: hp5970k.I

Sanple Info: 118510,naic3,960530k,jpt,,1770,GEI


Colui-in phase: COP Column dianetcr: 0.53

16 2-Butanone

Scan 196 (8.795 Min) of k1338.d Ion 13.00 1.8 61"1.1 •^ lj\1.0 .3i ff ^6 3.6 •2i I 3.2 .H

£ 2.8 •o-i \ 0.9-1 2 2.0 x ' ? 0.8-1 1

>• \'.2 , k 0.7^ 1 0.8 5 O.B-: I 0.1 1 1 IU 3^9 v 0.5-! 0.0 IJ > IK > viii ii i « i , . 0 11 J I

50 75 100 125 150 175 200 225 250 275 300 • f I M/Z 0.3H \

,̂ Scan 196 (8.795 iiin) of k1338.d (Subtracted) °-2-: / V, 01^ O.H 7 T^ji1.5J 4 0 Oi /WAI nr (r̂ \ Mr

1.0 8.10 8.60 8.80 9.00 9.20 ^6 3.5 Min

Ion 57.00 ~ 3.0 1.2- | ,

r 2.5 ! ; .1 il 2 2.0 '• 1

1.0 m" 1. 5 *• i.o 0.9-j i0.5 ^19 0.8-; 'I

0.0 1.1 1• i • .1 , . ;̂ ^^ 7-'

50 75 100 125 150 175 200 225 250 275 300 n | I M/Z ^> 0.6-:

_ 0 V • t m

U 1 x%>^ 16 2-Butanone (Reference SpectruM) x 0.5^ 10.0,

9.0 " 0.1-: 8.0

' 1 °-3^ 7.0 °-2^ I

6-0 n :::;ILIi ULL x 1.0 8.40 8.60 8.80 9.00 9.20 ~ 3.0 Min

2.0 /72 Ion 72.00 , 1.1, I1.0 h S*0.0 iii 1 1 1 1 1 1 1.0- I

50 75 100 125 150 175 260 225 250 275 300 ^ *• I3.6: fli Scan 196 (8.795 Min) of k1338.d (x DIFFERENCE)

M/Z

ICO, 61-^ y96 80 >/

3"-: 1 2-8: fll

60 « 2.1- / 40- ^> : J" 2.0- I20 i :

8 ° ''I 1 " •n i r • \ . >- '-6: /

i -20 1.2-:• Ii i -10 0.8-:

-60 ' 0.1- In/

-80 • Ifl fl"0 0--ICO8. '10 8.60 8.80 9.00 9.20 50 75 100 125 150 175 200 225 250 275 300 Min M/Z

30043

HP MS k!338.d. Scan 496: 8,795 min. (SUB) "•^43

1.0

0.9

0.8

0.7

~ 0.6^^ o 0.5

* 0.4> 0.3

0.2 "\

0.1111 Illillll , 1 ill 1 10.0

50 75 100 125 150 175 200 225 250 275 300 m/z

^HP MS k!338.d. Scan 492: 8.742 min.

4.4

4.0- /96

3.6- '

3.2

- 2.8< 2 4 o ^* x 2.0

1*6">1.2

0.8- /43 / 8N ^2 0.4

,1. , 1 Jill , . 1 i l l I 1 1 I I i0.040 50 60 70 80 90 100 110 120 130 140 150 160

m/z HP MS k!338.d. Scan 496: 8.795 min. (DIFF)

^43 1.0

0.9

0.8

0.7

^ 0.6

x 0.4

^ 0.3

0.2-9N

0.1-llli \fy, • i i ill , , ,̂ 0.0

50 75 100 125 150 175 200 225 250 275 300 m/z

300.H


Date : 30-f1flY-96 20:27

Cllent ID: naic3 Instrunent: hp5970k.i

Saitple Info: 118510,naic3,960530k, jpt,, 1770,GEI


Colunn phase: CflP Colunn diaiieter: 0.53

18 1,2-Dichloroethene (total) .Scan 195 (8.782 Min) of k1338.d Ion 96.00 ^61 1.0-i

5.0 3.8J 1.5- 9o\^ 3.5^ 1.0 3.2^ 3.5 3.0J

? 3.0 o 2.5 2.5^ 5 2.0 ? 2.2^ y3 >. 1.5 / o 2.0^

/1 00 B K8i1.0 / yl 16 - . 2 i ili.l 1 ii. III! i • •I 0.0

10 60 80 100 120 110 160 i.o-i M/Z 0.8-i

Scan 195 (8.782 nin) of k1338.d (Subtracted) 0.5^ 5.0 0.2^

l.i j. . md c 0.0-^J—^ " «T . O

6.0 8.0 10.0 12.0 1.0 Kin 3.5 Ion 61.00

? 3.0 6.0; k 2.5 5.6-i * 2.0 5.2.; 5_ 1.5 / 4.8-!

A 00 / /1 16 4.63

1.0. 0.5 4.0;'

II I / \0.0 II.. 1 ..Illl I 1 . 1 .1 . . ^ 3.6^

10 60 80 100 120 110 160 M/Z < :

2 2.8; 18 1,2-13 jchloroethene (total) (Reference SpectruM) 10.0, i 2.1-! 9.0. >- 2.0^ 8.0 1.6; 96\ 7.0 \ 1 ,2i

£ 6.0 0.8;:

0.4-; .. .. ...JWL ,„]'

"x 1.06.0 8.0 10.0 12.0 ^^ O S\3.0. Min

2.0 43 xlOO Ion 98. 00 1.0 x0.0 1, III, .I i i i i .1 2.6-;

10 60 80 100 120 110 160 2.4.; M/Z 2.2^

Scan 195 (8.782 Min) of k1338.d (x DIFFERENCE) 100 2.0^ 80 .8-; 60 ? .6-; 10 y43 ^ '*'• 20 "x -2; 72\ 96\' ( /'°°

f -20 0.6^ £ -10 0.6^

-60 0.4-: -80 0.2^ 1

-ICO Q o ^i 1.1 -Aj^i » u j lAi • 10 60 80 100 120 110 160 6.0 8.0 10.0 12.0

M/Z Hin

30045

Data Fi le: /chei-i/hp5970k. 1/960530. b/kl 338.d

Date : 30-nflY-96 20:27

Cl lent ID: naic3 Instruhent: hp5970k.i

Sanple Info: 148540,naic3,960530k, jpt,, 1770,GEI


Coluhn phase: CfiP Colunn diaiieter: 0.53

26 1 ]2-Di chI oroethane Scan 674 (11.128 Min) of M338.d Ion 62.00

^-62 1.6

1.4

1.2

1.0

0.8

0.6

0.4

0.2

0.0- III! I llllll ill 11 i i 40 60 80 100 120 140 160 180

M/Z

Scan 574 (11.128 Min) of k1338.d (Subtracted) 1.6 1.4 10.8011.0011.2011.4011.60 1.2 Hin

1.0 Ion 64.00

0.8 0.6 0.4 0.2 0.0 IIJ il i

40 60 80 100 120 140 160 180 H/z

10.0 D :̂̂ 1 i2-Dichloroethane (Reference Spectruii)

9.0 8.0 7.0 6.0 5.0 4.0 3.0

0.010.8011.0011.2011.40 11.60

nin 2.0 Ion 100.00 1.0 0.0 ,J „ Ll 1 .1,1 1

/1 02

\.\f 40 60 80 too 120 140 160 180

M/Z

ICO Scan 674 (11.128 Min) of k1338.d (x DIFFERENCE)

80 60

40 20 0

x ft 5•^^ V • o

-20 -40

-60 -80

-ICO 40 60 80 100 12O 140 16O 180 10.80 I t . 0011.20 I t . 4011.60

H/Z din

300JP

Data Fi le: /chen/hp5970k.i/960530.b/k1338.d

Date : 30-MHY-96 20:27

Cl lent ID: naic3 InstruMent: hp5970k.i

Sanple Info: 148540,naIc3,960530k, jpt,, 1770,GEI


Column phase: CRP Column dioneten: 0.53

27 Benzene

8.0 Scan 669 (11.063 nin) of k1338.d

8.01Ion 78.00

A

7.0g2

\ 7.5-!_ ;7.0-:

AI li M 6.0 6-5J

~ 5.0 6.0-: o

*% 3 3.0 1 S^s- l >• 2.0

1.0

0.0 40 60

1 11

1 i 80

hlli 100

/115 /

1 120 140 160 180 200 220

258\ \

I 240

$>x^

"

^°1 3.5-: 3.0J

2 '5^ 2.0-i

/

1

6.0

Scan 6^9n/z

(11.063 nin) of k1338.d (Subtracted) 1 ,5-i

•'•°i0-5^0 0 !A

1 )

f/

\ H

\\ l\ iA 10. 60 10. 80 1 1 .00 1 1 . 20 11 .40

5.0 __ nin \ o 4.0

Data Fil e : /chen/hp5970k. i/960530.b/k1338.d

Date : 30-MFIY-96 20:27

Cl lent ID: naic3 Instrunent: hp5970k.i

Sanple Info: 118540, naic3 ,960530k, jpt,, 1770, GE I

Purge Voluiie: 5.0 Operator: jpt

Colunn phase: CRP Colunn dianetcr: 0.53

29 Trichloroethene Scan 805 (12.845 Hin) of k1338.d Ion 130.00

13O-" 4.2, 4.0 4.0-; 3.6 3.8-! 3.2 3.5^ 2.8 3.2-;

3.0^ 2.8-i

2.4 2.0 2.5-i

2.2\ 1.2 o 2.0-i 0.8 U6 £ 1.8-;

X 1.5-i 0.0

40 50 60 70 80 90 1OO 1 10 120 130 H/z 0.8-1 Scan 805 (12.845 Hin) of k1338.d (Subtracted) 0.5-j 95-'- 130-"'

4.0 0.2-i 3.6

12.4012.6012.8013.0013.20 3.2 Hin 2.8 Ion 95.00 2.4

4.0^ 2.0 3.8-j 1.6 3.5^ 1.2 0.8 0.4 2.8^ 0.0 2.5-i

40 50 60 70 60 90 100 110 120 130 2.2J M/z 2.0-i

29 Trichloroethene (Rc |Spnce Spect run) 10.0 9.0 8.0

7.0 0.8-i 0.5^

5.0 0.0-4.0

12.4012.6012.8013.0013.203.0 nin 2.0 Ion 97.00 1.0 0.0 I, .. i , i

40 50 60 70 80 90 100 110 120 130 M/Z

Scan 805 (12.845 din) of k1338.d (x DIFFERENCE) ICO 80 60

40 I30\20 X37 X67 7v H • ,,... L. -20

-40

-60 -80

•100 40 50 6O 70 80 90 100 1 JO 120 130 12.40 12.60 12.80 13. CO 13.20 _aZz_ ttiD

30048

http:12.4012.6012.8013.0013.20http:12.4012.6012.8013.0013.20

Data File: /chen/hpS970k.i/960530.b/k1338.d

Date : 30-MRY-96 20:27

Cl ient ID: naic3 Instrunent: hp5970k.1

Sanple Info: 118510,naic3,960530k,jpt,,1770,GEI


Column phase: CflP Colunn diaHetcr: 0.53

33 1-ttethyl-2-Pentonone

5.0 13'

Scan 1038 (15.900 hin) of k1338.d 5-2:

Ion 13.00

1.51.0 3.5 3.0 2.5

x 2.0 1.5 5v 1.0 0.5 0.0

/>* /" T1 1 10 50 60 70 80 90 100

M/r

5.0 pan 1038 (15.900 nin) of k1338.d (Subtracted)

1.5 1.0 15.6015.8016.0016.20 3.5 Bin

3.0 Ion 58.00

2.5 x 2.0

1.0

0.5

0.0 X1

7\ 9\

10 50 60 70 80 90 100 H/Z

10.0 33 1-Mcthyl-2-Pentonone (Reference Spectrun)

9.0 8.0 7.0 6.0

Data Fi le: /chcn/hp5970k.i/960530.b/k1338.d

Date : 30-MRY-96 20:27


Sahiple Info: 148540,naic3,960530k, jpt,, 1770,GEI

Purge Volui-ie: 5.0 Operator: jpt

Colurin phase: CRP Coluim diarieter: 0.53

•5

36 Toluene

7.0

Scan J£57 (16.280 Min) of k1338.d 7.5-:•» rt

! 7.0-^

Ion 91.00 t\ |\ 1

6.0 6.5^

~»r <

5.0

4.0

6.0-; 5.5^ 5-0-i

"x

>

3 O

2.0 x39

1.0

0.0 .illLii...Jk . .mill. >40 60

hi *>. t 80

,100 c

120 140 160 180 200 ^

- 4.5-::vr 4.0 2 3.5 5 3.0^ - 2.5-:

2.0^

1

1 M/Z 1.5^ \

Scan 1067 (1J3,280 Min) of k1338.d (Subtracted) 1.0-i / \

7.0 0.5Ho o 1

/ - -^

V ^

6.0 16.CO 16. 20 16. 40 16. 60 16.8 Kin

~ 5>0 Ion 92.00

T 4.0 \J

H 3-° ^\4.0-;3.8J

A/I 1

> 2.0

1.0

39 j/

3-5i3 2^** '

\ 11 1

I

0.0 1.1. Jl > /*U ^7 . _ _ I I 1 40 60 80 100 120

M/Z 140 160 180 200

"'? 2-5';

10.036 To luene91*^

(Reference Spectrun) ŝ* (i 1.8^

1 1

1 9.0

nO

8.0

7.0 6'°

*

- K5J:!•? n'fl10.8-;10.5-;;-n

/

/ iJ

.. J \\1\

V. .. 16.0016.2016.4016.6016.83.0- y-39

2.0 , 1.0 xlOO 0.0 1.1Jl ,

Min

40 60 80 100 120 140 160 180 200 M/Z

Scan 1067 (16.280 nin) of k1338.d (X DIFFERENCE)100, 80 60 40

X17 X9820 n

£ -2O 2 -40

-60 -80

-ICO 40 60 80 100 120 140 160 180 200

M/Z

30050


Date : 30-MRY-96 20:27

Cl lent ID: naic3 Instrument: hp5970k.i

Saiiple Info: 118510, nai c3,960530k, jpt,, 1770, GE I


Colui-in phase: CRP Colunn dianeter: 0.53

45 Ethyl benzene

scon ng4 (20.436 Min) of k1338.d Ion 106.00 9.0, SI 3.0-: 1 8.0 2-8: I 7.0 2'6^ \ \6.0 2-^i \\ 1

« 5.0 ^ n2 4.0 /^ X106

10" « \

2 3.0 I '% »• 2.0

I 207 -x


Date : 30-MRY-96 20:27

Client ID: naic3 Instrument: hp5970k.i

SUMP Ie Info: 148540,naic3,960530k,jpt,,1770,GEI


Column phase: CRP Co I nun dianeter: 0.53

46 11 and p-Xylene

sca^y. 0 (20.777 Min) of k1338.d Ion 106.00 3.0; 1

6.0 2 -8 - 1

/"5.0 /*> 2-4^ |\ 1

x106 £ ^'0 <

:2o 3.0 "x «: M1 1S • r" 2.0 k -6^ /> 2 .4^

2J1 sc 11.0 i ^ 2 j I


NAIC30596DL Lab Name: NET CAMBRIDGE Contract: GEI

Lab Code: CAMBRG Case No. : SAS No. : SDG No.: 1855

Matrix: (soil/water) WATER Lab Sample ID: 148540DL







74-87-3 Chlorome thane 10 U 74-83-9 Bromome thane 10 U 75-01-4 Vinyl Chloride 10 U 75-00-3 Chloroethane 10 U 75-09-2 Methylene Chloride ~ 14 D 67-64-1 Acetone 50 U 75-15-0 Carbon Disulfide 10 U 75-35-4 1,1 -Dichloroethene 10 U 75-34-3 1,1 -Pi chloroethane 10 U 540-59-0 1,2-Dichloroethene (total) 40 D 67-66-3 Chloroform 10 U 107-06-2 1,2-Dichloroethane 10 U 78-93-3 2-Butanone 380 D 71-55-6 1,1,1-Tri chloroethane 10 U 56-23-5 Carbon Tetrachloride 10 U 75-27-4 Bromodichlorome thane 10 U 78-87-5 1, 2-Dichloropropane_ 10 u

10 u 18

124-48-1 10 U 79-00-5 1,1,2-Trichloroethane 10 U

10 u 32-6 trans -1,3-Dichloropropene_ 10 u 2 Bromof orm ~ 10 u

1-10-1 4 -Methyl-2 - Pent onone 50 u 591-78-6 2 -Hexanone 50 u 127-18-4 Tetrachloroethene 10 u

T -L ,7 ?-r . u79-34-R'JJ**J 1 -L , ̂ , ^ . 10 16 D

108-90-7 Chlorobenz ene_ 10 U 100-41-4 Ethylbenzene_^ 10 u 100-42-5 Styrene 10 u 75-69-4 10 u

FORM I VOA 3/90





Sample wt/vol: 5.000 (g/mL) ML

Level: (low/med) LOW



Soil Extract Volume: (uL)

CAS NO. COMPOUND

1 fiP-fi^-4. i i n-7^-fl

QC_A*7-£ CA~\ _7*a _i

i n£-4.£-7 qc en 1- yo~3'J~ -L

NAIC30596DL Contract: GEI


Lab Sample ID: 148540DL

Lab File ID: K1393






10 u 10 u 10 u 10 u 10 u 10 u 10 u

FORM I VOA 3/90

o o o o -o c/> r> o o

C C5 *> B 3 W — 33 » / • » • • -n • D O O — 3- — 3 O — O B c -n » i •• W 3 O t_ 19 » •• 3 C "V . . . . B Z O

— — I 3" o at -ik o — R 3D • CD U CD X•o O in o CD ^x

• ~ O> 3" 8 — Ol

3 tn co B •• >J — J> O O to ^ CO

CO

8 ID 88 8

•-BronochloroMethane (9.387) u CO u

-1,2-Dlchloroethane-d^ (10.931)+ >J

o


•-Toluene-d8 (16.111)+ o o o r> 3 — f> n c •» i S

o 3 a. •»

3

3

1

tn co

8Chlorobenzinc-d5 (20.008) p

en

Bronof luorobenzene (23.326)

r ?055

—

—

—


NET Cambridge

VOLATILE ISTD AND RATIO REPORT Data file /chem/hp5970k.i/960601.b/k!393.d Lab Smp Id 148540 Client Smp ID: naic3 Inj Date Ol-JUN-1996 15:42 Operator nmr Inst ID: hp5970k.i Smp Info 148540,naic3,960601k,nmr,2,1770,GEI Misc Info 1855,0,,,1,0,,,,,,,21-may-1996 Comment Method /chem/hp5970k.i/960601.b/kvoa.m Meth Date Ol-Jun-1996 15:01 Quant Type: ISTD Cal Date Ol-JUN-96 13:41 Cal File: k!390.d Als bottle 5 Dil Factor 2.000 Integrator HP RTE Compound Sublist: 8240.sub Target Version: 3.12 Concentration Formula: Uf * 1



CONCENTRATIONS



10 MeChylene Chloride 84.00 5.545 5. 518 (0 .591) 74334 6.76 13 . 53(aM)

14 1,1-Dichloroethane 63.00 7.210 7. 131 (0 .768) 95557 4.34 8. 69(aM)

16 2-Bucanone 43.00 8.915 9. 098 (0 .950) 120791 189 .90 379 .80(M)

18 1,2-Dichloroethene (total) 96.00 a.771 6. 122 (0.934) 118216 19 .87 39 .74(QM) * 20 Bromochloromethane 128.00 9.387 9. 334 (1 .000) 537599 50 .00

S 25 l,2-Dichloroethane-d4 65.00 10 .934 10. 881 (1 .165) 870620 50 .04 50 .04

26 1,2-Dichloroethane 62.00 11 .144 11. 078 (1 .187) 70459 3.50 7.00(a) * 28 1,4-Difluorobenzene 114.00 12 .206 12. 167 (1 .000) 2073310 SO .00

29 Trichloroethene 130.00 12 .862 12. 809 (1 .054) 161474 8.89 17 .78 (a)

33 4-Methyl-2-Pentonone 43.00 15 .891 15. 904 (0 .795) 256950 22 .04 44 .08

S 35 Toluene-d8 98.00 16 .114 16. 074

Data File: /chen/hp5970k.i/960601,b/k1393.d

Date : 01-JUN-1996 15:12

Client ID: naic3

Sanple Info: 118510,naic3,960601k,nnr,2,1770,GEI

Purge Volune: 5.0

Coluiin phase: CflP

Instrudcnt: hp5970k.i

Operator: nnr

Colunn dianeter: 0.53

10 llethylene Chloride

1.1

1.2

1.0

0.8

0.6

0.1

0.2

0.0

1.1

I.2

1.0

0.8

0.6

0.1

0.2

0.0

10.0 9.0 8.0

7.0 6.0 5.0 1.0 3.0

2.0 1.0 0.0

ICO eo 60

10 20 0

-20 -10

-60 -SO

-ICO

19-"* Scan 248 (5.515 din) of k1393.d Ion 81.00

Xs6

2 1.

10 50 60 70 80 H/Z

90

Scfin 218 (5.515 urn) of k1393.d

100 110 120

(Subtracted)

130

5.20 5.105.6O I1in

Ion 19.00

5.80 6.00

10 i. i

'35\ 50 60 70 80

H/z 90 1 0 0 1 1 0 1 2 0 1 3 0

10 llethylene Chloride (Reference Spectrun)

X37 x70

5.20 5.10 5.60 Hin

Ion 51.00

5.80 6.00

10 50 60 70 80 H/z

90 100 HO 120

Scan 218 (5.515 Min) of k1393.d (x DIFFERENCE)

130

131

10 50 60 70 80 90 100 110 1 2 0 1 3 0 5.20 5.10 5.60 5.80 6.00 H/Z M i n

Data F i le : /cheii/hp5970k. i/960601 ,b/k1393.d

Date : 01-JUN-1996 15:42

Cl lent ID: naic3 Instrunent: hp5970k. i

Sai-iple Info: 118540,naic3,960601k,nun,2,1770,GEI

Purge Volune: 5.0 Operator: nnr


14 1i1-Dlchloroethane

\ 1i 1-Dichloroethane (Reference Spectrun)

63-" Scan 375 (7.210 Hin) of k1393.d Ion bJ. 00

i 9.0 8.0

7.0

9.0:

8.0-; I

J

~To x~

*"

6.0 5.0

«-•• 3.0

2.0 1.0 0.0

9.0 3 0• V'

40 ll

1

60 80 100 120 140 160

ISSD M/Z

/** A 00 / /120

, ll /Illll III 1 1 ill 1

375 (7.210 nin) of M393.d (Subtracted)

180

202 ^

1 200

7.0^

6.0-; ;

P 5.0^ o : x ^.o: %^

*• 3.0:

2.0^

1.0:

o o w A;6.80

A j\i,/ 1\MAAW

I \\\/ \

V . . fVVVU/»*

/'/ /

i

K

,

7.1: »6' 7.2 6 7.46 7.60 7.0 n n

~ 6.0 Ion 65. 00

C 5.0. 2.8:

~*"

3.0 2.0

1.0 0.0 ll 1

. \ \

/**

.ih .il ll 11 ill1 f

X120 /1 ^2 ^1

2.6: 2.4: 2.2: 2.0: 1.8:

if

JnfV

40 60 80 100 120 140 160 180 200 o 1-6: H/Z O 1.4:

10.0, 63-^ "x 1.2: N^

9.0 >. i.o-i / 8.0 0.8-: 7.0 0.6: /

0.4: 6'° o0.2: i> 5.0

(iki — a Q 0.0: f

X T . V

6.80 7.CO 7.2< D 7.40 7.60 3.0 o- nni 2.0 / Ion 83. 00 1.0 X102 li i.e.: 0.0 h. , A .11, \\( '

40 60 80 100 120 140 16O 180 200 1.6H/Z

Scan 375 (7.210 Hin) of k1393.d (x DIFFERENCE) 1.4^ ICC eo 1.2-' 60 i^ !

o i n ' 40 b^> :1 50 ^/73 1̂00 12o ?02 20 \ x 0.8-'

i 1

... 1 i., . . ..1. i i ~ '•II 'N* a ° .1. ' ' 1 ' *• 0.6- A£ -20 fl ,

2 -40 0.4J i , i J

-60 : 1 -60

°'2: I II 1-ICO o.o: ll 111 11 JlL 40 60 80 100 120 140 160 180 2OO 6. 8O 7.0 O 7.2< 5 7.40 7.60

H/Z Hi n

30058

Data File: /chen/hp5970k.i/960601,b/k1393.d

Date : 01-JUN-1996 15:42

Cllent ID: naic3 InstruHent: hp5970k.I

SaMple Info: 148540,naic3,960601k.nnr,2,1770.GEI

Purge Volune: 5.0 Operator: ntir

Colutin phase: CflP Colu im dianeter: 0.53

16 2-Butanone Scan 505 (8.915 tiin) of k1393.d Ion 43.00

9.0 8.0 7.0 6.0

5.0 4.0 3.0 2.0 168̂

X251 1.0 III III 0.0

H/Z

50 75 100 ?25 fs5 f75200 22"!250 275 300 325 h/z

Scan 505 (8.915 nin) of k1393.d (Subtracted) 9.0 8.0 7.0 Min

9.40

6.0 Ion 57.00 5.0 900

4.0 800 3.0 2.0 1.0

168v x251 32 700

600 0.0 I

SO 75 100 125 ISO 175 200 225 250 275 300 325 500 h/Z

10.0, 16 2-Butanone (Reference SpectruM) >. 400

9.0 300 8.0 7.0 200

6.0 1005.0 4.0 o. 3.0 8.80 9.00nin

9.20 9.40

2.0 Ion 72.00 1.0 0.0 ,1.1.

50 75 100 125 150 175 200 225 250 275 300325

Scan 505 (8.915 nin) of k1393.d (x DIFFERENCE) 100 80 60

168v X251 20

0 -20 I

-40 -60^ -80

-1COJ 50 75 1OO 125 150 175 200 225 250 275 300325 8.80 9.00 9.20 9.40

H/Z _ "In

3005?

Data F i l e : /chen/hp5970k.i/960601.b/M393.d

Date : 01-JUN-1996 15:12

Cllent ID: naic3

Sanple Info: 148540,naic3,960601k,niir,2,1770,GEI

Purge Volume: 5.0

Colunn phase: CflP

18 1,2-Dichloroethene (total)

Scan 494 (8.771 Hin) of k1393.d 3.2, ^61

2.8

2.4- /

~ 2.0

• 0.8

0.4- A 67 252v /280 382

0.0- iL ii i L, , r , r >

Instrunent: hp5970k.i

Operator: nnr

Colunn diaiteter: 0.53

2.2

2.0^

1.8^

1.6:

1.4-; ? 1.2: 2 ,.0 = x :

oc y/wO 4 o^ *iCO lOA oe**20 /36 /• /167 252X ^80 482 x 0.7^ a ° 0.6-! »• I «•••••» »i **-• i i * « ,

E -20 *• 0.5J 0.4^ i -400.3^ -60 0.2-;

-80 0. 1-j-ICO Q 0 '*

40 80 120 160 200 240 280 320 360 M/Z ,

Ion 96.00

4.0 6.0Min

Ion 61.00

8.0

4.0 6.0Hin

Ion 98.00

8.0 Ii 1

jIJJ' M i n i n i i 1 III

4.0 6.0 8.0 HiC

300(70

3.2,

2.8

2.4

~ 2.0

£ 1.6

"x 1.2

>• 0.8

0.4

0.0

10.0, 9.0 8.0 7.0

0 ® ' ® '

< 5.0 o

i j. 3.0

2.0 I1 ft • V

0.6-j 40 80 120 160 200 240 280 320 360 h/Z OV • ~ 4-~

Scon 494 (8.771 hin) of k1393.d (Subtracted) 0.2^

/*"

3.2-. 3.0-: 2.8-: 2.6^ 2.4-:

/1 67 252\ y280 382 2.2-: I /il, In • i

40 80 120 160

J8 1 ,2-Dichloroethene^61

'

0.0 I I I . 40

ICO, 80 6O 40

ii i 80 120 160

Scan 494 (8.771 Min) of k1393.d (x DIFFERENCE) .2-1

•M r*. "0*

f 0.9\ 6 0.8-j

N / \i i i 2.0-:

200 240 280 320 360 ? 1. 8 -; M/Z < 16- ' (total) (Reference Spectrun) x I-'':

^ 1.2-:

0.8-j 0.6-! 0.4-: 0.2-i

.6-; .

5 jT 200 240 280 320 360 4 ' • ~™ M/Z

.3-1

Data File: /cheM/hp5970k.i/960601.b/k1393.d

Date : 01-JUN-1996 15:12


Sanple Info: 148540,naic3,960601k,nun,2,1770,GEI

Purge Volune: 5.0 Operator: niir

ColUMn phase: CRP Colunn dianeter: 0.53

26 I > 2-D i chI oroethane

-̂6 2 1.0 0.9 0.8 0.7

? 0.6 f

o 0.5 x O.4 ^^ _ 0.3 I

0.2 ll I0.1 UiLI 1 I)0.0 40 E10

an1.0 48 0.9 0.8

70 . / ' £ 0.6

0 n

x 4.0 3 • 0 •

2.0 1.0 ,1 ,b 0.0

40 £10

Scon 675 (11.144 Min) of k1393.d Ion 62.00

/1CC 252x 284vs^ x321

lllll 1 1 1 1 120 160 200 240 280 320 360

M/Z

675 (11.144 Min) of k1393.d (Subtracted)

10. 60 10. 80 11. 00 11. 20 11. 40 din

Ion 64.00 3.4^ I 3.2-j U 3.0-: R| 2.8-: 1 1

/'«> 252X 284, ,321 ll ^ * *'*^ 1 1 .lid 1 i i i I'ol / ll

120 160 200 240 280 320 360 2-Dichloroethane (Reference SpectruM) 5 '•

Data File: /chei-i/hp5970k. i/960601 .b/k!393.d

Date : 01-JUN-1996 15:12

Cl lent ID: naic3 Instrument: hp5970k.i

Scuiplc Info: 148540,naic3,960601k,nnr,2,1770,GEI

Purge Voluiie: 5.0 Operator: nnr


29 Trichlorocthene

Scan8j06 (12.862 nin) of k1393.d Ion 130.00 i

2.2 2.2-1 ll 2.0 : \\ 1.8 2'°: /1.6 1.8:

? ' - ^ 1.6

2 i!o /» ~ 0.8 -^ >- 0.6 1 -i

£ K0i0.2-

171X 224^ 35^ 1 \0.4 >• 0-8-: / IJli

40 80 120 160 2CO 240 280 320 0.6^ \ M/Z rt

0.0- lllU i I* lit i l i t i :

4:0.4, IIScan 806 (U,862 nin) of k1393.d (Subtracted)

2.2 0.2: / \ 2.0 0.0 ̂ IL ^ 1.8 12.4012.6012.8013.0013.20 1.6 Min

~^

1.4 . o

2-2-;

Ion 95.00

fl 2 KO i0.8

y6O/^ 2.0-: 1(1 >. 0.6 1.8:

0.4 0.2

17,x 224X 35^ 1.6-: 1 I

0.0 ,l,i 40

IM ill

80 120i

160 2CO i

240 280 320 i

^'•^•i

; 1 1

| j n/z * I 1

10.0. 22 Trichloroethene (Reference Spect run)

^95 ^£

1.0: ' '•

J 1 I I

9.0 > °-8: j 1 8.0 0.6-; I 1

£

Data F i l e : /chen/hp5970k. I/9606O1 .b/M393.d

Date : 01-JUH-1996 15:42

Cllent ID: naic3 Instrunent: hp5970k.i

Saiiple Info: 148540,naic3,960601k,nnr,2,1770,GEI

Purge Volune: 5.0 Operator: nnr

Colunn phase: COP Colunn dianeter: 0.53

33 4-nethyl-2-Pcntonone Scan 1037 (15.891 Hin) of k1393.d Ion 43.0O

3.2

2.8 2.4

- 0.8

0.4 103 145

0.0 10 60 80 100 120 110 160

n/2 33 4-Methyl-2-Pentonone (Reference Spectrun)

10.0 9.0 8.0 7.0 6.0 5.0 1-0

15.6015.8016.0016.2016.4 3.0 Hin 2.0 Ion 100.00 1.0 .6-! 0.0 .5-1

40 60 80 100 120 110 160 H/Z

Scan 1037 (15.891 Min) of k1393.d (x DIFFERENCE) 100 8O 60

0.9-! 10 0.8-1 20 103 0.7-!

0 0.6J -20 0.5,:

-10 0.4-i

-60 -80

0.3^ 0.2\ o.i-:

-100 0.0-=40 60 80 100 120 140 160 15.6015.8016.0016.2016.1

ttifl

300(7.?

Data F i le : /chen/hp5970k.i/960601.b/k1393.d

Date : Ol-JUN-1996 15:12

Cl ient ID: naic3

SUMP Ic Info: 118510,naic3,960601k,nnr,2,1770,GEI

Purge Volume: 5.0

Colui-m phase: CflP

36 Toluene Scan 1067 146.281 Min) of k1393.d

1.1 1.0 3.6 3.2

~ 2.8 T 2.1 2 2.0 i 1.6 >- 1.2

0.8 0.1 0.0

1.1 1.0 3.6 3.2

~ 2.8 T 2.1 2 2.0 £ 1.6 >- 1.2

0.8 0.1 O.OJ

10.0, 9.0 8.0

7.0 £ 6.0 £ 5.0

~ 3.0

2.0 1.0 0.0

ICC, 80 6O

40 20

3

E -20 i -40

-6O -80

-100

ill tnli .III,, illiL 1. i .li| .40 60 80 160

M/Z

Scan 1067 (16.281. win) of"•^•91

X39 /*

III II I, «lll,l llllll , . .> .1 1. 1 1,1 .10 60 80 100

M/Z

X121 r 12O 140

Instrunent: hp5970k.I

Operator: niir

Colunn diaMeter: 0.53

Ion 91 .00

3.6: M

3.2: |

^ 2'9~ \

12'°^ 1 1


NAII0596 Lab Name: NET CAMBRIDGE Contract: GEI









74-87-3 Chlorome thane U 74-83-9 Bromotnethane 5 U 75-01-4 Vinyl Chloride 5 U 75-00-3 Chloroethane 5 U 75-09-2 Methylene Chloride 5 U

25 U 75-15-0 Carbon Disulf ide 75-35-4 1,1-Dichloroethene 75-34-3 1,1-Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform [ 107-06-2 1,2-Dichloroethane

555555

U U U U U U

78-93-3 2- But anone 25 U 71-55-6 1,1,1-Trichloroe thane 56-23-5 Carbon Tetrachloride 75-27-4 Bromodi chlorome thane 78-87-5 1,2-Dichloropropane 10061-01-5 cis-l,3-Dichloropropene 79-01-6 Trichloroethene

•5 1,1/2 -Trichloroe thane

•02-6 trans -1,3 -Dichloropropene_ • 2 Bromof orm

55555555555


)-l 4-Methyl-2- 25 U 1-6 2 - Hexanone 25 U

127-18-4 " 79-34-5 1,1,2, 2-Tetrachloroethane

108-90-7 Chi orobenz ene 100-41-4 Ethylbenzene 100-42-5 Styrene__^ 75-69-4 Trichlorofluorome thane

5555555

U U U U U U U

FORM I VOA 3/90


NAII0596 Lab Name: NET CAMBRIDGE Contract: GEI









T riG — fiC. A — 5 U T i n 7C. f t J.J.U" /3— O 5 U

5 U QCy3 A 7 _ £ * ± / ~ o ""AyJ-SIIc 5 U CA.1 _7"1 -1 . 5 U 1 n£-A£_7 5 U QC crj-1 5 U

FORM I VOA 3/90

Y (x10~6)

O O O TI O) O O O O C C — P C — " 5 3 — ft ft c o T> a n c 3 W — 3 3 » — (D W 3> • 00 O> 3 •O O Ol -V

U -" 3" Jl CD -O - •• Ol 3 J» CO C ^ if

(O

8 Ol sM (O 01

•-Brotiochloronethanc (9.410)

8 K>

•-1,2-Dichloroethane-d4 (10.941)

•-1>1-Difluorobenzene (12.215)

•-Toluene-dS (16.109) 0 O

— "°

1 1 I c

O 3 a. -> B̂. •»

§ p> -o r» *-» (O •O T Ol

roO"

Ch7orobenzene-d5 (20.002) Ol U

BroMof luorobenzenc (23.319)'

ro O>

f

Data File: /chem/hp5970k.i/960529.

4> gei consultants inc.mr. bob mullin gei consultants/nh suffolk building 53 regional drive concord,...

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