5 :u · 2020. 12. 13. · 3 3g2 1a epa sample volatile organics analysis data sheet ____ lab name:...

/ IA EPA SAMPLE NCrry*• VOLATILE ORGANICS ANALYSIS DATA SHEET _____________

1 5I VBLK5029OH !

.ab Name: CAMBRQ_______________^Contract: NOVAK_____ !___________!

_ab Code: CAMBRQ Case No. : NOVAK3 SAS No. : ______ SDC No. : _____

latrix: (coil/uater) HATER Lab Sample ID: 6306 043090

Sample ut/vol: 5. 0

3 349

IE EPA SAMPLE NO.(,' VOLATILE ORGANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDS !{ VBLK50290H

,ab Name: CAMBRG________________ Contract: NOVAK_____ !__________

_ab Code: CAMBRQ Case No. : NOVAK3 SAS No. : ______ SDG No. :

latrix: (soil/mater) WATER Lab Sample ID: 6306 043090

Jample ut/vol: 5. 0 (g/mL) MJ._ Lab File ID: H3515_____

.evel: (lou/med) LOU Date Received: ______

Moisture: not dec. ___ Date Analyzed: 05/05/90

olumn (pack/cap) PACK Dilution Factor: 1. 0______

CONCENTRATION UNITSumber TICs found: _0 (ug/L or ug/Kg) UG/L

CAS NUMBERsssssszsxssssssss

COMPOUND NAME RTSSSBCSSSS

£57======

CONC.======

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&R300807T i in A —••*»

3 351A EPA SAMPLE N

VOLATILE ORGANICS ANALYSIS DATA SHEET ___

I VBLK30390K_ao Name: CAM3RG________________ Contract: NOVAK_____ !__________

.ab Code: CAMBRG Case No. : NOVAK3 SAS No. : ______ SDG No. :

Matrix: (soil/water) WATER Lab Sample ID: 6306-Q5Q390

Sample ut/vol: 5. 0 (g/mL) ML___ Lab File ID: K5559______

.evel: (lou/med) LOW Date Received: _______

. Moisture: not dec. ___ Date Analyzed: 05/03/90

clumn: (pack/cap) PACK Dilution Factor: 1 0_______

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UQ/L Q '

74-87-3————————Ch loromethane___________74-S3-9———————Bromome thane____________75-01-4———————Vinyl Chloride__________75-00-3————————Ch loroethane____________75-09-2———————Me th y 1 ene Ch i or i d e______67-64-1———————Acetone________________75-15-0———————Carbon Disulfide________75-35-4———————1, 1-Dichloroethene_______75-34-3———————1. 1-Dich loroethane__________54O-59-0———————1. 2-Dichloroeth»ne (total).67-66-3————————Chloroform______________107-06-2———————1. 2-Dich loroethane_______78-93-3———————2-8 u tan one______________71-55-6———————I/ 1» l-Trichloroathane____56-23-5———————Car b on Te trac h 1 or i d e_____108-05-4———————Vinyl Acetate___________75-27-4———————Bromod ich 1 oromethane_____78-87-5———————1. 2-Dich loropropane______1O061-01-5—————cis-1* 3-Dichloropropene__79-01-6———————Trichloroethene_________124-48-1——————Dibromoc hi oromethane_______79-00-5———————1. 1* 2-Trichloro»thane____71-43-2———————Benzene_______________1O061-02-6————tran s-1» 3-Dichloropropen»__75-25-2———————Bromof orm_______________________10B-10-1——————4-M*thyl-2-Pentanone____591-78-6——————2-H»xanone____________127-18-4——————Te trac hi or oe th ene______79-34-5———————1» 1» 2. 2-T»trachloroethane.108-88-3——————Toluene_______________108-9O-7——————Chlorobenzene_________10O-41-4——————Ethyl benzene__________100-42-5——————S t y r » n 9 _______________1330-2O-7—————Xyluna (total)_________

10 :u10 :u10 ;u10 !Us :u

16 i5 :u5 ;i?5 :u5 :u5 :u5 :u10 :u5 ;u5 :u

10 :u5 :u5 :u5 :u5 :u5 :u5 :u5 :u5 :u5 ;u10 :u10 !U5 ,'U5 !U5 :u5 !U5 :u5 :u5 :u

3 35IE EPA SAMPLE NO

I ) VOLATILE ORCANICS ANALYSIS DATA SHEET-̂̂ TENTATIVELY IDENTIFIED COMPOUNDS

! VBLK50390KLab Name: CAMBRG________________ Contract: NOVAK_____ !__________

_ab Code: CAMBRC Case No. : NOVAK3 SAS No. : ______ SDG No. :

"latrix: (soil/water) WATER Lab Sample ID: 6306-050390

sample ut/vol: 5. 0 (g/mL) __L_ Lab Fil« ID: K5559__________

_evel: (low/med) LOW Date Received. ______

" Moisture: not dec. ___ Date Analyzed C5/C3/90

Tolumn (pack/cap) PACK Dilution Factor- 1 0____

CONCENTRATION UNITS.'umber TICs found: _0 (ug/L or ug/Kc) UG/L

CAS NUMBER COMPOUND NAME===S===S====B=E=BSX:=BESB=B==

i ii »! RT !! === = = = = = j S£

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RR300809

3 3G21A EPA SAMPLE

VOLATILE ORGANICS ANALYSIS DATA SHEET ____

Lab Name: CAMBRQ________________ Contract: NOVAKV8LK50590K

Lab Code: CAMBRQ Case No. : NOVAK3 SAS No. : ______ SDC No.:

.latrix: (soil/water) WATER Lab Sample ID: 6306-053090

Sample ut/vol: 5. O (g/mL) ML Lab File ID: K2573______

Level: (lou/msd) LOW Dat* Received: _______

" Moisture: not dec. ___ Date Analyzed: 05/05/̂ 0

Islumn: (pack/cap) PACK Dilution Factor: 1. 0_____

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L

74-87-3————————Chloromethane_______________74-83-9————————Bromomethana__________________75-01-4————————Vinyl Chloride_____________75—OO-3————————Ch loroethane____________75-O9-2———————Methyl ene Chloride______67-64-1————————Acetone________________75-15-O————————Carbon Disulfid*_________75-35-4————————1. 1-Dichloroethene_______75-34-3————————1. 1-Dich loroethane________54O-59-O———————1, 2-Dichloroethsne (total).67-66-3————————Chloroform______________107-06-2———————I, 2-Dich loroethane__________78-93-3————————2-3 ut anon e_____________71-55-6———————I, If 1-Trich ioroethane____56-23-5————————Carbon Tttrachloride_____108-O5-4———————Vinyl Acetate___________75-27-4———————Bromod ich 1 oromethane_____78-87-5————————1. 2-Dich loropropane______10061-01-5—————cis-1. 3-Dich loroproptne__79-01 -6————————Tr ichloroeth en *_________124-48-1———————Dibromoch 1 or om* thane_____79-OO-5————————If 1. 2-Trichloro»than»____71-43-2———————Benzsne_______________10O61-02-6—————trans-1. 3-Dichloropropene_73-25-2————————Bromo f~brm__________________108-10-1——————4-Methyl-2-Pentanone_______391-78-6——————2-Hexanone_____________127-18-4——————Tetrachloroethene__________79-34-5———————1. If 2* 2-Tetrachloroethane__108-88-3——————To 1 u e n e ________;____________1OS-9O-7——————Ch 1 or ob *nz en e__________100-41-4——————Ethyl b en z ene___________1OO-42-5———————Styrene________________1330-20-7—————Xylene (total)__________

10 !U10 :u10 :u10 :u5 !U15 :s :u5 :u5 ,'U5 ju5 :u5 !U10 :u5 :u5 :u10 :u5. :u5 IU5 !U5 ;u5 :u5 iU5 !U5 JU5 !U10 :u10 :u5 :u5 JU5 :u5 !U5 !U5 !U


(J VOLATILE ORGAN I CS ANALYSIS DATA SHEET^ '

_____________ /TENTATIVELY IDENTIFIED COMPOUNDS (

VBLK50590K_ab Name: CAMBRC _________________ Contract: NOVAK _____

_ab Code: CAMBRC Case No. : NOVAK3 SAS No. : ______ SDG No. :

latrix: (soil/water) WATER Lab Sample ID: 6306-053Q90

Sample ut/vol: 5. 0 (g/mL) ML. Lab File ID: K2573________

.evel: (lou/med> LOW Date Received: _______

. Moisture: not dec. ___ Date Analyze,: 05/05/90

.lunn (pack/cap) PACK Dilution Factor 1 0____

CONCENTRATION UNITS.r TICs found: _0 (ug/L or ug/Kg) UG/L

CAS NUMBER================

COMPOUND NAME============================

„ - , . . ,

• i: RT :j ======== •i i

E5T. CONC G===========SB =====

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AR3008It

4 344

IB EPA SAMPLESEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

I SBLK42790J_ab Name: CAMBRQ ________________ Contract: NOVAK _____ I

_ab Code: CAMBRQ Case No. : NOVAK3 SAS No. : ______ SOS No. :

latrix: (soil/water) WATER Lab Sample ID: 9003213-BLK2R

Sample ut/vol: 1000 (g/mL) Ml,_ Lab File ID: J6936_____

.evel: (lou/med) LOW Data Received: _______

Moisture: not dec. ___ dec. ___ Date Extracted: 04/57/90

ixtraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 05/01/9Q

PC Cleanup: (Y/N) fcj_ pH: 7. 0 Dilution Factor: 1. 0

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg> UG/L

108-95-2 ————111-44-4 ————95-57-8 —————541-73-1 ————106-46-7 ————100-51-6 ————95-50-1 —————93-48-7 —————w * OwO Jtt ™_L WQ *T*T J« — »~

621-64-7 ————67-72-1 —————98-95-3 —————78-59-1 —————_%«_T^«_a __BS—73—3————————105-67-9 ————65-83-O —————111-91-1 ————120-83-2 ————« on_.Q̂ _. 1 _______ _JO— oS— 1 —— —— •91-20-3 —————1O6-47-8 ————87-68-3 —————BO ~/\ T _3*7—3Q— • /— ——— ——Ol _17_A.—— —— — —T 1 9 t O ̂^ —77-47-4 —————B8-O6-2 —————T— 1 " W *tVA — wt> /RP—7-1— A——— — ——OtJ / *? *T —131-11-3 ————«iUO TO O————

606-20-2 ————

—— Phenol—— bis(2-Chloroethyl)Ether—— 2-Chloroohenol—— 1* 3-Dichlorobenzene—— 1» 4-Dichlorobenzene—— Benzyl Alcohol—— If 2-Dichlorobenzene—— 2-Mathyl phenol—— b.5(2-Chloroisopropyl)Ethe—— 4-Msthul phenol—— N— Nitroso-Di-n-Propy lamine—— He xach loroethane—— Nitrobenzene—— Isophorona—— 2-Nitroohenol—— 2f 4-Dimethylphenol—— Benzoic Acid—— -b i s (2-Ch lor oe thoxy )Ma thane—— 2, 4-Dichlorophenol—— 1* 2* 4-Trichlorobenzene—— Naphthalene „—— 4-Chloroaniline—— Hexachlorobutadiene _.—— 4-Ch 1 or o— 3-Me th

4 3451C EPA SAMPLE NO.

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _____________

I SBLK42790J ILab Name: CAMBRG________________ Contract: NOVAK_____ I___________\

_ab Code: CAMBRG Case No. : NOVAK3 SAS No. : _____ SDG No. :

latrix: (soil/water) WATER Lab Sample ID: 900321S-BLK2R

Sample wt/vol: 1000 (g/mL) __-_ Lab File ID: J65S6_____

.evel: (lou/med) LOW Date Received: ______

'. Moisture: not dec. ___ dec. ___ Date Extracted: 04/27/90

:xtraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 05/01/90

JPC Cleanup: (Y/N) N_ pH: 7. 0 Dilution Factor: 1. 0


1 • 11 1S 99-09-2 ——————— 3-Nitroaniline ! 50} B3-32-9 ——————— Acenaohthene51-28-5 ——————— 2, 4-Dinitrcphenol100-02-7 ——————— 4-Ni tr op h eno 1 . ...

! 10! 50i 50

132-64-9 ——————— Dibenzofuran S 10121-14-2 ——————— 2, 4~Dinitro toluene,S4-66-2 ——————— D iethylohthalate7005-72-3 ————— 4-Ch lor op henyl-phenyl ether __86-73-7 ——————— Fluor ene100-10-6 —————— 4-Ni troani line .„„534-52-1 ——————— 4f 6-Dinitro-2-Methylphenol __86-30-6 ——————— N-Nitrosodiphenylamine (l) __101-55-3 ———— • — 4-Bromop henyl-phenyl ether ___118-74-1 —————— Hexachlorobenzene87-86-5 — ————— Pen ta c h 1 or op h eno 185-O1-B ——————— Phenanthrene______120-12-7 ——————— Anthracene __ ,..,S4-74-2 ——————— Di-n-Butylphthalate .2O6-44-O ——————— Fluoranthene __129-OO-0 ————— -PyreneS5-6B-7 ———————— Butylbenzylphthalate.91-94-1 ——————— 3, 3'-Bichlorobenzidine .,_,„, .56-55-3 —— — —— Benzo (a) Anthracene ,_218-O1-9 ——————— Chrysene117-81-7 —————— bis(2-Ethylhexyl)Phth«late __117-04-0 ——————— Di-n-Octyl Phthalate2O5-99-2 —————— Benzo (b)Fluoranthene .2O7-08-9- ———— -Benzo (k)FluorantheneSO-32-8 —————— Benzo

I Wl\l I _ _(*

4 34?

IF EPA SAMPLESEMIVOLATILE ORGANICS ANALYSIS DATA SHEET __________

TENTATIVELY IDENTIFIED COMPOUNDSI SBLK42790J J

_ab Name: CAMBRQ_______________ Contract: NOVAK_____ !____________J

_ab Code: CAMBRQ Case No. : NOVAK3 SAS No. : _____ SDG No. : _____

latrix: (soil/water) WATER Lab Sample ID: 9003513-BLKSR

Samp 1» ut/vol: 1000 (g/mL) ML_ Lab File ID: J6556______

.aval: (lou/med) LOW Date Received: ______


xtraction: (SepF/Cont/Sonc> SERF Date Analyzed: 05/01/90

PC Cleanup: (Y/N) N_ pH: 7. 0 Dilution Factor: 1. 0

CONCENTRATION UNITS:umber TICs found: _0 (ug/L or ug/Kg) UQ/l

NUMBER J COMPOUND NAME J RT ! EST. CONC.

AR3008U

4 35,

IB EPA SAMPLE NO.SEMIVOLATILE ORCANICS ANALYSIS DATA SHEET ___________

I II SBLK43090J J

Lab Name: CAMBRQ_______________ Contract: NOVAK_____ J_______________i

_ab Code: CAMBRQ Case No. : NOVAK3 SAS No. : _____ SDC No. :

latrix: (foil/water) WATER Lab Sample ID: 9004279-BLK1

Sample wt/vol: 1OOO (g/mL) __L_ Lab File ID: J6754_____


: Moisture: not dec. ___ dec. .___> Date Extracted: 04/30/90

Txtraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 05/17/9O

••PC Cleanup: (Y/N> _J_ pH: 7. O Dilution Factor: 1. 0

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg> UC/L

108-95-2——————Phenol__________________ 10 JU111-44-4——————bis(2-Chloroethyl)Ether_____ 10 JU

!U

541-73-1 —————— If 3-Dichlorobenzene106-46-7 —————— If 4-Dichlorobenzene100-51-6 —————— Benzul Alcohol _95-50-1 ——————— If 2-Dichlorobenzene95-48-7 ———————— 2-Methylohenol39638-32-9 ———— bis (2-Chloroisopropyl )Ether _106-44-5 ——————— 4-Methylphenol ,621-64-7 ————— • — N-Nitroso-Di-n-Propylamine __67-72-1 ——————— Hexach loroethane98-95-3 ———————— Nitrobenzene78-59-1 ——————— IsophoroneBB-75-5 ———————— 2-Ni trophenol .105-67-9 ——————— 2f 4-Dimethylphenol ,_,.„65-B5-O ———————— Benzoic Acid111-91-1 —————— b is (2-Chloroethoxy)Me thane __120-83-2 —————— 2, 4-Dichlorophenol__12O-B2-1- —————— If 2f 4-Trichlorobenzenen 4 *̂ f\ *9.. «.«.kt K«k4.k»klM*ltfKvi— zo— 3— ̂ — — —— Naphthalene106-47-B —————— 4-Ch lor can i line.B7-68-3 ——— - ——— -He xac h 1 or ob utad i ene59-50-7 ———————— 4-Chloro-3-M*thylphenol91-57-6 ——————— 2-Methylnaphthalene...... ,77—47-4- —— — — — — Hexaehlorocuclopentadiene88-06-2 ——————— 2. 4. 6-Trichlorophenol95-95-4 ———————— 2* 4. S-Trichlorophenol ..,„91-5B-7— —— — —— — 2-Ch lor onaph thai ene_ ___BB-74-4 ———————— 2-Ni troani line,131-11-3 ——————— Dimethyl Phthfllate__ ..,„„.2O8-96-8-—— • —— -AcenaphthylentA06-20-2 ——————— 2. 6-Dinitrotoloen*. _ .„_. _

10101010101010101010101010501010101010101010i nIV105010so1010ffl_ _affto

4 352

1C EPA SAMPLE NfSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ___________J_=X

J SBLK43090J J_ab Name: CAMBRQ_______________ Contract: NOVAK_____ I____________J

.ab Code: CAHBRQ Case No. : NOVAK3 SAS No. : _____ SDG No. :

latrix: (soil/water) WATER Lab Sample ID: 9004279-BLK1

sample ut/vol: 1000 (g/mL) ML__ Lab File ID: J6734_______

.aval: (lou/med> LOW Date Received: ______

. Moisture: not dec. ___ dec. ___ Date Extracted: 04/30/90

ixtraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 05/17/90


CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/t

99-09-2 ——————— 3-Nitroaniline33-32-9 ——————— Ac enaphthene51-2B-5 ——————— 2. 4-Dinitroohenol1 OO-O2-7 ——————— 4-N itroohenol132-64-9 ——————— Dibenzofuran121-14-2 ——————— 2f 4-Dinitrotoluene84-66-2 ——————— Diethuloh thai ate7005-72-3 ————— 4-Chloropheny 1-pheny 1 ether __86-73-7 ——————— Fl uor ene100-10-6 ——————— 4-Ni troani line534-52-1 —————— 4f 6-Dinitro-2-Me thy 1 phenol __86-3O-6 ——————— N-Nitrosodiphenylamine (1) __101-55-3 —————— 4-Bromoph eny 1-ph eny 1 eth er ___118-74-1 —————— Hexachlorobenzene87-86-5 ——————— Pentachloroohenol8 5-0 1 -8 ——————— P henanthrene12O-12-7 ——————— AnthraceneB4-74-2 ——————— D i -n-B u t u 1 D h t h a 1 a t »2O6-44-O ——————— Fluoranthene129-OO-O ——————— Pyrene., ._„..._.B3-6B-7 ——————— -Bo t«j 1 b en z y 1 t>h th a late91-94-1 ——————— 3. 3'-Dichlorobenzidin»36-33-3 ——————— Ben zo ( a TAnthrac en e2 1 B-0 1 -9 —————— C h r y s e n e117-31-7 —————— bi*FluorantheneSO-32-3 ——————— Benzo(a)Pyrene193-39-5 —————— -Indenodf 2f 3-cd)Pyrene53-70-3 —— ~ ——— Dibenz(af h)Anthracen»191-24-2 —————— Benzo (t)f h< i)Perylene

JJ

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JSI11JI

JJSI

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5010505010101010105030101010501010101010102010101010101010101010

11JUIU:u:uJU:uJUJU:u:u!U:u:u,'UJU:uJU:u:uJUJUJUIU:u:uJUJU:uIUJUIU IJBR3Q

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0816(1) - Cannot be separated from Diphanylamine

4 35

IF EPA SAMPLE NO.CS ANALYSIS DATA £

TENTATIVELY IDENTIFIED COMPOUNDS[} SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

i SBLK43090J J.ab Name: CAMBRQ____________________ Contract: NOVAK_____ I____________!

.ab Code: CAMBRQ Case No. : NOVAK3 SAS No. : ______ SDC No. : _____

•atrix: (soil/water) WATER Lab Sample ID: 9004279-BLK1

ample ut/vol: 1000 (g/mL) __L_ Lab File ID: J6754_____

evel: (low/med) LOW Date Received: ______

Moisture: not dec. ___ dec. _nmr. Date Extracted: 04/30/90

xtraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 05/17/90

3C Cleanup: (Y/N) N_ pH: 7. O Dilution Factor: 1. 0

CONCENTRATION UNITS:jmber TICs found: ._p_ (ug/L or ug/Kg) UQ/L

J i JCAS NUMBER ! COMPOUND NAME ! RT ! EST. CONC.

w - -;; .fiR3008!7

O/ r\ —v.

IB EPA SAMPLE NOTSEMI VOLATILE ORGANICS ANALYSIS DATA SHEET

I S3LK50390J I.ab Name: CAMBRQ ________________ Contract: NOVAK _____ J _____________ }

_ab Code: CAMBRQ Case No. : NOVAK3 SAS No. : _____ SDQ No. : ____

tatrix: (soil/water) WATER Lab Sample ID: 9004290-3LK

Sample ut/vol: 1000 (g/mL) ML_ Lab File ID: J6909_____

.aval: (lou/med) LOW Date Received: ______

Moisture: not dac. ___ dec. ___ Date Extracted: 05/03/90

xtraction: (SepF/Cont/Sonc) CONT Date Analyzed: 05/31/90

?C Cleanup: (Y/N) N_ pH: 7. 0 Dilution Factor: 1. 0

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UQ/L

1 09-9 3-2 —————— P h e n o 1111-44-4 ——

341-73-1 ——106-46-7 ——100-51-6 ——95-50-1 ———

106-44-5 ——621-64-7 ——67-72-1 ———98-95-3 ———78-59-1 ———88-75-5 ———103-67-9 ——

111-91-1 ——120-83-2 ——

91-20-3 ———106-47-8——o/— otJ— J——59-30-7 ———

77-47-4 ———

93-95-4 ———91-38-7 ———8B-74-4 ———

• m _1 1 _.*3_._—

S 208-96-8 ——I 606-20-2 ——!

———— bis

4 361C EPA SAMPLE NO.

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET .

i SBLK50390J J.ab Name: CAMBRG ____________________ Contract: NOVAK _____ t _______ !

.ab Code: CAHBRQ Case No. : NOVAK3 SAS No. : _____ SDC No. : _____

•atrix: (soil/water) WATER Lab Sample ID: 90042SO-BLK

ample ut/vol: 1000 (g/mL) £___ Lab File ID: J6909_____

evel: (lou/med) LOW Date Received: ______


xtraction: (SepF/Cont/Sonc) CONT Date Analyzed: 05/31/90

3C Cleanup: (Y/N) N_ pH: 7. 0 Dilution Factor: 1. 0


99-09-2 ——————— 3-Ni tr oani 1 ine .83-32-9 ——————— Acenaphthene ,51-28-5 ——————— 2, 4-Dinitrophenol100-02-7 ——————— 4-Nitrophenol132-64-9 —————— Di b en z of uran121-14-2 —————— 2, 4-Dinitrotoluene84-66-2 —————— — DiethylPhthalate

86-73-7 ——————— Fluor ene _.100-10-6 —————— 4-Ni troani line ..534-52-1 —————— 4f 6-Dinitro-2-Methyl phenol __B6-3O-6 ———————— N-Nitrosodiphenylamine (1)101-55-3 —————— 4-Br omop h eny 1-p h eny 1 e th er ___

87-86-5 ——————— Pentachlorophenol85-01-8 ——————— Phenanthrene120-12-7 —————— -Anthracene..84-74-2 ——————— Di-n-Butulphthalate206— 44-O —————— Fluoranthene129-OO-O ——————— Pyrene85-68-7- —————— Butylbenzylphthalate91-94-1 ——————— 3, 3'-Dichlorobenzidine56-55-3— —— - ——— Benzo(a)Anthracene218-O1-9 —————— Chrycene117-81-7 —————— bis(2-Ethylhexvl)Phthalate __117-B4-O —————— Di-n-Octyl Phthalate205-99-2 —————— Ben z o ( b >F1 uoranth ene207-08-9 —————— Benzo ( k )FluorantheneSO-32-B ——————— B enzo(a)Pyrene.,._ .193-39-5 —————— Indeno (1,2, 3-cd )Purene53-70-3 ——————— Dibenz(a, h) Anthracene191-24-2 —————— -Benzo(Gf hf i)Perylene

i

501050501010101010505010101050101010101010201O10310101010101010

1;uJU:u:uJUJU:uJUJUJU:uJUIUIUJUJUJU:uJU:u:uJU:uIUuxxxIU;uIUIUJUIU I

19__•_•. _____________ F» £_̂ _̂B̂ M»'

(1) - Cannot be separated from Diphenylamine

4IF EPA SAMPLE

SEMIVOLATILE OROANICS ANALYSIS DATA SHEET ___________TENTATIVELY IDENTIFIED COMPOUNDS !

I SBLK30390JLab Name: CAM3RQ________________ Contract: NOVAK_____ J__________

.ab Cods: CAMBRQ Case No. : NOVAK3 SAS No. : _____ SDG No. :

-latrix: (toil/water) WATER Lab Sample ID: 9004530-BLK

Sample uit/vol: 1000 (g/mL) ML_ Lab File ID: J6909_____

.evel: (lou/med) LOW Data Received: ______(


'xtraction: (SepF/Cont/Sonc) CONT Date Analyzed: 05/31/90


CONCENTRATION UNITS:umber TICs found: ___. (ug/L or ug/Kg)

CAS NUMBER J COMPOUND NAME J RT J EST. CONC. !3333 { 3333333333333333333333333333 J 33333333 J =333333333333 J :

I Unknown I 7. 30 ! 10 U

flR300820

r wnn _ o v — c. _ i o i n *t v .

IB EPA SAMPLE NO.SEMIVOLATILE ORCANICS ANALYSIS DATA SHEET

I !I SBLK50290F I

.ab Name: CAMBRG______________________ Contract: NOVAK_____ { ________8

.ab Code: CAMBRQ Case No. : NOVAK3 SAS No. : _____ SDC No. : _____


•ample wt/vol: 1000 (g/mL> tJL_ Lab File ID: F2022_____

evel: (low/med) LOW Date Received: ______

Moisture: not dec. ___ dec. _ L_... Date Extracted: 05/02/90


=>C Cleanup: (Y/N) N_ pH: 7. 0 Dilution Factor: 1. 0


108-95-2 ——————— Phenol111-44-4 ——————— bis(2-Chloroethyl)Ether95-57-8 ——————— 2-Chlororhenol _541-73-1 —————— If 3-Dichlorobenzene_1 06-46-7 —————— 1 f 4-Di c h 1 or ob en z en e100-51-6 —————— Benzul Alcohol95-50-1 ——————— If 2-Dichlorobenzene95-48-7 ———————— 2-Methylphenol .39638-32-9 ———— bis(2-Chloroisopropy 1 )Ether _106-44-5 ——————— 4-Methvlohenol ',621-64-7- —————— N-Nitrcso-Di-n-Propylamine __67-72-1 ——————— He xach loroethane

78—59—1— —— •- —— • — Isophorone

105-67-9 —————— 2, 4-Dimethvlphenol_,65-B5-O ———————— Benzoic Acid111-91-1 —————— b is

41C EPA SAMP

i•

1C EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

II SBLK30290F

Lab Name: CAMBRQ _______________ Contract: NOVAK _____ }__•,

_ab Cod*: CAMBRQ Case No. : NOVAK3 SAS No. : ______ SDG No. :

Matrix: (soil/water) WATER Lab Sample ID: 9004330-BLK1

Sample ut/vol: 1000 (g/mL) ML_ Lab File ID: F5022_____

_evel: (lou/med) LOW Date Received: ______


Txtraction: (S*pF/Cont/Sonc) SEPF Date Analyzad: 05/22/90

•PC Cleanup: (Y/N) N_ pH: 7. 0 Dilution Factor: 1. 0____

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UQ/t

99-09-2 ———————— 3-Nitroani 1 ine83-32-9 ——————— Ac enaoh th ene51-28-5— ————— 2f 4-Dini trophenol1 00-02-7 —————— 4-N itrophenol1 32-64-9 ——————— D ibenzofuran121-14-2 ——————— 2* 4-Dini trotoluene84-66-2 ——————— D iethulohthalate70O5-72-3 —————— 4-Ch loropheny 1-ph eny 1 eth »r __

1 00- 1 0-6 ——————— 4-N itroaniline534-32-1 —————— 4, 6-Dinitro-2-Methylph»nol __86-30-6 ——————— N-Nitrosodiphenylamine ( 1 > __101-55-3 —————— 4-Bromoph eny 1-ph eny 1 a th er ___118-74-1 —————— Hexachlorobenzene87-B6-5 ——————— Pentachloroohenol85-01-8 ——————— Phenanthrene120-12-7 —————— AnthraceneS4-74-2 ——————— D i -n-B u t u 1 P h t h a 1 a t e206-44-0 —————— Fluoranthene129-00-0 — - ———— Pyrene33-63-7 ——————— Bu ty Ibanzylohthalate91-94-1 ———————— 3. 3'-Dichlorobenzidine36-33-3 ——————— Benzo (a) Anthracene213-O1-9 —————— Chrysene . .117-91-7 —————— bis(2-Ethylhexyl)Phthalate __117-B4-0 ——————— Di-n-Octyl Phthalate2O3-99-2 —————— Benzo (b)Fluoranthene207-03-9 —————— Benzo(k)FluorantheneSO-32-S —— • ———— Benzo ( a )Pi(r ene. . „,.,.,.„193-39-3 —————— Indanod. 2. 3-cd)Pureno !33-7O-3 ——————— Dibenz(a, h) Anthracene J

I 191-24-2 —————— Benzofq. h. i)Pertflene _ !I i

5010505010101010105030101010501010101010102010101010101010101010

11:u:uIUJU:uIU:u:u:u:uJUIUJUJUIU:uJUJUJUJUIUJUJUIUJUJU:uIU:uJU

! I

\̂ >

Ĵ

(1) - Cannot be separated from Dinhsnui

4 360IF EPA SAMPLE NO.

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _______________TENTATIVELY IDENTIFIED COMPOUNDS I

J SBLK50290F.ab Name: CAMBRQ___________________ Contract: NOVAK_______ I____________!



Sample wt/vol: 1OOO (g/mL) __L_ Lab File ID: F2052________




PC Cleanup: (Y/N) N_ pH: 7. 0 Dilution Factor: 1 0

CONCENTRATION UNITS:umber TICs found: ___ (ug/L or ug/Kg) UQ/L

. . . _ _

~*S NUMBER ! COMPOUND NAME 5 RT ! EST. CONC. Jŝs=s:ccss:cecss { ecBa=sscsrsBBccsccs:CBcess=cKs:es J eesseecc ' csccsscseccee J «

. SUnknoun ! 7. 10 J 20 !J

6R300823

5 251ID EPA SAMPLE NO

PESTICIDE ORGANICS ANALYSIS DATA SHEET!I PBLK J

_ab Name: CAMBRO _______________ Contract: NOVAK _____ ! ____________ {

.ab Code: JCAMBRQ Case No. : NQVAK3 SAS No. : _____ SDO No. :

-latrix: (soil/water) WATER Lab Sample ID: 9004266-BLK1

Sample ut/vol: 1000 (g/mL) Ml,_ Lab File ID: _________

.evel: (low/mad) LOW Date Received: ______

. Moisture: not dec. _ dec. _ Date Extracted: 04/27/90

extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 05/19/9O


CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

!1 4 Q O 41 ' — * -i K -» OLJ/*JIT— 94— o—— —— alpha— one4^4 O QK •» 1- — +. — OUf^3lT— H3— 7——— —— — —— oeta— oMC31 9-36-3 ——————— d e 1 ta-BHC^Q__.OO___Q ___ ___ _ _ l { n ,4 -_M n

7A-44-9 ———————— Hep tac h 1 or309-OO-2 ——————— A 1 d r i n1024-57-3 —————— Hep ta chlor epoxide939-9B-S ——————— Endosulfan I6O-57-1 ——————— Dieldrin

72-20-3 ——————— En d r i n33213-63-9 ————— Endosulfan II72-54-3 ———————— 4, 4 '-ODD1O31-O7-B ————— Endosulfan sulfata30-29-3 ———————— 4, 4 '-DOT72-43-3 ——————— Methoxychl or33494-70-3 ————— Endrin ketone5103-71-9 —————— alPha-Chlordane31O3-74-2 ————— qamma-ChlordaneBOO 1 -33-2 —————— To x a p h e n e

8 12A74-11-2 ————— Aroclor-1016 ,! 11104-2B-2 ————— Aroelor-1221,! 11 141-1 A-S ————— Ar oclor-1232J SS4&9-21-9 ————— Ar oclor-1242 „.,.„.,.,.,! 1 9&72-29-A ————— Ar o c 1 or- 1 243 ,,..,,_,,, .1 11097-&9-1 ————— Aroclor-1234r 11096-82-3 ————— Aroclor-1260S

10. 050 JU0. 030 8 Uo. 050 :u0. 030 JU0. 050 IU0. 050 1 U0. 050 1 U0. 050 IU0. 10IU0. 10JU0. 10JU0. 10IU0. 10IU0. 10IU0. 10IU0. 50 JU0. 10JU0. 50JU0. 50 1 U1. OJU

0. SOIU0. 30JU0. SOIU0. SOIU0. SOIU1. OIUl.OJU

J

FORM I PEST 1/37 R*v

5 25

ID EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET ____________i

J PBLK i.ab Name: CAMBRQ________________ Contract: NOVAK_____ I____________S

.ab Code: CAMBRQ Case No. : NOVAK3 SAS No. : _____ SDC No. :

-latrix: (soil/water) WATER Lab Sample ID: 9004330-BLKl

Sample ut/vol: 1000 (g/mL) __L_ Lab File ID: __________



Jxtraction: (SepF/Cont/Sonc) SEP P.- Date Analyzed: 05/24/90

•PC Cleanup: (Y/N) N_ pH: 6. 0 Dilution Factor: 1. 00

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UQ/L Q

!J 319-84-6 ———319-85-7 —— -319-86-8 ———58-89-9 ————76-44-B ————309-OO-2 ———1O24-57-3 ——

——— alpha-BHC——— beta-BHC——— delta-BHC ,——— Lindane .——— Hep tac h lor ,,„„„,,„„——— Aldrin——— Heotachlor eocxide

959-9B-B ——————— Endosulfan I6O-57-1 ————72-55-9 ————72-20-8 ————

——— Dieldrin _ ,——— 4. 4 '-DDE——— Endrin

33213-65-9 ————— Endosulfan II72-54-8 ————1031-07-8 ——50-29-3 ————

S 72-43-5 ————1 53494-70-5 —S 51O3-71-9 ——8 5103-74-2 ——I 8OO 1-35-2 ——I 12674-11-2—I 11104-28-2—I 11141-16-5—t ci'3&AO~Pi ~Q~~.i %JO*rOT fc* >I 12672-29-6—8 11O97-69-1 —i 1 1U~CJ— Oel— 3I

——— 4, 4 '-ODD— —— Endosulfan sulfate——— 4. 4 '-DOT——— Methoxychlor ,„_,,,.,„—— —Endrin k e tone _,,_,„_,_„——— alpha-Chlordane——— gamma-Chlordane., . , ....——— Toxaphene ^r——— Aroclor-1016 „. .——— Aroclor-1221_, „_——— Aroclor-1232 irT. ... ,.——— Aroclor-1242,_l, , . ,..——— Arocler-124Bi._——— Aroelor~1254,,,« •- ,..,,.,——— Aroclor-1260

!

!0. 050 JU0. 050 JU0. 050 8 U0. 050 JU0. 050 JU0. 050 JU0. 050 JU0. 050 JU0. 10 5 U0. 10IU0. 10JU0. 10JU0. 108U0. 10JU0. 108U0. 50 JU0. 10 IU0. 50JU0. 50 JU1.0IU

0/50IU0. 50JU0. SOIU IO.SOIU I0. 508Ul.OIU Il.OIU I

I 1

ftR300825

5 25

ID EPA SAMPLE Nl jPESTICIDE ORQANICS ANALYSIS DATA SHEET ______________^

i i8 PBLK1 J

.ab Name: CAMBRQ_______________ Contract: NOVAK_____ I____________!


tatrix: (soil/water) WATER Lab Sample ID: 90043Q7-BLK1

Sample wt/vol: 1000 (g/mL) ML,_ Lab File ID: _________



extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 05/19/9O

,?C Cleanup: (Y/N> N_ pH: 6. 0 Dilution Factor: 1. 00


3 1 9-34-6 ——————— a 1 o h a-BHC319-33-7 ——————— b eta-BHC*_« Q_Q_. Q_ __ ~* A 1 v> -« QUf

58-39-9 ———————— Lindane76-44-3 ———————— Heptachlor309-OO-2 ——————— A 1 d r i n1O24-57-3 —————— Heptachlor apox ide959-98-3 ——————— Endoaulfan I60-57- 1 ———————— D i e 1 d r i n72-55-9 ———————— 4, 4 '-DDE72-20-3 ———————— En d r i n33213-63-9 ————— Endosulfan II/_£— 3*r O —————— ———*ft *t ~UUU1O31-O7-3 —————— Endosulfan sulfate30-29-3 ———————— 4, 4 '-DOT72-43-5 ———————— Methoxychlor33494-70-3 ————— Endrin ketone . ,5103-71-9 —————— alpha-Chlordane31O3-74-2 —————— qamma-ChlordaneBOO1-33-2 —————— Toxaphene_ .12A74-11-2 ————— Aroelor-1016 ,,__. _„,..._11104-2B-2 ————— Aroclor-1221 ,11141-16-3 ————— Aroerar-1232_, ,,..,,.334A9-21-9 ————— Ar or 1 or-124212A72-29-A ————— Aroclor-1243 , . . . 111097-&9-1 ————— Aroelor-1234 , 81109A-B2-3 ————— Aroclor-1260 ...,. ..,.„. 8

8

1

0. 050 ! U0. 050 !U0. 050 JU0. 030 JU0. 030 JU0. 050 1 U0. 050 ! U0. 050 1 U0. 10 JU0. 10JU0. 10JU0. 10JU0. 10 JU0. 10JU0. 10JU0. 50 i U0. 10 JU0. 50 S U0. 30 J U1.0,'U

0. 30 8 U0. 50 1 U0. 508U0. SOIU0. SOIUl.OIUl.OIU

8

AR300826

ID EPA SAMPLE NO.PESTICIDE ORCANICS ANALYSIS DATA SHEET

I PBLK3 ILab Name: CAMBRG_______________ Contract: NOVAK_____ I____________I

_ab Code: CAMBRG Case No. : NOVAK3 SAS No. : _____ SDC No. :

latrix: (soil/uater) WATER Lab Sample ID: 900434l-BLKl

Sample ut/vol: 1000 (g/mL) __L_ Lab File ID: __________

.evel: (lou/med) LOW Date Received: _________

'. Moisture: not dec. _ dec. _ Date Extracted: 05/03/90

extraction: (SepF/Cont/Sonc) CDNT Date Analyzed: 05/24/90

?PC Cleanup: (Y/N) N_ pH: 7.0 Dilution Factor: 1. 00

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/K§) UG/L G

O f G_Ct_1 4______ »_« n 1 n It m _BLJ»^ '

319-B5-7 ——————— beta-BHC .^««n M/ « _ _ «l *i t 4- « fill/*31 v— BO— B— — — —— d e i ta— cHC58-89-9 ——————— Lindane76-44-B ———————— Heotachlor _3O9-OO-2 ——————— Aldrin1024-57-3 ————— Hectachlor epoxide959-9B-B ——————— Endosulfan I60-57-1 ——————— Dieldrin72-55-9 ———————— 4, 4 '-DDE72-20-8 ———————— Endrin..,.33213-65-9 ————— Endosulfan II72-54-8 ———————— 4, 4 '-ODD1O31-O7-8 ————— Endosulfan sulfate50-29-3 ——————— 4, 4 '-DOT72-43-5 ——————— Methoxychlor— _,53494-70-5 ————— Endrin ketone51O3-71-9 ————— alpha-Chlordane.51O3-74-2 ——— • —— gamma -Chlordane8001-35-2 —————— Toxaphene ..12674-11-2 ————— Aroclor-101611104-2B-2 ————— Ar oclor-1221.11141-16-3 ————— Aroclor-1232 ... _53469-21-9 ————— Ar oc 1 or-1242...,12672-29-6 ————— Aroclor-1248_11097-69-1 ————— Arecler-1254 _

8 11O96-B2-5 ——— Arocler-126OI

1•jtI1

1, I

t1

S

1,I11

1

88f818II

IIt88I

1 1• 1

0. 050 8 U 80. 050 J U 8O. 050 8 U0. 0508U 80. 050 8 U I0. 050 8 U i0. 050 8 U _H ull

C t,j_._o oonô jjrt'' \0. 10JU0. 10JU0. 108U0. 10 8 U0. 10 8 U0. 10JU

C.it -0. 0099 ,'JX u-fc0. 50 JU0. 108U0. 50 JU0. 508U1. OiU

0. 50IU0. SOIU0. SOIU0. 50 IU0. SOIUl.OIUl.OIU

8

RR300827

5 Z6r ID EPA SAMPLE NP( PESTICIDE ORGANICS ANALYSIS DATA SHEET

J8 PBLK3

lab Name: CAMBRQ ________________ Contract: NOVAK _____ 8

_ab Code: CAMBRQ Case No. : NOVAK3 SAS No. : _____ SDQ No. :

-latrix: (soil/water) WATER Lab Sample ID: 9O04341-BLK2

Sample wt/vol: 1OOO (g/mL) ML,_ Lab File ID: __________

_evel: (lou/med) LOW Date Received: ______

'. Moisture: not dec. _ dec. _ Date Extracted: 05/03/90

Extraction: (SepF/Cont/Sonc> CONT Date Analyzed: 03/24/90

?PC Cleanup: (Y/N) N_ pH: 7. 0 Dilution Factor: 1. 00

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UQ/L Q

319-B5-7 ——————— beta-BHC319-86-3 ——————— delta-BHCSB-39-9 ——————— Lindane7A-44-3 ———————— Hep tach 1 or3O9-OO-2 —————— A 1 d r i n1O24-57-3 —————— Heptachlor ep oxide939-9B-B ——————— Endosulfan I6O-57- 1 ————— • — D i e 1 d r i n*7«% K B A /i /i * nncr72-20-3 ——————— En d r i n33213-63-9 ————— Endosulfan II72-34-B ———————— 4, 4 '-ODD1O31-O7-3 —————— Endosulfan sulfate3O-29-3 ———————— 4. 4 '-DOT72-43-3 ——————— M ethoxychlor33494-7O-3 ————— Endrin ketone3103-71-9 —————— alpha-Chlordane31O3-74-2 ————— qamma-ChlordaneBOO 1 -3 5-2 ————— T oxaphene12&74-11-2 ————— Aroclor-lO16..11104-29-2 ————— Ar oclor-1221 _.1 1 141-16-3 ————— Ar oc 1 or -1232 ...33449-21-9 ————— Aroclor-1242 !12A72-29-& ————— Aroclor-1243 ..,__,.„ !11097-A9-1 ————— Aroelor-1234 ., !1109A-92-3 ————— Aroe lor- 1260 !

I

J 0. 0308 U1 0. OSOIU

0. 030 8 U0. OSOIU0. 050 8 U0. 030 JU0. 050 JU0. 030 J U0. 10 8 U0. 10 8 U0. 108U0. 108U0. 10 8 U0. 108U S&

£./0-3. 02QJJX-K.0. 508U0. 10 8 U0. 50 8 U0. 508Ul.OIU

0. SOIU0. SOJUo. soiu0. SOIU0. SOIUl.OIUl.OIU

I

'\J

flR300828PORM T PP«5T

U.S. SPA - CLP-, r : f.3 ' ' '

BLANKS

Lab Na"me: NF.T-CAMBRIDGE DIVISION Contract:

Lab Code: CAMBRG Case- No.: NOVAK SAS Mo.: SDG No.: 211

Preparation Blank Matrix (soil/water): WATER

Preparation Blank Concentration Units fuci/L or mg/kcj: UOr 'L

11111»11

! Ansivts!I Aluminum8 Ant imonv8 Arsenic! B^r i U.TIJ Beryl 3 iumi Cadmium'CdlciuiTi8 ChromiumSCobaJ t:! Copper! IronI Lead* Maanes i um5 Manganese•MercuryI NickelI Potassium! Selenium8 Si 1 verI Sod iumSThellium8 VanadiumiZinc'Cyanide8

;Initial !Cs I i b .Blank !•-ig.'L) CI

11

60 . 0 i L! I_o.o:u;•v . o : u :SS.OJ'J!i . o : u :s.Ofu:

33 . o : u :i o . o ; u ;20 . o : u :5.08U!

20 . o : u :2.0M.J8

70.0IUJ3.0JU!O.28U815.08U8

sso.oiu:R.08U88.08U8

140.0 JU 85.08U811.08U!7.08U8

10 -O !Oul• i» i

Cone znu insPlank

1 C

74 . 7 ! B !60.0JUI•4.08U832.0JU!i . •:< : u s5.0 8 U!

7S . a : p j10.0 lu:20 . 0 8 U !5.O8U!

20.586!2.01 U 5

149.1 5B!3 . 0 1 U ,'0 . 2 1 U 8iS.oiB!

830 . 0 i U t£ . 0 8 U 8

10. 4S I727.18B85.08U8le.OIBJ-7.58B8lO-O-'u.!

8 8

Cali _:• ratio n(ua/L>2 C

S?. . 4* ! P i60.0! U!4.0 JU!22 . 0 ! U r1.08LJ85 . o : u :

71.98BJ10.05U;20.0 :u:5-8 IP;

20.O8U82.0,'Ui

1 1 4 . 2 1 B 83.0: U 8

. 0 . 2 ! U 815.0JU8

830.0! U!2.08U88.08U8

655.98B85.08U812.18B8-7.08B!IO-O 8u!

8 t

, »; \

r |> 1

: 1

1 t1 1

_; .— - i i-V '^11

f 1

115.2:3! i60 . o : u : :4 . o : u : ;22.0JL1: :1 . 0 8 U 8 ts . o : u : :

7i.= IB; :i o . o : u ; :20.OIU! ts.Oiu: :20.0 !U! ,'2 . o i u i :

98 . 7 : B ! i3 . o : u .- :o . 2 : u : :i5.o:u: :

eao". o : u : :2.OIU8 !8.0 :u: :

605. 98B! !5 . o : u : :12.3IBI J7.O8U8 8io-o JM. 8 8

1 I I

» 1i •1 1• t

Freer- : 1ration i ,'Blar.fc C : :i

I »

6

U.S. EPA - CLP

3BLANKS

Lab Name: NET-CAMBRIDGE DIVISION Contract:

Lab Code: CAMBRG Case No.: NOVAK SAS No.: SPG No.: 21?

Preparation Blank Matrix (eoi1/water):

Preparation Blank Concentration Units

U.S. EPA - CLP

3BLANKS

32

Lab NaTne: NET-CAMBRIDGE DIVISION Contract:

Lab Code: CAMBRG C»sa No.: NOVAK SAS No.: SDG No.: 2113

Preparation Blank Matrix (soi1/water>:

Preparation Blank Concentration Units Cug/L or mg/kg):

f11

tI*I

1 Analvteti

! Aluminum• A 4> " -—i F̂ m? i /«io ¥*iv! Arseni c!3ar iu.Ti'Bervl 1 j ufr.i Cadmium8Ca] ciuf»! Chromium{Cobalt{Copper! Iron{Lead{Magnesium{Manganese{Mercurv{Nickeli Potass ium

{Silver'Sodium•Thalliumt Vanad i urn8 Zinc(Cyanide8

InitialCalib.Bl*nk(ug/L) C

2.0 U

Continuing CalibrationBlank (ug/L)

1 C 2 " C 3 C

2.0

0.2

5.0888 lo-o8

U

U

U

0.

0.2

5.0

8

!

U

U

0.2

5.0

u

u

8: 8 t

11f1

?t-ss5- :ration !Blank C IM

lta l

IN

-̂*n:N• N:!N.NiININ!IN(MIFINIIM!C'• NIINF

INF8NI8FINf:NF: {ttf

i : 5 "

FORM III - IN AR300831 7/37

U.S. EPA - CLP

3BLANKS

L*b Name: NET-CAMBRIDGE DIVISION Contract:

Lab Code: CAMBRG Case No.: NOVAK SAS No.: SFifi No.: 211

Preparation Blank Matrix (soil/Hater):

Preparation BlanK Concentration Units Cug/L or mg/kg):

1

i

1

f8 AnsiyteI•

{Aluminum•Antimony! Arseni c• BariumJBervl ) j um8CaaiRiu.il!Cal c ium8 Chromium

'Copper8 Iron8 LeadSM&gnes? um• Manganese•Mercury!Nick*l{Potassium8 Selenium5 Silver•SodiumI Thallium{Vanadium(Zinc(Cyanide8

InitialCal is.Blant;(ug/L) C

i1 i1

Continuing CalibrationBlank (ug/L)

1 C 2 C 3 C

<1

0.2, ''

,

U'

88

5.08U888

0.2.

1

_____ S . 8 ________ 8 _ 8 __

U 0.2 U

Prepa-rationBlank C

1 8t !

! i !t 8 ! 5

t1

111

It11

{f8111ntrif'. r-:r:r8N{!•>8N• r

sci hi 1*1ININ:N

i 8N8 8F8 8N8 INIi 8N

_8 8_.

FORM III - IN fiR30083a_

U.S. EPA - CLP 3 '

3BLANK:

Lab Mam»: NET-CAMBRIDGE DIVISION Contract:

Lab Code: CAMBRG Cass No.: NOVAK SAS No.: SDG Mo.: Sn3C

Preparation Blank Matrix (soil/water?:

Preparation Blank Concentration Units -lug/L or me/kg):

11

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AR300839

3-- 156

1A EPA SAMPLE NO.VOLATILE ORCANICS ANALYSIS DATA SHEET

i NSL-MW1C 01Bab Name: CAhBRG_______________ Contract: NOVAK_____ 8___________

ab Code: CAMBRC Gate No. : NOVAK3 SAS No. : ______ SDC No. :

jtrix: (soil/water) WATER Lab Sample ID: 9004341-01A

ample ut/vol: 5. 0 (g/mL) JJL_ Lab File ID: K2533_____

•vel: (lou/med) LOU Date Received: 04/28/90


lumn: (pack/cap) PACK Dilution Factor: 1.0____

CONCENTRATION UNITS:CAS NO. COMPOUND , (ug/L or ug/Kg) UC/L

74-87-3 ——————— Chloromethane^.74-B3-9 ———————— Bromomethane75-01-4 ———————— Vinyl Chloride. .„75-OO-3 ———————— Chloreethane^ ____75-O9-2 ———————— Methylene Chloride67-64-1 ———————— Acetone75-15-0 ———————— Carbon Disulfide75-35-4 ———————— 1. 1-Dichloroethene .75-34-3 ———————— 1. 1-Dich loroethane540-59-0- ————— 1,2-Dichlcroethene (total) __67-66-3 ———————— Chloroform107-06-2 ——————— 1. 2-Dichloroethane _ .7B— 93— 3—— — —— —— 2— Butanone71-55-6 ——————— 1. 1. 1-Trich loroethane ,56-23-5 ———————— Car b on Te trac h 1 or id elOfi-05-4 ——————— Vinyl Acetate75-27-4 ——————— Bromodi Chloromethane7B-87-5 ———————— 1, 2-Dichlerepropane _ _10061-01-5 ———— cis-li 3-Dichloropropene79-O1-6 ——————— Trichloroethene,.124-4B-1 — - ———— Dibromeehleromethane ,_. . ,_.79-00-5 ———————— i. 1. 2-Tri eh loroethane .71-43-2 ———————— Benrane .„ , , , , ,„„1O061— O2-6— ——— -tr«n*-l« 3-DiehIoropropene_ __75-25-2- ——— •• —— -Bromof orm10S-10-1 ——————— 4-Methyl-2-Pentanene . _591-78-6 —————— 2-Hexanone .•..._.127-1B-4 ——— • ——— Tetrach loroethene79-34-5 ——————— 1, 1,2, 2-Tetrachloroethane ___1OS-BB-3 —— • ——— • — Toluene1OB-9O-7' —————— Ch 1 or eb en z ene1OO-41-4 —— • ———— Ethyl benzene100-42-5 ———————— Styrene.. .. .1330-20-7 ————— Xylene < total )^

101010105105555S510

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3~157IE EPA SAMPLE NO.

VOLATILE OROANICS ANALYSIS DATA SHEET ____________TENTATIVELY IDENTIFIED COMPOUNDS I

I NSL-MW1C_01S• D Name: CAMBRQ_________________ Contract: NOVAK_____ !____________

Code: CAMBRQ Case No. : NOVAK3 SAS No. : ______ SDG No. :

trix: (soil/water) WATER Lab Sample ID: 900434l-QiA

,nple ut/vol: 5 0 (g/mL) ML__ Lab File ID: K5533_____

vel: (lou/med) LOW Date Received: 04/2S/9Q


lyrmn (pack/cap) PACK Dilution Factor: 1 Q_______

CONCENTRATION UNITS:TICs found: _0 (ug/L or ug/Kg) UQ/L

11

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AR3008M

3 105

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET __

Name: CAMBRQ _______________ _ Contract: NOVAKNSL-MW-09B-O/ !

-ab Code: CAMBRQ Case No. : NOVAK3 SAS No. : _____ SDG No. :

latrix: (soil/water) WATER Lab Sample ID: 90Q4330-04A

Sample wt/vol: 5. 0 (g/mL) QL_ Lab File ID: H3552_____

.evel: (low/med) LOW Date Received: 04/57/90


rlumn: (pack/cap) PACK Dilution Factor 1. 0______


/ "T O / J

75-01-4 ——75-00-3 ——/ w \J7 A£

67-64-1 ——75-15-0 ——75-35-4 ——75-34-3 ——540-59-0 —67-66-3 ——107-06-2 —

71-55-6 ——56-23-5 ——108-05-4—75-27-4 ——

10061-01-579-01-6 ——124-48-1 —79-00-5 ——

10061-02-675-25-2 ——108-10-1 —591-78-6—

108-88-3 —108-90-7 —100-41-4 —

8 100-42-5 —8 1330-20-7-1

————— Chloromethane————— Bromomethane————— Vinyl Chloride————— C hloroethane ,.— —— — Methulene Chloride————— A c e t o n e

————— 1* 1-Dich loroethene————— Ii 1-DichI oroethane————— 1, 2-Dichloroethene (total ) __————— Chloroform———— Ii 2-Dichloroethane————— 2-Butanone———— 1» 1* 1-Trichloroethane————— Carbon Tetrachloride————— Vinyl Acetate————— Bromodi Chloromethane————— 1. 2-DichloroprcDane————— cis-1. 3-DichlcrcDroDene_————— Trich loroethene————— Dibromoc hi or erne thane— ———— If 1, 2-Trichloroethane ,r— • — • — Benzene———— trant-J-» 3-Dichloropropene—— . — -Bromoform n———— 4-Methi/l-2-Pentanone————— 2-He ranone———— Tetrachloroethene———— 1» 1* 2» 2-Tetrachloroethane ___—— « —— Toluene————— Chlorobenzene————— Ethulbenzene————— Sturene————— Xulene (total ) _____„„„

1010101071055555574551055555555510105555e

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3 106

IE EPA SAMPLE/-.,. VOLATILE ORQANICS ANALYSIS DATA SHEET __________

TENTATIVELY IDENTIFIED COMPOUNDS

_ab Name: CAMBRQ ________________ Contract: NOVAKNSL-MW-09Q -

.ab Code: CAMBRQ Case No. : NOVAK3 SAS No. : ______ SDG No. :

Matrix: (soil/water) WATER Lab Sample ID: 90Q4330-04A

Sample wt/vol: 5. 0 (g/mL) ML,_ Lab File ID: H3552________

-evel: (lou/med) LOW Date Received: 04/57/9O


olumr, (pack/cap) PACK Dilution Factor: 1. 0____

CONCENTRATION UNITS:umber TICs found: __1. (ug/L or ug/Kg) UQ/L

CAS NUMBER==

COMPOUND

KNOWN **-**. n-̂ iT-fi Lra n

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11

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IB EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

8 NSL-MW1C-01B 8_ab Name: CAMBRC_________________ Contract: NOVAK_____ t __________j

-ab Code: CAMBRC Ca«e No. : NOVAK3 SAS No. : __________ SDG No. : -

•latrix: (soil/water) WATER Lab Sample ID: 9004341-O1H

•ample wt/vol: 1000 (g/mL> (__._ Lab File ID: J6S63_____

4 JS5\_

1C EPA SAMPLE NO.l SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ______________

8 !8 NSL-MW1C-01B 8

Lab Name: CAMBRQ ________________ Contract: NOVAK _____ 8 _____________ !

_ab Code: CAM8RQ Case No. : NQVAK3 SAS No. : ______ SDG No. : ____

latrix: (soil/water) WATER Lab Sample ID: 9004341-01H

Sample uit/vol: 1000 (g/mL) ML Lab File ID: J6563_______

_evel: (lou/med) LOW Date Received: 04/2S/90

: Moisture: not dec. ___ dec. ___ Date Extracted: 05/03/90

Txtraction: (SepF/Cont/Sonc) CDNT Date Analyzed: 05/55/90

,PC Cleanup: (Y/N) N_ pH: 7. 0 Dilution Factor: 1 0_____


99-09-2 ——————— 3-NitroanilineS3-32-9 ——————— Acenaphthene51-2S-5 ——————— 3, 4-Dini tr oo h eno 11 00-02-7 ——————— 4-N itroohenol1 32-64-9 ——————— Di benzofuran121-14-2 ——————— 2, 4-Dini tro toluene34-66-2 ——————— D iethylphthalate7005-72-3 —————— 4-Ch 1 oroph eny 1-ph eny 1 eth er __86-73-7 ——————— Fl u or ene100-10-6 ——————— 4-Ni troani 1 ine534-52-1 ——————— 4, 6-Dinitro-2-Methyl phenol __86-30-6 ——————— N-Nitrosodiphenylamine ( 1 ) __101-55-3 —————— 4-Bromop henyl-phenyl ether ___1 18-74-1 —————— Hexach lorobenzene87-86-5 ——————— Pentac hi oroph eno 185-01-8 ——————— Phenanthrene1 20- 1 2-7 —————— An thracene84-74-2 ——————— Di-n-Butylphthalate206-44-0 —————— Fl uoranth ene129-00-0 —————— Pyrene85-69-7 ——————— Butyl benzyl phthalate91-94-1 ——————— 3, 3 '-Di.ch 1 orob enz i dine36-33-3 ——————— Benzo ( a >An thracene218-O1-9 —————— Chrusene117-S1-7 —————— bis(2-Ethylhexyl)Phthalate .117-34-0 —————— Di-n-Octul Phthalate205-99-2 —————— Ben zo(. )F1 uoranth ene207-08-9 —————— Benzo (k)Fluoranthene50-32-8 ——————— Banzo(a)Pyr»ne193-39-5 —————— Indenod, 2< 3-cd)Pyrene53-70-3 ——————— Dibenz(a, h) Anthracene191-24-2 —————— Benza(q* h, i)P»rylens

501050501010101010505010101050101010l Ui U:ui \J:ui U;ui U:u:u:u• u:u8UIUIU!U f-

8 ___(1) - Cannot be separated from Diphenylaminff

4 16IF EPA SAMPLE NO.

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ___________TENTATIVELY IDENTIFIED COMPOUNDS

! NSL-MW1C-O1B 8Lab Name: CAMBRG____.___________ Contract: NOVAK_____ \ _________8

.ab Code: CAMBRG Case No. : NOVAK3 SAS No. : _____ SDG No. :

latrix: (soil/uater) WATER Lab Sample ID: 9004341-O1H

Sample ut/vol: 1OOO (g/mL) QL_ Lab File ID: J6863_________

-evel: (lou/med) LOW Date Received: 04/2S/9O


:xtraction: (SepF/Cont/Sonc) CONT Date Analyzed: 05/25/90

PC Cleanup: (Y/N) N_ pH: 7. 0 Dilution Factor: 1. 0______

CONCENTRATION UNITS:umber TICs found: ___, (ug/L or ug/Kg) UG/L

"AS NUMBER* sscssssssssss/v__ , .

: 88 COMPOUND NAME 8

E ! esssssssessssecesccssssscssc j cs•Dimethylbenzene isomer 88 8

RTSECCSS

5. 90

8EST. CONC. 8 Q

cessssss=cesc { esses10 i J

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6R3008U6

rurm _ sv-s: i/o/ -ev.

4 113

IB . EPA SAMPLESEMI VOLATILE ORGAN I CS ANALYSIS DATA SHEET

I . NSL-MW-09-1B 8_ab Name: CAMBRQ _______________ Contract: NOVAK _____ I ____________ 8

-ab Cod»: CAMBRG Case No. : NOVAK3 SAS No. : ______ SD9 No. :

latrix: (soil/water) WATER Lab Sample ID: 900433Q-04G

Sample uit/vol: 1000 (g/mL) Ml,_ Lab File ID: F5026______

.evel: (low/med) LOW Date Received: 04/27/90


Ixtraction: (SepF/Cont/Sonc) 5EPF Date Analyzed: 05/25/90

:-PC Cleanup: (Y/N) N_ pH: 7. 0 Dilution Factor: 1. 0______


\108-95-2———————P h en o 1 ___________________111-44-4——————bis(2-Chloroethyl)Ether____95-57-9———————2-Chlorophenol____________541-73-1———————\, 3-Dich lorobenzene_______106-46-7——————— 11 4—Dichlorobenzene_______100-51-6———————Benzyl Alcohol____________95-50-1 ——————— 1 • 2-D ichlorobenz ene_______95-48-7———————2-M»thylphenol____________39639-32-9————bis(2-Chloroisopropy1)Ether_106-44-5——————4-Methyl phenol___________621-64-7——————N-Nitroso-Di-n-Propylamine_67-72-1———————He xac hi oroethane____________98-95-3———————Nitrobenzene_____________78-59-1 ——————— Isophorone_______________98-75-5———————2-Ni tr op h eno 1_____________105-67-9———————2. 4-Dimethylphenol________65-85-0———————Benzoic Acid_____________111-91-1——————bis(2-Chloro_thoxy)M»thane_120-93-2——————2i 4-Dichlorophenol________12O-92-1——————1* 2, 4-Trichlorobenzene_____91 -20-3———————Na phthalen e_____________106-47-8——————4-Ch 1 or oani 1 ine__________87-69-3———————Hexachlorobutadiene_______59.50-7———————4-Ch 1 or o-3-M» t h y 1 p h eno 1 ____91-37-6———————2-Metht) Inaph thai en*_______77-47-4———————He x a c h 1 or oc y c 1 op en tad i en e__88—06-2———————2. 4. 6-Trichlorophenol_____95-95-4———————2* 4» 5-Trichlorophenol_____91-59-7——————»2-Chloronaphthalene_______.

10 IU10 8U10 !U10 :u10 :u10 :u10 :u10 :u10 :u10 !U10 :u10 :u10 :u10 :u10 :u10 8Uso :u10 :u10 ;u10 :u10 :u10 :u10 :u10 :u10 ;u10 :u10 !U30 8U10 :u

88-74-4———————2-Ni troani line____________J 30 8 U 8131-11-3——————Dimethyl Phthalate________8 10 !U I2O8-96-9——————Acenaphthyltne____________J 10 JU. n ̂ A I. 16O6-20-2——————2, 6-Oinitrotoluen*________.8 lo{\Rl»0 UU ? ̂ '

4 114

1C EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ________

I NSL-MW-09-1B 8.ab Name: CAMBRQ________________________ Contract: NOVAK_____ 8 _________f

.ab Code: CAMBRQ Case No. : NOVAK3 SAS No. : _____ SDG No. :

latrix: (soil/uater) WATER Lab Sample ID: 9004330-04Q

sample ut/vol: 1000 (g/mL) QL_ Lab File ID: F2026________

.evel: (lou/med) LOW Date Received: 04/27/90

. Moisture: not dec. ___ dec. ___ Date Extracted: Q5/Q2/90

:xtraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 05/55/90

PC Cleanup: (Y/N) £J_ pH: 7. O Dilution Factor: 1. 0_______

CONCENTRATION UNITS:CAS NO. COMPOUND ; (ug/L or ug/Kg) UQ/L

B3-32-9 ——————— Acenaphthene51-2B-5 ——————— 2. 4-Dini troohenol1OO-O2-7 ——————— 4-Ni trophenol132-64-9 —————— Dibenzofuran121-14-2 —————— 2, 4-Dini trotolueneS4-66-2 ——————— D iethylDhthalate7O05-72-3 ————— 4-Ch 1 or op h eny 1-p h eny 1 e t h er __S6-73-7 ——————— Fluor ene__ _1OO-1O-6 ——————— 4-Ni troani line534-52-1 —————— 4/6-Dinitro-2-Methylphenol __86-30-6 ——————— N-Nitrosodiphenylamine (1) __1O1-55-3 —————— 4-Bromophenyl-phenyl ether ___11B-74-1 —————— HexachlorobenzeneB7-86-5 ——————— PentachlorochenolBS-Ol-B ——————— Phenanthrene1 2O- 1 2-7 ——————— An thracene84-74-2 ——————— Di-n-Butulohthalate2O6-44-0 —————— Fluoranthene129-OO-O —————— PyreneB5-6B-7 ——————— Butylbenzulohthalate91-94-1 ——————— 3, 3'-Dichlorobenzidine_.36-53-3- ——————— Benzo (a) Anthracene218-O1-9 ——————— Chrysene _ _117-81-7 —————— bis(2-Ethylhejctfl)Phthalate __117-B4-O —————— Di-n-Octyl Phthalate2O5-99-2 ——— • —— Benzo (b )F1 uoranth ene2O7-08-9 —————— Benzo (k)Fluoranthene5O-32-8 — • — • —— •Benzo(a)Purene_193-39-5 — - ———— Indenod, 2< 3-cd)Pyrene53-7O-3 ——— - —— -Dibenz (a* h ) Anthracene ________191-24-2— — • ——— Benzo (gi hi i)Perylene_

4 115IF EPA SAMPLE Nl J

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _______ __~TENTATIVELY IDENTIFIED COMPOUNDS 8

8 NSL-MW-09-1BLab Name: CAMBRQ________________ Contract: NOVAK_____ 8________

_ab Code: CAMBRG Case No. : NQVAK3 SAS No. : ______ SDG No. :

latrix: (soil/water) WATER Lab Sample ID: 9004330-04Q

Sample ut/vol: 100O (g/mL) ML_ Lab File ID: F2056________


'. Moisture: not dec. ___ dec. ___ Date Extracted: 05/02/90

•!xtraction: (SepF/Cont/Sonc) 5EPF Date Analyzed: 05/22/90

,PC Cleanup: (Y/N) N_ pH: 7. 0 Dilution Factor: 1. 0

CONCENTRATION UNITS:lumber TICs found: _0 (ug/L or ug/Kg) UQ/L

3

"AS NUMBER5========:=!=!==

118 COMPOUND: ' ===============3ii

NAME============

RT33333333

EST. CONC.3333333=33333

11

8 Q! =====11

SR300849

5 05!

ID EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET __ __

! NSL-MW1C-01BLab Name: CAMBRG ________________ Contract: NOVAK !

Lab Code: CAMBRC Case No. : NOVAK3 SAS No. : ______ SDC No. :

latrix: (scil/uater) WATER Lab Sample ID: 9P04341-01

Sample wt/vol: 1000 (g/mL) JJL_ Lab File ID: ________

.evel: (low/med) LOW Date Received: 04/2B/9O

: Moisture: not dec. _ dec. _ Date Extracted: 05/03/90

Ixtraction: (SepF/Cont/Sonc) CONT Date Analyzed: 05/54/90

•PC Cleanup: (Y/N) fcj_ pH: 7. 0 Dilution Factor: 1. 00


•i8 319-B4-6 ————

J 319-86-8 ————• PQ_DO_C__._____l 5tJ- 'OT— V—— — • •———

l «3W~ UU _»——————»—

J 1024-57-3 ————1 Q̂ Q C1C *•»i V5Y— Y8— H—— ——— "8 60-57-1 —————8 72-55-9 —————' *~f)_9A_D_______t /^— cJO— _J———— —~ -

8 33213-65-9 ———• 79—S-1.-C.-—— •— '_——i /̂ — 3*>— 13— ̂̂ ^̂ ^̂J 1O3 1-07-8 ————

! 72-43-5 ——————I 53494-70-5 ———S 5103-71-9 ————8 5103-74-2 ————1 8001-35-2 ————J 12674-11-2 ———I 111O4-2B-2 ———

—— aloha-BHC•— ' — U £ vci*~Orĵ

—— delta-BHC• — Lindane• — Hectachlor- — Aldrin• — Heptachlor epoxide—Endosulfan I _,,,,• — Dieldrin—— 4, 4 '-DDE— —Endrin—— Endosulfan !!___,, , „—— 4. 4 '-ODD• — Endosulfan sulfate— 4. 4 '-DOT—— Me thoxych lor „_.,__,_— Endrin ketone^^,— aloha-Chlordane.— gamma -Chlordane.— Toxaphene _ r— Aroclor-1016—— ArocleF-1221

I 1 1 141-16-5 ————— Ar cc 1 or-1232 , ,„1 33469-21-9 ————— Aroclor-1242• 1 1f *T~I_1O_< ____• ZitO/ei— «V— O——— "1 11097-69-1 ———i i 1WTO — tS«£ SI

— Aroclor-1248.iiir^— Aroc lor- 1254 ,„„„_— Aroclor-1260

811It

8888i••iiii•iii8811

8i__^ i818811I888ii

8 I0. OSOIU 80. 050 8U0. 050 8 U0. 050 i U0. 050 8 U0. 050 8 U0. 050 8 U0. 050 8 U0. 10,'U0. 10 8 U0. 108U0. 10,'U0. 10 8 U0. 108U i0. 108U 80. SOIU 10. 10 8 U 10. 50 8 U 80. 50 JU J1.0,'U 1

0. SOIU 10. 50JU 10. SOIU i0. 50!U0. SOIU il.OJU 11.0,'U 1

: iRR300850

5 04$

ID EPA SAMPLE NPESTICIDE ORGANICS ANALYSIS DATA SHEET

8 NSL-MW09-01B_ab Name: CAMBRG ________________ Contract: NQVAK _____ I


latrix: (soil/uater) WATER Lab Sample ID: 9004330-04

Sample ut/vol: 1000 (g/mL) ML,_ Lab File ID: _________


Moisture: not dec. _ dec. _ Date Extracted: 05/01/90

Ixtraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 05/24/90

PC Cleanup: (Y/N) N__ pH: 6. 0 Dilution Factor: 1. 00

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UQ/l

u.s. E?A - CLP 0000£

ANALYSIS Dr.TA SHEET

L*b N&me: NET-CAMS? IHC-E DIVI5I-N Contract.:

Lsb Code: CAMBRG Case No.: NCVAk SAS No.: SDG No.: 21 inCw

Matrix < soi l.';-«&t.r > : MATSR :_*.B Sample ID: •'—3-1—M.=

Lev«l < low-me_> » !_'jt--r Drt— r-:sr&'. .'i5_,:: •!->• r'r*'-1 •

C :--'-r •?•>- T -s- ;_••-> Jr.i*,« 'us-''L c-r m._/*-'e ci'."-.- t-sv.r?1': UG-L

_ ".' ".'-•• ..-. ;.;_-. _=•

l̂:.̂ ẑ-?i 40-59- r7i4.;— -i -7T̂ .̂.;.-̂ .J.--7 _._,i"i- — i'.—a74̂..;. — .T-S7440_45-_v"-w.:— so— =7-Orc-?r-->•'439-3=-i7̂ 3?-=5--»?-»3«-=c-57439-=7-s7̂ 4̂ _,:>g_.;,744O-09— 7T78_-A9-27440- 22-47,-+4r._£3_t,744O— =3— :•7440-cg-S74i.0-i.-e

i 1

1 ** •". ~ 1 - * (" "• *

' A 1 ' L -i • ' « i

1 B 5

20U.S. EPA - CLP

i EPA SAMPI.EN~

16U.S. EPA - CLP

1 EPA SAMPLE NOINORGANIC ANALYSIS DATA SHEET

8 ' MW0901BLab Name: NET-CAMBRIDGE DIVISION Contract:

Lab Ccrde: CAMBRG Gate No.: NOVAK SAS No.: SDG No.: 2112i

Matrix (soil/water): WATER Lsb Sample ID: O4330-O4

Level : LOU Dsire Received: 04/27/90

*/. So lids: 0.0

Concentration Units (ug/L or mg/Kg arv weisht): UG/L

11

!CAS Mo.*1

! 74P9-90-5• 744O-36-0• 74 7_3{ 7-̂ 0-49-4{ 744O-50-S! 7439-39-687439-02-18 7439-95-48 7429-96-5! 7439-97-6! 7440-02-08 744O-09-78 7782-49-2• 7440-22-4i 744O-23-5• 7440-29-0! 7440-62-28 7440-66-61 __8 ~ __

t

', Analvte» • ' - , ' " - • •» - - '

.' Aluminum8 An time ny[ArsenicI Bar ium; Beryl 1 ium'Cadmium8 Calcium'Chromium! Cobalt: Copper8 IroniLesc! Magnesium8 Manganese•Mercury8 NickelIPottEEium: SeleniumSSilver•Sodium{Thallium! Vanadium8 Zinc(Cyanide 18 8

Concentrst i on 1C! Ql li i

1 1 9 . OO 1 B !60 . 00 : U :4 . 00 ! M !

32 . 00 ! tj 1I.OOJLJ:S.OOIUi

173. 008 B!10.00IUJ20 . OO 1 U l5 . OO ! u !40 . so : B :3 . 20 : B 1 *87 . 70 1 B 83 . 00 8 U 1O.SOiU!

15.0O8U!S30.O08U!2 . OO ! U !8 . 00 8 U 8

71 SO. 00 8 !5.OO8U!

1 1 . 00 1 U 87.608P!10.008U!

; :

• .l

:Mi•

IPIP:F:P:P:P;P!PIP!P:P:FIFIP:cv!P,'P!F!P8P8F:P!P!C*»

Color Beforet Clarity Before: Texture:

Color After: Clarity After: Artifacts

Comments:

the* cample was clear and colorless; no artifacts

FORM I- IN flR30085l*

Trip Blanks

AR300855

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET __________

I J8 TBLK0423 . . 8

-ab Name: CAMBRG_________________ Contract: NOVAK_____ ! /M«crrfe~ l-

.ab Code: CAMBRQ Case No.: NOVAK3 SAS No.: _____ SDG No.: _

latrix: (soil/water) WATER Lab Sample ID: 9004266-03C

Sample ut/vol: 5. 0 (g/mL) __L_ Lab File ID: H3477_____



;olumn: (pack/cap) PACK Dilution Factor: 1.0____


74-87-3———————Chloromethane_____________8 10 !U74-83-9———————Bromomethane_____________I 10 !U75-01-4———————Vinyl Chloride__________________8 10 8U75-00-3———————Ch loroethane_____________! 10 8U75-09-2———————Methylene Chloride___________8 5 !U67-64-1————————Acetone____________________! 10 8U75-15-0———————Carbon Diculfide__________! 5 !U75-35-4———————1, 1-Dichloroethene________8 5 !U75-34-3———————i, 1-Dichloroethane_________8 5 !U540-59-0——————1,2-Dichloroethene (total)__8 5 !U67-66-3——•—————Ch 1 orof orm _____1O7-06-2———————1.2-Dich loroethane__78-93-3———————2-Butanone _______71-55-6———————1* 1. 1-Trichloroethane.56-23-5————•———Car b on Te tr a chloride

5 !Us :u10 :u5 :u5 :u10 :us :us :u5 :u5 !U5 :u5 :u5 :us iu5 IU10 :u10 :u5 !U5 :u5 8U5 :u5 i5 I

I 1330-20-7—————Xylene (total)____________8 5 SU8__________________________________\__________

108-05-4——————Vinyl Acetate__________75-27-4———————Br omodichl or erne thane____78-87-5-——————Ii 2-Dichloropropane_____10061-01-5————cis-l»3-Dichloropropene_79-0 i -6———————Tr i c h 1 or o ethene ______124-48-1—•—•——Dibromochloromethane____79-OO-5—-————1. 1> 2-Trichlcroethane___71 -43-2———————B e n z e n e ___________________10061-02-6————trans-1, 3-Dichloropropene.75-25-2——————Bromoform____________1O8-1O-1——————4-Meth«l-2-Pentanone____591-78-6——————2-Hexanone____________

8 127-18-4——————Tetrachloroethene______I 79-34-5——————-1. 1. 2. 2-Tetrach loroethane.j 108-88-3——————Toluene_______________{ 108-90-7—————-Chlorobenzene _______I 100-41-4———————EthulbenieneI 1OO-42-5——————Styrcne

3 245

IE EPA SAMPLEVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 8 !

8 TBLK0423. • 8.ab Name: CAMBRQ ________________ Contract: NQVAK _____ \f*wT&- /-V/?5/ro 8

_ab Code: CAMBRQ Case No. : NOVAK3 SAS No. : ______ SDG No. : _____

latrix: (soil/water) WATER Lab Sample ID: 90Q4266-Q3Q

Sample ut/vol: 5. 0 (g/mL) ML _ Lab File ID: H3477 ________

.evel: (lou/med) LOU Date Received: 04/24/90


olumn (pack/cap) PACK Dilution Factor: 1. 0 ____

CONCENTRATION UNITS:umber TICs found: 0 (ug/L or ug/Kg) UQ/L

CAS NUMBER 8 COMPOUND NAME 8 RT 8 EST. CONC. 8•33333333=3332 | 3333333333333333333333333333 { 33333333 { 3333333333S33 {

flR300857

3 238

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ____________

\ \\ TBLK0424 . i

.ab Name: CAMBRG_______________ Contract: NOVAK_____ lMt>>TE.-t-

.ab Code: CAMBRG Case No. : NQVAK3 SAS No. : ______ SDG No. :

latrix: (toil/water) WATER Lab Sample ID: 9004279-17A

Sample ut/vol: 5. 0 (g/mL) fiL_ Lab File ID: H3S12________

.evel: (lou/med) LOU Date Received: 04/25/90


olumn: (pack/cap) PACK Dilution Factor: 1,J)____

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UC/L

74-87-3 ——————— Chloromethane _74-B3-9 ——————— Bromome thane75-O1-4 ——————— Vinul Chloride75-OO-3 ——————— Ch loroethane75-09-2 ——————— Methulene Chloride67-64- 1 ———————— Ac e t o n e75-15-0 ——————— Carbon Disulfide75-35-4 ——————— 1, 1-Dich loroethene75-34-3 ———————— 1, 1-Dich loroethane540-59-0 —————— 1.2-Dichloroethene (total) __67-66-3 ———————— Chloroform107-06-2 ——————— 1,2-Dichloree thane

- 78-93-3 ——————— 2-Butanone71-55-6 ———————— 1. 1. 1-Trichloroethane56-23-5 ——————— Carbon Tetraehloride108-05-4 ——————— Vinyl Acetate ' „ _ ,

8 75-27-4 ——————— Bromodichleremethane8 78-87-5 ——————— 1. 2-Dichloropropane1 10061-01-5 —— • —— cls-l« 3-DichloropropeneI 79-O1-6 ——————— Trich loroethene..,, .,.,_.1 124-48-1—— ——— — DibromochloromethaneJ 79-00-5 ——————— 1, 1.2-Trichloroethane\ 71-43-2 ———————— Benzene ,. ,8 10061-02-6- — • — -trans -1» 3-Dichloropropene ___8 75—25—2— — — —— — Bromoform1 108-10-1 —————— 4-Methvl-2-Pentanone..___ . _! 591-7B-6 ——————— 2-Hexanenei 127-1B-4 —————— TetrachloroetheneJ 79-34-5 ——————— 1* It 2* 2-Tetrechloroeth«ne ___{4 /IO O0_*9____ _ ̂— m . - — — . —lOo— BB— a—— —— — TolueneI 1O8-90-7-- ——— — Chlorobenzene1 100-41-4 —————— Ethylbenzene1 100-42-5 ——————— BtyreneJ 1330-2O-7 ————— Xylene (total).... _1

!1010101051055555510551055555555510105555555

•I

IU;u:uIUIB:u:u:u:u:u:u:u:u:u:u:u:u:u:u:uIUIUIUIUIUIUIU!UIUIUIUIU

!$R3!8

30858

3 239

IE EPA SAMPLEVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS 8

I TBLK0424 8_ab Name: CAMBRQ _______________ Contract: NOVAK _____ tMuJTfe-t- HlMf 7» 8

-ab Code: CAMBRQ Case No. : NQVAK3 SAS No. : ______ SDG No. :

latrix: (.oil/water) WATER Lab Sample ID: 9004379-17A

Sample ut/vol: 5. 0 (g/mL) ML_ Lab File ID: H3312________

-evel: (lou/med) LOW Date Received: 04/25/9O

', Moisture: not dec. ___ Date Analyzed: 05/02/90

:olumn (pack/cap) PACK Dilution Factor: 1. 0____

CONCENTRATION UNITS:lumber TICs found: _0 (ug/L or ug/Kg) UQ/L

i j i——————-CAS NUMBER 8 COMPOUND NAME 8 RT ! EST. CONC. 8

/ 8_________________________8_______8___________8

&R300859

3 24!

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ___

S {I TBLK0425 ,1

_ab Name: CAMBRQ _______________ Contract: NOVAK _____ I

_ab Code: CAMERG Case No.: NOVAK3 SAS No.: _____ SDG No.:

latrix: (soil/water) WATER Lab Sample ID: 90Q43Q7-O3A

sample wt/vol: 5. 0 (g/uiL) fll._ Lab File ID: K2532_______



olumn: (pack/cap) PACK Dilution Factor: 1. 0______


1

8 74-87-3 ——————— Chloromethane1 74-83-9 ——————— Bromomethane8 75-01-4 ——————— Vinul Chloride8 75-00-3 ——————— Ch loroethane8 75-09-2 ———————— Methylene Chloride8 67-64-1 ———————— Acetone8 75-15-0 ——————— Carbon Disulfide8 75-35-4 ——————— 1, 1-Dich loroethene, ,,,8 75-34-3 ———————— 1. 1-Dich loroethane8 540-59-0 —————— 1.2-Dichloroethene (total) __8 67-66-3 ——————— Chloroform! 107-06-2 ——————— 1, 2-Dichloroethane8 7B-93-3 ———————— 2-Butanone8 71-55-6 ——————— 1. 1. 1-Trichloroethane1 56-23-5 ———————— Carbon Tetrachloride .. _ .8 1O8-05-4 —————— Vinul Acetate .,8 75-27-4 ——————— Bromodich lorcmethane8 7B-B7-5 ———————— 1. 2-Dichloropropane . , ,8 1OO61-O1-5 ————— cis-1, 3-Dichloropropene8 79-01-6 ——————— Trichloroethene _ ._J 124-4B— 1- ————— -Dibromechloremethane} 79-00-5 ——————— 1.1,2-Trichleroethane .1 71-43-2 ——————— Benzene., .1 1O061-O2-6 ———— trans-l» 3-Dichloropropene_____1 75-25-2— —————— -BromoformJ lOB-lO-1 —————— 4-Methyl-2-Pentanone . .„.I 591-7S-6 ——————— 2-Hexanone! 127-1S-4 —————— Tetrach loroethene1 79-34-5 —————— 1. 1* 2* 2-Tetraehloroethane ___8 10B-BB-3 ——————— Toluene. ..._.,,„..,J 1OS-9O-7 —————— Chlorobenzene_.! 100-41-4 ——————— Ethulbenzene ....,_1 100-42-5 ——————— Styrene . ____ ,„.,1 1330-20-7 ————— Xvlene ( total >__._._8

1010101021055555510551055S55555510105555555RP

1I

:u:u:u:u:u:ui..t w

:u:u:u:u:u:u:u:u:uiu:u:uIUIUiuIUIUIUtuIU:uIU!U:uIU:uISOHB

3 250

IE EPA SAMPLEVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS I 8

I TBLK0425.ab Name: CAMBRQ ________________ Contract: NOVAK 8

.ab Code: CAMBRQ Case No. : NOVAK3 SAS No. : ______ SDO No. :

latrix: (soil/uater) WATER Lab Sample ID: 9004307-03A

Sample ut/vol: 5. 0 (g/mL) ML,_ Lab File ID: K2332______

.*vel: (lou/med) LOW Date Received: 04/56/90


alumn (pack/cap) PACK Dilution Factor: 1. 0_____

CONCENTRATION UNITS:umber TICs found: ___. (ug/L or ug/Kg) UG/L

i i—————j ;CAS NUMBER 8 COMPOUND NAME ! RT 8 EST. CONC. 8

3333333333333333 { 3333333333333333333333333333 | 33333333 j 3333333333333 { 3=

8 TETRAHYDROFURAN 8 69. 23 8 39 8 J

&R300861

3 0701A EPA SAMPLE NO.

VOLATILE ORGANICS ANALYSIS DATA SHEET _____________88 < MW-TB

Lab Name: CAMBRG_______________ Contract: NOVAK_____


latrix: (soil/uater) WATER Lab Sample ID: 9004330-05A

.ample ut/vol: 5. 0 (g/mL) QL._ Lab File ID: H3523_______

_evel: (lou/med) LOW Date Received: 04/27/90


Talumn: (pack/cap) PACK Dilution Factor. 1. 0____


74-87-3———————Chloromethane___________74-83-9———————Bromomethane__________________75-01-4———————Vinyl Chloride_________75—00-3———————Ch loroethane _______75-09-2———————Me th y 1 ene Ch 1 or i d e_________67-64-1————————Acetone________________75-15-C————————Car b on Di s u 1 f i d e_________75-35-A———————i, 1-Dich loroethene______75-34-3———————l. 1-Dich loroethane______540-59-0——————1, 2-Dichloroethene (total).67-66-3———————C h 1 o r o form_______107-06-2—•————1* 2-Dichloroethane______78-93-3————————2-Butanone__________________71-55-6———————I. 1. 1-Trich loroethane____56-23-5———————Carbon Te tree h lor ide_____108-05-4———————Vinyl Acetate___________75-27-4———————Bromodichloromethane_____78-87-5———————1. 2-Dichloropropane______1O061-01-5-————cis-1. 3-Dichloropropene__79-01 -6———————Tr ichloroeth ene_________124-48-1——————Dibromochloromethane_____79-00-5———————1* it 2-Trichloroethane____71-43-2——-————Benzene___________________1OO61-O2-6————tr«ns»l* 3-Dichloropropene_75-25—2———•———Bromoform___________________1O8-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4——————Tetrach loroethene______79-34-5———————1< 1. 2. 2-Tetrachloroethane.108-88-3——————Toluene______________________108-90-7———————Chlorobenzene ________100-41 -4——————Et hylbenzene __ ______100-42-5——————Styrene_______________133O-20-7—————Xylene (total)______________

10 :u10 :u10 tu10 :u2 iJ

32 IB5 IU5 !U5 .'U5 IU5 !U5 !U10 !U5 :u5 :u10 :u5 :u5 :u5 :u5 :us :u5 8U5 :us :u5 :u10 :u10 :u5 :u5 :u5 !Us :u5 JU5 :u


VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

ab Name: CAMBRG Contract:

ab Code: CAMBRQ Case No. : NOVAK3 SAS No. :

atrix: (soil/uater) WATER

ample ut/vol: 5. 0 (g/mL) ML

svel: (lou/med) LOW

Moisture: not dec.

3lumn (oack/cap) PACK

NOVAK

Lab Samp

Lab File

Date Rac

Date Ana

Dilution

CONCENTRATIONumber TICs found: __ 1. (ug/L or ug/Kg

l il 1

GAS NUMBER 1 COMPOUND NAME !

i K. i >-• ./ - t l i . ...Ill) * - i

RT

>̂ -MW-TB i /Aifc/TB-y-y/?$/?o

SDG No. :

le ID: 9004330-05A

ID: H3523

eived: 04/S7/9O

lyzed: 05/05/90

Factor: 1. 0

UNITS.) UG/L

« t 11 1 1

: EST. CONC. : Q :! ==========s==r= { sssss ;

1 1 t1 I 1

C

SR300863FORM I VOA-TIC 1/87 Rev

3 231

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

I TBLK0427Lab Name: CAMBRQ _______________ Contract: NOVAK _____ | t*UT&y-

-ab Code: CAMBRG Case No. : NOVAK3 SAS No. : _____ SDG No. :

latrix: (coil/water) WATER Lab Sample ID: 9004341-06A

Sample ut/vol: 5. 0 (g/mL) QL_ Lab File ID: K2538______


' Moisture: not dec. ___ Date Analyzed: 05/03/90

rolumn: (pack/cap) PACK Dilution Factor: l.,_0____


74-87-3———————Chloromethane,________________74-83-9———————B romomethan e ____________75-01-4———————Vinyl Chloride_________75-00-3—————•—Chloroethane_________________75-O9-2———————Methylene Chloride______67-64-1———————Ac e t one________________75-15-0———————Carbon DUulfide________75-35-4———————1« 1-Dich loroethene______75-34-3———————1, 1-Dich loroethane_________540-59-0——————1,2-Dichloroethene (total).67-66-3———————Ch lor of orm_________________1O7-06-2——————1.2-Dich loroethane______78-93-3———————2-Butanone _________________71-55-6————————1. 1. 1-Trichloroethane____56-23-5———————Carbon Tetrachloride_____108-05-4——————Vinyl Acetate__________75-27-4 —————/ o O /--̂ ^̂ ~~"~"

10061-01-5 ———79-01-6 —————. «;-»— *rO 1 «_>_t«7Q— rtn_ *!————— / _— _.A WWO L ̂VeC O75-25-2 —————108-10-1 ————591-76-6 ————1 97— >1 R— A——— ——. t / 1 _—•*-.————•7O_'î — 2-Tetrachloroethane. _—— Toluene „.,„.,— Chlorobenzene _l..nf—— Ethylbenzene ,„..—— Sturene .— Xulene (total ).,.,., .

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C IE EPA SAMPLE NC. vVOLATILE ORGANICS ANALYSIS DATA SHEET ______________-'TENTATIVELY IDENTIFIED COMPOUNDS 8 8

8 TBLK0427 . 8_ab Name: CAMBRQ_______________ Contract: NOVAK_____ 8 fcuTfl-T-«j|l"T/g» 8

.ab Code: CAMBRQ Case No. : NOVAK3 SAS No. : ______ SDQ No. : _____

latrix: doil/uater) WATER Lab Sample ID: 9004341-06A

Sample ut/vol: 5. Q (g/mL) ML_ Lab File ID: K2338______



alumn (pack/cap) PACK Dilution Factor: 1.0_____

CONCENTRATION UNITS:lumber TICs found: _0 (ug/L or ug/Kg) UG/l

CAS NUMBER3333333333333333

COMPOUND NAME3333333333333333333333323333

RT33333333

EST. CONC.3333333333333

1

8 Qi 33333

1

&R300865

Field Duplicates

ftR3Q0866

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1A EPA SAMPLE NrVOLATILE ORGANICS ANALYSIS DATA SHEET

I NSL-MW6R-0/ao Name: CAM9RG _________________ Contract: NOVAK _____ !

ab Code: CAMBRC Case No. . NQVAK3 SAS No. : ______ SDG No.

atrix: (soil/uater) WATER Lab Sample ID: 900434 1-04A

e ut/vol: 5 0 ig/mi_; ML Lab File ID: K253= ______

?vel: (iou/meo) LOW Date Received: 0&/25/aO

.loisture not oec ___ Date Analyzed 0? /0?-'e-"

:lu;r.r>- ( D ac k -'cac .' PACK Dilution Facts'- : C _____

CONCENTRATION UNITS.CAS N~ COMPOUND (ug/L or ug/Kg) UC/L

74-S7-3————————Ch 1 oromethane

75-01-4————————Vinyl Chloriae____75-00-3————————C hlorcethane ______75-09-2————————Metfty iene Chloride.67-6--i————————Acetone__________75-15-0————————C ar b on Disulfiie _________75-25--————————1. 1-Dicnlsroethene_______75-34-3————————i. 1-Dic M oroetnane_______540-59-0———————I/ 2-Dicr. loroethene < total >.67-6_>-3————————Ch loroform_______________107-06-r——————— 1 • 2-Dicr. Isroethane _______7S-93-3————————2-Sutanone_______________71-55-6—————�

5 :u · 2020. 12. 13. · 3 3g2 1a epa sample volatile organics analysis data sheet ____ lab name:...

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