7.245 560z-[t 60r-] lsv i,o'z i ooz{vovi,rra {8.258 /l- 8.240,/ - ' 7.9272- 7.e0e ==-...

16
o & t-.000 ..- 2.047 ..-------_- 2.034 - Z.ULJ b.15d 2.1,03 __\_ -l A N- 7.245 5.837 5.802 3.t25 5.119 q nq6 \ Ith < 2.352 I Yhh 0.840 0 .552 z a / \\v \ -a) t3 I Electronic Supplementary Material (ESI) for Dalton Transactions This journal is © The Royal Society of Chemistry 2011

Upload: others

Post on 28-Mar-2020

1 views

Category:

Documents


0 download

TRANSCRIPT

Page 1: 7.245 560z-[t 60r-] Lsv I,o'z I ooz{vovI,rra {8.258 /l- 8.240,/ - ' 7.9272- 7.e0e ==- 7.856 T.B4O 7.346 7.332 7.317 7.255 7.241 7.225 7.070 7.053-- 4.317 4.307 zI-.2 /\ (n=A

o&

t - .000..-

2.047..-------_-

2.034-

Z . U L J

b . 1 5 d

2.1 ,03__\_

-l

A

N -

7 .245

5 .8375 .8023 . t 2 5

5 .119q n q 6

\ I t h <

2.352

I Y h h

0 .840

0 . 552

za

/\\v

\

-a)t3

I

Electronic Supplementary Material (ESI) for Dalton TransactionsThis journal is © The Royal Society of Chemistry 2011

Page 2: 7.245 560z-[t 60r-] Lsv I,o'z I ooz{vovI,rra {8.258 /l- 8.240,/ - ' 7.9272- 7.e0e ==- 7.856 T.B4O 7.346 7.332 7.317 7.255 7.241 7.225 7.070 7.053-- 4.317 4.307 zI-.2 /\ (n=A

7 .284

V*a))--z

/ r

0.950.92

1.00-------\- 611

1 .15

11 .08- - \ -

3.224

-/- t.421- \= - 2 .649

--/-

_/-

\

L . 645t . o z 4

L .203I . I 6 J

I t t x x

I . U / O

Electronic Supplementary Material (ESI) for Dalton TransactionsThis journal is © The Royal Society of Chemistry 2011

helena.lovick
Rectangle
helena.lovick
Line
Page 3: 7.245 560z-[t 60r-] Lsv I,o'z I ooz{vovI,rra {8.258 /l- 8.240,/ - ' 7.9272- 7.e0e ==- 7.856 T.B4O 7.346 7.332 7.317 7.255 7.241 7.225 7.070 7.053-- 4.317 4.307 zI-.2 /\ (n=A

8.307./ 8.277

7.9097.8807.8807.317

8Lz {

s8s-[t

oc'c -f

gZ'2, I 7.2527.2337.Q747.072

=- 4.3044.280

z--z/ \@fl A=U)

/ \ / \T. i . ?. T.' u ! -u -oa - - a

1.9681.9451.9421.9381 .9161.5211.0801.0571 .0180.9950.964

N\-.-_ o.e4o0.9020.8880.8780.8650.8290.806

r l r r t t l t t t t l t i r t l t tl r r l

O ( J I J J N )o o ( ' t o

O O O

c=

A- +

A

sjt _g1 o

Electronic Supplementary Material (ESI) for Dalton TransactionsThis journal is © The Royal Society of Chemistry 2011

Page 4: 7.245 560z-[t 60r-] Lsv I,o'z I ooz{vovI,rra {8.258 /l- 8.240,/ - ' 7.9272- 7.e0e ==- 7.856 T.B4O 7.346 7.332 7.317 7.255 7.241 7.225 7.070 7.053-- 4.317 4.307 zI-.2 /\ (n=A

60z- [t

60r- ]

Lsv I,o'z I

ooz{

vovI

,rra

{

8.258

/l- 8.240

, / - 7.927' 2- 7.e0e

7.856==- T.B4O7.3467.3327.3177.2557.2417.2257.0707.053

-- 4.3174.307

z I - .2/ \(n=A A=(Jto / \ , / r o

T. T. T. T.! T ! - I la a a a

2.0492.0352.0211.5521.0691 .0551 .0311.0170.9540.9410 .9160.9020.8910.8770.8550.8410 .8160.802

, l r r ] , r r l , . , 1 r l , r r 1 ] r r l , t r , l t t t t i r t t t l l

6 , 9 < r r J r N ) N ) . , ( tb9srPsr 'PgnU O O O O O O

of)

J

:

aI

Electronic Supplementary Material (ESI) for Dalton TransactionsThis journal is © The Royal Society of Chemistry 2011

Page 5: 7.245 560z-[t 60r-] Lsv I,o'z I ooz{vovI,rra {8.258 /l- 8.240,/ - ' 7.9272- 7.e0e ==- 7.856 T.B4O 7.346 7.332 7.317 7.255 7.241 7.225 7.070 7.053-- 4.317 4.307 zI-.2 /\ (n=A

1 -39 . l - 35L32 . 859L29 . 6L5L29 .047L28 .324r21 . 3301 a / t ? O O

L24 .382L20 .353t_17 .860

1 l , 26817 .0L57 6 . 7 6L

2 ) ? ? , 4

3 l_ .91530 . BB430 .458L6 .9A l16 . B1B1-6 .501 -L6 . 453

,a'-

?--=-------

\

\

-r/--

\

z- -z/ \

@f, T=U)o / \ / \ o

i . T . T . T .l l ! ! ' ua a a a

N)O

@ -O

O \ -

F, N _

O

N _

g ) o -t ^

l v

N)

@ _O

O \ _

| 5 -

'I

N )_ - !

O

O +

Ui-=

Electronic Supplementary Material (ESI) for Dalton TransactionsThis journal is © The Royal Society of Chemistry 2011

Page 6: 7.245 560z-[t 60r-] Lsv I,o'z I ooz{vovI,rra {8.258 /l- 8.240,/ - ' 7.9272- 7.e0e ==- 7.856 T.B4O 7.346 7.332 7.317 7.255 7.241 7.225 7.070 7.053-- 4.317 4.307 zI-.2 /\ (n=A

1 . 920I . 9027 .8337 .8L77 . 3631 . 346t . 3091 .29 r1 . 2281 . 2027 . l _BB1 .L121 . L34] . LL17 .L04

f4U-

N\N

\

/<

ffWN

\

3 . B843 . 86B3 . 7833 .77Lr . 123L . 1LOL .698l_ .685L . 634r . 620L . 607:_ .59sL .279L .250L .245L .2331 - .L26I . L I41 .1011 .090L . 042L . 029t - . 015l_ .004

OOc=b)zr-z

(b

(tJ

(/J

O . W g \ - -n q q ?

f f i ; \

z . J 1 / -

n . 7 - _" ' " " : -1 . l -21 - r

I n ir\.- ,SL . W J Z

-l-.-qqF

NJ

T--;; ?\-

ryr=/ 4 1 r n L

t n l q -I t t \ t -- . " - : / .

!rl=

Electronic Supplementary Material (ESI) for Dalton TransactionsThis journal is © The Royal Society of Chemistry 2011

Page 7: 7.245 560z-[t 60r-] Lsv I,o'z I ooz{vovI,rra {8.258 /l- 8.240,/ - ' 7.9272- 7.e0e ==- 7.856 T.B4O 7.346 7.332 7.317 7.255 7.241 7.225 7.070 7.053-- 4.317 4.307 zI-.2 /\ (n=A

/ -1 .e61/ , / ' - 1 .849

t t - - - 7 .156- - - = - ' j ' i A 1

=\r_

7 .3L21 .2421 .T68I . 0246 . 92L

3 .2363 .2203 , 2052 . 4112 . 4632 . 4432 . 430

A A 1 . q

-at'

z\

OO(XJH '=--/

r{ >rr'Y Y\\/ \,/

PO

f . OOb\u cor r - r ^ -L . L Z J

I . U O i \- _ \

) . , L " -A .d ;a . a w v / -

. a ^ - /

L . . | 6 ) /

aI

5 L r 7

2 .320--

2 .2L2

c!=

Electronic Supplementary Material (ESI) for Dalton TransactionsThis journal is © The Royal Society of Chemistry 2011

Page 8: 7.245 560z-[t 60r-] Lsv I,o'z I ooz{vovI,rra {8.258 /l- 8.240,/ - ' 7.9272- 7.e0e ==- 7.856 T.B4O 7.346 7.332 7.317 7.255 7.241 7.225 7.070 7.053-- 4.317 4.307 zI-.2 /\ (n=A

1 4 1 0 t r O

L40 .939l_33 . 815L29 . 1 1 -2L2B . ALLL21 . 185126 . 77 0L26 . 47 4L24 . 5621 ) / t t r , ? ?

r 23 .859L22 . L I9LLA . BLA

4J / r -

zNN-

\ \ . _

\

17 . 27 81 l . 0227 6 . 168

54 . 928

40 .362

ool-\--{ )\:1 )-/

t 2--i.dh\

NYr\) \./

N]O

@

o\

PlFO

tst!O

?3('t

@

O'r

|F

Nj

(]cts

Electronic Supplementary Material (ESI) for Dalton TransactionsThis journal is © The Royal Society of Chemistry 2011

Page 9: 7.245 560z-[t 60r-] Lsv I,o'z I ooz{vovI,rra {8.258 /l- 8.240,/ - ' 7.9272- 7.e0e ==- 7.856 T.B4O 7.346 7.332 7.317 7.255 7.241 7.225 7.070 7.053-- 4.317 4.307 zI-.2 /\ (n=A

4 . 420.--------------.

nF---Zr r-r-z v - o L L

8 .038 - r -

2 .000

L . 9 7 9--....--..--.--.a

o)

4LN

\

5 . 1 0 ' 7

7 . 1047 .L987 .L937 .L721 .L527 .L3L7 .0107 .0557 .436

Electronic Supplementary Material (ESI) for Dalton TransactionsThis journal is © The Royal Society of Chemistry 2011

Page 10: 7.245 560z-[t 60r-] Lsv I,o'z I ooz{vovI,rra {8.258 /l- 8.240,/ - ' 7.9272- 7.e0e ==- 7.856 T.B4O 7.346 7.332 7.317 7.255 7.241 7.225 7.070 7.053-- 4.317 4.307 zI-.2 /\ (n=A

L43 .5601 -42 . 846L42 . 647L33 .125L29 . 607L2B .656L28 .50 '712B .066L27 . l 4LI21 . 385L27 . 282L21 ,LBLL26 .558L24 .LBOL22 . 058LLA .636rL2 .242

17 .30977 .05276 .196

62 . 089

trl/f//a_////-

%-

NN

\-I

N

O

tso\

tsr!O

IF

z--z

r{ Ft3l

O

(tI

-{

@O

Electronic Supplementary Material (ESI) for Dalton TransactionsThis journal is © The Royal Society of Chemistry 2011

Page 11: 7.245 560z-[t 60r-] Lsv I,o'z I ooz{vovI,rra {8.258 /l- 8.240,/ - ' 7.9272- 7.e0e ==- 7.856 T.B4O 7.346 7.332 7.317 7.255 7.241 7.225 7.070 7.053-- 4.317 4.307 zI-.2 /\ (n=A

o -

g.71- 6

tiz\aoi-w9:17.,- I

@t

J

@

o)

1.75

5.47 r -

5.85-_------_'!

.

'

o-

( , r -

F -

lrllrM-/ /r%N\rN

\

z\

-=d-

5 . 52L

2.8502 . 6 Z l J

2.8052 .7822 .759

7 .8627 ,8497 . 4567 . 4267 .3237.3r47 . 30 "7t . z Y tt . 2 6 2"7 .249 '7 .2237 .2207 . L6L -7 .1357 .L077 .482

O.9BB0 .9650 .8280 .805

-'

Electronic Supplementary Material (ESI) for Dalton TransactionsThis journal is © The Royal Society of Chemistry 2011

Page 12: 7.245 560z-[t 60r-] Lsv I,o'z I ooz{vovI,rra {8.258 /l- 8.240,/ - ' 7.9272- 7.e0e ==- 7.856 T.B4O 7.346 7.332 7.317 7.255 7.241 7.225 7.070 7.053-- 4.317 4.307 zI-.2 /\ (n=A

t/[

4NN

I

2 7 . 1 2 1

22 . 488

LAL .845

139 .006133 .875L29 . 407l -28 . B1BL28 .240L27 . 0L8L26 .356L26 . 035L24 . 03LL24 . 006L22 . 9L0L22 . 60 rLL6 . 544L rA .334

71 . 29277 .03676 .783

(.,

{-L-()

N-)O

O

Ol

'FO

N)

P

O

oI

(o

O

O lO

|F

N)O

oU=

Electronic Supplementary Material (ESI) for Dalton TransactionsThis journal is © The Royal Society of Chemistry 2011

Page 13: 7.245 560z-[t 60r-] Lsv I,o'z I ooz{vovI,rra {8.258 /l- 8.240,/ - ' 7.9272- 7.e0e ==- 7.856 T.B4O 7.346 7.332 7.317 7.255 7.241 7.225 7.070 7.053-- 4.317 4.307 zI-.2 /\ (n=A

7 .8947 . B6B7 .8391 .1877 .1597 .6401 .6L47 . 4927 .4797 . 4627 . 431'7 . 4327 . 4227 .3967 . 311 ,7 .360'7 . 2977 . 2716 .050

tr/t[

JlL-L

NNTNN

-no5\- o-1st-

2.00r-12.60:s2/-

1.66

{

o)

ctl

s

@

I\)o

N)

-

o-

E _ro

Electronic Supplementary Material (ESI) for Dalton TransactionsThis journal is © The Royal Society of Chemistry 2011

Page 14: 7.245 560z-[t 60r-] Lsv I,o'z I ooz{vovI,rra {8.258 /l- 8.240,/ - ' 7.9272- 7.e0e ==- 7.856 T.B4O 7.346 7.332 7.317 7.255 7.241 7.225 7.070 7.053-- 4.317 4.307 zI-.2 /\ (n=A

L42 . 495t -38 .052L34 .626L34 .022L29 . 5 r4L29 .L4BL29 , ALBL28 .397L2B .33 II 21 . 200L26 .L52L25 .867r24 .27 rL24 . L24L23 . 265L22 . I 3L118 .508LL1 . 341LLA .924

71 . 29011 .03576 .7BL

fr%

-_ - R\,.--__\N\

-\\\\\\-

\\\\\-\\\\L\ \ \ \\\v

\ \ -\L

of),rW

z--z( )J \ -\lrO

\_/-

N]O _O

ts@ -O

ts

O

O

tsN J -

O

O r _O

POO

aN)

@ _

O

N -O

fr!=

Electronic Supplementary Material (ESI) for Dalton TransactionsThis journal is © The Royal Society of Chemistry 2011

Page 15: 7.245 560z-[t 60r-] Lsv I,o'z I ooz{vovI,rra {8.258 /l- 8.240,/ - ' 7.9272- 7.e0e ==- 7.856 T.B4O 7.346 7.332 7.317 7.255 7.241 7.225 7.070 7.053-- 4.317 4.307 zI-.2 /\ (n=A

3 . ttt\' 1 1 t r ? \f . r J / \ _ _

t-J:Tv;--;;;-

< \ < |J . J J J r a

f . b b f . /

4 .520 /

F

\]

Ol

|F

(,

N)

P

t - .000

arl.lN

a 1 4 /o . r J _ o_._-.-..-\-4 .365

x-6-;-;--2 . 6 L 3

6 . J J 4 -

F-

Fr1H

a zz{ 9-k a

t fr\ itr- lf,

\d

?I'11

A

?

.7 Rtr. A

7 . 5391 . 61 -97 .5 tL7 . 4927 . 3L57 .300t . z 6 )

7 . 2487 . 2297 . 2077 . 1 -95/ . J - 6 c ,

7 .L777 . L621 .L467 .L277 .TT37 .0587 .046t . v z v

7 .0137 .0077 .001 -5 .925

3 . 4083 .2813 .2703 . L23

r : +oz1 / t n . A

I . J d J

L .255

0 .367n n " ?

t\

_----_::-l--

Electronic Supplementary Material (ESI) for Dalton TransactionsThis journal is © The Royal Society of Chemistry 2011

Page 16: 7.245 560z-[t 60r-] Lsv I,o'z I ooz{vovI,rra {8.258 /l- 8.240,/ - ' 7.9272- 7.e0e ==- 7.856 T.B4O 7.346 7.332 7.317 7.255 7.241 7.225 7.070 7.053-- 4.317 4.307 zI-.2 /\ (n=A

,-4-

//-/ //-

' / / / -

h-N\\

\\\-\ \ -\\-L

1 -55 .L97L49 . 684L46 . 402_ L J / . U l _ 6

L28 . 432'li. ^ ^L Z 6 . J ) 6

" . K ^I Z 6 . I U Y4 4 - a A 6r z t . o v 6

1 -26 . 7 401_25 .801_L25 .55L] -25 . 462124 . 7 49] -24 .5834 4 - d - aL r I . v I o

L L I . Z Y 6A a 6

r L + . v o z9 zzg o '> 'o

+ 2r -r J m \ !ru- '$ \rd\

a.1.1

A

____-----, i57 .355- - - 65 .733

--------"-- 44.020

25 . 5L9

L5 . 021 ,

F|tr

P@o

H

HN)

o\

|F

F

O oI

NCJ

N)

IJrijH

Electronic Supplementary Material (ESI) for Dalton TransactionsThis journal is © The Royal Society of Chemistry 2011