aboratory testing guidel

Laboratory Testing GuideLaboratory Testing Guide2021

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CONNECT WITH AN EXPERT1.800.860.1775 | [email protected]

2

Tabl

e of

Con

tent

s General Information

3 Introduction

4 Operations and Services

4 Submitting Samples and Blanks

4 Shipping

4 Sampling Media

4 Confidentiality

5 Blanks for IH and Environmental Analysis

5 Radiological Samples

5 Sample Disposal

5 Analysis Fees

5 Turn-around Times

6 Payment Terms

6 Accreditations/Certifications

7 Abbreviations

Analytical Services8 Industrial Hygiene - Inorganics

19 Industrial Hygiene - Organics

60 Industrial Hygiene Profiles

63 Environmental and Wet Chemistry - Inorganics

69 Environmental and Wet Chemistry - Organics

70 Environmental and Wet Chemistry - Sample Prep

73 Powdered Metal Services

73 Mining and Mineral Services

74 Mineral Identification and Characterization

76 Asbestos Analytical Services

78 Construction Materials Laboratory Services

80 Materials and Particulate Characterization

86 Granular Activated Carbon Services

88 Gypsum, Gypsum Products, Anhydride (CaSO4) and FGD Byproducts

89 Calcium Carbonate, Limestone, Dolomite & Related Products

90 Coal, Ash & Bag House Dust

91 Talc

92 Kaolin/Kaolinite

93 Detrimental Materials, Glasses, Bioactive Glasses, Borosilicate Glasses, Ceramics

94 Pharmaceutical Analytical Services

96 Criminal Forensics (Trace Evidence)

97 Terms and Conditions

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Thank you for choosing RJ Lee Group for your analytical

services needs. We are committed to providing our

clients with quality service and reliable results in a

timeframe to meet their needs. We have more than 30

years of experience as an analytical services laboratory

and have diligently served thousands of clients. Our

industrial hygiene and environmental experts are well-

informed of methodologies mandated by government

standards. Laboratory tests are conducted using standard

test methods approved and/or mandated by OSHA,

NIOSH, EPA, MSHA, ASTM and others. Our laboratory

testing services are provided in response to regulatory

requirements as well as for material and product

requirements and specifications.

Each sample is unique and given the attention necessary

to perform the required analysis. Our protocols ensure

that chains of custody are intact and sample preparation

methods maintain sample integrity. All staff follow

standard procedures to maintain our high quality

standards, and reports are issued and explained with

clarity and attention to clients’ requirements.

Our service offerings extend far beyond the testing

services listed in this document. We routinely conduct

problem-solving and investigative studies for a broad

range of industry. Our multi-disciplinary technical

staff of subject matter experts (SMEs) are available for

consultation and scientific investigations, and have

collective centuries of experience in root cause failure

analysis, remaining life assessments, corrosion studies,

product development, material identification, and

reverse engineering. This often requires project and

sample-specific testing protocols that combine multiple

existing laboratory methods into the investigation.

Method development in sample preparation or analysis is

also not uncommon and our laboratory staff, under the

direction of our SMEs, is experienced in performing and

documenting analytical methods tailored for the issues

at hand. When necessary, this investigative approach

provides our clients with high value results, and has

withstood regulatory and legal scrutiny because the

developed methods are guided by established standards.

RJ Lee Group Laboratory ServicesRJ Lee Group Laboratory ServicesA Higher Measure of Confidence

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Submitting Samples Samples are to be submitted to the laboratory along with appropriate chain-of-custody documentation and the following information clearly indicated:

» Sample identification

» Type of analysis requested

» Sample volume (where applicable)

» Analysis turn-around time

» Report to name, address, phone number and email address

» Bill to name, address, phone number, and email address

» Special instructions (if any)

» Signature and printed name, phone number, and email address of person remitting the sample.

Clients are encouraged to use the Chain of Custody form available on our website at www.rjleegroup.com. Multi-print carbonless forms are also available by contacting a client services representative.

ShippingThe client is responsible for all shipping costs and special handling fees (e.g., hazardous materials or international destinations) as well as costs associated with return shipping of sample containers and samples.

Sampling Media Common sampling media are provided to clients at no charge, provided the media are returned for analysis. The client is responsible for all overnight shipping charges. Clients will be responsible for the costs of any specialty media requested as well as related shipping costs.

Operations and ServicesSample Receiving HoursSamples are received Monday through Friday during normal business hours:

RJ Lee Group Headquarters Laboratory Monroeville, PA from 8 AM to 5 PM (EST)

Columbia Basin Analytical LaboratoriesPasco, WA from 8AM to 5 PM (PST)

Please notify client services if samples will be submitted outside of normal business hours. Any samples received after 12 PM or on weekends will be logged in the next business day.

Holding TimesSome samples may have preservation requirements and are subject to specified holding times. For samples that are suitable for analysis, provided and received in a timely manner we will make every effort to meet all holding time requirements prescribed for the preparation and analysis of the samples.

Hazardous WasteHazardous waste is managed in accordance with local, state, and federal regulations. The waste is segregated, bulked, neutralized, labeled for shipment, and stored by a hazardous waste technician in controlled waste storage areas. We reserve the right to return to the client, at the client’s expense, any unused portions of samples that may be considered hazardous waste.

Record RetentionRJ Lee Group retains records of laboratory analysis for the period of time required by the appropriate accrediting body, according to contract requirements, or as per client specific requests. We reserve the right to assess record retention fees for those records that, at the client’s request, are retained beyond accreditation or contract requirements. Confidentiality

All laboratory data and reports are kept strictly confidential with discretion applied toward proprietary materials and processes. Clients must provide written authorization if analytical results or reports are to be released to a third party.

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Turn-around Times (TAT)Unless a client indicates otherwise, all samples received will be logged and processed for standard turn-around times (TAT) as indicated below. TAT is measured in business days; for example, a sample arriving today for 1-Day TAT would be due at the end of the next business day. Same-day TAT (anything less than 24 hours) is also available for some testing services. Same day TAT requires 24-hour advance notice and samples must be received by 10 AM the day of analysis. Please contact a client service representative for more information.

Service Area Standard TAT

Industrial Hygiene 5-10

Environmental & Wet Chemistry 7-10

Specialty Chemicals & Coatings 10

Asbestos Analysis 5-10

Coal Mine Industry Testing 5-10

Construction Materials 15

Materials Characterization 5-10

Criminal Forensics 5-10

Pharmaceutical 5

Mineral Characterization/ID 10

Blanks for IH and Environmental AnalysisSome of the analytical methods listed in this document require that blanks be submitted with the samples. At a minimum, one blank sample should be included with every batch of samples submitted. When submitting large numbers of samples, typically one blank for every 10 samples should be included. Blank samples are invoiced at standard sample rates.

Radiological SamplesOur Columbia Basin Analytics Laboratory facility is licensed to handle and analyze radiological samples in a variety of matrices using a number of analytical methods. We also have the capability to conduct R&D, bench testing, and waste-form development studies. RJ Lee Group will either return samples to the client or dispose of them at client expense. Please contact us for details and pricing.

Sample DisposalSamples submitted will be stored for 30 days before being discarded unless the client notifies otherwise. Shipping and handling fees will be assessed for the return of any samples. The client will be responsible for any additional costs incurred in the disposal of unusual or hazardous material samples that do not comply with RJ Lee Group’s standard disposal practices. We reserve the right to assess sample storage fees if a client requests that samples be retained for more than 30 days.

Analysis FeesPrices listed are subject to change without prior notification. This document lists standard commercial prices for samples analyzed following specified methods. Please contact a client service representative to discuss price adjustments based on sample volume or turn-around times. Custom projects may incur additional analysis or consulting fees for test set up, data compilation, interpretation, and customized reporting.

We also offer more specialized analysis. If the method or analyte is not listed, please call. For some media, such PPI’s, POVM and Jewel Impactors cassettes, additional media fees apply. For odd chemicals, additional fees could apply for the calibration standards. Most prices listed are for single analytes and might include the preparation fee. Please call if you need pricing for multiple analytes in the same sample using the same methodology/technique.

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Payment Terms A copy of RJ Lee Group’s Terms & Conditions of Sale are included in this document. Unless otherwise indicated in writing (authorization by an officer of RJ Lee Group), terms of payment shall be net thirty (30) days after date of invoice. After the invoice due date, RJ Lee Group reserves the right to assess the lesser of one and one-half percent (1.5%) of the unpaid balance (annual rate of 18%) or the maximum late payment penalty charge permitted by law shall be added for each month or part thereof that payment is delinquent. RJ Lee Group has the right at any time to change the amount of credit or terms of payment or to withdraw credit and to require partial or full payment in advance as a condition of performing services. Payments shall be made regardless of the results of the testing or other services performed by RJ Lee Group. RJ Lee Group also accepts MasterCard, VISA, and American Express.

HQ - Pittsburgh East, Pennsylvania

» American Assoication for Laboratory Accreditation (A2LA)

» American Association of State Highway and Transportation Officials (AASHTO)

» American Industrial Hygiene Association - Laboratory Accreditation Program (AIHA-LAP, LLC)

» ANSI National Accreditation Board » Pennsylvania Department of Environmental

Protection (DEP) » Commonwealth of Virginia Department of

Professional and Occupational Regulation (DPOR) » Food & Drug Administration Registered (FDA

(Registration Number 1000313868) » National Voluntary Laboratory Accreditation Program

(NVLAP) » State of California ELAP » State of Maryland DHMH Office of Health Care

Quality » State of New York ELAP - Lab ID# 10884 » State of West Virginia Bureau for Public Health Office

of Environmental Health Services » Texas Forensic Science Commission » Texas Commission on Environmental Quality » US Department of Justice: Drug Enforcement

Administration (DEA)

Pasco, Washington

» American Industrial Hygiene Assocation - Laboratory accreditation Program (AIHA-LAP, LLC)

» ASME NQA-1 Compliant » State of Oregon ELAP » State of Washington Department of Ecology » State of Washington Radioactive Materials » US Department of Energy Consolidated Audit

Program (DOECAP)

Accreditations and CertificationsRJ Lee Group is committed to delivering services that not only meet, but exceed, regulatory requirements and client expectations for value, consistency, and reliability. Our Pennsylvania Laboratory is ISO/IEC 17025:2005 accreditated, and both laboratories are accredited to perform specific analyses by the entities listed below:

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AbbreviationsAES Auger Electron Spectroscopy

Ag Silver Membrane

AHERA Asbestos Hazard Emergency Response Act

ASTM American Society for Testing Materials

BZ Sol Benzene Soluble

CCSEM Computer-Controlled Scanning Electron Microscopy

Charcoal Charcoal Tube

CVAA Cold Vapor, Atomic Absorption Spectrophotometry

CMS Carbon Molecular Sieve

DNPH Dinitrophenylhydrazine

DSC Differential Scanning Calorimeter

EC/OC Elemental Carbon / Organic Carbon

EDS Energy Dispersive Spectroscopy

EPA Environmental Protection Agency

FE-SEM Field Emission - Scanning Electron Microscopy

FL Fluorescence Detector

FLAA Flame Atomic Absorption Spectrophotometry

FTIR Fourier Transform Infrared Spectroscopy

GC-FID Gas Chromatography with Flame Ionization Detection

GC-ECD Gas Chromatography with Electron Capture Detection

GC-MS Gas Chromatography with Mass Spectrometric Detection

GC Gas Chromatography with Thermal Energy Analyzer

GFF Glass Fiber Filter

Grav Gravimetric

HPLC-UVHigh Performance Liquid Chromatography with UV

Detection

HPLC-UV/FLHigh Performance Liquid Chromatography with

Fluorescence and UV Detection

IC Ion Chromatography

ICP-AESInductively Coupled Plasma Atomic Emission

Spectrophotometry

ICP-MS Inductively Coupled Plasma – Mass Spectrometry

IC-UV Ion Chromatography with UV Detector

IMP Impinger

IR Infrared Spectroscopy

ISE Ion Specific Electrode

L Liter

LPM Liters Per Minute

MCE Mixed Cellulose Ester

MSA Mine Safety Appliances

MSHA Mine Safety and Health Administration

N/A Not Applicable

NC No Charge

NIOSH National Institute for Occupational Safety and Health

OSHA Occupational Safety and Health Administration

OVS OSHA Versatile Sampler

PAH Polynuclear Aromatic Hydrocarbons

PC Polycarbonate

PCB Polychlorinated Biphenyl

PCM Phase Contrast Microscopy

PLM Polarized Light Microscopy

POVM Passive Organic Vapor Monitor

PTFE Polytetrafluoroethylene Filter

PVC Polyvinyl Chloride Filter

PVC-PH Polyvinyl Chloride Pure Homopolymer Filter

SEM Scanning Electron Microscopy

STEM Scanning Transmission Electron Microscopy

TGA Thermogravimetric Analyzer

TEM Transmission Electron Microscopy

USP U.S. Pharmacopeia

UV Ultraviolet Detector

VAS Visible Absorption Spectrophotometry

XPS X-ray Photoelectron Spectroscopy

XRD X-ray Diffraction

XRF X-ray Fluorescence

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Industrial HygieneIndustrial HygieneInorganics

Analyte CAS # Method Technique Sampling Media Sampling Rate

Suggested Volume

Price TAT Matrix Unit

Aluminum (Al) 7429-90-5 NIOSH 7300 mod./NIOSH 7303

ICP-AES MCE/PVC 1 - 4 5 - 100 $42.00* 5 Day Air Each

Aluminum Oxide (Al2O3)

1344-28-1 NIOSH 7300 mod (special digestion)

ICP-AES MCE/PVC 1 - 4 5 - 100 $100.00 5 Day Air Each

Antimony (Sb) 7440-36-0 NIOSH 7300 mod./NIOSH 7303

ICP-AES/ICP-MS

MCE/PVC 1-4 50-2000 $42.00* 5 Day Air Each

Arsenic (As) 7440-38-2 NIOSH 7300 mod./NIOSH 7303

ICP-AES/ICP-MS

MCE/PVC 1 - 4 5 - 2000 $42.00* 5 Day Air Each

Asbestos NIOSH 7400 PCM MCE 0.5 - 16 (See Method)

$13.00 5 Day Air Each

Asbestos NIOSH 7402 TEM MCE 0.5 - 16 (See Method)


*Compatible analytes billed at $22

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Industrial HygieneIndustrial HygieneInorganics (cont.)


Suggested Volume


Barium (Ba) 7440-39-3 NIOSH 7300 mod./NIOSH 7303

ICP-AES/ICP-MS


Beryllium (Be) 7440-41-7 NIOSH 7300 mod./NIOSH 7303

ICP-MS MCE/PVC 1 - 4 1250 - 2000

$42.00* 5 Day Air Each

Beryllium Oxide (BeO)


ICP-MS MCE/PVC 1 - 4 1250 - 2000


Bismuth (Bi) 1304-43-4 NIOSH 7300 mod./NIOSH 7303

ICP-AES/ICP-MS


Boron (B) 7440-42-8 NIOSH 7303 ICP-AES MCE 1 - 4 480 - 960 $42.00* 5 Day Air Each

Cadmium (Cd) 7440-43-9 NIOSH 7300 mod./NIOSH 7303

ICP-AES/ICP-MS


Calcium (Ca) 7440-70-2 NIOSH 7300 mod./NIOSH 7303


Calcium Hydroxide (CaOH)

1305-62-0 NIOSH 7303 ICP-AES MCE $50.00 5 Day Air Each

Calcium Oxide (CaO) 1305-78-8 NIOSH 7303 ICP-AES MCE $50.00 5 Day Air Each

Carbon Black 1333-86-4 NIOSH 5000 Gravimetric PVC - preweighed

1 - 2 30 - 570 $22.00 5 Day Air Each

Chromium (Cr) 7440-47-3 NIOSH 7300 mod./NIOSH 7303

ICP-AES/ICP-MS



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Suggested Volume


Chromium, Hexavalent (CrVI) Paint

18540-29-9

OSHA 215 IC-UV PVC 2 960 $75.00 5 Day Air Each

Chromium, Hexavalent (CrVI) Welding Fume/Plating Operation

18540-29-9

OSHA 215 IC-UV PVC 2 960 $70.00 5 Day Air Each

Cobalt (Co) 7440-48-4 NIOSH 7300 mod./NIOSH 7303

ICP-AES/ICP-MS


Compendium IO-3.4 Compendium IO-3.1 / IO-3.4

ICP-AES Call 5 Day Air Each

Compendium IO-3.5 Compendium IO-3.1 / IO-3.5

ICP-MS Call 5 Day Air Each

Copper (Cu) 7440-50-8 NIOSH 7300 mod./NIOSH 7303

ICP-AES/ICP-MS


Diesel Particulate Matter-DPM

NIOSH 5040 Thermal Optic EC/

OC

Quartz fiber 2 - 4 142 - 1920 $60.00 10 Day Air Each

Diesel Particulate Matter-DPM

NIOSH 5040 Thermal Optic EC/

OC

Jeweled impactor cassette

1.7 - 2.0 142 - 1920 $89.00 10 Day Air Each


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Suggested Volume


Dust, Respirable NIOSH 0600 Gravimetric PVC preweighed 1.7-8.0 (size selective

sampler

dependent)

20 - 1200 $22.00 5 Day Air Each

Dust, Total NIOSH 0500 Gravimetric PVC preweighed 1 - 2 20 - 1200 $22.00 5 Day Air Each

Elemental Carbon NIOSH 5040 Thermal Optic EC/

OC

Quartz fiber 2 - 4 142 - 1920 $60.00 10 Day Air Each

Gallium (Ga) 7440-55-3 NIOSH 7303 ICP-AES/ICP-MS

MCE $52.00 5 Day Air Each

Gold (Au) 7440-57-5 NIOSH 7303 ICP-AES/ICP-MS

MCE 1 - 4 1 - 3300 $52.00 5 Day Air Each

Hafnium (Hf) 7440-65-5 NIOSH 7300 mod (special digestion)

ICP-AES/ICP-MS

MCE/PVC 1 - 4 5 - 200 $100.00 5 Day Air Each

Hydrochloric Acid (Hydrogen Chloride, HCl)

7647-01-0 NIOSH 7903 IC SKC 226-10-03 0.2 - 0.5 3 - 100 $55.00 5 Day Air Each

Hydrogen Bromide (HBr, Hydrobromic Acid)


Hydrogen Fluoride (HF)



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Suggested Volume


Indium (In) 7440-74-6 NIOSH 7303 ICP-AES/ICP-MS


Iron (Fe) 7439-89-6 NIOSH 7300 mod./NIOSH 7303


Iron Oxide Fume (Fe) 1309-37-16 NIOSH 7303 ICP-AES MCE/PVC 1 - 4 5 - 100 $42.00* 5 Day Air Each

Lanthanum (La) 7439-91-0 NIOSH 7300 mod. ICP-AES/ICP-MS

MCE/PVC $62.00 5 Day Air Each

Lead (Pb) 7439-92-1 NIOSH 7300 mod./NIOSH 7303

ICP-AES/ICP-MS


Lead oxide (Pb) 1317-36-8 NIOSH 7303 ICP-AES/ICP-MS

MCE 1 - 4 50 - 2000 $42.00* 5 Day Air Each

Lead (Pb) 7439-92-1 EPA 3050/EPA 6010C ICP-AES Soil $20.00 5 Day Solid/Bulk

Each

Lead (Pb) 7439-92-1 EPA 3050/EPA 6010C ICP-AES Paint $20.00 5 Day Solid/Bulk

Each

Lead (Pb) (Determination of surface contamination by lead and its compounds)

7439-92-1 EPA 3050/EPA 6010C ICP-AES ASTM certified wipe

1 - 2 $20.00 5 Day Wipe Each


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Suggested Volume


Lithium (Li) 7439-93-2 NIOSH 7300 mod. ICP-AES/ICP-MS


Magnesium (Mg) 7439-95-4 NIOSH 7300 mod./NIOSH 7303

ICP-AES MCE/PVC $42.00* 5 Day Air Each

Manganese (Mn) 7439-96-5 NIOSH 7300 mod./NIOSH 7303

ICP-AES/ICP-MS


Mercury (Hg) Particulate

7439-97-6 OSHA 145 CVAA MCE 2 10 $55.00 5 Day Air Each

Mercury (Hg) Passive 7439-97-6 OSHA 140 CVAA SKC 520-02A/520-03

0.02 9.6 $55.00 5 Day Air Each

Mercury (Hg) Vapor or Particulate

7439-97-6 NIOSH 6009 CVAA 226-17-1A 0.15 - 0.25

2 - 100 $55.00 5 Day Air Each

Mercury (Hg) Wipes 7439-97-6 OSHA 145 CVAA Wipe $55.00 5 Day Wipe Each

Molybdenum (Mo) 7439-98-7 NIOSH 7300 mod./NIOSH 7303

ICP-AES/ICP-MS


Neodymium (Nd) 7440-00-8 NIOSH 7303 ICP-AES/ICP-MS


Nickel (Ni) 7440-02-0 NIOSH 7300 mod./NIOSH 7303

ICP-AES/ICP-MS


Nitric Acid (HNO3) 7697-37-2 NIOSH 7903 IC SKC 226-10-03 0.2 - 0.5 3 - 100 $55.00 5 Day Air Each


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Suggested Volume


Nuisance Dust, Respirable

NIOSH 0600 Gravimetric PVC - preweighed

1.7-8.0 (Size selective

sampler

dependant)

20 - 1200 $22.00 5 Day Air Each

Nuisance Dust, Total NIOSH 0500 Gravimetric PVC - preweighed

1 - 2 20 - 1200 $22.00 5 Day Air Each

Ozone 10028-15-6 OSHA 214 IC SKC 225-9014 1.5 90 $70.00 5 Day Air Each

Palladium (Pd) 7440-05-3 NIOSH 7303 ICP-AES/ICP-MS


Particulates not otherwise regulated, Respirable

NIOSH 0600 Gravimetric PVC - preweighed 1.7-8.0 (Size selective

sampler

dependent)

20-1200 $22.00 5 Day Air Each

Particulates not otherwise regulated, Total

NIOSH 0500 Gravimetric PVC - preweighed

1.5 - 2.0 20 - 1200 $22.00 5 Day Air Each

Phosphoric Acid (H3PO4)


Phosphorus (P) 7723-14-0 NIOSH 7300 mod./NIOSH 7303

ICP-AES MCE/PVC $42.00 5 Day Air Each

Platinum (Pt) 7440-06-4 NIOSH 7303 ICP-AES/ICP-MS

MCE 1 - 4 200 - 5000 $52.00 5 Day Air Each


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Suggested Volume


Potassium (K) 7440-09-7 NIOSH 7300 mod./NIOSH 7303


Selenium (Se) 7782-49-2 NIOSH 7300 mod./NIOSH 7303

ICP-AES/ICP-MS


Silica, Respirable Crystalline ( ~5 ug nominal reporting limit for Quartz - Cristobalite and Tridymite) and Dust

Various NIOSH 7500/0600 XRD/Grav PVC - preweighed

1.7-8.0 (Size selective

sampler

dependant)

400 - 1000 $106.00 5 day Air Each

Silica, Respirable Crystalline (~2.5 ug nominal reporting limit for Quartz ~5 ug nominal reporting limit for Cristobalite and Tridymite) and Dust

Various NIOSH 7500/0600 XRD/Grav PVC - preweighed

1.7-8.0 (Size selevtive

sampler

dependant)

400 - 1000 $212.00 10 day Air Each

Silver (Ag) 7440-22-4 NIOSH 7300 mod. ICP-AES/ICP-MS


Sodium (Na) 7440-23-5 NIOSH 7303 ICP-AES MCE 1 - 4 13 - 2000 $42.00* 5 Day Air Each


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Suggested Volume


Strontium (Sr) 7440-24-6 NIOSH 7300 mod./NIOSH 7303

ICP-AES/ICP-MS


Sulfuric Acid (H2SO4) 7664-93-9 NIOSH 7903 IC SKC 226-10-03 0.2 - 0.5 3 - 100 $55.00 5 Day Air Each

Tantalum (Ta) 7440-25-7 NIOSH 7300 mod (special digestion)

ICP-AES MCE/PVC 1 - 4 200 - 400 $100.00 5 Day Air Each

Tellurium (Te) 13494-80-9

NIOSH 7300 mod./NIOSH 7303

ICP-AES/ICP-MS


Thallium (Tl) 7440-28-0 NIOSH 7300 mod./NIOSH 7303

ICP-AES/ICP-MS


Tin (Sn) 7440-31-5 NIOSH 7300 mod./NIOSH 7303

ICP-AES/ICP-MS


Titanium (Ti) 7440-32-6 NIOSH 7300 mod./7303 ICP-AES/ICP-MS

MCE/PVC $42.00 5 Day Air Each

Titanium Dioxide (TiO2)


ICP-AES/ICP-MS


Total Particulate NIOSH 0500 Gravimetric PVC - preweighed

1 - 2 20 - 1200 $22.00 5 Day Air Each

Tungsten (W) 7440-33-7 NIOSH 7300 mod (special digestion)

ICP-AES/ICP-MS


Vanadium (V) 7440-62-6 NIOSH 7300 mod./NIOSH 7303

ICP-AES/ICP-MS



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Suggested Volume


Welding Fume Particulate

NIOSH 0500 Gravimetric PVC - preweighed or Matched-wight

MCE

1 - 4 200 - 1200 $22.00 5 Day Air Each

Yttrium (Y) 7440-65-5 NIOSH 7300 mod./NIOSH 7303

ICP-AES/ICP-MS


Zinc (Zn) 7646-85-7 NIOSH 7300 mod./NIOSH 7303

ICP-AES/ICP-MS


Zinc Oxide (ZnO) 1314-13-2 NIOSH 7303 ICP-AES/ICP-MS


Zirconium (Zr) 7440-67-7 NIOSH 7300 mod. ICP-AES/ICP-MS


Zirconium Oxide (ZrO2)


ICP-AES/ICP-MS



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Industrial HygieneIndustrial Hygiene

Solids and Hazardous Waste

Analyte CAS # Method Technique Sampling Media Price TAT Matrix Unit

Lead (Pb) 7439-92-1 EPA 3050/ EPA 6010C ICP-AES Soil $20.00 5 Day Solid/Bulk Each

Lead (Pb) 7439-92-1 EPA 3050/ EPA 6010C ICP-AES Paint $20.00 5 Day Solid/Bulk Each

Lead (Pb) (Determination of surface contamination by lead and its compounds)

7439-92-1 EPA 3050/ EPA 6010C ICP-AES ASTM certified wipe

$20.00 5 Day Wipe Each

Inorganics (cont.)

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Industrial HygieneIndustrial HygieneOrganics

Analyte CAS # Method Technique Sampling Media

Sampling Rate

Suggested Volume


1, 1, 2 - Trichloroethane 79-00-5 NIOSH 1003

GC-FID SKC 226-01 0.01 - 0.2 2 - 60 $55.00 10 Day Air Each

1, 1, 2 - Trichloroethane 79-00-5 OSHA 11 GC-FID SKC 226-01 0.2 10 $55.00 10 Day Air Each

1, 1, 2 - Trichloroethane 79-00-5 NIOSH 1500 Mod

GC-FID POVM 3M 3500 POVM SKC 575-001

8 hrs $55.00 10 Day Air Each

1, 1, 1 - Trichloroethane (methyl chloroform)

71-55-6 NIOSH 1003

GC-FID SKC 226-01 0.01 - 0.2 0.1 - 8 $55.00 10 Day Air Each


71-55-6 OSHA 14 GC-FID SKC 226-01 0.2 3 $55.00 10 Day Air Each


71-55-6 NIOSH 1500 Mod



1, 1, 2 -Trichloro-1 , 2 , 2 -trifluoroethane (Refrigerant 113)

76-13-1 OSHA 113 Mod

GC-FID POVM SKC 575-001


1, 1, 2 -Trichloro-1 , 2 , 2 -trifluoroethane (Refrigerant 113)

76-13-1 NIOSH 1020

GC-FID (2) SKC 226-01

0.01 - 0.05 0.1 - 3 $70.00 10 Day Air Each

1, 1-Dichloroethane 75-34-3 NIOSH 1003


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Industrial HygieneIndustrial HygieneOrganics (cont.)


Sampling Rate

Suggested Volume


1, 1-Dichloroethane 75-34-3 NIOSH 1500 Mod



1, 2, 3 - Trichloropropane

96-18-4 NIOSH 1003


1, 2, 3 - Trichloropropane

96-18-4 NIOSH 1500 Mod



1, 2, 3 - Trimethylbenzene

526-73-8 NIOSH 1502


1, 2-Dichloroethylene 540-59-0 NIOSH 1003


1, 2-Dichloroethylene 540-59-0 NIOSH 1500 Mod



1, 3 Butylene Glycol (1,3 Butanediol)

107-88-0 NIOSH 5523

GC-FID GFF & SKC 226-57

0.5 - 2.0 5 - 60 $70.00 10 Day Air Each

1,6-Hexamethylene Diisocyanate (HDI)

822-06-0 OSHA 42 HPLC SKC 225-9002

1 15 $100.00 10 Day Air Each

1-Methoxy-2-Propanol (Propylene glycol methylether)

107-98-2 OSHA 99 GC-FID SKC 226-01 0.1 5 - 10 $55.00 10 Day Air Each

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Industrial HygieneIndustrial HygieneOrganics (cont.)Analyte CAS # Method Technique Sampling

MediaSampling

RateSuggested

VolumePrice TAT Matrix Unit

1-Methoxy-2-Propanol Acetate (Propylene glycol methyl ether acetate)

108-65-6 OSHA 99 GC-FID POVM SKC 575-002


2, 4 -Toluene Diisocyanate (TDI)

584-84-9 OSHA 42 HPLC-UV SKC 225-9002

1 15 $100.00 10 Day Air Each

2, 6 -Toluene Diisocyanate (TDI)

91-08-7 OSHA 42 HPLC-UV SKC 225-9002

1 15 $100.00 10 Day Air Each

2-Butanone (MEK) 78-93-3 OSHA 1004 GC-FID POVM 3M 3520 POVM SKC 575-002


2-Butanone (MEK) 78-93-3 NIOSH 2500

GC-FID SKC 226-81A 0.01 - 0.2 0.25 - 12 $55.00 10 Day Air Each

2-Butoxyethanol (Butyl Cellosolve)



111-76-2 NIOSH 1500 Mod


or 002



111-76-2 NIOSH 1403


DH_04202021


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MediaSampling

RateSuggested


2-Butoxyethyl acetate (Butyl Cellosolve Acetate)

112-07-2 OSHA 83 GC-FID POVM 3M 3500 POVM SKC 575-002


2-Butoxyethyl acetate (Butyl Cellosolve Acetate)


2-Ethoxyethoxy Ethanol (Carbitol )

111-90-0 NIOSH 1403

GC-FID SKC 226-01 0.01 - 0.05 10 $55.00 10 Day Air Each

2-Ethoxyethoxy Ethanol (Carbitol )

111-90-0 NIOSH 1403 mod.

GC-FID POVM SKC 575-001 or

002


2-Heptanone (Methyl n-Amyl ketone)

110-43-0 NIOSH 1301 GC-FID SKC 226-01 0.01 - 0.2 1 - 25 $55.00 10 Day Air Each


110-43-0 NIOSH 2553



110-43-0 NIOSH 1500 Mod



2-Methoxyethanol 109-86-4 NIOSH 1403


DH_04202021


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MediaSampling

RateSuggested


2-Methoxyethanol 109-86-4 NIOSH 1403


4-Vinyl Toluene, 3-vinyl Toluene

39294-88-7 NIOSH 1501 GC-FID POVM 3M 3500 POVM SKC 575-001


4,4 - Methylene diphenyl diisocycanate

101-68-8 OSHA 42 HPLC SKC 225-9002

1 15 $100.00 10 Day Air Each

5-Methyl-3-Heptanone 541-85-5 NIOSH 1301 GC-FID SKC 226-01 0.01 - 0.2 1 - 25 $55.00 10 Day Air Each

5-Methyl-3-Heptanone 541-85-5 NIOSH 1500 Mod


or 002


Acenaphthylene 208-96-8 NIOSH 5506

HPLC-UV/FL PTFE + SKC 226-30-04

2 200 - 5000 $100.00 10 Day Air Each

Acenapthene 83-32-9 NIOSH 5506


2 200 - 1000 $100.00 10 Day Air Each

Acetaldehyde 75-07-0 NIOSH 2539

HPLC-UV SKC 226-118 0.01 - 0.05 5 $100.00 10 Day Air Each

Acetone 67-64-1 NIOSH 1300

GC-FID SKC 226-01 0.01 - 0.20 0.5 - 3.0 $55.00 10 Day Air Each

Acetone 67-64-1 OSHA 69 GC-FID ORBO 91 0.05 3 $55.00 10 Day Air Each

DH_04202021


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MediaSampling

RateSuggested


Acetone 67-64-1 NIOSH 1500 Mod



Acetonitrile 75-05-8 NIOSH 1606


Acetonitrile 75-05-8 NIOSH 1500 Mod


or 002


Acrolein 107-02-8 NIOSH 2539

GC-FID & GC-MS

SKC 226-118 0.01 - 0.05 48 $100.00 10 Day Air Each

Acrylonitrile 107-13-1 NIOSH 1604


Allyl Alcohol 107-18-6 NIOSH 1402


Allyl Alcohol 107-18-6 NIOSH 1500 Mod


or 002


a-Methyl Styrene 98-83-9 NIOSH 1501 GC-FID SKC 226-01 0.01 - 0.2 1 - 30 $55.00 10 Day Air Each

a-Methyl Styrene 98-83-9 NIOSH 1500 Mod



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MediaSampling

RateSuggested


Aniline 62-53-3 NIOSH 2002


Aniline 62-53-3 NIOSH 2017

GC-FID SKC 225-9004 & SKC

226-15

0.1 - 0.2 5 - 50 $100.00 10 Day Air Each

Aniline 62-53-3 OSHA PV2079

GC-FID SKC 226-98 0.2 30 $70.00 10 Day Air Each

Anthracene 120-12-7 NIOSH 5506


2 200 - 1000 $100.00 10 Day Air Each

Benz (a) anthracene 56-55-3 NIOSH 5506


2 200 - 1000 $100.00 10 Day Air Each

Benzene 71-43-2 OSHA 1005 GC-FID POVM 3M 3500, SKC

575-001,002


Benzene 71-43-2 NIOSH 1501 GC-FID SKC 226-01 0.01 - 0.2 5 - 30 $55.00 10 Day Air Each

Benzene Sol (Coal Tar Pit Vol, Asphalt Fumes)

8052-42-4 NIOSH 5042 / 0500

Grav. / BZSOL PTFE - Preweighed

1 - 4 28 - 400 $75.00 10 Day Air Each

DH_04202021


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MediaSampling

RateSuggested


Benzene Sol (Coal Tar Pit Vol, Asphalt Fumes) Additional characterization by HPLC available

Various OSHA 58 Grav. / BZSOL GFF 2 960 $75.00 10 Day Air Each

Benzene, Ethyl Benzene, Toluene and Xylene, Total Hydrocarbon (VOC as Hexane)

Various NIOSH 1501 GC-FID SKC 226-01 3M 3500,

POVM or SKC 575-001 or

002

0.1 - 0.5 10 $70.00 10 Day Air Each

Benzo (a) pyrene 50-32-8 NIOSH 5506


2 200 - 1000 $100.00 10 Day Air Each

Benzo (b) fluoranthene 205-99-2 NIOSH 5506


2 200 - 1000 $100.00 10 Day Air Each

Benzo (e) pyrene 192-97-2 NIOSH 5506


2 200 - 1000 $100.00 10 Day Air Each

Benzo (ghi) perylene 191-24-2 NIOSH 5506


2 200 - 1000 $100.00 10 Day Air Each

Benzo (k) fluoranthene 207-08-9 NIOSH 5506


2 200 - 1000 $100.00 10 Day Air Each

Benzyl Acetate 140-11-4 OSHA PV2124


DH_04202021


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MediaSampling

RateSuggested


Benzyl Chloride 100-44-7 NIOSH 1003


Benzyl Chloride 100-44-7 NIOSH 1500 Mod


or 002


Biphenyl (Diphenyl) 92-52-4 NIOSH 2530

GC-FID SKC 226-35-01

0.01 - 0.5 15 - 30 $55.00 10 Day Air Each

Bromoform 75-25-2 NIOSH 1003


Bromoform 75-25-2 NIOSH 1500 Mod



Butyl Acrylate 141-32-2 NIOSH 1450 mod.


Butyl Carbitol (Diethylene Glycol Monobutyl Ether)

112-34-5 NIOSH 1403 mod.


Butyl Carbitol (Diethylene Glycol Monobutyl Ether)

112-34-5 NIOSH 1403 mod.

GC-FID SKC 575-002 8 hrs $55.00 10 Day Air Each

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MediaSampling

RateSuggested


Butyl Cellosolve (2-Butoxyethanol)

111-76-2 NIOSH 1500 Mod


or 002


Butyl Cellosolve (2-Butoxyethanol)

111-76-2 NIOSH 1403


Butyraldehyde 123-72-8 NIOSH 2539 mod.

HPLC-UV SKC 226-118 0.01 - 0.05 5 $100.00 10 Day Air Each

Camphor 76-22-2 NIOSH 1301 GC-FID SKC 226-01 0.01 - 0.2 1 - 25 $55.00 10 Day Air Each

Camphor 76-22-2 NIOSH 1500 Mod


or 002


Carbitol (2-Ethoxyethoxy Ethanol)

111-90-0 NIOSH 1403 mod.


Carbon Tetrachloride 56-23-5 NIOSH 1003


Carbon Tetrachloride 56-23-5 NIOSH 1500 Mod



DH_04202021


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MediaSampling

RateSuggested


Cellosolve (2-Ethoxyethanol)

110-80-5 NIOSH 1500 Mod


or 002


Cellosolve Acetate (2-Ethoxyethyl Acetate)

111-15-9 NIOSH 1450



111-15-9 NIOSH 1500 Mod


or 002




Chlorobenzene 108-90-7 NIOSH 1003


Chlorobenzene 108-90-7 NIOSH 1500 Mod


or 002


Chlorobromomethane 74-97-5 NIOSH 1003


DH_04202021


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MediaSampling

RateSuggested


Chlorobromomethane 74-97-5 NIOSH 1500 Mod



Chloroform 67-66-3 NIOSH 1003


Chloroform 67-66-3 NIOSH 1500 Mod



Chloroprene (2-Chloro-1,3-butadiene)

126-99-8 OSHA 112 GC-FID SKC 226-111A 0.05 6 $55.00 10 Day Air Each

Chloroprene (2-Chloro-1,3-butadiene)

126-99-8 NIOSH 1002


Chrysene 218-01-9 NIOSH 5506


2 200 - 1000 $100.00 10 Day Air Each

Coal Tar Naphtha Various NIOSH 1550


Coal Tar Naphtha Various NIOSH 1550

GC-FID POVM 3M 3500 POVM

SKC


DH_04202021


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MediaSampling

RateSuggested


Coal Tar Pitch Volatiles Additional characterization by HPLC available

65996-93-2 OSHA 58 Grav. / BZSOL GFF 2 960 $75.00 10 Day Air Each

Cumene 92-82-8 NIOSH 1501 GC-FID SKC 226-01 0.01 - 0.2 1 - 30 $55.00 10 Day Air Each

Cumene 92-82-8 NIOSH 1500 Mod


or 002


Cyclohexane 110-82-7 NIOSH 1500


Cyclohexane 110-82-7 NIOSH 1500 Mod


or 002


Cyclohexanol 108-93-0 NIOSH 1402


Cyclohexanol 108-93-0 NIOSH 1500 Mod


or 002


Cyclohexanone 108-94-1 NIOSH 1300


Cyclohexanone 108-94-1 OSHA 01 GC-FID SKC 226-110 0.02-0.05 10 $55.00 10 Day Air Each

DH_04202021


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MediaSampling

RateSuggested


Cyclohexanone 108-94-1 NIOSH 1500 Mod

GC-FID POVM 3M 3500


Cyclohexene 110-83-8 NIOSH 1500

GC-FID SKC 226-01 0.01- 0.2 5 - 7 $55.00 10 Day Air Each

Cyclohexene 110-83-8 NIOSH 1500 Mod


or 002


Cyclopentane 287-92-3 NIOSH 1500 Mod


Cyclopentane 287-92-3 NIOSH 1500 Mod

GC-FID POVM 3M 3520, POVM SKC 575-001


Diacetone Alcohol 123-42-2 NIOSH 1402


Diacetone Alcohol 123-42-2 NIOSH 1500 Mod



Dibenz (a,h) anthracene

53-70-3 NIOSH 5506

HPLC-UV/FL PTFE & SKC 226-30-04

2 200 - 1000 $100.00 10 Day Air Each

Dibutylphthalate 84-74-2 NIOSH 5020

GC-FID MCE/PVC 1 - 3 6 - 200 $55.00 10 Day Air Each

DH_04202021


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MediaSampling

RateSuggested


Dibutylphthalate 84-74-2 OSHA 104 GC-FID SKC 226-56 1 240 $55.00 10 Day Air Each

Dichlorofluoromethane 75-43-4 NIOSH 2516

GC-FID (2) SKC 226-09

0.01 - 0.05 0.25 - 3.0 $70.00 10 Day Air Each

Dichloromethane (Methylene Chloride)

75-09-2 NIOSH 1005

GC-FID (2) SKC 226-01

0.01 - 0.2 0.5 - 2.5 $70.00 10 Day Air Each


75-09-2 OSHA 80 GC-FID ORBO 91 0.05 3 $70.00 10 Day Air Each


75-09-2 NIOSH 1005 mod.


Diesel Fuel NIOSH 1550

GC-FID SKC 226-01 Send reference

material in separate shipment

0.01 - 0.2 1.3 - 20 $70.00 10 Day Air Each

Diethyl Ether (Ethyl Oxide)

60-29-7 NIOSH 1610 mod.




60-29-7 NIOSH 1610 GC-FID SKC 226-01 0.01 - 0.2 0.25 - 3.0 $55.00 10 Day Air Each


60-29-7 NIOSH 1500 Mod



DH_04202021


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MediaSampling

RateSuggested


Diethylene Glycol 111-46-6 NIOSH 5523


0.5 - 2.0 5 - 60 $70.00 10 Day Air Each

Diethylene Glycol Monoethyl Ether

111-90-0 NIOSH 1403 mod.


4 - 8 hrs $70.00 10 Day Air Each

Diisobutyl Ketone 108-83-8 NIOSH 1300


Diisobutyl Ketone 108-83-8 NIOSH 1500 Mod



Diisooctylphthalate (bis (2-ethylhexyl)-phthalate)

117-81-7 NIOSH 5020

GC-FID MCE/PVC 1 - 3 10 - 200 $55.00 10 Day Air Each

Dimethoxymethane (Methylal)


Dimethoxymethane (Methylal)

109-87-5 NIOSH 1500 Mod



Dimethylacetamide 127-19-5 NIOSH 1500 Mod

GC-FID POVM 3M 3500


Dimethylacetamide (N,N-dimethylacetamide)

127-19-5 NIOSH 2004

GC-FID SKC 226-10 0.01 - 1 15 - 80 $55.00 10 Day Air Each

DH_04202021


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MediaSampling

RateSuggested


Dimethylformamide 68-12-2 NIOSH 2004


Dimethylformamide 68-12-2 NIOSH 1500 Mod



Di-n-Octyl Phthalate (DNOP)

117-84-0 OSHA 104 GC-FID SKC 226-56 1.0 - 3.0 10 - 240 $55.00 10 Day Air Each

Dipropylene Glycol Methyl Ether

34590-94-8 NIOSH 1403 mod.



Dipropylene Glycol Methyl Ether

34590-94-8 NIOSH 1403 mod.


Divinylbenzene 1321-74-0 OSHA 89 GC-FID SKC 226-73 0.05 12 $70.00 10 Day Air Each

Divinylbenzene 1321-74-0 OSHA 89 GC-FID POVM 3M 3500


Epichlorohydrin 106-89-8 NIOSH 1010 GC-FID SKC 226-01 0.01 - 0.2 2 - 30 $55.00 10 Day Air Each

Epichlorohydrin 106-89-8 NIOSH 1500 Mod


or 002


Esters 1 (one analyte) Various NIOSH 1450

GC-FID SKC 226-01 0.01-0.2 1.0 - 10 $55.00 10 Day Air Each

DH_04202021


36


MediaSampling

RateSuggested


Ethanol (Ethyl Alcohol) 64-17-5 NIOSH 1400


Ethanol (Ethyl Alcohol) 64-17-5 OSHA 5001 GC-FID SKC 226-82(Two Tubes in

Series)

0.05 12 $100.00 10 Day Air Per Set

Ethanol (Ethyl Alcohol) 64-17-5 NIOSH 1500 Mod



Ethanol (Ethyl Alcohol) 64-17-5 NIOSH 1400 mod.



Ethyl Acetate 141-78-6 NIOSH 1500 Mod


or 002


Ethyl Acetate 141-78-6 NIOSH 1457


Ethyl Acrylate 140-88-5 NIOSH 1450


Ethyl Acrylate 140-88-5 OSHA 92 GC-FID SKC 226-73 0.05 12 $55.00 10 Day Air Each

DH_04202021


37


MediaSampling

RateSuggested


Ethyl Acrylate 140-88-5 OSHA 92 GC-FID POVM 3M 3500 POVM SKC 575-002


Ethyl Amyl Ketone (3-Octanone)

106-68-3 NIOSH 1500 Mod


Ethyl Bromide (Bromoethane)

74-96-4 OSHA PV2061



74-96-4 NIOSH 1500 Mod




74-96-4 NIOSH 1011 GC-FID SKC 226-01 0.01 - 0.2 0.5 - 4 $100.00 10 Day Air Each

Ethyl Butyl Ketone 106-35-4 NIOSH 1301 GC-FID SKC 226-01 0.01 - 0.2 1 - 25 $55.00 10 Day Air Each

Ethyl Butyl Ketone 106-35-4 NIOSH 1500 Mod


Ethyl Butyl Ketone 106-35-4 NIOSH 1500 Mod


or 002


Ethyl Cellosolve (2-Ethoxyethanol)

110-80-5 NIOSH 1500 Mod


or 002


DH_04202021


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MediaSampling

RateSuggested



110-80-5 NIOSH 1403



110-80-5 NIOSH 1450


Ethyl Chloride (Chloroethane)

75-00-3 NIOSH 2519

GC-FID (2) SKC-226-25

0.02 - 0.05 0.3 - 3 $100.00 10 Day Air Per Set

Ethyl Methacrylate 97-63-2 NIOSH 2537


0.01 - 0.05 1 - 8 $55.00 10 Day Air Each

Ethylbenzene 100-41-4 OSHA 1002 GC-FID POVM SKC 575-002

240 min 50 $55.00 10 Day Air Each

Ethylbenzene 100-41-4 NIOSH 1500 Mod

GC-FID POVM 3M 3500, SKC575-001,002

4 hours $55.00 10 Day Air Each

Ethylbenzene 100-41-4 NIOSH 1501 GC-FID SKC 226-01 0.01 - 0.2 1 - 24 $55.00 10 Day Air Each

Ethylene Chlorohydrin (2-Chloroethanol)

107-07-3 NIOSH 2513Mod

GC-FID SKC 226-81A 0.01 - 0.2 2 - 35 $55.00 10 Day Air Each

Ethylene Chlorohydrin (2-Chloroethanol)

107-07-3 NIOSH 1500 Mod

GC-FID POVM 3M 3500

15 min (STEL), 8 hrs (TWA)


Ethylene Dichloride (1, 2 Dichloroethane)

107-06-2 NIOSH 1003


DH_04202021


39


MediaSampling

RateSuggested


Ethylene Dichloride (1, 2 Dichloroethane)

107-06-2 NIOSH 1500 Mod



Ethylene Glycol 107-21-1 NIOSH 5523


0.5 - 2 5 - 60 $70.00 10 Day Air Each

Ethylene Glycol Monobutyl Ether (Butyl Cellosolve, 2-butoxyethanol)

111-76-2 NIOSH 1403


Fluoranthene 206-44-0 NIOSH 5506


2 200 - 1000 $100.00 10 Day Air Each

Fluorene 86-73-7 NIOSH 5506


2 200 - 1000 $100.00 10 Day Air Each

Formaldehyde 50-00-0 NIOSH 2016

HPLC POVM SKC UMEX 100

15 min - 24 hrs $100.00 10 Day Air Each

Formaldehyde 50-00-0 NIOSH 2016

HPLC SKC 226-119 0.3 - 1.5 1 - 15 $100.00 10 Day Air Each

Furfural 98-01-1 NIOSH 2529


Furfural 98-01-1 OSHA 72 Mod

GC-FID POVM 3M 3500


Furfuryl Alcohol 98-00-0 NIOSH 2505


DH_04202021


40


MediaSampling

RateSuggested


Furfuryl Alcohol 98-00-0 NIOSH 1500 Mod

GC-FID POVM 3M 3500


Gasoline NIOSH 1500 mod.


Gasoline NIOSH 1500 mod.

GC-FID POVM 3M 3500


Glutaraldehyde 111-30-6 OSHA 64 HPLC-UV SKC 225-9003

0.05 - 0.5 1 - 30 $100.00 10 Day Air Each

Heptane 142-82-5 NIOSH 1500 Mod


or 002


Heptyl Alcohol (1-Heptanol)

111-70-6 NIOSH 1402 mod.


Hexachloroethane 67-72-1 NIOSH 1003


Hexachloroethane 67-72-1 NIOSH 1500 Mod



Hexone (MIBK--Methyl-isobutylketone)

108-10-1 NIOSH 1300





DH_04202021


41


MediaSampling

RateSuggested



108-10-1 NIOSH 1500 Mod



Hydrocarbons - Aromatic

NIOSH 1501 Personnel Sampler

GC-FID SKC-226-01 See method See method $70.00 10 Day Air Each

Hydrocarbons, Total (Hydrocarbons, BP 36-216 Degrees C)

NIOSH 1500 mod.

GC-FID SKC 226-01 0.2 5 - 20 $70.00 10 Day Air Each

Indeno (1,2,3cd) pyrene 193-39-5 NIOSH 5506


2 200 - 1000 $100.00 10 Day Air Each

Isoamyl Acetate 123-92-2 NIOSH 1450


Isoamyl Acetate 123-92-2 NIOSH 1500 Mod


or 002


Isoamyl Alcohol 123-51-3 NIOSH 1402


Isoamyl Alcohol 123-51-3 NIOSH 1500 Mod



DH_04202021


42


MediaSampling

RateSuggested


Isobutyl Acetate 110-19-0 NIOSH 1450


Isobutyl Acetate 110-19-0 NIOSH 1500 Mod



Isobutyl Alcohol 78-83-1 NIOSH 1401 GC-FID SKC 226-01 0.01 - 0.2 2 - 10 $55.00 10 Day Air Each

Isobutyl Alcohol 78-83-1 NIOSH 1500 Mod



Isooctane (2,2,4-Trimethylpen-tane)

540-84-1 NIOSH 1500 mod.


Isooctane (2,2,4-Trimethylpen-tane)

540-84-1 NIOSH 1500 mod.



Isophorone 78-59-1 NIOSH 2508 Mod

GC-FID SKC 226-81A 0.01 - 1.0 25 $55.00 10 Day Air Each

Isophorone 78-59-1 NIOSH 1500 Mod



Isophrone Di-Isocyanate (IPDI)

4098-71-9 OSHA PV2034

HPLC SKC 225-9002

1 60 $100.00 10 Day Air Each

DH_04202021


43


MediaSampling

RateSuggested


Isophrone Di-Isocyanate (IPDI)

4098-71-9 OSHA 42 mod.

HPLC SKC 225-9002

1 15 - 30 $100.00 10 Day Air Each

Isopropyl Acetate 108-21-4 NIOSH 1454


Isopropyl Acetate 108-21-4 NIOSH 1500 Mod


or 002


Isopropyl Alcohol (2-Propanol)

67-63-0 NIOSH 1400



67-63-0 OSHA 5001 GC-FID SKC 226-82 (Two Tubes in

Series)

0.05 12 $100.00 10 Day Air Per Set


67-63-0 NIOSH 1500 Mod



Isovaleraldehyde 590-86-3 NIOSH 2539 mod.

HPLC SKC 226-118 0.01 - 0.05 5 $100.00 10 Day Air Each

Kerosene (Diesel Fuel) 8008-20-6 NIOSH 1550


Limonene 138-86-3 NIOSH 1552 GC-FID SKC 226-01 0.01 - 0.2 2 - 30 $55.00 10 Day Air Each

Limonene 138-86-3 OSHA PV2036


DH_04202021


44


MediaSampling

RateSuggested


MDI Methylene bisphenyl isocyanate

101-68-8 OSHA 47 HPLC-UV SKC 225-9002

1 15 $100.00 10 Day Air Each

Mesityl Oxide 141-79-7 NIOSH 1301 GC-FID SKC 226-01 0.01 - 0.2 1 - 25 $55.00 10 Day Air Each

Mesityl Oxide 141-79-7 NIOSH 1500 Mod


Mesityl Oxide 141-79-7 NIOSH 1500 Mod

GC-FID POVM 3M 3500 POVM

SKC


Methanol (Methyl Alcohol)

67-56-1 OSHA 5001 GC-FID SKC 226-82 (Two Tubes in

Series)

0.05 3-5 based on relative humidity

$100.00 10 Day Air Per Set

Methanol (Methyl Alcohol)

67-56-1 NIOSH 2000


Methyl Acetate 79-20-9 NIOSH 1458


Methyl Acetate 79-20-9 NIOSH 1500 Mod



Methyl Acrylate 96-33-3 NIOSH 1459


Methyl Acrylate 96-33-3 OSHA 92 GC-FID SKC 226-73 0.05 12 $55.00 10 Day Air Each

DH_04202021


45


MediaSampling

RateSuggested


Methyl Acrylate 96-33-3 NIOSH 1500 Mod



Methyl Cellosolve (2-Methoxyethanol)

109-86-4 NIOSH 1500 Mod


or 002


Methyl Cellosolve Acetate (2-Methoxyethyl Acetate)

110-49-6 NIOSH 1451 GC-FID SKC 226-01 0.01 - 0.20 0.20 - 20 $55.00 10 Day Air Each

Methyl Cellosolve Acetate (2-Methoxyethyl Acetate)


Methyl Ethyl Ketone (MEK) (2-Butanone)

78-93-3 NIOSH 2500

GC-FID SKC 226-81A 0.01 - .20 0.25 - 12 $55.00 10 Day Air Each

Methyl Isoamyl Acetate 108-84-9 NIOSH 1450


Methyl Isoamyl Ketone (5-methyl-2-hexanone)

110-12-3 NIOSH 1500 Mod


DH_04202021


46


MediaSampling

RateSuggested


Methyl Isoamyl Ketone (5-methyl-2-hexanone)

110-12-3 NIOSH 1500 Mod



Methyl Isobutyl Carbinol (Methyl Amyl Alcohol)

108-11-2 NIOSH 1402


Methyl Isobutyl Carbinol (Methyl Amyl Alcohol)

108-11-2 NIOSH 1402 mod.



Methyl Isobutyl Ketone (4-Methyl 2 Pentanone, MIBK, hexone isopropyl acetone)

108-10-1 NIOSH 1300






108-10-1 NIOSH 1500 Mod



Methyl Methacrylate 80-62-6 NIOSH 2537


0.01 - 0.05 1 - 8 $55.00 10 Day Air Each

DH_04202021


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MediaSampling

RateSuggested


Methyl Methacrylate 80-62-6 OSHA 94 GC-FID SKC 226-73 0.01 - 0.05 10 $55.00 10 Day Air Each

Methyl Methacrylate 80-62-6 NIOSH 1500 Mod



Methyl n-Amyl ketone (2 - Heptanone)


Methyl n-Amyl ketone (2 - Heptanone)

110-43-0 NIOSH 1500 Mod



Methyl n-Butyl Ketone (MBK, 2-Hexanone)

591-78-6 NIOSH 1300


Methyl n-Butyl Ketone (MBK, 2-Hexanone)

591-78-6 NIOSH 1500 Mod



Methyl Propyl Ketone (2-Pentanone)

107-87-9 NIOSH 1300 mod.

GC-FID POVM 3M 3500 SKC 575-

001 or 002



107-87-9 NIOSH 1300



107-87-9 NIOSH 1500 Mod


or 002


DH_04202021


48


MediaSampling

RateSuggested


Methyl tert-Amyl Ether 994-05-8 NIOSH 1615 mod.


Methyl tert-Butyl Ether (MTBE)

1634-04-4 NIOSH 1615 GC-FID SKC 226-37 (Two Tubes in

Series)

0.1 - 0.2 2 - 96 $100.00 10 Day Air Per Set

Methylcyclohexane 108-87-2 NIOSH 1500


Methylcyclohexane 108-87-2 NIOSH 1500 Mod



Methylene Chloride (Dichloromethane)

75-09-2 NIOSH 1005

GC-FID (2) SKC 226-01 (Two Tubes in

Series)

0.01 - 0.2 0.5 - 2.5 $100.00 10 Day Air Per Set




75-09-2 NIOSH 1005 mod.


n-Amyl Acetate 628-63-7 NIOSH 1450


n-Amyl Acetate 628-63-7 NIOSH 1500 Mod


or 002


DH_04202021


49



Sampling Rate

Suggested Volume


Naphtha (Coal Tar/Petroleum)

NIOSH 1550

GC-FID SKC 226-01 Send reference

material in separate shipment

0.01 - 0.2 1.3 - 20 $70.00 10 Day Air Each

Naphthalene 91-20-3 NIOSH 5506


2 200 - 1000 $100.00 10 Day Air Each

Naphthalene 91-20-3 OSHA 35 GC-FID SKC 226-110 0.2 10 $55.00 10 Day Air Each

Naphthalene 91-20-3 NIOSH 1500 Mod

GC-FID POVM 3M 3500


Naphthalene 91-20-3 NIOSH 1501 mod.

GC-FID SKC 226-01 0.01 100 - 200 $55.00 10 Day Air Each

n-Butyl Acetate 123-86-4 NIOSH 1450


n-Butyl Acetate 123-86-4 OSHA 1009 GC-FID POVM 3M 3500 POVM SKC 575-001

or 002


n-Butyl Alcohol (1-Butanol)

71-36-3 NIOSH 1500 Mod


or 002


n-Butyl Alcohol (1-Butanol)


DH_04202021


50


MediaSampling

RateSuggested


n-Butyl Glycidyl Ether 192337 NIOSH 1616 GC-FID SKC 226-01 0.01 - 0.2 15 - 30 $55.00 10 Day Air Each

n-Butyl Glycidyl Ether 192337 NIOSH 1500 Mod



n-Butyl Methacrylate 97-88-1 NIOSH 2537 mod.


0.01 - 0.5 1 - 8 $55.00 10 Day Air Each

n-Decane 124-18-5 NIOSH 1500

GC-FID SKC 226-01 0.01- 0.2 5 $55.00 10 Day Air Each

n-Decane 124-18-5 NIOSH 1500 Mod



n-Heptane 142-82-5 NIOSH 1500

GC-FID SKC 226-01 0.01-0.2 4 $55.00 10 Day Air Each

n-Hexane 110-54-3 NIOSH 1500


n-Hexane 110-54-3 NIOSH 1500 Mod


or 002


Nicotine 54-11-5 NIOSH 2551 GC-NPD SKC 226-93 0.1 - 1.0 0.5 -6 00 $70.00 10 Day Air Each

Nitrobenzene 98-95-3 NIOSH 2005


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MediaSampling

RateSuggested


Nitromethane 75-52-5 NIOSH 2527 Mod

GC-NPD SKC 226-111A 0.01 - 0.05 1.2 - 3 $70.00 10 Day Air Each

NMP (n-Methy-2-Pyrrolidone)

872-50-4 NIOSH 1302


n-Octane 111-65-9 NIOSH 1500


n-Octane 111-65-9 NIOSH 1500 Mod


or 002


n-Pentane 109-66-0 NIOSH 1500


n-Pentane 109-66-0 NIOSH 1500 Mod



n-Propyl Acetate 109-60-4 NIOSH 1450


n-Propyl Acetate 109-60-4 NIOSH 1500 Mod


or 002


n-Propyl Alcohol 71-23-8 NIOSH 1401 GC-FID SKC 226-01 0.01 - 0.2 1 - 10 $55.00 10 Day Air Each

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MediaSampling

RateSuggested


n-Propyl Alcohol 71-23-8 NIOSH 1500 Mod


or 002


n-Vinyl 2-Pyrrolidone 88-12-0 NIOSH 1302


Oil Mist (Metalworking Fluids (MWF) All Categories)

8012-95-1 NIOSH 5026

FTIR MCE, PCV or GFF

Send reference material in separate

shipment. Oil must be solvent

soluble.

1 - 3 20 - 500 $90.00 10 Day Air Each

ortho-Dichlorobenzene (1,2-Dichlorobenzene)

95-50-1 NIOSH 1003



95-50-1 NIOSH 1500 Mod


or 002



95-50-1 NIOSH 1501 GC-FID SKC 226-01 0.2 2 - 30 $55.00 10 Day Air Each

para-Dichlorobenzene (1,4-Dichlorobenzene)

106-46-7 NIOSH 1501 GC-FID SKC 226-01 0.2 2 - 30 $55.00 10 Day Air Each

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MediaSampling

RateSuggested



106-46-7 NIOSH 1500 Mod


or 002



106-46-7 NIOSH 1003


Paraffin Wax Fume 8002-74-2 OSHA CSI GC-FID GFF 1 200 - 600 $70.00 10 Day Air Each

Perchloroethylene (Tetrachloroethylene)

127-18-4 NIOSH 1003






127-18-4 NIOSH 1500 Mod


or 002


Petroleum Distillate NIOSH 1550


Petroleum Ether (VM&P Naphtha, Ligroin)

8032-32-4 NIOSH 1550


Petroleum Naphtha 8002-05-09 NIOSH 1550


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MediaSampling

RateSuggested


Phenanthrene 85-01-8 NIOSH 5506

HPLC-UV/FL PTFE & SKC 226-30-04

2 200 - 1000 $100.00 10 Day Air Each

Phenol 108-95-2 OSHA 32 HPLC 226-95 0.1 24 $100.00 10 Day Air Each

Phenyl Ether 101-84-8 NIOSH 1617 GC-FID SKC 226-01 0.01 - 0.2 1 - 50 $55.00 10 Day Air Each

Phenyl Ether 101-84-8 NIOSH 1500 Mod



Phenylethylene (Styrene)

100-42-5 NIOSH 1500 Mod



Phenylethylene (Styrene)


Propylene Glycol 57-55-6 NIOSH 5523


0.5 - 2.0 5 - 60 $70.00 10 Day Air Each

Propylene Glycol Methyl Ether (PGME) (Propylene Glycol Monomethyl Ethers/Acetates)

107-98-2,1589-47-5

OSHA 99 GC-FID SKC 226-01 0.1 5 - 10 $55.00 10 Day Air Each

Propylene Oxide 75-56-9 NIOSH 1612 GC-FID SKC 226-01 0.01 - 0.2 0.5 - 5 $100.00 10 Day Air Each

Propylene Oxide 75-56-9 OSHA 88 GC-FID SKC 226-81A 0.1 5 $100.00 10 Day Air Each

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MediaSampling

RateSuggested


Propylene Oxide 75-56-9 NIOSH 1500 Mod


or 002


Pseudocumene (1, 2, 4 - Trimethylbenzene)

95-63-6 NIOSH 1501 GC-FID SKC 226-01 0.01 - 0.2 30 $55.00 10 Day Air Each

p-tert-Butyl Toluene 98-51-1 NIOSH 1501 GC-FID SKC 226-01 0.01 - 0.2 1 - 29 $55.00 10 Day Air Each

Pyrene 129-00-0 NIOSH 5506


2 200 - 1000 $100.00 10 Day Air Each

Pyridine 110-86-1 NIOSH 1613 GC-FID SKC 226-01 0.01 - 1.0 18 - 150 $55.00 10 Day Air Each

Refrigerant 113 (1,1,2-Trichloro-2,2,1-trifluoroethane)

76-13-1 NIOSH 1020


Rubber Solvent 8030-30-6 NIOSH 1550


sec-Amyl Acetate 626-38-0 NIOSH 1450

GC-FID SKC 226-01 or POVM SKC

575-001

0.01 - 0.20 1 - 10 $55.00 10 Day Air Each

sec-Amyl Acetate 626-38-0 NIOSH 1500 Mod



sec-Butyl Acetate 105-46-4 NIOSH 1450


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MediaSampling

RateSuggested


sec-Butyl Acetate 105-46-4 NIOSH 1500 Mod


or 002


sec-Butyl Alcohol (2-Butanol)


sec-Butyl Alcohol (2-Butanol)

78-92-2 NIOSH 1401 GC-FID POVM 3M 3500 POVM SKC 575-001

or 002


Silica, Quartz (Respirable Coal Mine Dust)

NIOSH 7603 (P7)

FTIR/Grav. PVC-MSHA 2 480 - 960 $106.00 10 Day Air Each

Stoddard Solvent (Mineral Spirits)

8052-41-3 NIOSH 1550


Styrene 100-42-5 NIOSH 1501 GC-FID SKC 226-01 0.01- 1 1 - 14 $55.00 10 Day Air Each

Styrene 100-42-5 NIOSH 1501 mod.

GC-FID POVM 3M 3500, SKC

575-002 or575-006


t-Butyl Glycidyl Ether 7665-72-7 OSHA CSI GC-FID SKC 226-01 0.2 10 $55.00 10 Day Air Each

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MediaSampling

RateSuggested


TDI as mixture (2,4-Toluene Diisocyanate and/or 2,6-Toluene Diisocyanate)

584-84-9, 91-08-7

OSHA 42 HPLC-UV SKC 225-9002

1 15 $100.00 10 Day Air Each

tert-Butyl Acetate 540-88-5 NIOSH 1450


tert-Butyl Acetate 540-88-5 NIOSH 1500 Mod


or 002


tert-Butyl Alcohol (2-methyl-2-propanol)

75-65-0 NIOSH 1400


tert-Butyl Alcohol (2-methyl-2-propanol)

75-65-0 NIOSH 1400 mod.



Tetrahydrofuran 109-99-9 NIOSH 1609


Tetrahydrofuran 109-99-9 NIOSH 1500 Mod



Toluene 108-88-3 OSHA 111 GC-FID POVM SKC 575-002

12L/240 min $55.00 10 Day Air Each

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MediaSampling

RateSuggested


Toluene 108-88-3 OSHA 1005 GC-FID POVM 3M 3500 POVM SKC 575-001

or 002


Toluene 108-88-3 NIOSH 1501 GC-FID SKC 226-01 0.01 - 0.2 1 - 8 $55.00 10 Day Air Each

Total Hydrocarbons NIOSH 1500 mod.


Tri(ethylene) Glycol 112-27-6 NIOSH 5523


0.5 - 1.0 5 - 60 $70.00 10 Day Air Each

Trichloroethylene 79-01-6 NIOSH 1022


Trichloroethylene 79-01-6 NIOSH 1500 Mod


or 002


Turpentine 8006-64-2 NIOSH 1550


Vinyl Acetate 108-05-4 OSHA 51 mod.


24 $70.00 10 Day Air Each

Vinyl Bromide (Bromoethene)

593-60-2 NIOSH 1009


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Sampling Rate

Suggested Volume


Vinyl Bromide (Bromoethene)


Vinyl Chloride (Chloroethylene)


Vinyl Chloride (Chloroethylene)

75-01-4 NIOSH 1007

GC-FID (2) SKC 226-01

Ship sample refrigerated

overnight delivery

0.05 0.7 - 5.0 $70.00 10 Day Air Each

Xylene, Total (all isomers)



1330-20-7 NIOSH 1501 mod.


0.05 12L/240 min $70.00 10 Day Air Each


1330-20-7 NIOSH 1500 Mod


or 002


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Industrial Hygiene ProfilesIndustrial Hygiene ProfilesTest Analyte Method Technique Sampling

MediaSampling

RateSuggested


Aldehyde Profile

Acetaldehyde, Acrolein, Butyraldehyde, Crotonaldehyde, Formaldehyde, Furfural, Glutaraldehyde, Heptanal, Hexanal, Isobutyaldehyde, Isovaleraldehyde, Propionaldehyde

NIOSH 2016 Mod. / TO-11A HPLC

SKC 226-119 .1-1.5 15 $400.00 10 Day Air Group

BTEX ProfileBenzene, Ethyl Benzene, Toluene and Xylene, Total Hydrocarbon (VOC as Hexane)

NIOSH 1501 GC-FID

SKC 226-01 or 3M 3500

POVM or SKC 575-

001 or 002

0.1 - 0.5 10 $150.00 10 Day Air Group

Diisocyanate Profile HDI, MDI, 2,4-TDI, 2,6,-TDI OSHA 42 & 47 HPLC-UV/FL Trtd. GFF 0.2 - 1.0 15 - 30 $250.00 10 Day Air Group

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Industrial Hygiene ProfilesIndustrial Hygiene ProfilesTest Analyte Method Technique Sampling

MediaSampling

RateSuggested


Inorganic Acid Profile

Hydrobromic Acid, Hydrochloric Acid, Hydofluoric Acid, Nitric Acid, Phosphoric Acid, Sulfuric Acid

NIOSH 7903 IC SKC 226-10-03

0.2 - 0.4 100 $225.00 5 Day Air Group

MSHA Welding Fume Profile (14 metals)

Arsenic, Beryllium, Cadmium, Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Molybdenum, Nickel, Vanadium, Zinc

NIOSH 7300 / OSHA ID 125

ICP-AES/ICP-MS

MCE or PVC 1.0 - 2.0 200 - 1000 $230.00 5 Day Air Group

OSHA 58 Benzene Soluble Fraction by HPLC (5 PAH’s Profile)

Anthracene, Benzo(a)pyrene, Chrysene, Phenanathrene, Pyrene

NIOSH 5506 HPLC-UV/FL

PTFE Benzene, Soluble Fraction

2 200 - 960 $250.00 10 Day Air Group

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Industrial Hygiene ProfilesIndustrial Hygiene Profiles

Test Analyte Method TechniqueSampling

MediaSampling

RateSuggested

Volume Price TAT Matrix Unit

Polynuclear Aromatic Hydrocarbons Profile (PAH’s also known as PNA’s)

Acenaphthene, Acenapththylene, Anthracene, Benz(a)anthracene, Benzo(b)fluoranthene, Benzo(k)fluoranthene, Benzo(ghi)perylene, Benzo(a)pyrene, Benzo(e)pyrene, Chrysene, Dibenz(a,h)anthracene, Fluoranthene, Fluorene, Indeno(1,2,3-cd)pyrene, Naphthalene, Phenanthrene, Pyrene

NIOSH 5506 HPLC-UV/FL

PTFE + SKC 226-30-04 Transfer filters to glass vials after sam-pling; wrap to protect from light. Ship sample re-frigerated overnight delivery.

2.0 200 - 1000 $400.00 10 Day Air Group

Welding Fume Profile (15 metals)

Aluminum, Antimony, Beryllium, Cadmium, Chromium, Cobalt, Copper, Iron, Lead, Manganese, Molybdenum, Nickel, Titanium, Vanadium, Zinc


ICP-AES/ICP-MS


Welding Fume Profile+As (16 metals)

Arsenic, Aluminum, Antimony, Beryllium, Cadmium, Chromium, Cobalt, Copper, Iron, Lead, Manganese, Molybdenum, Nickel, Titanium, Vanadium, Zinc


ICP-AES/ICP-MS


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Environmental & Wet ChemistryEnvironmental & Wet ChemistryInorganicsNon-potable & Drinking Water

Test Analyte Method Technique Price TAT Matrix Unit

Drinking Water - Asbestos Asbestos EPA 100.2 TEM $190.00 5 Day Water Each

Drinking Water - Determination of Inorganic Anions

Chloride, Fluoride, Nitrate, Nitrite, Orthophosphate, Sulfate

EPA 300.0 IC $55.00 5 Day Water Each

Drinking Water - Determination of Inorganic Anions

Chloride, Fluoride, Nitrate, Orthophosphate, Sulfate

EPA 300.0 IC $225.00 5 Day Water Group

Drinking Water - Determination of Trace Elements and Metals

Al, Ba, B, Ca, Cr, Cu, Fe, Mg, Mn, Mo, Ni, K, Ag, Na, V, Zn

EPA 200.7 ICP-AES $22.00 5 Day Water Each

Drinking Water - Determination of Trace Elements and Metals

Al, Sb, As, Ba, Be, B, Cd, Cr,Cu, Pb, Mn, Hg, Mo, Ni, Se Ag, Tl, V, Zn

EPA 200.8 ICP-MS $22.00 5 Day Water Each

Drinking Water - Lead (Pb) and Copper (Cu)

Lead (Pb) and Copper (Cu) EPA 200.8/EPA 200.7 ICP-MS/ICP-AES

$50.00 5 Day Water Each

Drinking Water - Mercury Hg EPA 245.1 CVAA $55.00 5 Day Water Each

Non-potable Water - Asbestos Asbestos EPA 100.1 TEM $230.00 5 Day Water Each

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Environmental & Wet ChemistryEnvironmental & Wet ChemistryInorganicsNon-potable & Drinking Water (cont.)


Non-potable water - Chromium (VI)

Chromium, Hexavalent (CrVI) EPA 3060A/EPA 7199 IC $65.00 5 Day Water Each

Non-potable water - Determination of Inorganic Anions

Bromide, Chloride, Fluoride, Nitrate, Orthophosphate, Sulfate

EPA 300.0/EPA 9056A

IC $225.00 5 Day Water Group

Non-potable water - Determination of Inorganic Anions

Bromide, Chloride, Fluoride, Nitrate, Nitrite, Orthophosphate, Sulfate

EPA 300.0/EPA 9056A

IC $55.00 5 Day Water Each

Non-potable water - Determination of Trace Elements and Metals

Al, Sb, As, Ba, Be, B, Cd, Ca, Cr, Co, Cu, Fe, Pb, Li, Mg, Mn, Mo, Ni, K, Se, Ag, Na, Sr, Tl, Sn, Ti, V, Zn

EPA 200.7/EPA 6010C ICP-AES $22.00 5 Day Water Each

Non-potable water - Determination of Trace Elements and Metals

Al, Sb, As, Ba, Be, B, Cd, Cr, Co, Cu, Fe, Pb, Li, Mn, Hg, Mo, Ni, Se, Ag, Sr, Tl, Sn, Ti, V, Zn

EPA 200.8/EPA 6020 ICP-MS $22.00 5 Day Water Each

Non-potable water - Mercury Hg EPA 245.1 / 7470A CVAA $55.00 5 Day Water Each

Non-potable water or Drinking Water - Conductivity

Conductivity SM 2510B Conductivity Meter

$25.00 5 Day Water Each

Non-potable water or Drinking Water - Hardness (calc.)

Hardness (calc) (Ca, Mg by ICP-AES)

EPA 200.7/SM2340B 6010C

ICP-AES $22.00 5 Day Water Each

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Environmental & Wet ChemistryEnvironmental & Wet ChemistryInorganics


Non-Potable Water or Drinking Water - Lead (Pb)

Lead (Pb) EPA 6020/200.8 ICP-MS $35.00 5 Day Water Each

Non-potable water or Drinking Water - pH (Corrosivity)

pH SM 4500-H+B Electrode $25.00 5 Day Water Each

Non-potable water or Drinking Water - Residue, Filterable (TDS)

Residue, Filterable (TDS) SM 2540C Gravimetric $50.00 5 Day Water Each

Non-potable water or Drinking Water - Residue, Non-Filterable (TSS)

Residue, Non-Filterable (TSS) SM 2540D Gravimetric $50.00 5 Day Water Each

Non-potable water or Drinking Water - Residue, Total (TS)

Residue, Total (TS) SM 2540B Gravimetric $50.00 5 Day Water Each

Non-potable water or Drinking Water- Turbidity

Turbidity SM 2130B Turbidimeter $25.00 5 Day Water Each

Non-potable & Drinking Water (cont.)

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Solids & Hazardous Waste - Bulk Asbestos Analysis

Asbestos EPA 600/R-93/116 PLM $15.75 5 Day Solid/Bulk

(building

Layer

Solids & Hazardous Waste - Bulk Asbestos Analysis

Asbestos EPA 600/R-93/116 PLM $52.50 10 Day Solid/Bulk (Soil/Rock/Raw

Each

Solids & Hazardous Waste - Chemical/ElementalComposition, Quantitative (w/construction of calibrationcurve)

Quantification of calibrated elements In-house XRF call for pricing

10 Day (after construction of

curve)

Solid/Bulk

Each

Solids & Hazardous Waste - Chemical/ElementalComposition, Semi-Quant

Scan-Quantification of major elements Semi-Quant XRF $165.00 10 Day Solid/Bulk

Each

Solids & Hazardous Waste - Chromium (VI)

Chromium, Hexavalent (CrVI) EPA 3060/EPA 7199 IC $70.00 5 Day Solid/Bulk

Each

Solids & Hazardous Waste - Determination of Inorganic Anions


EPA 9056A IC $225.00 5 Day Solid/Bulk

Group


Solid & Hazardous Waste

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Solids & Hazardous Waste - Determination of Inorganic Anions


EPA 9056A IC $55.00 5 Day Solid/Bulk

Each

Solids & Hazardous Waste - Mercury

Hg EPA 7471A CVAA $55.00 5 Day Solid/Bulk

Each

Solids & Hazardous Waste - pH pH EPA 9045D Electrode $25.00 5 Day Solid/Bulk

Each

Solids & Hazardous Waste - Qualitative Phase ID

Scan - Phase ID of Major Crystalline Materials

Search & Match (using ICDD PDF 4+

Database)

XRD $225-$300

10 Day Solid/Bulk

Each

Solids & Hazardous Waste - Qualitative Phase ID and Silica, Total Crystalline (Quartz, Cristobalite, Tridymite)

Scan - Phase ID of Major Crystalline Materials and Silica, Total Crystalline (Quartz, Cristobalite, Tridymite)

NIOSH 7500 mod. Search & Match

(using ICDD PDF 4+ Database)

XRD $300-$500

10 Day Solid/Bulk

Each

Solids & Hazardous Waste - Quantitative Phase ID

Scan - Phase ID and Quantification o of Major Crystalline Materials. Total Amorphous quantification is also possible

By Rietveld Method, limitations apply,

additional analyses might be needed,

please call for more information

XRD $400-$725

10 to 20 days Solid/Bulk

Each

Solids & Hazardous Waste - Silica, Amorphous and Total Crystalline

Silica, Amorphous and Total Crystalline (Quartz, Cristobalite, Tridymite)

NIOSH 7501 & NIOSH 7500 mod.

XRD $500-$635

10 Day Solid/Bulk

Each


Solid & Hazardous Waste (cont.)

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Solids & Hazardous Waste - Silica, Amorphous Only

Silica, Amorphous Only NIOSH 7501 mod. XRD $450-$585

10 Day Solid/Bulk

Each

Solids & Hazardous Waste - Silica, Total Crystalline &Respirable (CCSEM)

Silica, Total Crystalline (Quartz, Cristobalite, Tridymite) & Respirable (Si Rich by CCSEM < 10 um)

NIOSH 7500 mod and Size Separation

XRD/ CCSEM $500-$705

10 Day Solid/Bulk

Each

Solids & Hazardous Waste - Silica, Total Crystalline &Respirable (Stokes)

Silica, Total Crystalline (Quartz, Cristobalite, Tridymite) & Respirable (Stokes Settling < 10 um)


XRD/Stokes Settling

$560-$705

10 Day Solid/Bulk

Each

Solids & Hazardous Waste - Silica, Total Crystalline (Quartz, Cristobalite, Tridymite)

Silica, Total Crystalline (Quartz, Cristobalite, Tridymite)

NIOSH 7500 mod. XRD $225-$405

10 Day Solid/Bulk

Each

Solids & Hazardous Waste - Trace Elements

Al, Sb, As, Ba, Be, B, Cd, Ca, Cr, Co, Cu, Fe, Pb, Li, Mg, Mn, Mo, Ni, P, K, Se, Ag, Na, Sr, Tl, Sn, Ti, V, Zn

EPA 6010C ICP-AES $22.00 5 Day Solid/Bulk

Each

Solids & Hazardous Waste - Trace Elements

As, Cd, Hg, Pb EPA 6020 ICP-MS $22.00 5 Day Solid/Bulk

Each

Dinnerware Extraction from Glazed Ceramic Surfaces

Pb, Cd ASTM C738 ICP-MS call for pricing

10 Day Solid/Bulk

Group

Dinnerware Extraction from the Lip and Rim Area of Glass Tumblers

Pb, Cd ASTM C927 ICP-MS call for pricing

10 Day Solid/Bulk

Group


Solid & Hazardous Waste (cont.)

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OrganicsEnvironmental & Wet ChemistryEnvironmental & Wet Chemistry

Test Method Technique Price Unit

Volatile Aromatics EPA 524.3 GC-MS $185.00 Group

Volatile Halocarbons EPA 524.3 GC-MS $125.00 Group

Fuel Oxygenates EPA 8260C GC-MS $125.00 Group

Polychlorinated Biphenyls EPA 608 / 8082 GC $90.00 Group

Polynuclear Aromatics EPA 625 / 8270D GC-MS $250.00 Group

Purgeable Aromatics EPA 625 / 8260B / 8270D GC-MS $150.00 Group

Purgeable Halocarbons EPA 624 / 8260C GC-MS $125.00 Group

Purgeable Organics EPA 8260C GC-MS $125.00 Group

Volatile Chlorinated Organics EPA 8260C GC-MS $125.00 Group

Non-potable & Drinking Water

Solid and Hazardous Waste


Acrylates EPA 8260B GC-MS $125.00 Group

Chlorinated Hydrocarbons EPA 8260B / 8270C GC-MS $190.00 Group

Haloethers EPA 8270C GC-MS $225.00 Group

Polychlorinated Biphenyls EPA 8082 GC $90.00 Group

Polynuclear Aromatics EPA 8260B GC-MS $125.00 Group

Purgeable Halocarbons EPA 8260B GC-MS $125.00 Group

Purgeable Organics EPA 8260B GC-MS $125.00 Group

Volatile Chlorinated Organics EPA 8260B GC-MS $125.00 Group

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Environmental & Wet ChemistryEnvironmental & Wet ChemistryOrganicsAir and Emissions


Acrylates EPA TO-17 / TO-15 GC-MS $300.00 Group

Air Analysis TO-11 HPLC-DAD $185.00 Group

Amines Internal Method LC/MS/MS $350.00

Chlorinated Hydrocarbons EPA TO-14A / TO-15 GC / GC-MS $300.00 Group

Polychlorinated Biphenyls EPA TO-10A GC-MS $150.00 Group

Polynuclear Aromatics EPA TO-13 GC-MS $250.00 Group

Purgeable Aromatics EPA TO-14A / TO-13 GC / GC-MS $250.00 Group

Purgeable Halocarbons EPA TO-14A / TO-15 / TO-17 GC / GC-MS $300.00 Group

Volatile Chlorinated Organics EPA TO-14A / TO-15 GC / GC-MS $300.00 Group

Volatile Organics EPA TO-14A / TO-15 / TO-17 GC / GC-MS $300.00 Group

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Environmental & Wet ChemistryEnvironmental & Wet ChemistrySample PreparationTest Method Technique Price Unit

Acid digestion of solids EPA 3050B Digestion $20.00 Each

Dissolved metals EPA3005A Digestion $20.00 Each

Hot plate acid digestion (HNO3 + HCI) EPA 3010A Digestion $20.00 Each

Microwave digestion - solids (HNO3 + HF) EPA 3052 Digestion $70.00 Each

Microwave digestion - solids (HNO3 only) EPA 3051 Digestion $70.00 Each

Microwave-assisted acid digestion EPA 3015 Digestion $70.00 Each

Organic Continuous Liquid-Liquid Extraction EPA 3520C $50.00 Each

Separatory Funnel Liquid-Liquid Extraction EPA 3510C $50.00 Each

Solids & Hazardous Waste - synthetic precipitation leaching procedure (SPLP)- Inorganic

EPA 1312 Extraction $50.00 Each

Solids & Hazardous Waste - Toxicity characteristic leaching procedure (TCLP) -Inorganic

EPA 1311 Extraction $50.00 Each

Solids & Hazardous Waste - Waste Extraction Test (WET) STLC

CCR Chapter 11, Article 5, Appendix II

Extraction $100.00 Each

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Powdered Metal AnalysisPowdered Metal Analysis

Analysis Technique

Contaminant Identification of Ceramics, Non-metallics, and Metallic Aluminum Heavy Liquid Separation

Particle Size Distribution and Shape Analysis CCSEM w/optional EDS

Powder Cross-contamination Detection CCSEM/EDS

Manual SEM/EDS Analysis SEM/EDS

In Powder Metals (PM) applications such as 3D printing, the flow and packing behavior of PM is influenced by particle size and shape distributions. These properties can be measured in statistically meaningful ways using computer controlled scanning electron microscopy (CCSEM). Compositional information can also be performed with the particle-by-particle analysis using EDS. This will allow investigation of changes in powder metal composition, or the presence of extraneous particulate. The experts at RJ Lee Group can work with your team to answer questions and find solutions for your powder metal manufacturing facility.

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RJ Lee Group’s combination of evaluation, sampling, and assessments provides the geologic consulting expertise you need to support your industrial minerals operation.

Mining & Mineral ServicesMining & Mineral Services

» Geotechnical Analyses

» Field Support Services

» MSHA Safety & Compliance Testing

Understanding sub-surface geology mitigates risk and safety concerns when experts utilize proper sampling

techniques for minerals, such as naturally occurring asbestos, crystalline silica, and heavy metals. Our roots

in environmental and particulate studies provide the experience and support needed to safely assess active

operations and greenfield sites.

» Mineral Assessments

» Due Diligence

» Petrography

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Mineral Identification & CharacterizationMineral Identification & Characterization

Test Analyte Method Price Matrix UnitQualitative Phase ID Scan - Phase ID of Major Crystalline Materials Search & Match (using

ICDD PDF 4+ Database)$225-$300 Solid/Bulk Each

Quantitative Phase ID Scan - Phase ID and Quantification o of Major Crystalline Materials. Total Amorphous quantification is also possible

By Rietveld Method, limitations apply, additional analyses might be needed,

please call for more information

$400-$725 Solid/Bulk Each



NIOSH 7500 mod. $225-$405 Solid/Bulk Each

Qualitative Phase ID and Silica, Total Crystalline (Quartz, Cristobalite, Tridymite)

Scan - Phase ID of Major Crystalline Materials and Silica, Total Crystalline (Quartz, Cristobalite, Tridymite)

NIOSH 7500 mod. Search & Match (using ICDD PDF 4+

Database)


Silica, Amorphous Only Silica, Amorphous Only NIOSH 7501 mod. $450-$585 Solid/Bulk Each

Silica, Amorphous and Total Crystalline

Silica, Amorphous and Total Crystalline (Quartz, Cristobalite, Tridymite)

NIOSH 7501 & NIOSH 7500 mod.


Silica, Total Crystalline & Respirable (Stokes)

Silica, Total Crystalline (Quartz, Cristobalite, Tridymite) & Respirable (Stokes Settling < 10 um)



XRF - 10 Day TAT

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XRF - 10 Day TAT

Microscopy - 5-10 Day TAT

Test Analyte Method Price Matrix UnitSilica, Total Crystalline & Respirable (CCSEM)

Silica, Total Crystalline (Quartz, Cristobalite, Tridymite) & Respirable (Si Rich by CCSEM < 10 um)



Qualitative Clay Phase ID (Expansive/Full)

Scan - Phase ID of Major Crystalline Materials plus Phase ID of Clays i.e. Bentonite

USGS Mineral ID $345-$550 Each

XRF - 10 Day TAT (cont.)

Test Analyte Method Technique Price Matrix UnitChemical/Elemental Composition, Semi-Quant Scan-Quantification of major

elementsSemi-Quant XRF $165.00 Solid/Bulk Each

Chemical/Elemental Composition, Quantitative (w/construction of calibration curve)

Quantification of calibrated elements

In-house XRF call for pricing Solid/Bulk Each

10 Day TAT after construction of curve

Method Price Matrix Unit PLM $150.00 Solid/Bulk Each

SEM call for pricing Solid/Bulk Hour

Other ServicesTest Method Technique Price Matrix Unit

Total Incombustible Content (Rock Dust) - Bulk MH 102 $50.00 Solid/Bulk Each

MSHA Welding Fume Profile-14 analytes (As, Be, Cd, Cr, Co, Cu, Fe, Pb, Mg, Mn, Mo, Ni, V, Zn)

OSHA ID 125 / NIOSH 7300 ICP-AES $210.00 Air Group

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Asbestos Analytical ServicesAsbestos Analytical ServicesTEM - 5 Day TAT unless otherwise indicated

Type of Analysis/Service Price Per Sample Turnaround

AHERA Clearance Samples - Air (Submitted in sets of five) $80.00 5 working days

NIOSH 7402 Methodology – Air $112.00 5 working days

NIOSH 7402 – Air w/RCF Fibers $168.00 5 working days

ISO 10312 (direct) - Air $270.00 10 working days

ISO 13794 (indirect) - Air $330.00 10 working days

ISO 22262-2 – Bulk $577.00 10 working days

ASTM D5756 – Bulk $577.00 10 working days

ASTM – Dust 5755 - Microvac $160.00 5 working days

ASTM D6480 – Surface dust wipe $160.00 5 working days

USEPA 100.1 - Non-potable water $230.00 5 working days

USEPA 100.2 - Drinking Water $190.00 5 working days

Chatfield SOP-1988-02/NY ELAP 198.4 (NOB) - Bulk $75.00 5 working days

Sludge or Mud sample: (weight percent) $510.00 10 working days

USAEPA Draft Contract 68-02-3266 (Yamate) - Level I $85.00 5 working days

USAEPA Draft Contract 68-02-3266 (Yamate) - Level II $158.00 5 working days

USAEPA Draft Contract 68-02-3266 (Yamate) - Level III Call for Quote

Gravimetric Reduction Prep is recommended for problem matrix materials such as NOB’s (Non-Friable Organically Bound Materials).

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Asbestos Analytical ServicesAsbestos Analytical Services

Phase Contrast Microscopy (PCM)

NIOSH 7400 Methodology – Air (Sampling media available upon request Media for additional fee.)

$15.00 5 working days

Polarized Light Microscopy (PLM)

EPA 600/R-93/116 or NYELAP 198.1 -

Bulk (visual estimate - per layer) $20.00 per layer 5 working days

Untreated 400 Point Count $46.75 10 working days

Treated 400 Point Count $76.00 10 working days

Untreated 1000 Point Count $130.95 10 working days

Treated 1000 Point Count $160.50 10 working days

Soil/Rock/Raw Materials/Debris $53.50 10 working days

CARB 435 – serpentine aggregate $147.50 10 working days

ISO 22262-1 $53.50 10 working days

ISO 22262-2 Call for quote

Fly ash determination in sediment $127.00 10 working days

Component Characterization / Mineral ID Call for Quote

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Construction Materials Laboratory ServicesConstruction Materials Laboratory ServicesRJ Lee Group routinely conducts testing and evaluation of construction materials including concrete, stucco and aggregate using petrography, chemical analyses and physical tests according to the standard methods listed below. We have significant experience in conducting small and large-scale analytical programs to assess defects and premature product failures. Please contact a representative to discuss your needs and to obtain a cost estimate.

Concrete Testing Method

Acid Soluble Chloride in Mortar and Concrete ASTM C1152 // AASHTO T260

Cement Composition Internal Method

Chemical Analysis of Cements ASTM C114 // AASHTO T105

Cement Content ASTM C1084

Concrete Coating Analyses Organic Chemistry and Microscopy

Concrete Contaminant Identification & Analysis Organic Chemistry and Microscopy

Concrete Petrography ASTM C856

Density, Absorption, and Voids in Hardened Concrete ASTM C642

Freeze/Thaw Durability ASTM C666

Mix Design Confirmation Internal Method

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Construction Materials Laboratory ServicesConstruction Materials Laboratory Services

Standard turnaround times vary.

Aggregate Testing Method

Aggregate Sieve Analysis ASTM C136, ASTM C117

Crystalline Mineral Identification and Quantification X-ray Diffraction (XRD)

Iron Staining in Light Weight Concrete Aggregates ASTM C641

Petrographic Examination of Aggregates for Concrete ASTM C295

Slag Characterization for use as Aggregate Fill or Road Base Multiple Techniques

Sulfur Content and Speciation Multiple Techniques

Concrete Testing Method

Hardened Masonry Mortar Characterization ASTM C1324

Non-destructive Concrete Testing Services Multiple Techniques

Air Void Parameters in Hardened Concrete ASTM C457

Phase Identification & Quantification using Thermal Methods

TGA and DSC

Rapid Chloride Permeability Test (RCPT) ASTM C1202

Scanning Electron Microscopy of Hardened Concrete ASTM C1723

Water Soluble Chloride in Mortar and Concrete ASTM C1218

Water-Cement Ratio Estimation ASTM C856

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Materials & Particulate CharacterizationMaterials & Particulate CharacterizationMaterials AnalysisOur analytical laboratory is supported by a team of subject matter experts whose experience spans the world of materials including: steel, ceramics, polymers, natural materials, composites, organics. Our facilities are equipped to evaluate material chemical composition, compositional distribution, and properties from the macro- to the micro- to the nano-scale. We evaluate component parts (large and small), thin films, welds, coatings, catalysts, fibers, pharmaceuticals, medical devices, construction equipment, concrete, and more. Field-deployable capabilities to perform analysis in situ are available, as well as contaminant, dimension, and composition analysis for additive manufacturing is also available.

Product Development and CommercializationWe help our clients transform their innovations into new products that can be manufactured reliably with the expected performance. We support their efforts in quality control measures and provide scientific insight to inform corrective actions. We perform accelerated life performance and remaining life assessment testing in simulated operational environments. We strive to work as partners with our clients in the development process or as a third party to demonstrate materials performance.

Particulate CharacterizationWhether foreign particulate assessments in pharmaceutical manufacturing, evaluation of nuisance dust claims or environmental health and safety issues, our experienced staff coupled with our suite of state-of-the-art electron microscopes are ideally suited to address even the most complex particulate issues. Our subject matter experts routinely assist our clients in recommending sampling proce-dures and protocols, determining particulate composition and ultimately the source of the particulate. We provide our clients with a scientific foundation to respond to regulatory concerns, institute appropriate health and safety measures, and establish mitigation procedures. Our experts are at the forefront of tech-nical efforts surrounding nano-particulate and are available to respond to inquiries regarding laboratory analysis of any type or field sampling strategies.

Learn more about our analytical capabilities & instrumentation on the next page »

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Materials & Particulate CharacterizationMaterials & Particulate Characterization

Optical Microscopy 110-200 hr

Features: » Stereo optical microscopy » Polarized light microscopy » Digital microscopy (portable)

Scanning Electron Microscopy with Energy Dispersive X-ray Spectroscopy (SEM/EDS) Call for Quote

Features: » Variable pressure and large-size chambers » Tungsten and field emission SEM » Secondary electron and backscattered electron imaging » Light element EDS detection » X-ray element mapping

Ultra High-Resolution In-Lens SEM/STEM Call for Quote

Features: » 60x - 2,000,000x » 0.2kV to 30kV accelerating voltage » Secondary and backscattered electron imaging » Dark field and bright field STEM imaging » Cold field emission source » 30mm2 SDD EDS detector

Particle sizing available upon request

Computer Controlled SEM (CCSEM) Call for quote

Inclusion Analysis / Steel Cleanliness Analysis

Particle Size Distribution (PSD) Analysis

Particle Size Distribution with Elemental Composition (PSD/EDS) Analysis

High Atomic Number (High-Z) Feature/Particle Analysis

Rates are based on a standard turn-around time and do not include interpretation or report preparation. Please call for a project-specific quotation.

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High Resolution Scanning Transmission Electron Microscopy (STEM) Call for quote

Features: » 100x - 10,000,000x » 120kV or 200kV accelerating voltage » SE, DF, and BF imaging » Electron diffraction » Field emission source » EDS detector

Particle sizing available upon request

Transmission Electron Microscopy Call for quote

Features: » 120kV or 200kV accelerating voltage » Electron diffraction » EDS detector

X-ray Photoelectron Spectroscopy (XPS) Call for quote

Survey Spectra (Qualitative and quantitative information)

Depth Profiling Analysis

High Resolution Spectra (Chemical state analysis)

Line Scans

Area Mapping

Raman Spectroscopy Call for quote

Features: » High spatial and spectral resolutions (800mm spectrometer) » 3 laser sources: 473nm (blue), 633nm (red), 785nm (near IR) » Wide mapping capabilities from 2 microns to 100mm x 80mm » High precision, ultra-fast confocal imaging


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Metallurgical Services Call for quote

Full-Service Metallography Lab (Etching, sample cross sectioning, drilling, cutting, mounting,

grinding, polishing, grain size analysis)

Heat Treatment

Hardness/Microhardness Testing

Corrosion Assessment and Testing

Metallurgical Modeling

Field Deployable Services: » Digital Microscopy (Portable) » Surface Replicas » Handheld XRF for Chemical Analysis » Field Metallography and Microstructural Evaluation

Non-Destructive Evaluations Call for quote

Dye Penetrant Testing

Magnetic Particle Inspection

Impact Echo

Radiography

Fourier Transform Infrared (FTIR) Spectroscopy 400 ea

Attenuated Total Reflectance (Ge crystal)

Grazing Angle

Reflectance

Raman AnalysisRates are based on a standard turn-around time and do not include interpretation or report preparation. Please call for a project-specific quotation.Additional preparation fees may apply.

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Gas Chromatography with Mass Spectrometric Detection (GC/MS) Call for quote

Elemental Analysis (AA, ICP/AES, ICP/MS, OES, Leco) Call for quote

Surface Area /BET Analysis (Gas adsorption - desorption) 100-350 ea

Particle Sizing by Laser Light Scattering 200 ea

Environmental Chamber Testing 50 day

TGA / DSC

Thermogravimetric Analysis (TGA) 150 ea

Differential Scanning Calorimetry (DSC) 250 ea

Simultaneous DSC/TGA 400 to 600 ea

Sample Preparation Services

Ultra-microtomy 150 hr

Electropolishing, Tripod Polishing, & Electrojet Polishing 150-175 hr

Carbon & Metal Coating 65 hr

Extraction Replicas 110-150 hr

Dimple Grinding 150 hr

Unique sample preparations developed per client or sample requirements Call for quote

The above prices are provided as reference only and refer to the cost of analyzing per sample per run under our standard conditions. Any changes to these conditions might result in additional changes. These might include method development and set up fees, hourly run times fees, and data processing fees. Please call for details and project-specific quotation.


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Additional Testing & Services Available Call for quote

Auger Electron Spectroscopy

Wavelength Dispersive X-ray Spectroscopy

Mechancial Testing

Focused Ion Beam Sample Preparation

HR-TEM

Ion Milling

Additive Manufacturing Quality Control Testing

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Granular Activated Carbon (GAC)Granular Activated Carbon (GAC)

Test Analyte Method

Grinding As required by method --

Moisture Moisture (oven) ASTM D2867 (TGA Leco)

Particle Size Test By Sieving Apparent Density ASTM D2854

Particle Size Distribution (PSD) ASTM D2862

Mean Particle Diameter, mm AWWA B-604/ASTM D2862

Effective Size AWWA B-604/ASTM D2862

Uniformity Coefficient AWWA B-604/ASTM D2862

Hardness Number Hardness Number ASTM D3802

Abrasion Number Abrasion Number AWWA B-604/ASTM D3802

Particle Size By Laser Diffraction Particle Size Distribution (PSD) In house (wet analysis)

Apparent Density Apparent Density ASTM D2854

BET Surface Analysis Specific Area In house

Volatile Matter Volatile Matter ASTM D3175 (TGA Leco)

Total Ash Total Ash ASTM D2866 (TGA Leco)

pH pH ASTM D3838

Contact pH pH ASTM D6851-02

RJ Lee Group’s accredited laboratory offers carbon analysis capabilities to help provide quality assurance across your product line. Our experts’ approach for activated carbon is to duplicate the analytical procedures our customers have instituted for their products using their exact methodologies, e.g., in-house methods, as well as traditional methodologies.

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Granular Activated Carbon (GAC)Granular Activated Carbon (GAC)Test Analyte Method

Water Solubles Water Solubles ASTM D5029-98

Halides and Sulfur Br, Cl, F and S Solid via Combustion & IC

Iodine Number Iodine Number AWWA B-604/ ASTM D4607/USP/FCC

Methylene Blue Number Methylene Blue Number JIS K 1474

Acid -soluble Ash Total Ash ASTM D-2866 (TGA Leco)

Acid -soluble Ash ASTM D6385

Acid-soluble Iron Acid-soluble Iron ASTM D6647 mod (ICP-AES)

Acid-soluble Ash and Iron Total Ash ASTM D2866 (TGA Leco)

Acid -soluble Ash ASTM D6385

Acid-soluble Iron ASTM D6647 mod (ICP-AES)

Board of Water Supply Metals/Anions/pH BWS 102.7

Prop 65 Sec 1.4 Column – As, Al, Sb Prop 65 Sec 1.4

GAC CA Prop 65 Section 1.5 Beaker – As, Al, Sb Prop 65 Sec 1.5

Block CA Prop 65 Section 1.6 Beaker Block – As, Al, Sb Prop 65 Section 1.6

Molasses Molasses number Client provide method/Molasses

Silver Extraction Ag content Call lab

RJLG is able to analyze powdered and pelletized activated carbon samples with the techniques listed above. Please call for more information and specific capabilities.

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Gypsum, Gypsum Products, Anhydride (CaSO4) Gypsum, Gypsum Products, Anhydride (CaSO4) and FGD Byproductsand FGD Byproducts

Elemental Analysis By borate fusion / XRF (majors) - ASTM E1621 By acid digestion / ICP-AES / ICP-MS (major, minors, trace including heavy metals)

XRD analysis for crystalline phase identification

XRD Rietveld Analysis for crystalline phase quantification (plus total amorphous component concentration if necessary)

Total and Respirable Crystalline SIlica by NIOSH 7500 mod (XRD)

Asbestos by PLM or TEM

Free-water, Combined water, Gypsum purity by ASTM C471

Silicon Dioxide and Other Acid Insoluble Matter by ASTM C471

Thermogravimetric analysis studies (TGA) / Loss on ignition (LOI) / Moisture

Soluble Salts by IC/ICP (Halogens, Alkali and Alkaline Earth Metals)

Water-Soluble Chloride by ASTM C1218/C114

Acid-Soluble Chloride by ASTM C1152/C114 or ASTM C471M

Elemental Sulfur (S8) by GC-ECD (ASTM C471M mod)

Sulfite (SO3) by Iodine titration (EPRI M2) or TGA

Total Sulfur (S) (multiple techniques including EPRI M4, ASTM D4239)

Calcium Carbonate (CCE-Calcium Carbonate Equivalent by ASTM C25)

Free lime (CaO) by ASTM C25

Gypsum USP and FCC monographs Identification Assay Impurities (Flouride by ISE, Lead and Selenium by ICPMS, Iron by ICP-AES) LOD - Loss on Dying

Whiteness

Particle Size Distribution (PSD) by laser diffraction or microscopy

Test

We have summarized product testing in the pages below. These tests are listed throughout previous sections in the guide. Product testing may not be routine, please call for a quote.

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Calcium Carbonate, Limestone, Dolomite & Calcium Carbonate, Limestone, Dolomite & Related ProductsRelated Products






Calcium Carbonate Equivalent by ASTM C25

Free lime by ASTM C25

Thermogravimetric analysis studies (TGA) / Loss on ignition (LOI)

Purity

Current USP and FCC monographs Identification Calcium Carbonate Assay Acid Insolubles Substances Mg/Alkali Salts Heavy metals and metal impurities by ICP-AES / ICP-MS (Lead, Arsenic, Mercury, Iron, Barium) Fluoride by ISE LOD - Loss on Dying

Water-Soluble Chloride by ASTM C1218/C114

Acid-Soluble Chloride by ASTM C1152/C114

Whiteness


Test

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Coal and Ash (CCR - Coal Combustion Coal and Ash (CCR - Coal Combustion Residuals)Residuals)

Elemental Analysis By borate fusion / XRF (majors) - ASTM D4326 By acid digestion / ICP-AES (major, minors, trace) - ASTM D6349 and D6357 Hg by CVAA - ASTM D6414

Moisture, Ash, Volatile Matter by ASTM D7582

Sulfur by ASTM D4239

Chlorine by ASTM D4208

Test

Bag House DustBag House DustS-Sulfur by special digestion/ICP analysis (EPA 6010C)

Total Hex Chromium by IC (EPA 3060/7199)

Al,Be,Cd,Cr,Co,Mn,Mo,Ni,Se,Ti,V,Zn,As,Pb by special digestion ICP-AES/MS analysis (EPA 6010C, EPA 6020)

Test

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TalcTalc





Current USP and foreign Pharmacopeia Monographs Identification (FTIR) Mg, Fe, Ca, Al content Water and Acid Soluble Substances Acidity / Alkalinity Absence of Asbestos (FTIR/XRD) Loss on Ignition (LOI) Heavy metals

Thermogravimetric analysis studies (TGA) / Loss on ignition (LOI)

Whiteness


Test

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Kaolin/KaoliniteKaolin/Kaolinite






Current USP Monographs Identification LOI - Loss on ignition Heavy metals and metal impurities by ICP-AES / ICP-MS Acid Soluble Substances Carbonate Thermogravimetric analysis studies (TGA) / Loss on ignition (LOI) Whiteness

Whiteness


Test

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Detrimental MaterialsDetrimental Materials

Shop Products Mercury by CVAA Antimony, Bismuth, Cadmium, Lead, Tin, Zinc by ICP Halides (Bromide, Chloride, Fluoride) by IC Sulfur by ICP Phosphorous by ICP

Solid nonmetallic materials Mercury by CVAA Halides (Bromide, Chloride, Fluoride) by IC Sulfur by ICP

Test

Glasses, bioactive glasses, (bioglass), Glasses, bioactive glasses, (bioglass), borosilicate glasses and ceramicsborosilicate glasses and ceramics

Elemental Analysis By borate fusion/XRF (majors) - ASTM E1621 By acid digestion /ICP-AES / ICP-MS (major, minors, trace including heavy metals) Microwave Cold HF B

Other minerals and compounds RJLG offer analytical services for other materials such as perlite, clays (including bentonite), quartz/sand, garnets, diatomaceous earth, alumina, rutile, calcium citrate, hydroxyapatite, sodium and magnesium chloride etc. Please call for additional information.

Test

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Pharmaceutical Analytical ServicesPharmaceutical Analytical ServicesTest Technique Price TAT Unit

USP 788 - Particulate Matter in Injections Light Obscuration (HIAC) $220.00 5 Day Each

Foreign Particulate Matter (FPM) - Full Particulate Characterization

FTIR, SEM/EDS, Raman, Optical Microscopy, PLM $1050.00 5 Day

Each

Foreign Particulate Matter - FTIR FTIR Analysis $550.00 5 Day Each

Foreign Particulate Matter - SEM/EDS SEM/EDS Analysis $550.00 5 Day Each

Foreign Particulate Matter - XRD XRD Analysis $550.00 10 Day Each

Foreign Particulate Matter - PLM PLM Analysis $300.00 5 Day Each

Foreign Particulate Matter - Optical Optical Imaging and Sizing $220.00 5 Day Each

Foreign Particulate Matter (FPM) - Full Particulate Characterization

FTIR, SEM/EDS, Optical Microscopy, PLM $1,550.00 2-3 Day

Each

Foreign Particulate Matter - FTIR FTIR Analysis $825.00 2-3 Day Each

Foreign Particulate Matter - SEM/EDS SEM/EDS Analysis $825.00 2-3 Day Each

Foreign Particulate Matter - PLM PLM Analysis $450.00 2-3 Day Each

Foreign Particulate Matter - Optical Optical Imaging and Sizing $275.00 2-3 Day Each

Automated Particulate Characterization - CCSEM CCSEM Analysis $1,200.00 5-10 Day Each

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Pharmaceutical Analytical ServicesPharmaceutical Analytical Services

Test Technique Price TAT Unit

Morphology and Content Uniformity Testing - FE-SEM FE-SEM Analysis $600.00 5-10 Day Each

Morphology and Content Uniformity Testing - High and Ultra High Resolution SEM/EDS HR SEM/EDS (Hitachi) $600.00

5-10 Day Hour

Morphology and Content Uniformity Testing - EDS Mapping

EDS Mapping $600.005-10 Day

Hour

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Criminal Forensics (Trace Evidence)Criminal Forensics (Trace Evidence)Gunshot Residue Analysis by SEM - 5 to 10 Day TAT Price Unit

GSR Kits 325175

Stub sampleControl stub sample

Particle Extraction 425 Stub sample

ISID (Instant shooter identification kit) 525 Swab sample

XCAT Samplers/Lift Samplers 425 Strip sample

Additional Forensic Analytical Services

Trace Evidence Analysis (Fiber, hair, tape & cordage) 300 hr

Distance Determination 500 hr

Consulting 300 hr

Court Testimony*3,000 (Plus expenses & Travel)

Trial

Video Conferencing / Depositions 275 Hour + expenses

Products

Gunshot Residue Collection Kit (For skin) ** 20 ea

Fabric/Surface Sampling Kit ** 20 ea

Sales Tax: PA-7%, CA-9.75%, WA-8.3%, NY-8.875%)Shipping will be invoiced unless a shipping account number is provided.Additional charges may apply for work days longer than 12 hours.Call for additional information.

*$2,000 added for each day over 2 days out of office.

** GSR Skin & Fabric/Surface Sampling Kit Price deducted from Trace Evidence Analysis Price when kit & analysis are purchased from RJ Lee Group.

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1. FORMATION OF CONTRACT. Any term of Customer’s order or of releases pertaining thereto or in any communications from Customer, which is in any way inconsistent with or in addition to the Terms and Conditions set forth hereof, is objected to by RJ Lee Group (RJLG). In the event that the Customer objects to any of these Terms and Conditions, such objection shall be in writing and must be received and accepted by an RJLG signatory pri-or to commencement of work. The receipt of a Customer’s order for any of the services provided by RJLG shall be conclusively deemed to be acceptance of all these Terms and Conditions. RJLG’s failure to object to terms contained in any communication from Cus-tomer shall not be deemed to be a waiver of these Terms and Conditions. Any references to purchase orders or to other oral or written requests for services are for purposes of description only, and any terms contained therein shall not become part of this agreement. If Customer issues multiple purchase orders, releases or other requests for services, all such orders, releases and requests shall be subject to these Terms and Conditions regard-less of the provisions of any such order, release or request, and regardless of the method of order including, but not limited to, orders issued by telephone or orders issued by company purchase order or release.

2. PRICES. Prices for standard tests and services shall be in conformance with the RJLG standard price lists in effect at the time the order is accepted. Price lists are subject to change without notice. Where a single order provides for or contemplates multiple ship-ment dates, the price shall be determined at the time each release is accepted. Any test or service not listed will be sold at a price determined by RJLG. All charges for courier or expedited services used at the request of the Customer shall be prepaid; otherwise, RJLG reserves the right to invoice for these services. A premium will be charged for samples that must be processed on an expedited or special basis. RJLG reserves the right to charge 50% of the priority price differential for expedited samples that are requested but are canceled or otherwise not received by RJLG, or whose priority status is lowered by the Customer. Additional analysis requested after results have been reported will incur the cost per test/analyte plus an additional reporting fee(s).

3. SAMPLE MEDIA/SUPPLIES AND SHIPPING. RJLG provides standard media supplies to existing customers at no cost provided samples are returned to RJLG for analysis. If sam-ples are not returned within 90 days of the original order date, the Customer is responsible for all sampling media and associated shipping costs. Costs for specialty media shall be paid for by the Customer and are described in RJLG’s price lists or written quote/proposal for services. Shipping services shall be paid by Customer for requests for sample media that require shipment in less than two working days, and for shipments that have special handling requirements, including hazardous material shipments and international ship-ments. Sample shipping costs shall be paid for by the Customer unless otherwise agreed upon in a written quotation or proposal for services. All costs associated with the return shipment of samples shall be paid by the Customer. All return shipping costs for Customer supplied shipping containers shall be paid by the Customer.

4. TAXES. Prices do not include any applicable sales, value-added or similar taxes or any duties. All such taxes or duties, whether now in existence (or hereafter enacted), that are applicable to any services performed by RJLG shall be Customer’s responsibility. Such taxes and duties shall be added by RJLG to the invoice amount, where appropriate.

5. PAYMENT TERMS. Unless specified to the contrary in writing approved by an officer of RJLG, payment terms shall be net thirty (30) days after the invoice date. After the invoice due date, the lesser of one and one-half percent (1.5%) of the unpaid balance (annual rate of 18%) or the maximum late payment penalty charge permitted by law shall be added for each month or part thereof that payment is delinquent. RJLG has the right, at any time, to change the amount of credit or terms of payment or to withdraw credit and to require partial or full payment in advance as a condition of performing services. Payments shall be made regardless of the results of the testing or other services performed by RJLG.

6. PROCESSING SCHEDULES. All samples and other requests for services submitted by Customer to RJLG shall be processed by RJLG in accordance with RJLG’s normal schedul-ing procedures and are not guaranteed for any specific time or date. If RJLG agrees in writ-ing, by a duly authorized representative of the Company, to process Customer’s order by a certain date or in accordance with a certain schedule, RJLG shall make reasonable efforts to comply with such dates or schedules.

7. FORCE MAJEURE. RJLG shall not be liable for any delay in performance, or for non-performance, in whole or in part caused by the occurrence of any contingency beyond the reasonable control of RJLG including but not limited to fires, floods, labor troubles, strikes, break- downs, regulation order or requirement of any government, war (whether an official declaration thereof is made or not), failure or delay in transportation, act of any govern-ment or any agency or subdivision thereof affecting the terms of the contract or otherwise, judicial action, accident, explosion, storm or other act of God. Any such delays shall excuse RJLG from performance, and RJLG’s time for performance shall be extended for the period of the delays and for a reasonable period thereafter.

8. SUBCONTRACTING. In the event of unforeseen circumstances, such as workload, need for further expertise, or for the reasons described above (force majeure), RJLG may re-quest to subcontract work. The Customer will be immediately advised of the request and work will not commence until consent is received from the Customer, preferably in writing.

9. OTHER PROVISIONS CONCERNING SAMPLES AND REPORTS. Packaging and Labelin - Customer shall mark, package and protect all samples sent to RJLG. Suitability for Analy-sis - It is the responsibility of the Customer to ensure that samples are correctly taken, la-beled, and packaged. Samples must be accompanied with a Chain-of-Custody form along with any potential hazardous warnings, including appropriate Safety Data Sheets (SDS). RJLG reserves the right to refuse samples for analysis which are obviously unsuitable due to damage, incorrect or insufficient labeling, incorrect sample loading, or that may be deemed to be considered hazardous to RJLG personnel. RJLG will notify the Customer as reasonably soon as such a problem is identified and will discuss with the Customer the course of action to be taken. Detection Levels - Certain samples may present chemical or physical interference which could cause deviations of detection levels set forth by regula-tory organizations and methods.

10. USE OF SAMPLES AFTER TESTING. RJLG shall not be obligated to keep prepared samples or any remaining portions of samples for more than thirty (30) days after comple-tion of the requested analyses unless a prior written agreement has been made between RJLG and the Customer. After expiration of this thirty (30) day period, RJLG may either: return the sample to the Customer or dispose of the sample (shipping and handling fees or disposal fees may apply). If prior to expiration of the thirty (30) day period, the Customer

requests that RJLG place the sample in storage or return the sample to the Customer, RJLG reserves the right to charge a special handling or storage fee.

11. REPORTS. Where RJLG’s contract so stipulates, RJLG shall provide to Customer a writ-ten report(s) of the results of the testing and other services performed on Customer’s be-half. The extent, nature, form, and content of the report shall be determined by RJLG, at its sole discretion, unless RJLG and Customer agree to the contrary in writing signed by an officer of RJLG. RJLG assumes no responsibility for the manner in which samples are ob-tained or the effect that the method of obtaining such samples might have on the results of the tests performed by RJLG, or the Customer’s use or interpretation of the test results and reports provided to it by RJLG. When requested by Customer, RJLG will report preliminary test results by telephone, facsimile, and/or email. Any turn-around time requested by Cus-tomer shall be considered to be satisfied with such contact. All such preliminary results are provisional and subject to confirmation. The Customer shall specify the recipient of the preliminary report, by telephone, facsimile number, email address, or electronic data exchange (with prior approval from RJLG) to which the report shall be submitted and will designate an alternate recipient in the event the primary recipient cannot be reached. RJLG will use its best efforts to contact the designated recipient(s) but is not responsible for delays resulting from the failure of the recipient(s) to respond to inquiries. Additional fees may apply for the development, implementation, and on-going maintenance of an elec-tronic data exchange process. RJLG retains records of laboratory analysis for the period of time required by the appropriate accrediting body, according to contract requirements, or as per client-specific requests. RJLG reserves the right to assess record retention fees for those records that, at the client’s request, are retained beyond accreditation or contract re-quirements. In the event a Customer requests additional copies of archived reports, RJLG reserves the right to charge a fee for the retrieval and issuance of such documents.

12. WARRANTIES. Customer is solely responsible for the use and the interpretation of RJLG’s reports and test results. RJLG has no duty or obligation to provide services that it has not expressly agreed in writing to provide. The foregoing express warranties of RJLG are in lieu of all other warranties, express, implied or statutory, including but not limited to, any implied warranty of merchantability or fitness for particular purpose, and in lieu of any other warranty obligation on the part of RJLG.

13. LIMITATIONS OF REMEDIES AND DAMAGES (a) RJLG is solely responsible for the performance of this contract, and no parent, subsidiary or affiliated company, or any of its directors, officers, employees, agents or subcontractors shall have any legal responsibility hereunder, whether in contract or tort, including negligence.

(b) The sole and exclusive remedy of Customer, and responsibility of RJLG for any breach of warranty or other breach of contract, or any claim of negligence, shall be at RJLG’s sole option (i) to repair or replace any defective product, (ii) to correct any defective perfor-mance, (iii) to retest the same or a replacement sample without costs, (iv) to refund any amounts paid by Customer for the defective sample product or other service or (v) to refund any sample priority price differential if a sample is not processed within the time requested by Customer.

(c) In no event, shall RJLG be liable to anyone, whether in contract, strict liability, or tort, including the negligence of RJLG or its employees, agents or representatives, for any inci-dental, consequential, special or indirect damages of any kind or charter, under or arising out of any contract between the parties.

(d) RJLG’s maximum liability under or arising out of this contract shall be the contract price of any services improperly performed. Liability for injury or damage to persons or property arising out of this work shall be limited to the amount covered by the general comprehensive liability insurance carried by RJLG.

14. WAIVER. In the event of any default or breach of contract (or anticipatory breach) by Customer, RJLG has the right to refuse to provide any additional services to Customer. RJLG’s failure to enforce at any time or for any period of time any of the provisions of this contract shall not constitute a waiver of such provisions or the right of RJLG to enforce each and every provision.

15. AMENDMENTS. No addition or amendment to, or modification of, any printed pro-vision of these Terms and Conditions of Sale will be binding upon RJLG unless made in writing and signed by an officer of RJLG. Except to the extent expressly provided herein, no course of dealing, usage of trade, or course of performance will be deemed relevant to explain or supplement any provision of these Terms and Conditions of sale.

16. PERIOD OF LIMITATION OF ACTION. No action shall be brought against RJLG for any breach of this contract after a period of more than one (1) year after the performance of work by RJLG.

17. GOVERNING LAW. The validity, construction, and performance of this contract and the transactions to which it relates shall be governed by the laws of the Commonwealth of Pennsylvania. All actions claims or legal proceedings, in any way pertaining to this con-tract or such transaction, shall be commenced and maintained in the courts of such Com-monwealth or in the United States District Court for the Western District of Pennsylvania and in no other court or tribunal whatsoever, and the parties hereto each agree to submit themselves to the jurisdiction and venue of such courts.

18. LIMITATION OF USE AND DISSEMINATION. Test results and reports prepared by RJLG are prepared and intended solely and exclusively for the person or entity named on such test results or report and are therefore not to be used or relied on by any other person or entity.

Terms & Conditions of Sale for RJ Lee Group ServicesTerms & Conditions of Sale for RJ Lee Group Services

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