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Page 1 27 February 2013 Mr. Jerry O’Callaghan Manager IDEM, Office of Land Quality State Cleanup Section MC 66-30 (1370) 100 N. Senate Avenue, IGCN 1101 Indianapolis, IN 46204-2251 RE: Annual Progress Report Remediation and Closure Activities Component Machine Property 1631 North Gent Avenue, Indianapolis, Indiana Dear Jerry: Acuity Environmental Solutions (AcuityES) is pleased to present the following progress report to detail environmental remediation activities completed at the above-referenced property (Site). This progress report details the work completed by AcuityES in 2012. Introduction During 2012 AcuityES completed multiple field activities, including the following: operation and maintenance of the recirculation system, installation of three horizontal injection wells, injection of approximately 41,000 gallons of potassium permanganate solution, collection of groundwater samples from o extraction wells, o injection wells, and o four quarterly sampling events of the monitoring well network. In addition to field activities, AcuityES met with the Indiana Department of Environmental Management (IDEM) on 30 August 2012 to develop a closure strategy for the Site and agreed to complete closure using “Stability Monitoring”. The agreement would be contingent upon two issues: 1) Citizen’s Energy Group must agree to the approach since they operate the City water supply well near the Site, and 2) The Stability Monitoring default statistical analysis demonstrates groundwater plume stability. The IDEM’s preferred analysis is the Mann – Kendall Trend Test. AcuityES has completed this analysis with the currently available data for monitoring wells that will meet the data requirements (PMW-1, PMW-4, PMW-5, and PMW-6), and at this point, the monitoring wells would meet the Mann – Kendall Trend Test requirements for plume stability of tetrachloroethene (PCE) and trichloroethene (TCE). Six of the eight trend analyses are decreasing, with the exception of PCE in PMW-6 (stable/no trend) and TCE in PMW-4 (stable/no trend). However, an element of the Mann – Kendall statistical analysis that should be addressed is that the method does not consider the magnitude of contamination. For example, the Reference 45 Page 1

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Page 1: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

Page 1

27 February 2013 Mr. Jerry O’Callaghan Manager IDEM, Office of Land Quality State Cleanup Section MC 66-30 (1370) 100 N. Senate Avenue, IGCN 1101 Indianapolis, IN 46204-2251 RE: Annual Progress Report Remediation and Closure Activities

Component Machine Property 1631 North Gent Avenue, Indianapolis, Indiana

Dear Jerry: Acuity Environmental Solutions (AcuityES) is pleased to present the following progress report to detail environmental remediation activities completed at the above-referenced property (Site). This progress report details the work completed by AcuityES in 2012.

Introduction

During 2012 AcuityES completed multiple field activities, including the following:

operation and maintenance of the recirculation system,

installation of three horizontal injection wells,

injection of approximately 41,000 gallons of potassium permanganate solution,

collection of groundwater samples from

o extraction wells,

o injection wells, and

o four quarterly sampling events of the monitoring well network.

In addition to field activities, AcuityES met with the Indiana Department of Environmental Management (IDEM) on 30 August 2012 to develop a closure strategy for the Site and agreed to complete closure using “Stability Monitoring”. The agreement would be contingent upon two issues: 1) Citizen’s Energy Group must agree to the approach since they operate the City water supply well near the Site, and 2) The Stability Monitoring default statistical analysis demonstrates groundwater plume stability. The IDEM’s preferred analysis is the Mann – Kendall Trend Test. AcuityES has completed this analysis with the currently available data for monitoring wells that will meet the data requirements (PMW-1, PMW-4, PMW-5, and PMW-6), and at this point, the monitoring wells would meet the Mann – Kendall Trend Test requirements for plume stability of tetrachloroethene (PCE) and trichloroethene (TCE). Six of the eight trend analyses are decreasing, with the exception of PCE in PMW-6 (stable/no trend) and TCE in PMW-4 (stable/no trend). However, an element of the Mann – Kendall statistical analysis that should be addressed is that the method does not consider the magnitude of contamination. For example, the

Reference 45 Page 1

Page 2: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

Annual Progress Report Component Machine Property

1024-1003-02 27 February 2013

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concentrations of PCE in PMW-6 are below residential standards. The current PCE commercial/industrial closure criteria (considering vapor intrusion) is 0.47 mg/L and the residential criteria is 0.11 mg/L, and laboratory analyses of groundwater samples from one Site well exceeds the residential criteria (PMW-4). Groundwater samples from off-Site monitoring well MW-15 also exceed the residential criteria. The selected approach to reach closure will be the use of both stability monitoring (which requires 28 sampling events) and default closure level compliance. Groundwater sampling from monitoring wells has occurred at the Site since 2004, and a total of 24 groundwater sampling events have been completed. Groundwater samples will need to be collected from Site wells for an additional 4 events (the four quarterly events for 2013). If the Mann-Kendall Trend Test displays stability or a decline in concentrations, Site closure will be pursued.

Background

Historical wastewater management at the Site included the usage of an oil/water separator and grit settling basin consisting of a concrete vault. The vault received wash waters and cleaning solutions which were used to clean engine parts. Some solutions contained tetrachloroethene (PCE) and trichloroethene (TCE) which seeped through the concrete vault into soil and groundwater. Both PCE and TCE are considered constituents of concern (CoCs) for the Site.

In order to best treat the Site-related CoCs, AcuityES implemented a Pilot Test (as outlined in the June 18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate) for groundwater remediation. In addition to the activities outlined in the Pilot Test Plan, AcuityES installed eight (8) monitoring wells (MW-9 through MW-16) to further assess the extent of the CoC plume.

Recirculation System Operation and Maintenance

The recirculation system used for the in-situ treatment of Site COCs in groundwater was operational for portions of 2012, and processed approximately 442,000 gallons of water. As previously detailed in the Pilot Test Plan, the system is remotely accessed and controlled, which allows for reduced operational costs. An AcuityES representative conducts a Site visit approximately weekly to visually inspect the system, ensure Site security, and perform general maintenance if required. During 2012, the system was shut down during several field events, including the installation of the horizontal wells and the subsequent injection activities. An additional unexpected shutdown occurred between the dates of November 15th and December 7th. Troubleshooting revealed that the system control panel had experienced several voltage fluctuations. When these fluctuations occur, they result in the shutdown of the panel and require a manual reset. While troubleshooting revealed that this issue could potentially be overcome via the installation of an emergency battery backup, the benefits are deemed to be marginal; weekly Site visits would continue to occur regardless of the presence of an additional power source, and any further panel shutdowns could be addressed without the need for incurring additional costs.

Installation of Horizontal Injection Wells & Injection of Permanganate Solution

Three two inch diameter horizontal injection wells constructed with new high density polyethylene were completed during the months of January and February. The openings in the wells consist of ports which allow for greater dispersion during injection than slotted or milled screens.

The wells were installed with a southwest-northeast orientation beneath the Component Machine building, to depths of approximately 15 to 17 feet below grade. Difficulties in advancing the eastern well

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Annual Progress Report Component Machine Property

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were encountered during drilling activities; consequently, the eastern well represents the “shallowest” elevation of the injection wells.

During 2012, approximately 41,000 of gallons of permanganate (3% strength weight/weight) were injected through the horizontal wells into the subsurface. The injections occurred in three phases; 16,000 gallons in February, 12,000 gallons in May, and 13,000 gallons in June. While initial plans called for the additional injection of a vegetable oil product slip-streamed with dechlorinating microorganisms, sampling conducted in the vicinity of the horizontal wells revealed that the permanganate injections had lowered COC concentrations on the eastern portion of the Site. Given that the recirculation system was operational during the year, the lower concentrations of COCs in the eastern portion of the Site (i.e., in proximity to the recirculation system and injection wells) is to be expected, as samples would represent treated and untreated water.

Due to drought-like conditions during the summer, it appears that a substantial amount of permanganate may be suspended above the current water table and slightly below the horizontal wells which were used to introduce the permanganate into the aquifer beneath the Component Machine building. AcuityES will continue groundwater monitoring through the Spring of 2013, when groundwater levels are anticipated to rise. The winter groundwater sampling results will be reviewed before additional decisions regarding treatment or management of the groundwater plume are made. Groundwater elevations (Figure 1) collected during December of 2012 show generalized groundwater flow to be in a southwesterly direction, consistent with previously observed elevations.

Data Collection

Groundwater Sampling

Four groundwater sampling events were completed in 2012 (April, June, September, and December). Data collected from the monitoring well network are displayed in Table 1, and a summary of data collected from the monitoring well network (as well as the extraction and injection wells) is displayed on Figure 2. In general, concentrations of PCE are decreasing (see Charts 1 and 2). Furthermore, on July 31 2012, the IDEM released updated documentation regarding the toxicity parameters of PCE, detailing the modification of the commercial/industrial closure criteria to 0.47 mg/L and the residential criteria to 0.11 mg/L. As such, only PMW-4 and MW-15 contain reported concentrations of PCE in excess of IDEM residential closure criteria, and no wells exceed the commercial/industrial closure criteria for PCE. While TCE has been reported above the IDEM screening levels throughout the monitoring well network (with the exception of PMW-5 and MW-13), the Mann – Kendall Trend Test demonstrates that TCE concentrations are generally decreasing (see Charts 1 and 3).

Field parameters collected during the low flow groundwater sampling events are presented in Appendix A. The data indicates that the Site’s groundwater is aerobic and relatively neutral. Oxidation reduction potential (ORP) and pH values have reported relatively consistent values during the previous two years.

Laboratory reports of the groundwater sampling analyses are provided in Appendix B.

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Annual Progress Report Component Machine Property

1024-1003-02 27 February 2013

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Conclusions and Recommendations

Sampling results have shown that Site COCs (PCE and TCE) are either decreasing or stable. In order to complete the 7 year stability monitoring requirement for the Mann – Kendall Trend Test, an additional four quarterly monitoring events will be conducted during the calendar year 2013. Upon completion of the 28 sampling events, AcuityES will reevaluate the data, and provided that either continued stability or a decline in concentrations is observed, Site closure will be pursued.

Should you have any questions regarding the Site or this progress report please do not hesitate to contact the undersigned.

Sincerely,

Eric Peterson Ray Milejczak, L.P.G. Staff Scientist Principal Geologist

Attachments: Table 1 Figures 1 and 2 Charts 1 through 3 Appendices A and B

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Page 5: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

Table 1Groundwater Sampling Results

Component Machine Site, Indianapolis, IN

Page 1 of 5

Well ID Date 1,1,1-TCA

Qua

l Carbon tetrachloride Q

ual

Chloroform

Qua

l

cis-1,2-DCE

Qua

l

PCE

Qua

l

TCE

Qua

l

12/02/04 0.0071 <0.005 <0.005 0.026 0.27 0.2702/25/05 0.0072 <0.005 <0.005 0.028 0.17 0.208/18/05 <0.005 <0.005 <0.005 <0.005 0.071 0.06711/19/05 <0.005 <0.005 <0.005 0.0073 0.11 0.08804/29/06 0.0051 <0.001 <0.001 0.021 0.2 0.1708/09/06 <0.005 <0.005 <0.005 0.017 0.13 0.1303/20/07 0.0033 <0.001 <0.005 0.0033 0.12 0.08509/18/07 0.0021 <0.001 <0.001 <0.001 0.13 0.06601/16/08 <0.005 <0.005 <0.005 <0.005 0.0571 0.026805/14/08 <0.005 <0.005 <0.005 <0.005 0.0878 0.045708/25/08 <0.005 <0.005 <0.005 <0.005 0.173 0.13112/16/08 <0.005 <0.005 <0.005 <0.005 0.0503 0.025310/16/09 0.00035 J 0.0011 0.00042 J <0.001 0.021 0.008708/20/10 0.00067 J 0.00039 J 0.0011 J 0.002 0.037 0.02411/19/10 <0.001 <0.001 0.0005 J <0.001 0.0098 0.005102/15/11 <0.001 0.00098 J 0.00046 J <0.001 0.0085 0.00306/10/11 0.001 0.0005 J 0.0011 J 0.003 0.1 0.05307/27/11 0.00084 J <0.001 0.00064 J 0.0026 0.075 0.0409/22/11 0.00047 J 0.00078 J 0.0018 J 0.0082 0.024 0.01612/22/11 <0.001 <0.001 <0.005 0.0032 0.069 0.03404/02/12 <0.001 <0.001 <0.005 0.0019 0.037 J6 0.0206/07/12 <0.001 <0.001 <0.005 <0.001 0.032 0.01209/17/12 <0.001 <0.001 <0.005 0.0018 0.019 0.009312/18/12 <0.001 <0.001 <0.005 <0.001 0.016 0.006412/02/04 <0.005 <0.005 <0.005 <0.005 0.14 0.1202/25/05 0.0098 <0.005 <0.005 <0.005 0.13 0.1608/18/05 0.0077 <0.005 <0.005 <0.005 0.093 0.1411/19/05 0.0062 <0.005 <0.005 <0.005 0.17 0.1104/29/06 <0.005 <0.005 <0.005 <0.005 0.14 0.1108/09/06 0.0053 <0.005 <0.005 <0.005 0.12 0.103/21/07 0.0088 <0.001 <0.005 <0.001 0.16 0.1209/18/07 0.0067 <0.001 <0.001 <0.001 0.14 0.1101/16/08 0.0062 <0.005 <0.005 <0.005 0.138 0.10705/14/08 <0.005 <0.005 <0.005 <0.005 0.164 0.068308/25/08 <0.005 <0.005 <0.005 <0.005 0.152 0.085612/02/04 <0.005 <0.005 <0.005 <0.005 <0.005 0.08802/25/05 <0.005 <0.005 <0.005 <0.005 <0.005 0.07708/18/05 <0.005 <0.005 <0.005 <0.005 <0.005 0.09711/19/05 0.0074 <0.005 <0.005 <0.005 <0.005 0.1204/29/06 0.003 <0.001 <0.001 <0.001 0.0016 0.06808/09/06 <0.005 <0.005 <0.005 <0.005 <0.005 0.07203/21/07 0.0026 <0.001 <0.005 <0.001 0.002 0.05909/18/07 0.0056 <0.001 <0.001 <0.001 0.0022 0.09301/16/08 <0.005 <0.005 <0.005 <0.005 <0.005 0.075805/14/08 <0.005 <0.005 <0.005 <0.005 <0.005 0.056108/25/08 <0.005 <0.005 <0.005 <0.005 <0.005 0.0813

PMW-1

PMW-2

PMW-3

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Reference 45 Page 5

Page 6: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

Table 1Groundwater Sampling Results

Component Machine Site, Indianapolis, IN

Page 2 of 5

Well ID Date 1,1,1-TCA

Qua

l Carbon tetrachloride Q

ual

Chloroform

Qua

l

cis-1,2-DCE

Qua

l

PCE

Qua

l

TCE

Qua

l

12/02/04 <0.005 <0.005 0.011 0.018 0.24 0.04302/25/05 <0.005 <0.005 0.012 0.024 0.22 0.0408/18/05 <0.005 <0.005 0.0079 0.025 0.2 0.03111/19/05 <0.005 <0.005 0.0095 0.026 0.28 0.03904/29/06 <0.01 <0.01 <0.01 0.018 0.19 0.02208/09/06 <0.005 <0.005 0.0073 0.035 0.2 0.02403/20/07 <0.005 <0.001 <0.005 0.013 0.19 0.01809/18/07 0.0025 <0.001 0.0079 0.033 0.24 0.01801/16/08 <0.005 <0.005 <0.005 0.0279 0.274 0.029205/14/08 <0.005 <0.005 0.0067 0.0192 0.25 0.028308/25/08 <0.005 <0.005 0.0097 0.0227 0.184 0.041612/16/08 0.0092 <0.005 0.0097 0.0179 0.279 0.05210/16/09 0.0055 0.00082 J 0.013 0.016 0.21 0.04408/20/10 0.0036 <0.001 0.0069 0.0057 0.22 0.02911/19/10 0.0032 <0.001 0.0077 0.0056 0.12 0.02302/15/11 0.004 <0.001 0.0079 0.0042 0.18 V 0.0306/10/11 0.0037 <0.001 0.0059 0.0041 0.22 0.03707/27/11 0.0038 J <0.005 0.0046 J 0.0064 0.22 0.04409/22/11 0.003 <0.001 0.0029 J 0.0059 0.16 0.03612/22/11 0.0025 <0.002 <0.01 0.0046 0.12 0.03204/02/12 0.0029 <0.001 0.0064 0.0088 0.12 0.03906/07/12 0.0032 <0.001 <0.005 0.011 0.2 0.0509/17/12 <0.002 <0.002 <0.01 0.091 0.092 0.0312/18/12 0.0018 <0.001 <0.005 0.013 0.13 0.04312/02/04 <0.005 <0.005 0.009 <0.005 0.064 0.01802/25/05 <0.005 <0.005 0.0075 <0.005 0.03 0.008808/18/05 <0.005 <0.005 0.0073 <0.005 0.041 0.01511/19/05 <0.005 <0.005 0.0088 <0.005 0.049 0.01404/29/06 <0.001 <0.01 0.0078 <0.001 0.036 0.008308/09/06 <0.005 <0.005 0.0073 <0.005 0.035 0.008303/20/07 0.0014 <0.001 <0.005 <0.001 0.031 0.006409/18/07 <0.001 <0.001 0.0052 <0.001 0.036 0.00701/16/08 <0.005 <0.005 <0.005 <0.005 0.041 <0.00505/14/08 <0.005 <0.005 0.054 <0.005 0.0453 0.007808/25/08 <0.005 <0.005 0.0065 <0.005 0.0348 0.008712/16/08 <0.005 <0.005 <0.005 <0.005 0.0569 0.012810/16/09 0.00069 J <0.001 0.0086 <0.001 0.033 0.005408/20/10 <0.001 <0.001 0.011 <0.001 0.012 0.002611/19/10 <0.001 <0.001 0.0094 <0.001 0.014 0.001302/15/11 <0.001 <0.001 0.014 <0.001 0.026 0.001506/10/11 <0.001 <0.001 <0.005 <0.001 <0.001 <0.00107/27/11 <0.001 <0.001 0.011 <0.001 0.018 0.00109/22/11 <0.001 <0.001 0.0096 <0.001 0.0083 0.0005 J12/22/11 <0.001 <0.001 0.01 <0.001 0.0073 <0.00104/02/12 <0.001 <0.001 0.012 <0.001 0.0084 <0.00106/07/12 <0.001 <0.001 0.0088 <0.001 0.018 <0.00109/17/12 <0.001 <0.001 0.0067 <0.001 0.012 <0.00112/18/12 <0.001 <0.001 <0.005 <0.001 0.016 <0.001

PMW-4

PMW-5

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Page 7: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

Table 1Groundwater Sampling Results

Component Machine Site, Indianapolis, IN

Page 3 of 5

Well ID Date 1,1,1-TCA

Qua

l Carbon tetrachloride Q

ual

Chloroform

Qua

l

cis-1,2-DCE

Qua

l

PCE

Qua

l

TCE

Qua

l

12/02/04 <0.005 <0.005 0.0076 0.006 <0.005 0.06402/25/05 0.0052 <0.005 0.0072 0.0055 <0.005 0.06708/18/05 <0.005 <0.005 0.006 <0.005 <0.005 0.0511/19/05 0.0059 <0.005 0.0084 <0.005 <0.005 0.07904/29/06 0.004 0.0017 0.0052 0.0013 0.0029 0.05908/09/06 <0.005 <0.005 <0.005 <0.005 <0.005 0.06103/20/07 0.0069 <0.001 <0.005 0.0048 0.01 0.09309/18/07 <0.001 0.0034 0.0057 <0.001 0.036 0.00701/16/08 0.0056 <0.005 <0.005 <0.005 0.009 0.097605/14/08 0.0055 0.0055 0.0052 <0.005 <0.005 0.077408/25/08 <0.005 <0.005 0.0057 <0.005 <0.005 0.047812/16/08 0.0081 <0.005 0.0063 <0.005 0.0055 0.064610/16/09 0.0042 0.003 0.0073 0.0014 0.0036 0.0708/20/10 0.003 <0.001 0.0082 0.0016 0.0035 0.06411/19/10 0.0029 0.0022 0.0067 0.0022 0.0055 0.05402/15/11 0.0031 0.002 0.0087 0.0046 0.014 0.06106/10/11 0.0023 0.0016 0.0068 0.0015 0.0055 0.0507/27/11 0.0027 0.002 0.0069 0.0018 0.0055 0.05409/22/11 0.0033 0.0028 0.0079 0.0017 0.0063 0.061 J612/22/11 0.0023 0.0021 <0.005 0.0021 0.0092 0.0504/03/12 0.0022 0.0018 0.0056 0.0014 0.011 0.05206/07/12 0.0024 0.0018 0.0058 0.0013 0.011 0.05609/17/12 0.0016 <0.001 <0.005 0.0012 0.0017 0.02412/18/12 0.0024 0.0019 0.006 <0.001 0.0086 0.05208/20/10 <0.001 <0.001 0.003 J 0.0027 0.041 0.007511/19/10 <0.001 <0.001 0.014 0.0065 0.016 0.002802/15/11 <0.001 <0.001 0.0084 0.00087 J 0.015 0.002206/10/11 0.00048 J <0.001 0.0071 0.012 0.038 0.01107/27/11 0.00058 J <0.001 0.0094 0.0087 0.039 0.01409/23/11 0.00094 J <0.001 0.0098 0.0049 0.051 0.02312/22/11 <0.001 <0.001 <0.005 0.007 0.036 0.01504/02/12 0.0011 <0.001 0.0081 0.018 0.028 0.01906/07/12 0.0015 <0.001 0.01 0.018 0.05 0.02809/17/12 <0.001 <0.001 0.01 0.0051 0.03 0.02112/18/12 0.0013 <0.001 0.016 0.01 0.039 0.02908/20/10 <0.001 <0.001 0.0076 0.0018 0.015 0.002611/19/10 0.0012 <0.001 0.0038 J 0.0048 0.04 0.01702/15/11 0.00086 J <0.001 0.0041 J 0.0038 0.036 0.01106/10/11 0.0006 J <0.001 0.0061 0.0038 0.03 0.009307/27/11 0.0016 <0.001 0.0032 J 0.0045 0.066 0.02209/23/11 0.0016 <0.001 0.0034 J 0.0029 0.05 0.01912/23/11 <0.001 <0.001 <0.005 0.0023 0.037 0.01204/02/12 0.0013 <0.001 <0.005 0.0029 0.076 0.02306/07/12 0.0013 <0.001 <0.005 0.0024 0.092 0.02509/18/12 <0.001 <0.001 <0.005 0.0082 0.048 0.01312/19/12 <0.001 <0.001 <0.005 0.0026 0.048 0.013

PMW-6

MW-8

MW-9

1024-1003-02

Reference 45 Page 7

Page 8: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

Table 1Groundwater Sampling Results

Component Machine Site, Indianapolis, IN

Page 4 of 5

Well ID Date 1,1,1-TCA

Qua

l Carbon tetrachloride Q

ual

Chloroform

Qua

l

cis-1,2-DCE

Qua

l

PCE

Qua

l

TCE

Qua

l

08/20/10 <0.001 <0.001 0.016 <0.001 0.013 0.004711/19/10 0.00067 J <0.001 0.013 <0.001 0.022 0.01902/15/11 <0.001 <0.001 0.02 <0.001 0.018 0.008506/10/11 0.0047 <0.001 0.00053 J 0.0029 0.0021 0.07107/27/11 0.00063 J <0.001 0.0082 <0.001 0.024 0.0209/23/11 <0.001 <0.001 0.012 <0.001 0.021 0.009712/22/11 <0.001 <0.001 0.013 <0.001 0.0052 0.002304/02/12 <0.001 <0.001 0.028 <0.001 0.0056 0.002706/07/12 <0.001 <0.001 0.031 <0.001 0.01 0.004409/17/12 <0.001 <0.001 0.011 <0.001 0.0088 0.003612/19/12 <0.001 <0.001 0.012 <0.001 0.012 0.006208/20/10 0.006 <0.001 0.00057 J 0.0017 0.0023 0.09211/19/10 0.0041 <0.001 0.0012 J 0.001 J 0.0039 0.05402/15/11 0.00059 J <0.001 <0.005 <0.001 0.00051 J 0.004806/10/11 <0.001 <0.001 0.011 <0.001 0.0098 0.007907/27/11 0.0038 <0.001 0.00038 J 0.0019 0.0022 0.05409/22/11 0.002 <0.001 <0.005 0.00047 J 0.001 0.02312/22/11 0.0013 <0.001 <0.005 <0.001 <0.001 0.01604/03/12 0.0022 <0.001 <0.005 0.0019 0.0018 0.02906/07/12 0.0019 <0.001 <0.005 0.0023 0.0038 0.03209/17/12 0.0019 0.0015 <0.005 <0.001 0.0048 0.03712/19/12 0.0017 <0.001 <0.005 <0.001 0.0039 0.02307/27/11 0.00043 J 0.00083 J 0.0082 <0.001 0.016 0.008309/23/11 0.00052 J 0.0015 0.02 <0.001 0.018 0.009412/22/11 <0.001 <0.001 0.0072 <0.001 0.018 0.008504/02/12 <0.001 0.0012 0.0054 <0.001 0.025 0.009406/07/12 <0.001 0.0012 <0.005 <0.001 0.023 0.009109/18/12 <0.001 <0.001 <0.005 <0.001 0.0099 0.004312/18/12 <0.001 0.0013 0.0053 <0.001 0.018 0.009707/27/11 <0.001 <0.001 0.018 <0.001 <0.001 <0.00109/23/11 <0.001 <0.001 0.026 <0.001 <0.001 <0.00112/23/11 <0.001 <0.001 0.017 <0.001 <0.001 <0.00104/03/12 <0.001 <0.001 0.026 <0.001 <0.001 <0.00106/07/12 <0.001 <0.001 0.032 <0.001 0.0013 0.001609/18/12 <0.001 <0.001 0.017 <0.001 <0.001 <0.00112/19/12 <0.001 <0.001 0.02 <0.001 0.0042 0.003607/27/11 0.003 <0.001 0.003 J 0.0032 0.052 0.0609/23/11 0.0032 <0.001 0.0025 J 0.0026 0.044 0.05912/23/11 0.002 <0.001 <0.005 0.0012 0.064 0.04504/03/12 0.0024 <0.001 <0.005 0.0014 0.067 0.05206/07/12 0.0018 <0.001 <0.005 0.0016 0.04 0.04609/18/12 0.0023 <0.001 <0.005 0.0018 0.044 0.05312/19/12 0.0028 <0.001 <0.005 0.0011 0.048 0.055

MW-10

MW-11

MW-12

MW-13

MW-14

1024-1003-02

Reference 45 Page 8

Page 9: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

Table 1Groundwater Sampling Results

Component Machine Site, Indianapolis, IN

Page 5 of 5

Well ID Date 1,1,1-TCA

Qua

l Carbon tetrachloride Q

ual

Chloroform

Qua

l

cis-1,2-DCE

Qua

l

PCE

Qua

l

TCE

Qua

l

07/27/11 0.0028 <0.001 0.0016 J <0.001 0.16 0.05109/23/11 0.0055 <0.001 0.0017 J <0.001 0.12 V 0.08212/23/11 0.0028 <0.001 <0.005 <0.001 0.15 0.05704/03/12 0.0039 <0.001 <0.005 <0.001 0.12 0.0706/07/12 0.0027 <0.001 <0.005 <0.001 0.14 0.05609/18/12 0.0036 <0.001 <0.005 <0.001 0.15 0.07812/19/12 0.0038 <0.001 <0.005 <0.001 0.076 0.06607/27/11 0.011 <0.001 0.00042 J <0.001 0.0054 0.09909/23/11 0.016 <0.001 <0.005 <0.001 0.004 0.1112/23/11 0.01 <0.001 <0.005 <0.001 0.0033 0.08604/03/12 0.012 <0.001 <0.005 <0.001 0.0034 0.106/07/12 0.0098 <0.001 <0.005 <0.001 0.0032 0.08709/18/12 0.011 <0.001 <0.005 <0.001 0.0041 0.112/19/12 0.011 <0.001 <0.005 <0.001 0.0035 0.08410/16/09 <0.001 <0.001 <0.005 <0.001 <0.001 <0.00108/20/10 <0.001 <0.001 <0.005 <0.001 <0.001 <0.00111/19/10 <0.001 <0.001 <0.005 <0.001 <0.001 <0.00102/15/11 <0.001 <0.001 <0.005 <0.001 <0.001 <0.00106/10/11 <0.001 <0.001 <0.005 <0.001 <0.001 <0.00107/27/11 <0.001 <0.001 <0.005 <0.001 <0.001 <0.00109/23/11 <0.001 <0.001 <0.005 <0.001 <0.001 <0.00112/23/11 <0.001 <0.001 <0.005 <0.001 <0.001 <0.00104/03/12 <0.001 <0.001 <0.005 <0.001 <0.001 <0.00106/07/12 <0.001 <0.001 <0.005 <0.001 <0.001 <0.00109/17/12 <0.001 <0.001 <0.005 <0.001 <0.001 <0.00112/18/12 <0.001 <0.001 <0.005 <0.001 <0.001 <0.00110/16/09 0.00038 J 0.00099 J 0.00038 J 0.0021 0.02 0.009608/20/10 0.0052 <0.001 0.00054 J 0.0017 0.0022 0.08911/19/10 0.0041 <0.001 0.0012 J 0.0011 0.0039 0.05202/15/11 <0.001 <0.001 0.014 <0.001 0.018 0.00099 J06/10/11 0.0049 <0.001 0.00058 J 0.0032 0.0022 0.07207/27/11 0.0048 <0.001 0.00045 J 0.0022 0.003 0.07309/23/11 0.0036 <0.001 0.0037 J 0.0057 0.14 0.03612/22/11 <0.001 <0.001 <0.005 0.0037 0.074 0.03804/03/12 <0.001 0.0014 0.0055 <0.001 0.026 0.0106/07/12 0.0026 <0.001 <0.005 0.0094 0.14 0.0409/17/12 0.0026 0.0022 0.0062 0.0012 0.0094 0.06212/18/12 <0.001 <0.001 <0.005 <0.001 0.017 0.0067

0.47 *0.11 *

NOTESValues displayed im mg/L*= Values from the 31 July 2012 IDEM PCE AnnouncementBOLD text indicates a detection above laboratory reporting limits

J= (EPA) - Estimated value below the lowest calibration point. Confidence correlates with concentration.J6= The sample matrix interfered with the ability to make any accurate determination; spike value is low.V= (ESC) - Additional QC Info: The sample concentration is too high to evaluate accurate spike recoveries.

Red highlighting indicates exceedance of Industrial Default Closure Level Blue highlighting indicates exceedance of Residential Default Closure Level

0.031RISC IDCL 29 0.022 1 1RISC RDCL 0.0050.2 0.005 0.08 0.07

TRIP BLANK

DUPLICATE

MW-15

MW-16

1024-1003-02

Reference 45 Page 9

Page 10: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

CO

NCRETE

CONCRETE

ED

GE O

F PAVEM

EN

T

CH

AIRBACK CU

RB

CHAIRBACK CURB

CH

AIRBACK CU

RB

EDGE OF P

AVEMENT

ASPHALT

ASPHALT

ASPHALT

ASPHALT

ASPHALT

ASPH

ALT

ASPH

ALT

ASPHALT

CO

NCRETE

MW-13

MW-14

MW-15MW-16

MW-11

PMW-6

PMW-5

PMW-4

MW-12

MW-8

MW-9

MW-10

PMW-1

EW-2EW-1

683.47

683.38

683.38

683.38

683.15

683.18

683.05

683.20

682.20

682.83

682.84

682.83

683.40

683.20

683.00

7965 E. 106th Street, Suite 128

Fishers, IN 46038

317-570-4919

TITLE

GENERALIZED GROUNDWATER FLOW

19 DECEMBER 2012

PROJECT

Component Machine Site

1631 North Gent Ave.

Indianapolis, IN

1024-1003

DATE

FEBRUARY 2013

Proj. NO.

CK'd. BY DWG. BY

RM EP

VER DWG NO.

1

1

50

0

GRAPHIC SCALE

( IN FEET )

LEGEND

MONITORING WELL

LOCATION

GENERAL GROUNDWATER

FLOW DIRECTION

Reference 45 Page 10

Page 11: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

CO

NCRETE

CONCRETE

ED

GE O

F PAVEM

EN

T

CH

AIRBACK CU

RB

CHAIRBACK CURB

CH

AIRBACK CU

RB

EDGE OF P

AVEMENT

ASPHALT

ASPHALT

ASPHALT

ASPHALT

ASPHALT

ASPH

ALT

ASPH

ALT

ASPHALT

CO

NCRETE

MW-13

MW-14

MW-15MW-16

MW-11

PMW-6

PMW-5

PMW-4

MW-12

MW-8

MW-9

MW-10

PMW-1

PMW-1

2-15-11 6-10-117-27-11

9-22-1112-22-11 4-2-12

6-7-129-17-12 12-18-12

PCE

0.0085 0.10 0.075 0.024 0.069 0.037 0.032 0.019 0.016

TCE0.003 0.053 0.04 0.016 0.034 0.02 0.012 0.0093 0.0064

cis-1,2 DCE<0.001 0.003 0.0026 0.0082 0.0032 0.0019 <0.001 0.0018 <0.001

1,1,1 TCA<0.001 0.001 0.00084 0.00047 <0.001 <0.001 <0.001 <0.001 <0.001

Carbon Tet

0.00098 0.0005 <0.001 0.00078 <0.001 <0.001 <0.001 <0.001 <0.001

MW-102-15-11 6-10-11 7-27-11 9-22-11 12-22-11 4-2-12 6-7-12 9-17-12 12-19-12

PCE 0.018 0.0021 0.024 0.021 0.0052 0.0056 0.01 0.0088 0.012

TCE 0.0085 0.071 0.02 0.0097 0.0023 0.0027 0.0044 0.0036 0.0062

1,1,1 TCA

<0.001 0.0047 0.00063 0.00063 <0.001 <0.001 <0.001 <0.001 <0.001

Carbon Tet <0.001 0.00053 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001

MW-9

2-15-11 6-10-117-27-11

9-22-1112-22-11 4-2-12

6-7-12 9-18-12 12-19-12

PCE 0.036 0.03 0.066 0.050 0.037 0.076 0.092 0.048 0.048

TCE 0.011 0.0093 0.022 0.019 0.012 0.023 0.025 0.013 0.013

cis-1,2 DCE

<0.001 0.003 0.0026 0.0029 <0.001 0.0029 0.0024 0.0082 0.0026

1,1,1 TCA

0.00086 0.0006 0.0016 0.0016 <0.001 0.0013 0.0013 <0.001 <0.001

Carbon Tet <0.001 0.0011 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001

MW-82-15-11 6-10-11 7-27-11 9-22-11 12-22-11 4-2-12 6-7-12 9-17-12 12-18-12

PCE 0.015 0.038 0.039 0.051 0.036 0.028 0.05 0.03 0.039

TCE 0.0022 0.011 0.014 0.023 0.015 0.019 0.028 0.021 0.029

cis-1,2 DCE

0.00087 0.012 0.0087 0.0049 0.007 0.018 0.018 0.0051 0.01

1,1,1 TCA

<0.001 0.00048 0.00058 0.00094 <0.001 0.0011 0.0015 <0.001 0.0013

Carbon Tet <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001

MW-127-27-11 9-22-11 12-22-11 4-2-12 6-7-12 9-18-12 12-18-12

PCE 0.016 0.018 0.018 0.018 0.023 0.0099 0.018

TCE 0.0083 0.0094 0.0085 0.0094 0.0091 0.0043 0.0097

cis-1,2 DCE

<0.001 <0.001 <0.001 <0.001 <0.005 <0.001 <0.001

1,1,1 TCA

0.00043 0.00052 <0.001 <0.001 <0.005 <0.001 <0.001

Carbon Tet 0.00083 0.0015 <0.001 0.0012 0.0012 <0.001 0.0013

PMW-52-15-11 6-10-11

7-27-119-22-11

12-22-114-2-12 6-7-12 9-17-12 12-18-12

PCE 0.026 <0.001 0.018 0.0083 0.0073 0.0084 0.018 0.012 0.016

TCE 0.0015 <0.001 0.001 0.0005 <0.001 <0.001 <0.001 <0.001 <0.001

1,1,1 TCA

<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.001 <0.001

Carbon Tet <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.001 <0.001

PMW-42-15-11 6-10-11 7-27-11 9-22-11 12-22-11 4-2-12 6-7-12 9-17-12 12-18-12

PCE 0.18 0.22 0.22 0.16 0.12 0.12 0.2 0.092 0.13

TCE 0.03 0.037 0.044 0.036 0.032 0.039 0.05 0.03 0.043

cis-1,2 DCE

0.0042 0.0041 0.0064 0.0059 0.0046 0.0088 0.011 0.091 0.013

1,1,1 TCA

0.004 0.0037 0.0038 0.003 0.0025 0.0029 <0.005 <0.002 0.0018

MW-112-15-11 6-10-11 7-27-11 9-22-11 12-22-11 4-3-12 6-7-12 9-17-12 12-19-12

PCE 0.00051 0.0098 0.0022 0.001 <0.001 0.0018 0.0038 0.0048 0.0039

TCE 0.0048 0.0079 0.054 0.023 0.016 0.029 0.032 0.037 0.023

cis-1,2 DCE

0.00051 0.0098 0.0022 0.00047 <0.001 0.0019 0.0023 <0.001 <0.001

1,1,1 TCA

0.00059 <0.001 0.0038 0.002 0.0013 0.0022 0.0019 0.0019 0.0017

Carbon Tet <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 0.0015 <0.001

MW-13 7-27-119-22-11

12-22-114-3-12 6-7-12 9-18-12 12-19-12

PCE <0.001 <0.001 <0.001 <0.001 0.0013 <0.001 0.0042

TCE <0.001 <0.001 <0.001 <0.001 0.0016 <0.001 0.0036

cis-1,2 DCE

<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001

1,1,1 TCA

<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001

Carbon Tet <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001

MW-147-27-11 9-22-11 12-22-11 4-3-12 6-7-12 9-18-12 12-19-12

PCE 0.052 0.044 0.064 0.067 0.04 0.044 0.048

TCE 0.06 0.059 0.045 0.052 0.046 0.053 0.055

cis-1,2 DCE

0.0032 0.0026 0.0012 0.0014 0.0016 0.0018 0.0011

1,1,1 TCA

0.003 0.0032 0.002 0.0024 0.0018 0.0023 0.0028

Carbon Tet <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001

MW-157-27-11 9-22-11 12-22-11 4-3-12 6-7-12 9-18-12 12-19-12

PCE 0.16 0.12 0.15 0.12 0.14 0.15 0.076

TCE 0.051 0.082 0.057 0.07 0.056 0.078 0.066

cis-1,2 DCE

<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001

1,1,1 TCA

0.0028 0.0055 0.0028 0.0039 0.0027 0.0036 0.0038

Carbon Tet <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001

MW-167-27-11 9-22-11 12-22-11 4-3-12 6-7-12 9-18-12 12-19-12

PCE 0.0054 0.004 0.0033 0.0034 0.0032 0.0041 0.0035

TCE 0.099 0.11 0.086 0.10 0.087 0.1 0.084

cis-1,2 DCE

<0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001

1,1,1 TCA

0.011 0.016 0.010 0.012 0.0098 0.011 0.011

Carbon Tet <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001

West

Line:60':NE

01-10-12

PCE 0.14

TCE 0.0085

cis-1,2 DCE

0.0038

1,1,1 TCA

<0.001

Carbon Tet <0.001

Center

Line:90':SW

02-07-125-16-12

PCE 0.0021 <0.005

TCE <0.001 <0.005

cis-1,2 DCE

<0.001 <0.005

1,1,1 TCA

<0.001 <0.005

Carbon Tet <0.001 0.0325

Chloroform <0.001 0.116

EW-2EW-1

EW-205-16-12

07-17-12

PCE 0.033 0.0447

TCE 0.0059 0.0070

cis-1,2 DCE

<0.005 <0.005

1,1,1 TCA

<0.005 <0.005

Carbon Tet <0.005 <0.005

West Line

120' NE

01-10-12 02-07-12

PCE 0.25 0.25

TCE 0.017 0.011

cis-1,2 DCE

0.0049 0.0037

1,1,1 TCA

<0.001 <0.001

Carbon Tet <0.001 <0.001

West Line

90' NE

05-16-12

PCE <0.005

TCE <0.005

cis-1,2 DCE

<0.005

1,1,1 TCA

<0.005

Carbon Tet <0.005

West Line

60' NE

01-10-12

PCE 0.14

TCE 0.0085

cis-1,2 DCE

0.0038

1,1,1 TCA

<0.001

Carbon Tet <0.001

West Line

40' SW

02-07-12

PCE 0.25

TCE 0.011

cis-1,2 DCE

0.0035

1,1,1 TCA

<0.001

Carbon Tet <0.001

EW-1 05-16-12 07-17-12

PCE 0.0856 0.0817

TCE 0.0374 0.0296

cis-1,2 DCE

<0.005 0.0151

1,1,1 TCA

<0.005 <0.005

Carbon Tet <0.005 <0.005

PMW-62-15-11 6-10-11 7-27-11 9-22-11 12-22-11 4-3-12 6-7-12 9-17-12 12-19-12

PCE 0.014 0.0055 0.0055 0.0063 0.0092 0.011 0.011 0.0017 0.0086

TCE 0.061 0.05 0.054 0.061 0.05 0.052 0.056 0.024 0.052

cis-1,2 DCE

0.0042 0.0041 0.0064 0.0017 0.0021 0.0014 0.0013 0.0012 <0.001

1,1,1 TCA

0.0031 0.0023 0.0027 0.0033 0.0023 0.0022 0.0024 0.0016 0.0024

Carbon Tet 0.002 0.0016 0.002 0.0028 0.0021 0.0018 0.0018 <0.001 0.0019

7965 E. 106th Street, Suite 128

Fishers, IN 46038

317-570-4919

TITLE

Groundwater Sampling Results

PROJECT

Component Machine Site

1631 North Gent Ave.

Indianapolis, IN

1024-1003

DATE

FEBRUARY 2013

Proj. NO.

CK'd. BY DWG. BY

RM EP

VER DWG NO.

1

2

50

0

GRAPHIC SCALE

( IN FEET )

MW-1 RDCL IDCL

PCE

see above see above

TCE 0.005 0.031

cis-1,2-DCE

0.07 1

1,1,1-TCA

0.2 29

Carbon Tet 0.005 0.022

ALL CONCENTRATIONS ARE GIVEN IN

MILLIGRAMS PER LITER (mg/L)

PCE concentrations have been compared to

residential (0.11) and commercial/industrial

(0.47) levels based upon noncarcinogenic

effects outlined in IDEM's July 31, 2012 PCE

guidance

BLUE SHADED RESULTS EXCEED IDEM

RESIDENTIAL SCREENING LEVELS (SHOWN

BELOW)

RED SHADED RESULTS EXCEED IDEM

INDUSTRIAL SCREENING LEVELS (SHOWN

BELOW)

tetrachloroethene

trichloroethene

cis-1,2-dichloroethene

1,1,1-trichloroethane

Carbon Tetrachloride

PCE:

TCE:

cis-1,2-DCE:

1,1,1-TCA:

Carbon Tet:

LEGEND

= MONITORING WELL LOCATION

Reference 45 Page 11

Page 12: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

Chart 1Plot of Tetrachloroethene and Trichloroethene Concentrations

Groundwater Samples Collected From Upgradient and Downgradient Monitoring WellsComponent Machine Site, Indianapolis, IN

R² = 0.4809

R² = 0.1314

0

0.05

0.1

0.15

0.2

0.25

0.3PMW-4 - ON-SITE, DOWNGRADIENT EDGE OF PLUME

PCE

TCE

Poly. (PCE)

Poly. (TCE)

R² = 0.0319

R² = 0.14

0.00

0.05

0.10

0.15

0.20

0.25

0.30PMW-6 - OFF-SITE, DOWNGRADIENT EDGE OF PLUME

PCE

TCE

Poly. (PCE)

Poly. (TCE)

R² = 0.6443R² = 0.8451

0

0.05

0.1

0.15

0.2

0.25

0.3PMW-5 - DOWNGRADIENT EDGE AND SOUTHEASTERN BOUNDARY

PCE

TCE

Poly. (PCE)

Expon. (TCE)

R² = 0.6002

R² = 0.6162

0

0.05

0.1

0.15

0.2

0.25

0.3

PMW-1 - ADJACENT TO PERMANGANATE INJECTION CAISSONS

PCE

TCE

Poly. (PCE)

Expon. (TCE)

AcuityES Job No. 1024-1003-02

Reference 45 Page 12

Page 13: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

Chart 27 Year Mann - Kendall Analysis of Tetrachloroethene Concentrations

Component Machine

-0.050

0.050.1

0.150.2

0.250.3

1 3 5 7 9 11 13 15 17 19 21 23 25 27Con

cent

ratio

n (m

g/l)

Sampling Events

PMW-1: PCE 7 Year Time Series

00.020.040.060.08

0.1

1 3 5 7 9 11 13 15 17 19 21 23 25 27Con

cent

ratio

n (m

g/l)

Sampling Events

PMW-6: PCE 7 Year Time Series

00.05

0.10.15

0.20.25

0.3

1 3 5 7 9 11 13 15 17 19 21 23 25 27Con

cent

ratio

n (m

g/l)

Sampling Events

PMW-4: PCE 7 Year Time Series

-0.020

0.020.040.060.08

0.1

1 3 5 7 9 11 13 15 17 19 21 23 25 27

Con

cent

ratio

n (m

g/l)

Sampling Events

PMW-5: PCE 7 Year Time Series

AcuityES # 1024-1003

Reference 45 Page 13

Page 14: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

Chart 37 Year Mann - Kendall Analysis of Trichloroethene Concentrations

Component Machine

-0.1-0.05

00.05

0.10.15

0.20.25

0.3

1 3 5 7 9 11 13 15 17 19 21 23 25 27

Con

cent

ratio

n (u

g/l)

Sampling Event

PMW-1: TCE 7 Year Time Series

00.03

0.060.090.12

0.15

1 3 5 7 9 11 13 15 17 19 21 23 25 27

Con

cent

ratio

n (u

g/l)

Sampling Event

PMW-4: TCE 7 Year Time Series

00.03

0.060.090.12

0.15

1 3 5 7 9 11 13 15 17 19 21 23 25 27

Con

cent

ratio

n (u

g/l)

Sampling Event

PMW-5: TCE 7 Year Time Series

00.03

0.060.090.12

0.15

1 3 5 7 9 11 13 15 17 19 21 23 25 27C

once

ntra

tion

(ug/

l)

Sampling Event

PMW-6: TCE 7 Year Time Series

AcuityES #:1024-1003

Reference 45 Page 14

Page 15: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

04/02/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 21 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 802.71 [mL]

17.72 [ft] Calculated Sample Rate 322 [sec]10 [ft] Sample rate 322 [sec]5 [in] 0 [in]

15.79 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-0.03 +/-0.1 +/-0.1 +/-10+/-3 % +/-10 % +/-10 %

14:57:21 12.89 7.35 624.06 262.20 4.44 0.1414:59:57 12.60 7.33 620.98 188.95 4.41 0.1415:02:25 12.56 7.32 621.81 145.84 4.47 0.1415:05:13 12.70 7.32 622.88 101.68 4.45 0.1415:08:01 12.55 7.31 621.81 62.11 4.44 0.1315:02:25 -0.04 -0.01 0.83 -43.12 0.07 0.0015:05:13 0.14 0.00 1.07 -44.16 -0.02 0.0015:08:01 -0.15 -0.01 -1.07 -39.57 -0.01 0.00

Notes: 60 degrees F

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

BLADDER pumpTEFLON

MW 10

1024-1003

Tubing TypeACUITYESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:MILEJCZAK Pump Model/Type

Reference 45 Page 15

Page 16: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

04/03/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 21 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 802.71 [mL]

18.08 [ft] Calculated Sample Rate 322 [sec]10 [ft] Sample rate 322 [sec]5 [in] 0 [in]

12.78 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-0.03 +/-0.1 +/-0.1 +/-10+/-3 % +/-10 % +/-10 %

9:19:54 12.68 7.25 596.96 110.84 2.38 0.069:22:28 12.68 7.24 597.40 79.98 2.16 0.069:24:56 12.69 7.23 598.72 73.68 2.03 0.069:29:15 12.72 7.22 600.71 57.68 1.79 0.059:31:43 12.73 7.21 601.49 55.91 1.69 0.059:24:56 0.01 -0.01 1.32 -6.29 -0.13 0.009:29:15 0.02 -0.02 1.99 -16.00 -0.24 0.009:31:43 0.01 -0.01 0.78 -1.77 -0.10 0.00

Notes: 56 degrees F

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

BLADDER pumpTEFLON

MW 11

1024-1003

Tubing TypeACUITYESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:MILEJCZAK Pump Model/Type

Reference 45 Page 16

Page 17: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

04/02/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 21 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 802.71 [mL]

24.45 [ft] Calculated Sample Rate 322 [sec]10 [ft] Sample rate 322 [sec]5 [in] 0 [in]

14.02 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-0.03 +/-0.1 +/-0.1 +/-10+/-3 % +/-10 % +/-10 %

11:18:27 12.73 7.32 577.11 64.30 5.90 0.1211:22:19 12.75 7.31 577.51 59.96 5.83 0.1211:26:07 12.78 7.31 577.82 54.06 5.79 0.1211:29:08 12.83 7.31 578.33 49.37 5.75 0.1211:31:34 12.86 7.31 578.74 45.82 5.74 0.1211:26:07 0.03 0.00 0.31 -5.91 -0.04 0.0011:29:08 0.05 0.00 0.51 -4.68 -0.04 0.0011:31:34 0.04 0.00 0.41 -3.55 -0.01 0.00

Notes:

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:MILEJCZAK Pump Model/Type

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

Tubing LengthTubing Diameter

BLADDER pumpTEFLON

MW 12

1024-1003

Tubing TypeACUITYESComponent Machine

51 degrees F Duplicate taken

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Reference 45 Page 17

Page 18: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

04/03/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 25 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 841.32 [mL]

24.46 [ft] Calculated Sample Rate 337 [sec]10 [ft] Sample rate 337 [sec]5 [in] 0 [in]

12.47 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-0.03 +/-0.1 +/-0.1 +/-10+/-3 % +/-10 % +/-10 %

10:52:15 15.10 7.44 628.82 100.51 6.28 0.1310:58:04 14.21 7.43 613.61 103.28 6.40 0.1411:03:53 14.02 7.44 608.82 92.09 6.56 0.1411:09:43 14.05 7.44 609.29 77.66 6.55 0.1411:18:48 14.15 7.44 612.73 57.88 6.30 0.1411:03:53 -0.19 0.00 -4.79 -11.19 0.16 0.0011:09:43 0.03 0.00 0.47 -14.43 -0.01 0.0011:18:48 0.10 0.00 3.44 -19.78 -0.25 0.00

Notes: 63 degrees F

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

BLADDER pumpTEFLON

MW 13

1024-1003

Tubing TypeACUITYESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:MILEJCZAK Pump Model/Type

Reference 45 Page 18

Page 19: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

04/03/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 25 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 841.32 [mL]

24.63 [ft] Calculated Sample Rate 337 [sec]10 [ft] Sample rate 337 [sec]5 [in] 0 [in]

12.12 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-0.03 +/-0.1 +/-0.1 +/-10+/-3 % +/-10 % +/-10 %

15:01:06 23.99 7.31 835.67 86.88 3.14 0.1215:06:55 22.65 7.29 811.41 76.10 3.01 0.1215:12:44 22.01 7.28 798.32 65.51 2.93 0.1215:18:34 21.84 7.27 799.08 58.77 2.75 0.1215:24:23 21.66 7.26 801.42 60.06 2.59 0.1215:12:44 -0.64 -0.01 -13.09 -10.59 -0.08 0.0015:18:34 -0.18 -0.01 0.76 -6.74 -0.18 0.0015:24:23 -0.17 -0.01 2.34 1.29 -0.16 0.00

Notes: 73 degrees F

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

BLADDER pumpTEFLON

MW 14

1024-1003

Tubing TypeACUITYESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:MILEJCZAK Pump Model/Type

Reference 45 Page 19

Page 20: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

04/03/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 25 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 841.32 [mL]

24.61 [ft] Calculated Sample Rate 337 [sec]10 [ft] Sample rate 337 [sec]5 [in] 0 [in]

12.83 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-0.03 +/-0.1 +/-0.1 +/-10+/-3 % +/-10 % +/-10 %

14:16:55 21.59 7.38 779.79 315.62 1.17 0.1214:22:43 21.22 7.38 767.89 269.69 1.25 0.1214:28:33 21.18 7.37 763.95 186.13 1.40 0.1214:32:05 21.18 7.37 762.34 168.35 1.45 0.1214:37:11 21.39 7.37 763.76 140.28 1.46 0.1214:28:33 -0.04 0.00 -3.95 -83.57 0.15 0.0014:32:05 -0.01 0.00 -1.60 -17.78 0.05 0.0014:37:11 0.21 0.00 1.42 -28.07 0.01 0.00

Notes: 73 degrees F

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

BLADDER pumpTEFLON

MW 15

1024-1003

Tubing TypeACUITYESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:MILEJCZAK Pump Model/Type

Reference 45 Page 20

Page 21: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

04/03/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 25 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 841.32 [mL]

24.62 [ft] Calculated Sample Rate 337 [sec]10 [ft] Sample rate 337 [sec]5 [in] 0 [in]

12.7 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-0.03 +/-0.1 +/-0.1 +/-10+/-3 % +/-10 % +/-10 %

13:27:14 18.84 7.28 757.98 93.19 0.59 0.1313:33:03 18.85 7.27 759.03 78.08 0.58 0.1313:38:52 18.95 7.27 762.38 70.09 0.57 0.1313:44:42 18.79 7.27 762.20 51.80 0.60 0.1213:50:31 18.94 7.26 764.52 50.65 0.59 0.1213:38:52 0.09 -0.01 3.36 -8.00 -0.01 0.0013:44:42 -0.16 0.00 -0.18 -18.29 0.03 0.0013:50:31 0.15 0.00 2.32 -1.15 -0.01 0.00

Notes: 73 degrees F

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

BLADDER pumpTEFLON

MW 16

1024-1003

Tubing TypeACUITYESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:MILEJCZAK Pump Model/Type

Reference 45 Page 21

Page 22: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

04/02/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 28 [ft]

5 [ft]

Well ID 150 [mL/min]1 [in] 870.28 [mL]

24.66 [ft] Calculated Sample Rate 349 [sec]10 [ft] Sample rate 349 [sec]5 [in] 0 [in]

14.76 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-0.03 +/-0.1 +/-0.1 +/-10+/-3 % +/-10 % +/-10 %

14:19:07 13.51 7.34 609.06 290.94 7.58 0.1314:22:02 13.54 7.33 619.00 197.35 7.51 0.1314:26:06 13.54 7.33 621.00 121.56 7.44 0.1314:29:50 13.47 7.32 620.29 91.29 7.39 0.1314:32:48 13.45 7.33 624.44 67.92 7.39 0.1314:26:06 0.00 -0.01 2.00 -75.78 -0.07 0.0014:29:50 -0.07 0.00 -0.71 -30.27 -0.05 0.0014:32:48 -0.02 0.01 4.15 -23.37 0.00 0.00

Notes: 57 degrees F

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

BLADDER pumpTEFLON

MW 8

1024-1003

Tubing TypeACUITYESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:MILEJCZAK Pump Model/Type

Reference 45 Page 22

Page 23: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

04/02/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 21 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 802.71 [mL]

18.2 [ft] Calculated Sample Rate 322 [sec]10 [ft] Sample rate 322 [sec]5 [in] 0 [in]

15.48 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-0.03 +/-0.1 +/-0.1 +/-10+/-3 % +/-10 % +/-10 %

10:34:46 11.79 7.22 658.64 43.46 4.42 0.1110:38:23 11.83 7.23 656.38 29.06 4.17 0.1110:41:46 11.84 7.23 657.56 26.31 3.96 0.1210:45:35 11.84 7.25 654.13 17.33 3.91 0.1210:48:16 11.85 7.27 653.86 13.13 3.85 0.1210:41:46 0.01 0.00 1.18 -2.76 -0.21 0.0010:45:35 0.00 0.02 -3.43 -8.98 -0.05 0.0010:48:16 0.01 0.01 -0.27 -4.20 -0.07 0.00

Notes: 51 degrees F

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

PERISTALTIC pumpTEFLON

MW 9

1024-1003

Tubing TypeACUITYESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:MILEJCZAK Pump Model/Type

Reference 45 Page 23

Page 24: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

04/02/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 21 [ft]

5 [ft]

Well ID 150 [mL/min]2 [in] 802.71 [mL]

23.46 [ft] Calculated Sample Rate 322 [sec]10 [ft] Sample rate 322 [sec]5 [in] 0 [in]

15.9 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-0.03 +/-0.1 +/-0.1 +/-10+/-3 % +/-10 % +/-10 %

9:53:41 13.07 7.35 585.20 19.78 7.41 0.109:56:14 13.24 7.35 584.46 17.07 7.39 0.109:58:59 13.27 7.34 584.76 16.06 7.35 0.10

10:01:28 13.38 7.34 586.23 16.08 7.35 0.1010:04:27 13.12 7.33 586.32 18.96 7.34 0.109:58:59 0.03 -0.01 0.30 -1.00 -0.04 0.00

10:01:28 0.12 0.00 1.46 0.02 0.00 0.0010:04:27 -0.26 0.00 0.10 2.88 -0.01 0.00

Notes: 51 degrees F MS/MSD TAKEN

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

geocontrol bladder pumpTEFLON

PMW 1

1024-1003

Tubing TypeACUITYESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:MILEJCZAK Pump Model/Type

Reference 45 Page 24

Page 25: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

04/02/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 21 [ft]

5 [ft]

Well ID 150 [mL/min]2 [in] 802.71 [mL]

21.41 [ft] Calculated Sample Rate 322 [sec]10 [ft] Sample rate 322 [sec]5 [in] 0 [in]

13.72 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-0.03 +/-0.1 +/-0.1 +/-10+/-3 % +/-10 % +/-10 %

12:02:47 15.39 7.27 656.58 84.29 0.90 0.1212:05:59 15.47 7.27 658.05 76.48 0.79 0.1212:08:43 15.58 7.27 660.72 76.14 0.74 0.1212:11:13 15.59 7.27 662.20 74.23 0.69 0.1212:14:39 15.67 7.26 664.49 84.61 0.62 0.1212:08:43 0.11 0.00 2.67 -0.34 -0.05 0.0012:11:13 0.01 0.00 1.48 -1.91 -0.05 0.0012:14:39 0.09 0.00 2.30 10.38 -0.07 0.00

Notes: 52 degrees F

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

BLADDER pumpTEFLON

PMW 4

1024-1003

Tubing TypeACUITYESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:MILEJCZAK Pump Model/Type

Reference 45 Page 25

Page 26: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

04/02/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 21 [ft]

5 [ft]

Well ID 150 [mL/min]2 [in] 802.71 [mL]

20.91 [ft] Calculated Sample Rate 322 [sec]10 [ft] Sample rate 322 [sec]5 [in] 0 [in]

13.73 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-0.03 +/-0.1 +/-0.1 +/-10+/-3 % +/-10 % +/-10 %

13:36:49 15.60 7.36 703.10 19.01 4.08 0.1313:39:51 15.58 7.36 702.49 19.31 4.05 0.1313:43:04 15.55 7.36 702.33 15.08 4.03 0.1313:48:22 15.58 7.36 703.38 15.42 4.02 0.1313:52:06 15.59 7.35 705.21 13.49 4.02 0.1313:43:04 -0.03 0.00 -0.16 -4.23 -0.02 0.0013:48:22 0.03 0.00 1.05 0.34 -0.01 0.0013:52:06 0.02 0.00 1.82 -1.94 0.00 0.00

Notes: 57 degrees F

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

BLADDER pumpTEFLON

PMW 5

1024-1003

Tubing TypeACUITYESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:MILEJCZAK Pump Model/Type

Reference 45 Page 26

Page 27: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

04/03/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 18 [ft]

5 [ft]

Well ID 150 [mL/min]2 [in] 773.75 [mL]

21.11 [ft] Calculated Sample Rate 310 [sec]10 [ft] Sample rate 310 [sec]5 [in] 0 [in]

13.1 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-0.03 +/-0.1 +/-0.1 +/-10+/-3 % +/-10 % +/-10 %

9:57:56 13.26 7.27 692.95 27.31 3.39 0.1110:03:17 13.13 7.26 690.31 31.47 3.05 0.1210:06:42 13.10 7.26 689.29 36.05 2.94 0.1210:12:04 13.12 7.26 689.73 36.06 2.82 0.1210:17:25 13.14 7.26 689.87 32.83 2.76 0.1210:06:42 -0.03 0.00 -1.02 4.58 -0.11 0.0010:12:04 0.03 0.00 0.44 0.01 -0.12 0.0010:17:25 0.02 0.00 0.15 -3.23 -0.05 0.00

Notes: 60 degrees F

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

BLADDER pumpTEFLON

PMW 6

1024-1003

Tubing TypeACUITYESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:MILEJCZAK Pump Model/Type

Reference 45 Page 27

Page 28: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

06/07/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 22 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 762.36 [mL]

17.75 [ft] Calculated Sample Rate 305 [sec]5 [ft] Sample rate 305 [sec]

120 [in] 4 [in]16.63 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

11:51:03 20.29 7.13 811.02 186.43 1.81 128.1411:53:53 19.32 7.20 794.06 145.01 1.87 128.8411:56:39 19.08 7.22 788.27 46.46 1.87 126.0511:59:12 19.12 7.22 790.39 43.35 1.83 122.4112:01:50 19.43 7.22 796.05 48.27 1.78 117.8411:56:39 -0.23 0.02 -5.79 -98.56 0.00 -2.7811:59:12 0.03 0.00 2.12 -3.11 -0.04 -3.6412:01:50 0.31 0.00 5.66 4.92 -0.06 -4.57

Notes: sample taken at 1205

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

Peristaltic pumpTLPE

MW-10

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 28

Page 29: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

06/07/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 20 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 743.06 [mL]

17.93 [ft] Calculated Sample Rate 298 [sec]5 [ft] Sample rate 298 [sec]

120 [in] 4 [in]15.57 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

13:47:09 20.39 7.05 797.58 54.43 2.03 133.7213:49:22 19.88 7.04 789.90 45.61 1.57 119.2213:51:30 19.59 7.04 784.01 35.78 1.25 105.0113:53:42 19.31 7.04 778.80 29.62 1.03 91.4913:55:55 19.11 7.04 775.12 26.64 0.90 79.1213:51:30 -0.29 0.00 -5.89 -9.83 -0.32 -14.2113:53:42 -0.29 0.00 -5.21 -6.15 -0.22 -13.5213:55:55 -0.19 0.00 -3.68 -2.98 -0.13 -12.37

Notes: sample taken at 1400

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

bladder pumpTLPE

MW-11

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 29

Page 30: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

06/07/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 26 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 800.97 [mL]

24.17 [ft] Calculated Sample Rate 321 [sec]5 [ft] Sample rate 321 [sec]

120 [in] 4 [in]14.88 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

12:55:18 20.35 7.29 762.80 83.20 5.61 180.6612:57:49 19.34 7.28 745.78 72.36 5.46 179.6613:00:18 18.70 7.27 731.98 68.67 5.38 178.5213:03:07 18.28 7.26 723.51 65.12 5.26 177.0413:05:37 18.09 7.26 716.34 53.24 5.25 175.5613:00:18 -0.63 -0.01 -13.79 -3.69 -0.08 -1.1413:03:07 -0.43 -0.01 -8.47 -3.55 -0.12 -1.4813:05:37 -0.19 -0.01 -7.16 -11.87 -0.01 -1.48

Notes: sample taken at 1305

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

Peristaltic pumpTLPE

MW-12

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 30

Page 31: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

06/08/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 21 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 752.71 [mL]

19.25 [ft] Calculated Sample Rate 302 [sec]5 [ft] Sample rate 302 [sec]

120 [in] 4 [in]13.32 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

11:44:26 23.02 7.32 836.73 30.22 5.31 146.8011:46:25 22.73 7.31 843.23 27.96 5.10 143.8711:48:28 22.72 7.30 848.44 26.04 4.86 140.9711:50:28 22.65 7.28 854.60 26.32 4.68 138.5811:52:28 22.67 7.27 859.95 22.32 4.26 135.9811:48:28 -0.02 -0.01 5.21 -1.93 -0.24 -2.9011:50:28 -0.07 -0.01 6.16 0.28 -0.18 -2.3911:52:28 0.03 -0.01 5.35 -4.00 -0.41 -2.60

Notes: sample taken at 1220

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

bladder pumpTLPE

MW-13

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 31

Page 32: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

06/08/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 26 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 800.97 [mL]

24.3 [ft] Calculated Sample Rate 321 [sec]5 [ft] Sample rate 321 [sec]

120 [in] 4 [in]12.95 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

11:15:43 20.97 7.30 855.69 146.64 2.03 169.3311:18:07 20.53 7.28 851.07 122.33 1.39 167.3711:20:33 20.27 7.26 846.49 112.51 1.11 165.1111:23:15 20.08 7.26 840.41 113.71 1.02 162.4211:25:39 20.00 7.26 834.60 98.82 1.03 160.0711:20:33 -0.27 -0.01 -4.58 -9.82 -0.28 -2.2611:23:15 -0.18 -0.01 -6.08 1.20 -0.08 -2.6911:25:39 -0.08 0.00 -5.81 -14.90 0.01 -2.35

Notes: sample taken at 1125

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

bladder pumpTLPE

MW-14

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 32

Page 33: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

06/08/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 26 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 800.97 [mL]

24.28 [ft] Calculated Sample Rate 321 [sec]5 [ft] Sample rate 321 [sec]

120 [in] 4 [in]13.77 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

10:50:58 19.19 7.32 697.76 248.83 2.33 164.8210:53:52 19.17 7.31 691.76 191.94 2.44 164.6610:56:15 19.16 7.31 688.50 128.11 2.51 164.5310:59:25 19.18 7.31 685.85 98.99 2.58 164.1911:00:50 19.21 7.31 686.31 87.46 2.60 164.1110:56:15 -0.01 0.00 -3.25 -63.83 0.06 -0.1210:59:25 0.02 0.00 -2.65 -29.12 0.07 -0.3411:00:50 0.03 0.00 0.46 -11.53 0.02 -0.08

Notes: sample taken at 1100

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

bladder pumpTLPE

MW-15

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 33

Page 34: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

06/08/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 26 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 800.97 [mL]

24.35 [ft] Calculated Sample Rate 321 [sec]5 [ft] Sample rate 321 [sec]

120 [in] 4 [in]13.67 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

10:10:03 19.78 7.31 772.46 159.44 1.36 177.3310:12:48 19.41 7.28 765.48 157.51 1.19 174.8210:15:30 19.27 7.27 758.78 163.32 1.13 172.3410:18:21 19.14 7.26 755.24 140.31 1.12 169.1710:20:56 19.08 7.25 753.00 129.68 1.13 166.0310:15:30 -0.14 -0.02 -6.70 5.81 -0.06 -2.4810:18:21 -0.13 -0.01 -3.53 -23.02 -0.01 -3.1710:20:56 -0.06 -0.01 -2.25 -10.63 0.01 -3.14

Notes: sample taken at 1025

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

bladder pumpTLPE

MW-16

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 34

Page 35: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

06/07/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 23 [ft]

5 [ft]

Well ID 150 [mL/min]2 [in] 772.01 [mL]

21.06 [ft] Calculated Sample Rate 309 [sec]5 [ft] Sample rate 309 [sec]

120 [in] 4 [in]13.94 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

13:21:32 18.42 7.23 780.75 28.73 4.08 171.5913:23:50 17.94 7.22 773.86 29.76 3.58 170.0713:26:07 17.60 7.21 770.54 35.66 3.38 167.7413:28:23 17.46 7.20 768.25 41.79 3.24 165.3813:30:41 17.30 7.20 763.82 39.49 3.22 163.8413:26:07 -0.34 -0.01 -3.32 5.89 -0.20 -2.3313:28:23 -0.14 -0.01 -2.29 6.13 -0.13 -2.3613:30:41 -0.16 -0.01 -4.42 -2.30 -0.03 -1.55

Notes: sample taken at 1335

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

Peristaltic pumpTLPE

MW-6

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 35

Page 36: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

06/07/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 25 [ft]

5 [ft]

Well ID 150 [mL/min]1 [in] 791.32 [mL]

24.57 [ft] Calculated Sample Rate 317 [sec]5 [ft] Sample rate 317 [sec]

120 [in] 4 [in]15.64 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

10:03:49 16.66 7.25 698.76 209.15 5.50 185.3010:07:22 16.25 7.26 689.14 108.05 5.49 185.2110:09:58 15.94 7.26 686.50 86.71 5.42 184.8610:11:51 15.84 7.24 684.90 81.89 5.44 184.5110:12:19 15.80 7.25 684.67 76.23 5.37 184.4710:09:58 -0.31 0.00 -2.65 -21.35 -0.07 -0.3510:11:51 -0.10 -0.02 -1.60 -4.81 0.02 -0.3510:12:19 -0.04 0.01 -0.23 -5.67 -0.07 -0.04

Notes: sample taken at 1010

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

ontrol Pro Bladder PumpTLPE skip bonded

MW-8

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 36

Page 37: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

06/07/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 22 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 762.36 [mL]

18.26 [ft] Calculated Sample Rate 305 [sec]5 [ft] Sample rate 305 [sec]

120 [in] 4 [in]16.41 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

11:18:21 20.04 7.09 1125.22 63.37 0.53 160.8311:20:58 19.84 7.10 1125.48 36.04 0.47 153.1911:23:11 19.72 7.11 1114.15 34.92 0.42 146.5611:26:02 19.66 7.12 1117.77 27.37 0.38 138.4811:28:15 19.68 7.12 1116.54 17.72 0.35 132.2411:23:11 -0.11 0.01 -11.32 -1.11 -0.05 -6.6311:26:02 -0.06 0.01 3.62 -7.55 -0.04 -8.0811:28:15 0.02 0.00 -1.23 -9.64 -0.04 -6.25

Notes: sample taken at 1130

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

Peristaltic pumpTLPE

MW-9

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 37

Page 38: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

06/07/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 23 [ft]

5 [ft]

Well ID 150 [mL/min]2 [in] 772.01 [mL]

23.24 [ft] Calculated Sample Rate 309 [sec]5 [ft] Sample rate 309 [sec]

120 [in] 4 [in]16.74 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

10:36:11 18.19 7.24 664.91 36.97 7.15 181.4110:38:40 17.75 7.23 662.34 42.88 7.10 181.0710:40:57 17.45 7.23 658.94 34.29 7.07 180.7210:43:20 17.20 7.23 657.26 36.60 7.01 180.3310:45:40 17.09 7.23 657.79 30.45 6.98 179.7710:40:57 -0.30 0.00 -3.40 -8.58 -0.04 -0.3510:43:20 -0.25 0.00 -1.68 2.31 -0.05 -0.3910:45:40 -0.11 0.00 0.53 -6.14 -0.04 -0.56

Notes: sample taken at 1045. MS/MSD TAKEN

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

ontrol Pro Bladder PumpTLPE skip bonded

PMW-1

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 38

Page 39: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

06/07/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 22 [ft]

5 [ft]

Well ID 150 [mL/min]2 [in] 762.36 [mL]

21.43 [ft] Calculated Sample Rate 305 [sec]10 [ft] Sample rate 305 [sec]60 [in] 4 [in]

14.58 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

8:43:04 18.65 7.22 1018.55 80.37 1.77 162.478:45:38 18.67 7.21 1018.00 68.20 1.81 163.488:48:01 18.69 7.21 1017.46 57.74 1.92 164.148:50:33 18.72 7.20 1017.67 49.84 2.03 164.558:52:44 18.77 7.20 1020.42 43.29 2.16 164.878:48:01 0.02 0.00 -0.54 -10.47 0.11 0.678:50:33 0.03 0.00 0.21 -7.90 0.11 0.418:52:44 0.06 0.00 2.75 -6.55 0.13 0.32

Notes: sample taken at 0855. DUPLICATE TAKEN

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

ontrol Pro Bladder PumpTLPE skip bonded

PMW-4

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 39

Page 40: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

06/07/12

Operator NameCompany NameProject Name 0.25 [in]Site Name 22 [ft]

5 [ft]

Well ID 150 [mL/min]2 [in] 762.36 [mL]

20.93 [ft] Calculated Sample Rate 305 [sec]5 [ft] Sample rate 305 [sec]

120 [in] 4 [in]14.62 [ft]

Time Temp [C] pH [pH] Cond [µS/cm] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

9:18:11 17.95 7.38 716.74 88.18 5.80 173.139:20:26 17.69 7.35 701.06 77.67 5.70 172.859:22:51 17.54 7.34 694.77 68.65 5.67 172.609:25:04 17.41 7.33 689.16 57.13 5.66 172.399:27:31 17.39 7.32 686.73 42.71 5.64 172.109:22:51 -0.16 -0.01 -6.30 -9.02 -0.03 -0.259:25:04 -0.13 -0.01 -5.61 -11.52 -0.01 -0.219:27:31 -0.02 -0.01 -2.43 -14.42 -0.02 -0.29

Notes: sample taken at 0930

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

ontrol Pro Bladder PumpTLPE skip bonded

PMW-5

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 40

Page 41: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

09/17/12

Operator NameCompany NameProject Name 0.38 [in]Site Name 21 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 1018.34 [mL]

17.71 [ft] Calculated Sample Rate 408 [sec]5 [ft] Sample rate 408 [sec]

15 [in] 4 [in]16.06 [ft]

Time Temp [C] pH [pH] Cond [µS/cm @25C] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

13:37:30 22.56 7.01 1108.40 108.32 1.27 136.0113:38:53 22.57 7.00 1110.05 108.75 1.24 135.2413:43:03 22.63 6.99 1110.04 57.51 1.16 133.2913:46:36 22.67 6.99 1112.09 64.83 1.14 131.6313:49:18 22.54 6.98 1117.58 33.40 1.12 130.7813:43:03 0.05 -0.01 0.00 -51.24 -0.08 -1.9613:46:36 0.04 0.00 2.04 7.32 -0.02 -1.6613:49:18 -0.12 -0.01 5.49 -31.43 -0.02 -0.85

Notes: sampled at 1358

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

bladderhdpe

MW-10

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 41

Page 42: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

09/17/12

Operator NameCompany NameProject Name 0.38 [in]Site Name 23 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 1062.94 [mL]

21.11 [ft] Calculated Sample Rate 426 [sec]5 [ft] Sample rate 426 [sec]

15 [in] 4 [in]13.36 [ft]

Time Temp [C] pH [pH] Cond [µS/cm @25C] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

10:30:26 19.57 7.06 896.16 176.95 4.05 117.2510:32:01 19.51 7.06 894.98 142.98 4.11 117.8510:35:05 19.44 7.05 893.67 87.56 4.15 119.1310:38:17 19.40 7.05 892.57 56.98 4.35 120.0310:41:23 19.37 7.05 891.85 48.97 4.38 120.8810:35:05 -0.07 -0.01 -1.32 -55.42 0.04 1.2810:38:17 -0.04 0.00 -1.10 -30.58 0.20 0.9010:41:23 -0.03 0.00 -0.71 -8.01 0.03 0.86

Notes: sampled at 1050. Duplicate taken.

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

bladderhdpe

mw-11

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 42

Page 43: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

09/18/12

Operator NameCompany NameProject Name 0.38 [in]Site Name 26 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 1129.85 [mL]

24.41 [ft] Calculated Sample Rate 452 [sec]5 [ft] Sample rate 452 [sec]

15 [in] 4 [in]14.27 [ft]

Time Temp [C] pH [pH] Cond [µS/cm @25C] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

12:41:27 18.35 7.10 860.94 167.84 3.56 193.1312:43:08 18.28 7.10 860.35 140.37 3.55 193.2212:46:05 18.07 7.09 860.62 121.34 3.54 193.1812:50:18 17.82 7.09 860.40 81.98 3.54 192.9212:52:05 17.91 7.08 862.38 92.72 3.54 192.7512:46:05 -0.21 0.00 0.28 -19.03 0.00 -0.0412:50:18 -0.25 -0.01 -0.23 -39.35 0.00 -0.2612:52:05 0.09 0.00 1.98 10.73 -0.01 -0.17

Notes: sampled at 1255

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

bladderhdpe

MW-12

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 43

Page 44: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

09/18/12

Operator NameCompany NameProject Name 0.38 [in]Site Name 26 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 1129.85 [mL]

24.47 [ft] Calculated Sample Rate 452 [sec]5 [ft] Sample rate 452 [sec]

15 [in] 4 [in]12.75 [ft]

Time Temp [C] pH [pH] Cond [µS/cm @25C] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

15:32:57 24.86 7.26 939.60 121.85 4.22 145.9915:33:57 24.88 7.25 937.77 114.66 4.18 145.9515:37:36 24.97 7.24 935.32 72.07 4.04 145.6415:40:04 25.03 7.24 933.56 62.05 4.00 145.3015:43:09 25.05 7.24 931.58 59.45 3.88 144.6715:37:36 0.09 -0.01 -2.46 -42.59 -0.14 -0.3015:40:04 0.07 0.00 -1.76 -10.03 -0.04 -0.3415:43:09 0.01 0.00 -1.98 -2.59 -0.11 -0.64

Notes: sampled at 1550

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

bladderhdpe

MW-13

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 44

Page 45: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

09/18/12

Operator NameCompany NameProject Name 0.38 [in]Site Name 26 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 1129.85 [mL]

24.52 [ft] Calculated Sample Rate 452 [sec]5 [ft] Sample rate 452 [sec]

15 [in] 4 [in]12.44 [ft]

Time Temp [C] pH [pH] Cond [µS/cm @25C] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

14:54:40 22.32 7.25 884.66 384.34 2.70 152.4014:58:03 22.22 7.20 887.91 384.60 2.48 152.4115:00:44 22.22 7.18 888.22 266.28 2.48 152.2915:04:04 21.96 7.17 887.54 182.54 2.55 152.0315:07:29 21.81 7.16 888.28 170.38 2.73 151.5115:00:44 0.00 -0.02 0.31 -118.32 -0.01 -0.1215:04:04 -0.26 -0.01 -0.69 -83.74 0.07 -0.2615:07:29 -0.15 0.00 0.74 -12.16 0.18 -0.52

Notes: sampled at 1510

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

bladderhdpe

MW-14

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 45

Page 46: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

09/18/12

Operator NameCompany NameProject Name 0.38 [in]Site Name 26 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 1129.85 [mL]

24.53 [ft] Calculated Sample Rate 452 [sec]5 [ft] Sample rate 452 [sec]

15 [in] 4 [in]13.18 [ft]

Time Temp [C] pH [pH] Cond [µS/cm @25C] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

14:24:59 20.48 7.29 854.43 976.77 1.54 151.4614:27:41 20.44 7.27 848.58 697.30 2.14 150.9914:31:35 20.15 7.26 841.27 475.42 2.83 150.9414:33:46 20.07 7.25 838.44 397.40 3.00 151.0614:36:33 20.12 7.25 835.62 294.95 3.14 151.2714:31:35 -0.29 -0.01 -7.31 -221.87 0.69 -0.0514:33:46 -0.09 -0.01 -2.83 -78.03 0.18 0.1214:36:33 0.05 0.00 -2.82 -102.45 0.14 0.21

Notes:

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

Tubing LengthTubing Diameter

bladderhdpe

MW-15

1024-1003

Tubing TypeAcuityESComponent Machine

sampled at 1450

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Reference 45 Page 46

Page 47: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

09/18/12

Operator NameCompany NameProject Name 0.38 [in]Site Name 26 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 1129.85 [mL]

24.54 [ft] Calculated Sample Rate 452 [sec]5 [ft] Sample rate 452 [sec]

15 [in] 4 [in]13.11 [ft]

Time Temp [C] pH [pH] Cond [µS/cm @25C] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

13:53:36 20.73 7.19 835.67 295.74 1.33 156.1313:56:44 20.60 7.17 827.17 205.12 1.25 155.3613:59:44 20.91 7.15 818.75 187.40 1.33 154.8414:02:41 21.12 7.14 809.81 159.48 1.46 154.0814:05:58 21.24 7.14 802.11 183.19 1.58 153.1613:59:44 0.31 -0.02 -8.42 -17.71 0.08 -0.5114:02:41 0.21 -0.01 -8.94 -27.92 0.13 -0.7614:05:58 0.12 -0.01 -7.70 23.70 0.12 -0.93

Notes: sampled at 1425

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

bladderhdpe

MW-16

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 47

Page 48: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

09/17/12

Operator NameCompany NameProject Name 0.38 [in]Site Name 27 [ft]

5 [ft]

Well ID 150 [mL/min]1 [in] 1152.15 [mL]

24.54 [ft] Calculated Sample Rate 461 [sec]5 [ft] Sample rate 461 [sec]

15 [in] 4 [in]15.06 [ft]

Time Temp [C] pH [pH] Cond [µS/cm @25C] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

12:26:26 21.43 6.96 1102.47 108.17 3.15 134.4812:29:22 21.33 6.95 1097.05 84.86 3.11 134.8212:32:21 21.24 6.96 1092.69 77.74 3.09 134.7412:35:45 21.25 6.95 1088.91 54.75 3.06 134.6112:38:21 21.14 6.95 1089.88 47.53 3.04 134.7412:32:21 -0.09 0.00 -4.36 -7.12 -0.03 -0.0812:35:45 0.02 -0.01 -3.77 -22.99 -0.02 -0.1312:38:21 -0.11 0.00 0.96 -7.21 -0.02 0.13

Notes: sampled at 1238

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

bladderhdpe

MW-8

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 48

Page 49: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

09/18/12

Operator NameCompany NameProject Name 0.38 [in]Site Name 20 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 996.04 [mL]

18.17 [ft] Calculated Sample Rate 399 [sec]5 [ft] Sample rate 399 [sec]

15 [in] 4 [in]15.8 [ft]

Time Temp [C] pH [pH] Cond [µS/cm @25C] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

13:19:02 22.74 6.99 1095.37 12.00 1.48 176.7513:21:28 22.90 6.99 1092.52 11.35 1.32 173.3013:23:34 22.84 6.98 1088.70 6.86 1.14 170.7913:24:02 22.80 6.99 1087.53 9.63 1.12 170.1913:27:56 22.97 7.00 1076.09 7.30 0.92 166.1413:23:34 -0.06 0.00 -3.82 -4.49 -0.18 -2.5113:24:02 -0.04 0.00 -1.18 2.77 -0.02 -0.6013:27:56 0.17 0.02 -11.43 -2.32 -0.20 -4.05

Notes: sampled at 1330

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

bladderhdpe

MW-9

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 49

Page 50: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

09/17/12

Operator NameCompany NameProject Name 0.38 [in]Site Name 26 [ft]

5 [ft]

Well ID 150 [mL/min]1 [in] 1129.85 [mL]

23.18 [ft] Calculated Sample Rate 452 [sec]5 [ft] Sample rate 452 [sec]

15 [in] 4 [in]16.21 [ft]

Time Temp [C] pH [pH] Cond [µS/cm @25C] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

13:01:12 19.34 7.10 768.20 25.71 6.76 139.8613:03:07 19.28 7.09 768.57 26.62 6.69 140.7513:07:22 19.14 7.08 770.75 19.62 6.51 142.1613:10:03 19.09 7.08 771.33 21.56 6.49 142.5813:12:58 19.01 7.08 772.39 20.39 6.45 142.8013:07:22 -0.13 -0.01 2.18 -7.01 -0.18 1.4113:10:03 -0.06 0.00 0.58 1.94 -0.02 0.4313:12:58 -0.07 0.00 1.05 -1.17 -0.04 0.21

Notes: sampled at 1325

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

bladderhdpe

PMW-1

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 50

Page 51: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

09/17/12

Operator NameCompany NameProject Name 0.38 [in]Site Name 23 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 1062.94 [mL]

21.46 [ft] Calculated Sample Rate 426 [sec]5 [ft] Sample rate 426 [sec]

15 [in] 4 [in]14.03 [ft]

Time Temp [C] pH [pH] Cond [µS/cm @25C] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

11:04:42 20.76 7.68 1320.22 83.93 1.83 113.6011:07:46 20.57 7.73 1330.18 51.02 1.72 110.1411:10:43 20.47 7.75 1333.61 38.05 1.61 107.3611:12:41 20.40 7.75 1336.53 30.02 1.68 106.2511:16:46 20.34 7.76 1341.15 22.85 1.71 103.8111:10:43 -0.09 0.03 3.44 -12.97 -0.11 -2.7811:12:41 -0.08 0.00 2.91 -8.03 0.06 -1.1111:16:46 -0.06 0.00 4.62 -7.17 0.04 -2.44

Notes: sampled at 1120

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

bladderhdpe

PMW-4

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 51

Page 52: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

09/17/12

Operator NameCompany NameProject Name 0.38 [in]Site Name 22 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 1040.64 [mL]

20.92 [ft] Calculated Sample Rate 417 [sec]5 [ft] Sample rate 417 [sec]

15 [in] 4 [in]14.07 [ft]

Time Temp [C] pH [pH] Cond [µS/cm @25C] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

11:33:42 19.51 7.30 906.06 91.94 2.35 112.4011:36:15 19.39 7.25 895.95 50.36 2.46 113.0011:39:19 19.33 7.21 889.88 34.75 2.63 114.2011:42:17 19.30 7.19 886.80 28.65 2.81 114.8811:46:08 19.25 7.18 885.85 23.78 2.99 115.9911:39:19 -0.06 -0.04 -6.07 -15.61 0.16 1.2011:42:17 -0.03 -0.02 -3.08 -6.10 0.18 0.6811:46:08 -0.05 -0.01 -0.95 -4.87 0.19 1.11

Notes: sampled at 1155. MS/MSD TAKEN

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

bladderhdpe

PMW-5

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 52

Page 53: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

09/17/12

Operator NameCompany NameProject Name 0.38 [in]Site Name 20 [ft]

5 [ft]

Well ID 150 [mL/min]1.5 [in] 996.04 [mL]

18.08 [ft] Calculated Sample Rate 399 [sec]5 [ft] Sample rate 399 [sec]

15 [in] 4 [in]13 [ft]

Time Temp [C] pH [pH] Cond [µS/cm @25C] Turb [NTU] RDO [mg/L] ORP [mV]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

9:55:18 19.78 6.92 992.53 79.94 2.17 111.989:58:08 19.78 6.91 992.49 52.91 2.23 109.64

10:00:57 19.79 6.89 992.47 49.85 2.20 108.2410:04:08 19.78 6.88 992.89 32.07 2.23 106.7110:07:07 19.82 6.88 989.98 24.59 2.25 105.8210:00:57 0.00 -0.02 -0.02 -3.05 -0.03 -1.4010:04:08 0.00 -0.01 0.42 -17.79 0.02 -1.5310:07:07 0.04 0.00 -2.91 -7.48 0.02 -0.89

Notes: sampled at 1010

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

bladderhdpe

pmw-6

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:Milejczak Pump Model/Type

Reference 45 Page 53

Page 54: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12/19/12

Operator NameCompany NameProject Name 0.17 [in]Site Name 25 [ft]

15 [ft]

Well ID 150 [mL/min]1.5 [in] 661.59 [mL]

17.71 [ft] Calculated Sample Rate 265 [sec]10 [ft] Sample rate 265 [sec]

180 [in] 3 [in]16 [ft]

Time Temp [F] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

9:23:51 54.59 7.18 688.08 115.63 4.57 0.139:24:55 54.65 7.17 688.58 110.85 4.52 0.139:26:34 54.73 7.15 690.25 100.99 4.48 0.139:28:18 54.96 7.15 691.76 93.77 4.46 0.139:29:49 55.01 7.14 692.43 90.97 4.47 0.139:26:34 0.08 -0.02 1.67 -9.87 -0.04 0.009:28:18 0.23 0.00 1.51 -7.21 -0.02 0.009:29:49 0.05 0.00 0.67 -2.80 0.01 0.00

Notes: SAMPLE @ 0940

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

peristallictlpe

MW-10

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:W Milejczak Pump Model/Type

Reference 45 Page 54

Page 55: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12/19/12

Operator NameCompany NameProject Name 0.17 [in]Site Name 25 [ft]

15 [ft]

Well ID 150 [mL/min]1.5 [in] 661.59 [mL]

18.01 [ft] Calculated Sample Rate 265 [sec]10 [ft] Sample rate 265 [sec]

180 [in] 3 [in]12.91 [ft]

Time Temp [F] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

8:59:33 57.06 6.92 839.72 134.79 0.74 0.139:01:46 57.36 6.91 843.45 105.59 0.65 0.139:03:40 57.54 6.91 846.22 86.31 0.58 0.129:05:17 57.75 6.91 848.24 71.64 0.53 0.129:07:05 57.80 6.91 849.51 90.12 0.45 0.129:03:40 0.18 0.00 2.76 -19.28 -0.07 0.009:05:17 0.21 0.00 2.02 -14.67 -0.05 0.009:07:05 0.06 0.00 1.27 18.48 -0.08 0.00

Notes: SAMPLE @ 0910

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

bladdertlpe

MW-11

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:W Milejczak Pump Model/Type

Reference 45 Page 55

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12/18/12

Operator NameCompany NameProject Name 0.17 [in]Site Name 30 [ft]

20 [ft]

Well ID 150 [mL/min]2 [in] 683.9 [mL]

24.17 [ft] Calculated Sample Rate 274 [sec]10 [ft] Sample rate 274 [sec]

180 [in] 3 [in]14.24 [ft]

Time Temp [F] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

9:46:34 59.60 7.00 662.42 31.83 5.17 0.159:51:10 59.59 7.06 662.57 26.54 5.11 0.149:55:47 59.58 7.08 662.10 21.62 5.05 0.14

10:00:24 59.70 7.10 663.33 16.34 5.01 0.1410:05:01 59.72 7.10 664.11 18.22 4.96 0.149:55:47 -0.02 0.02 -0.47 -4.92 -0.05 0.00

10:00:24 0.12 0.02 1.23 -5.28 -0.04 0.0010:05:01 0.02 0.01 0.78 1.89 -0.05 0.00

Notes: SAMPLE @ 1010MS/MSD Taken

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

BLADDERtlpe

MW-12

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:W Milejczak Pump Model/Type

Reference 45 Page 56

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12/19/12

Operator NameCompany NameProject Name 0.17 [in]Site Name 30 [ft]

15 [ft]

Well ID 150 [mL/min]1.5 [in] 683.9 [mL]

24.48 [ft] Calculated Sample Rate 274 [sec]10 [ft] Sample rate 274 [sec]

180 [in] 3 [in]12.7 [ft]

Time Temp [F] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

11:47:15 54.62 7.38 676.60 73.51 8.59 0.1111:49:16 54.66 7.38 676.28 61.53 8.60 0.1111:51:32 54.71 7.36 676.60 48.54 8.54 0.1111:53:24 54.70 7.35 675.62 53.44 8.51 0.1111:55:04 54.73 7.36 677.71 53.89 8.46 0.1111:51:32 0.05 -0.02 0.32 -12.99 -0.06 0.0011:53:24 -0.01 -0.01 -0.97 4.90 -0.03 0.0011:55:04 0.02 0.01 2.09 0.45 -0.05 0.00

Notes: SAMPLE @ 1250

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

bladdertlpe

MW-13

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:W Milejczak Pump Model/Type

Reference 45 Page 57

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12/19/12

Operator NameCompany NameProject Name 0.17 [in]Site Name 30 [ft]

20 [ft]

Well ID 150 [mL/min]1.5 [in] 683.9 [mL]

24.54 [ft] Calculated Sample Rate 274 [sec]10 [ft] Sample rate 274 [sec]

180 [in] 3 [in]12.34 [ft]

Time Temp [F] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

11:22:52 59.79 7.19 739.28 118.31 0.70 0.0911:24:59 59.80 7.19 738.51 122.96 0.54 0.0911:27:11 59.88 7.19 738.12 108.34 0.45 0.0811:28:50 59.95 7.18 737.55 100.98 0.40 0.0811:30:34 59.99 7.18 737.37 102.83 0.35 0.0811:27:11 0.08 0.00 -0.38 -14.61 -0.08 0.0011:28:50 0.07 -0.01 -0.57 -7.36 -0.05 0.0011:30:34 0.03 0.00 -0.19 1.85 -0.06 0.00

Notes: SAMPLE @ 1155

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

bladdertlpe

MW-14

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:W Milejczak Pump Model/Type

Reference 45 Page 58

Page 59: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

Operator Name:

Company Name:

Project Name:

Site Name:

Well ID:

Well diameter:

Well total depth:

Depth to top of screen:

Screen length:

Depth to Water:

Time Temp [F] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-1 +/-1 +/-1 +/-10

+/-3 % +/-10 % +/-10 %

10:59:42 59.32 7.36 627.71 161.97 0.63 0.08

11:01:39 59.56 7.35 629.81 175.86 0.57 0.08

11:03:38 59.84 7.34 632.34 148.77 0.58 0.07

11:05:38 60.03 7.34 633.62 123.45 0.77 0.07

11:07:24 60.16 7.34 634.34 100.64 0.92 0.07

11:03:38 0.28 -0.01 2.53 -27.09 0.00 0.00

11:05:38 0.19 0.00 1.28 -25.32 0.19 0.00

11:07:24 0.13 0.00 0.72 -22.81 0.15 0.00

Notes:

Stabilized drawdown:

150 [mL/min]

683.9 [mL]

274 [sec]

274 [sec]

3 [in]

Flowcell volume:

Calculated Sample Rate:

Final pumping rate:

Low-Flow Sampling Stabilization Summary

Stabilization Settings

Pump Model/Type:

MW-15

1.5 [in]

24.55 [ft]

W Milejczak

AcuityES

13.08 [ft]

Sample rate:

ISI Low-Flow Log

Troll 9000 Low-Flow System

12/19/12

Pump Information

bladder

1024-1003

Project Information

Tubing Diameter:

Tubing Type:

Component Machine

Well Information Pumping information

tlpe

SAMPLE @ 1120

0.17 [in]

30 [ft]

20 [ft]

Last 5 Readings

Variance in last 3 readings

Tubing Length:

10 [ft]

180 [in]

Pump placement from TOC:

Reference 45 Page 59

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12/19/12

Operator NameCompany NameProject Name 0.17 [in]Site Name 30 [ft]

20 [ft]

Well ID 150 [mL/min]1.5 [in] 683.9 [mL]

24.58 [ft] Calculated Sample Rate 274 [sec]10 [ft] Sample rate 274 [sec]

180 [in] 3 [in]13 [ft]

Time Temp [F] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

10:34:40 56.48 7.29 586.53 139.55 0.98 0.0710:36:37 56.56 7.27 588.11 146.99 0.85 0.0710:38:26 56.52 7.27 588.35 146.53 0.74 0.0710:41:20 56.62 7.26 588.24 124.30 0.61 0.0710:43:03 56.73 7.25 587.39 123.43 0.61 0.0710:38:26 -0.04 0.00 0.25 -0.45 -0.12 0.0010:41:20 0.10 -0.01 -0.12 -22.23 -0.13 0.0010:43:03 0.11 -0.01 -0.85 -0.87 0.00 0.00

Notes: SAMPLE @ 1045

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

bladdertlpe

MW-16

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:W Milejczak Pump Model/Type

Reference 45 Page 60

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12/18/12

Operator NameCompany NameProject Name 0.17 [in]Site Name 30 [ft]

20 [ft]

Well ID 150 [mL/min]1 [in] 683.9 [mL]

24.59 [ft] Calculated Sample Rate 274 [sec]10 [ft] Sample rate 274 [sec]

180 [in] 3 [in]15 [ft]

Time Temp [F] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

15:31:07 59.29 7.13 701.82 47.31 4.52 0.1615:35:43 59.48 7.12 706.21 37.67 4.49 0.1615:40:19 59.37 7.12 706.23 20.15 4.49 0.1515:44:54 59.07 7.12 705.18 12.29 4.48 0.1515:49:29 59.07 7.12 705.53 10.71 4.50 0.1515:40:19 -0.11 0.00 0.02 -17.52 0.01 0.0015:44:54 -0.30 0.00 -1.05 -7.87 -0.01 0.0015:49:29 0.00 0.00 0.35 -1.57 0.02 0.00

Notes: SAMPLE @ 1550

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

Peristallictlpe

MW-8

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:W Milejczak Pump Model/Type

Reference 45 Page 61

Page 62: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12/19/12

Operator NameCompany NameProject Name 0.17 [in]Site Name 25 [ft]

15 [ft]

Well ID 150 [mL/min]1.5 [in] 661.59 [mL]

18.21 [ft] Calculated Sample Rate 265 [sec]10 [ft] Sample rate 265 [sec]

180 [in] 3 [in]15.74 [ft]

Time Temp [F] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

9:47:56 56.22 6.92 782.24 76.73 1.01 0.089:49:35 56.48 6.93 786.14 75.02 1.02 0.079:51:26 56.52 6.94 789.20 56.66 0.83 0.059:53:04 56.65 6.94 790.97 51.24 0.73 0.059:55:10 56.86 6.95 795.19 43.97 0.60 0.049:51:26 0.03 0.01 3.06 -18.36 -0.19 -0.019:53:04 0.13 0.00 1.77 -5.42 -0.09 -0.019:55:10 0.21 0.01 4.22 -7.27 -0.13 -0.01

Notes: SAMPLE @ 1010

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

peristallictlpe

MW-9

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:W Milejczak Pump Model/Type

Reference 45 Page 62

Page 63: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12/18/12

Operator NameCompany NameProject Name 0.17 [in]Site Name 30 [ft]

20 [ft]

Well ID 150 [mL/min]2 [in] 683.9 [mL]

23.23 [ft] Calculated Sample Rate 274 [sec]10 [ft] Sample rate 274 [sec]

180 [in] 3 [in]16.12 [ft]

Time Temp [F] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

10:48:36 50.50 7.24 639.39 142.29 6.98 0.2010:53:11 52.01 7.20 654.86 59.15 6.13 0.1810:57:47 52.86 7.18 662.05 43.83 5.86 0.1711:02:23 53.28 7.18 665.48 32.12 5.82 0.1611:06:59 52.84 7.18 661.31 33.33 5.77 0.1610:57:47 0.85 -0.02 7.18 -15.32 -0.27 -0.0111:02:23 0.42 0.00 3.43 -11.70 -0.05 -0.0111:06:59 -0.43 0.00 -4.17 1.21 -0.05 -0.01

Notes: SAMPLE @ 1115DUPLICATE Taken

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

BLADDERtlpe

PMW-1

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:W Milejczak Pump Model/Type

Reference 45 Page 63

Page 64: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12/18/12

Operator NameCompany NameProject Name 0.17 [in]Site Name 30 [ft]

20 [ft]

Well ID 150 [mL/min]2 [in] 683.9 [mL]

21.4 [ft] Calculated Sample Rate 274 [sec]10 [ft] Sample rate 274 [sec]

180 [in] 3 [in]13.95 [ft]

Time Temp [F] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

11:44:27 49.31 7.44 757.73 93.60 2.37 0.1611:49:02 50.20 7.43 775.95 90.71 1.40 0.1611:53:39 51.07 7.43 790.43 92.27 0.97 0.1511:58:15 51.34 7.43 793.77 69.90 0.85 0.1512:02:50 51.62 7.43 797.35 58.98 0.75 0.1511:53:39 0.87 0.00 14.48 1.56 -0.43 0.0011:58:15 0.27 0.00 3.33 -22.37 -0.13 0.0012:02:50 0.28 0.00 3.59 -10.92 -0.09 0.00

Notes: SAMPLE @ 1205

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

BLADDERtlpe

PMW-4

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:W Milejczak Pump Model/Type

Reference 45 Page 64

Page 65: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12/18/12

Operator NameCompany NameProject Name 0.17 [in]Site Name 30 [ft]

20 [ft]

Well ID 150 [mL/min]1.5 [in] 683.9 [mL]

20.96 [ft] Calculated Sample Rate 274 [sec]10 [ft] Sample rate 274 [sec]

180 [in] 3 [in]13.99 [ft]

Time Temp [F] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

14:13:26 50.16 7.25 620.35 71.68 4.08 0.1614:18:03 50.27 7.24 623.83 68.44 3.75 0.1614:22:39 50.56 7.23 628.48 74.91 3.63 0.1614:27:15 50.82 7.23 631.38 57.01 3.67 0.1514:31:51 50.93 7.23 632.49 66.35 3.75 0.1514:22:39 0.29 -0.01 4.65 6.47 -0.11 0.0014:27:15 0.26 0.00 2.90 -17.90 0.04 0.0014:31:51 0.11 0.00 1.11 9.34 0.07 0.00

Notes: SAMPLE @ 1433

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

BLADDERtlpe

PMW-5

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:W Milejczak Pump Model/Type

Reference 45 Page 65

Page 66: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12/18/12

Operator NameCompany NameProject Name 0.17 [in]Site Name 30 [ft]

20 [ft]

Well ID 150 [mL/min]1.5 [in] 683.9 [mL]

21.04 [ft] Calculated Sample Rate 274 [sec]10 [ft] Sample rate 274 [sec]

180 [in] 3 [in]13.3 [ft]

Time Temp [F] pH [pH] Cond [µS/cm] Turb [FNU] RDO [mg/L] ORP [V]

+/-0.1 +/-1 +/-1 +/-1 +/-10+/-3 % +/-10 % +/-10 %

12:49:20 49.96 7.26 617.62 164.91 3.62 0.1612:53:56 50.49 7.22 608.29 154.29 3.61 0.1612:58:33 50.80 7.21 602.69 190.66 3.67 0.1613:03:08 51.01 7.20 599.98 170.27 3.78 0.1513:07:44 51.46 7.19 601.88 168.02 3.83 0.1512:58:33 0.31 -0.02 -5.60 36.37 0.05 0.0013:03:08 0.21 -0.01 -2.70 -20.39 0.11 0.0013:07:44 0.45 0.00 1.90 -2.25 0.05 0.00

Notes: SAMPLE @ 1305

Stabilized drawdown

Flowcell volumeWell diameterWell total depthDepth to top of screen

Depth to Water

Last 5 Readings

Variance in last 3 readings

Low-Flow Sampling Stabilization Summary

Tubing LengthTubing Diameter

BLADDERtlpe

PMW-6

1024-1003

Tubing TypeAcuityESComponent Machine

Stabilization Settings

Pumping information:Final pumping rate

Pump placement from TOC

Well Information:

Screen length

ISI Low-Flow LogTroll 9000 Low-Flow System

Pump Information:Project Information:W Milejczak Pump Model/Type

Reference 45 Page 66

Page 67: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

Mrs. Wendy MilejczakAcuity Environmental Solutions7965 East 106th St. Suite 128Fishers, IN 46038

Report Summary

Thursday April 05, 2012

Report Number: L568306

Samples Received: 04/04/12

Client Project: 1024-1003-01

Description: Component Machine

The analytical results in this report are based upon information suppliedby you, the client, and are for your exclusive use. If you have anyquestions regarding this data package, please do not hesitate to call.

Entire Report Reviewed By: ____________________________________

T. Alan Harvill , ESC Representative

Laboratory Certification NumbersA2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197,FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,NC - ENV375/DW21704/BIO041, ND - R-140. NJ - TN002, NJ NELAP - TN002,SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,TX - T104704245-11-3, OK - 9915, PA - 68-02979

Accreditation is only applicable to the test methods specified on each scope of accreditation heldby ESC Lab Sciences.Note: The use of the preparatory EPA Method 3511 is not approved or endorsed by the CA ELAP.

This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.Where applicable, sampling conducted by ESC is performed per guidance providedin laboratory standard operating procedures: 060302, 060303, and 060304.

Page 1 of 49

Reference 45 Page 67

Page 68: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-01 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : PMW-4

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/02/12 12:15

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone 53. 50. ug/l 8260B 04/04/12 1 Acrolein BDL 50. ug/l 8260B 04/04/12 1 Acrylonitrile BDL 10. ug/l 8260B 04/04/12 1 Benzene BDL 1.0 ug/l 8260B 04/04/12 1 Bromobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 04/04/12 1 Bromoform BDL 1.0 ug/l 8260B 04/04/12 1 Bromomethane BDL 5.0 ug/l 8260B 04/04/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 04/04/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 04/04/12 1 Chloroethane BDL 5.0 ug/l 8260B 04/04/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 04/04/12 1 Chloroform 6.4 5.0 ug/l 8260B 04/04/12 1 Chloromethane BDL 2.5 ug/l 8260B 04/04/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 04/04/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 04/04/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 04/04/12 1 Dibromomethane BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 04/04/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 cis-1,2-Dichloroethene 8.8 1.0 ug/l 8260B 04/04/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 04/04/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 04/04/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 04/04/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 2 of 49

Reference 45 Page 68

Page 69: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-01 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : PMW-4

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/02/12 12:15

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 04/04/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 04/04/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 04/04/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/04/12 1 Naphthalene BDL 5.0 ug/l 8260B 04/04/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Styrene BDL 1.0 ug/l 8260B 04/04/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/04/12 1 Tetrachloroethene 120 1.0 ug/l 8260B 04/04/12 1 Toluene BDL 5.0 ug/l 8260B 04/04/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,1,1-Trichloroethane 2.9 1.0 ug/l 8260B 04/04/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 Trichloroethene 39. 1.0 ug/l 8260B 04/04/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 04/04/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/04/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 04/04/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 04/04/12 1

Surrogate Recovery Toluene-d8 110. % Rec. 8260B 04/04/12 1 Dibromofluoromethane 112. % Rec. 8260B 04/04/12 1 4-Bromofluorobenzene 85.4 % Rec. 8260B 04/04/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 04/05/12 16:22 Printed: 04/05/12 16:46

Page 3 of 49

Reference 45 Page 69

Page 70: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-02 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : PMW-5

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/02/12 13:50

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 04/05/12 1 Acrolein BDL 50. ug/l 8260B 04/05/12 1 Acrylonitrile BDL 10. ug/l 8260B 04/05/12 1 Benzene BDL 1.0 ug/l 8260B 04/05/12 1 Bromobenzene BDL 1.0 ug/l 8260B 04/05/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 04/05/12 1 Bromoform BDL 1.0 ug/l 8260B 04/05/12 1 Bromomethane BDL 5.0 ug/l 8260B 04/05/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 04/05/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 04/05/12 1 Chloroethane BDL 5.0 ug/l 8260B 04/05/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 04/05/12 1 Chloroform 12. 5.0 ug/l 8260B 04/05/12 1 Chloromethane BDL 2.5 ug/l 8260B 04/05/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 04/05/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 04/05/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 04/05/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 04/05/12 1 Dibromomethane BDL 1.0 ug/l 8260B 04/05/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 04/05/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 04/05/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/05/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 04/05/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/05/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/05/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 04/05/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 04/05/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 04/05/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/05/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/05/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 04/05/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 04/05/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 04/05/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 04/05/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 4 of 49

Reference 45 Page 70

Page 71: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-02 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : PMW-5

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/02/12 13:50

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 04/05/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 04/05/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 04/05/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/05/12 1 Naphthalene BDL 5.0 ug/l 8260B 04/05/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 Styrene BDL 1.0 ug/l 8260B 04/05/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/05/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/05/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/05/12 1 Tetrachloroethene 8.4 1.0 ug/l 8260B 04/05/12 1 Toluene BDL 5.0 ug/l 8260B 04/05/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 04/05/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 04/05/12 1 Trichloroethene BDL 1.0 ug/l 8260B 04/05/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 04/05/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/05/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 04/05/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 04/05/12 1

Surrogate Recovery Toluene-d8 109. % Rec. 8260B 04/05/12 1 Dibromofluoromethane 109. % Rec. 8260B 04/05/12 1 4-Bromofluorobenzene 81.0 % Rec. 8260B 04/05/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 04/05/12 16:22 Printed: 04/05/12 16:46

Page 5 of 49

Reference 45 Page 71

Page 72: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-03 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : MW-8

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/02/12 14:35

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 04/05/12 1 Acrolein BDL 50. ug/l 8260B 04/05/12 1 Acrylonitrile BDL 10. ug/l 8260B 04/05/12 1 Benzene BDL 1.0 ug/l 8260B 04/05/12 1 Bromobenzene BDL 1.0 ug/l 8260B 04/05/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 04/05/12 1 Bromoform BDL 1.0 ug/l 8260B 04/05/12 1 Bromomethane BDL 5.0 ug/l 8260B 04/05/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 04/05/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 04/05/12 1 Chloroethane BDL 5.0 ug/l 8260B 04/05/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 04/05/12 1 Chloroform 8.1 5.0 ug/l 8260B 04/05/12 1 Chloromethane BDL 2.5 ug/l 8260B 04/05/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 04/05/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 04/05/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 04/05/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 04/05/12 1 Dibromomethane BDL 1.0 ug/l 8260B 04/05/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 04/05/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 04/05/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/05/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 04/05/12 1 cis-1,2-Dichloroethene 18. 1.0 ug/l 8260B 04/05/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/05/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 04/05/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 04/05/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 04/05/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/05/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/05/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 04/05/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 04/05/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 04/05/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 04/05/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 6 of 49

Reference 45 Page 72

Page 73: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-03 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : MW-8

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/02/12 14:35

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 04/05/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 04/05/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 04/05/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/05/12 1 Naphthalene BDL 5.0 ug/l 8260B 04/05/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 Styrene BDL 1.0 ug/l 8260B 04/05/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/05/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/05/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/05/12 1 Tetrachloroethene 28. 1.0 ug/l 8260B 04/05/12 1 Toluene BDL 5.0 ug/l 8260B 04/05/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,1,1-Trichloroethane 1.1 1.0 ug/l 8260B 04/05/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 04/05/12 1 Trichloroethene 19. 1.0 ug/l 8260B 04/05/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 04/05/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/05/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 04/05/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 04/05/12 1

Surrogate Recovery Toluene-d8 109. % Rec. 8260B 04/05/12 1 Dibromofluoromethane 112. % Rec. 8260B 04/05/12 1 4-Bromofluorobenzene 82.1 % Rec. 8260B 04/05/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 04/05/12 16:22 Printed: 04/05/12 16:46

Page 7 of 49

Reference 45 Page 73

Page 74: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-04 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : MW-11

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/03/12 09:30

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 04/05/12 1 Acrolein BDL 50. ug/l 8260B 04/05/12 1 Acrylonitrile BDL 10. ug/l 8260B 04/05/12 1 Benzene BDL 1.0 ug/l 8260B 04/05/12 1 Bromobenzene BDL 1.0 ug/l 8260B 04/05/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 04/05/12 1 Bromoform BDL 1.0 ug/l 8260B 04/05/12 1 Bromomethane BDL 5.0 ug/l 8260B 04/05/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 04/05/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 04/05/12 1 Chloroethane BDL 5.0 ug/l 8260B 04/05/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 04/05/12 1 Chloroform BDL 5.0 ug/l 8260B 04/05/12 1 Chloromethane BDL 2.5 ug/l 8260B 04/05/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 04/05/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 04/05/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 04/05/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 04/05/12 1 Dibromomethane BDL 1.0 ug/l 8260B 04/05/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 04/05/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 04/05/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/05/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 04/05/12 1 cis-1,2-Dichloroethene 1.9 1.0 ug/l 8260B 04/05/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/05/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 04/05/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 04/05/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 04/05/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/05/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/05/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 04/05/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 04/05/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 04/05/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 04/05/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 8 of 49

Reference 45 Page 74

Page 75: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-04 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : MW-11

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/03/12 09:30

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 04/05/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 04/05/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 04/05/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/05/12 1 Naphthalene BDL 5.0 ug/l 8260B 04/05/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 Styrene BDL 1.0 ug/l 8260B 04/05/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/05/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/05/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/05/12 1 Tetrachloroethene 1.8 1.0 ug/l 8260B 04/05/12 1 Toluene BDL 5.0 ug/l 8260B 04/05/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,1,1-Trichloroethane 2.2 1.0 ug/l 8260B 04/05/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 04/05/12 1 Trichloroethene 29. 1.0 ug/l 8260B 04/05/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 04/05/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/05/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 04/05/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 04/05/12 1

Surrogate Recovery Toluene-d8 109. % Rec. 8260B 04/05/12 1 Dibromofluoromethane 111. % Rec. 8260B 04/05/12 1 4-Bromofluorobenzene 83.7 % Rec. 8260B 04/05/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 04/05/12 16:22 Printed: 04/05/12 16:46

Page 9 of 49

Reference 45 Page 75

Page 76: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05, 2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-05 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : PMW-1

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/02/12 10:10

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 04/04/12 1 Acrolein BDL 50. ug/l 8260B 04/04/12 1 Acrylonitrile BDL 10. ug/l 8260B 04/04/12 1 Benzene BDL 1.0 ug/l 8260B 04/04/12 1 Bromobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 04/04/12 1 Bromoform BDL 1.0 ug/l 8260B 04/04/12 1 Bromomethane BDL 5.0 ug/l 8260B 04/04/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 04/04/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 04/04/12 1 Chloroethane BDL 5.0 ug/l 8260B 04/04/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 04/04/12 1 Chloroform BDL 5.0 ug/l 8260B 04/04/12 1 Chloromethane BDL 2.5 ug/l 8260B 04/04/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 04/04/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 04/04/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 04/04/12 1 Dibromomethane BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 04/04/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 cis-1,2-Dichloroethene 1.9 1.0 ug/l 8260B 04/04/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 04/04/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 04/04/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 04/04/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 10 of 49

Reference 45 Page 76

Page 77: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05, 2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-05 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : PMW-1

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/02/12 10:10

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 04/04/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 04/04/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 04/04/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/04/12 1 Naphthalene BDL 5.0 ug/l 8260B 04/04/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Styrene BDL 1.0 ug/l 8260B 04/04/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/04/12 1 Tetrachloroethene 37. 1.0 ug/l 8260B 04/04/12 1 Toluene BDL 5.0 ug/l 8260B 04/04/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 Trichloroethene 20. 1.0 ug/l 8260B 04/04/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 04/04/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/04/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 04/04/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 04/04/12 1

Surrogate Recovery Toluene-d8 109. % Rec. 8260B 04/04/12 1 Dibromofluoromethane 111. % Rec. 8260B 04/04/12 1 4-Bromofluorobenzene 83.5 % Rec. 8260B 04/04/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 04/05/12 16:22 Printed: 04/05/12 16:46

Page 11 of 49

Reference 45 Page 77

Page 78: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05, 2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-06 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : PMW-1 MS

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/02/12 10:10

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Matrix Spike See QC Report for % Rec. and RPD

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 04/05/12 16:22 Printed: 04/05/12 16:46

Page 12 of 49

Reference 45 Page 78

Page 79: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-07 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : PMW-1 MSD

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/02/12 10:10

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics MSD See QC Report for % Rec and RPD

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 04/05/12 16:22 Printed: 04/05/12 16:46

Page 13 of 49

Reference 45 Page 79

Page 80: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-08 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : MW-10

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/02/12 15:10

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 04/04/12 1 Acrolein BDL 50. ug/l 8260B 04/04/12 1 Acrylonitrile BDL 10. ug/l 8260B 04/04/12 1 Benzene BDL 1.0 ug/l 8260B 04/04/12 1 Bromobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 04/04/12 1 Bromoform BDL 1.0 ug/l 8260B 04/04/12 1 Bromomethane BDL 5.0 ug/l 8260B 04/04/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 04/04/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 04/04/12 1 Chloroethane BDL 5.0 ug/l 8260B 04/04/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 04/04/12 1 Chloroform 28. 5.0 ug/l 8260B 04/04/12 1 Chloromethane BDL 2.5 ug/l 8260B 04/04/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 04/04/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 04/04/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 04/04/12 1 Dibromomethane BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 04/04/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 04/04/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 04/04/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 04/04/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 14 of 49

Reference 45 Page 80

Page 81: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-08 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : MW-10

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/02/12 15:10

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 04/04/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 04/04/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 04/04/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/04/12 1 Naphthalene BDL 5.0 ug/l 8260B 04/04/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Styrene BDL 1.0 ug/l 8260B 04/04/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/04/12 1 Tetrachloroethene 5.6 1.0 ug/l 8260B 04/04/12 1 Toluene BDL 5.0 ug/l 8260B 04/04/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 Trichloroethene 2.7 1.0 ug/l 8260B 04/04/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 04/04/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/04/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 04/04/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 04/04/12 1

Surrogate Recovery Toluene-d8 98.0 % Rec. 8260B 04/04/12 1 Dibromofluoromethane 101. % Rec. 8260B 04/04/12 1 4-Bromofluorobenzene 95.5 % Rec. 8260B 04/04/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 04/05/12 16:22 Printed: 04/05/12 16:46

Page 15 of 49

Reference 45 Page 81

Page 82: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-09 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : MW-9

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/02/12 10:50

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 04/04/12 1 Acrolein BDL 50. ug/l 8260B 04/04/12 1 Acrylonitrile BDL 10. ug/l 8260B 04/04/12 1 Benzene BDL 1.0 ug/l 8260B 04/04/12 1 Bromobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 04/04/12 1 Bromoform BDL 1.0 ug/l 8260B 04/04/12 1 Bromomethane BDL 5.0 ug/l 8260B 04/04/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 04/04/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 04/04/12 1 Chloroethane BDL 5.0 ug/l 8260B 04/04/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 04/04/12 1 Chloroform BDL 5.0 ug/l 8260B 04/04/12 1 Chloromethane BDL 2.5 ug/l 8260B 04/04/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 04/04/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 04/04/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 04/04/12 1 Dibromomethane BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 04/04/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 cis-1,2-Dichloroethene 2.9 1.0 ug/l 8260B 04/04/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 04/04/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 04/04/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 04/04/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 16 of 49

Reference 45 Page 82

Page 83: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-09 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : MW-9

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/02/12 10:50

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 04/04/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 04/04/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 04/04/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/04/12 1 Naphthalene BDL 5.0 ug/l 8260B 04/04/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Styrene BDL 1.0 ug/l 8260B 04/04/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/04/12 1 Tetrachloroethene 76. 1.0 ug/l 8260B 04/04/12 1 Toluene BDL 5.0 ug/l 8260B 04/04/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,1,1-Trichloroethane 1.3 1.0 ug/l 8260B 04/04/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 Trichloroethene 23. 1.0 ug/l 8260B 04/04/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 04/04/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/04/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 04/04/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 04/04/12 1

Surrogate Recovery Toluene-d8 98.9 % Rec. 8260B 04/04/12 1 Dibromofluoromethane 99.7 % Rec. 8260B 04/04/12 1 4-Bromofluorobenzene 98.4 % Rec. 8260B 04/04/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 04/05/12 16:22 Printed: 04/05/12 16:46

Page 17 of 49

Reference 45 Page 83

Page 84: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-10 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : PMW-6

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/03/12 10:20

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 04/04/12 1 Acrolein BDL 50. ug/l 8260B 04/04/12 1 Acrylonitrile BDL 10. ug/l 8260B 04/04/12 1 Benzene BDL 1.0 ug/l 8260B 04/04/12 1 Bromobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 04/04/12 1 Bromoform BDL 1.0 ug/l 8260B 04/04/12 1 Bromomethane BDL 5.0 ug/l 8260B 04/04/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Carbon tetrachloride 1.8 1.0 ug/l 8260B 04/04/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 04/04/12 1 Chloroethane BDL 5.0 ug/l 8260B 04/04/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 04/04/12 1 Chloroform 5.6 5.0 ug/l 8260B 04/04/12 1 Chloromethane BDL 2.5 ug/l 8260B 04/04/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 04/04/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 04/04/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 04/04/12 1 Dibromomethane BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 04/04/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 cis-1,2-Dichloroethene 1.4 1.0 ug/l 8260B 04/04/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 04/04/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 04/04/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 04/04/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 18 of 49

Reference 45 Page 84

Page 85: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-10 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : PMW-6

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/03/12 10:20

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 04/04/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 04/04/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 04/04/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/04/12 1 Naphthalene BDL 5.0 ug/l 8260B 04/04/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Styrene BDL 1.0 ug/l 8260B 04/04/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/04/12 1 Tetrachloroethene 11. 1.0 ug/l 8260B 04/04/12 1 Toluene BDL 5.0 ug/l 8260B 04/04/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,1,1-Trichloroethane 2.2 1.0 ug/l 8260B 04/04/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 Trichloroethene 52. 1.0 ug/l 8260B 04/04/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 04/04/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/04/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 04/04/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 04/04/12 1

Surrogate Recovery Toluene-d8 99.2 % Rec. 8260B 04/04/12 1 Dibromofluoromethane 101. % Rec. 8260B 04/04/12 1 4-Bromofluorobenzene 93.2 % Rec. 8260B 04/04/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 04/05/12 16:22 Printed: 04/05/12 16:46

Page 19 of 49

Reference 45 Page 85

Page 86: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-11 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : MW-12

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/02/12 11:30

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 04/04/12 1 Acrolein BDL 50. ug/l 8260B 04/04/12 1 Acrylonitrile BDL 10. ug/l 8260B 04/04/12 1 Benzene BDL 1.0 ug/l 8260B 04/04/12 1 Bromobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 04/04/12 1 Bromoform BDL 1.0 ug/l 8260B 04/04/12 1 Bromomethane BDL 5.0 ug/l 8260B 04/04/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Carbon tetrachloride 1.2 1.0 ug/l 8260B 04/04/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 04/04/12 1 Chloroethane BDL 5.0 ug/l 8260B 04/04/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 04/04/12 1 Chloroform 5.4 5.0 ug/l 8260B 04/04/12 1 Chloromethane BDL 2.5 ug/l 8260B 04/04/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 04/04/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 04/04/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 04/04/12 1 Dibromomethane BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 04/04/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 04/04/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 04/04/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 04/04/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 20 of 49

Reference 45 Page 86

Page 87: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-11 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : MW-12

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/02/12 11:30

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 04/04/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 04/04/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 04/04/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/04/12 1 Naphthalene BDL 5.0 ug/l 8260B 04/04/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Styrene BDL 1.0 ug/l 8260B 04/04/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/04/12 1 Tetrachloroethene 25. 1.0 ug/l 8260B 04/04/12 1 Toluene BDL 5.0 ug/l 8260B 04/04/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 Trichloroethene 9.4 1.0 ug/l 8260B 04/04/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 04/04/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/04/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 04/04/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 04/04/12 1

Surrogate Recovery Toluene-d8 98.4 % Rec. 8260B 04/04/12 1 Dibromofluoromethane 102. % Rec. 8260B 04/04/12 1 4-Bromofluorobenzene 95.5 % Rec. 8260B 04/04/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 04/05/12 16:22 Printed: 04/05/12 16:46

Page 21 of 49

Reference 45 Page 87

Page 88: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-12 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : MW-13

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/03/12 11:15

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 04/04/12 1 Acrolein BDL 50. ug/l 8260B 04/04/12 1 Acrylonitrile BDL 10. ug/l 8260B 04/04/12 1 Benzene BDL 1.0 ug/l 8260B 04/04/12 1 Bromobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 04/04/12 1 Bromoform BDL 1.0 ug/l 8260B 04/04/12 1 Bromomethane BDL 5.0 ug/l 8260B 04/04/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 04/04/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 04/04/12 1 Chloroethane BDL 5.0 ug/l 8260B 04/04/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 04/04/12 1 Chloroform 26. 5.0 ug/l 8260B 04/04/12 1 Chloromethane BDL 2.5 ug/l 8260B 04/04/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 04/04/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 04/04/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 04/04/12 1 Dibromomethane BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 04/04/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 04/04/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 04/04/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 04/04/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 22 of 49

Reference 45 Page 88

Page 89: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-12 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : MW-13

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/03/12 11:15

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 04/04/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 04/04/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 04/04/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/04/12 1 Naphthalene BDL 5.0 ug/l 8260B 04/04/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Styrene BDL 1.0 ug/l 8260B 04/04/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/04/12 1 Tetrachloroethene BDL 1.0 ug/l 8260B 04/04/12 1 Toluene BDL 5.0 ug/l 8260B 04/04/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 Trichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 04/04/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/04/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 04/04/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 04/04/12 1

Surrogate Recovery Toluene-d8 98.5 % Rec. 8260B 04/04/12 1 Dibromofluoromethane 106. % Rec. 8260B 04/04/12 1 4-Bromofluorobenzene 94.0 % Rec. 8260B 04/04/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 04/05/12 16:22 Printed: 04/05/12 16:46

Page 23 of 49

Reference 45 Page 89

Page 90: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-13 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : MW-14

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/03/12 15:25

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 04/04/12 1 Acrolein BDL 50. ug/l 8260B 04/04/12 1 Acrylonitrile BDL 10. ug/l 8260B 04/04/12 1 Benzene BDL 1.0 ug/l 8260B 04/04/12 1 Bromobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 04/04/12 1 Bromoform BDL 1.0 ug/l 8260B 04/04/12 1 Bromomethane BDL 5.0 ug/l 8260B 04/04/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 04/04/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 04/04/12 1 Chloroethane BDL 5.0 ug/l 8260B 04/04/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 04/04/12 1 Chloroform BDL 5.0 ug/l 8260B 04/04/12 1 Chloromethane BDL 2.5 ug/l 8260B 04/04/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 04/04/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 04/04/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 04/04/12 1 Dibromomethane BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 04/04/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 cis-1,2-Dichloroethene 1.4 1.0 ug/l 8260B 04/04/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 04/04/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 04/04/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 04/04/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 24 of 49

Reference 45 Page 90

Page 91: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-13 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : MW-14

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/03/12 15:25

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 04/04/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 04/04/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 04/04/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/04/12 1 Naphthalene BDL 5.0 ug/l 8260B 04/04/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Styrene BDL 1.0 ug/l 8260B 04/04/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/04/12 1 Tetrachloroethene 67. 1.0 ug/l 8260B 04/04/12 1 Toluene BDL 5.0 ug/l 8260B 04/04/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,1,1-Trichloroethane 2.4 1.0 ug/l 8260B 04/04/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 Trichloroethene 52. 1.0 ug/l 8260B 04/04/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 04/04/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/04/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 04/04/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 04/04/12 1

Surrogate Recovery Toluene-d8 100. % Rec. 8260B 04/04/12 1 Dibromofluoromethane 107. % Rec. 8260B 04/04/12 1 4-Bromofluorobenzene 99.8 % Rec. 8260B 04/04/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 04/05/12 16:22 Printed: 04/05/12 16:46

Page 25 of 49

Reference 45 Page 91

Page 92: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-14 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : MW-15

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/03/12 14:40

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 04/04/12 1 Acrolein BDL 50. ug/l 8260B 04/04/12 1 Acrylonitrile BDL 10. ug/l 8260B 04/04/12 1 Benzene BDL 1.0 ug/l 8260B 04/04/12 1 Bromobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 04/04/12 1 Bromoform BDL 1.0 ug/l 8260B 04/04/12 1 Bromomethane BDL 5.0 ug/l 8260B 04/04/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 04/04/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 04/04/12 1 Chloroethane BDL 5.0 ug/l 8260B 04/04/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 04/04/12 1 Chloroform BDL 5.0 ug/l 8260B 04/04/12 1 Chloromethane BDL 2.5 ug/l 8260B 04/04/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 04/04/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 04/04/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 04/04/12 1 Dibromomethane BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 04/04/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 04/04/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 04/04/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 04/04/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 26 of 49

Reference 45 Page 92

Page 93: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-14 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : MW-15

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/03/12 14:40

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 04/04/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 04/04/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 04/04/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/04/12 1 Naphthalene BDL 5.0 ug/l 8260B 04/04/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Styrene BDL 1.0 ug/l 8260B 04/04/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/04/12 1 Tetrachloroethene 120 1.0 ug/l 8260B 04/04/12 1 Toluene BDL 5.0 ug/l 8260B 04/04/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,1,1-Trichloroethane 3.9 1.0 ug/l 8260B 04/04/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 Trichloroethene 70. 1.0 ug/l 8260B 04/04/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 04/04/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/04/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 04/04/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 04/04/12 1

Surrogate Recovery Toluene-d8 99.4 % Rec. 8260B 04/04/12 1 Dibromofluoromethane 103. % Rec. 8260B 04/04/12 1 4-Bromofluorobenzene 92.8 % Rec. 8260B 04/04/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 04/05/12 16:22 Printed: 04/05/12 16:46

Page 27 of 49

Reference 45 Page 93

Page 94: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-15 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : MW-16

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/03/12 13:50

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 04/04/12 1 Acrolein BDL 50. ug/l 8260B 04/04/12 1 Acrylonitrile BDL 10. ug/l 8260B 04/04/12 1 Benzene BDL 1.0 ug/l 8260B 04/04/12 1 Bromobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 04/04/12 1 Bromoform BDL 1.0 ug/l 8260B 04/04/12 1 Bromomethane BDL 5.0 ug/l 8260B 04/04/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 04/04/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 04/04/12 1 Chloroethane BDL 5.0 ug/l 8260B 04/04/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 04/04/12 1 Chloroform BDL 5.0 ug/l 8260B 04/04/12 1 Chloromethane BDL 2.5 ug/l 8260B 04/04/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 04/04/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 04/04/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 04/04/12 1 Dibromomethane BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 04/04/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 04/04/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 04/04/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 04/04/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 28 of 49

Reference 45 Page 94

Page 95: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-15 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : MW-16

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/03/12 13:50

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 04/04/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 04/04/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 04/04/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/04/12 1 Naphthalene BDL 5.0 ug/l 8260B 04/04/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Styrene BDL 1.0 ug/l 8260B 04/04/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/04/12 1 Tetrachloroethene 3.4 1.0 ug/l 8260B 04/04/12 1 Toluene BDL 5.0 ug/l 8260B 04/04/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,1,1-Trichloroethane 12. 1.0 ug/l 8260B 04/04/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 Trichloroethene 100 1.0 ug/l 8260B 04/04/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 04/04/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/04/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 04/04/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 04/04/12 1

Surrogate Recovery Toluene-d8 98.6 % Rec. 8260B 04/04/12 1 Dibromofluoromethane 95.0 % Rec. 8260B 04/04/12 1 4-Bromofluorobenzene 98.0 % Rec. 8260B 04/04/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 04/05/12 16:22 Printed: 04/05/12 16:46

Page 29 of 49

Reference 45 Page 95

Page 96: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-16 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : DUPLICATE

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/03/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 04/05/12 1 Acrolein BDL 50. ug/l 8260B 04/05/12 1 Acrylonitrile BDL 10. ug/l 8260B 04/05/12 1 Benzene BDL 1.0 ug/l 8260B 04/05/12 1 Bromobenzene BDL 1.0 ug/l 8260B 04/05/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 04/05/12 1 Bromoform BDL 1.0 ug/l 8260B 04/05/12 1 Bromomethane BDL 5.0 ug/l 8260B 04/05/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 Carbon tetrachloride 1.4 1.0 ug/l 8260B 04/05/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 04/05/12 1 Chloroethane BDL 5.0 ug/l 8260B 04/05/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 04/05/12 1 Chloroform 5.5 5.0 ug/l 8260B 04/05/12 1 Chloromethane BDL 2.5 ug/l 8260B 04/05/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 04/05/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 04/05/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 04/05/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 04/05/12 1 Dibromomethane BDL 1.0 ug/l 8260B 04/05/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 04/05/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 04/05/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/05/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 04/05/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/05/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/05/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 04/05/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 04/05/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 04/05/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/05/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/05/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 04/05/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 04/05/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 04/05/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 04/05/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 30 of 49

Reference 45 Page 96

Page 97: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-16 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : DUPLICATE

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/03/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 04/05/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 04/05/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 04/05/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/05/12 1 Naphthalene BDL 5.0 ug/l 8260B 04/05/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 Styrene BDL 1.0 ug/l 8260B 04/05/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/05/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/05/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/05/12 1 Tetrachloroethene 26. 1.0 ug/l 8260B 04/05/12 1 Toluene BDL 5.0 ug/l 8260B 04/05/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 04/05/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 04/05/12 1 Trichloroethene 10. 1.0 ug/l 8260B 04/05/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 04/05/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/05/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 04/05/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 04/05/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 04/05/12 1

Surrogate Recovery Toluene-d8 97.9 % Rec. 8260B 04/05/12 1 Dibromofluoromethane 108. % Rec. 8260B 04/05/12 1 4-Bromofluorobenzene 91.0 % Rec. 8260B 04/05/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 04/05/12 16:22 Printed: 04/05/12 16:46

Page 31 of 49

Reference 45 Page 97

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12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-17 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : TRIP BLANK

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/03/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 04/04/12 1 Acrolein BDL 50. ug/l 8260B 04/04/12 1 Acrylonitrile BDL 10. ug/l 8260B 04/04/12 1 Benzene BDL 1.0 ug/l 8260B 04/04/12 1 Bromobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 04/04/12 1 Bromoform BDL 1.0 ug/l 8260B 04/04/12 1 Bromomethane BDL 5.0 ug/l 8260B 04/04/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 04/04/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 04/04/12 1 Chloroethane BDL 5.0 ug/l 8260B 04/04/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 04/04/12 1 Chloroform BDL 5.0 ug/l 8260B 04/04/12 1 Chloromethane BDL 2.5 ug/l 8260B 04/04/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 04/04/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 04/04/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 04/04/12 1 Dibromomethane BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 04/04/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 04/04/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 04/04/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 04/04/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 04/04/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 04/04/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 32 of 49

Reference 45 Page 98

Page 99: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak April 05,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L568306-17 Date Received : April 04, 2012 Description : Component Machine

Site ID : Sample ID : TRIP BLANK

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 04/03/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 04/04/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 04/04/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 04/04/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 04/04/12 1 Naphthalene BDL 5.0 ug/l 8260B 04/04/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Styrene BDL 1.0 ug/l 8260B 04/04/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 04/04/12 1 Tetrachloroethene BDL 1.0 ug/l 8260B 04/04/12 1 Toluene BDL 5.0 ug/l 8260B 04/04/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 04/04/12 1 Trichloroethene BDL 1.0 ug/l 8260B 04/04/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 04/04/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 04/04/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 04/04/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 04/04/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 04/04/12 1

Surrogate Recovery Toluene-d8 98.9 % Rec. 8260B 04/04/12 1 Dibromofluoromethane 102. % Rec. 8260B 04/04/12 1 4-Bromofluorobenzene 92.6 % Rec. 8260B 04/04/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 04/05/12 16:22 Printed: 04/05/12 16:46

Page 33 of 49

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Attachment AList of Analytes with QC Qualifiers

Sample Work Sample Run Number Group Type Analyte ID Qualifier ________________ ___________ _______ ________________________________________ __________ __________

L568306-05 WG586298 SAMP 2-Chloroethyl vinyl ether R2105701 J6J3 WG586298 SAMP Tetrachloroethene R2105701 J6

L568306-08 WG586301 SAMP 2-Chloroethyl vinyl ether R2106793 J6J3 WG586301 SAMP 2,2-Dichloropropane R2106793 J3

Page 34 of 49

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Attachment BExplanation of QC Qualifier Codes

Qualifier Meaning __________________ _______________________________________________________________________________

J3 The associated batch QC was outside the established quality control rangefor precision.

J6 The sample matrix interfered with the ability to make any accuratedetermination; spike value is low

Qualifier Report Information

ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program andas required by most certifying bodies including NELAC. In addition to the EPA qualifiers adoptedby ESC, we have implemented ESC qualifiers to provide more information pertaining to our analyticalresults. Each qualifier is designated in the qualifier explanation as either EPA or ESC.Data qualifiers are intended to provide the ESC client with more detailed information concerningthe potential bias of reported data. Because of the wide range of constituents and variety ofmatrices incorporated by most EPA methods,it is common for some compounds to fall outside ofestablished ranges. These exceptions are evaluated and all reported data is valid and useable"unless qualified as 'R' (Rejected)."

DefinitionsAccuracy - The relationship of the observed value of a known sample to the

true value of a known sample. Represented by percent recovery andrelevant to samples such as: control samples, matrix spike recoveries,surrogate recoveries, etc.

Precision - The agreement between a set of samples or between duplicate samples.Relates to how close together the results are and is represented byRelative Percent Differrence.

Surrogate - Organic compounds that are similar in chemical composition, extraction,and chromotography to analytes of interest. The surrogates are used todetermine the probable response of the group of analytes that are chem-ically related to the surrogate compound. Surrogates are added to thesample and carried through all stages of preparation and analyses.

TIC - Tentatively Identified Compound: Compounds detected in samples that arenot target compounds, internal standards, system monitoring compounds,or surrogates.

Page 35 of 49

Reference 45 Page 101

Page 102: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 April 05, 2012

L568306

Laboratory BlankAnalyte Result Units % Rec Limit Batch Date Analyzed

1,1,1,2-Tetrachloroethane < .001 mg/l WG586298 04/04/12 12:16 1,1,1-Trichloroethane < .001 mg/l WG586298 04/04/12 12:16 1,1,2,2-Tetrachloroethane < .001 mg/l WG586298 04/04/12 12:16 1,1,2-Trichloroethane < .001 mg/l WG586298 04/04/12 12:16 1,1,2-Trichlorotrifluoroethane < .001 mg/l WG586298 04/04/12 12:16 1,1-Dichloroethane < .001 mg/l WG586298 04/04/12 12:16 1,1-Dichloroethene < .001 mg/l WG586298 04/04/12 12:16 1,1-Dichloropropene < .001 mg/l WG586298 04/04/12 12:16 1,2,3-Trichlorobenzene < .001 mg/l WG586298 04/04/12 12:16 1,2,3-Trichloropropane < .001 mg/l WG586298 04/04/12 12:16 1,2,3-Trimethylbenzene < .001 mg/l WG586298 04/04/12 12:16 1,2,4-Trichlorobenzene < .001 mg/l WG586298 04/04/12 12:16 1,2,4-Trimethylbenzene < .001 mg/l WG586298 04/04/12 12:16 1,2-Dibromo-3-Chloropropane < .005 mg/l WG586298 04/04/12 12:16 1,2-Dibromoethane < .001 mg/l WG586298 04/04/12 12:16 1,2-Dichlorobenzene < .001 mg/l WG586298 04/04/12 12:16 1,2-Dichloroethane < .001 mg/l WG586298 04/04/12 12:16 1,2-Dichloropropane < .001 mg/l WG586298 04/04/12 12:16 1,3,5-Trimethylbenzene < .001 mg/l WG586298 04/04/12 12:16 1,3-Dichlorobenzene < .001 mg/l WG586298 04/04/12 12:16 1,3-Dichloropropane < .001 mg/l WG586298 04/04/12 12:16 1,4-Dichlorobenzene < .001 mg/l WG586298 04/04/12 12:16 2,2-Dichloropropane < .001 mg/l WG586298 04/04/12 12:16 2-Butanone (MEK) < .01 mg/l WG586298 04/04/12 12:16 2-Chloroethyl vinyl ether < .05 mg/l WG586298 04/04/12 12:16 2-Chlorotoluene < .001 mg/l WG586298 04/04/12 12:16 4-Chlorotoluene < .001 mg/l WG586298 04/04/12 12:16 4-Methyl-2-pentanone (MIBK) < .01 mg/l WG586298 04/04/12 12:16 Acetone < .05 mg/l WG586298 04/04/12 12:16 Acrolein < .025 mg/l WG586298 04/04/12 12:16 Acrylonitrile < .01 mg/l WG586298 04/04/12 12:16 Benzene < .001 mg/l WG586298 04/04/12 12:16 Bromobenzene < .001 mg/l WG586298 04/04/12 12:16 Bromodichloromethane < .001 mg/l WG586298 04/04/12 12:16 Bromoform < .001 mg/l WG586298 04/04/12 12:16 Bromomethane < .005 mg/l WG586298 04/04/12 12:16 Carbon tetrachloride < .001 mg/l WG586298 04/04/12 12:16 Chlorobenzene < .001 mg/l WG586298 04/04/12 12:16 Chlorodibromomethane < .001 mg/l WG586298 04/04/12 12:16 Chloroethane < .005 mg/l WG586298 04/04/12 12:16 Chloroform < .005 mg/l WG586298 04/04/12 12:16 Chloromethane < .0025 mg/l WG586298 04/04/12 12:16 cis-1,2-Dichloroethene < .001 mg/l WG586298 04/04/12 12:16 cis-1,3-Dichloropropene < .001 mg/l WG586298 04/04/12 12:16 Di-isopropyl ether < .001 mg/l WG586298 04/04/12 12:16 Dibromomethane < .001 mg/l WG586298 04/04/12 12:16 Dichlorodifluoromethane < .005 mg/l WG586298 04/04/12 12:16 Ethylbenzene < .001 mg/l WG586298 04/04/12 12:16 Hexachloro-1,3-butadiene < .001 mg/l WG586298 04/04/12 12:16 Isopropylbenzene < .001 mg/l WG586298 04/04/12 12:16 Methyl tert-butyl ether < .001 mg/l WG586298 04/04/12 12:16 Methylene Chloride < .005 mg/l WG586298 04/04/12 12:16 n-Butylbenzene < .001 mg/l WG586298 04/04/12 12:16 n-Propylbenzene < .001 mg/l WG586298 04/04/12 12:16 Naphthalene < .005 mg/l WG586298 04/04/12 12:16 p-Isopropyltoluene < .001 mg/l WG586298 04/04/12 12:16 sec-Butylbenzene < .001 mg/l WG586298 04/04/12 12:16 Styrene < .001 mg/l WG586298 04/04/12 12:16 tert-Butylbenzene < .001 mg/l WG586298 04/04/12 12:16

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 36 of 49

Reference 45 Page 102

Page 103: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 April 05, 2012

L568306

Laboratory BlankAnalyte Result Units % Rec Limit Batch Date Analyzed

Tetrachloroethene < .001 mg/l WG586298 04/04/12 12:16 Toluene < .005 mg/l WG586298 04/04/12 12:16 trans-1,2-Dichloroethene < .001 mg/l WG586298 04/04/12 12:16 trans-1,3-Dichloropropene < .001 mg/l WG586298 04/04/12 12:16 Trichloroethene < .001 mg/l WG586298 04/04/12 12:16 Trichlorofluoromethane < .005 mg/l WG586298 04/04/12 12:16 Vinyl chloride < .001 mg/l WG586298 04/04/12 12:16 Xylenes, Total < .003 mg/l WG586298 04/04/12 12:16 4-Bromofluorobenzene % Rec. 81.99* 82-120 WG586298 04/04/12 12:16 Dibromofluoromethane % Rec. 111.7 82-126 WG586298 04/04/12 12:16 Toluene-d8 % Rec. 110.9 92-112 WG586298 04/04/12 12:16

1,1,1,2-Tetrachloroethane < .001 mg/l WG586301 04/04/12 20:25 1,1,1-Trichloroethane < .001 mg/l WG586301 04/04/12 20:25 1,1,2,2-Tetrachloroethane < .001 mg/l WG586301 04/04/12 20:25 1,1,2-Trichloroethane < .001 mg/l WG586301 04/04/12 20:25 1,1,2-Trichlorotrifluoroethane < .001 mg/l WG586301 04/04/12 20:25 1,1-Dichloroethane < .001 mg/l WG586301 04/04/12 20:25 1,1-Dichloroethene < .001 mg/l WG586301 04/04/12 20:25 1,1-Dichloropropene < .001 mg/l WG586301 04/04/12 20:25 1,2,3-Trichlorobenzene < .001 mg/l WG586301 04/04/12 20:25 1,2,3-Trichloropropane < .001 mg/l WG586301 04/04/12 20:25 1,2,3-Trimethylbenzene < .001 mg/l WG586301 04/04/12 20:25 1,2,4-Trichlorobenzene < .001 mg/l WG586301 04/04/12 20:25 1,2,4-Trimethylbenzene < .001 mg/l WG586301 04/04/12 20:25 1,2-Dibromo-3-Chloropropane < .005 mg/l WG586301 04/04/12 20:25 1,2-Dibromoethane < .001 mg/l WG586301 04/04/12 20:25 1,2-Dichlorobenzene < .001 mg/l WG586301 04/04/12 20:25 1,2-Dichloroethane < .001 mg/l WG586301 04/04/12 20:25 1,2-Dichloropropane < .001 mg/l WG586301 04/04/12 20:25 1,3,5-Trimethylbenzene < .001 mg/l WG586301 04/04/12 20:25 1,3-Dichlorobenzene < .001 mg/l WG586301 04/04/12 20:25 1,3-Dichloropropane < .001 mg/l WG586301 04/04/12 20:25 1,4-Dichlorobenzene < .001 mg/l WG586301 04/04/12 20:25 2,2-Dichloropropane < .001 mg/l WG586301 04/04/12 20:25 2-Butanone (MEK) < .01 mg/l WG586301 04/04/12 20:25 2-Chloroethyl vinyl ether < .05 mg/l WG586301 04/04/12 20:25 2-Chlorotoluene < .001 mg/l WG586301 04/04/12 20:25 4-Chlorotoluene < .001 mg/l WG586301 04/04/12 20:25 4-Methyl-2-pentanone (MIBK) < .01 mg/l WG586301 04/04/12 20:25 Acetone < .05 mg/l WG586301 04/04/12 20:25 Acrolein < .025 mg/l WG586301 04/04/12 20:25 Acrylonitrile < .01 mg/l WG586301 04/04/12 20:25 Benzene < .001 mg/l WG586301 04/04/12 20:25 Bromobenzene < .001 mg/l WG586301 04/04/12 20:25 Bromodichloromethane < .001 mg/l WG586301 04/04/12 20:25 Bromoform < .001 mg/l WG586301 04/04/12 20:25 Bromomethane < .005 mg/l WG586301 04/04/12 20:25 Carbon tetrachloride < .001 mg/l WG586301 04/04/12 20:25 Chlorobenzene < .001 mg/l WG586301 04/04/12 20:25 Chlorodibromomethane < .001 mg/l WG586301 04/04/12 20:25 Chloroethane < .005 mg/l WG586301 04/04/12 20:25 Chloroform < .005 mg/l WG586301 04/04/12 20:25 Chloromethane < .0025 mg/l WG586301 04/04/12 20:25 cis-1,2-Dichloroethene < .001 mg/l WG586301 04/04/12 20:25 cis-1,3-Dichloropropene < .001 mg/l WG586301 04/04/12 20:25 Di-isopropyl ether < .001 mg/l WG586301 04/04/12 20:25 Dibromomethane < .001 mg/l WG586301 04/04/12 20:25

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 37 of 49

Reference 45 Page 103

Page 104: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 April 05, 2012

L568306

Laboratory BlankAnalyte Result Units % Rec Limit Batch Date Analyzed

Dichlorodifluoromethane < .005 mg/l WG586301 04/04/12 20:25 Ethylbenzene < .001 mg/l WG586301 04/04/12 20:25 Hexachloro-1,3-butadiene < .001 mg/l WG586301 04/04/12 20:25 Isopropylbenzene < .001 mg/l WG586301 04/04/12 20:25 Methyl tert-butyl ether < .001 mg/l WG586301 04/04/12 20:25 Methylene Chloride < .005 mg/l WG586301 04/04/12 20:25 n-Butylbenzene < .001 mg/l WG586301 04/04/12 20:25 n-Propylbenzene < .001 mg/l WG586301 04/04/12 20:25 Naphthalene < .005 mg/l WG586301 04/04/12 20:25 p-Isopropyltoluene < .001 mg/l WG586301 04/04/12 20:25 sec-Butylbenzene < .001 mg/l WG586301 04/04/12 20:25 Styrene < .001 mg/l WG586301 04/04/12 20:25 tert-Butylbenzene < .001 mg/l WG586301 04/04/12 20:25 Tetrachloroethene < .001 mg/l WG586301 04/04/12 20:25 Toluene < .005 mg/l WG586301 04/04/12 20:25 trans-1,2-Dichloroethene < .001 mg/l WG586301 04/04/12 20:25 trans-1,3-Dichloropropene < .001 mg/l WG586301 04/04/12 20:25 Trichloroethene < .001 mg/l WG586301 04/04/12 20:25 Trichlorofluoromethane < .005 mg/l WG586301 04/04/12 20:25 Vinyl chloride < .001 mg/l WG586301 04/04/12 20:25 Xylenes, Total < .003 mg/l WG586301 04/04/12 20:25 4-Bromofluorobenzene % Rec. 102.2 82-120 WG586301 04/04/12 20:25 Dibromofluoromethane % Rec. 95.82 82-126 WG586301 04/04/12 20:25 Toluene-d8 % Rec. 100.4 92-112 WG586301 04/04/12 20:25

Laboratory Control SampleAnalyte Units Known Val Result % Rec Limit Batch

1,1,1,2-Tetrachloroethane mg/l .025 0.0224 89.6 77-128 WG586298 1,1,1-Trichloroethane mg/l .025 0.0271 109. 71-126 WG586298 1,1,2,2-Tetrachloroethane mg/l .025 0.0230 92.0 78-130 WG586298 1,1,2-Trichloroethane mg/l .025 0.0230 91.9 81-121 WG586298 1,1,2-Trichlorotrifluoroethane mg/l .025 0.0198 79.3 53-143 WG586298 1,1-Dichloroethane mg/l .025 0.0277 111. 73-123 WG586298 1,1-Dichloroethene mg/l .025 0.0196 78.5 54-134 WG586298 1,1-Dichloropropene mg/l .025 0.0256 102. 67-127 WG586298 1,2,3-Trichlorobenzene mg/l .025 0.0296 119. 77-130 WG586298 1,2,3-Trichloropropane mg/l .025 0.0212 84.6 68-130 WG586298 1,2,3-Trimethylbenzene mg/l .025 0.0291 116. 70-127 WG586298 1,2,4-Trichlorobenzene mg/l .025 0.0287 115. 76-127 WG586298 1,2,4-Trimethylbenzene mg/l .025 0.0234 93.7 77-129 WG586298 1,2-Dibromo-3-Chloropropane mg/l .025 0.0262 105. 55-142 WG586298 1,2-Dibromoethane mg/l .025 0.0212 84.9 78-124 WG586298 1,2-Dichlorobenzene mg/l .025 0.0276 110. 82-121 WG586298 1,2-Dichloroethane mg/l .025 0.0261 104. 69-128 WG586298 1,2-Dichloropropane mg/l .025 0.0280 112. 77-121 WG586298 1,3,5-Trimethylbenzene mg/l .025 0.0237 94.7 78-127 WG586298 1,3-Dichlorobenzene mg/l .025 0.0218 87.3 77-127 WG586298 1,3-Dichloropropane mg/l .025 0.0226 90.3 78-117 WG586298 1,4-Dichlorobenzene mg/l .025 0.0270 108. 79-117 WG586298 2,2-Dichloropropane mg/l .025 0.0295 118. 63-130 WG586298 2-Butanone (MEK) mg/l .125 0.127 102. 58-144 WG586298 2-Chloroethyl vinyl ether mg/l .125 0.138 110. 26-172 WG586298 2-Chlorotoluene mg/l .025 0.0242 96.8 78-123 WG586298 4-Chlorotoluene mg/l .025 0.0230 92.2 78-122 WG586298 4-Methyl-2-pentanone (MIBK) mg/l .125 0.142 114. 58-147 WG586298 Acetone mg/l .125 0.101 80.5 49-153 WG586298 Acrolein mg/l .125 0.0144 11.5 10-181 WG586298 Acrylonitrile mg/l .125 0.131 105. 53-153 WG586298

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 38 of 49

Reference 45 Page 104

Page 105: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 April 05, 2012

L568306

Laboratory Control SampleAnalyte Units Known Val Result % Rec Limit Batch

Benzene mg/l .025 0.0264 106. 72-119 WG586298 Bromobenzene mg/l .025 0.0234 93.5 76-121 WG586298 Bromodichloromethane mg/l .025 0.0271 108. 75-127 WG586298 Bromoform mg/l .025 0.0204 81.6 61-136 WG586298 Bromomethane mg/l .025 0.0217 86.8 42-172 WG586298 Carbon tetrachloride mg/l .025 0.0255 102. 63-129 WG586298 Chlorobenzene mg/l .025 0.0223 89.4 78-123 WG586298 Chlorodibromomethane mg/l .025 0.0223 89.4 73-128 WG586298 Chloroethane mg/l .025 0.0236 94.6 52-164 WG586298 Chloroform mg/l .025 0.0274 110. 76-122 WG586298 Chloromethane mg/l .025 0.0270 108. 50-141 WG586298 cis-1,2-Dichloroethene mg/l .025 0.0252 101. 75-121 WG586298 cis-1,3-Dichloropropene mg/l .025 0.0272 109. 74-124 WG586298 Di-isopropyl ether mg/l .025 0.0293 117. 66-129 WG586298 Dibromomethane mg/l .025 0.0256 102. 77-124 WG586298 Dichlorodifluoromethane mg/l .025 0.0224 89.8 33-173 WG586298 Ethylbenzene mg/l .025 0.0224 89.7 77-124 WG586298 Hexachloro-1,3-butadiene mg/l .025 0.0272 109. 71-134 WG586298 Isopropylbenzene mg/l .025 0.0241 96.4 74-126 WG586298 Methyl tert-butyl ether mg/l .025 0.0254 102. 67-127 WG586298 Methylene Chloride mg/l .025 0.0235 94.0 67-122 WG586298 n-Butylbenzene mg/l .025 0.0323 129. 74-130 WG586298 n-Propylbenzene mg/l .025 0.0243 97.1 77-125 WG586298 Naphthalene mg/l .025 0.0263 105. 70-134 WG586298 p-Isopropyltoluene mg/l .025 0.0242 96.9 77-132 WG586298 sec-Butylbenzene mg/l .025 0.0244 97.7 77-130 WG586298 Styrene mg/l .025 0.0228 91.0 69-145 WG586298 tert-Butylbenzene mg/l .025 0.0231 92.5 76-131 WG586298 Tetrachloroethene mg/l .025 0.0188 75.2 69-131 WG586298 Toluene mg/l .025 0.0260 104. 75-114 WG586298 trans-1,2-Dichloroethene mg/l .025 0.0233 93.0 63-127 WG586298 trans-1,3-Dichloropropene mg/l .025 0.0252 101. 69-124 WG586298 Trichloroethene mg/l .025 0.0244 97.7 69-131 WG586298 Trichlorofluoromethane mg/l .025 0.0209 83.5 53-161 WG586298 Vinyl chloride mg/l .025 0.0227 90.8 55-142 WG586298 Xylenes, Total mg/l .075 0.0666 88.8 77-123 WG586298 4-Bromofluorobenzene 85.53 82-120 WG586298 Dibromofluoromethane 109.4 82-126 WG586298 Toluene-d8 111.9 92-112 WG586298

1,1,1,2-Tetrachloroethane mg/l .025 0.0267 107. 77-128 WG586301 1,1,1-Trichloroethane mg/l .025 0.0216 86.5 71-126 WG586301 1,1,2,2-Tetrachloroethane mg/l .025 0.0245 98.0 78-130 WG586301 1,1,2-Trichloroethane mg/l .025 0.0255 102. 81-121 WG586301 1,1,2-Trichlorotrifluoroethane mg/l .025 0.0244 97.7 53-143 WG586301 1,1-Dichloroethane mg/l .025 0.0231 92.2 73-123 WG586301 1,1-Dichloroethene mg/l .025 0.0229 91.5 54-134 WG586301 1,1-Dichloropropene mg/l .025 0.0232 92.9 67-127 WG586301 1,2,3-Trichlorobenzene mg/l .025 0.0259 104. 77-130 WG586301 1,2,3-Trichloropropane mg/l .025 0.0248 99.1 68-130 WG586301 1,2,3-Trimethylbenzene mg/l .025 0.0229 91.8 70-127 WG586301 1,2,4-Trichlorobenzene mg/l .025 0.0277 111. 76-127 WG586301 1,2,4-Trimethylbenzene mg/l .025 0.0260 104. 77-129 WG586301 1,2-Dibromo-3-Chloropropane mg/l .025 0.0253 101. 55-142 WG586301 1,2-Dibromoethane mg/l .025 0.0256 102. 78-124 WG586301 1,2-Dichlorobenzene mg/l .025 0.0259 103. 82-121 WG586301 1,2-Dichloroethane mg/l .025 0.0209 83.7 69-128 WG586301 1,2-Dichloropropane mg/l .025 0.0249 99.7 77-121 WG586301

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 39 of 49

Reference 45 Page 105

Page 106: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 April 05, 2012

L568306

Laboratory Control SampleAnalyte Units Known Val Result % Rec Limit Batch

1,3,5-Trimethylbenzene mg/l .025 0.0265 106. 78-127 WG586301 1,3-Dichlorobenzene mg/l .025 0.0266 106. 77-127 WG586301 1,3-Dichloropropane mg/l .025 0.0248 99.3 78-117 WG586301 1,4-Dichlorobenzene mg/l .025 0.0249 99.6 79-117 WG586301 2,2-Dichloropropane mg/l .025 0.0229 91.7 63-130 WG586301 2-Butanone (MEK) mg/l .125 0.130 104. 58-144 WG586301 2-Chloroethyl vinyl ether mg/l .125 0.127 102. 26-172 WG586301 2-Chlorotoluene mg/l .025 0.0252 101. 78-123 WG586301 4-Chlorotoluene mg/l .025 0.0247 98.9 78-122 WG586301 4-Methyl-2-pentanone (MIBK) mg/l .125 0.128 102. 58-147 WG586301 Acetone mg/l .125 0.0704 56.4 49-153 WG586301 Acrolein mg/l .125 0.0200 16.0 10-181 WG586301 Acrylonitrile mg/l .125 0.113 90.3 53-153 WG586301 Benzene mg/l .025 0.0228 91.1 72-119 WG586301 Bromobenzene mg/l .025 0.0238 95.2 76-121 WG586301 Bromodichloromethane mg/l .025 0.0229 91.4 75-127 WG586301 Bromoform mg/l .025 0.0267 107. 61-136 WG586301 Bromomethane mg/l .025 0.0319 128. 42-172 WG586301 Carbon tetrachloride mg/l .025 0.0228 91.1 63-129 WG586301 Chlorobenzene mg/l .025 0.0260 104. 78-123 WG586301 Chlorodibromomethane mg/l .025 0.0259 104. 73-128 WG586301 Chloroethane mg/l .025 0.0270 108. 52-164 WG586301 Chloroform mg/l .025 0.0226 90.2 76-122 WG586301 Chloromethane mg/l .025 0.0294 118. 50-141 WG586301 cis-1,2-Dichloroethene mg/l .025 0.0229 91.7 75-121 WG586301 cis-1,3-Dichloropropene mg/l .025 0.0236 94.5 74-124 WG586301 Di-isopropyl ether mg/l .025 0.0236 94.4 66-129 WG586301 Dibromomethane mg/l .025 0.0239 95.5 77-124 WG586301 Dichlorodifluoromethane mg/l .025 0.0276 110. 33-173 WG586301 Ethylbenzene mg/l .025 0.0264 106. 77-124 WG586301 Hexachloro-1,3-butadiene mg/l .025 0.0260 104. 71-134 WG586301 Isopropylbenzene mg/l .025 0.0286 115. 74-126 WG586301 Methyl tert-butyl ether mg/l .025 0.0220 88.2 67-127 WG586301 Methylene Chloride mg/l .025 0.0206 82.5 67-122 WG586301 n-Butylbenzene mg/l .025 0.0243 97.4 74-130 WG586301 n-Propylbenzene mg/l .025 0.0255 102. 77-125 WG586301 Naphthalene mg/l .025 0.0240 95.9 70-134 WG586301 p-Isopropyltoluene mg/l .025 0.0271 108. 77-132 WG586301 sec-Butylbenzene mg/l .025 0.0267 107. 77-130 WG586301 Styrene mg/l .025 0.0259 104. 69-145 WG586301 tert-Butylbenzene mg/l .025 0.0269 108. 76-131 WG586301 Tetrachloroethene mg/l .025 0.0270 108. 69-131 WG586301 Toluene mg/l .025 0.0244 97.6 75-114 WG586301 trans-1,2-Dichloroethene mg/l .025 0.0223 89.2 63-127 WG586301 trans-1,3-Dichloropropene mg/l .025 0.0227 90.8 69-124 WG586301 Trichloroethene mg/l .025 0.0248 99.1 69-131 WG586301 Trichlorofluoromethane mg/l .025 0.0265 106. 53-161 WG586301 Vinyl chloride mg/l .025 0.0277 111. 55-142 WG586301 Xylenes, Total mg/l .075 0.0789 105. 77-123 WG586301 4-Bromofluorobenzene 94.42 82-120 WG586301 Dibromofluoromethane 93.73 82-126 WG586301 Toluene-d8 99.70 92-112 WG586301

Laboratory Control Sample DuplicateAnalyte Units Result Ref %Rec Limit RPD Limit Batch

1,1,1,2-Tetrachloroethane mg/l 0.0223 0.0224 89.0 77-128 0.580 20 WG586298 1,1,1-Trichloroethane mg/l 0.0252 0.0271 101. 71-126 7.37 20 WG586298 1,1,2,2-Tetrachloroethane mg/l 0.0225 0.0230 90.0 78-130 2.22 20 WG586298

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 40 of 49

Reference 45 Page 106

Page 107: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 April 05, 2012

L568306

Laboratory Control Sample DuplicateAnalyte Units Result Ref %Rec Limit RPD Limit Batch

1,1,2-Trichloroethane mg/l 0.0230 0.0230 92.0 81-121 0.270 20 WG586298 1,1,2-Trichlorotrifluoroethane mg/l 0.0174 0.0198 69.0 53-143 13.2 20 WG586298 1,1-Dichloroethane mg/l 0.0276 0.0277 110. 73-123 0.440 20 WG586298 1,1-Dichloroethene mg/l 0.0199 0.0196 80.0 54-134 1.35 20 WG586298 1,1-Dichloropropene mg/l 0.0252 0.0256 101. 67-127 1.39 20 WG586298 1,2,3-Trichlorobenzene mg/l 0.0285 0.0296 114. 77-130 3.75 20 WG586298 1,2,3-Trichloropropane mg/l 0.0214 0.0212 86.0 68-130 1.20 20 WG586298 1,2,3-Trimethylbenzene mg/l 0.0294 0.0291 118. 70-127 0.980 20 WG586298 1,2,4-Trichlorobenzene mg/l 0.0283 0.0287 113. 76-127 1.38 20 WG586298 1,2,4-Trimethylbenzene mg/l 0.0230 0.0234 92.0 77-129 1.75 20 WG586298 1,2-Dibromo-3-Chloropropane mg/l 0.0252 0.0262 101. 55-142 4.08 20 WG586298 1,2-Dibromoethane mg/l 0.0215 0.0212 86.0 78-124 1.26 20 WG586298 1,2-Dichlorobenzene mg/l 0.0280 0.0276 112. 82-121 1.59 20 WG586298 1,2-Dichloroethane mg/l 0.0265 0.0261 106. 69-128 1.66 20 WG586298 1,2-Dichloropropane mg/l 0.0275 0.0280 110. 77-121 1.63 20 WG586298 1,3,5-Trimethylbenzene mg/l 0.0230 0.0237 92.0 78-127 3.00 20 WG586298 1,3-Dichlorobenzene mg/l 0.0218 0.0218 87.0 77-127 0.310 20 WG586298 1,3-Dichloropropane mg/l 0.0231 0.0226 92.0 78-117 2.32 20 WG586298 1,4-Dichlorobenzene mg/l 0.0273 0.0270 109. 79-117 1.33 20 WG586298 2,2-Dichloropropane mg/l 0.0275 0.0295 110. 63-130 7.04 20 WG586298 2-Butanone (MEK) mg/l 0.122 0.127 98.0 58-144 4.02 20 WG586298 2-Chloroethyl vinyl ether mg/l 0.141 0.138 113. 26-172 2.42 22 WG586298 2-Chlorotoluene mg/l 0.0240 0.0242 96.0 78-123 0.790 20 WG586298 4-Chlorotoluene mg/l 0.0228 0.0230 91.0 78-122 1.25 20 WG586298 4-Methyl-2-pentanone (MIBK) mg/l 0.140 0.142 112. 58-147 1.31 20 WG586298 Acetone mg/l 0.0995 0.101 80.0 49-153 1.09 21 WG586298 Acrolein mg/l 0.0167 0.0144 13.0 10-181 14.9 30 WG586298 Acrylonitrile mg/l 0.128 0.131 102. 53-153 2.18 20 WG586298 Benzene mg/l 0.0259 0.0264 104. 72-119 1.86 20 WG586298 Bromobenzene mg/l 0.0236 0.0234 94.0 76-121 0.830 20 WG586298 Bromodichloromethane mg/l 0.0271 0.0271 108. 75-127 0.150 20 WG586298 Bromoform mg/l 0.0203 0.0204 81.0 61-136 0.390 20 WG586298 Bromomethane mg/l 0.0222 0.0217 89.0 42-172 2.04 20 WG586298 Carbon tetrachloride mg/l 0.0236 0.0255 94.0 63-129 7.59 20 WG586298 Chlorobenzene mg/l 0.0222 0.0223 89.0 78-123 0.550 20 WG586298 Chlorodibromomethane mg/l 0.0218 0.0223 87.0 73-128 2.57 20 WG586298 Chloroethane mg/l 0.0249 0.0236 99.0 52-164 4.99 20 WG586298 Chloroform mg/l 0.0267 0.0274 107. 76-122 2.56 20 WG586298 Chloromethane mg/l 0.0314 0.0270 126. 50-141 15.0 20 WG586298 cis-1,2-Dichloroethene mg/l 0.0246 0.0252 98.0 75-121 2.36 20 WG586298 cis-1,3-Dichloropropene mg/l 0.0269 0.0272 108. 74-124 1.13 20 WG586298 Di-isopropyl ether mg/l 0.0284 0.0293 113. 66-129 3.37 20 WG586298 Dibromomethane mg/l 0.0259 0.0256 104. 77-124 1.14 20 WG586298 Dichlorodifluoromethane mg/l 0.0269 0.0224 107. 33-173 17.9 20 WG586298 Ethylbenzene mg/l 0.0219 0.0224 88.0 77-124 2.42 20 WG586298 Hexachloro-1,3-butadiene mg/l 0.0261 0.0272 104. 71-134 4.25 20 WG586298 Isopropylbenzene mg/l 0.0231 0.0241 92.0 74-126 4.08 20 WG586298 Methyl tert-butyl ether mg/l 0.0250 0.0254 100. 67-127 1.72 20 WG586298 Methylene Chloride mg/l 0.0229 0.0235 92.0 67-122 2.52 20 WG586298 n-Butylbenzene mg/l 0.0317 0.0323 127. 74-130 1.85 20 WG586298 n-Propylbenzene mg/l 0.0233 0.0243 93.0 77-125 4.17 20 WG586298 Naphthalene mg/l 0.0261 0.0263 104. 70-134 0.960 20 WG586298 p-Isopropyltoluene mg/l 0.0234 0.0242 94.0 77-132 3.25 20 WG586298 sec-Butylbenzene mg/l 0.0233 0.0244 93.0 77-130 4.49 20 WG586298 Styrene mg/l 0.0226 0.0228 90.0 69-145 0.540 20 WG586298 tert-Butylbenzene mg/l 0.0220 0.0231 88.0 76-131 4.91 20 WG586298 Tetrachloroethene mg/l 0.0189 0.0188 75.0 69-131 0.230 20 WG586298 Toluene mg/l 0.0254 0.0260 102. 75-114 2.28 20 WG586298 trans-1,2-Dichloroethene mg/l 0.0235 0.0233 94.0 63-127 1.12 20 WG586298

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 41 of 49

Reference 45 Page 107

Page 108: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 April 05, 2012

L568306

Laboratory Control Sample DuplicateAnalyte Units Result Ref %Rec Limit RPD Limit Batch

trans-1,3-Dichloropropene mg/l 0.0257 0.0252 103. 69-124 2.08 20 WG586298 Trichloroethene mg/l 0.0237 0.0244 95.0 69-131 2.88 20 WG586298 Trichlorofluoromethane mg/l 0.0223 0.0209 89.0 53-161 6.64 20 WG586298 Vinyl chloride mg/l 0.0254 0.0227 102. 55-142 11.2 20 WG586298 Xylenes, Total mg/l 0.0673 0.0666 90.0 77-123 1.00 20 WG586298 4-Bromofluorobenzene 85.62 82-120 WG586298 Dibromofluoromethane 103.9 82-126 WG586298 Toluene-d8 111.6 92-112 WG586298

1,1,1,2-Tetrachloroethane mg/l 0.0264 0.0267 106. 77-128 1.01 20 WG586301 1,1,1-Trichloroethane mg/l 0.0224 0.0216 90.0 71-126 3.56 20 WG586301 1,1,2,2-Tetrachloroethane mg/l 0.0233 0.0245 93.0 78-130 5.24 20 WG586301 1,1,2-Trichloroethane mg/l 0.0251 0.0255 100. 81-121 1.51 20 WG586301 1,1,2-Trichlorotrifluoroethane mg/l 0.0249 0.0244 100. 53-143 2.12 20 WG586301 1,1-Dichloroethane mg/l 0.0232 0.0231 93.0 73-123 0.700 20 WG586301 1,1-Dichloroethene mg/l 0.0231 0.0229 92.0 54-134 1.17 20 WG586301 1,1-Dichloropropene mg/l 0.0239 0.0232 96.0 67-127 3.04 20 WG586301 1,2,3-Trichlorobenzene mg/l 0.0257 0.0259 103. 77-130 0.810 20 WG586301 1,2,3-Trichloropropane mg/l 0.0236 0.0248 94.0 68-130 4.90 20 WG586301 1,2,3-Trimethylbenzene mg/l 0.0230 0.0229 92.0 70-127 0.0600 20 WG586301 1,2,4-Trichlorobenzene mg/l 0.0266 0.0277 106. 76-127 4.01 20 WG586301 1,2,4-Trimethylbenzene mg/l 0.0253 0.0260 101. 77-129 2.50 20 WG586301 1,2-Dibromo-3-Chloropropane mg/l 0.0234 0.0253 94.0 55-142 7.90 20 WG586301 1,2-Dibromoethane mg/l 0.0242 0.0256 97.0 78-124 5.62 20 WG586301 1,2-Dichlorobenzene mg/l 0.0255 0.0259 102. 82-121 1.56 20 WG586301 1,2-Dichloroethane mg/l 0.0209 0.0209 84.0 69-128 0.160 20 WG586301 1,2-Dichloropropane mg/l 0.0253 0.0249 101. 77-121 1.43 20 WG586301 1,3,5-Trimethylbenzene mg/l 0.0260 0.0265 104. 78-127 2.02 20 WG586301 1,3-Dichlorobenzene mg/l 0.0265 0.0266 106. 77-127 0.250 20 WG586301 1,3-Dichloropropane mg/l 0.0241 0.0248 96.0 78-117 3.03 20 WG586301 1,4-Dichlorobenzene mg/l 0.0248 0.0249 99.0 79-117 0.170 20 WG586301 2,2-Dichloropropane mg/l 0.0228 0.0229 91.0 63-130 0.530 20 WG586301 2-Butanone (MEK) mg/l 0.116 0.130 93.0 58-144 11.4 20 WG586301 2-Chloroethyl vinyl ether mg/l 0.121 0.127 96.0 26-172 5.18 22 WG586301 2-Chlorotoluene mg/l 0.0252 0.0252 101. 78-123 0.160 20 WG586301 4-Chlorotoluene mg/l 0.0245 0.0247 98.0 78-122 0.850 20 WG586301 4-Methyl-2-pentanone (MIBK) mg/l 0.114 0.128 91.0 58-147 11.5 20 WG586301 Acetone mg/l 0.0613 0.0704 49.0 49-153 13.9 21 WG586301 Acrolein mg/l 0.0163 0.0200 13.0 10-181 20.6 30 WG586301 Acrylonitrile mg/l 0.102 0.113 82.0 53-153 9.95 20 WG586301 Benzene mg/l 0.0229 0.0228 92.0 72-119 0.760 20 WG586301 Bromobenzene mg/l 0.0231 0.0238 92.0 76-121 2.85 20 WG586301 Bromodichloromethane mg/l 0.0224 0.0229 90.0 75-127 2.03 20 WG586301 Bromoform mg/l 0.0252 0.0267 101. 61-136 5.92 20 WG586301 Bromomethane mg/l 0.0314 0.0319 126. 42-172 1.49 20 WG586301 Carbon tetrachloride mg/l 0.0235 0.0228 94.0 63-129 2.94 20 WG586301 Chlorobenzene mg/l 0.0257 0.0260 103. 78-123 0.890 20 WG586301 Chlorodibromomethane mg/l 0.0254 0.0259 102. 73-128 1.94 20 WG586301 Chloroethane mg/l 0.0266 0.0270 106. 52-164 1.67 20 WG586301 Chloroform mg/l 0.0230 0.0226 92.0 76-122 1.92 20 WG586301 Chloromethane mg/l 0.0292 0.0294 117. 50-141 0.640 20 WG586301 cis-1,2-Dichloroethene mg/l 0.0232 0.0229 93.0 75-121 1.43 20 WG586301 cis-1,3-Dichloropropene mg/l 0.0231 0.0236 92.0 74-124 2.33 20 WG586301 Di-isopropyl ether mg/l 0.0236 0.0236 94.0 66-129 0.0900 20 WG586301 Dibromomethane mg/l 0.0234 0.0239 94.0 77-124 1.91 20 WG586301 Dichlorodifluoromethane mg/l 0.0291 0.0276 116. 33-173 5.25 20 WG586301 Ethylbenzene mg/l 0.0267 0.0264 107. 77-124 1.02 20 WG586301 Hexachloro-1,3-butadiene mg/l 0.0264 0.0260 106. 71-134 1.68 20 WG586301

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 42 of 49

Reference 45 Page 108

Page 109: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 April 05, 2012

L568306

Laboratory Control Sample DuplicateAnalyte Units Result Ref %Rec Limit RPD Limit Batch

Isopropylbenzene mg/l 0.0287 0.0286 115. 74-126 0.240 20 WG586301 Methyl tert-butyl ether mg/l 0.0220 0.0220 88.0 67-127 0.0200 20 WG586301 Methylene Chloride mg/l 0.0208 0.0206 83.0 67-122 1.09 20 WG586301 n-Butylbenzene mg/l 0.0247 0.0243 99.0 74-130 1.35 20 WG586301 n-Propylbenzene mg/l 0.0256 0.0255 102. 77-125 0.350 20 WG586301 Naphthalene mg/l 0.0225 0.0240 90.0 70-134 6.16 20 WG586301 p-Isopropyltoluene mg/l 0.0268 0.0271 107. 77-132 1.22 20 WG586301 sec-Butylbenzene mg/l 0.0267 0.0267 107. 77-130 0.220 20 WG586301 Styrene mg/l 0.0253 0.0259 101. 69-145 2.47 20 WG586301 tert-Butylbenzene mg/l 0.0268 0.0269 107. 76-131 0.190 20 WG586301 Tetrachloroethene mg/l 0.0268 0.0270 107. 69-131 0.900 20 WG586301 Toluene mg/l 0.0240 0.0244 96.0 75-114 1.46 20 WG586301 trans-1,2-Dichloroethene mg/l 0.0225 0.0223 90.0 63-127 1.01 20 WG586301 trans-1,3-Dichloropropene mg/l 0.0220 0.0227 88.0 69-124 2.86 20 WG586301 Trichloroethene mg/l 0.0247 0.0248 99.0 69-131 0.270 20 WG586301 Trichlorofluoromethane mg/l 0.0269 0.0265 107. 53-161 1.55 20 WG586301 Vinyl chloride mg/l 0.0279 0.0277 112. 55-142 0.780 20 WG586301 Xylenes, Total mg/l 0.0788 0.0789 105. 77-123 0.0700 20 WG586301 4-Bromofluorobenzene 92.42 82-120 WG586301 Dibromofluoromethane 92.68 82-126 WG586301 Toluene-d8 99.72 92-112 WG586301

Matrix SpikeAnalyte Units MS Res Ref Res TV % Rec Limit Ref Samp Batch

1,1,1,2-Tetrachloroethane mg/l 0.0227 0 .025 90.8 71-130 L568306-05 WG586298 1,1,1-Trichloroethane mg/l 0.0287 0 .025 115. 58-137 L568306-05 WG586298 1,1,2,2-Tetrachloroethane mg/l 0.0253 0 .025 101. 64-149 L568306-05 WG586298 1,1,2-Trichloroethane mg/l 0.0241 0 .025 96.4 73-128 L568306-05 WG586298 1,1,2-Trichlorotrifluoroethane mg/l 0.0222 0 .025 88.8 36-159 L568306-05 WG586298 1,1-Dichloroethane mg/l 0.0286 0 .025 114. 58-133 L568306-05 WG586298 1,1-Dichloroethene mg/l 0.0211 0 .025 84.6 32-152 L568306-05 WG586298 1,1-Dichloropropene mg/l 0.0274 0 .025 109. 50-140 L568306-05 WG586298 1,2,3-Trichlorobenzene mg/l 0.0298 0 .025 119. 68-135 L568306-05 WG586298 1,2,3-Trichloropropane mg/l 0.0237 0 .025 95.0 74-137 L568306-05 WG586298 1,2,3-Trimethylbenzene mg/l 0.0304 0 .025 121. 67-133 L568306-05 WG586298 1,2,4-Trichlorobenzene mg/l 0.0294 0 .025 118. 67-133 L568306-05 WG586298 1,2,4-Trimethylbenzene mg/l 0.0238 0 .025 95.2 62-141 L568306-05 WG586298 1,2-Dibromo-3-Chloropropane mg/l 0.0292 0 .025 117. 55-148 L568306-05 WG586298 1,2-Dibromoethane mg/l 0.0234 0 .025 93.4 71-129 L568306-05 WG586298 1,2-Dichlorobenzene mg/l 0.0285 0 .025 114. 75-125 L568306-05 WG586298 1,2-Dichloroethane mg/l 0.0275 0 .025 110. 59-135 L568306-05 WG586298 1,2-Dichloropropane mg/l 0.0287 0 .025 115. 68-126 L568306-05 WG586298 1,3,5-Trimethylbenzene mg/l 0.0240 0 .025 95.9 67-136 L568306-05 WG586298 1,3-Dichlorobenzene mg/l 0.0218 0 .025 87.2 69-131 L568306-05 WG586298 1,3-Dichloropropane mg/l 0.0235 0 .025 93.8 70-122 L568306-05 WG586298 1,4-Dichlorobenzene mg/l 0.0274 0 .025 110. 70-123 L568306-05 WG586298 2,2-Dichloropropane mg/l 0.0303 0 .025 121. 51-141 L568306-05 WG586298 2-Butanone (MEK) mg/l 0.110 0 .125 88.1 51-149 L568306-05 WG586298 2-Chloroethyl vinyl ether mg/l 0.00240 0 .125 1.92* 10-161 L568306-05 WG586298 2-Chlorotoluene mg/l 0.0250 0 .025 99.9 65-133 L568306-05 WG586298 4-Chlorotoluene mg/l 0.0234 0 .025 93.5 67-129 L568306-05 WG586298 4-Methyl-2-pentanone (MIBK) mg/l 0.163 0 .125 130. 53-154 L568306-05 WG586298 Acetone mg/l 0.0790 0 .125 63.2 34-146 L568306-05 WG586298 Acrolein mg/l 0.0353 0 .125 28.2 10-189 L568306-05 WG586298 Acrylonitrile mg/l 0.148 0 .125 118. 49-162 L568306-05 WG586298 Benzene mg/l 0.0269 0 .025 108. 51-134 L568306-05 WG586298 Bromobenzene mg/l 0.0238 0 .025 95.3 64-130 L568306-05 WG586298 Bromodichloromethane mg/l 0.0273 0 .025 109. 67-132 L568306-05 WG586298

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 43 of 49

Reference 45 Page 109

Page 110: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 April 05, 2012

L568306

Matrix SpikeAnalyte Units MS Res Ref Res TV % Rec Limit Ref Samp Batch

Bromoform mg/l 0.0223 0 .025 89.1 59-137 L568306-05 WG586298 Bromomethane mg/l 0.0231 0 .025 92.2 23-177 L568306-05 WG586298 Carbon tetrachloride mg/l 0.0267 0 .025 107. 49-140 L568306-05 WG586298 Chlorobenzene mg/l 0.0225 0 .025 90.0 69-126 L568306-05 WG586298 Chlorodibromomethane mg/l 0.0233 0 .025 93.4 68-130 L568306-05 WG586298 Chloroethane mg/l 0.0268 0 .025 107. 32-177 L568306-05 WG586298 Chloroform mg/l 0.0281 0 .025 112. 64-130 L568306-05 WG586298 Chloromethane mg/l 0.0319 0 .025 127. 27-155 L568306-05 WG586298 cis-1,2-Dichloroethene mg/l 0.0272 0.00190 .025 101. 54-137 L568306-05 WG586298 cis-1,3-Dichloropropene mg/l 0.0268 0 .025 107. 63-127 L568306-05 WG586298 Di-isopropyl ether mg/l 0.0293 0 .025 117. 58-133 L568306-05 WG586298 Dibromomethane mg/l 0.0272 0 .025 109. 68-131 L568306-05 WG586298 Dichlorodifluoromethane mg/l 0.0279 0 .025 112. 16-188 L568306-05 WG586298 Ethylbenzene mg/l 0.0227 0 .025 90.7 64-135 L568306-05 WG586298 Hexachloro-1,3-butadiene mg/l 0.0276 0 .025 110. 64-140 L568306-05 WG586298 Isopropylbenzene mg/l 0.0245 0 .025 98.0 62-134 L568306-05 WG586298 Methyl tert-butyl ether mg/l 0.0268 0 .025 107. 55-136 L568306-05 WG586298 Methylene Chloride mg/l 0.0237 0 .025 94.8 52-130 L568306-05 WG586298 n-Butylbenzene mg/l 0.0336 0 .025 134. 62-142 L568306-05 WG586298 n-Propylbenzene mg/l 0.0248 0 .025 99.3 62-137 L568306-05 WG586298 Naphthalene mg/l 0.0284 0 .025 114. 65-140 L568306-05 WG586298 p-Isopropyltoluene mg/l 0.0249 0 .025 99.6 64-142 L568306-05 WG586298 sec-Butylbenzene mg/l 0.0253 0 .025 101. 67-139 L568306-05 WG586298 Styrene mg/l 0.0231 0 .025 92.4 58-152 L568306-05 WG586298 tert-Butylbenzene mg/l 0.0236 0 .025 94.4 66-139 L568306-05 WG586298 Tetrachloroethene mg/l 0.0506 0.0370 .025 54.4* 56-139 L568306-05 WG586298 Toluene mg/l 0.0266 0 .025 106. 61-126 L568306-05 WG586298 trans-1,2-Dichloroethene mg/l 0.0238 0 .025 95.4 45-137 L568306-05 WG586298 trans-1,3-Dichloropropene mg/l 0.0267 0 .025 107. 59-130 L568306-05 WG586298 Trichloroethene mg/l 0.0420 0.0200 .025 88.1 40-155 L568306-05 WG586298 Trichlorofluoromethane mg/l 0.0243 0 .025 97.1 35-177 L568306-05 WG586298 Vinyl chloride mg/l 0.0269 0 .025 107. 32-159 L568306-05 WG586298 Xylenes, Total mg/l 0.0680 0 .075 90.6 64-133 L568306-05 WG586298 4-Bromofluorobenzene 85.27 82-120 WG586298 Dibromofluoromethane 109.7 82-126 WG586298 Toluene-d8 110.6 92-112 WG586298

1,1,1,2-Tetrachloroethane mg/l 0.0252 0 .025 101. 71-130 L568306-08 WG586301 1,1,1-Trichloroethane mg/l 0.0215 0 .025 86.0 58-137 L568306-08 WG586301 1,1,2,2-Tetrachloroethane mg/l 0.0228 0 .025 91.3 64-149 L568306-08 WG586301 1,1,2-Trichloroethane mg/l 0.0239 0 .025 95.7 73-128 L568306-08 WG586301 1,1,2-Trichlorotrifluoroethane mg/l 0.0258 0 .025 103. 36-159 L568306-08 WG586301 1,1-Dichloroethane mg/l 0.0221 0 .025 88.5 58-133 L568306-08 WG586301 1,1-Dichloroethene mg/l 0.0223 0 .025 89.2 32-152 L568306-08 WG586301 1,1-Dichloropropene mg/l 0.0220 0 .025 88.0 50-140 L568306-08 WG586301 1,2,3-Trichlorobenzene mg/l 0.0227 0 .025 90.7 68-135 L568306-08 WG586301 1,2,3-Trichloropropane mg/l 0.0233 0 .025 93.1 74-137 L568306-08 WG586301 1,2,3-Trimethylbenzene mg/l 0.0205 0 .025 82.1 67-133 L568306-08 WG586301 1,2,4-Trichlorobenzene mg/l 0.0247 0 .025 98.8 67-133 L568306-08 WG586301 1,2,4-Trimethylbenzene mg/l 0.0239 0 .025 95.5 62-141 L568306-08 WG586301 1,2-Dibromo-3-Chloropropane mg/l 0.0230 0 .025 91.9 55-148 L568306-08 WG586301 1,2-Dibromoethane mg/l 0.0236 0 .025 94.4 71-129 L568306-08 WG586301 1,2-Dichlorobenzene mg/l 0.0228 0 .025 91.2 75-125 L568306-08 WG586301 1,2-Dichloroethane mg/l 0.0193 0 .025 77.4 59-135 L568306-08 WG586301 1,2-Dichloropropane mg/l 0.0231 0 .025 92.5 68-126 L568306-08 WG586301 1,3,5-Trimethylbenzene mg/l 0.0249 0 .025 99.6 67-136 L568306-08 WG586301 1,3-Dichlorobenzene mg/l 0.0252 0 .025 101. 69-131 L568306-08 WG586301 1,3-Dichloropropane mg/l 0.0237 0 .025 94.8 70-122 L568306-08 WG586301

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 44 of 49

Reference 45 Page 110

Page 111: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 April 05, 2012

L568306

Matrix SpikeAnalyte Units MS Res Ref Res TV % Rec Limit Ref Samp Batch

1,4-Dichlorobenzene mg/l 0.0226 0 .025 90.5 70-123 L568306-08 WG586301 2,2-Dichloropropane mg/l 0.0223 0 .025 89.4 51-141 L568306-08 WG586301 2-Butanone (MEK) mg/l 0.0816 0 .125 65.3 51-149 L568306-08 WG586301 2-Chloroethyl vinyl ether mg/l 0.0463 0 .125 37.1 10-161 L568306-08 WG586301 2-Chlorotoluene mg/l 0.0240 0 .025 96.1 65-133 L568306-08 WG586301 4-Chlorotoluene mg/l 0.0235 0 .025 93.9 67-129 L568306-08 WG586301 4-Methyl-2-pentanone (MIBK) mg/l 0.110 0 .125 87.9 53-154 L568306-08 WG586301 Acetone mg/l 0.0628 0 .125 50.2 34-146 L568306-08 WG586301 Acrolein mg/l 0.134 0 .125 107. 10-189 L568306-08 WG586301 Acrylonitrile mg/l 0.108 0 .125 86.8 49-162 L568306-08 WG586301 Benzene mg/l 0.0212 0 .025 84.7 51-134 L568306-08 WG586301 Bromobenzene mg/l 0.0223 0 .025 89.2 64-130 L568306-08 WG586301 Bromodichloromethane mg/l 0.0203 0 .025 81.2 67-132 L568306-08 WG586301 Bromoform mg/l 0.0243 0 .025 97.2 59-137 L568306-08 WG586301 Bromomethane mg/l 0.0249 0 .025 99.5 23-177 L568306-08 WG586301 Carbon tetrachloride mg/l 0.0227 0 .025 91.0 49-140 L568306-08 WG586301 Chlorobenzene mg/l 0.0244 0 .025 97.5 69-126 L568306-08 WG586301 Chlorodibromomethane mg/l 0.0241 0 .025 96.5 68-130 L568306-08 WG586301 Chloroethane mg/l 0.0226 0 .025 90.5 32-177 L568306-08 WG586301 Chloroform mg/l 0.0495 0.0280 .025 86.0 64-130 L568306-08 WG586301 Chloromethane mg/l 0.0232 0 .025 92.6 27-155 L568306-08 WG586301 cis-1,2-Dichloroethene mg/l 0.0211 0 .025 84.4 54-137 L568306-08 WG586301 cis-1,3-Dichloropropene mg/l 0.0212 0 .025 84.7 63-127 L568306-08 WG586301 Di-isopropyl ether mg/l 0.0220 0 .025 87.8 58-133 L568306-08 WG586301 Dibromomethane mg/l 0.0209 0 .025 83.7 68-131 L568306-08 WG586301 Dichlorodifluoromethane mg/l 0.0262 0 .025 105. 16-188 L568306-08 WG586301 Ethylbenzene mg/l 0.0253 0 .025 101. 64-135 L568306-08 WG586301 Hexachloro-1,3-butadiene mg/l 0.0252 0 .025 101. 64-140 L568306-08 WG586301 Isopropylbenzene mg/l 0.0278 0 .025 111. 62-134 L568306-08 WG586301 Methyl tert-butyl ether mg/l 0.0206 0 .025 82.4 55-136 L568306-08 WG586301 Methylene Chloride mg/l 0.0184 0 .025 73.7 52-130 L568306-08 WG586301 n-Butylbenzene mg/l 0.0239 0 .025 95.7 62-142 L568306-08 WG586301 n-Propylbenzene mg/l 0.0252 0 .025 101. 62-137 L568306-08 WG586301 Naphthalene mg/l 0.0204 0 .025 81.4 65-140 L568306-08 WG586301 p-Isopropyltoluene mg/l 0.0265 0 .025 106. 64-142 L568306-08 WG586301 sec-Butylbenzene mg/l 0.0262 0 .025 105. 67-139 L568306-08 WG586301 Styrene mg/l 0.0240 0 .025 95.9 58-152 L568306-08 WG586301 tert-Butylbenzene mg/l 0.0262 0 .025 105. 66-139 L568306-08 WG586301 Tetrachloroethene mg/l 0.0324 0.00560 .025 107. 56-139 L568306-08 WG586301 Toluene mg/l 0.0220 0 .025 88.2 61-126 L568306-08 WG586301 trans-1,2-Dichloroethene mg/l 0.0202 0 .025 81.0 45-137 L568306-08 WG586301 trans-1,3-Dichloropropene mg/l 0.0201 0 .025 80.6 59-130 L568306-08 WG586301 Trichloroethene mg/l 0.0253 0.00270 .025 90.5 40-155 L568306-08 WG586301 Trichlorofluoromethane mg/l 0.0254 0 .025 101. 35-177 L568306-08 WG586301 Vinyl chloride mg/l 0.0261 0 .025 104. 32-159 L568306-08 WG586301 Xylenes, Total mg/l 0.0750 0 .075 99.9 64-133 L568306-08 WG586301 4-Bromofluorobenzene 96.93 82-120 WG586301 Dibromofluoromethane 92.77 82-126 WG586301 Toluene-d8 98.93 92-112 WG586301

Matrix Spike DuplicateAnalyte Units MSD Ref %Rec Limit RPD Limit Ref Samp Batch

1,1,1,2-Tetrachloroethane mg/l 0.0233 0.0227 93.2 71-130 2.61 20 L568306-05 WG586298 1,1,1-Trichloroethane mg/l 0.0290 0.0287 116. 58-137 0.920 20 L568306-05 WG586298 1,1,2,2-Tetrachloroethane mg/l 0.0256 0.0253 102. 64-149 1.13 20 L568306-05 WG586298 1,1,2-Trichloroethane mg/l 0.0244 0.0241 97.7 73-128 1.33 20 L568306-05 WG586298 1,1,2-Trichlorotrifluoroethane mg/l 0.0209 0.0222 83.6 36-159 6.08 21 L568306-05 WG586298 1,1-Dichloroethane mg/l 0.0288 0.0286 115. 58-133 0.610 20 L568306-05 WG586298

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 45 of 49

Reference 45 Page 111

Page 112: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 April 05, 2012

L568306

Matrix Spike DuplicateAnalyte Units MSD Ref %Rec Limit RPD Limit Ref Samp Batch

1,1-Dichloroethene mg/l 0.0210 0.0211 84.2 32-152 0.490 20 L568306-05 WG586298 1,1-Dichloropropene mg/l 0.0271 0.0274 108. 50-140 0.800 20 L568306-05 WG586298 1,2,3-Trichlorobenzene mg/l 0.0309 0.0298 124. 68-135 3.57 20 L568306-05 WG586298 1,2,3-Trichloropropane mg/l 0.0248 0.0237 99.2 74-137 4.31 20 L568306-05 WG586298 1,2,3-Trimethylbenzene mg/l 0.0305 0.0304 122. 67-133 0.370 20 L568306-05 WG586298 1,2,4-Trichlorobenzene mg/l 0.0292 0.0294 117. 67-133 0.680 20 L568306-05 WG586298 1,2,4-Trimethylbenzene mg/l 0.0246 0.0238 98.2 62-141 3.16 20 L568306-05 WG586298 1,2-Dibromo-3-Chloropropane mg/l 0.0306 0.0292 122. 55-148 4.72 22 L568306-05 WG586298 1,2-Dibromoethane mg/l 0.0235 0.0234 93.8 71-129 0.380 20 L568306-05 WG586298 1,2-Dichlorobenzene mg/l 0.0294 0.0285 118. 75-125 3.19 20 L568306-05 WG586298 1,2-Dichloroethane mg/l 0.0279 0.0275 112. 59-135 1.53 20 L568306-05 WG586298 1,2-Dichloropropane mg/l 0.0288 0.0287 115. 68-126 0.310 20 L568306-05 WG586298 1,3,5-Trimethylbenzene mg/l 0.0246 0.0240 98.4 67-136 2.58 20 L568306-05 WG586298 1,3-Dichlorobenzene mg/l 0.0231 0.0218 92.3 69-131 5.62 20 L568306-05 WG586298 1,3-Dichloropropane mg/l 0.0248 0.0235 99.4 70-122 5.74 20 L568306-05 WG586298 1,4-Dichlorobenzene mg/l 0.0277 0.0274 111. 70-123 1.07 20 L568306-05 WG586298 2,2-Dichloropropane mg/l 0.0305 0.0303 122. 51-141 0.910 20 L568306-05 WG586298 2-Butanone (MEK) mg/l 0.109 0.110 87.4 51-149 0.870 22 L568306-05 WG586298 2-Chloroethyl vinyl ether mg/l 0.00114 0.00240 0.909* 10-161 71.4* 40 L568306-05 WG586298 2-Chlorotoluene mg/l 0.0257 0.0250 103. 65-133 2.82 20 L568306-05 WG586298 4-Chlorotoluene mg/l 0.0241 0.0234 96.5 67-129 3.12 20 L568306-05 WG586298 4-Methyl-2-pentanone (MIBK) mg/l 0.166 0.163 133. 53-154 1.88 21 L568306-05 WG586298 Acetone mg/l 0.0819 0.0790 65.5 34-146 3.54 22 L568306-05 WG586298 Acrolein mg/l 0.0359 0.0353 28.7 10-189 1.65 30 L568306-05 WG586298 Acrylonitrile mg/l 0.150 0.148 120. 49-162 1.54 20 L568306-05 WG586298 Benzene mg/l 0.0271 0.0269 108. 51-134 0.960 20 L568306-05 WG586298 Bromobenzene mg/l 0.0248 0.0238 99.3 64-130 4.06 20 L568306-05 WG586298 Bromodichloromethane mg/l 0.0278 0.0273 111. 67-132 1.71 20 L568306-05 WG586298 Bromoform mg/l 0.0228 0.0223 91.2 59-137 2.42 20 L568306-05 WG586298 Bromomethane mg/l 0.0230 0.0231 92.1 23-177 0.0900 21 L568306-05 WG586298 Carbon tetrachloride mg/l 0.0274 0.0267 110. 49-140 2.41 20 L568306-05 WG586298 Chlorobenzene mg/l 0.0233 0.0225 93.2 69-126 3.51 20 L568306-05 WG586298 Chlorodibromomethane mg/l 0.0235 0.0233 94.1 68-130 0.770 20 L568306-05 WG586298 Chloroethane mg/l 0.0270 0.0268 108. 32-177 0.950 21 L568306-05 WG586298 Chloroform mg/l 0.0288 0.0281 115. 64-130 2.35 20 L568306-05 WG586298 Chloromethane mg/l 0.0317 0.0319 127. 27-155 0.460 20 L568306-05 WG586298 cis-1,2-Dichloroethene mg/l 0.0283 0.0272 106. 54-137 3.81 20 L568306-05 WG586298 cis-1,3-Dichloropropene mg/l 0.0269 0.0268 108. 63-127 0.340 20 L568306-05 WG586298 Di-isopropyl ether mg/l 0.0300 0.0293 120. 58-133 2.25 20 L568306-05 WG586298 Dibromomethane mg/l 0.0278 0.0272 111. 68-131 2.10 20 L568306-05 WG586298 Dichlorodifluoromethane mg/l 0.0281 0.0279 112. 16-188 0.900 22 L568306-05 WG586298 Ethylbenzene mg/l 0.0231 0.0227 92.3 64-135 1.79 20 L568306-05 WG586298 Hexachloro-1,3-butadiene mg/l 0.0277 0.0276 111. 64-140 0.0600 20 L568306-05 WG586298 Isopropylbenzene mg/l 0.0250 0.0245 99.8 62-134 1.88 20 L568306-05 WG586298 Methyl tert-butyl ether mg/l 0.0272 0.0268 109. 55-136 1.34 20 L568306-05 WG586298 Methylene Chloride mg/l 0.0244 0.0237 97.8 52-130 3.05 20 L568306-05 WG586298 n-Butylbenzene mg/l 0.0341 0.0336 136. 62-142 1.58 20 L568306-05 WG586298 n-Propylbenzene mg/l 0.0253 0.0248 101. 62-137 1.98 20 L568306-05 WG586298 Naphthalene mg/l 0.0294 0.0284 118. 65-140 3.42 20 L568306-05 WG586298 p-Isopropyltoluene mg/l 0.0255 0.0249 102. 64-142 2.37 20 L568306-05 WG586298 sec-Butylbenzene mg/l 0.0254 0.0253 102. 67-139 0.500 20 L568306-05 WG586298 Styrene mg/l 0.0240 0.0231 95.8 58-152 3.68 20 L568306-05 WG586298 tert-Butylbenzene mg/l 0.0244 0.0236 97.7 66-139 3.47 20 L568306-05 WG586298 Tetrachloroethene mg/l 0.0536 0.0506 66.4 56-139 5.75 20 L568306-05 WG586298 Toluene mg/l 0.0271 0.0266 108. 61-126 1.80 20 L568306-05 WG586298 trans-1,2-Dichloroethene mg/l 0.0248 0.0238 99.0 45-137 3.76 20 L568306-05 WG586298 trans-1,3-Dichloropropene mg/l 0.0270 0.0267 108. 59-130 1.21 20 L568306-05 WG586298 Trichloroethene mg/l 0.0430 0.0420 91.9 40-155 2.24 20 L568306-05 WG586298 Trichlorofluoromethane mg/l 0.0242 0.0243 96.8 35-177 0.230 23 L568306-05 WG586298

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

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12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 April 05, 2012

L568306

Matrix Spike DuplicateAnalyte Units MSD Ref %Rec Limit RPD Limit Ref Samp Batch

Vinyl chloride mg/l 0.0270 0.0269 108. 32-159 0.440 21 L568306-05 WG586298 Xylenes, Total mg/l 0.0706 0.0680 94.2 64-133 3.86 20 L568306-05 WG586298 4-Bromofluorobenzene 85.80 82-120 WG586298 Dibromofluoromethane 109.9 82-126 WG586298 Toluene-d8 109.4 92-112 WG586298

1,1,1,2-Tetrachloroethane mg/l 0.0257 0.0252 103. 71-130 1.97 20 L568306-08 WG586301 1,1,1-Trichloroethane mg/l 0.0255 0.0215 102. 58-137 16.9 20 L568306-08 WG586301 1,1,2,2-Tetrachloroethane mg/l 0.0241 0.0228 96.3 64-149 5.30 20 L568306-08 WG586301 1,1,2-Trichloroethane mg/l 0.0242 0.0239 96.6 73-128 0.930 20 L568306-08 WG586301 1,1,2-Trichlorotrifluoroethane mg/l 0.0296 0.0258 118. 36-159 13.5 21 L568306-08 WG586301 1,1-Dichloroethane mg/l 0.0250 0.0221 100. 58-133 12.4 20 L568306-08 WG586301 1,1-Dichloroethene mg/l 0.0255 0.0223 102. 32-152 13.3 20 L568306-08 WG586301 1,1-Dichloropropene mg/l 0.0257 0.0220 103. 50-140 15.6 20 L568306-08 WG586301 1,2,3-Trichlorobenzene mg/l 0.0243 0.0227 97.0 68-135 6.75 20 L568306-08 WG586301 1,2,3-Trichloropropane mg/l 0.0233 0.0233 93.2 74-137 0.120 20 L568306-08 WG586301 1,2,3-Trimethylbenzene mg/l 0.0228 0.0205 91.1 67-133 10.4 20 L568306-08 WG586301 1,2,4-Trichlorobenzene mg/l 0.0265 0.0247 106. 67-133 6.94 20 L568306-08 WG586301 1,2,4-Trimethylbenzene mg/l 0.0249 0.0239 99.4 62-141 4.01 20 L568306-08 WG586301 1,2-Dibromo-3-Chloropropane mg/l 0.0252 0.0230 101. 55-148 9.31 22 L568306-08 WG586301 1,2-Dibromoethane mg/l 0.0241 0.0236 96.6 71-129 2.27 20 L568306-08 WG586301 1,2-Dichlorobenzene mg/l 0.0248 0.0228 99.1 75-125 8.27 20 L568306-08 WG586301 1,2-Dichloroethane mg/l 0.0217 0.0193 86.7 59-135 11.4 20 L568306-08 WG586301 1,2-Dichloropropane mg/l 0.0241 0.0231 96.4 68-126 4.12 20 L568306-08 WG586301 1,3,5-Trimethylbenzene mg/l 0.0259 0.0249 104. 67-136 3.91 20 L568306-08 WG586301 1,3-Dichlorobenzene mg/l 0.0258 0.0252 103. 69-131 2.67 20 L568306-08 WG586301 1,3-Dichloropropane mg/l 0.0243 0.0237 97.3 70-122 2.58 20 L568306-08 WG586301 1,4-Dichlorobenzene mg/l 0.0251 0.0226 100. 70-123 10.2 20 L568306-08 WG586301 2,2-Dichloropropane mg/l 0.0274 0.0223 110. 51-141 20.5* 20 L568306-08 WG586301 2-Butanone (MEK) mg/l 0.0955 0.0816 76.4 51-149 15.7 22 L568306-08 WG586301 2-Chloroethyl vinyl ether mg/l 0.0112 0.0463 8.94* 10-161 122.* 40 L568306-08 WG586301 2-Chlorotoluene mg/l 0.0247 0.0240 98.8 65-133 2.76 20 L568306-08 WG586301 4-Chlorotoluene mg/l 0.0241 0.0235 96.4 67-129 2.65 20 L568306-08 WG586301 4-Methyl-2-pentanone (MIBK) mg/l 0.122 0.110 97.6 53-154 10.4 21 L568306-08 WG586301 Acetone mg/l 0.0750 0.0628 60.0 34-146 17.7 22 L568306-08 WG586301 Acrolein mg/l 0.159 0.134 127. 10-189 17.4 30 L568306-08 WG586301 Acrylonitrile mg/l 0.125 0.108 99.6 49-162 13.8 20 L568306-08 WG586301 Benzene mg/l 0.0239 0.0212 95.4 51-134 11.9 20 L568306-08 WG586301 Bromobenzene mg/l 0.0229 0.0223 91.5 64-130 2.61 20 L568306-08 WG586301 Bromodichloromethane mg/l 0.0220 0.0203 88.0 67-132 7.99 20 L568306-08 WG586301 Bromoform mg/l 0.0260 0.0243 104. 59-137 6.63 20 L568306-08 WG586301 Bromomethane mg/l 0.0287 0.0249 115. 23-177 14.1 21 L568306-08 WG586301 Carbon tetrachloride mg/l 0.0257 0.0227 103. 49-140 12.3 20 L568306-08 WG586301 Chlorobenzene mg/l 0.0254 0.0244 102. 69-126 4.15 20 L568306-08 WG586301 Chlorodibromomethane mg/l 0.0250 0.0241 100. 68-130 3.61 20 L568306-08 WG586301 Chloroethane mg/l 0.0271 0.0226 108. 32-177 17.8 21 L568306-08 WG586301 Chloroform mg/l 0.0524 0.0495 97.7 64-130 5.77 20 L568306-08 WG586301 Chloromethane mg/l 0.0271 0.0232 108. 27-155 15.5 20 L568306-08 WG586301 cis-1,2-Dichloroethene mg/l 0.0240 0.0211 96.1 54-137 13.0 20 L568306-08 WG586301 cis-1,3-Dichloropropene mg/l 0.0226 0.0212 90.4 63-127 6.44 20 L568306-08 WG586301 Di-isopropyl ether mg/l 0.0247 0.0220 98.6 58-133 11.5 20 L568306-08 WG586301 Dibromomethane mg/l 0.0226 0.0209 90.3 68-131 7.58 20 L568306-08 WG586301 Dichlorodifluoromethane mg/l 0.0302 0.0262 121. 16-188 14.3 22 L568306-08 WG586301 Ethylbenzene mg/l 0.0270 0.0253 108. 64-135 6.75 20 L568306-08 WG586301 Hexachloro-1,3-butadiene mg/l 0.0270 0.0252 108. 64-140 7.12 20 L568306-08 WG586301 Isopropylbenzene mg/l 0.0295 0.0278 118. 62-134 5.92 20 L568306-08 WG586301 Methyl tert-butyl ether mg/l 0.0229 0.0206 91.6 55-136 10.5 20 L568306-08 WG586301 Methylene Chloride mg/l 0.0211 0.0184 84.2 52-130 13.3 20 L568306-08 WG586301

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

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12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 April 05, 2012

L568306

Matrix Spike DuplicateAnalyte Units MSD Ref %Rec Limit RPD Limit Ref Samp Batch

n-Butylbenzene mg/l 0.0257 0.0239 103. 62-142 7.18 20 L568306-08 WG586301 n-Propylbenzene mg/l 0.0264 0.0252 106. 62-137 4.57 20 L568306-08 WG586301 Naphthalene mg/l 0.0225 0.0204 90.1 65-140 10.1 20 L568306-08 WG586301 p-Isopropyltoluene mg/l 0.0274 0.0265 110. 64-142 3.15 20 L568306-08 WG586301 sec-Butylbenzene mg/l 0.0274 0.0262 110. 67-139 4.43 20 L568306-08 WG586301 Styrene mg/l 0.0249 0.0240 99.5 58-152 3.70 20 L568306-08 WG586301 tert-Butylbenzene mg/l 0.0276 0.0262 110. 66-139 5.23 20 L568306-08 WG586301 Tetrachloroethene mg/l 0.0332 0.0324 110. 56-139 2.61 20 L568306-08 WG586301 Toluene mg/l 0.0243 0.0220 97.0 61-126 9.60 20 L568306-08 WG586301 trans-1,2-Dichloroethene mg/l 0.0230 0.0202 92.0 45-137 12.7 20 L568306-08 WG586301 trans-1,3-Dichloropropene mg/l 0.0215 0.0201 85.8 59-130 6.31 20 L568306-08 WG586301 Trichloroethene mg/l 0.0271 0.0253 97.5 40-155 6.64 20 L568306-08 WG586301 Trichlorofluoromethane mg/l 0.0297 0.0254 119. 35-177 15.9 23 L568306-08 WG586301 Vinyl chloride mg/l 0.0288 0.0261 115. 32-159 10.1 21 L568306-08 WG586301 Xylenes, Total mg/l 0.0777 0.0750 104. 64-133 3.57 20 L568306-08 WG586301 4-Bromofluorobenzene 93.07 82-120 WG586301 Dibromofluoromethane 100.3 82-126 WG586301 Toluene-d8 99.05 92-112 WG586301

Batch number /Run number / Sample number cross reference

WG586298: R2105701: L568306-01 02 03 04 05 06 07WG586301: R2106793: L568306-08 09 10 11 12 13 14 15 16 17

* * Calculations are performed prior to rounding of reported values.* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

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12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 April 05, 2012

L568306

The data package includes a summary of the analytic results of the qualitycontrol samples required by the SW-846 or CWA methods. The quality controlsamples include a method blank, a laboratory control sample, and the matrixspike/matrix spike duplicate analysis. If a target parameter is outsidethe method limits, every sample that is effected is flagged with theappropriate qualifier in Appendix B of the analytic report.

Method Blank - an aliquot of reagent water carried through theentire analytic process. The method blank results indicate ifany possible contamination exposure during the sample handling,digestion or extraction process, and analysis. Concentrations oftarget analytes above the reporting limit in the method blank arequalified with the "B" qualifier.

Laboratory Control Sample - is a sample of known concentrationthat is carried through the digestion/extraction and analysisprocess. The percent recovery, expressed as a percentage of thetheoretical concentration, has statistical control limitsindicating that the analytic process is "in control". If atarget analyte is outside the control limits for the laboratorycontrol sample or any other control sample, the parameter isflagged with a "J4" qualifier for all effected samples.

Matrix Spike and Matrix Spike Duplicate - is two aliquots of anenvironmental sample that is spiked with known concentrations oftarget analytes. The percent recovery of the target analytesalso has statistical control limits. If any recoveries that areoutside the method control limits, the sample that was selectedfor matrix spike/matrix spike duplicate analysis is flagged witheither a "J5" or a "J6". The relative percent difference (%RPD)between the matrix spike and the matrix spike duplicaterecoveries is all calculated. If the RPD is above the methodlimit, the effected samples are flagged with a "J3" qualifier.

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12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

Mrs. Wendy MilejczakAcuity Environmental Solutions7965 East 106th St. Suite 128Fishers, IN 46038

Report Summary

Friday June 15, 2012

Report Number: L579547

Samples Received: 06/09/12

Client Project: 1024-1003-01

Description: Component Machine

The analytical results in this report are based upon information suppliedby you, the client, and are for your exclusive use. If you have anyquestions regarding this data package, please do not hesitate to call.

Entire Report Reviewed By: ____________________________________

T. Alan Harvill , ESC Representative

Laboratory Certification NumbersA2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197,FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,NC - ENV375/DW21704/BIO041, ND - R-140. NJ - TN002, NJ NELAP - TN002,SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,TX - T104704245-11-3, OK - 9915, PA - 68-02979

Accreditation is only applicable to the test methods specified on each scope of accreditation heldby ESC Lab Sciences.Note: The use of the preparatory EPA Method 3511 is not approved or endorsed by the CA ELAP.

This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.Where applicable, sampling conducted by ESC is performed per guidance providedin laboratory standard operating procedures: 060302, 060303, and 060304.

Page 1 of 49

Reference 45 Page 116

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12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-01 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : PMW-4

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 08:55

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 06/10/12 1 Acrolein BDL 50. ug/l 8260B 06/10/12 1 Acrylonitrile BDL 10. ug/l 8260B 06/10/12 1 Benzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 06/10/12 1 Bromoform BDL 1.0 ug/l 8260B 06/10/12 1 Bromomethane BDL 5.0 ug/l 8260B 06/10/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 06/10/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 Chloroethane BDL 5.0 ug/l 8260B 06/10/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 06/10/12 1 Chloroform BDL 5.0 ug/l 8260B 06/10/12 1 Chloromethane BDL 2.5 ug/l 8260B 06/10/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 06/10/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 06/10/12 1 Dibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,2-Dichloroethene 11. 1.0 ug/l 8260B 06/10/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 06/10/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 2 of 49

Reference 45 Page 117

Page 118: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-01 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : PMW-4

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 08:55

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 06/10/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 06/10/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 06/10/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Naphthalene BDL 5.0 ug/l 8260B 06/10/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Styrene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 06/10/12 1 Tetrachloroethene 200 5.0 ug/l 8260B 06/13/12 5 Toluene BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1-Trichloroethane 3.2 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 Trichloroethene 50. 1.0 ug/l 8260B 06/10/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 06/10/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 06/10/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 06/10/12 1

Surrogate Recovery Toluene-d8 99.0 % Rec. 8260B 06/10/12 1 Dibromofluoromethane 98.5 % Rec. 8260B 06/10/12 1 4-Bromofluorobenzene 105. % Rec. 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 06/15/12 15:49 Printed: 06/15/12 15:49

Page 3 of 49

Reference 45 Page 118

Page 119: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-02 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : PMW-5

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 09:30

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 06/10/12 1 Acrolein BDL 50. ug/l 8260B 06/10/12 1 Acrylonitrile BDL 10. ug/l 8260B 06/10/12 1 Benzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 06/10/12 1 Bromoform BDL 1.0 ug/l 8260B 06/10/12 1 Bromomethane BDL 5.0 ug/l 8260B 06/10/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 06/10/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 Chloroethane BDL 5.0 ug/l 8260B 06/10/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 06/10/12 1 Chloroform 8.8 5.0 ug/l 8260B 06/10/12 1 Chloromethane BDL 2.5 ug/l 8260B 06/10/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 06/10/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 06/10/12 1 Dibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 06/10/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 4 of 49

Reference 45 Page 119

Page 120: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-02 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : PMW-5

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 09:30

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 06/10/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 06/10/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 06/10/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Naphthalene BDL 5.0 ug/l 8260B 06/10/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Styrene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 06/10/12 1 Tetrachloroethene 18. 1.0 ug/l 8260B 06/10/12 1 Toluene BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 Trichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 06/10/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 06/10/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 06/10/12 1

Surrogate Recovery Toluene-d8 99.9 % Rec. 8260B 06/10/12 1 Dibromofluoromethane 99.2 % Rec. 8260B 06/10/12 1 4-Bromofluorobenzene 107. % Rec. 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 06/15/12 15:49 Printed: 06/15/12 15:49

Page 5 of 49

Reference 45 Page 120

Page 121: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-03 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : MW-8

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 10:10

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 06/10/12 1 Acrolein BDL 50. ug/l 8260B 06/10/12 1 Acrylonitrile BDL 10. ug/l 8260B 06/10/12 1 Benzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 06/10/12 1 Bromoform BDL 1.0 ug/l 8260B 06/10/12 1 Bromomethane BDL 5.0 ug/l 8260B 06/10/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 06/10/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 Chloroethane BDL 5.0 ug/l 8260B 06/10/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 06/10/12 1 Chloroform 10. 5.0 ug/l 8260B 06/10/12 1 Chloromethane BDL 2.5 ug/l 8260B 06/10/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 06/10/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 06/10/12 1 Dibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,2-Dichloroethene 18. 1.0 ug/l 8260B 06/10/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 06/10/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 6 of 49

Reference 45 Page 121

Page 122: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-03 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : MW-8

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 10:10

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 06/10/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 06/10/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 06/10/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Naphthalene BDL 5.0 ug/l 8260B 06/10/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Styrene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 06/10/12 1 Tetrachloroethene 50. 1.0 ug/l 8260B 06/10/12 1 Toluene BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1-Trichloroethane 1.5 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 Trichloroethene 28. 1.0 ug/l 8260B 06/10/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 06/10/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 06/10/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 06/10/12 1

Surrogate Recovery Toluene-d8 100. % Rec. 8260B 06/10/12 1 Dibromofluoromethane 99.6 % Rec. 8260B 06/10/12 1 4-Bromofluorobenzene 105. % Rec. 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 06/15/12 15:49 Printed: 06/15/12 15:50

Page 7 of 49

Reference 45 Page 122

Page 123: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-04 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : MW-11

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 14:00

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 06/10/12 1 Acrolein BDL 50. ug/l 8260B 06/10/12 1 Acrylonitrile BDL 10. ug/l 8260B 06/10/12 1 Benzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 06/10/12 1 Bromoform BDL 1.0 ug/l 8260B 06/10/12 1 Bromomethane BDL 5.0 ug/l 8260B 06/10/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 06/10/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 Chloroethane BDL 5.0 ug/l 8260B 06/10/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 06/10/12 1 Chloroform BDL 5.0 ug/l 8260B 06/10/12 1 Chloromethane BDL 2.5 ug/l 8260B 06/10/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 06/10/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 06/10/12 1 Dibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,2-Dichloroethene 2.3 1.0 ug/l 8260B 06/10/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 06/10/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 8 of 49

Reference 45 Page 123

Page 124: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-04 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : MW-11

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 14:00

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 06/10/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 06/10/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 06/10/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Naphthalene BDL 5.0 ug/l 8260B 06/10/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Styrene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 06/10/12 1 Tetrachloroethene 3.8 1.0 ug/l 8260B 06/10/12 1 Toluene BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1-Trichloroethane 1.9 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 Trichloroethene 32. 1.0 ug/l 8260B 06/10/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 06/10/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 06/10/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 06/10/12 1

Surrogate Recovery Toluene-d8 99.3 % Rec. 8260B 06/10/12 1 Dibromofluoromethane 98.1 % Rec. 8260B 06/10/12 1 4-Bromofluorobenzene 106. % Rec. 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 06/15/12 15:49 Printed: 06/15/12 15:50

Page 9 of 49

Reference 45 Page 124

Page 125: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15, 2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-05 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : PMW-1

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 10:45

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 06/10/12 1 Acrolein BDL 50. ug/l 8260B 06/10/12 1 Acrylonitrile BDL 10. ug/l 8260B 06/10/12 1 Benzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 06/10/12 1 Bromoform BDL 1.0 ug/l 8260B 06/10/12 1 Bromomethane BDL 5.0 ug/l 8260B 06/10/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 06/10/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 Chloroethane BDL 5.0 ug/l 8260B 06/10/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 06/10/12 1 Chloroform BDL 5.0 ug/l 8260B 06/10/12 1 Chloromethane BDL 2.5 ug/l 8260B 06/10/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 06/10/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 06/10/12 1 Dibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 06/10/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 10 of 49

Reference 45 Page 125

Page 126: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15, 2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-05 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : PMW-1

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 10:45

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 06/10/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 06/10/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 06/10/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Naphthalene BDL 5.0 ug/l 8260B 06/10/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Styrene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 06/10/12 1 Tetrachloroethene 32. 1.0 ug/l 8260B 06/10/12 1 Toluene BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 Trichloroethene 12. 1.0 ug/l 8260B 06/10/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 06/10/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 06/10/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 06/10/12 1

Surrogate Recovery Toluene-d8 99.0 % Rec. 8260B 06/10/12 1 Dibromofluoromethane 97.9 % Rec. 8260B 06/10/12 1 4-Bromofluorobenzene 108. % Rec. 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 06/15/12 15:49 Printed: 06/15/12 15:50

Page 11 of 49

Reference 45 Page 126

Page 127: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15, 2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-06 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : PMW-1 MS

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 10:45

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Matrix Spike See QC Report for % Rec. and RPD

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 06/15/12 15:49 Printed: 06/15/12 15:50

Page 12 of 49

Reference 45 Page 127

Page 128: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-07 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : PMW-1 MSD

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 10:45

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics MSD See QC Report for % Rec and RPD

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 06/15/12 15:49 Printed: 06/15/12 15:50

Page 13 of 49

Reference 45 Page 128

Page 129: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-08 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : MW-10

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 12:05

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 06/10/12 1 Acrolein BDL 50. ug/l 8260B 06/10/12 1 Acrylonitrile BDL 10. ug/l 8260B 06/10/12 1 Benzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 06/10/12 1 Bromoform BDL 1.0 ug/l 8260B 06/10/12 1 Bromomethane BDL 5.0 ug/l 8260B 06/10/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 06/10/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 Chloroethane BDL 5.0 ug/l 8260B 06/10/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 06/10/12 1 Chloroform 31. 5.0 ug/l 8260B 06/10/12 1 Chloromethane BDL 2.5 ug/l 8260B 06/10/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 06/10/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 06/10/12 1 Dibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 06/10/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 14 of 49

Reference 45 Page 129

Page 130: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-08 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : MW-10

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 12:05

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 06/10/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 06/10/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 06/10/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Naphthalene BDL 5.0 ug/l 8260B 06/10/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Styrene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 06/10/12 1 Tetrachloroethene 10. 1.0 ug/l 8260B 06/10/12 1 Toluene BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 Trichloroethene 4.4 1.0 ug/l 8260B 06/10/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 06/10/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 06/10/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 06/10/12 1

Surrogate Recovery Toluene-d8 101. % Rec. 8260B 06/10/12 1 Dibromofluoromethane 101. % Rec. 8260B 06/10/12 1 4-Bromofluorobenzene 105. % Rec. 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 06/15/12 15:49 Printed: 06/15/12 15:50

Page 15 of 49

Reference 45 Page 130

Page 131: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-09 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : MW-9

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 11:30

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 06/10/12 1 Acrolein BDL 50. ug/l 8260B 06/10/12 1 Acrylonitrile BDL 10. ug/l 8260B 06/10/12 1 Benzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 06/10/12 1 Bromoform BDL 1.0 ug/l 8260B 06/10/12 1 Bromomethane BDL 5.0 ug/l 8260B 06/10/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 06/10/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 Chloroethane BDL 5.0 ug/l 8260B 06/10/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 06/10/12 1 Chloroform BDL 5.0 ug/l 8260B 06/10/12 1 Chloromethane BDL 2.5 ug/l 8260B 06/10/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 06/10/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 06/10/12 1 Dibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,2-Dichloroethene 2.4 1.0 ug/l 8260B 06/10/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 06/10/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 16 of 49

Reference 45 Page 131

Page 132: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-09 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : MW-9

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 11:30

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 06/10/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 06/10/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 06/10/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Naphthalene BDL 5.0 ug/l 8260B 06/10/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Styrene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 06/10/12 1 Tetrachloroethene 92. 1.0 ug/l 8260B 06/10/12 1 Toluene BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1-Trichloroethane 1.3 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 Trichloroethene 25. 1.0 ug/l 8260B 06/10/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 06/10/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 06/10/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 06/10/12 1

Surrogate Recovery Toluene-d8 99.4 % Rec. 8260B 06/10/12 1 Dibromofluoromethane 98.6 % Rec. 8260B 06/10/12 1 4-Bromofluorobenzene 107. % Rec. 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 06/15/12 15:49 Printed: 06/15/12 15:50

Page 17 of 49

Reference 45 Page 132

Page 133: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-10 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : PMW-6

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 13:35

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 06/10/12 1 Acrolein BDL 50. ug/l 8260B 06/10/12 1 Acrylonitrile BDL 10. ug/l 8260B 06/10/12 1 Benzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 06/10/12 1 Bromoform BDL 1.0 ug/l 8260B 06/10/12 1 Bromomethane BDL 5.0 ug/l 8260B 06/10/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Carbon tetrachloride 1.8 1.0 ug/l 8260B 06/10/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 Chloroethane BDL 5.0 ug/l 8260B 06/10/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 06/10/12 1 Chloroform 5.8 5.0 ug/l 8260B 06/10/12 1 Chloromethane BDL 2.5 ug/l 8260B 06/10/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 06/10/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 06/10/12 1 Dibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,2-Dichloroethene 1.3 1.0 ug/l 8260B 06/10/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 06/10/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 18 of 49

Reference 45 Page 133

Page 134: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-10 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : PMW-6

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 13:35

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 06/10/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 06/10/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 06/10/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Naphthalene BDL 5.0 ug/l 8260B 06/10/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Styrene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 06/10/12 1 Tetrachloroethene 11. 1.0 ug/l 8260B 06/10/12 1 Toluene BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1-Trichloroethane 2.4 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 Trichloroethene 56. 1.0 ug/l 8260B 06/10/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 06/10/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 06/10/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 06/10/12 1

Surrogate Recovery Toluene-d8 100. % Rec. 8260B 06/10/12 1 Dibromofluoromethane 98.4 % Rec. 8260B 06/10/12 1 4-Bromofluorobenzene 105. % Rec. 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 06/15/12 15:49 Printed: 06/15/12 15:50

Page 19 of 49

Reference 45 Page 134

Page 135: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-11 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : MW-12

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 13:05

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 06/10/12 1 Acrolein BDL 50. ug/l 8260B 06/10/12 1 Acrylonitrile BDL 10. ug/l 8260B 06/10/12 1 Benzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 06/10/12 1 Bromoform BDL 1.0 ug/l 8260B 06/10/12 1 Bromomethane BDL 5.0 ug/l 8260B 06/10/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Carbon tetrachloride 1.2 1.0 ug/l 8260B 06/10/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 Chloroethane BDL 5.0 ug/l 8260B 06/10/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 06/10/12 1 Chloroform BDL 5.0 ug/l 8260B 06/10/12 1 Chloromethane BDL 2.5 ug/l 8260B 06/10/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 06/10/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 06/10/12 1 Dibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 06/10/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 20 of 49

Reference 45 Page 135

Page 136: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-11 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : MW-12

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 13:05

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 06/10/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 06/10/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 06/10/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Naphthalene BDL 5.0 ug/l 8260B 06/10/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Styrene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 06/10/12 1 Tetrachloroethene 23. 1.0 ug/l 8260B 06/10/12 1 Toluene BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 Trichloroethene 9.1 1.0 ug/l 8260B 06/10/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 06/10/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 06/10/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 06/10/12 1

Surrogate Recovery Toluene-d8 101. % Rec. 8260B 06/10/12 1 Dibromofluoromethane 98.7 % Rec. 8260B 06/10/12 1 4-Bromofluorobenzene 107. % Rec. 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 06/15/12 15:49 Printed: 06/15/12 15:50

Page 21 of 49

Reference 45 Page 136

Page 137: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-12 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : MW-13

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 12:20

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 06/10/12 1 Acrolein BDL 50. ug/l 8260B 06/10/12 1 Acrylonitrile BDL 10. ug/l 8260B 06/10/12 1 Benzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 06/10/12 1 Bromoform BDL 1.0 ug/l 8260B 06/10/12 1 Bromomethane BDL 5.0 ug/l 8260B 06/10/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 06/10/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 Chloroethane BDL 5.0 ug/l 8260B 06/10/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 06/10/12 1 Chloroform 32. 5.0 ug/l 8260B 06/10/12 1 Chloromethane BDL 2.5 ug/l 8260B 06/10/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 06/10/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 06/10/12 1 Dibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 06/10/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 22 of 49

Reference 45 Page 137

Page 138: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-12 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : MW-13

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 12:20

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 06/10/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 06/10/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 06/10/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Naphthalene BDL 5.0 ug/l 8260B 06/10/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Styrene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 06/10/12 1 Tetrachloroethene 1.3 1.0 ug/l 8260B 06/10/12 1 Toluene BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 Trichloroethene 1.6 1.0 ug/l 8260B 06/10/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 06/10/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 06/10/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 06/10/12 1

Surrogate Recovery Toluene-d8 102. % Rec. 8260B 06/10/12 1 Dibromofluoromethane 103. % Rec. 8260B 06/10/12 1 4-Bromofluorobenzene 102. % Rec. 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 06/15/12 15:49 Printed: 06/15/12 15:50

Page 23 of 49

Reference 45 Page 138

Page 139: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-13 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : MW-14

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 11:25

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 06/10/12 1 Acrolein BDL 50. ug/l 8260B 06/10/12 1 Acrylonitrile BDL 10. ug/l 8260B 06/10/12 1 Benzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 06/10/12 1 Bromoform BDL 1.0 ug/l 8260B 06/10/12 1 Bromomethane BDL 5.0 ug/l 8260B 06/10/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 06/10/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 Chloroethane BDL 5.0 ug/l 8260B 06/10/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 06/10/12 1 Chloroform BDL 5.0 ug/l 8260B 06/10/12 1 Chloromethane BDL 2.5 ug/l 8260B 06/10/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 06/10/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 06/10/12 1 Dibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,2-Dichloroethene 1.6 1.0 ug/l 8260B 06/10/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 06/10/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 24 of 49

Reference 45 Page 139

Page 140: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-13 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : MW-14

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 11:25

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 06/10/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 06/10/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 06/10/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Naphthalene BDL 5.0 ug/l 8260B 06/10/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Styrene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 06/10/12 1 Tetrachloroethene 40. 1.0 ug/l 8260B 06/10/12 1 Toluene BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1-Trichloroethane 1.8 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 Trichloroethene 46. 1.0 ug/l 8260B 06/10/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 06/10/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 06/10/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 06/10/12 1

Surrogate Recovery Toluene-d8 102. % Rec. 8260B 06/10/12 1 Dibromofluoromethane 103. % Rec. 8260B 06/10/12 1 4-Bromofluorobenzene 101. % Rec. 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 06/15/12 15:49 Printed: 06/15/12 15:50

Page 25 of 49

Reference 45 Page 140

Page 141: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-14 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : MW-15

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 11:00

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 06/10/12 1 Acrolein BDL 50. ug/l 8260B 06/10/12 1 Acrylonitrile BDL 10. ug/l 8260B 06/10/12 1 Benzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 06/10/12 1 Bromoform BDL 1.0 ug/l 8260B 06/10/12 1 Bromomethane BDL 5.0 ug/l 8260B 06/10/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 06/10/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 Chloroethane BDL 5.0 ug/l 8260B 06/10/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 06/10/12 1 Chloroform BDL 5.0 ug/l 8260B 06/10/12 1 Chloromethane BDL 2.5 ug/l 8260B 06/10/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 06/10/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 06/10/12 1 Dibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 06/10/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 26 of 49

Reference 45 Page 141

Page 142: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-14 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : MW-15

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 11:00

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 06/10/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 06/10/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 06/10/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Naphthalene BDL 5.0 ug/l 8260B 06/10/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Styrene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 06/10/12 1 Tetrachloroethene 140 1.0 ug/l 8260B 06/10/12 1 Toluene BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1-Trichloroethane 2.7 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 Trichloroethene 56. 1.0 ug/l 8260B 06/10/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 06/10/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 06/10/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 06/10/12 1

Surrogate Recovery Toluene-d8 102. % Rec. 8260B 06/10/12 1 Dibromofluoromethane 105. % Rec. 8260B 06/10/12 1 4-Bromofluorobenzene 103. % Rec. 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 06/15/12 15:49 Printed: 06/15/12 15:50

Page 27 of 49

Reference 45 Page 142

Page 143: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-15 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : MW-16

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 10:25

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 06/10/12 1 Acrolein BDL 50. ug/l 8260B 06/10/12 1 Acrylonitrile BDL 10. ug/l 8260B 06/10/12 1 Benzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 06/10/12 1 Bromoform BDL 1.0 ug/l 8260B 06/10/12 1 Bromomethane BDL 5.0 ug/l 8260B 06/10/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 06/10/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 Chloroethane BDL 5.0 ug/l 8260B 06/10/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 06/10/12 1 Chloroform BDL 5.0 ug/l 8260B 06/10/12 1 Chloromethane BDL 2.5 ug/l 8260B 06/10/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 06/10/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 06/10/12 1 Dibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 06/10/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 28 of 49

Reference 45 Page 143

Page 144: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-15 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : MW-16

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 10:25

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 06/10/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 06/10/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 06/10/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Naphthalene BDL 5.0 ug/l 8260B 06/10/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Styrene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 06/10/12 1 Tetrachloroethene 3.2 1.0 ug/l 8260B 06/10/12 1 Toluene BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1-Trichloroethane 9.8 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 Trichloroethene 87. 1.0 ug/l 8260B 06/10/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 06/10/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 06/10/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 06/10/12 1

Surrogate Recovery Toluene-d8 102. % Rec. 8260B 06/10/12 1 Dibromofluoromethane 104. % Rec. 8260B 06/10/12 1 4-Bromofluorobenzene 101. % Rec. 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 06/15/12 15:49 Printed: 06/15/12 15:50

Page 29 of 49

Reference 45 Page 144

Page 145: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-16 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : DUP

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 06/10/12 1 Acrolein BDL 50. ug/l 8260B 06/10/12 1 Acrylonitrile BDL 10. ug/l 8260B 06/10/12 1 Benzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 06/10/12 1 Bromoform BDL 1.0 ug/l 8260B 06/10/12 1 Bromomethane BDL 5.0 ug/l 8260B 06/10/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 06/10/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 Chloroethane BDL 5.0 ug/l 8260B 06/10/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 06/10/12 1 Chloroform BDL 5.0 ug/l 8260B 06/10/12 1 Chloromethane BDL 2.5 ug/l 8260B 06/10/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 06/10/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 06/10/12 1 Dibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,2-Dichloroethene 9.4 1.0 ug/l 8260B 06/10/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 06/10/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 30 of 49

Reference 45 Page 145

Page 146: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-16 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : DUP

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 06/10/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 06/10/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 06/10/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Naphthalene BDL 5.0 ug/l 8260B 06/10/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Styrene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 06/10/12 1 Tetrachloroethene 140 1.0 ug/l 8260B 06/10/12 1 Toluene BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1-Trichloroethane 2.6 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 Trichloroethene 40. 1.0 ug/l 8260B 06/10/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 06/10/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 06/10/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 06/10/12 1

Surrogate Recovery Toluene-d8 104. % Rec. 8260B 06/10/12 1 Dibromofluoromethane 105. % Rec. 8260B 06/10/12 1 4-Bromofluorobenzene 103. % Rec. 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 06/15/12 15:49 Printed: 06/15/12 15:50

Page 31 of 49

Reference 45 Page 146

Page 147: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-17 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : TRIP BLANK

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 06/10/12 1 Acrolein BDL 50. ug/l 8260B 06/10/12 1 Acrylonitrile BDL 10. ug/l 8260B 06/10/12 1 Benzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 06/10/12 1 Bromoform BDL 1.0 ug/l 8260B 06/10/12 1 Bromomethane BDL 5.0 ug/l 8260B 06/10/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 06/10/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 Chloroethane BDL 5.0 ug/l 8260B 06/10/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 06/10/12 1 Chloroform BDL 5.0 ug/l 8260B 06/10/12 1 Chloromethane BDL 2.5 ug/l 8260B 06/10/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 06/10/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 06/10/12 1 Dibromomethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 06/10/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 06/10/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 06/10/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 32 of 49

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12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak June 15,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L579547-17 Date Received : June 09, 2012 Description : Component Machine

Site ID : Sample ID : TRIP BLANK

Project # : 1024-1003-01 Collected By : W. Milejczak Collection Date : 06/07/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 06/10/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 06/10/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 06/10/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 06/10/12 1 Naphthalene BDL 5.0 ug/l 8260B 06/10/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Styrene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 06/10/12 1 Tetrachloroethene BDL 1.0 ug/l 8260B 06/10/12 1 Toluene BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 06/10/12 1 Trichloroethene BDL 1.0 ug/l 8260B 06/10/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 06/10/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 06/10/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 06/10/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 06/10/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 06/10/12 1

Surrogate Recovery Toluene-d8 103. % Rec. 8260B 06/10/12 1 Dibromofluoromethane 104. % Rec. 8260B 06/10/12 1 4-Bromofluorobenzene 101. % Rec. 8260B 06/10/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 06/15/12 15:49 Printed: 06/15/12 15:50

Page 33 of 49

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Attachment AList of Analytes with QC Qualifiers

Sample Work Sample Run Number Group Type Analyte ID Qualifier ________________ ___________ _______ ________________________________________ __________ __________

L579547-05 WG597107 SAMP 2-Chloroethyl vinyl ether R2206795 J3

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Attachment BExplanation of QC Qualifier Codes

Qualifier Meaning __________________ _______________________________________________________________________________

J3 The associated batch QC was outside the established quality control rangefor precision.

Qualifier Report Information

ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program andas required by most certifying bodies including NELAC. In addition to the EPA qualifiers adoptedby ESC, we have implemented ESC qualifiers to provide more information pertaining to our analyticalresults. Each qualifier is designated in the qualifier explanation as either EPA or ESC.Data qualifiers are intended to provide the ESC client with more detailed information concerningthe potential bias of reported data. Because of the wide range of constituents and variety ofmatrices incorporated by most EPA methods,it is common for some compounds to fall outside ofestablished ranges. These exceptions are evaluated and all reported data is valid and useable"unless qualified as 'R' (Rejected)."

DefinitionsAccuracy - The relationship of the observed value of a known sample to the

true value of a known sample. Represented by percent recovery andrelevant to samples such as: control samples, matrix spike recoveries,surrogate recoveries, etc.

Precision - The agreement between a set of samples or between duplicate samples.Relates to how close together the results are and is represented byRelative Percent Differrence.

Surrogate - Organic compounds that are similar in chemical composition, extraction,and chromotography to analytes of interest. The surrogates are used todetermine the probable response of the group of analytes that are chem-ically related to the surrogate compound. Surrogates are added to thesample and carried through all stages of preparation and analyses.

TIC - Tentatively Identified Compound: Compounds detected in samples that arenot target compounds, internal standards, system monitoring compounds,or surrogates.

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Summary of Remarks For Samples Printed06/15/12 at 15:50:25

TSR Signing Reports: 364R5 - Desired TAT

Quarterly sampling, always log with QC4 per standing order from client.

Sample: L579547-01 Account: SEABREFIN Received: 06/09/12 09:00 Due Date: 06/15/12 00:00 RPT Date: 06/15/12 15:49 QC4Sample: L579547-02 Account: SEABREFIN Received: 06/09/12 09:00 Due Date: 06/15/12 00:00 RPT Date: 06/15/12 15:49

Sample: L579547-03 Account: SEABREFIN Received: 06/09/12 09:00 Due Date: 06/15/12 00:00 RPT Date: 06/15/12 15:49

Sample: L579547-04 Account: SEABREFIN Received: 06/09/12 09:00 Due Date: 06/15/12 00:00 RPT Date: 06/15/12 15:49

Sample: L579547-05 Account: SEABREFIN Received: 06/09/12 09:00 Due Date: 06/15/12 00:00 RPT Date: 06/15/12 15:49 MS/MSDSample: L579547-06 Account: SEABREFIN Received: 06/09/12 09:00 Due Date: 06/15/12 00:00 RPT Date: 06/15/12 15:49

Sample: L579547-07 Account: SEABREFIN Received: 06/09/12 09:00 Due Date: 06/15/12 00:00 RPT Date: 06/15/12 15:49

Sample: L579547-08 Account: SEABREFIN Received: 06/09/12 09:00 Due Date: 06/15/12 00:00 RPT Date: 06/15/12 15:49

Sample: L579547-09 Account: SEABREFIN Received: 06/09/12 09:00 Due Date: 06/15/12 00:00 RPT Date: 06/15/12 15:49

Sample: L579547-10 Account: SEABREFIN Received: 06/09/12 09:00 Due Date: 06/15/12 00:00 RPT Date: 06/15/12 15:49

Sample: L579547-11 Account: SEABREFIN Received: 06/09/12 09:00 Due Date: 06/15/12 00:00 RPT Date: 06/15/12 15:49

Sample: L579547-12 Account: SEABREFIN Received: 06/09/12 09:00 Due Date: 06/15/12 00:00 RPT Date: 06/15/12 15:49

Sample: L579547-13 Account: SEABREFIN Received: 06/09/12 09:00 Due Date: 06/15/12 00:00 RPT Date: 06/15/12 15:49

Sample: L579547-14 Account: SEABREFIN Received: 06/09/12 09:00 Due Date: 06/15/12 00:00 RPT Date: 06/15/12 15:49

Sample: L579547-15 Account: SEABREFIN Received: 06/09/12 09:00 Due Date: 06/15/12 00:00 RPT Date: 06/15/12 15:49

Sample: L579547-16 Account: SEABREFIN Received: 06/09/12 09:00 Due Date: 06/15/12 00:00 RPT Date: 06/15/12 15:49

Sample: L579547-17 Account: SEABREFIN Received: 06/09/12 09:00 Due Date: 06/15/12 00:00 RPT Date: 06/15/12 15:49

Reference 45 Page 151

Page 152: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 June 15, 2012

L579547

Laboratory BlankAnalyte Result Units % Rec Limit Batch Date Analyzed

1,1,1,2-Tetrachloroethane < .001 mg/l WG597107 06/10/12 00:35 1,1,1-Trichloroethane < .001 mg/l WG597107 06/10/12 00:35 1,1,2,2-Tetrachloroethane < .001 mg/l WG597107 06/10/12 00:35 1,1,2-Trichloroethane < .001 mg/l WG597107 06/10/12 00:35 1,1,2-Trichlorotrifluoroethane < .001 mg/l WG597107 06/10/12 00:35 1,1-Dichloroethane < .001 mg/l WG597107 06/10/12 00:35 1,1-Dichloroethene < .001 mg/l WG597107 06/10/12 00:35 1,1-Dichloropropene < .001 mg/l WG597107 06/10/12 00:35 1,2,3-Trichlorobenzene < .001 mg/l WG597107 06/10/12 00:35 1,2,3-Trichloropropane < .001 mg/l WG597107 06/10/12 00:35 1,2,3-Trimethylbenzene < .001 mg/l WG597107 06/10/12 00:35 1,2,4-Trichlorobenzene < .001 mg/l WG597107 06/10/12 00:35 1,2,4-Trimethylbenzene < .001 mg/l WG597107 06/10/12 00:35 1,2-Dibromo-3-Chloropropane < .005 mg/l WG597107 06/10/12 00:35 1,2-Dibromoethane < .001 mg/l WG597107 06/10/12 00:35 1,2-Dichlorobenzene < .001 mg/l WG597107 06/10/12 00:35 1,2-Dichloroethane < .001 mg/l WG597107 06/10/12 00:35 1,2-Dichloropropane < .001 mg/l WG597107 06/10/12 00:35 1,3,5-Trimethylbenzene < .001 mg/l WG597107 06/10/12 00:35 1,3-Dichlorobenzene < .001 mg/l WG597107 06/10/12 00:35 1,3-Dichloropropane < .001 mg/l WG597107 06/10/12 00:35 1,4-Dichlorobenzene < .001 mg/l WG597107 06/10/12 00:35 2,2-Dichloropropane < .001 mg/l WG597107 06/10/12 00:35 2-Butanone (MEK) < .01 mg/l WG597107 06/10/12 00:35 2-Chloroethyl vinyl ether < .05 mg/l WG597107 06/10/12 00:35 2-Chlorotoluene < .001 mg/l WG597107 06/10/12 00:35 4-Chlorotoluene < .001 mg/l WG597107 06/10/12 00:35 4-Methyl-2-pentanone (MIBK) < .01 mg/l WG597107 06/10/12 00:35 Acetone < .05 mg/l WG597107 06/10/12 00:35 Acrolein < .025 mg/l WG597107 06/10/12 00:35 Acrylonitrile < .01 mg/l WG597107 06/10/12 00:35 Benzene < .001 mg/l WG597107 06/10/12 00:35 Bromobenzene < .001 mg/l WG597107 06/10/12 00:35 Bromodichloromethane < .001 mg/l WG597107 06/10/12 00:35 Bromoform < .001 mg/l WG597107 06/10/12 00:35 Bromomethane < .005 mg/l WG597107 06/10/12 00:35 Carbon tetrachloride < .001 mg/l WG597107 06/10/12 00:35 Chlorobenzene < .001 mg/l WG597107 06/10/12 00:35 Chlorodibromomethane < .001 mg/l WG597107 06/10/12 00:35 Chloroethane < .005 mg/l WG597107 06/10/12 00:35 Chloroform < .005 mg/l WG597107 06/10/12 00:35 Chloromethane < .0025 mg/l WG597107 06/10/12 00:35 cis-1,2-Dichloroethene < .001 mg/l WG597107 06/10/12 00:35 cis-1,3-Dichloropropene < .001 mg/l WG597107 06/10/12 00:35 Di-isopropyl ether < .001 mg/l WG597107 06/10/12 00:35 Dibromomethane < .001 mg/l WG597107 06/10/12 00:35 Dichlorodifluoromethane < .005 mg/l WG597107 06/10/12 00:35 Ethylbenzene < .001 mg/l WG597107 06/10/12 00:35 Hexachloro-1,3-butadiene < .001 mg/l WG597107 06/10/12 00:35 Isopropylbenzene < .001 mg/l WG597107 06/10/12 00:35 Methyl tert-butyl ether < .001 mg/l WG597107 06/10/12 00:35 Methylene Chloride < .005 mg/l WG597107 06/10/12 00:35 n-Butylbenzene < .001 mg/l WG597107 06/10/12 00:35 n-Propylbenzene < .001 mg/l WG597107 06/10/12 00:35 Naphthalene < .005 mg/l WG597107 06/10/12 00:35 p-Isopropyltoluene < .001 mg/l WG597107 06/10/12 00:35 sec-Butylbenzene < .001 mg/l WG597107 06/10/12 00:35 Styrene < .001 mg/l WG597107 06/10/12 00:35 tert-Butylbenzene < .001 mg/l WG597107 06/10/12 00:35

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 36 of 49

Reference 45 Page 152

Page 153: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 June 15, 2012

L579547

Laboratory BlankAnalyte Result Units % Rec Limit Batch Date Analyzed

Tetrachloroethene < .001 mg/l WG597107 06/10/12 00:35 Toluene < .005 mg/l WG597107 06/10/12 00:35 trans-1,2-Dichloroethene < .001 mg/l WG597107 06/10/12 00:35 trans-1,3-Dichloropropene < .001 mg/l WG597107 06/10/12 00:35 Trichloroethene < .001 mg/l WG597107 06/10/12 00:35 Trichlorofluoromethane < .005 mg/l WG597107 06/10/12 00:35 Vinyl chloride < .001 mg/l WG597107 06/10/12 00:35 Xylenes, Total < .003 mg/l WG597107 06/10/12 00:35 4-Bromofluorobenzene % Rec. 107.6 82-120 WG597107 06/10/12 00:35 Dibromofluoromethane % Rec. 97.26 82-126 WG597107 06/10/12 00:35 Toluene-d8 % Rec. 99.80 92-112 WG597107 06/10/12 00:35

1,1,1,2-Tetrachloroethane < .001 mg/l WG597108 06/09/12 23:12 1,1,1-Trichloroethane < .001 mg/l WG597108 06/09/12 23:12 1,1,2,2-Tetrachloroethane < .001 mg/l WG597108 06/09/12 23:12 1,1,2-Trichloroethane < .001 mg/l WG597108 06/09/12 23:12 1,1,2-Trichlorotrifluoroethane < .001 mg/l WG597108 06/09/12 23:12 1,1-Dichloroethane < .001 mg/l WG597108 06/09/12 23:12 1,1-Dichloroethene < .001 mg/l WG597108 06/09/12 23:12 1,1-Dichloropropene < .001 mg/l WG597108 06/09/12 23:12 1,2,3-Trichlorobenzene < .001 mg/l WG597108 06/09/12 23:12 1,2,3-Trichloropropane < .001 mg/l WG597108 06/09/12 23:12 1,2,3-Trimethylbenzene < .001 mg/l WG597108 06/09/12 23:12 1,2,4-Trichlorobenzene < .001 mg/l WG597108 06/09/12 23:12 1,2,4-Trimethylbenzene < .001 mg/l WG597108 06/09/12 23:12 1,2-Dibromo-3-Chloropropane < .005 mg/l WG597108 06/09/12 23:12 1,2-Dibromoethane < .001 mg/l WG597108 06/09/12 23:12 1,2-Dichlorobenzene < .001 mg/l WG597108 06/09/12 23:12 1,2-Dichloroethane < .001 mg/l WG597108 06/09/12 23:12 1,2-Dichloropropane < .001 mg/l WG597108 06/09/12 23:12 1,3,5-Trimethylbenzene < .001 mg/l WG597108 06/09/12 23:12 1,3-Dichlorobenzene < .001 mg/l WG597108 06/09/12 23:12 1,3-Dichloropropane < .001 mg/l WG597108 06/09/12 23:12 1,4-Dichlorobenzene < .001 mg/l WG597108 06/09/12 23:12 2,2-Dichloropropane < .001 mg/l WG597108 06/09/12 23:12 2-Butanone (MEK) < .01 mg/l WG597108 06/09/12 23:12 2-Chloroethyl vinyl ether < .05 mg/l WG597108 06/09/12 23:12 2-Chlorotoluene < .001 mg/l WG597108 06/09/12 23:12 4-Chlorotoluene < .001 mg/l WG597108 06/09/12 23:12 4-Methyl-2-pentanone (MIBK) < .01 mg/l WG597108 06/09/12 23:12 Acetone < .05 mg/l WG597108 06/09/12 23:12 Acrolein < .025 mg/l WG597108 06/09/12 23:12 Acrylonitrile < .01 mg/l WG597108 06/09/12 23:12 Benzene < .001 mg/l WG597108 06/09/12 23:12 Bromobenzene < .001 mg/l WG597108 06/09/12 23:12 Bromodichloromethane < .001 mg/l WG597108 06/09/12 23:12 Bromoform < .001 mg/l WG597108 06/09/12 23:12 Bromomethane < .005 mg/l WG597108 06/09/12 23:12 Carbon tetrachloride < .001 mg/l WG597108 06/09/12 23:12 Chlorobenzene < .001 mg/l WG597108 06/09/12 23:12 Chlorodibromomethane < .001 mg/l WG597108 06/09/12 23:12 Chloroethane < .005 mg/l WG597108 06/09/12 23:12 Chloroform < .005 mg/l WG597108 06/09/12 23:12 Chloromethane < .0025 mg/l WG597108 06/09/12 23:12 cis-1,2-Dichloroethene < .001 mg/l WG597108 06/09/12 23:12 cis-1,3-Dichloropropene < .001 mg/l WG597108 06/09/12 23:12 Di-isopropyl ether < .001 mg/l WG597108 06/09/12 23:12 Dibromomethane < .001 mg/l WG597108 06/09/12 23:12

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 37 of 49

Reference 45 Page 153

Page 154: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 June 15, 2012

L579547

Laboratory BlankAnalyte Result Units % Rec Limit Batch Date Analyzed

Dichlorodifluoromethane < .005 mg/l WG597108 06/09/12 23:12 Ethylbenzene < .001 mg/l WG597108 06/09/12 23:12 Hexachloro-1,3-butadiene < .001 mg/l WG597108 06/09/12 23:12 Isopropylbenzene < .001 mg/l WG597108 06/09/12 23:12 Methyl tert-butyl ether < .001 mg/l WG597108 06/09/12 23:12 Methylene Chloride < .005 mg/l WG597108 06/09/12 23:12 n-Butylbenzene < .001 mg/l WG597108 06/09/12 23:12 n-Propylbenzene < .001 mg/l WG597108 06/09/12 23:12 Naphthalene < .005 mg/l WG597108 06/09/12 23:12 p-Isopropyltoluene < .001 mg/l WG597108 06/09/12 23:12 sec-Butylbenzene < .001 mg/l WG597108 06/09/12 23:12 Styrene < .001 mg/l WG597108 06/09/12 23:12 tert-Butylbenzene < .001 mg/l WG597108 06/09/12 23:12 Tetrachloroethene < .001 mg/l WG597108 06/09/12 23:12 Toluene < .005 mg/l WG597108 06/09/12 23:12 trans-1,2-Dichloroethene < .001 mg/l WG597108 06/09/12 23:12 trans-1,3-Dichloropropene < .001 mg/l WG597108 06/09/12 23:12 Trichloroethene < .001 mg/l WG597108 06/09/12 23:12 Trichlorofluoromethane < .005 mg/l WG597108 06/09/12 23:12 Vinyl chloride < .001 mg/l WG597108 06/09/12 23:12 Xylenes, Total < .003 mg/l WG597108 06/09/12 23:12 4-Bromofluorobenzene % Rec. 100.1 82-120 WG597108 06/09/12 23:12 Dibromofluoromethane % Rec. 105.2 82-126 WG597108 06/09/12 23:12 Toluene-d8 % Rec. 101.5 92-112 WG597108 06/09/12 23:12

Tetrachloroethene < .001 mg/l WG597428 06/13/12 01:14 4-Bromofluorobenzene % Rec. 107.1 82-120 WG597428 06/13/12 01:14 Dibromofluoromethane % Rec. 100.5 82-126 WG597428 06/13/12 01:14 Toluene-d8 % Rec. 98.27 92-112 WG597428 06/13/12 01:14

Laboratory Control SampleAnalyte Units Known Val Result % Rec Limit Batch

1,1,1,2-Tetrachloroethane mg/l .025 0.0279 112. 77-128 WG597107 1,1,1-Trichloroethane mg/l .025 0.0247 98.7 71-126 WG597107 1,1,2,2-Tetrachloroethane mg/l .025 0.0272 109. 78-130 WG597107 1,1,2-Trichloroethane mg/l .025 0.0277 111. 81-121 WG597107 1,1,2-Trichlorotrifluoroethane mg/l .025 0.0256 103. 53-143 WG597107 1,1-Dichloroethane mg/l .025 0.0225 89.9 73-123 WG597107 1,1-Dichloroethene mg/l .025 0.0253 101. 54-134 WG597107 1,1-Dichloropropene mg/l .025 0.0236 94.5 67-127 WG597107 1,2,3-Trichlorobenzene mg/l .025 0.0275 110. 77-130 WG597107 1,2,3-Trichloropropane mg/l .025 0.0289 115. 68-130 WG597107 1,2,3-Trimethylbenzene mg/l .025 0.0245 98.1 77-126 WG597107 1,2,4-Trichlorobenzene mg/l .025 0.0276 111. 76-127 WG597107 1,2,4-Trimethylbenzene mg/l .025 0.0282 113. 77-129 WG597107 1,2-Dibromo-3-Chloropropane mg/l .025 0.0280 112. 55-142 WG597107 1,2-Dibromoethane mg/l .025 0.0280 112. 78-124 WG597107 1,2-Dichlorobenzene mg/l .025 0.0254 102. 82-121 WG597107 1,2-Dichloroethane mg/l .025 0.0233 93.0 69-128 WG597107 1,2-Dichloropropane mg/l .025 0.0233 93.1 77-121 WG597107 1,3,5-Trimethylbenzene mg/l .025 0.0280 112. 78-127 WG597107 1,3-Dichlorobenzene mg/l .025 0.0288 115. 77-127 WG597107 1,3-Dichloropropane mg/l .025 0.0256 102. 78-117 WG597107 1,4-Dichlorobenzene mg/l .025 0.0252 101. 79-117 WG597107 2,2-Dichloropropane mg/l .025 0.0224 89.5 63-130 WG597107 2-Butanone (MEK) mg/l .125 0.142 113. 58-144 WG597107 2-Chloroethyl vinyl ether mg/l .125 0.123 98.6 26-172 WG597107

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 38 of 49

Reference 45 Page 154

Page 155: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 June 15, 2012

L579547

Laboratory Control SampleAnalyte Units Known Val Result % Rec Limit Batch

2-Chlorotoluene mg/l .025 0.0269 108. 78-123 WG597107 4-Chlorotoluene mg/l .025 0.0271 108. 78-122 WG597107 4-Methyl-2-pentanone (MIBK) mg/l .125 0.132 105. 58-147 WG597107 Acetone mg/l .125 0.139 112. 49-153 WG597107 Acrolein mg/l .125 0.123 98.5 10-181 WG597107 Acrylonitrile mg/l .125 0.117 93.6 53-153 WG597107 Benzene mg/l .025 0.0237 94.8 72-119 WG597107 Bromobenzene mg/l .025 0.0261 104. 76-121 WG597107 Bromodichloromethane mg/l .025 0.0252 101. 75-127 WG597107 Bromoform mg/l .025 0.0304 122. 61-136 WG597107 Bromomethane mg/l .025 0.0239 95.5 42-172 WG597107 Carbon tetrachloride mg/l .025 0.0248 99.3 63-129 WG597107 Chlorobenzene mg/l .025 0.0273 109. 78-123 WG597107 Chlorodibromomethane mg/l .025 0.0280 112. 73-128 WG597107 Chloroethane mg/l .025 0.0230 92.1 52-164 WG597107 Chloroform mg/l .025 0.0239 95.5 76-122 WG597107 Chloromethane mg/l .025 0.0184 73.7 50-141 WG597107 cis-1,2-Dichloroethene mg/l .025 0.0246 98.5 75-121 WG597107 cis-1,3-Dichloropropene mg/l .025 0.0252 101. 74-124 WG597107 Di-isopropyl ether mg/l .025 0.0214 85.7 66-129 WG597107 Dibromomethane mg/l .025 0.0262 105. 77-124 WG597107 Dichlorodifluoromethane mg/l .025 0.0200 80.1 33-173 WG597107 Ethylbenzene mg/l .025 0.0275 110. 77-124 WG597107 Hexachloro-1,3-butadiene mg/l .025 0.0278 111. 71-134 WG597107 Isopropylbenzene mg/l .025 0.0280 112. 74-126 WG597107 Methyl tert-butyl ether mg/l .025 0.0243 97.2 67-127 WG597107 Methylene Chloride mg/l .025 0.0236 94.5 67-122 WG597107 n-Butylbenzene mg/l .025 0.0251 101. 74-130 WG597107 n-Propylbenzene mg/l .025 0.0275 110. 77-125 WG597107 Naphthalene mg/l .025 0.0269 107. 70-134 WG597107 p-Isopropyltoluene mg/l .025 0.0291 116. 77-132 WG597107 sec-Butylbenzene mg/l .025 0.0282 113. 77-130 WG597107 Styrene mg/l .025 0.0281 113. 69-145 WG597107 tert-Butylbenzene mg/l .025 0.0281 112. 76-131 WG597107 Tetrachloroethene mg/l .025 0.0288 115. 69-131 WG597107 Toluene mg/l .025 0.0251 100. 75-114 WG597107 trans-1,2-Dichloroethene mg/l .025 0.0249 99.6 63-127 WG597107 trans-1,3-Dichloropropene mg/l .025 0.0278 111. 69-124 WG597107 Trichloroethene mg/l .025 0.0262 105. 69-131 WG597107 Trichlorofluoromethane mg/l .025 0.0244 97.6 53-161 WG597107 Vinyl chloride mg/l .025 0.0205 81.9 55-142 WG597107 Xylenes, Total mg/l .075 0.0829 111. 77-123 WG597107 4-Bromofluorobenzene 109.1 82-120 WG597107 Dibromofluoromethane 96.46 82-126 WG597107 Toluene-d8 101.4 92-112 WG597107

1,1,1,2-Tetrachloroethane mg/l .025 0.0242 96.9 77-128 WG597108 1,1,1-Trichloroethane mg/l .025 0.0252 101. 71-126 WG597108 1,1,2,2-Tetrachloroethane mg/l .025 0.0264 106. 78-130 WG597108 1,1,2-Trichloroethane mg/l .025 0.0255 102. 81-121 WG597108 1,1,2-Trichlorotrifluoroethane mg/l .025 0.0256 103. 53-143 WG597108 1,1-Dichloroethane mg/l .025 0.0251 100. 73-123 WG597108 1,1-Dichloroethene mg/l .025 0.0249 99.7 54-134 WG597108 1,1-Dichloropropene mg/l .025 0.0252 101. 67-127 WG597108 1,2,3-Trichlorobenzene mg/l .025 0.0267 107. 77-130 WG597108 1,2,3-Trichloropropane mg/l .025 0.0257 103. 68-130 WG597108 1,2,3-Trimethylbenzene mg/l .025 0.0242 96.8 77-126 WG597108 1,2,4-Trichlorobenzene mg/l .025 0.0265 106. 76-127 WG597108

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 39 of 49

Reference 45 Page 155

Page 156: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 June 15, 2012

L579547

Laboratory Control SampleAnalyte Units Known Val Result % Rec Limit Batch

1,2,4-Trimethylbenzene mg/l .025 0.0254 102. 77-129 WG597108 1,2-Dibromo-3-Chloropropane mg/l .025 0.0281 112. 55-142 WG597108 1,2-Dibromoethane mg/l .025 0.0253 101. 78-124 WG597108 1,2-Dichlorobenzene mg/l .025 0.0252 101. 82-121 WG597108 1,2-Dichloroethane mg/l .025 0.0249 99.8 69-128 WG597108 1,2-Dichloropropane mg/l .025 0.0253 101. 77-121 WG597108 1,3,5-Trimethylbenzene mg/l .025 0.0252 101. 78-127 WG597108 1,3-Dichlorobenzene mg/l .025 0.0254 102. 77-127 WG597108 1,3-Dichloropropane mg/l .025 0.0246 98.5 78-117 WG597108 1,4-Dichlorobenzene mg/l .025 0.0247 98.9 79-117 WG597108 2,2-Dichloropropane mg/l .025 0.0242 96.7 63-130 WG597108 2-Butanone (MEK) mg/l .125 0.139 111. 58-144 WG597108 2-Chloroethyl vinyl ether mg/l .125 0.137 110. 26-172 WG597108 2-Chlorotoluene mg/l .025 0.0249 99.5 78-123 WG597108 4-Chlorotoluene mg/l .025 0.0244 97.5 78-122 WG597108 4-Methyl-2-pentanone (MIBK) mg/l .125 0.140 112. 58-147 WG597108 Acetone mg/l .125 0.133 107. 49-153 WG597108 Acrolein mg/l .125 0.129 103. 10-181 WG597108 Acrylonitrile mg/l .125 0.137 110. 53-153 WG597108 Benzene mg/l .025 0.0254 101. 72-119 WG597108 Bromobenzene mg/l .025 0.0243 97.1 76-121 WG597108 Bromodichloromethane mg/l .025 0.0261 104. 75-127 WG597108 Bromoform mg/l .025 0.0270 108. 61-136 WG597108 Bromomethane mg/l .025 0.0247 98.9 42-172 WG597108 Carbon tetrachloride mg/l .025 0.0247 98.9 63-129 WG597108 Chlorobenzene mg/l .025 0.0247 98.7 78-123 WG597108 Chlorodibromomethane mg/l .025 0.0255 102. 73-128 WG597108 Chloroethane mg/l .025 0.0251 100. 52-164 WG597108 Chloroform mg/l .025 0.0243 97.0 76-122 WG597108 Chloromethane mg/l .025 0.0226 90.3 50-141 WG597108 cis-1,2-Dichloroethene mg/l .025 0.0249 99.6 75-121 WG597108 cis-1,3-Dichloropropene mg/l .025 0.0264 106. 74-124 WG597108 Di-isopropyl ether mg/l .025 0.0259 104. 66-129 WG597108 Dibromomethane mg/l .025 0.0263 105. 77-124 WG597108 Dichlorodifluoromethane mg/l .025 0.0202 81.0 33-173 WG597108 Ethylbenzene mg/l .025 0.0252 101. 77-124 WG597108 Hexachloro-1,3-butadiene mg/l .025 0.0262 105. 71-134 WG597108 Isopropylbenzene mg/l .025 0.0252 101. 74-126 WG597108 Methyl tert-butyl ether mg/l .025 0.0256 103. 67-127 WG597108 Methylene Chloride mg/l .025 0.0241 96.6 67-122 WG597108 n-Butylbenzene mg/l .025 0.0257 103. 74-130 WG597108 n-Propylbenzene mg/l .025 0.0252 101. 77-125 WG597108 Naphthalene mg/l .025 0.0263 105. 70-134 WG597108 p-Isopropyltoluene mg/l .025 0.0259 103. 77-132 WG597108 sec-Butylbenzene mg/l .025 0.0254 102. 77-130 WG597108 Styrene mg/l .025 0.0251 101. 69-145 WG597108 tert-Butylbenzene mg/l .025 0.0254 102. 76-131 WG597108 Tetrachloroethene mg/l .025 0.0249 99.8 69-131 WG597108 Toluene mg/l .025 0.0254 102. 75-114 WG597108 trans-1,2-Dichloroethene mg/l .025 0.0253 101. 63-127 WG597108 trans-1,3-Dichloropropene mg/l .025 0.0264 106. 69-124 WG597108 Trichloroethene mg/l .025 0.0254 102. 69-131 WG597108 Trichlorofluoromethane mg/l .025 0.0244 97.6 53-161 WG597108 Vinyl chloride mg/l .025 0.0239 95.5 55-142 WG597108 Xylenes, Total mg/l .075 0.0746 99.5 77-123 WG597108 4-Bromofluorobenzene 98.93 82-120 WG597108 Dibromofluoromethane 102.4 82-126 WG597108 Toluene-d8 103.2 92-112 WG597108

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 40 of 49

Reference 45 Page 156

Page 157: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 June 15, 2012

L579547

Laboratory Control SampleAnalyte Units Known Val Result % Rec Limit Batch

Tetrachloroethene mg/l .025 0.0252 101. 69-131 WG597428 4-Bromofluorobenzene 102.4 82-120 WG597428 Dibromofluoromethane 97.85 82-126 WG597428 Toluene-d8 99.54 92-112 WG597428

Laboratory Control Sample DuplicateAnalyte Units Result Ref %Rec Limit RPD Limit Batch

1,1,1,2-Tetrachloroethane mg/l 0.0281 0.0279 112. 77-128 0.950 20 WG597107 1,1,1-Trichloroethane mg/l 0.0257 0.0247 103. 71-126 4.19 20 WG597107 1,1,2,2-Tetrachloroethane mg/l 0.0276 0.0272 110. 78-130 1.36 20 WG597107 1,1,2-Trichloroethane mg/l 0.0276 0.0277 110. 81-121 0.650 20 WG597107 1,1,2-Trichlorotrifluoroethane mg/l 0.0268 0.0256 107. 53-143 4.65 20 WG597107 1,1-Dichloroethane mg/l 0.0229 0.0225 92.0 73-123 1.91 20 WG597107 1,1-Dichloroethene mg/l 0.0259 0.0253 104. 54-134 2.65 20 WG597107 1,1-Dichloropropene mg/l 0.0241 0.0236 96.0 67-127 2.07 20 WG597107 1,2,3-Trichlorobenzene mg/l 0.0276 0.0275 110. 77-130 0.480 20 WG597107 1,2,3-Trichloropropane mg/l 0.0284 0.0289 114. 68-130 1.68 20 WG597107 1,2,3-Trimethylbenzene mg/l 0.0244 0.0245 97.0 77-126 0.600 20 WG597107 1,2,4-Trichlorobenzene mg/l 0.0282 0.0276 113. 76-127 1.99 20 WG597107 1,2,4-Trimethylbenzene mg/l 0.0283 0.0282 113. 77-129 0.390 20 WG597107 1,2-Dibromo-3-Chloropropane mg/l 0.0276 0.0280 110. 55-142 1.43 20 WG597107 1,2-Dibromoethane mg/l 0.0280 0.0280 112. 78-124 0.0700 20 WG597107 1,2-Dichlorobenzene mg/l 0.0256 0.0254 102. 82-121 0.910 20 WG597107 1,2-Dichloroethane mg/l 0.0233 0.0233 93.0 69-128 0.0100 20 WG597107 1,2-Dichloropropane mg/l 0.0237 0.0233 95.0 77-121 1.66 20 WG597107 1,3,5-Trimethylbenzene mg/l 0.0284 0.0280 114. 78-127 1.53 20 WG597107 1,3-Dichlorobenzene mg/l 0.0291 0.0288 116. 77-127 1.15 20 WG597107 1,3-Dichloropropane mg/l 0.0253 0.0256 101. 78-117 1.00 20 WG597107 1,4-Dichlorobenzene mg/l 0.0257 0.0252 103. 79-117 1.69 20 WG597107 2,2-Dichloropropane mg/l 0.0234 0.0224 94.0 63-130 4.58 20 WG597107 2-Butanone (MEK) mg/l 0.137 0.142 110. 58-144 3.10 20 WG597107 2-Chloroethyl vinyl ether mg/l 0.124 0.123 99.0 26-172 0.500 22 WG597107 2-Chlorotoluene mg/l 0.0272 0.0269 109. 78-123 1.22 20 WG597107 4-Chlorotoluene mg/l 0.0275 0.0271 110. 78-122 1.47 20 WG597107 4-Methyl-2-pentanone (MIBK) mg/l 0.129 0.132 103. 58-147 1.84 20 WG597107 Acetone mg/l 0.135 0.139 108. 49-153 3.41 21 WG597107 Acrolein mg/l 0.124 0.123 99.0 10-181 0.990 30 WG597107 Acrylonitrile mg/l 0.118 0.117 94.0 53-153 0.640 20 WG597107 Benzene mg/l 0.0244 0.0237 98.0 72-119 2.90 20 WG597107 Bromobenzene mg/l 0.0262 0.0261 105. 76-121 0.360 20 WG597107 Bromodichloromethane mg/l 0.0258 0.0252 103. 75-127 2.22 20 WG597107 Bromoform mg/l 0.0302 0.0304 121. 61-136 0.600 20 WG597107 Bromomethane mg/l 0.0243 0.0239 97.0 42-172 1.63 20 WG597107 Carbon tetrachloride mg/l 0.0259 0.0248 103. 63-129 4.10 20 WG597107 Chlorobenzene mg/l 0.0272 0.0273 109. 78-123 0.290 20 WG597107 Chlorodibromomethane mg/l 0.0282 0.0280 113. 73-128 1.03 20 WG597107 Chloroethane mg/l 0.0240 0.0230 96.0 52-164 4.10 20 WG597107 Chloroform mg/l 0.0242 0.0239 97.0 76-122 1.54 20 WG597107 Chloromethane mg/l 0.0189 0.0184 76.0 50-141 2.65 20 WG597107 cis-1,2-Dichloroethene mg/l 0.0250 0.0246 100. 75-121 1.69 20 WG597107 cis-1,3-Dichloropropene mg/l 0.0255 0.0252 102. 74-124 0.990 20 WG597107 Di-isopropyl ether mg/l 0.0218 0.0214 87.0 66-129 1.53 20 WG597107 Dibromomethane mg/l 0.0267 0.0262 107. 77-124 2.02 20 WG597107 Dichlorodifluoromethane mg/l 0.0211 0.0200 84.0 33-173 5.07 20 WG597107 Ethylbenzene mg/l 0.0278 0.0275 111. 77-124 1.34 20 WG597107 Hexachloro-1,3-butadiene mg/l 0.0286 0.0278 114. 71-134 3.08 20 WG597107 Isopropylbenzene mg/l 0.0284 0.0280 114. 74-126 1.61 20 WG597107

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 41 of 49

Reference 45 Page 157

Page 158: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 June 15, 2012

L579547

Laboratory Control Sample DuplicateAnalyte Units Result Ref %Rec Limit RPD Limit Batch

Methyl tert-butyl ether mg/l 0.0246 0.0243 98.0 67-127 1.17 20 WG597107 Methylene Chloride mg/l 0.0243 0.0236 97.0 67-122 2.94 20 WG597107 n-Butylbenzene mg/l 0.0256 0.0251 102. 74-130 1.67 20 WG597107 n-Propylbenzene mg/l 0.0278 0.0275 111. 77-125 1.25 20 WG597107 Naphthalene mg/l 0.0267 0.0269 107. 70-134 0.730 20 WG597107 p-Isopropyltoluene mg/l 0.0295 0.0291 118. 77-132 1.51 20 WG597107 sec-Butylbenzene mg/l 0.0286 0.0282 114. 77-130 1.29 20 WG597107 Styrene mg/l 0.0285 0.0281 114. 69-145 1.12 20 WG597107 tert-Butylbenzene mg/l 0.0286 0.0281 114. 76-131 1.77 20 WG597107 Tetrachloroethene mg/l 0.0292 0.0288 117. 69-131 1.14 20 WG597107 Toluene mg/l 0.0257 0.0251 103. 75-114 2.45 20 WG597107 trans-1,2-Dichloroethene mg/l 0.0253 0.0249 101. 63-127 1.57 20 WG597107 trans-1,3-Dichloropropene mg/l 0.0273 0.0278 109. 69-124 1.51 20 WG597107 Trichloroethene mg/l 0.0268 0.0262 107. 69-131 2.04 20 WG597107 Trichlorofluoromethane mg/l 0.0257 0.0244 103. 53-161 5.24 20 WG597107 Vinyl chloride mg/l 0.0209 0.0205 84.0 55-142 2.21 20 WG597107 Xylenes, Total mg/l 0.0837 0.0829 112. 77-123 0.920 20 WG597107 4-Bromofluorobenzene 108.4 82-120 WG597107 Dibromofluoromethane 97.46 82-126 WG597107 Toluene-d8 101.0 92-112 WG597107

1,1,1,2-Tetrachloroethane mg/l 0.0248 0.0242 99.0 77-128 2.20 20 WG597108 1,1,1-Trichloroethane mg/l 0.0257 0.0252 103. 71-126 2.13 20 WG597108 1,1,2,2-Tetrachloroethane mg/l 0.0261 0.0264 104. 78-130 1.11 20 WG597108 1,1,2-Trichloroethane mg/l 0.0257 0.0255 103. 81-121 0.810 20 WG597108 1,1,2-Trichlorotrifluoroethane mg/l 0.0264 0.0256 105. 53-143 2.79 20 WG597108 1,1-Dichloroethane mg/l 0.0252 0.0251 101. 73-123 0.240 20 WG597108 1,1-Dichloroethene mg/l 0.0252 0.0249 101. 54-134 1.09 20 WG597108 1,1-Dichloropropene mg/l 0.0255 0.0252 102. 67-127 1.27 20 WG597108 1,2,3-Trichlorobenzene mg/l 0.0270 0.0267 108. 77-130 1.33 20 WG597108 1,2,3-Trichloropropane mg/l 0.0247 0.0257 99.0 68-130 3.68 20 WG597108 1,2,3-Trimethylbenzene mg/l 0.0247 0.0242 99.0 77-126 2.22 20 WG597108 1,2,4-Trichlorobenzene mg/l 0.0268 0.0265 107. 76-127 1.33 20 WG597108 1,2,4-Trimethylbenzene mg/l 0.0257 0.0254 103. 77-129 1.29 20 WG597108 1,2-Dibromo-3-Chloropropane mg/l 0.0254 0.0281 101. 55-142 10.2 20 WG597108 1,2-Dibromoethane mg/l 0.0254 0.0253 101. 78-124 0.410 20 WG597108 1,2-Dichlorobenzene mg/l 0.0256 0.0252 102. 82-121 1.93 20 WG597108 1,2-Dichloroethane mg/l 0.0249 0.0249 100. 69-128 0.0100 20 WG597108 1,2-Dichloropropane mg/l 0.0259 0.0253 104. 77-121 2.38 20 WG597108 1,3,5-Trimethylbenzene mg/l 0.0258 0.0252 103. 78-127 2.47 20 WG597108 1,3-Dichlorobenzene mg/l 0.0258 0.0254 103. 77-127 1.64 20 WG597108 1,3-Dichloropropane mg/l 0.0246 0.0246 98.0 78-117 0.0400 20 WG597108 1,4-Dichlorobenzene mg/l 0.0249 0.0247 100. 79-117 0.850 20 WG597108 2,2-Dichloropropane mg/l 0.0249 0.0242 99.0 63-130 2.81 20 WG597108 2-Butanone (MEK) mg/l 0.135 0.139 108. 58-144 2.98 20 WG597108 2-Chloroethyl vinyl ether mg/l 0.136 0.137 109. 26-172 0.780 22 WG597108 2-Chlorotoluene mg/l 0.0258 0.0249 103. 78-123 3.46 20 WG597108 4-Chlorotoluene mg/l 0.0248 0.0244 99.0 78-122 1.66 20 WG597108 4-Methyl-2-pentanone (MIBK) mg/l 0.134 0.140 107. 58-147 4.00 20 WG597108 Acetone mg/l 0.130 0.133 104. 49-153 2.74 21 WG597108 Acrolein mg/l 0.125 0.129 100. 10-181 3.08 30 WG597108 Acrylonitrile mg/l 0.132 0.137 106. 53-153 3.33 20 WG597108 Benzene mg/l 0.0255 0.0254 102. 72-119 0.410 20 WG597108 Bromobenzene mg/l 0.0246 0.0243 98.0 76-121 1.34 20 WG597108 Bromodichloromethane mg/l 0.0262 0.0261 105. 75-127 0.400 20 WG597108 Bromoform mg/l 0.0269 0.0270 108. 61-136 0.240 20 WG597108 Bromomethane mg/l 0.0268 0.0247 107. 42-172 7.87 20 WG597108 Carbon tetrachloride mg/l 0.0254 0.0247 102. 63-129 2.56 20 WG597108

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 42 of 49

Reference 45 Page 158

Page 159: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 June 15, 2012

L579547

Laboratory Control Sample DuplicateAnalyte Units Result Ref %Rec Limit RPD Limit Batch

Chlorobenzene mg/l 0.0253 0.0247 101. 78-123 2.67 20 WG597108 Chlorodibromomethane mg/l 0.0255 0.0255 102. 73-128 0.130 20 WG597108 Chloroethane mg/l 0.0257 0.0251 103. 52-164 2.11 20 WG597108 Chloroform mg/l 0.0248 0.0243 99.0 76-122 2.24 20 WG597108 Chloromethane mg/l 0.0237 0.0226 95.0 50-141 4.90 20 WG597108 cis-1,2-Dichloroethene mg/l 0.0254 0.0249 101. 75-121 1.82 20 WG597108 cis-1,3-Dichloropropene mg/l 0.0269 0.0264 108. 74-124 1.73 20 WG597108 Di-isopropyl ether mg/l 0.0261 0.0259 104. 66-129 0.650 20 WG597108 Dibromomethane mg/l 0.0266 0.0263 106. 77-124 0.930 20 WG597108 Dichlorodifluoromethane mg/l 0.0204 0.0202 82.0 33-173 1.00 20 WG597108 Ethylbenzene mg/l 0.0261 0.0252 104. 77-124 3.47 20 WG597108 Hexachloro-1,3-butadiene mg/l 0.0274 0.0262 110. 71-134 4.65 20 WG597108 Isopropylbenzene mg/l 0.0258 0.0252 103. 74-126 2.22 20 WG597108 Methyl tert-butyl ether mg/l 0.0252 0.0256 101. 67-127 1.84 20 WG597108 Methylene Chloride mg/l 0.0242 0.0241 97.0 67-122 0.0200 20 WG597108 n-Butylbenzene mg/l 0.0263 0.0257 105. 74-130 2.17 20 WG597108 n-Propylbenzene mg/l 0.0257 0.0252 103. 77-125 2.04 20 WG597108 Naphthalene mg/l 0.0260 0.0263 104. 70-134 1.28 20 WG597108 p-Isopropyltoluene mg/l 0.0264 0.0259 105. 77-132 1.84 20 WG597108 sec-Butylbenzene mg/l 0.0260 0.0254 104. 77-130 2.32 20 WG597108 Styrene mg/l 0.0257 0.0251 103. 69-145 2.13 20 WG597108 tert-Butylbenzene mg/l 0.0260 0.0254 104. 76-131 2.14 20 WG597108 Tetrachloroethene mg/l 0.0255 0.0249 102. 69-131 2.32 20 WG597108 Toluene mg/l 0.0258 0.0254 103. 75-114 1.58 20 WG597108 trans-1,2-Dichloroethene mg/l 0.0259 0.0253 104. 63-127 2.36 20 WG597108 trans-1,3-Dichloropropene mg/l 0.0263 0.0264 105. 69-124 0.230 20 WG597108 Trichloroethene mg/l 0.0260 0.0254 104. 69-131 2.40 20 WG597108 Trichlorofluoromethane mg/l 0.0251 0.0244 100. 53-161 2.88 20 WG597108 Vinyl chloride mg/l 0.0246 0.0239 98.0 55-142 2.94 20 WG597108 Xylenes, Total mg/l 0.0762 0.0746 102. 77-123 2.13 20 WG597108 4-Bromofluorobenzene 99.57 82-120 WG597108 Dibromofluoromethane 101.3 82-126 WG597108 Toluene-d8 104.7 92-112 WG597108

Tetrachloroethene mg/l 0.0266 0.0252 106. 69-131 5.36 20 WG597428 4-Bromofluorobenzene 103.4 82-120 WG597428 Dibromofluoromethane 99.50 82-126 WG597428 Toluene-d8 99.50 92-112 WG597428

Matrix SpikeAnalyte Units MS Res Ref Res TV % Rec Limit Ref Samp Batch

1,1,1,2-Tetrachloroethane mg/l 0.0274 0 .025 110. 71-130 L579547-05 WG597107 1,1,1-Trichloroethane mg/l 0.0278 0 .025 111. 58-137 L579547-05 WG597107 1,1,2,2-Tetrachloroethane mg/l 0.0270 0 .025 108. 64-149 L579547-05 WG597107 1,1,2-Trichloroethane mg/l 0.0268 0 .025 107. 73-128 L579547-05 WG597107 1,1,2-Trichlorotrifluoroethane mg/l 0.0298 0 .025 119. 36-159 L579547-05 WG597107 1,1-Dichloroethane mg/l 0.0229 0 .025 91.6 58-133 L579547-05 WG597107 1,1-Dichloroethene mg/l 0.0276 0 .025 110. 32-152 L579547-05 WG597107 1,1-Dichloropropene mg/l 0.0255 0 .025 102. 50-140 L579547-05 WG597107 1,2,3-Trichlorobenzene mg/l 0.0282 0 .025 113. 68-135 L579547-05 WG597107 1,2,3-Trichloropropane mg/l 0.0279 0 .025 112. 74-137 L579547-05 WG597107 1,2,3-Trimethylbenzene mg/l 0.0249 0 .025 99.7 67-133 L579547-05 WG597107 1,2,4-Trichlorobenzene mg/l 0.0297 0 .025 119. 67-133 L579547-05 WG597107 1,2,4-Trimethylbenzene mg/l 0.0289 0 .025 116. 62-141 L579547-05 WG597107 1,2-Dibromo-3-Chloropropane mg/l 0.0272 0 .025 109. 55-148 L579547-05 WG597107 1,2-Dibromoethane mg/l 0.0271 0 .025 108. 71-129 L579547-05 WG597107 1,2-Dichlorobenzene mg/l 0.0256 0 .025 102. 75-125 L579547-05 WG597107

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 43 of 49

Reference 45 Page 159

Page 160: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 June 15, 2012

L579547

Matrix SpikeAnalyte Units MS Res Ref Res TV % Rec Limit Ref Samp Batch

1,2-Dichloroethane mg/l 0.0226 0 .025 90.4 59-135 L579547-05 WG597107 1,2-Dichloropropane mg/l 0.0227 0 .025 90.6 68-126 L579547-05 WG597107 1,3,5-Trimethylbenzene mg/l 0.0291 0 .025 116. 67-136 L579547-05 WG597107 1,3-Dichlorobenzene mg/l 0.0292 0 .025 117. 69-131 L579547-05 WG597107 1,3-Dichloropropane mg/l 0.0243 0 .025 97.4 70-122 L579547-05 WG597107 1,4-Dichlorobenzene mg/l 0.0258 0 .025 103. 70-123 L579547-05 WG597107 2,2-Dichloropropane mg/l 0.0261 0 .025 104. 51-141 L579547-05 WG597107 2-Butanone (MEK) mg/l 0.109 0 .125 87.4 51-149 L579547-05 WG597107 2-Chloroethyl vinyl ether mg/l 0.0545 0 .125 43.6 10-161 L579547-05 WG597107 2-Chlorotoluene mg/l 0.0275 0 .025 110. 65-133 L579547-05 WG597107 4-Chlorotoluene mg/l 0.0275 0 .025 110. 67-129 L579547-05 WG597107 4-Methyl-2-pentanone (MIBK) mg/l 0.122 0 .125 97.8 53-154 L579547-05 WG597107 Acetone mg/l 0.0815 0 .125 65.2 34-146 L579547-05 WG597107 Acrolein mg/l 0.150 0 .125 120. 10-189 L579547-05 WG597107 Acrylonitrile mg/l 0.115 0 .125 92.0 49-162 L579547-05 WG597107 Benzene mg/l 0.0242 0 .025 96.9 51-134 L579547-05 WG597107 Bromobenzene mg/l 0.0257 0 .025 103. 64-130 L579547-05 WG597107 Bromodichloromethane mg/l 0.0243 0 .025 97.1 67-132 L579547-05 WG597107 Bromoform mg/l 0.0293 0 .025 117. 59-137 L579547-05 WG597107 Bromomethane mg/l 0.0244 0 .025 97.7 23-177 L579547-05 WG597107 Carbon tetrachloride mg/l 0.0285 0 .025 114. 49-140 L579547-05 WG597107 Chlorobenzene mg/l 0.0268 0 .025 107. 69-126 L579547-05 WG597107 Chlorodibromomethane mg/l 0.0272 0 .025 109. 68-130 L579547-05 WG597107 Chloroethane mg/l 0.0248 0 .025 99.0 32-177 L579547-05 WG597107 Chloroform mg/l 0.0245 0 .025 97.9 64-130 L579547-05 WG597107 Chloromethane mg/l 0.0194 0 .025 77.6 27-155 L579547-05 WG597107 cis-1,2-Dichloroethene mg/l 0.0254 0 .025 101. 54-137 L579547-05 WG597107 cis-1,3-Dichloropropene mg/l 0.0245 0 .025 98.0 63-127 L579547-05 WG597107 Di-isopropyl ether mg/l 0.0213 0 .025 85.0 58-133 L579547-05 WG597107 Dibromomethane mg/l 0.0251 0 .025 100. 68-131 L579547-05 WG597107 Dichlorodifluoromethane mg/l 0.0230 0 .025 91.8 16-188 L579547-05 WG597107 Ethylbenzene mg/l 0.0280 0 .025 112. 64-135 L579547-05 WG597107 Hexachloro-1,3-butadiene mg/l 0.0306 0 .025 122. 64-140 L579547-05 WG597107 Isopropylbenzene mg/l 0.0292 0 .025 117. 62-134 L579547-05 WG597107 Methyl tert-butyl ether mg/l 0.0244 0 .025 97.4 55-136 L579547-05 WG597107 Methylene Chloride mg/l 0.0247 0 .025 98.6 52-130 L579547-05 WG597107 n-Butylbenzene mg/l 0.0277 0 .025 111. 62-142 L579547-05 WG597107 n-Propylbenzene mg/l 0.0289 0 .025 115. 62-137 L579547-05 WG597107 Naphthalene mg/l 0.0274 0 .025 110. 65-140 L579547-05 WG597107 p-Isopropyltoluene mg/l 0.0309 0 .025 124. 64-142 L579547-05 WG597107 sec-Butylbenzene mg/l 0.0301 0 .025 120. 67-139 L579547-05 WG597107 Styrene mg/l 0.0277 0 .025 111. 58-152 L579547-05 WG597107 tert-Butylbenzene mg/l 0.0299 0 .025 119. 66-139 L579547-05 WG597107 Tetrachloroethene mg/l 0.0630 0.0320 .025 124. 56-139 L579547-05 WG597107 Toluene mg/l 0.0253 0 .025 101. 61-126 L579547-05 WG597107 trans-1,2-Dichloroethene mg/l 0.0265 0 .025 106. 45-137 L579547-05 WG597107 trans-1,3-Dichloropropene mg/l 0.0266 0 .025 106. 59-130 L579547-05 WG597107 Trichloroethene mg/l 0.0379 0.0120 .025 104. 40-155 L579547-05 WG597107 Trichlorofluoromethane mg/l 0.0277 0 .025 111. 35-177 L579547-05 WG597107 Vinyl chloride mg/l 0.0227 0 .025 90.9 32-159 L579547-05 WG597107 Xylenes, Total mg/l 0.0843 0 .075 112. 64-133 L579547-05 WG597107 4-Bromofluorobenzene 108.3 82-120 WG597107 Dibromofluoromethane 99.21 82-126 WG597107 Toluene-d8 100.2 92-112 WG597107

1,1,1,2-Tetrachloroethane mg/l 0.0246 0 .025 98.3 71-130 L579573-03 WG597108 1,1,1-Trichloroethane mg/l 0.0266 0 .025 106. 58-137 L579573-03 WG597108 1,1,2,2-Tetrachloroethane mg/l 0.0256 0 .025 102. 64-149 L579573-03 WG597108

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 44 of 49

Reference 45 Page 160

Page 161: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 June 15, 2012

L579547

Matrix SpikeAnalyte Units MS Res Ref Res TV % Rec Limit Ref Samp Batch

1,1,2-Trichloroethane mg/l 0.0246 0 .025 98.3 73-128 L579573-03 WG597108 1,1,2-Trichlorotrifluoroethane mg/l 0.0283 0 .025 113. 36-159 L579573-03 WG597108 1,1-Dichloroethane mg/l 0.0259 0 .025 104. 58-133 L579573-03 WG597108 1,1-Dichloroethene mg/l 0.0272 0 .025 109. 32-152 L579573-03 WG597108 1,1-Dichloropropene mg/l 0.0265 0 .025 106. 50-140 L579573-03 WG597108 1,2,3-Trichlorobenzene mg/l 0.0278 0 .025 111. 68-135 L579573-03 WG597108 1,2,3-Trichloropropane mg/l 0.0237 0 .025 94.8 74-137 L579573-03 WG597108 1,2,3-Trimethylbenzene mg/l 0.0253 0 .025 101. 67-133 L579573-03 WG597108 1,2,4-Trichlorobenzene mg/l 0.0284 0 .025 114. 67-133 L579573-03 WG597108 1,2,4-Trimethylbenzene mg/l 0.0257 0 .025 103. 62-141 L579573-03 WG597108 1,2-Dibromo-3-Chloropropane mg/l 0.0255 0 .025 102. 55-148 L579573-03 WG597108 1,2-Dibromoethane mg/l 0.0246 0 .025 98.4 71-129 L579573-03 WG597108 1,2-Dichlorobenzene mg/l 0.0259 0 .025 104. 75-125 L579573-03 WG597108 1,2-Dichloroethane mg/l 0.0251 0 .025 100. 59-135 L579573-03 WG597108 1,2-Dichloropropane mg/l 0.0256 0 .025 102. 68-126 L579573-03 WG597108 1,3,5-Trimethylbenzene mg/l 0.0259 0 .025 104. 67-136 L579573-03 WG597108 1,3-Dichlorobenzene mg/l 0.0256 0 .025 102. 69-131 L579573-03 WG597108 1,3-Dichloropropane mg/l 0.0237 0 .025 95.0 70-122 L579573-03 WG597108 1,4-Dichlorobenzene mg/l 0.0252 0 .025 101. 70-123 L579573-03 WG597108 2,2-Dichloropropane mg/l 0.0262 0 .025 105. 51-141 L579573-03 WG597108 2-Butanone (MEK) mg/l 0.118 0 .125 94.7 51-149 L579573-03 WG597108 2-Chloroethyl vinyl ether mg/l 0.0418 0 .125 33.5 10-161 L579573-03 WG597108 2-Chlorotoluene mg/l 0.0253 0 .025 101. 65-133 L579573-03 WG597108 4-Chlorotoluene mg/l 0.0247 0 .025 98.7 67-129 L579573-03 WG597108 4-Methyl-2-pentanone (MIBK) mg/l 0.130 0 .125 104. 53-154 L579573-03 WG597108 Acetone mg/l 0.0874 0 .125 69.9 34-146 L579573-03 WG597108 Acrolein mg/l 0.130 0 .125 104. 10-189 L579573-03 WG597108 Acrylonitrile mg/l 0.134 0 .125 107. 49-162 L579573-03 WG597108 Benzene mg/l 0.0261 0 .025 104. 51-134 L579573-03 WG597108 Bromobenzene mg/l 0.0245 0 .025 97.9 64-130 L579573-03 WG597108 Bromodichloromethane mg/l 0.0263 0 .025 105. 67-132 L579573-03 WG597108 Bromoform mg/l 0.0263 0 .025 105. 59-137 L579573-03 WG597108 Bromomethane mg/l 0.0266 0 .025 106. 23-177 L579573-03 WG597108 Carbon tetrachloride mg/l 0.0262 0 .025 105. 49-140 L579573-03 WG597108 Chlorobenzene mg/l 0.0245 0 .025 98.0 69-126 L579573-03 WG597108 Chlorodibromomethane mg/l 0.0251 0 .025 100. 68-130 L579573-03 WG597108 Chloroethane mg/l 0.0266 0 .025 106. 32-177 L579573-03 WG597108 Chloroform mg/l 0.0250 0 .025 100. 64-130 L579573-03 WG597108 Chloromethane mg/l 0.0251 0 .025 100. 27-155 L579573-03 WG597108 cis-1,2-Dichloroethene mg/l 0.0262 0 .025 105. 54-137 L579573-03 WG597108 cis-1,3-Dichloropropene mg/l 0.0265 0 .025 106. 63-127 L579573-03 WG597108 Di-isopropyl ether mg/l 0.0266 0 .025 106. 58-133 L579573-03 WG597108 Dibromomethane mg/l 0.0265 0 .025 106. 68-131 L579573-03 WG597108 Dichlorodifluoromethane mg/l 0.0229 0 .025 91.6 16-188 L579573-03 WG597108 Ethylbenzene mg/l 0.0255 0 .025 102. 64-135 L579573-03 WG597108 Hexachloro-1,3-butadiene mg/l 0.0285 0 .025 114. 64-140 L579573-03 WG597108 Isopropylbenzene mg/l 0.0262 0 .025 105. 62-134 L579573-03 WG597108 Methyl tert-butyl ether mg/l 0.0257 0 .025 103. 55-136 L579573-03 WG597108 Methylene Chloride mg/l 0.0257 0 .025 103. 52-130 L579573-03 WG597108 n-Butylbenzene mg/l 0.0279 0 .025 112. 62-142 L579573-03 WG597108 n-Propylbenzene mg/l 0.0261 0 .025 104. 62-137 L579573-03 WG597108 Naphthalene mg/l 0.0267 0 .025 107. 65-140 L579573-03 WG597108 p-Isopropyltoluene mg/l 0.0270 0 .025 108. 64-142 L579573-03 WG597108 sec-Butylbenzene mg/l 0.0269 0 .025 108. 67-139 L579573-03 WG597108 Styrene mg/l 0.0249 0 .025 99.5 58-152 L579573-03 WG597108 tert-Butylbenzene mg/l 0.0264 0 .025 105. 66-139 L579573-03 WG597108 Tetrachloroethene mg/l 0.0258 0 .025 103. 56-139 L579573-03 WG597108 Toluene mg/l 0.0257 0 .025 103. 61-126 L579573-03 WG597108 trans-1,2-Dichloroethene mg/l 0.0267 0 .025 107. 45-137 L579573-03 WG597108

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 45 of 49

Reference 45 Page 161

Page 162: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 June 15, 2012

L579547

Matrix SpikeAnalyte Units MS Res Ref Res TV % Rec Limit Ref Samp Batch

trans-1,3-Dichloropropene mg/l 0.0260 0 .025 104. 59-130 L579573-03 WG597108 Trichloroethene mg/l 0.0270 0 .025 108. 40-155 L579573-03 WG597108 Trichlorofluoromethane mg/l 0.0272 0 .025 109. 35-177 L579573-03 WG597108 Vinyl chloride mg/l 0.0261 0 .025 104. 32-159 L579573-03 WG597108 Xylenes, Total mg/l 0.0759 0 .075 101. 64-133 L579573-03 WG597108 4-Bromofluorobenzene 97.97 82-120 WG597108 Dibromofluoromethane 105.0 82-126 WG597108 Toluene-d8 104.3 92-112 WG597108

Tetrachloroethene mg/l 0.0267 0 .025 107. 56-139 L579111-01 WG597428 4-Bromofluorobenzene 103.3 82-120 WG597428 Dibromofluoromethane 96.64 82-126 WG597428 Toluene-d8 98.19 92-112 WG597428

Matrix Spike DuplicateAnalyte Units MSD Ref %Rec Limit RPD Limit Ref Samp Batch

1,1,1,2-Tetrachloroethane mg/l 0.0281 0.0274 112. 71-130 2.34 20 L579547-05 WG597107 1,1,1-Trichloroethane mg/l 0.0271 0.0278 108. 58-137 2.56 20 L579547-05 WG597107 1,1,2,2-Tetrachloroethane mg/l 0.0280 0.0270 112. 64-149 3.89 20 L579547-05 WG597107 1,1,2-Trichloroethane mg/l 0.0278 0.0268 111. 73-128 3.60 20 L579547-05 WG597107 1,1,2-Trichlorotrifluoroethane mg/l 0.0295 0.0298 118. 36-159 0.950 21 L579547-05 WG597107 1,1-Dichloroethane mg/l 0.0233 0.0229 93.0 58-133 1.50 20 L579547-05 WG597107 1,1-Dichloroethene mg/l 0.0275 0.0276 110. 32-152 0.550 20 L579547-05 WG597107 1,1-Dichloropropene mg/l 0.0256 0.0255 102. 50-140 0.230 20 L579547-05 WG597107 1,2,3-Trichlorobenzene mg/l 0.0286 0.0282 114. 68-135 1.31 20 L579547-05 WG597107 1,2,3-Trichloropropane mg/l 0.0292 0.0279 117. 74-137 4.57 20 L579547-05 WG597107 1,2,3-Trimethylbenzene mg/l 0.0246 0.0249 98.6 67-133 1.15 20 L579547-05 WG597107 1,2,4-Trichlorobenzene mg/l 0.0293 0.0297 117. 67-133 1.19 20 L579547-05 WG597107 1,2,4-Trimethylbenzene mg/l 0.0292 0.0289 117. 62-141 1.13 20 L579547-05 WG597107 1,2-Dibromo-3-Chloropropane mg/l 0.0277 0.0272 111. 55-148 1.83 22 L579547-05 WG597107 1,2-Dibromoethane mg/l 0.0283 0.0271 113. 71-129 4.11 20 L579547-05 WG597107 1,2-Dichlorobenzene mg/l 0.0260 0.0256 104. 75-125 1.51 20 L579547-05 WG597107 1,2-Dichloroethane mg/l 0.0229 0.0226 91.5 59-135 1.19 20 L579547-05 WG597107 1,2-Dichloropropane mg/l 0.0232 0.0227 92.8 68-126 2.41 20 L579547-05 WG597107 1,3,5-Trimethylbenzene mg/l 0.0290 0.0291 116. 67-136 0.480 20 L579547-05 WG597107 1,3-Dichlorobenzene mg/l 0.0296 0.0292 118. 69-131 1.34 20 L579547-05 WG597107 1,3-Dichloropropane mg/l 0.0254 0.0243 102. 70-122 4.19 20 L579547-05 WG597107 1,4-Dichlorobenzene mg/l 0.0260 0.0258 104. 70-123 1.04 20 L579547-05 WG597107 2,2-Dichloropropane mg/l 0.0252 0.0261 101. 51-141 3.33 20 L579547-05 WG597107 2-Butanone (MEK) mg/l 0.115 0.109 92.0 51-149 5.13 22 L579547-05 WG597107 2-Chloroethyl vinyl ether mg/l 0.0128 0.0545 10.2 10-161 124.* 40 L579547-05 WG597107 2-Chlorotoluene mg/l 0.0283 0.0275 113. 65-133 2.66 20 L579547-05 WG597107 4-Chlorotoluene mg/l 0.0282 0.0275 113. 67-129 2.29 20 L579547-05 WG597107 4-Methyl-2-pentanone (MIBK) mg/l 0.130 0.122 104. 53-154 6.53 21 L579547-05 WG597107 Acetone mg/l 0.0860 0.0815 68.8 34-146 5.40 22 L579547-05 WG597107 Acrolein mg/l 0.152 0.150 122. 10-189 1.68 30 L579547-05 WG597107 Acrylonitrile mg/l 0.120 0.115 95.9 49-162 4.16 20 L579547-05 WG597107 Benzene mg/l 0.0246 0.0242 98.4 51-134 1.57 20 L579547-05 WG597107 Bromobenzene mg/l 0.0265 0.0257 106. 64-130 2.85 20 L579547-05 WG597107 Bromodichloromethane mg/l 0.0249 0.0243 99.6 67-132 2.58 20 L579547-05 WG597107 Bromoform mg/l 0.0305 0.0293 122. 59-137 3.78 20 L579547-05 WG597107 Bromomethane mg/l 0.0242 0.0244 96.9 23-177 0.850 21 L579547-05 WG597107 Carbon tetrachloride mg/l 0.0288 0.0285 115. 49-140 1.23 20 L579547-05 WG597107 Chlorobenzene mg/l 0.0278 0.0268 111. 69-126 3.79 20 L579547-05 WG597107 Chlorodibromomethane mg/l 0.0281 0.0272 112. 68-130 3.20 20 L579547-05 WG597107 Chloroethane mg/l 0.0246 0.0248 98.2 32-177 0.860 21 L579547-05 WG597107 Chloroform mg/l 0.0248 0.0245 99.1 64-130 1.19 20 L579547-05 WG597107

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 46 of 49

Reference 45 Page 162

Page 163: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 June 15, 2012

L579547

Matrix Spike DuplicateAnalyte Units MSD Ref %Rec Limit RPD Limit Ref Samp Batch

Chloromethane mg/l 0.0194 0.0194 77.4 27-155 0.270 20 L579547-05 WG597107 cis-1,2-Dichloroethene mg/l 0.0258 0.0254 103. 54-137 1.81 20 L579547-05 WG597107 cis-1,3-Dichloropropene mg/l 0.0250 0.0245 99.9 63-127 1.92 20 L579547-05 WG597107 Di-isopropyl ether mg/l 0.0214 0.0213 85.7 58-133 0.730 20 L579547-05 WG597107 Dibromomethane mg/l 0.0256 0.0251 102. 68-131 2.04 20 L579547-05 WG597107 Dichlorodifluoromethane mg/l 0.0232 0.0230 92.8 16-188 1.04 22 L579547-05 WG597107 Ethylbenzene mg/l 0.0288 0.0280 115. 64-135 2.53 20 L579547-05 WG597107 Hexachloro-1,3-butadiene mg/l 0.0299 0.0306 120. 64-140 2.27 20 L579547-05 WG597107 Isopropylbenzene mg/l 0.0295 0.0292 118. 62-134 1.24 20 L579547-05 WG597107 Methyl tert-butyl ether mg/l 0.0241 0.0244 96.6 55-136 0.870 20 L579547-05 WG597107 Methylene Chloride mg/l 0.0249 0.0247 99.6 52-130 0.950 20 L579547-05 WG597107 n-Butylbenzene mg/l 0.0275 0.0277 110. 62-142 0.990 20 L579547-05 WG597107 n-Propylbenzene mg/l 0.0293 0.0289 117. 62-137 1.38 20 L579547-05 WG597107 Naphthalene mg/l 0.0276 0.0274 110. 65-140 0.640 20 L579547-05 WG597107 p-Isopropyltoluene mg/l 0.0312 0.0309 125. 64-142 1.04 20 L579547-05 WG597107 sec-Butylbenzene mg/l 0.0301 0.0301 120. 67-139 0.110 20 L579547-05 WG597107 Styrene mg/l 0.0286 0.0277 114. 58-152 3.23 20 L579547-05 WG597107 tert-Butylbenzene mg/l 0.0296 0.0299 118. 66-139 0.980 20 L579547-05 WG597107 Tetrachloroethene mg/l 0.0622 0.0630 121. 56-139 1.21 20 L579547-05 WG597107 Toluene mg/l 0.0260 0.0253 104. 61-126 2.82 20 L579547-05 WG597107 trans-1,2-Dichloroethene mg/l 0.0261 0.0265 104. 45-137 1.46 20 L579547-05 WG597107 trans-1,3-Dichloropropene mg/l 0.0270 0.0266 108. 59-130 1.33 20 L579547-05 WG597107 Trichloroethene mg/l 0.0382 0.0379 105. 40-155 0.780 20 L579547-05 WG597107 Trichlorofluoromethane mg/l 0.0280 0.0277 112. 35-177 1.06 23 L579547-05 WG597107 Vinyl chloride mg/l 0.0223 0.0227 89.2 32-159 1.89 21 L579547-05 WG597107 Xylenes, Total mg/l 0.0858 0.0843 114. 64-133 1.73 20 L579547-05 WG597107 4-Bromofluorobenzene 108.8 82-120 WG597107 Dibromofluoromethane 96.77 82-126 WG597107 Toluene-d8 101.0 92-112 WG597107

1,1,1,2-Tetrachloroethane mg/l 0.0250 0.0246 100. 71-130 1.75 20 L579573-03 WG597108 1,1,1-Trichloroethane mg/l 0.0269 0.0266 108. 58-137 1.23 20 L579573-03 WG597108 1,1,2,2-Tetrachloroethane mg/l 0.0256 0.0256 102. 64-149 0.230 20 L579573-03 WG597108 1,1,2-Trichloroethane mg/l 0.0258 0.0246 103. 73-128 4.80 20 L579573-03 WG597108 1,1,2-Trichlorotrifluoroethane mg/l 0.0292 0.0283 117. 36-159 2.90 21 L579573-03 WG597108 1,1-Dichloroethane mg/l 0.0266 0.0259 106. 58-133 2.83 20 L579573-03 WG597108 1,1-Dichloroethene mg/l 0.0274 0.0272 109. 32-152 0.730 20 L579573-03 WG597108 1,1-Dichloropropene mg/l 0.0272 0.0265 109. 50-140 2.46 20 L579573-03 WG597108 1,2,3-Trichlorobenzene mg/l 0.0282 0.0278 113. 68-135 1.62 20 L579573-03 WG597108 1,2,3-Trichloropropane mg/l 0.0238 0.0237 95.1 74-137 0.300 20 L579573-03 WG597108 1,2,3-Trimethylbenzene mg/l 0.0253 0.0253 101. 67-133 0.0500 20 L579573-03 WG597108 1,2,4-Trichlorobenzene mg/l 0.0286 0.0284 114. 67-133 0.450 20 L579573-03 WG597108 1,2,4-Trimethylbenzene mg/l 0.0263 0.0257 105. 62-141 2.51 20 L579573-03 WG597108 1,2-Dibromo-3-Chloropropane mg/l 0.0255 0.0255 102. 55-148 0.0600 22 L579573-03 WG597108 1,2-Dibromoethane mg/l 0.0250 0.0246 100. 71-129 1.61 20 L579573-03 WG597108 1,2-Dichlorobenzene mg/l 0.0260 0.0259 104. 75-125 0.490 20 L579573-03 WG597108 1,2-Dichloroethane mg/l 0.0255 0.0251 102. 59-135 1.39 20 L579573-03 WG597108 1,2-Dichloropropane mg/l 0.0262 0.0256 105. 68-126 2.38 20 L579573-03 WG597108 1,3,5-Trimethylbenzene mg/l 0.0265 0.0259 106. 67-136 2.28 20 L579573-03 WG597108 1,3-Dichlorobenzene mg/l 0.0260 0.0256 104. 69-131 1.51 20 L579573-03 WG597108 1,3-Dichloropropane mg/l 0.0243 0.0237 97.2 70-122 2.30 20 L579573-03 WG597108 1,4-Dichlorobenzene mg/l 0.0254 0.0252 102. 70-123 0.710 20 L579573-03 WG597108 2,2-Dichloropropane mg/l 0.0272 0.0262 109. 51-141 3.94 20 L579573-03 WG597108 2-Butanone (MEK) mg/l 0.120 0.118 96.4 51-149 1.74 22 L579573-03 WG597108 2-Chloroethyl vinyl ether mg/l 0.00222 0.0418 1.78* 10-161 180.* 40 L579573-03 WG597108 2-Chlorotoluene mg/l 0.0255 0.0253 102. 65-133 0.750 20 L579573-03 WG597108 4-Chlorotoluene mg/l 0.0254 0.0247 101. 67-129 2.81 20 L579573-03 WG597108 4-Methyl-2-pentanone (MIBK) mg/l 0.130 0.130 104. 53-154 0.170 21 L579573-03 WG597108

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 47 of 49

Reference 45 Page 163

Page 164: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 June 15, 2012

L579547

Matrix Spike DuplicateAnalyte Units MSD Ref %Rec Limit RPD Limit Ref Samp Batch

Acetone mg/l 0.0859 0.0874 68.7 34-146 1.67 22 L579573-03 WG597108 Acrolein mg/l 0.128 0.130 102. 10-189 1.53 30 L579573-03 WG597108 Acrylonitrile mg/l 0.136 0.134 108. 49-162 1.00 20 L579573-03 WG597108 Benzene mg/l 0.0267 0.0261 107. 51-134 2.35 20 L579573-03 WG597108 Bromobenzene mg/l 0.0248 0.0245 99.1 64-130 1.17 20 L579573-03 WG597108 Bromodichloromethane mg/l 0.0267 0.0263 107. 67-132 1.47 20 L579573-03 WG597108 Bromoform mg/l 0.0270 0.0263 108. 59-137 2.65 20 L579573-03 WG597108 Bromomethane mg/l 0.0275 0.0266 110. 23-177 3.51 21 L579573-03 WG597108 Carbon tetrachloride mg/l 0.0271 0.0262 108. 49-140 3.65 20 L579573-03 WG597108 Chlorobenzene mg/l 0.0251 0.0245 100. 69-126 2.53 20 L579573-03 WG597108 Chlorodibromomethane mg/l 0.0256 0.0251 102. 68-130 2.10 20 L579573-03 WG597108 Chloroethane mg/l 0.0275 0.0266 110. 32-177 3.37 21 L579573-03 WG597108 Chloroform mg/l 0.0257 0.0250 103. 64-130 2.59 20 L579573-03 WG597108 Chloromethane mg/l 0.0250 0.0251 100. 27-155 0.130 20 L579573-03 WG597108 cis-1,2-Dichloroethene mg/l 0.0266 0.0262 106. 54-137 1.34 20 L579573-03 WG597108 cis-1,3-Dichloropropene mg/l 0.0266 0.0265 106. 63-127 0.0800 20 L579573-03 WG597108 Di-isopropyl ether mg/l 0.0270 0.0266 108. 58-133 1.54 20 L579573-03 WG597108 Dibromomethane mg/l 0.0261 0.0265 104. 68-131 1.60 20 L579573-03 WG597108 Dichlorodifluoromethane mg/l 0.0228 0.0229 91.3 16-188 0.320 22 L579573-03 WG597108 Ethylbenzene mg/l 0.0260 0.0255 104. 64-135 2.05 20 L579573-03 WG597108 Hexachloro-1,3-butadiene mg/l 0.0287 0.0285 115. 64-140 0.590 20 L579573-03 WG597108 Isopropylbenzene mg/l 0.0268 0.0262 107. 62-134 2.04 20 L579573-03 WG597108 Methyl tert-butyl ether mg/l 0.0260 0.0257 104. 55-136 1.19 20 L579573-03 WG597108 Methylene Chloride mg/l 0.0260 0.0257 104. 52-130 1.28 20 L579573-03 WG597108 n-Butylbenzene mg/l 0.0281 0.0279 112. 62-142 0.830 20 L579573-03 WG597108 n-Propylbenzene mg/l 0.0265 0.0261 106. 62-137 1.52 20 L579573-03 WG597108 Naphthalene mg/l 0.0269 0.0267 108. 65-140 1.05 20 L579573-03 WG597108 p-Isopropyltoluene mg/l 0.0279 0.0270 112. 64-142 3.12 20 L579573-03 WG597108 sec-Butylbenzene mg/l 0.0272 0.0269 109. 67-139 1.00 20 L579573-03 WG597108 Styrene mg/l 0.0257 0.0249 103. 58-152 3.44 20 L579573-03 WG597108 tert-Butylbenzene mg/l 0.0269 0.0264 108. 66-139 2.05 20 L579573-03 WG597108 Tetrachloroethene mg/l 0.0266 0.0258 106. 56-139 3.03 20 L579573-03 WG597108 Toluene mg/l 0.0260 0.0257 104. 61-126 1.22 20 L579573-03 WG597108 trans-1,2-Dichloroethene mg/l 0.0277 0.0267 111. 45-137 3.54 20 L579573-03 WG597108 trans-1,3-Dichloropropene mg/l 0.0260 0.0260 104. 59-130 0.150 20 L579573-03 WG597108 Trichloroethene mg/l 0.0268 0.0270 107. 40-155 0.560 20 L579573-03 WG597108 Trichlorofluoromethane mg/l 0.0278 0.0272 111. 35-177 1.99 23 L579573-03 WG597108 Vinyl chloride mg/l 0.0260 0.0261 104. 32-159 0.100 21 L579573-03 WG597108 Xylenes, Total mg/l 0.0775 0.0759 103. 64-133 2.12 20 L579573-03 WG597108 4-Bromofluorobenzene 97.23 82-120 WG597108 Dibromofluoromethane 104.2 82-126 WG597108 Toluene-d8 101.7 92-112 WG597108

Tetrachloroethene mg/l 0.0281 0.0267 112. 56-139 5.39 20 L579111-01 WG597428 4-Bromofluorobenzene 105.9 82-120 WG597428 Dibromofluoromethane 98.29 82-126 WG597428 Toluene-d8 98.94 92-112 WG597428

Batch number /Run number / Sample number cross reference

WG597107: R2206795: L579547-01 02 03 04 05 06 07 08 09 10 11WG597108: R2206898: L579547-12 13 14 15 16 17WG597428: R2208255: L579547-01

* * Calculations are performed prior to rounding of reported values.* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 48 of 49

Reference 45 Page 164

Page 165: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 June 15, 2012

L579547

The data package includes a summary of the analytic results of the qualitycontrol samples required by the SW-846 or CWA methods. The quality controlsamples include a method blank, a laboratory control sample, and the matrixspike/matrix spike duplicate analysis. If a target parameter is outsidethe method limits, every sample that is effected is flagged with theappropriate qualifier in Appendix B of the analytic report.

Method Blank - an aliquot of reagent water carried through theentire analytic process. The method blank results indicate ifany possible contamination exposure during the sample handling,digestion or extraction process, and analysis. Concentrations oftarget analytes above the reporting limit in the method blank arequalified with the "B" qualifier.

Laboratory Control Sample - is a sample of known concentrationthat is carried through the digestion/extraction and analysisprocess. The percent recovery, expressed as a percentage of thetheoretical concentration, has statistical control limitsindicating that the analytic process is "in control". If atarget analyte is outside the control limits for the laboratorycontrol sample or any other control sample, the parameter isflagged with a "J4" qualifier for all effected samples.

Matrix Spike and Matrix Spike Duplicate - is two aliquots of anenvironmental sample that is spiked with known concentrations oftarget analytes. The percent recovery of the target analytesalso has statistical control limits. If any recoveries that areoutside the method control limits, the sample that was selectedfor matrix spike/matrix spike duplicate analysis is flagged witheither a "J5" or a "J6". The relative percent difference (%RPD)between the matrix spike and the matrix spike duplicaterecoveries is all calculated. If the RPD is above the methodlimit, the effected samples are flagged with a "J3" qualifier.

Page 49 of 49

Reference 45 Page 165

Page 166: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

Mrs. Wendy MilejczakAcuity Environmental Solutions7965 East 106th St. Suite 128Fishers, IN 46038

Report Summary

Tuesday September 25, 2012

Report Number: L595984

Samples Received: 09/19/12

Client Project: 1024-1003-01

Description: Component Machine

The analytical results in this report are based upon information suppliedby you, the client, and are for your exclusive use. If you have anyquestions regarding this data package, please do not hesitate to call.

Entire Report Reviewed By: ____________________________________

T. Alan Harvill , ESC Representative

Laboratory Certification NumbersA2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197,FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,NC - ENV375/DW21704/BIO041, ND - R-140. NJ - TN002, NJ NELAP - TN002,SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,TX - T104704245-11-3, OK - 9915, PA - 68-02979

Accreditation is only applicable to the test methods specified on each scope of accreditation heldby ESC Lab Sciences.Note: The use of the preparatory EPA Method 3511 is not approved or endorsed by the CA ELAP.

This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.Where applicable, sampling conducted by ESC is performed per guidance providedin laboratory standard operating procedures: 060302, 060303, and 060304.

Page 1 of 49

Reference 45 Page 166

Page 167: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-01 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : PMW-4

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/17/12 11:20

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 100 ug/l 8260B 09/23/12 2 Acrolein BDL 100 ug/l 8260B 09/23/12 2 Acrylonitrile BDL 20. ug/l 8260B 09/23/12 2 Benzene BDL 2.0 ug/l 8260B 09/23/12 2 Bromobenzene BDL 2.0 ug/l 8260B 09/23/12 2 Bromodichloromethane BDL 2.0 ug/l 8260B 09/23/12 2 Bromoform BDL 2.0 ug/l 8260B 09/23/12 2 Bromomethane BDL 10. ug/l 8260B 09/23/12 2 n-Butylbenzene BDL 2.0 ug/l 8260B 09/23/12 2 sec-Butylbenzene BDL 2.0 ug/l 8260B 09/23/12 2 tert-Butylbenzene BDL 2.0 ug/l 8260B 09/23/12 2 Carbon tetrachloride BDL 2.0 ug/l 8260B 09/23/12 2 Chlorobenzene BDL 2.0 ug/l 8260B 09/23/12 2 Chlorodibromomethane BDL 2.0 ug/l 8260B 09/23/12 2 Chloroethane BDL 10. ug/l 8260B 09/23/12 2 2-Chloroethyl vinyl ether BDL 100 ug/l 8260B 09/23/12 2 Chloroform BDL 10. ug/l 8260B 09/23/12 2 Chloromethane BDL 5.0 ug/l 8260B 09/23/12 2 2-Chlorotoluene BDL 2.0 ug/l 8260B 09/23/12 2 4-Chlorotoluene BDL 2.0 ug/l 8260B 09/23/12 2 1,2-Dibromo-3-Chloropropane BDL 10. ug/l 8260B 09/23/12 2 1,2-Dibromoethane BDL 2.0 ug/l 8260B 09/23/12 2 Dibromomethane BDL 2.0 ug/l 8260B 09/23/12 2 1,2-Dichlorobenzene BDL 2.0 ug/l 8260B 09/23/12 2 1,3-Dichlorobenzene BDL 2.0 ug/l 8260B 09/23/12 2 1,4-Dichlorobenzene BDL 2.0 ug/l 8260B 09/23/12 2 Dichlorodifluoromethane BDL 10. ug/l 8260B 09/23/12 2 1,1-Dichloroethane BDL 2.0 ug/l 8260B 09/23/12 2 1,2-Dichloroethane BDL 2.0 ug/l 8260B 09/23/12 2 1,1-Dichloroethene BDL 2.0 ug/l 8260B 09/23/12 2 cis-1,2-Dichloroethene 91. 2.0 ug/l 8260B 09/23/12 2 trans-1,2-Dichloroethene 2.8 2.0 ug/l 8260B 09/23/12 2 1,2-Dichloropropane BDL 2.0 ug/l 8260B 09/23/12 2 1,1-Dichloropropene BDL 2.0 ug/l 8260B 09/23/12 2 1,3-Dichloropropane BDL 2.0 ug/l 8260B 09/23/12 2 cis-1,3-Dichloropropene BDL 2.0 ug/l 8260B 09/23/12 2 trans-1,3-Dichloropropene BDL 2.0 ug/l 8260B 09/23/12 2 2,2-Dichloropropane BDL 2.0 ug/l 8260B 09/23/12 2 Di-isopropyl ether BDL 2.0 ug/l 8260B 09/23/12 2 Ethylbenzene BDL 2.0 ug/l 8260B 09/23/12 2 Hexachloro-1,3-butadiene BDL 2.0 ug/l 8260B 09/23/12 2 Isopropylbenzene BDL 2.0 ug/l 8260B 09/23/12 2 p-Isopropyltoluene BDL 2.0 ug/l 8260B 09/23/12 2

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 2 of 49

Reference 45 Page 167

Page 168: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-01 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : PMW-4

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/17/12 11:20

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 20. ug/l 8260B 09/23/12 2 Methylene Chloride BDL 10. ug/l 8260B 09/23/12 2 4-Methyl-2-pentanone (MIBK) BDL 20. ug/l 8260B 09/23/12 2 Methyl tert-butyl ether BDL 2.0 ug/l 8260B 09/23/12 2 Naphthalene BDL 10. ug/l 8260B 09/23/12 2 n-Propylbenzene BDL 2.0 ug/l 8260B 09/23/12 2 Styrene BDL 2.0 ug/l 8260B 09/23/12 2 1,1,1,2-Tetrachloroethane BDL 2.0 ug/l 8260B 09/23/12 2 1,1,2,2-Tetrachloroethane BDL 2.0 ug/l 8260B 09/23/12 2 1,1,2-Trichlorotrifluoroethane BDL 2.0 ug/l 8260B 09/23/12 2 Tetrachloroethene 92. 2.0 ug/l 8260B 09/23/12 2 Toluene BDL 10. ug/l 8260B 09/23/12 2 1,2,3-Trichlorobenzene BDL 2.0 ug/l 8260B 09/23/12 2 1,2,4-Trichlorobenzene BDL 2.0 ug/l 8260B 09/23/12 2 1,1,1-Trichloroethane BDL 2.0 ug/l 8260B 09/23/12 2 1,1,2-Trichloroethane BDL 2.0 ug/l 8260B 09/23/12 2 Trichloroethene 30. 2.0 ug/l 8260B 09/23/12 2 Trichlorofluoromethane BDL 10. ug/l 8260B 09/23/12 2 1,2,3-Trichloropropane BDL 5.0 ug/l 8260B 09/23/12 2 1,2,4-Trimethylbenzene BDL 2.0 ug/l 8260B 09/23/12 2 1,2,3-Trimethylbenzene BDL 2.0 ug/l 8260B 09/23/12 2 1,3,5-Trimethylbenzene BDL 2.0 ug/l 8260B 09/23/12 2 Vinyl chloride BDL 2.0 ug/l 8260B 09/23/12 2 Xylenes, Total BDL 6.0 ug/l 8260B 09/23/12 2

Surrogate Recovery Toluene-d8 107. % Rec. 8260B 09/23/12 2 Dibromofluoromethane 102. % Rec. 8260B 09/23/12 2 4-Bromofluorobenzene 107. % Rec. 8260B 09/23/12 2

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 09/25/12 14:50 Printed: 09/25/12 16:30

Page 3 of 49

Reference 45 Page 168

Page 169: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25, 2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-02 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : PMW-5

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/17/12 11:55

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 09/23/12 1 Acrolein BDL 50. ug/l 8260B 09/23/12 1 Acrylonitrile BDL 10. ug/l 8260B 09/23/12 1 Benzene BDL 1.0 ug/l 8260B 09/23/12 1 Bromobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 09/23/12 1 Bromoform BDL 1.0 ug/l 8260B 09/23/12 1 Bromomethane BDL 5.0 ug/l 8260B 09/23/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 09/23/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 09/23/12 1 Chloroethane BDL 5.0 ug/l 8260B 09/23/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 09/23/12 1 Chloroform 6.7 5.0 ug/l 8260B 09/23/12 1 Chloromethane BDL 2.5 ug/l 8260B 09/23/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 09/23/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 09/23/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 09/23/12 1 Dibromomethane BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 09/23/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 09/23/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 09/23/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 09/23/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 4 of 49

Reference 45 Page 169

Page 170: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25, 2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-02 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : PMW-5

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/17/12 11:55

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 09/23/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 09/23/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 09/23/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 09/23/12 1 Naphthalene BDL 5.0 ug/l 8260B 09/23/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Styrene BDL 1.0 ug/l 8260B 09/23/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 09/23/12 1 Tetrachloroethene 12. 1.0 ug/l 8260B 09/23/12 1 Toluene BDL 5.0 ug/l 8260B 09/23/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 Trichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 09/23/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 09/23/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 09/23/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 09/23/12 1

Surrogate Recovery Toluene-d8 107. % Rec. 8260B 09/23/12 1 Dibromofluoromethane 103. % Rec. 8260B 09/23/12 1 4-Bromofluorobenzene 107. % Rec. 8260B 09/23/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 09/25/12 14:50 Printed: 09/25/12 16:30

Page 5 of 49

Reference 45 Page 170

Page 171: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25, 2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-03 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : PMW-5 MS

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/17/12 11:55

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Matrix Spike See QC Report for % Rec. and RPD

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 09/25/12 14:50 Printed: 09/25/12 16:30

Page 6 of 49

Reference 45 Page 171

Page 172: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-04 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : PMW-5 MSD

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/17/12 11:55

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics MSD See QC Report for % Rec and RPD

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 09/25/12 14:50 Printed: 09/25/12 16:30

Page 7 of 49

Reference 45 Page 172

Page 173: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-05 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : MW-8

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/17/12 12:38

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 09/23/12 1 Acrolein BDL 50. ug/l 8260B 09/23/12 1 Acrylonitrile BDL 10. ug/l 8260B 09/23/12 1 Benzene BDL 1.0 ug/l 8260B 09/23/12 1 Bromobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 09/23/12 1 Bromoform BDL 1.0 ug/l 8260B 09/23/12 1 Bromomethane BDL 5.0 ug/l 8260B 09/23/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 09/23/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 09/23/12 1 Chloroethane BDL 5.0 ug/l 8260B 09/23/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 09/23/12 1 Chloroform 10. 5.0 ug/l 8260B 09/23/12 1 Chloromethane BDL 2.5 ug/l 8260B 09/23/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 09/23/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 09/23/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 09/23/12 1 Dibromomethane BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 09/23/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 cis-1,2-Dichloroethene 5.1 1.0 ug/l 8260B 09/23/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 09/23/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 09/23/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 09/23/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 8 of 49

Reference 45 Page 173

Page 174: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-05 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : MW-8

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/17/12 12:38

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 09/23/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 09/23/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 09/23/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 09/23/12 1 Naphthalene BDL 5.0 ug/l 8260B 09/23/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Styrene BDL 1.0 ug/l 8260B 09/23/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 09/23/12 1 Tetrachloroethene 30. 1.0 ug/l 8260B 09/23/12 1 Toluene BDL 5.0 ug/l 8260B 09/23/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 Trichloroethene 21. 1.0 ug/l 8260B 09/23/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 09/23/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 09/23/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 09/23/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 09/23/12 1

Surrogate Recovery Toluene-d8 105. % Rec. 8260B 09/23/12 1 Dibromofluoromethane 104. % Rec. 8260B 09/23/12 1 4-Bromofluorobenzene 108. % Rec. 8260B 09/23/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 09/25/12 14:50 Printed: 09/25/12 16:30

Page 9 of 49

Reference 45 Page 174

Page 175: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-06 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : MW-11

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/17/12 10:50

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 09/23/12 1 Acrolein BDL 50. ug/l 8260B 09/23/12 1 Acrylonitrile BDL 10. ug/l 8260B 09/23/12 1 Benzene BDL 1.0 ug/l 8260B 09/23/12 1 Bromobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 09/23/12 1 Bromoform BDL 1.0 ug/l 8260B 09/23/12 1 Bromomethane BDL 5.0 ug/l 8260B 09/23/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Carbon tetrachloride 1.5 1.0 ug/l 8260B 09/23/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 09/23/12 1 Chloroethane BDL 5.0 ug/l 8260B 09/23/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 09/23/12 1 Chloroform BDL 5.0 ug/l 8260B 09/23/12 1 Chloromethane BDL 2.5 ug/l 8260B 09/23/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 09/23/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 09/23/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 09/23/12 1 Dibromomethane BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 09/23/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 09/23/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 09/23/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 09/23/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 10 of 49

Reference 45 Page 175

Page 176: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-06 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : MW-11

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/17/12 10:50

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 09/23/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 09/23/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 09/23/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 09/23/12 1 Naphthalene BDL 5.0 ug/l 8260B 09/23/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Styrene BDL 1.0 ug/l 8260B 09/23/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 09/23/12 1 Tetrachloroethene 4.8 1.0 ug/l 8260B 09/23/12 1 Toluene BDL 5.0 ug/l 8260B 09/23/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,1,1-Trichloroethane 1.9 1.0 ug/l 8260B 09/23/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 Trichloroethene 37. 1.0 ug/l 8260B 09/23/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 09/23/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 09/23/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 09/23/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 09/23/12 1

Surrogate Recovery Toluene-d8 105. % Rec. 8260B 09/23/12 1 Dibromofluoromethane 105. % Rec. 8260B 09/23/12 1 4-Bromofluorobenzene 108. % Rec. 8260B 09/23/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 09/25/12 14:50 Printed: 09/25/12 16:30

Page 11 of 49

Reference 45 Page 176

Page 177: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-07 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : PMW-11

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/17/12 13:25

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 09/23/12 1 Acrolein BDL 50. ug/l 8260B 09/23/12 1 Acrylonitrile BDL 10. ug/l 8260B 09/23/12 1 Benzene BDL 1.0 ug/l 8260B 09/23/12 1 Bromobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 09/23/12 1 Bromoform BDL 1.0 ug/l 8260B 09/23/12 1 Bromomethane BDL 5.0 ug/l 8260B 09/23/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 09/23/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 09/23/12 1 Chloroethane BDL 5.0 ug/l 8260B 09/23/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 09/23/12 1 Chloroform BDL 5.0 ug/l 8260B 09/23/12 1 Chloromethane BDL 2.5 ug/l 8260B 09/23/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 09/23/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 09/23/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 09/23/12 1 Dibromomethane BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 09/23/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 cis-1,2-Dichloroethene 1.8 1.0 ug/l 8260B 09/23/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 09/23/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 09/23/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 09/23/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 12 of 49

Reference 45 Page 177

Page 178: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-07 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : PMW-11

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/17/12 13:25

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 09/23/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 09/23/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 09/23/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 09/23/12 1 Naphthalene BDL 5.0 ug/l 8260B 09/23/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Styrene BDL 1.0 ug/l 8260B 09/23/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 09/23/12 1 Tetrachloroethene 19. 1.0 ug/l 8260B 09/23/12 1 Toluene BDL 5.0 ug/l 8260B 09/23/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 Trichloroethene 9.3 1.0 ug/l 8260B 09/23/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 09/23/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 09/23/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 09/23/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 09/23/12 1

Surrogate Recovery Toluene-d8 106. % Rec. 8260B 09/23/12 1 Dibromofluoromethane 101. % Rec. 8260B 09/23/12 1 4-Bromofluorobenzene 108. % Rec. 8260B 09/23/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 09/25/12 14:50 Printed: 09/25/12 16:30

Page 13 of 49

Reference 45 Page 178

Page 179: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-08 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : MW-10

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/17/12 13:58

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 09/23/12 1 Acrolein BDL 50. ug/l 8260B 09/23/12 1 Acrylonitrile BDL 10. ug/l 8260B 09/23/12 1 Benzene BDL 1.0 ug/l 8260B 09/23/12 1 Bromobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 09/23/12 1 Bromoform BDL 1.0 ug/l 8260B 09/23/12 1 Bromomethane BDL 5.0 ug/l 8260B 09/23/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 09/23/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 09/23/12 1 Chloroethane BDL 5.0 ug/l 8260B 09/23/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 09/23/12 1 Chloroform 11. 5.0 ug/l 8260B 09/23/12 1 Chloromethane BDL 2.5 ug/l 8260B 09/23/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 09/23/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 09/23/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 09/23/12 1 Dibromomethane BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 09/23/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 09/23/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 09/23/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 09/23/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 14 of 49

Reference 45 Page 179

Page 180: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-08 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : MW-10

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/17/12 13:58

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 09/23/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 09/23/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 09/23/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 09/23/12 1 Naphthalene BDL 5.0 ug/l 8260B 09/23/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Styrene BDL 1.0 ug/l 8260B 09/23/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 09/23/12 1 Tetrachloroethene 8.8 1.0 ug/l 8260B 09/23/12 1 Toluene BDL 5.0 ug/l 8260B 09/23/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 Trichloroethene 3.6 1.0 ug/l 8260B 09/23/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 09/23/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 09/23/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 09/23/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 09/23/12 1

Surrogate Recovery Toluene-d8 107. % Rec. 8260B 09/23/12 1 Dibromofluoromethane 105. % Rec. 8260B 09/23/12 1 4-Bromofluorobenzene 108. % Rec. 8260B 09/23/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 09/25/12 14:50 Printed: 09/25/12 16:30

Page 15 of 49

Reference 45 Page 180

Page 181: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-09 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : MW-9

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/18/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 09/23/12 1 Acrolein BDL 50. ug/l 8260B 09/23/12 1 Acrylonitrile BDL 10. ug/l 8260B 09/23/12 1 Benzene BDL 1.0 ug/l 8260B 09/23/12 1 Bromobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 09/23/12 1 Bromoform BDL 1.0 ug/l 8260B 09/23/12 1 Bromomethane BDL 5.0 ug/l 8260B 09/23/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 09/23/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 09/23/12 1 Chloroethane BDL 5.0 ug/l 8260B 09/23/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 09/23/12 1 Chloroform BDL 5.0 ug/l 8260B 09/23/12 1 Chloromethane BDL 2.5 ug/l 8260B 09/23/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 09/23/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 09/23/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 09/23/12 1 Dibromomethane BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 09/23/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 cis-1,2-Dichloroethene 8.2 1.0 ug/l 8260B 09/23/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 09/23/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 09/23/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 09/23/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 16 of 49

Reference 45 Page 181

Page 182: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-09 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : MW-9

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/18/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 09/23/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 09/23/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 09/23/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 09/23/12 1 Naphthalene BDL 5.0 ug/l 8260B 09/23/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Styrene BDL 1.0 ug/l 8260B 09/23/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 09/23/12 1 Tetrachloroethene 48. 1.0 ug/l 8260B 09/23/12 1 Toluene BDL 5.0 ug/l 8260B 09/23/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 Trichloroethene 13. 1.0 ug/l 8260B 09/23/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 09/23/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 09/23/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 09/23/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 09/23/12 1

Surrogate Recovery Toluene-d8 106. % Rec. 8260B 09/23/12 1 Dibromofluoromethane 102. % Rec. 8260B 09/23/12 1 4-Bromofluorobenzene 107. % Rec. 8260B 09/23/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 09/25/12 14:50 Printed: 09/25/12 16:30

Page 17 of 49

Reference 45 Page 182

Page 183: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-10 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : PMW-6

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/17/12 10:10

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 09/23/12 1 Acrolein BDL 50. ug/l 8260B 09/23/12 1 Acrylonitrile BDL 10. ug/l 8260B 09/23/12 1 Benzene BDL 1.0 ug/l 8260B 09/23/12 1 Bromobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 09/23/12 1 Bromoform BDL 1.0 ug/l 8260B 09/23/12 1 Bromomethane BDL 5.0 ug/l 8260B 09/23/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 09/23/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 09/23/12 1 Chloroethane BDL 5.0 ug/l 8260B 09/23/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 09/23/12 1 Chloroform BDL 5.0 ug/l 8260B 09/23/12 1 Chloromethane BDL 2.5 ug/l 8260B 09/23/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 09/23/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 09/23/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 09/23/12 1 Dibromomethane BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 09/23/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 cis-1,2-Dichloroethene 1.2 1.0 ug/l 8260B 09/23/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 09/23/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 09/23/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 09/23/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 18 of 49

Reference 45 Page 183

Page 184: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-10 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : PMW-6

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/17/12 10:10

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 09/23/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 09/23/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 09/23/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 09/23/12 1 Naphthalene BDL 5.0 ug/l 8260B 09/23/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Styrene BDL 1.0 ug/l 8260B 09/23/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 09/23/12 1 Tetrachloroethene 1.7 1.0 ug/l 8260B 09/23/12 1 Toluene BDL 5.0 ug/l 8260B 09/23/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,1,1-Trichloroethane 1.6 1.0 ug/l 8260B 09/23/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 Trichloroethene 24. 1.0 ug/l 8260B 09/23/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 09/23/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 09/23/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 09/23/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 09/23/12 1

Surrogate Recovery Toluene-d8 107. % Rec. 8260B 09/23/12 1 Dibromofluoromethane 105. % Rec. 8260B 09/23/12 1 4-Bromofluorobenzene 108. % Rec. 8260B 09/23/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 09/25/12 14:50 Printed: 09/25/12 16:31

Page 19 of 49

Reference 45 Page 184

Page 185: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-11 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : MW-12

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/18/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 09/23/12 1 Acrolein BDL 50. ug/l 8260B 09/23/12 1 Acrylonitrile BDL 10. ug/l 8260B 09/23/12 1 Benzene BDL 1.0 ug/l 8260B 09/23/12 1 Bromobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 09/23/12 1 Bromoform BDL 1.0 ug/l 8260B 09/23/12 1 Bromomethane BDL 5.0 ug/l 8260B 09/23/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 09/23/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 09/23/12 1 Chloroethane BDL 5.0 ug/l 8260B 09/23/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 09/23/12 1 Chloroform BDL 5.0 ug/l 8260B 09/23/12 1 Chloromethane BDL 2.5 ug/l 8260B 09/23/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 09/23/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 09/23/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 09/23/12 1 Dibromomethane BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 09/23/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 09/23/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 09/23/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 09/23/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 20 of 49

Reference 45 Page 185

Page 186: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-11 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : MW-12

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/18/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 09/23/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 09/23/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 09/23/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 09/23/12 1 Naphthalene BDL 5.0 ug/l 8260B 09/23/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Styrene BDL 1.0 ug/l 8260B 09/23/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 09/23/12 1 Tetrachloroethene 9.9 1.0 ug/l 8260B 09/23/12 1 Toluene BDL 5.0 ug/l 8260B 09/23/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 Trichloroethene 4.3 1.0 ug/l 8260B 09/23/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 09/23/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 09/23/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 09/23/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 09/23/12 1

Surrogate Recovery Toluene-d8 108. % Rec. 8260B 09/23/12 1 Dibromofluoromethane 104. % Rec. 8260B 09/23/12 1 4-Bromofluorobenzene 109. % Rec. 8260B 09/23/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 09/25/12 14:50 Printed: 09/25/12 16:31

Page 21 of 49

Reference 45 Page 186

Page 187: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-12 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : MW-13

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/18/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 09/23/12 1 Acrolein BDL 50. ug/l 8260B 09/23/12 1 Acrylonitrile BDL 10. ug/l 8260B 09/23/12 1 Benzene BDL 1.0 ug/l 8260B 09/23/12 1 Bromobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 09/23/12 1 Bromoform BDL 1.0 ug/l 8260B 09/23/12 1 Bromomethane BDL 5.0 ug/l 8260B 09/23/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 09/23/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 09/23/12 1 Chloroethane BDL 5.0 ug/l 8260B 09/23/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 09/23/12 1 Chloroform 17. 5.0 ug/l 8260B 09/23/12 1 Chloromethane BDL 2.5 ug/l 8260B 09/23/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 09/23/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 09/23/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 09/23/12 1 Dibromomethane BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 09/23/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 09/23/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 09/23/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 09/23/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 22 of 49

Reference 45 Page 187

Page 188: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-12 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : MW-13

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/18/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 09/23/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 09/23/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 09/23/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 09/23/12 1 Naphthalene BDL 5.0 ug/l 8260B 09/23/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Styrene BDL 1.0 ug/l 8260B 09/23/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 09/23/12 1 Tetrachloroethene BDL 1.0 ug/l 8260B 09/23/12 1 Toluene BDL 5.0 ug/l 8260B 09/23/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 Trichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 09/23/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 09/23/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 09/23/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 09/23/12 1

Surrogate Recovery Toluene-d8 107. % Rec. 8260B 09/23/12 1 Dibromofluoromethane 103. % Rec. 8260B 09/23/12 1 4-Bromofluorobenzene 108. % Rec. 8260B 09/23/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 09/25/12 14:50 Printed: 09/25/12 16:31

Page 23 of 49

Reference 45 Page 188

Page 189: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-13 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : MW-14

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/18/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 09/23/12 1 Acrolein BDL 50. ug/l 8260B 09/23/12 1 Acrylonitrile BDL 10. ug/l 8260B 09/23/12 1 Benzene BDL 1.0 ug/l 8260B 09/23/12 1 Bromobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 09/23/12 1 Bromoform BDL 1.0 ug/l 8260B 09/23/12 1 Bromomethane BDL 5.0 ug/l 8260B 09/23/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 09/23/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 09/23/12 1 Chloroethane BDL 5.0 ug/l 8260B 09/23/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 09/23/12 1 Chloroform BDL 5.0 ug/l 8260B 09/23/12 1 Chloromethane BDL 2.5 ug/l 8260B 09/23/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 09/23/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 09/23/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 09/23/12 1 Dibromomethane BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 09/23/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 cis-1,2-Dichloroethene 1.8 1.0 ug/l 8260B 09/23/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 09/23/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 09/23/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 09/23/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 24 of 49

Reference 45 Page 189

Page 190: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-13 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : MW-14

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/18/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 09/23/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 09/23/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 09/23/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 09/23/12 1 Naphthalene BDL 5.0 ug/l 8260B 09/23/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Styrene BDL 1.0 ug/l 8260B 09/23/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 09/23/12 1 Tetrachloroethene 44. 1.0 ug/l 8260B 09/23/12 1 Toluene BDL 5.0 ug/l 8260B 09/23/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,1,1-Trichloroethane 2.3 1.0 ug/l 8260B 09/23/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 Trichloroethene 53. 1.0 ug/l 8260B 09/23/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 09/23/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 09/23/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 09/23/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 09/23/12 1

Surrogate Recovery Toluene-d8 106. % Rec. 8260B 09/23/12 1 Dibromofluoromethane 104. % Rec. 8260B 09/23/12 1 4-Bromofluorobenzene 108. % Rec. 8260B 09/23/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 09/25/12 14:50 Printed: 09/25/12 16:31

Page 25 of 49

Reference 45 Page 190

Page 191: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-14 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : MW-15

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/18/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 09/24/12 1 Acrolein BDL 50. ug/l 8260B 09/24/12 1 Acrylonitrile BDL 10. ug/l 8260B 09/24/12 1 Benzene BDL 1.0 ug/l 8260B 09/24/12 1 Bromobenzene BDL 1.0 ug/l 8260B 09/24/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 09/24/12 1 Bromoform BDL 1.0 ug/l 8260B 09/24/12 1 Bromomethane BDL 5.0 ug/l 8260B 09/24/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 09/24/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 09/24/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 09/24/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 09/24/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 09/24/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 09/24/12 1 Chloroethane BDL 5.0 ug/l 8260B 09/24/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 09/24/12 1 Chloroform BDL 5.0 ug/l 8260B 09/24/12 1 Chloromethane BDL 2.5 ug/l 8260B 09/24/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 09/24/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 09/24/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 09/24/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 09/24/12 1 Dibromomethane BDL 1.0 ug/l 8260B 09/24/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 09/24/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 09/24/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 09/24/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 09/24/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 09/24/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 09/24/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 09/24/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 09/24/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 09/24/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 09/24/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 09/24/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 09/24/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/24/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/24/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 09/24/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 09/24/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 09/24/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 09/24/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 09/24/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 09/24/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 26 of 49

Reference 45 Page 191

Page 192: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-14 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : MW-15

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/18/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 09/24/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 09/24/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 09/24/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 09/24/12 1 Naphthalene BDL 5.0 ug/l 8260B 09/24/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 09/24/12 1 Styrene BDL 1.0 ug/l 8260B 09/24/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/24/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/24/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 09/24/12 1 Tetrachloroethene 150 1.0 ug/l 8260B 09/24/12 1 Toluene BDL 5.0 ug/l 8260B 09/24/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 09/24/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 09/24/12 1 1,1,1-Trichloroethane 3.6 1.0 ug/l 8260B 09/24/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 09/24/12 1 Trichloroethene 78. 1.0 ug/l 8260B 09/24/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 09/24/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 09/24/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 09/24/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 09/24/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 09/24/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 09/24/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 09/24/12 1

Surrogate Recovery Toluene-d8 97.6 % Rec. 8260B 09/24/12 1 Dibromofluoromethane 99.4 % Rec. 8260B 09/24/12 1 4-Bromofluorobenzene 101. % Rec. 8260B 09/24/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 09/25/12 14:50 Printed: 09/25/12 16:31

Page 27 of 49

Reference 45 Page 192

Page 193: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-15 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : MW-16

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/18/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 09/25/12 1 Acrolein BDL 50. ug/l 8260B 09/25/12 1 Acrylonitrile BDL 10. ug/l 8260B 09/25/12 1 Benzene BDL 1.0 ug/l 8260B 09/25/12 1 Bromobenzene BDL 1.0 ug/l 8260B 09/25/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 09/25/12 1 Bromoform BDL 1.0 ug/l 8260B 09/25/12 1 Bromomethane BDL 5.0 ug/l 8260B 09/25/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 09/25/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 09/25/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 09/25/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 09/25/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 09/25/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 09/25/12 1 Chloroethane BDL 5.0 ug/l 8260B 09/25/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 09/25/12 1 Chloroform BDL 5.0 ug/l 8260B 09/25/12 1 Chloromethane BDL 2.5 ug/l 8260B 09/25/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 09/25/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 09/25/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 09/25/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 09/25/12 1 Dibromomethane BDL 1.0 ug/l 8260B 09/25/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 09/25/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 09/25/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 09/25/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 09/25/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 09/25/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 09/25/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 09/25/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 09/25/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 09/25/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 09/25/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 09/25/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 09/25/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/25/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/25/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 09/25/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 09/25/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 09/25/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 09/25/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 09/25/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 09/25/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 28 of 49

Reference 45 Page 193

Page 194: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-15 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : MW-16

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/18/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 09/25/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 09/25/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 09/25/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 09/25/12 1 Naphthalene BDL 5.0 ug/l 8260B 09/25/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 09/25/12 1 Styrene BDL 1.0 ug/l 8260B 09/25/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/25/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/25/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 09/25/12 1 Tetrachloroethene 4.1 1.0 ug/l 8260B 09/25/12 1 Toluene BDL 5.0 ug/l 8260B 09/25/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 09/25/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 09/25/12 1 1,1,1-Trichloroethane 11. 1.0 ug/l 8260B 09/25/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 09/25/12 1 Trichloroethene 100 1.0 ug/l 8260B 09/25/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 09/25/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 09/25/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 09/25/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 09/25/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 09/25/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 09/25/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 09/25/12 1

Surrogate Recovery Toluene-d8 97.1 % Rec. 8260B 09/25/12 1 Dibromofluoromethane 102. % Rec. 8260B 09/25/12 1 4-Bromofluorobenzene 97.1 % Rec. 8260B 09/25/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 09/25/12 14:50 Printed: 09/25/12 16:31

Page 29 of 49

Reference 45 Page 194

Page 195: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-16 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : DUP

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/17/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 09/25/12 1 Acrolein BDL 50. ug/l 8260B 09/25/12 1 Acrylonitrile BDL 10. ug/l 8260B 09/25/12 1 Benzene BDL 1.0 ug/l 8260B 09/25/12 1 Bromobenzene BDL 1.0 ug/l 8260B 09/25/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 09/25/12 1 Bromoform BDL 1.0 ug/l 8260B 09/25/12 1 Bromomethane BDL 5.0 ug/l 8260B 09/25/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 09/25/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 09/25/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 09/25/12 1 Carbon tetrachloride 2.2 1.0 ug/l 8260B 09/25/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 09/25/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 09/25/12 1 Chloroethane BDL 5.0 ug/l 8260B 09/25/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 09/25/12 1 Chloroform 6.2 5.0 ug/l 8260B 09/25/12 1 Chloromethane BDL 2.5 ug/l 8260B 09/25/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 09/25/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 09/25/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 09/25/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 09/25/12 1 Dibromomethane BDL 1.0 ug/l 8260B 09/25/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 09/25/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 09/25/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 09/25/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 09/25/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 09/25/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 09/25/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 09/25/12 1 cis-1,2-Dichloroethene 1.2 1.0 ug/l 8260B 09/25/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 09/25/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 09/25/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 09/25/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 09/25/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/25/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/25/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 09/25/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 09/25/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 09/25/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 09/25/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 09/25/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 09/25/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 30 of 49

Reference 45 Page 195

Page 196: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-16 Date Received : September 19, 2012 Description : Component Machine

Site ID : Sample ID : DUP

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/17/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 09/25/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 09/25/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 09/25/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 09/25/12 1 Naphthalene BDL 5.0 ug/l 8260B 09/25/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 09/25/12 1 Styrene BDL 1.0 ug/l 8260B 09/25/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/25/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/25/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 09/25/12 1 Tetrachloroethene 9.4 1.0 ug/l 8260B 09/25/12 1 Toluene BDL 5.0 ug/l 8260B 09/25/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 09/25/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 09/25/12 1 1,1,1-Trichloroethane 2.6 1.0 ug/l 8260B 09/25/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 09/25/12 1 Trichloroethene 62. 1.0 ug/l 8260B 09/25/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 09/25/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 09/25/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 09/25/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 09/25/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 09/25/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 09/25/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 09/25/12 1

Surrogate Recovery Toluene-d8 99.1 % Rec. 8260B 09/25/12 1 Dibromofluoromethane 103. % Rec. 8260B 09/25/12 1 4-Bromofluorobenzene 95.2 % Rec. 8260B 09/25/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 09/25/12 14:50 Printed: 09/25/12 16:31

Page 31 of 49

Reference 45 Page 196

Page 197: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-17 Date Received : September 19, 2012 Description : Component Machine

Site ID : COMPONENT MACHINE Sample ID : TRIP BLANK

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/17/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 09/23/12 1 Acrolein BDL 50. ug/l 8260B 09/23/12 1 Acrylonitrile BDL 10. ug/l 8260B 09/23/12 1 Benzene BDL 1.0 ug/l 8260B 09/23/12 1 Bromobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 09/23/12 1 Bromoform BDL 1.0 ug/l 8260B 09/23/12 1 Bromomethane BDL 5.0 ug/l 8260B 09/23/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 09/23/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 09/23/12 1 Chloroethane BDL 5.0 ug/l 8260B 09/23/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 09/23/12 1 Chloroform BDL 5.0 ug/l 8260B 09/23/12 1 Chloromethane BDL 2.5 ug/l 8260B 09/23/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 09/23/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 09/23/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 09/23/12 1 Dibromomethane BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 09/23/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 09/23/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 09/23/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 09/23/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 09/23/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 09/23/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 32 of 49

Reference 45 Page 197

Page 198: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak September 25,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L595984-17 Date Received : September 19, 2012 Description : Component Machine

Site ID : COMPONENT MACHINE Sample ID : TRIP BLANK

Project # : 1024-1003-01 Collected By : W. Mileczak Collection Date : 09/17/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 09/23/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 09/23/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 09/23/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 09/23/12 1 Naphthalene BDL 5.0 ug/l 8260B 09/23/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Styrene BDL 1.0 ug/l 8260B 09/23/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 09/23/12 1 Tetrachloroethene BDL 1.0 ug/l 8260B 09/23/12 1 Toluene BDL 5.0 ug/l 8260B 09/23/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 09/23/12 1 Trichloroethene BDL 1.0 ug/l 8260B 09/23/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 09/23/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 09/23/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 09/23/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 09/23/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 09/23/12 1

Surrogate Recovery Toluene-d8 106. % Rec. 8260B 09/23/12 1 Dibromofluoromethane 102. % Rec. 8260B 09/23/12 1 4-Bromofluorobenzene 104. % Rec. 8260B 09/23/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 09/25/12 14:50 Printed: 09/25/12 16:31

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Attachment AList of Analytes with QC Qualifiers

Sample Work Sample Run Number Group Type Analyte ID Qualifier ________________ ___________ _______ ________________________________________ __________ __________

L595984-01 WG613527 SAMP 1,2-Dichlorobenzene R2360895 J4 L595984-02 WG613527 SAMP 2-Chloroethyl vinyl ether R2360895 J3

WG613527 SAMP 1,2-Dichlorobenzene R2360895 J4 L595984-05 WG613527 SAMP 1,2-Dichlorobenzene R2360895 J4 L595984-06 WG613527 SAMP 1,2-Dichlorobenzene R2360895 J4 L595984-07 WG613527 SAMP 1,2-Dichlorobenzene R2360895 J4 L595984-08 WG613527 SAMP 1,2-Dichlorobenzene R2360895 J4 L595984-09 WG613527 SAMP 1,2-Dichlorobenzene R2360895 J4 L595984-10 WG613527 SAMP 1,2-Dichlorobenzene R2360895 J4 L595984-11 WG613527 SAMP 1,2-Dichlorobenzene R2360895 J4 L595984-12 WG613527 SAMP 1,2-Dichlorobenzene R2360895 J4 L595984-13 WG613527 SAMP 1,2-Dichlorobenzene R2360895 J4 L595984-14 WG614424 SAMP Acetone R2362055 J4

WG614424 SAMP 2-Chloroethyl vinyl ether R2362055 J6J3 L595984-15 WG614424 SAMP Acetone R2362055 J4 L595984-16 WG614424 SAMP Acetone R2362055 J4 L595984-17 WG613527 SAMP 1,2-Dichlorobenzene R2360895 J4

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Attachment BExplanation of QC Qualifier Codes

Qualifier Meaning __________________ _______________________________________________________________________________

J3 The associated batch QC was outside the established quality control rangefor precision.

J4 The associated batch QC was outside the established quality control rangefor accuracy.

J6 The sample matrix interfered with the ability to make any accuratedetermination; spike value is low

Qualifier Report Information

ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program andas required by most certifying bodies including NELAC. In addition to the EPA qualifiers adoptedby ESC, we have implemented ESC qualifiers to provide more information pertaining to our analyticalresults. Each qualifier is designated in the qualifier explanation as either EPA or ESC.Data qualifiers are intended to provide the ESC client with more detailed information concerningthe potential bias of reported data. Because of the wide range of constituents and variety ofmatrices incorporated by most EPA methods,it is common for some compounds to fall outside ofestablished ranges. These exceptions are evaluated and all reported data is valid and useable"unless qualified as 'R' (Rejected)."

DefinitionsAccuracy - The relationship of the observed value of a known sample to the

true value of a known sample. Represented by percent recovery andrelevant to samples such as: control samples, matrix spike recoveries,surrogate recoveries, etc.

Precision - The agreement between a set of samples or between duplicate samples.Relates to how close together the results are and is represented byRelative Percent Differrence.

Surrogate - Organic compounds that are similar in chemical composition, extraction,and chromotography to analytes of interest. The surrogates are used todetermine the probable response of the group of analytes that are chem-ically related to the surrogate compound. Surrogates are added to thesample and carried through all stages of preparation and analyses.

TIC - Tentatively Identified Compound: Compounds detected in samples that arenot target compounds, internal standards, system monitoring compounds,or surrogates.

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Summary of Remarks For Samples Printed09/25/12 at 16:31:16

TSR Signing Reports: 364R5 - Desired TAT

Quarterly sampling, always log with QC4 per standing order from client.

Sample: L595984-01 Account: SEABREFIN Received: 09/19/12 09:00 Due Date: 09/26/12 00:00 RPT Date: 09/25/12 14:50 QC4Sample: L595984-02 Account: SEABREFIN Received: 09/19/12 09:00 Due Date: 09/26/12 00:00 RPT Date: 09/25/12 14:50 MS/MSD SampleSample: L595984-03 Account: SEABREFIN Received: 09/19/12 09:00 Due Date: 09/26/12 00:00 RPT Date: 09/25/12 14:50 MS/MSD SampleSample: L595984-04 Account: SEABREFIN Received: 09/19/12 09:00 Due Date: 09/26/12 00:00 RPT Date: 09/25/12 14:50 MS/MSD SampleSample: L595984-05 Account: SEABREFIN Received: 09/19/12 09:00 Due Date: 09/26/12 00:00 RPT Date: 09/25/12 14:50 QC4Sample: L595984-06 Account: SEABREFIN Received: 09/19/12 09:00 Due Date: 09/26/12 00:00 RPT Date: 09/25/12 14:50 QC4Sample: L595984-07 Account: SEABREFIN Received: 09/19/12 09:00 Due Date: 09/26/12 00:00 RPT Date: 09/25/12 14:50 QC4Sample: L595984-08 Account: SEABREFIN Received: 09/19/12 09:00 Due Date: 09/26/12 00:00 RPT Date: 09/25/12 14:50 QC4Sample: L595984-09 Account: SEABREFIN Received: 09/19/12 09:00 Due Date: 09/26/12 00:00 RPT Date: 09/25/12 14:50 QC4Sample: L595984-10 Account: SEABREFIN Received: 09/19/12 09:00 Due Date: 09/26/12 00:00 RPT Date: 09/25/12 14:50 QC4Sample: L595984-11 Account: SEABREFIN Received: 09/19/12 09:00 Due Date: 09/26/12 00:00 RPT Date: 09/25/12 14:50 QC4Sample: L595984-12 Account: SEABREFIN Received: 09/19/12 09:00 Due Date: 09/26/12 00:00 RPT Date: 09/25/12 14:50 QC4Sample: L595984-13 Account: SEABREFIN Received: 09/19/12 09:00 Due Date: 09/26/12 00:00 RPT Date: 09/25/12 14:50 QC4Sample: L595984-14 Account: SEABREFIN Received: 09/19/12 09:00 Due Date: 09/26/12 00:00 RPT Date: 09/25/12 14:50 QC4Sample: L595984-15 Account: SEABREFIN Received: 09/19/12 09:00 Due Date: 09/26/12 00:00 RPT Date: 09/25/12 14:50 QC4Sample: L595984-16 Account: SEABREFIN Received: 09/19/12 09:00 Due Date: 09/26/12 00:00 RPT Date: 09/25/12 14:50 QC4Sample: L595984-17 Account: SEABREFIN Received: 09/19/12 09:00 Due Date: 09/26/12 00:00 RPT Date: 09/25/12 14:50 QC4

Reference 45 Page 201

Page 202: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 September 25, 2012

L595984

Laboratory BlankAnalyte Result Units % Rec Limit Batch Date Analyzed

1,1,1,2-Tetrachloroethane < .001 mg/l WG613527 09/23/12 06:19 1,1,1-Trichloroethane < .001 mg/l WG613527 09/23/12 06:19 1,1,2,2-Tetrachloroethane < .001 mg/l WG613527 09/23/12 06:19 1,1,2-Trichloroethane < .001 mg/l WG613527 09/23/12 06:19 1,1,2-Trichlorotrifluoroethane < .001 mg/l WG613527 09/23/12 06:19 1,1-Dichloroethane < .001 mg/l WG613527 09/23/12 06:19 1,1-Dichloroethene < .001 mg/l WG613527 09/23/12 06:19 1,1-Dichloropropene < .001 mg/l WG613527 09/23/12 06:19 1,2,3-Trichlorobenzene < .001 mg/l WG613527 09/23/12 06:19 1,2,3-Trichloropropane < .001 mg/l WG613527 09/23/12 06:19 1,2,3-Trimethylbenzene < .001 mg/l WG613527 09/23/12 06:19 1,2,4-Trichlorobenzene < .001 mg/l WG613527 09/23/12 06:19 1,2,4-Trimethylbenzene < .001 mg/l WG613527 09/23/12 06:19 1,2-Dibromo-3-Chloropropane < .005 mg/l WG613527 09/23/12 06:19 1,2-Dibromoethane < .001 mg/l WG613527 09/23/12 06:19 1,2-Dichlorobenzene < .001 mg/l WG613527 09/23/12 06:19 1,2-Dichloroethane < .001 mg/l WG613527 09/23/12 06:19 1,2-Dichloropropane < .001 mg/l WG613527 09/23/12 06:19 1,3,5-Trimethylbenzene < .001 mg/l WG613527 09/23/12 06:19 1,3-Dichlorobenzene < .001 mg/l WG613527 09/23/12 06:19 1,3-Dichloropropane < .001 mg/l WG613527 09/23/12 06:19 1,4-Dichlorobenzene < .001 mg/l WG613527 09/23/12 06:19 2,2-Dichloropropane < .001 mg/l WG613527 09/23/12 06:19 2-Butanone (MEK) < .01 mg/l WG613527 09/23/12 06:19 2-Chloroethyl vinyl ether < .05 mg/l WG613527 09/23/12 06:19 2-Chlorotoluene < .001 mg/l WG613527 09/23/12 06:19 4-Chlorotoluene < .001 mg/l WG613527 09/23/12 06:19 4-Methyl-2-pentanone (MIBK) < .01 mg/l WG613527 09/23/12 06:19 Acetone < .05 mg/l WG613527 09/23/12 06:19 Acrolein < .025 mg/l WG613527 09/23/12 06:19 Acrylonitrile < .01 mg/l WG613527 09/23/12 06:19 Benzene < .001 mg/l WG613527 09/23/12 06:19 Bromobenzene < .001 mg/l WG613527 09/23/12 06:19 Bromodichloromethane < .001 mg/l WG613527 09/23/12 06:19 Bromoform < .001 mg/l WG613527 09/23/12 06:19 Bromomethane < .005 mg/l WG613527 09/23/12 06:19 Carbon tetrachloride < .001 mg/l WG613527 09/23/12 06:19 Chlorobenzene < .001 mg/l WG613527 09/23/12 06:19 Chlorodibromomethane < .001 mg/l WG613527 09/23/12 06:19 Chloroethane < .005 mg/l WG613527 09/23/12 06:19 Chloroform < .005 mg/l WG613527 09/23/12 06:19 Chloromethane < .0025 mg/l WG613527 09/23/12 06:19 cis-1,2-Dichloroethene < .001 mg/l WG613527 09/23/12 06:19 cis-1,3-Dichloropropene < .001 mg/l WG613527 09/23/12 06:19 Di-isopropyl ether < .001 mg/l WG613527 09/23/12 06:19 Dibromomethane < .001 mg/l WG613527 09/23/12 06:19 Dichlorodifluoromethane < .005 mg/l WG613527 09/23/12 06:19 Ethylbenzene < .001 mg/l WG613527 09/23/12 06:19 Hexachloro-1,3-butadiene < .001 mg/l WG613527 09/23/12 06:19 Isopropylbenzene < .001 mg/l WG613527 09/23/12 06:19 Methyl tert-butyl ether < .001 mg/l WG613527 09/23/12 06:19 Methylene Chloride < .005 mg/l WG613527 09/23/12 06:19 n-Butylbenzene < .001 mg/l WG613527 09/23/12 06:19 n-Propylbenzene < .001 mg/l WG613527 09/23/12 06:19 Naphthalene < .005 mg/l WG613527 09/23/12 06:19 p-Isopropyltoluene < .001 mg/l WG613527 09/23/12 06:19 sec-Butylbenzene < .001 mg/l WG613527 09/23/12 06:19 Styrene < .001 mg/l WG613527 09/23/12 06:19 tert-Butylbenzene < .001 mg/l WG613527 09/23/12 06:19

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

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12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 September 25, 2012

L595984

Laboratory BlankAnalyte Result Units % Rec Limit Batch Date Analyzed

Tetrachloroethene < .001 mg/l WG613527 09/23/12 06:19 Toluene < .005 mg/l WG613527 09/23/12 06:19 trans-1,2-Dichloroethene < .001 mg/l WG613527 09/23/12 06:19 trans-1,3-Dichloropropene < .001 mg/l WG613527 09/23/12 06:19 Trichloroethene < .001 mg/l WG613527 09/23/12 06:19 Trichlorofluoromethane < .005 mg/l WG613527 09/23/12 06:19 Vinyl chloride < .001 mg/l WG613527 09/23/12 06:19 Xylenes, Total < .003 mg/l WG613527 09/23/12 06:19 4-Bromofluorobenzene % Rec. 104.9 82-120 WG613527 09/23/12 06:19 Dibromofluoromethane % Rec. 102.3 82-126 WG613527 09/23/12 06:19 Toluene-d8 % Rec. 106.8 92-112 WG613527 09/23/12 06:19

1,1,1,2-Tetrachloroethane < .001 mg/l WG614424 09/24/12 22:49 1,1,1-Trichloroethane < .001 mg/l WG614424 09/24/12 22:49 1,1,2,2-Tetrachloroethane < .001 mg/l WG614424 09/24/12 22:49 1,1,2-Trichloroethane < .001 mg/l WG614424 09/24/12 22:49 1,1,2-Trichlorotrifluoroethane < .001 mg/l WG614424 09/24/12 22:49 1,1-Dichloroethane < .001 mg/l WG614424 09/24/12 22:49 1,1-Dichloroethene < .001 mg/l WG614424 09/24/12 22:49 1,1-Dichloropropene < .001 mg/l WG614424 09/24/12 22:49 1,2,3-Trichlorobenzene < .001 mg/l WG614424 09/24/12 22:49 1,2,3-Trichloropropane < .001 mg/l WG614424 09/24/12 22:49 1,2,3-Trimethylbenzene < .001 mg/l WG614424 09/24/12 22:49 1,2,4-Trichlorobenzene < .001 mg/l WG614424 09/24/12 22:49 1,2,4-Trimethylbenzene < .001 mg/l WG614424 09/24/12 22:49 1,2-Dibromo-3-Chloropropane < .005 mg/l WG614424 09/24/12 22:49 1,2-Dibromoethane < .001 mg/l WG614424 09/24/12 22:49 1,2-Dichlorobenzene < .001 mg/l WG614424 09/24/12 22:49 1,2-Dichloroethane < .001 mg/l WG614424 09/24/12 22:49 1,2-Dichloropropane < .001 mg/l WG614424 09/24/12 22:49 1,3,5-Trimethylbenzene < .001 mg/l WG614424 09/24/12 22:49 1,3-Dichlorobenzene < .001 mg/l WG614424 09/24/12 22:49 1,3-Dichloropropane < .001 mg/l WG614424 09/24/12 22:49 1,4-Dichlorobenzene < .001 mg/l WG614424 09/24/12 22:49 2,2-Dichloropropane < .001 mg/l WG614424 09/24/12 22:49 2-Butanone (MEK) < .01 mg/l WG614424 09/24/12 22:49 2-Chloroethyl vinyl ether < .05 mg/l WG614424 09/24/12 22:49 2-Chlorotoluene < .001 mg/l WG614424 09/24/12 22:49 4-Chlorotoluene < .001 mg/l WG614424 09/24/12 22:49 4-Methyl-2-pentanone (MIBK) < .01 mg/l WG614424 09/24/12 22:49 Acetone < .05 mg/l WG614424 09/24/12 22:49 Acrolein < .025 mg/l WG614424 09/24/12 22:49 Acrylonitrile < .01 mg/l WG614424 09/24/12 22:49 Benzene < .001 mg/l WG614424 09/24/12 22:49 Bromobenzene < .001 mg/l WG614424 09/24/12 22:49 Bromodichloromethane < .001 mg/l WG614424 09/24/12 22:49 Bromoform < .001 mg/l WG614424 09/24/12 22:49 Bromomethane < .005 mg/l WG614424 09/24/12 22:49 Carbon tetrachloride < .001 mg/l WG614424 09/24/12 22:49 Chlorobenzene < .001 mg/l WG614424 09/24/12 22:49 Chlorodibromomethane < .001 mg/l WG614424 09/24/12 22:49 Chloroethane < .005 mg/l WG614424 09/24/12 22:49 Chloroform < .005 mg/l WG614424 09/24/12 22:49 Chloromethane < .0025 mg/l WG614424 09/24/12 22:49 cis-1,2-Dichloroethene < .001 mg/l WG614424 09/24/12 22:49 cis-1,3-Dichloropropene < .001 mg/l WG614424 09/24/12 22:49 Di-isopropyl ether < .001 mg/l WG614424 09/24/12 22:49 Dibromomethane < .001 mg/l WG614424 09/24/12 22:49

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

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12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 September 25, 2012

L595984

Laboratory BlankAnalyte Result Units % Rec Limit Batch Date Analyzed

Dichlorodifluoromethane < .005 mg/l WG614424 09/24/12 22:49 Ethylbenzene < .001 mg/l WG614424 09/24/12 22:49 Hexachloro-1,3-butadiene < .001 mg/l WG614424 09/24/12 22:49 Isopropylbenzene < .001 mg/l WG614424 09/24/12 22:49 Methyl tert-butyl ether < .001 mg/l WG614424 09/24/12 22:49 Methylene Chloride < .005 mg/l WG614424 09/24/12 22:49 n-Butylbenzene < .001 mg/l WG614424 09/24/12 22:49 n-Propylbenzene < .001 mg/l WG614424 09/24/12 22:49 Naphthalene < .005 mg/l WG614424 09/24/12 22:49 p-Isopropyltoluene < .001 mg/l WG614424 09/24/12 22:49 sec-Butylbenzene < .001 mg/l WG614424 09/24/12 22:49 Styrene < .001 mg/l WG614424 09/24/12 22:49 tert-Butylbenzene < .001 mg/l WG614424 09/24/12 22:49 Tetrachloroethene < .001 mg/l WG614424 09/24/12 22:49 Toluene < .005 mg/l WG614424 09/24/12 22:49 trans-1,2-Dichloroethene < .001 mg/l WG614424 09/24/12 22:49 trans-1,3-Dichloropropene < .001 mg/l WG614424 09/24/12 22:49 Trichloroethene < .001 mg/l WG614424 09/24/12 22:49 Trichlorofluoromethane < .005 mg/l WG614424 09/24/12 22:49 Vinyl chloride < .001 mg/l WG614424 09/24/12 22:49 Xylenes, Total < .003 mg/l WG614424 09/24/12 22:49 4-Bromofluorobenzene % Rec. 98.57 82-120 WG614424 09/24/12 22:49 Dibromofluoromethane % Rec. 97.96 82-126 WG614424 09/24/12 22:49 Toluene-d8 % Rec. 101.7 92-112 WG614424 09/24/12 22:49

Laboratory Control SampleAnalyte Units Known Val Result % Rec Limit Batch

1,1,1,2-Tetrachloroethane mg/l .025 0.0221 88.4 77-128 WG613527 1,1,1-Trichloroethane mg/l .025 0.0222 88.9 71-126 WG613527 1,1,2,2-Tetrachloroethane mg/l .025 0.0225 89.9 78-130 WG613527 1,1,2-Trichloroethane mg/l .025 0.0237 94.7 81-121 WG613527 1,1,2-Trichlorotrifluoroethane mg/l .025 0.0222 88.9 53-143 WG613527 1,1-Dichloroethane mg/l .025 0.0230 92.2 73-123 WG613527 1,1-Dichloroethene mg/l .025 0.0205 82.1 54-134 WG613527 1,1-Dichloropropene mg/l .025 0.0220 88.0 67-127 WG613527 1,2,3-Trichlorobenzene mg/l .025 0.0195 78.0 77-130 WG613527 1,2,3-Trichloropropane mg/l .025 0.0218 87.2 68-130 WG613527 1,2,3-Trimethylbenzene mg/l .025 0.0214 85.5 77-126 WG613527 1,2,4-Trichlorobenzene mg/l .025 0.0213 85.1 76-127 WG613527 1,2,4-Trimethylbenzene mg/l .025 0.0219 87.6 77-129 WG613527 1,2-Dibromo-3-Chloropropane mg/l .025 0.0212 84.8 55-142 WG613527 1,2-Dibromoethane mg/l .025 0.0228 91.2 78-124 WG613527 1,2-Dichlorobenzene mg/l .025 0.0224 89.5 82-121 WG613527 1,2-Dichloroethane mg/l .025 0.0233 93.1 69-128 WG613527 1,2-Dichloropropane mg/l .025 0.0239 95.5 77-121 WG613527 1,3,5-Trimethylbenzene mg/l .025 0.0218 87.1 78-127 WG613527 1,3-Dichlorobenzene mg/l .025 0.0225 90.1 77-127 WG613527 1,3-Dichloropropane mg/l .025 0.0222 88.7 78-117 WG613527 1,4-Dichlorobenzene mg/l .025 0.0216 86.5 79-117 WG613527 2,2-Dichloropropane mg/l .025 0.0214 85.5 63-130 WG613527 2-Butanone (MEK) mg/l .125 0.146 117. 58-144 WG613527 2-Chloroethyl vinyl ether mg/l .125 0.0976 78.1 26-172 WG613527 2-Chlorotoluene mg/l .025 0.0223 89.0 78-123 WG613527 4-Chlorotoluene mg/l .025 0.0225 89.8 78-122 WG613527 4-Methyl-2-pentanone (MIBK) mg/l .125 0.123 98.7 58-147 WG613527 Acetone mg/l .125 0.172 138. 49-153 WG613527 Acrolein mg/l .125 0.109 86.9 10-181 WG613527 Acrylonitrile mg/l .125 0.118 94.2 53-153 WG613527

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 38 of 49

Reference 45 Page 204

Page 205: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 September 25, 2012

L595984

Laboratory Control SampleAnalyte Units Known Val Result % Rec Limit Batch

Benzene mg/l .025 0.0231 92.4 72-119 WG613527 Bromobenzene mg/l .025 0.0230 91.8 76-121 WG613527 Bromodichloromethane mg/l .025 0.0238 95.2 75-127 WG613527 Bromoform mg/l .025 0.0231 92.4 61-136 WG613527 Bromomethane mg/l .025 0.0212 84.7 42-172 WG613527 Carbon tetrachloride mg/l .025 0.0210 84.1 63-129 WG613527 Chlorobenzene mg/l .025 0.0228 91.1 78-123 WG613527 Chlorodibromomethane mg/l .025 0.0233 93.2 73-128 WG613527 Chloroethane mg/l .025 0.0218 87.4 52-164 WG613527 Chloroform mg/l .025 0.0239 95.7 76-122 WG613527 Chloromethane mg/l .025 0.0211 84.3 50-141 WG613527 cis-1,2-Dichloroethene mg/l .025 0.0226 90.4 75-121 WG613527 cis-1,3-Dichloropropene mg/l .025 0.0240 96.1 74-124 WG613527 Di-isopropyl ether mg/l .025 0.0238 95.2 66-129 WG613527 Dibromomethane mg/l .025 0.0240 96.1 77-124 WG613527 Dichlorodifluoromethane mg/l .025 0.0204 81.7 33-173 WG613527 Ethylbenzene mg/l .025 0.0219 87.5 77-124 WG613527 Hexachloro-1,3-butadiene mg/l .025 0.0213 85.1 71-134 WG613527 Isopropylbenzene mg/l .025 0.0230 92.0 74-126 WG613527 Methyl tert-butyl ether mg/l .025 0.0221 88.4 67-127 WG613527 Methylene Chloride mg/l .025 0.0216 86.3 67-122 WG613527 n-Butylbenzene mg/l .025 0.0214 85.5 74-130 WG613527 n-Propylbenzene mg/l .025 0.0225 90.0 77-125 WG613527 Naphthalene mg/l .025 0.0202 80.7 70-134 WG613527 p-Isopropyltoluene mg/l .025 0.0221 88.4 77-132 WG613527 sec-Butylbenzene mg/l .025 0.0218 87.3 77-130 WG613527 Styrene mg/l .025 0.0226 90.3 69-145 WG613527 tert-Butylbenzene mg/l .025 0.0222 88.9 76-131 WG613527 Tetrachloroethene mg/l .025 0.0210 84.0 69-131 WG613527 Toluene mg/l .025 0.0232 93.0 75-114 WG613527 trans-1,2-Dichloroethene mg/l .025 0.0213 85.3 63-127 WG613527 trans-1,3-Dichloropropene mg/l .025 0.0238 95.1 69-124 WG613527 Trichloroethene mg/l .025 0.0229 91.6 69-131 WG613527 Trichlorofluoromethane mg/l .025 0.0212 84.9 53-161 WG613527 Vinyl chloride mg/l .025 0.0198 79.1 55-142 WG613527 Xylenes, Total mg/l .075 0.0657 87.7 77-123 WG613527 4-Bromofluorobenzene 105.6 82-120 WG613527 Dibromofluoromethane 102.4 82-126 WG613527 Toluene-d8 106.7 92-112 WG613527

1,1,1,2-Tetrachloroethane mg/l .025 0.0256 102. 77-128 WG614424 1,1,1-Trichloroethane mg/l .025 0.0242 96.8 71-126 WG614424 1,1,2,2-Tetrachloroethane mg/l .025 0.0276 110. 78-130 WG614424 1,1,2-Trichloroethane mg/l .025 0.0268 107. 81-121 WG614424 1,1,2-Trichlorotrifluoroethane mg/l .025 0.0259 104. 53-143 WG614424 1,1-Dichloroethane mg/l .025 0.0252 101. 73-123 WG614424 1,1-Dichloroethene mg/l .025 0.0269 108. 54-134 WG614424 1,1-Dichloropropene mg/l .025 0.0249 99.4 67-127 WG614424 1,2,3-Trichlorobenzene mg/l .025 0.0258 103. 77-130 WG614424 1,2,3-Trichloropropane mg/l .025 0.0253 101. 68-130 WG614424 1,2,3-Trimethylbenzene mg/l .025 0.0235 94.2 77-126 WG614424 1,2,4-Trichlorobenzene mg/l .025 0.0265 106. 76-127 WG614424 1,2,4-Trimethylbenzene mg/l .025 0.0250 99.9 77-129 WG614424 1,2-Dibromo-3-Chloropropane mg/l .025 0.0258 103. 55-142 WG614424 1,2-Dibromoethane mg/l .025 0.0259 104. 78-124 WG614424 1,2-Dichlorobenzene mg/l .025 0.0253 101. 82-121 WG614424 1,2-Dichloroethane mg/l .025 0.0247 98.6 69-128 WG614424 1,2-Dichloropropane mg/l .025 0.0249 99.7 77-121 WG614424

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 39 of 49

Reference 45 Page 205

Page 206: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 September 25, 2012

L595984

Laboratory Control SampleAnalyte Units Known Val Result % Rec Limit Batch

1,3,5-Trimethylbenzene mg/l .025 0.0252 101. 78-127 WG614424 1,3-Dichlorobenzene mg/l .025 0.0255 102. 77-127 WG614424 1,3-Dichloropropane mg/l .025 0.0263 105. 78-117 WG614424 1,4-Dichlorobenzene mg/l .025 0.0247 98.7 79-117 WG614424 2,2-Dichloropropane mg/l .025 0.0214 85.7 63-130 WG614424 2-Butanone (MEK) mg/l .125 0.166 133. 58-144 WG614424 2-Chloroethyl vinyl ether mg/l .125 0.131 105. 26-172 WG614424 2-Chlorotoluene mg/l .025 0.0253 101. 78-123 WG614424 4-Chlorotoluene mg/l .025 0.0248 99.3 78-122 WG614424 4-Methyl-2-pentanone (MIBK) mg/l .125 0.134 107. 58-147 WG614424 Acetone mg/l .125 0.199 159.* 49-153 WG614424 Acrolein mg/l .125 0.0990 79.2 10-181 WG614424 Acrylonitrile mg/l .125 0.138 111. 53-153 WG614424 Benzene mg/l .025 0.0250 100. 72-119 WG614424 Bromobenzene mg/l .025 0.0245 98.0 76-121 WG614424 Bromodichloromethane mg/l .025 0.0235 94.0 75-127 WG614424 Bromoform mg/l .025 0.0257 103. 61-136 WG614424 Bromomethane mg/l .025 0.0296 118. 42-172 WG614424 Carbon tetrachloride mg/l .025 0.0258 103. 63-129 WG614424 Chlorobenzene mg/l .025 0.0258 103. 78-123 WG614424 Chlorodibromomethane mg/l .025 0.0263 105. 73-128 WG614424 Chloroethane mg/l .025 0.0263 105. 52-164 WG614424 Chloroform mg/l .025 0.0256 102. 76-122 WG614424 Chloromethane mg/l .025 0.0222 88.9 50-141 WG614424 cis-1,2-Dichloroethene mg/l .025 0.0243 97.3 75-121 WG614424 cis-1,3-Dichloropropene mg/l .025 0.0247 98.8 74-124 WG614424 Di-isopropyl ether mg/l .025 0.0248 99.2 66-129 WG614424 Dibromomethane mg/l .025 0.0249 99.7 77-124 WG614424 Dichlorodifluoromethane mg/l .025 0.0225 90.0 33-173 WG614424 Ethylbenzene mg/l .025 0.0250 99.9 77-124 WG614424 Hexachloro-1,3-butadiene mg/l .025 0.0246 98.3 71-134 WG614424 Isopropylbenzene mg/l .025 0.0261 105. 74-126 WG614424 Methyl tert-butyl ether mg/l .025 0.0261 104. 67-127 WG614424 Methylene Chloride mg/l .025 0.0267 107. 67-122 WG614424 n-Butylbenzene mg/l .025 0.0249 99.8 74-130 WG614424 n-Propylbenzene mg/l .025 0.0253 101. 77-125 WG614424 Naphthalene mg/l .025 0.0256 102. 70-134 WG614424 p-Isopropyltoluene mg/l .025 0.0255 102. 77-132 WG614424 sec-Butylbenzene mg/l .025 0.0258 103. 77-130 WG614424 Styrene mg/l .025 0.0246 98.4 69-145 WG614424 tert-Butylbenzene mg/l .025 0.0256 102. 76-131 WG614424 Tetrachloroethene mg/l .025 0.0261 104. 69-131 WG614424 Toluene mg/l .025 0.0254 101. 75-114 WG614424 trans-1,2-Dichloroethene mg/l .025 0.0253 101. 63-127 WG614424 trans-1,3-Dichloropropene mg/l .025 0.0245 98.1 69-124 WG614424 Trichloroethene mg/l .025 0.0258 103. 69-131 WG614424 Trichlorofluoromethane mg/l .025 0.0252 101. 53-161 WG614424 Vinyl chloride mg/l .025 0.0227 90.7 55-142 WG614424 Xylenes, Total mg/l .075 0.0766 102. 77-123 WG614424 4-Bromofluorobenzene 97.48 82-120 WG614424 Dibromofluoromethane 100.6 82-126 WG614424 Toluene-d8 99.07 92-112 WG614424

Laboratory Control Sample DuplicateAnalyte Units Result Ref %Rec Limit RPD Limit Batch

1,1,1,2-Tetrachloroethane mg/l 0.0208 0.0221 83.0 77-128 6.27 20 WG613527 1,1,1-Trichloroethane mg/l 0.0194 0.0222 78.0 71-126 13.7 20 WG613527 1,1,2,2-Tetrachloroethane mg/l 0.0208 0.0225 83.0 78-130 7.50 20 WG613527

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 40 of 49

Reference 45 Page 206

Page 207: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 September 25, 2012

L595984

Laboratory Control Sample DuplicateAnalyte Units Result Ref %Rec Limit RPD Limit Batch

1,1,2-Trichloroethane mg/l 0.0213 0.0237 85.0 81-121 10.4 20 WG613527 1,1,2-Trichlorotrifluoroethane mg/l 0.0191 0.0222 76.0 53-143 15.0 20 WG613527 1,1-Dichloroethane mg/l 0.0210 0.0230 84.0 73-123 9.49 20 WG613527 1,1-Dichloroethene mg/l 0.0190 0.0205 76.0 54-134 7.53 20 WG613527 1,1-Dichloropropene mg/l 0.0198 0.0220 79.0 67-127 10.4 20 WG613527 1,2,3-Trichlorobenzene mg/l 0.0193 0.0195 77.0 77-130 1.01 20 WG613527 1,2,3-Trichloropropane mg/l 0.0212 0.0218 85.0 68-130 2.94 20 WG613527 1,2,3-Trimethylbenzene mg/l 0.0197 0.0214 79.0 77-126 8.32 20 WG613527 1,2,4-Trichlorobenzene mg/l 0.0200 0.0213 80.0 76-127 6.11 20 WG613527 1,2,4-Trimethylbenzene mg/l 0.0202 0.0219 81.0 77-129 8.19 20 WG613527 1,2-Dibromo-3-Chloropropane mg/l 0.0204 0.0212 81.0 55-142 3.97 20 WG613527 1,2-Dibromoethane mg/l 0.0217 0.0228 87.0 78-124 4.91 20 WG613527 1,2-Dichlorobenzene mg/l 0.0205 0.0224 82.0 82-121 8.84 20 WG613527 1,2-Dichloroethane mg/l 0.0211 0.0233 84.0 69-128 9.92 20 WG613527 1,2-Dichloropropane mg/l 0.0223 0.0239 89.0 77-121 6.87 20 WG613527 1,3,5-Trimethylbenzene mg/l 0.0201 0.0218 80.0 78-127 7.94 20 WG613527 1,3-Dichlorobenzene mg/l 0.0208 0.0225 83.0 77-127 8.03 20 WG613527 1,3-Dichloropropane mg/l 0.0211 0.0222 84.0 78-117 4.76 20 WG613527 1,4-Dichlorobenzene mg/l 0.0199 0.0216 79.0 79-117 8.56 20 WG613527 2,2-Dichloropropane mg/l 0.0185 0.0214 74.0 63-130 14.4 20 WG613527 2-Butanone (MEK) mg/l 0.139 0.146 111. 58-144 5.25 20 WG613527 2-Chloroethyl vinyl ether mg/l 0.0965 0.0976 77.0 26-172 1.12 22 WG613527 2-Chlorotoluene mg/l 0.0202 0.0223 81.0 78-123 9.53 20 WG613527 4-Chlorotoluene mg/l 0.0206 0.0225 82.0 78-122 8.62 20 WG613527 4-Methyl-2-pentanone (MIBK) mg/l 0.114 0.123 91.0 58-147 7.68 20 WG613527 Acetone mg/l 0.169 0.172 135. 49-153 1.83 21 WG613527 Acrolein mg/l 0.101 0.109 81.0 10-181 7.09 30 WG613527 Acrylonitrile mg/l 0.111 0.118 89.0 53-153 5.51 20 WG613527 Benzene mg/l 0.0208 0.0231 83.0 72-119 10.3 20 WG613527 Bromobenzene mg/l 0.0208 0.0230 83.0 76-121 10.0 20 WG613527 Bromodichloromethane mg/l 0.0216 0.0238 86.0 75-127 9.82 20 WG613527 Bromoform mg/l 0.0216 0.0231 86.0 61-136 6.77 20 WG613527 Bromomethane mg/l 0.0179 0.0212 72.0 42-172 16.5 20 WG613527 Carbon tetrachloride mg/l 0.0186 0.0210 74.0 63-129 12.1 20 WG613527 Chlorobenzene mg/l 0.0212 0.0228 85.0 78-123 7.12 20 WG613527 Chlorodibromomethane mg/l 0.0216 0.0233 86.0 73-128 7.62 20 WG613527 Chloroethane mg/l 0.0194 0.0218 77.0 52-164 12.1 20 WG613527 Chloroform mg/l 0.0213 0.0239 85.0 76-122 11.4 20 WG613527 Chloromethane mg/l 0.0190 0.0211 76.0 50-141 10.1 20 WG613527 cis-1,2-Dichloroethene mg/l 0.0207 0.0226 83.0 75-121 8.69 20 WG613527 cis-1,3-Dichloropropene mg/l 0.0216 0.0240 86.0 74-124 10.6 20 WG613527 Di-isopropyl ether mg/l 0.0219 0.0238 87.0 66-129 8.54 20 WG613527 Dibromomethane mg/l 0.0213 0.0240 85.0 77-124 12.0 20 WG613527 Dichlorodifluoromethane mg/l 0.0174 0.0204 69.0 33-173 16.2 20 WG613527 Ethylbenzene mg/l 0.0202 0.0219 81.0 77-124 7.96 20 WG613527 Hexachloro-1,3-butadiene mg/l 0.0191 0.0213 76.0 71-134 10.6 20 WG613527 Isopropylbenzene mg/l 0.0208 0.0230 83.0 74-126 9.84 20 WG613527 Methyl tert-butyl ether mg/l 0.0204 0.0221 82.0 67-127 8.08 20 WG613527 Methylene Chloride mg/l 0.0197 0.0216 79.0 67-122 9.03 20 WG613527 n-Butylbenzene mg/l 0.0196 0.0214 78.0 74-130 8.76 20 WG613527 n-Propylbenzene mg/l 0.0207 0.0225 83.0 77-125 8.49 20 WG613527 Naphthalene mg/l 0.0192 0.0202 77.0 70-134 4.99 20 WG613527 p-Isopropyltoluene mg/l 0.0202 0.0221 81.0 77-132 9.19 20 WG613527 sec-Butylbenzene mg/l 0.0199 0.0218 80.0 77-130 9.14 20 WG613527 Styrene mg/l 0.0206 0.0226 82.0 69-145 9.17 20 WG613527 tert-Butylbenzene mg/l 0.0202 0.0222 81.0 76-131 9.46 20 WG613527 Tetrachloroethene mg/l 0.0189 0.0210 76.0 69-131 10.5 20 WG613527 Toluene mg/l 0.0210 0.0232 84.0 75-114 10.2 20 WG613527 trans-1,2-Dichloroethene mg/l 0.0195 0.0213 78.0 63-127 9.12 20 WG613527

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 41 of 49

Reference 45 Page 207

Page 208: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 September 25, 2012

L595984

Laboratory Control Sample DuplicateAnalyte Units Result Ref %Rec Limit RPD Limit Batch

trans-1,3-Dichloropropene mg/l 0.0221 0.0238 88.0 69-124 7.32 20 WG613527 Trichloroethene mg/l 0.0204 0.0229 82.0 69-131 11.4 20 WG613527 Trichlorofluoromethane mg/l 0.0185 0.0212 74.0 53-161 13.6 20 WG613527 Vinyl chloride mg/l 0.0183 0.0198 73.0 55-142 7.91 20 WG613527 Xylenes, Total mg/l 0.0615 0.0657 82.0 77-123 6.63 20 WG613527 4-Bromofluorobenzene 106.4 82-120 WG613527 Dibromofluoromethane 102.3 82-126 WG613527 Toluene-d8 106.2 92-112 WG613527

1,1,1,2-Tetrachloroethane mg/l 0.0250 0.0256 100. 77-128 2.43 20 WG614424 1,1,1-Trichloroethane mg/l 0.0236 0.0242 94.0 71-126 2.63 20 WG614424 1,1,2,2-Tetrachloroethane mg/l 0.0269 0.0276 107. 78-130 2.62 20 WG614424 1,1,2-Trichloroethane mg/l 0.0266 0.0268 106. 81-121 0.910 20 WG614424 1,1,2-Trichlorotrifluoroethane mg/l 0.0252 0.0259 101. 53-143 3.06 20 WG614424 1,1-Dichloroethane mg/l 0.0243 0.0252 97.0 73-123 3.90 20 WG614424 1,1-Dichloroethene mg/l 0.0269 0.0269 108. 54-134 0.0900 20 WG614424 1,1-Dichloropropene mg/l 0.0237 0.0249 95.0 67-127 4.98 20 WG614424 1,2,3-Trichlorobenzene mg/l 0.0250 0.0258 100. 77-130 3.18 20 WG614424 1,2,3-Trichloropropane mg/l 0.0254 0.0253 102. 68-130 0.560 20 WG614424 1,2,3-Trimethylbenzene mg/l 0.0235 0.0235 94.0 77-126 0 20 WG614424 1,2,4-Trichlorobenzene mg/l 0.0255 0.0265 102. 76-127 3.88 20 WG614424 1,2,4-Trimethylbenzene mg/l 0.0243 0.0250 97.0 77-129 2.68 20 WG614424 1,2-Dibromo-3-Chloropropane mg/l 0.0249 0.0258 99.0 55-142 3.54 20 WG614424 1,2-Dibromoethane mg/l 0.0265 0.0259 106. 78-124 2.21 20 WG614424 1,2-Dichlorobenzene mg/l 0.0250 0.0253 100. 82-121 1.56 20 WG614424 1,2-Dichloroethane mg/l 0.0239 0.0247 96.0 69-128 3.20 20 WG614424 1,2-Dichloropropane mg/l 0.0246 0.0249 98.0 77-121 1.08 20 WG614424 1,3,5-Trimethylbenzene mg/l 0.0246 0.0252 98.0 78-127 2.24 20 WG614424 1,3-Dichlorobenzene mg/l 0.0251 0.0255 100. 77-127 1.61 20 WG614424 1,3-Dichloropropane mg/l 0.0263 0.0263 105. 78-117 0.220 20 WG614424 1,4-Dichlorobenzene mg/l 0.0245 0.0247 98.0 79-117 0.490 20 WG614424 2,2-Dichloropropane mg/l 0.0216 0.0214 86.0 63-130 0.750 20 WG614424 2-Butanone (MEK) mg/l 0.164 0.166 131. 58-144 1.16 20 WG614424 2-Chloroethyl vinyl ether mg/l 0.134 0.131 107. 26-172 2.51 22 WG614424 2-Chlorotoluene mg/l 0.0249 0.0253 99.0 78-123 1.79 20 WG614424 4-Chlorotoluene mg/l 0.0248 0.0248 99.0 78-122 0.0900 20 WG614424 4-Methyl-2-pentanone (MIBK) mg/l 0.135 0.134 108. 58-147 0.890 20 WG614424 Acetone mg/l 0.194 0.199 155* 49-153 2.33 21 WG614424 Acrolein mg/l 0.0988 0.0990 79.0 10-181 0.210 30 WG614424 Acrylonitrile mg/l 0.134 0.138 107. 53-153 3.17 20 WG614424 Benzene mg/l 0.0243 0.0250 97.0 72-119 2.79 20 WG614424 Bromobenzene mg/l 0.0246 0.0245 98.0 76-121 0.430 20 WG614424 Bromodichloromethane mg/l 0.0234 0.0235 94.0 75-127 0.170 20 WG614424 Bromoform mg/l 0.0256 0.0257 102. 61-136 0.270 20 WG614424 Bromomethane mg/l 0.0290 0.0296 116. 42-172 1.99 20 WG614424 Carbon tetrachloride mg/l 0.0245 0.0258 98.0 63-129 5.18 20 WG614424 Chlorobenzene mg/l 0.0258 0.0258 103. 78-123 0.270 20 WG614424 Chlorodibromomethane mg/l 0.0259 0.0263 103. 73-128 1.50 20 WG614424 Chloroethane mg/l 0.0252 0.0263 101. 52-164 4.41 20 WG614424 Chloroform mg/l 0.0246 0.0256 98.0 76-122 3.87 20 WG614424 Chloromethane mg/l 0.0212 0.0222 85.0 50-141 4.57 20 WG614424 cis-1,2-Dichloroethene mg/l 0.0237 0.0243 95.0 75-121 2.44 20 WG614424 cis-1,3-Dichloropropene mg/l 0.0243 0.0247 97.0 74-124 1.55 20 WG614424 Di-isopropyl ether mg/l 0.0234 0.0248 94.0 66-129 5.67 20 WG614424 Dibromomethane mg/l 0.0242 0.0249 97.0 77-124 2.79 20 WG614424 Dichlorodifluoromethane mg/l 0.0208 0.0225 83.0 33-173 8.04 20 WG614424 Ethylbenzene mg/l 0.0253 0.0250 101. 77-124 1.38 20 WG614424 Hexachloro-1,3-butadiene mg/l 0.0243 0.0246 97.0 71-134 1.03 20 WG614424

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 42 of 49

Reference 45 Page 208

Page 209: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 September 25, 2012

L595984

Laboratory Control Sample DuplicateAnalyte Units Result Ref %Rec Limit RPD Limit Batch

Isopropylbenzene mg/l 0.0257 0.0261 103. 74-126 1.48 20 WG614424 Methyl tert-butyl ether mg/l 0.0249 0.0261 100. 67-127 4.62 20 WG614424 Methylene Chloride mg/l 0.0256 0.0267 102. 67-122 4.15 20 WG614424 n-Butylbenzene mg/l 0.0247 0.0249 99.0 74-130 0.880 20 WG614424 n-Propylbenzene mg/l 0.0250 0.0253 100. 77-125 1.46 20 WG614424 Naphthalene mg/l 0.0244 0.0256 98.0 70-134 4.76 20 WG614424 p-Isopropyltoluene mg/l 0.0250 0.0255 100. 77-132 1.99 20 WG614424 sec-Butylbenzene mg/l 0.0255 0.0258 102. 77-130 1.12 20 WG614424 Styrene mg/l 0.0246 0.0246 98.0 69-145 0.0500 20 WG614424 tert-Butylbenzene mg/l 0.0252 0.0256 101. 76-131 1.44 20 WG614424 Tetrachloroethene mg/l 0.0255 0.0261 102. 69-131 2.18 20 WG614424 Toluene mg/l 0.0252 0.0254 101. 75-114 0.750 20 WG614424 trans-1,2-Dichloroethene mg/l 0.0238 0.0253 95.0 63-127 5.86 20 WG614424 trans-1,3-Dichloropropene mg/l 0.0241 0.0245 96.0 69-124 1.83 20 WG614424 Trichloroethene mg/l 0.0250 0.0258 100. 69-131 3.02 20 WG614424 Trichlorofluoromethane mg/l 0.0242 0.0252 97.0 53-161 3.78 20 WG614424 Vinyl chloride mg/l 0.0213 0.0227 85.0 55-142 6.14 20 WG614424 Xylenes, Total mg/l 0.0761 0.0766 102. 77-123 0.630 20 WG614424 4-Bromofluorobenzene 96.59 82-120 WG614424 Dibromofluoromethane 96.86 82-126 WG614424 Toluene-d8 100.7 92-112 WG614424

Matrix SpikeAnalyte Units MS Res Ref Res TV % Rec Limit Ref Samp Batch

1,1,1,2-Tetrachloroethane mg/l 0.0220 0 .025 88.1 71-130 L595984-02 WG613527 1,1,1-Trichloroethane mg/l 0.0213 0 .025 85.3 58-137 L595984-02 WG613527 1,1,2,2-Tetrachloroethane mg/l 0.0209 0 .025 83.5 64-149 L595984-02 WG613527 1,1,2-Trichloroethane mg/l 0.0203 0 .025 81.4 73-128 L595984-02 WG613527 1,1,2-Trichlorotrifluoroethane mg/l 0.0211 0 .025 84.4 36-159 L595984-02 WG613527 1,1-Dichloroethane mg/l 0.0208 0 .025 83.2 58-133 L595984-02 WG613527 1,1-Dichloroethene mg/l 0.0189 0 .025 75.4 32-152 L595984-02 WG613527 1,1-Dichloropropene mg/l 0.0200 0 .025 80.2 50-140 L595984-02 WG613527 1,2,3-Trichlorobenzene mg/l 0.0200 0 .025 80.0 68-135 L595984-02 WG613527 1,2,3-Trichloropropane mg/l 0.0188 0 .025 75.4 74-137 L595984-02 WG613527 1,2,3-Trimethylbenzene mg/l 0.0202 0 .025 80.8 67-133 L595984-02 WG613527 1,2,4-Trichlorobenzene mg/l 0.0218 0 .025 87.0 67-133 L595984-02 WG613527 1,2,4-Trimethylbenzene mg/l 0.0212 0 .025 84.8 62-141 L595984-02 WG613527 1,2-Dibromo-3-Chloropropane mg/l 0.0205 0 .025 82.2 55-148 L595984-02 WG613527 1,2-Dibromoethane mg/l 0.0199 0 .025 79.6 71-129 L595984-02 WG613527 1,2-Dichlorobenzene mg/l 0.0209 0 .025 83.5 75-125 L595984-02 WG613527 1,2-Dichloroethane mg/l 0.0196 0 .025 78.3 59-135 L595984-02 WG613527 1,2-Dichloropropane mg/l 0.0213 0 .025 85.2 68-126 L595984-02 WG613527 1,3,5-Trimethylbenzene mg/l 0.0216 0 .025 86.6 67-136 L595984-02 WG613527 1,3-Dichlorobenzene mg/l 0.0214 0 .025 85.4 69-131 L595984-02 WG613527 1,3-Dichloropropane mg/l 0.0202 0 .025 80.8 70-122 L595984-02 WG613527 1,4-Dichlorobenzene mg/l 0.0205 0 .025 81.9 70-123 L595984-02 WG613527 2,2-Dichloropropane mg/l 0.0211 0 .025 84.4 51-141 L595984-02 WG613527 2-Butanone (MEK) mg/l 0.103 0 .125 82.6 51-149 L595984-02 WG613527 2-Chloroethyl vinyl ether mg/l 0.0418 0 .125 33.4 10-161 L595984-02 WG613527 2-Chlorotoluene mg/l 0.0214 0 .025 85.7 65-133 L595984-02 WG613527 4-Chlorotoluene mg/l 0.0213 0 .025 85.0 67-129 L595984-02 WG613527 4-Methyl-2-pentanone (MIBK) mg/l 0.108 0 .125 86.2 53-154 L595984-02 WG613527 Acetone mg/l 0.0843 0 .125 67.4 34-146 L595984-02 WG613527 Acrolein mg/l 0.0982 0 .125 78.5 10-189 L595984-02 WG613527 Acrylonitrile mg/l 0.106 0 .125 84.7 49-162 L595984-02 WG613527 Benzene mg/l 0.0200 0 .025 80.0 51-134 L595984-02 WG613527 Bromobenzene mg/l 0.0209 0 .025 83.5 64-130 L595984-02 WG613527 Bromodichloromethane mg/l 0.0217 0 .025 87.0 67-132 L595984-02 WG613527

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 43 of 49

Reference 45 Page 209

Page 210: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 September 25, 2012

L595984

Matrix SpikeAnalyte Units MS Res Ref Res TV % Rec Limit Ref Samp Batch

Bromoform mg/l 0.0207 0 .025 82.9 59-137 L595984-02 WG613527 Bromomethane mg/l 0.0175 0 .025 70.0 23-177 L595984-02 WG613527 Carbon tetrachloride mg/l 0.0198 0 .025 79.2 49-140 L595984-02 WG613527 Chlorobenzene mg/l 0.0209 0 .025 83.6 69-126 L595984-02 WG613527 Chlorodibromomethane mg/l 0.0210 0 .025 83.8 68-130 L595984-02 WG613527 Chloroethane mg/l 0.0192 0 .025 77.0 32-177 L595984-02 WG613527 Chloroform mg/l 0.0308 0.00670 .025 96.3 64-130 L595984-02 WG613527 Chloromethane mg/l 0.0175 0 .025 70.0 27-155 L595984-02 WG613527 cis-1,2-Dichloroethene mg/l 0.0209 0 .025 83.6 54-137 L595984-02 WG613527 cis-1,3-Dichloropropene mg/l 0.0211 0 .025 84.5 63-127 L595984-02 WG613527 Di-isopropyl ether mg/l 0.0221 0 .025 88.5 58-133 L595984-02 WG613527 Dibromomethane mg/l 0.0209 0 .025 83.5 68-131 L595984-02 WG613527 Dichlorodifluoromethane mg/l 0.0204 0 .025 81.8 16-188 L595984-02 WG613527 Ethylbenzene mg/l 0.0210 0 .025 84.2 64-135 L595984-02 WG613527 Hexachloro-1,3-butadiene mg/l 0.0217 0 .025 86.7 64-140 L595984-02 WG613527 Isopropylbenzene mg/l 0.0234 0 .025 93.4 62-134 L595984-02 WG613527 Methyl tert-butyl ether mg/l 0.0196 0 .025 78.5 55-136 L595984-02 WG613527 Methylene Chloride mg/l 0.0163 0 .025 65.3 52-130 L595984-02 WG613527 n-Butylbenzene mg/l 0.0218 0 .025 87.2 62-142 L595984-02 WG613527 n-Propylbenzene mg/l 0.0220 0 .025 87.9 62-137 L595984-02 WG613527 Naphthalene mg/l 0.0192 0 .025 76.6 65-140 L595984-02 WG613527 p-Isopropyltoluene mg/l 0.0223 0 .025 89.0 64-142 L595984-02 WG613527 sec-Butylbenzene mg/l 0.0220 0 .025 88.1 67-139 L595984-02 WG613527 Styrene mg/l 0.0206 0 .025 82.5 58-152 L595984-02 WG613527 tert-Butylbenzene mg/l 0.0222 0 .025 88.9 66-139 L595984-02 WG613527 Tetrachloroethene mg/l 0.0332 0.0120 .025 84.7 56-139 L595984-02 WG613527 Toluene mg/l 0.0207 0 .025 82.8 61-126 L595984-02 WG613527 trans-1,2-Dichloroethene mg/l 0.0179 0 .025 71.6 45-137 L595984-02 WG613527 trans-1,3-Dichloropropene mg/l 0.0209 0 .025 83.6 59-130 L595984-02 WG613527 Trichloroethene mg/l 0.0208 0 .025 83.2 40-155 L595984-02 WG613527 Trichlorofluoromethane mg/l 0.0200 0 .025 79.8 35-177 L595984-02 WG613527 Vinyl chloride mg/l 0.0180 0 .025 71.8 32-159 L595984-02 WG613527 Xylenes, Total mg/l 0.0631 0 .075 84.1 64-133 L595984-02 WG613527 4-Bromofluorobenzene 103.1 82-120 WG613527 Dibromofluoromethane 103.6 82-126 WG613527 Toluene-d8 106.3 92-112 WG613527

1,1,1,2-Tetrachloroethane mg/l 0.0230 0 .025 92.0 71-130 L595984-14 WG614424 1,1,1-Trichloroethane mg/l 0.0275 0.00360 .025 95.7 58-137 L595984-14 WG614424 1,1,2,2-Tetrachloroethane mg/l 0.0250 0 .025 99.9 64-149 L595984-14 WG614424 1,1,2-Trichloroethane mg/l 0.0253 0 .025 101. 73-128 L595984-14 WG614424 1,1,2-Trichlorotrifluoroethane mg/l 0.0251 0 .025 100. 36-159 L595984-14 WG614424 1,1-Dichloroethane mg/l 0.0243 0 .025 97.3 58-133 L595984-14 WG614424 1,1-Dichloroethene mg/l 0.0264 0 .025 105. 32-152 L595984-14 WG614424 1,1-Dichloropropene mg/l 0.0240 0 .025 96.2 50-140 L595984-14 WG614424 1,2,3-Trichlorobenzene mg/l 0.0248 0 .025 99.3 68-135 L595984-14 WG614424 1,2,3-Trichloropropane mg/l 0.0223 0 .025 89.0 74-137 L595984-14 WG614424 1,2,3-Trimethylbenzene mg/l 0.0229 0 .025 91.6 67-133 L595984-14 WG614424 1,2,4-Trichlorobenzene mg/l 0.0252 0 .025 101. 67-133 L595984-14 WG614424 1,2,4-Trimethylbenzene mg/l 0.0239 0 .025 95.4 62-141 L595984-14 WG614424 1,2-Dibromo-3-Chloropropane mg/l 0.0229 0 .025 91.5 55-148 L595984-14 WG614424 1,2-Dibromoethane mg/l 0.0247 0 .025 99.0 71-129 L595984-14 WG614424 1,2-Dichlorobenzene mg/l 0.0242 0 .025 96.6 75-125 L595984-14 WG614424 1,2-Dichloroethane mg/l 0.0230 0 .025 92.1 59-135 L595984-14 WG614424 1,2-Dichloropropane mg/l 0.0245 0 .025 97.9 68-126 L595984-14 WG614424 1,3,5-Trimethylbenzene mg/l 0.0241 0 .025 96.4 67-136 L595984-14 WG614424 1,3-Dichlorobenzene mg/l 0.0246 0 .025 98.2 69-131 L595984-14 WG614424 1,3-Dichloropropane mg/l 0.0249 0 .025 99.5 70-122 L595984-14 WG614424

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 44 of 49

Reference 45 Page 210

Page 211: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 September 25, 2012

L595984

Matrix SpikeAnalyte Units MS Res Ref Res TV % Rec Limit Ref Samp Batch

1,4-Dichlorobenzene mg/l 0.0244 0 .025 97.6 70-123 L595984-14 WG614424 2,2-Dichloropropane mg/l 0.0207 0 .025 82.6 51-141 L595984-14 WG614424 2-Butanone (MEK) mg/l 0.121 0 .125 96.6 51-149 L595984-14 WG614424 2-Chloroethyl vinyl ether mg/l 0.0410 0 .125 32.8 10-161 L595984-14 WG614424 2-Chlorotoluene mg/l 0.0238 0 .025 95.3 65-133 L595984-14 WG614424 4-Chlorotoluene mg/l 0.0242 0 .025 96.9 67-129 L595984-14 WG614424 4-Methyl-2-pentanone (MIBK) mg/l 0.121 0 .125 97.1 53-154 L595984-14 WG614424 Acetone mg/l 0.110 0 .125 88.1 34-146 L595984-14 WG614424 Acrolein mg/l 0.121 0 .125 97.2 10-189 L595984-14 WG614424 Acrylonitrile mg/l 0.125 0 .125 99.9 49-162 L595984-14 WG614424 Benzene mg/l 0.0241 0 .025 96.4 51-134 L595984-14 WG614424 Bromobenzene mg/l 0.0237 0 .025 94.8 64-130 L595984-14 WG614424 Bromodichloromethane mg/l 0.0224 0 .025 89.4 67-132 L595984-14 WG614424 Bromoform mg/l 0.0236 0 .025 94.3 59-137 L595984-14 WG614424 Bromomethane mg/l 0.0286 0 .025 114. 23-177 L595984-14 WG614424 Carbon tetrachloride mg/l 0.0214 0 .025 85.6 49-140 L595984-14 WG614424 Chlorobenzene mg/l 0.0249 0 .025 99.5 69-126 L595984-14 WG614424 Chlorodibromomethane mg/l 0.0242 0 .025 96.6 68-130 L595984-14 WG614424 Chloroethane mg/l 0.0248 0 .025 99.2 32-177 L595984-14 WG614424 Chloroform mg/l 0.0254 0 .025 102. 64-130 L595984-14 WG614424 Chloromethane mg/l 0.0219 0 .025 87.6 27-155 L595984-14 WG614424 cis-1,2-Dichloroethene mg/l 0.0236 0 .025 94.4 54-137 L595984-14 WG614424 cis-1,3-Dichloropropene mg/l 0.0233 0 .025 93.3 63-127 L595984-14 WG614424 Di-isopropyl ether mg/l 0.0231 0 .025 92.4 58-133 L595984-14 WG614424 Dibromomethane mg/l 0.0230 0 .025 91.8 68-131 L595984-14 WG614424 Dichlorodifluoromethane mg/l 0.0220 0 .025 87.9 16-188 L595984-14 WG614424 Ethylbenzene mg/l 0.0240 0 .025 96.1 64-135 L595984-14 WG614424 Hexachloro-1,3-butadiene mg/l 0.0245 0 .025 97.8 64-140 L595984-14 WG614424 Isopropylbenzene mg/l 0.0252 0 .025 101. 62-134 L595984-14 WG614424 Methyl tert-butyl ether mg/l 0.0239 0 .025 95.5 55-136 L595984-14 WG614424 Methylene Chloride mg/l 0.0255 0 .025 102. 52-130 L595984-14 WG614424 n-Butylbenzene mg/l 0.0246 0 .025 98.6 62-142 L595984-14 WG614424 n-Propylbenzene mg/l 0.0244 0 .025 97.6 62-137 L595984-14 WG614424 Naphthalene mg/l 0.0232 0 .025 92.8 65-140 L595984-14 WG614424 p-Isopropyltoluene mg/l 0.0243 0 .025 97.2 64-142 L595984-14 WG614424 sec-Butylbenzene mg/l 0.0247 0 .025 98.8 67-139 L595984-14 WG614424 Styrene mg/l 0.0233 0 .025 93.2 58-152 L595984-14 WG614424 tert-Butylbenzene mg/l 0.0240 0 .025 95.9 66-139 L595984-14 WG614424 Tetrachloroethene mg/l 0.175 0.150 .025 102. 56-139 L595984-14 WG614424 Toluene mg/l 0.0245 0 .025 98.1 61-126 L595984-14 WG614424 trans-1,2-Dichloroethene mg/l 0.0242 0 .025 97.0 45-137 L595984-14 WG614424 trans-1,3-Dichloropropene mg/l 0.0233 0 .025 93.3 59-130 L595984-14 WG614424 Trichloroethene mg/l 0.104 0.0780 .025 104. 40-155 L595984-14 WG614424 Trichlorofluoromethane mg/l 0.0245 0 .025 97.8 35-177 L595984-14 WG614424 Vinyl chloride mg/l 0.0219 0 .025 87.7 32-159 L595984-14 WG614424 Xylenes, Total mg/l 0.0736 0 .075 98.2 64-133 L595984-14 WG614424 4-Bromofluorobenzene 96.14 82-120 WG614424 Dibromofluoromethane 98.86 82-126 WG614424 Toluene-d8 100.6 92-112 WG614424

Matrix Spike DuplicateAnalyte Units MSD Ref %Rec Limit RPD Limit Ref Samp Batch

1,1,1,2-Tetrachloroethane mg/l 0.0213 0.0220 85.2 71-130 3.40 20 L595984-02 WG613527 1,1,1-Trichloroethane mg/l 0.0206 0.0213 82.4 58-137 3.45 20 L595984-02 WG613527 1,1,2,2-Tetrachloroethane mg/l 0.0218 0.0209 87.3 64-149 4.48 20 L595984-02 WG613527 1,1,2-Trichloroethane mg/l 0.0218 0.0203 87.4 73-128 7.10 20 L595984-02 WG613527 1,1,2-Trichlorotrifluoroethane mg/l 0.0209 0.0211 83.7 36-159 0.860 21 L595984-02 WG613527 1,1-Dichloroethane mg/l 0.0203 0.0208 81.4 58-133 2.19 20 L595984-02 WG613527

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 45 of 49

Reference 45 Page 211

Page 212: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 September 25, 2012

L595984

Matrix Spike DuplicateAnalyte Units MSD Ref %Rec Limit RPD Limit Ref Samp Batch

1,1-Dichloroethene mg/l 0.0186 0.0189 74.3 32-152 1.52 20 L595984-02 WG613527 1,1-Dichloropropene mg/l 0.0192 0.0200 76.8 50-140 4.27 20 L595984-02 WG613527 1,2,3-Trichlorobenzene mg/l 0.0181 0.0200 72.2 68-135 10.2 20 L595984-02 WG613527 1,2,3-Trichloropropane mg/l 0.0221 0.0188 88.6 74-137 16.1 20 L595984-02 WG613527 1,2,3-Trimethylbenzene mg/l 0.0193 0.0202 77.1 67-133 4.67 20 L595984-02 WG613527 1,2,4-Trichlorobenzene mg/l 0.0196 0.0218 78.5 67-133 10.3 20 L595984-02 WG613527 1,2,4-Trimethylbenzene mg/l 0.0202 0.0212 80.8 62-141 4.83 20 L595984-02 WG613527 1,2-Dibromo-3-Chloropropane mg/l 0.0219 0.0205 87.7 55-148 6.49 22 L595984-02 WG613527 1,2-Dibromoethane mg/l 0.0212 0.0199 84.6 71-129 6.07 20 L595984-02 WG613527 1,2-Dichlorobenzene mg/l 0.0210 0.0209 84.1 75-125 0.660 20 L595984-02 WG613527 1,2-Dichloroethane mg/l 0.0201 0.0196 80.5 59-135 2.75 20 L595984-02 WG613527 1,2-Dichloropropane mg/l 0.0216 0.0213 86.5 68-126 1.49 20 L595984-02 WG613527 1,3,5-Trimethylbenzene mg/l 0.0210 0.0216 83.9 67-136 3.15 20 L595984-02 WG613527 1,3-Dichlorobenzene mg/l 0.0205 0.0214 82.2 69-131 3.85 20 L595984-02 WG613527 1,3-Dichloropropane mg/l 0.0211 0.0202 84.4 70-122 4.36 20 L595984-02 WG613527 1,4-Dichlorobenzene mg/l 0.0200 0.0205 80.2 70-123 2.10 20 L595984-02 WG613527 2,2-Dichloropropane mg/l 0.0201 0.0211 80.2 51-141 5.05 20 L595984-02 WG613527 2-Butanone (MEK) mg/l 0.116 0.103 92.6 51-149 11.3 22 L595984-02 WG613527 2-Chloroethyl vinyl ether mg/l 0.0136 0.0418 10.9 10-161 102.* 40 L595984-02 WG613527 2-Chlorotoluene mg/l 0.0179 0.0214 71.8 65-133 17.7 20 L595984-02 WG613527 4-Chlorotoluene mg/l 0.0209 0.0213 83.6 67-129 1.64 20 L595984-02 WG613527 4-Methyl-2-pentanone (MIBK) mg/l 0.124 0.108 99.4 53-154 14.2 21 L595984-02 WG613527 Acetone mg/l 0.0949 0.0843 75.9 34-146 11.8 22 L595984-02 WG613527 Acrolein mg/l 0.0952 0.0982 76.2 10-189 3.05 30 L595984-02 WG613527 Acrylonitrile mg/l 0.119 0.106 94.9 49-162 11.4 20 L595984-02 WG613527 Benzene mg/l 0.0199 0.0200 79.6 51-134 0.520 20 L595984-02 WG613527 Bromobenzene mg/l 0.0205 0.0209 82.0 64-130 1.78 20 L595984-02 WG613527 Bromodichloromethane mg/l 0.0210 0.0217 83.9 67-132 3.62 20 L595984-02 WG613527 Bromoform mg/l 0.0220 0.0207 87.9 59-137 5.87 20 L595984-02 WG613527 Bromomethane mg/l 0.0168 0.0175 67.1 23-177 4.19 21 L595984-02 WG613527 Carbon tetrachloride mg/l 0.0195 0.0198 77.8 49-140 1.70 20 L595984-02 WG613527 Chlorobenzene mg/l 0.0206 0.0209 82.4 69-126 1.40 20 L595984-02 WG613527 Chlorodibromomethane mg/l 0.0214 0.0210 85.6 68-130 2.04 20 L595984-02 WG613527 Chloroethane mg/l 0.0183 0.0192 73.1 32-177 5.20 21 L595984-02 WG613527 Chloroform mg/l 0.0291 0.0308 89.8 64-130 5.43 20 L595984-02 WG613527 Chloromethane mg/l 0.0165 0.0175 66.1 27-155 5.80 20 L595984-02 WG613527 cis-1,2-Dichloroethene mg/l 0.0204 0.0209 81.6 54-137 2.42 20 L595984-02 WG613527 cis-1,3-Dichloropropene mg/l 0.0209 0.0211 83.7 63-127 0.900 20 L595984-02 WG613527 Di-isopropyl ether mg/l 0.0214 0.0221 85.7 58-133 3.18 20 L595984-02 WG613527 Dibromomethane mg/l 0.0207 0.0209 83.0 68-131 0.670 20 L595984-02 WG613527 Dichlorodifluoromethane mg/l 0.0189 0.0204 75.4 16-188 8.11 22 L595984-02 WG613527 Ethylbenzene mg/l 0.0209 0.0210 83.4 64-135 0.890 20 L595984-02 WG613527 Hexachloro-1,3-butadiene mg/l 0.0204 0.0217 81.6 64-140 6.09 20 L595984-02 WG613527 Isopropylbenzene mg/l 0.0232 0.0234 92.6 62-134 0.890 20 L595984-02 WG613527 Methyl tert-butyl ether mg/l 0.0193 0.0196 77.1 55-136 1.81 20 L595984-02 WG613527 Methylene Chloride mg/l 0.0163 0.0163 65.4 52-130 0.130 20 L595984-02 WG613527 n-Butylbenzene mg/l 0.0213 0.0218 85.3 62-142 2.19 20 L595984-02 WG613527 n-Propylbenzene mg/l 0.0219 0.0220 87.7 62-137 0.250 20 L595984-02 WG613527 Naphthalene mg/l 0.0191 0.0192 76.4 65-140 0.380 20 L595984-02 WG613527 p-Isopropyltoluene mg/l 0.0211 0.0223 84.3 64-142 5.43 20 L595984-02 WG613527 sec-Butylbenzene mg/l 0.0214 0.0220 85.7 67-139 2.74 20 L595984-02 WG613527 Styrene mg/l 0.0208 0.0206 83.3 58-152 0.960 20 L595984-02 WG613527 tert-Butylbenzene mg/l 0.0218 0.0222 87.0 66-139 2.16 20 L595984-02 WG613527 Tetrachloroethene mg/l 0.0332 0.0332 84.8 56-139 0.0800 20 L595984-02 WG613527 Toluene mg/l 0.0210 0.0207 84.1 61-126 1.60 20 L595984-02 WG613527 trans-1,2-Dichloroethene mg/l 0.0174 0.0179 69.5 45-137 3.06 20 L595984-02 WG613527 trans-1,3-Dichloropropene mg/l 0.0212 0.0209 84.8 59-130 1.37 20 L595984-02 WG613527 Trichloroethene mg/l 0.0205 0.0208 81.9 40-155 1.56 20 L595984-02 WG613527 Trichlorofluoromethane mg/l 0.0197 0.0200 78.7 35-177 1.39 23 L595984-02 WG613527

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

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12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 September 25, 2012

L595984

Matrix Spike DuplicateAnalyte Units MSD Ref %Rec Limit RPD Limit Ref Samp Batch

Vinyl chloride mg/l 0.0171 0.0180 68.2 32-159 5.19 21 L595984-02 WG613527 Xylenes, Total mg/l 0.0615 0.0631 82.0 64-133 2.57 20 L595984-02 WG613527 4-Bromofluorobenzene 105.4 82-120 WG613527 Dibromofluoromethane 100.4 82-126 WG613527 Toluene-d8 106.6 92-112 WG613527

1,1,1,2-Tetrachloroethane mg/l 0.0245 0.0230 98.1 71-130 6.39 20 L595984-14 WG614424 1,1,1-Trichloroethane mg/l 0.0276 0.0275 95.8 58-137 0.120 20 L595984-14 WG614424 1,1,2,2-Tetrachloroethane mg/l 0.0273 0.0250 109. 64-149 9.05 20 L595984-14 WG614424 1,1,2-Trichloroethane mg/l 0.0261 0.0253 104. 73-128 3.47 20 L595984-14 WG614424 1,1,2-Trichlorotrifluoroethane mg/l 0.0257 0.0251 103. 36-159 2.47 21 L595984-14 WG614424 1,1-Dichloroethane mg/l 0.0249 0.0243 99.7 58-133 2.45 20 L595984-14 WG614424 1,1-Dichloroethene mg/l 0.0277 0.0264 111. 32-152 4.83 20 L595984-14 WG614424 1,1-Dichloropropene mg/l 0.0244 0.0240 97.5 50-140 1.37 20 L595984-14 WG614424 1,2,3-Trichlorobenzene mg/l 0.0262 0.0248 105. 68-135 5.41 20 L595984-14 WG614424 1,2,3-Trichloropropane mg/l 0.0260 0.0223 104. 74-137 15.6 20 L595984-14 WG614424 1,2,3-Trimethylbenzene mg/l 0.0230 0.0229 92.2 67-133 0.650 20 L595984-14 WG614424 1,2,4-Trichlorobenzene mg/l 0.0263 0.0252 105. 67-133 4.28 20 L595984-14 WG614424 1,2,4-Trimethylbenzene mg/l 0.0240 0.0239 95.9 62-141 0.540 20 L595984-14 WG614424 1,2-Dibromo-3-Chloropropane mg/l 0.0269 0.0229 108. 55-148 16.3 22 L595984-14 WG614424 1,2-Dibromoethane mg/l 0.0261 0.0247 104. 71-129 5.14 20 L595984-14 WG614424 1,2-Dichlorobenzene mg/l 0.0252 0.0242 101. 75-125 4.05 20 L595984-14 WG614424 1,2-Dichloroethane mg/l 0.0243 0.0230 97.3 59-135 5.53 20 L595984-14 WG614424 1,2-Dichloropropane mg/l 0.0250 0.0245 100. 68-126 2.10 20 L595984-14 WG614424 1,3,5-Trimethylbenzene mg/l 0.0240 0.0241 95.9 67-136 0.490 20 L595984-14 WG614424 1,3-Dichlorobenzene mg/l 0.0250 0.0246 100. 69-131 1.75 20 L595984-14 WG614424 1,3-Dichloropropane mg/l 0.0257 0.0249 103. 70-122 3.42 20 L595984-14 WG614424 1,4-Dichlorobenzene mg/l 0.0247 0.0244 98.8 70-123 1.20 20 L595984-14 WG614424 2,2-Dichloropropane mg/l 0.0222 0.0207 88.8 51-141 7.14 20 L595984-14 WG614424 2-Butanone (MEK) mg/l 0.137 0.121 110. 51-149 12.5 22 L595984-14 WG614424 2-Chloroethyl vinyl ether mg/l 0.0122 0.0410 9.77* 10-161 108.* 40 L595984-14 WG614424 2-Chlorotoluene mg/l 0.0242 0.0238 96.9 65-133 1.67 20 L595984-14 WG614424 4-Chlorotoluene mg/l 0.0245 0.0242 97.9 67-129 0.970 20 L595984-14 WG614424 4-Methyl-2-pentanone (MIBK) mg/l 0.140 0.121 112. 53-154 14.2 21 L595984-14 WG614424 Acetone mg/l 0.129 0.110 104. 34-146 16.1 22 L595984-14 WG614424 Acrolein mg/l 0.144 0.121 115. 10-189 17.1 30 L595984-14 WG614424 Acrylonitrile mg/l 0.146 0.125 116. 49-162 15.3 20 L595984-14 WG614424 Benzene mg/l 0.0247 0.0241 98.7 51-134 2.38 20 L595984-14 WG614424 Bromobenzene mg/l 0.0242 0.0237 96.8 64-130 2.08 20 L595984-14 WG614424 Bromodichloromethane mg/l 0.0234 0.0224 93.8 67-132 4.73 20 L595984-14 WG614424 Bromoform mg/l 0.0253 0.0236 101. 59-137 6.90 20 L595984-14 WG614424 Bromomethane mg/l 0.0308 0.0286 123. 23-177 7.66 21 L595984-14 WG614424 Carbon tetrachloride mg/l 0.0218 0.0214 87.1 49-140 1.65 20 L595984-14 WG614424 Chlorobenzene mg/l 0.0251 0.0249 100. 69-126 0.870 20 L595984-14 WG614424 Chlorodibromomethane mg/l 0.0251 0.0242 100. 68-130 3.85 20 L595984-14 WG614424 Chloroethane mg/l 0.0261 0.0248 104. 32-177 5.04 21 L595984-14 WG614424 Chloroform mg/l 0.0265 0.0254 106. 64-130 4.06 20 L595984-14 WG614424 Chloromethane mg/l 0.0225 0.0219 90.1 27-155 2.79 20 L595984-14 WG614424 cis-1,2-Dichloroethene mg/l 0.0244 0.0236 97.6 54-137 3.35 20 L595984-14 WG614424 cis-1,3-Dichloropropene mg/l 0.0239 0.0233 95.7 63-127 2.60 20 L595984-14 WG614424 Di-isopropyl ether mg/l 0.0239 0.0231 95.6 58-133 3.43 20 L595984-14 WG614424 Dibromomethane mg/l 0.0253 0.0230 101. 68-131 9.64 20 L595984-14 WG614424 Dichlorodifluoromethane mg/l 0.0216 0.0220 86.5 16-188 1.62 22 L595984-14 WG614424 Ethylbenzene mg/l 0.0245 0.0240 97.9 64-135 1.87 20 L595984-14 WG614424 Hexachloro-1,3-butadiene mg/l 0.0239 0.0245 95.7 64-140 2.20 20 L595984-14 WG614424 Isopropylbenzene mg/l 0.0256 0.0252 102. 62-134 1.71 20 L595984-14 WG614424 Methyl tert-butyl ether mg/l 0.0260 0.0239 104. 55-136 8.67 20 L595984-14 WG614424 Methylene Chloride mg/l 0.0271 0.0255 108. 52-130 5.78 20 L595984-14 WG614424

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

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12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 September 25, 2012

L595984

Matrix Spike DuplicateAnalyte Units MSD Ref %Rec Limit RPD Limit Ref Samp Batch

n-Butylbenzene mg/l 0.0246 0.0246 98.4 62-142 0.200 20 L595984-14 WG614424 n-Propylbenzene mg/l 0.0247 0.0244 98.6 62-137 1.08 20 L595984-14 WG614424 Naphthalene mg/l 0.0255 0.0232 102. 65-140 9.54 20 L595984-14 WG614424 p-Isopropyltoluene mg/l 0.0253 0.0243 101. 64-142 3.86 20 L595984-14 WG614424 sec-Butylbenzene mg/l 0.0249 0.0247 99.6 67-139 0.810 20 L595984-14 WG614424 Styrene mg/l 0.0232 0.0233 92.9 58-152 0.280 20 L595984-14 WG614424 tert-Butylbenzene mg/l 0.0249 0.0240 99.7 66-139 3.93 20 L595984-14 WG614424 Tetrachloroethene mg/l 0.166 0.175 62.9 56-139 5.67 20 L595984-14 WG614424 Toluene mg/l 0.0249 0.0245 99.7 61-126 1.55 20 L595984-14 WG614424 trans-1,2-Dichloroethene mg/l 0.0257 0.0242 103. 45-137 5.81 20 L595984-14 WG614424 trans-1,3-Dichloropropene mg/l 0.0249 0.0233 99.5 59-130 6.49 20 L595984-14 WG614424 Trichloroethene mg/l 0.103 0.104 101. 40-155 0.780 20 L595984-14 WG614424 Trichlorofluoromethane mg/l 0.0253 0.0245 101. 35-177 3.33 23 L595984-14 WG614424 Vinyl chloride mg/l 0.0220 0.0219 88.0 32-159 0.300 21 L595984-14 WG614424 Xylenes, Total mg/l 0.0743 0.0736 99.1 64-133 0.980 20 L595984-14 WG614424 4-Bromofluorobenzene 94.27 82-120 WG614424 Dibromofluoromethane 98.35 82-126 WG614424 Toluene-d8 99.02 92-112 WG614424

Batch number /Run number / Sample number cross reference

WG613527: R2360895: L595984-01 02 03 04 05 06 07 08 09 10 11 12 13 17WG614424: R2362055: L595984-14 15 16

* * Calculations are performed prior to rounding of reported values.* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

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12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 September 25, 2012

L595984

The data package includes a summary of the analytic results of the qualitycontrol samples required by the SW-846 or CWA methods. The quality controlsamples include a method blank, a laboratory control sample, and the matrixspike/matrix spike duplicate analysis. If a target parameter is outsidethe method limits, every sample that is effected is flagged with theappropriate qualifier in Appendix B of the analytic report.

Method Blank - an aliquot of reagent water carried through theentire analytic process. The method blank results indicate ifany possible contamination exposure during the sample handling,digestion or extraction process, and analysis. Concentrations oftarget analytes above the reporting limit in the method blank arequalified with the "B" qualifier.

Laboratory Control Sample - is a sample of known concentrationthat is carried through the digestion/extraction and analysisprocess. The percent recovery, expressed as a percentage of thetheoretical concentration, has statistical control limitsindicating that the analytic process is "in control". If atarget analyte is outside the control limits for the laboratorycontrol sample or any other control sample, the parameter isflagged with a "J4" qualifier for all effected samples.

Matrix Spike and Matrix Spike Duplicate - is two aliquots of anenvironmental sample that is spiked with known concentrations oftarget analytes. The percent recovery of the target analytesalso has statistical control limits. If any recoveries that areoutside the method control limits, the sample that was selectedfor matrix spike/matrix spike duplicate analysis is flagged witheither a "J5" or a "J6". The relative percent difference (%RPD)between the matrix spike and the matrix spike duplicaterecoveries is all calculated. If the RPD is above the methodlimit, the effected samples are flagged with a "J3" qualifier.

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12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

Mrs. Wendy MilejczakAcuity Environmental Solutions7965 East 106th St. Suite 128Fishers, IN 46038

Report Summary

Thursday December 27, 2012

Report Number: L612291

Samples Received: 12/20/12

Client Project: 1024-1003-01

Description: Component Machine

The analytical results in this report are based upon information suppliedby you, the client, and are for your exclusive use. If you have anyquestions regarding this data package, please do not hesitate to call.

Entire Report Reviewed By: ____________________________________

T. Alan Harvill , ESC Representative

Laboratory Certification NumbersA2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197,FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,NC - ENV375/DW21704/BIO041, ND - R-140. NJ - TN002, NJ NELAP - TN002,SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364

Accreditation is only applicable to the test methods specified on each scope of accreditation heldby ESC Lab Sciences.Note: The use of the preparatory EPA Method 3511 is not approved or endorsed by the CA ELAP.

This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.Where applicable, sampling conducted by ESC is performed per guidance providedin laboratory standard operating procedures: 060302, 060303, and 060304.

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12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-01 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : PMW-4

Project # : 1024-1003-01 Collected By : Collection Date : 12/18/12 12:05

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 12/21/12 1 Acrolein BDL 50. ug/l 8260B 12/21/12 1 Acrylonitrile BDL 10. ug/l 8260B 12/21/12 1 Benzene BDL 1.0 ug/l 8260B 12/21/12 1 Bromobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 12/21/12 1 Bromoform BDL 1.0 ug/l 8260B 12/21/12 1 Bromomethane BDL 5.0 ug/l 8260B 12/21/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 12/21/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 12/21/12 1 Chloroethane BDL 5.0 ug/l 8260B 12/21/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 12/21/12 1 Chloroform BDL 5.0 ug/l 8260B 12/21/12 1 Chloromethane BDL 2.5 ug/l 8260B 12/21/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 12/21/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 12/21/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 12/21/12 1 Dibromomethane BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 12/21/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 cis-1,2-Dichloroethene 13. 1.0 ug/l 8260B 12/21/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 12/21/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 12/21/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 12/21/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

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12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-01 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : PMW-4

Project # : 1024-1003-01 Collected By : Collection Date : 12/18/12 12:05

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 12/21/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 12/21/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 12/21/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 12/21/12 1 Naphthalene BDL 5.0 ug/l 8260B 12/21/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Styrene BDL 1.0 ug/l 8260B 12/21/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 12/21/12 1 Tetrachloroethene 130 1.0 ug/l 8260B 12/21/12 1 Toluene BDL 5.0 ug/l 8260B 12/21/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,1,1-Trichloroethane 1.8 1.0 ug/l 8260B 12/21/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 Trichloroethene 43. 1.0 ug/l 8260B 12/21/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 12/21/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 12/21/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 12/21/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 12/21/12 1

Surrogate Recovery Toluene-d8 105. % Rec. 8260B 12/21/12 1 Dibromofluoromethane 114. % Rec. 8260B 12/21/12 1 4-Bromofluorobenzene 101. % Rec. 8260B 12/21/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 12/27/12 14:54 Printed: 12/27/12 14:55

Page 3 of 43

Reference 45 Page 218

Page 219: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-02 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : PMW-5

Project # : 1024-1003-01 Collected By : Collection Date : 12/18/12 14:33

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 12/21/12 1 Acrolein BDL 50. ug/l 8260B 12/21/12 1 Acrylonitrile BDL 10. ug/l 8260B 12/21/12 1 Benzene BDL 1.0 ug/l 8260B 12/21/12 1 Bromobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 12/21/12 1 Bromoform BDL 1.0 ug/l 8260B 12/21/12 1 Bromomethane BDL 5.0 ug/l 8260B 12/21/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 12/21/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 12/21/12 1 Chloroethane BDL 5.0 ug/l 8260B 12/21/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 12/21/12 1 Chloroform BDL 5.0 ug/l 8260B 12/21/12 1 Chloromethane BDL 2.5 ug/l 8260B 12/21/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 12/21/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 12/21/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 12/21/12 1 Dibromomethane BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 12/21/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 12/21/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 12/21/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 12/21/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 4 of 43

Reference 45 Page 219

Page 220: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-02 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : PMW-5

Project # : 1024-1003-01 Collected By : Collection Date : 12/18/12 14:33

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 12/21/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 12/21/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 12/21/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 12/21/12 1 Naphthalene BDL 5.0 ug/l 8260B 12/21/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Styrene BDL 1.0 ug/l 8260B 12/21/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 12/21/12 1 Tetrachloroethene 16. 1.0 ug/l 8260B 12/21/12 1 Toluene BDL 5.0 ug/l 8260B 12/21/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 Trichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 12/21/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 12/21/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 12/21/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 12/21/12 1

Surrogate Recovery Toluene-d8 104. % Rec. 8260B 12/21/12 1 Dibromofluoromethane 104. % Rec. 8260B 12/21/12 1 4-Bromofluorobenzene 103. % Rec. 8260B 12/21/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 12/27/12 14:54 Printed: 12/27/12 14:55

Page 5 of 43

Reference 45 Page 220

Page 221: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-03 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : MW-8

Project # : 1024-1003-01 Collected By : Collection Date : 12/18/12 15:50

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 12/21/12 1 Acrolein BDL 50. ug/l 8260B 12/21/12 1 Acrylonitrile BDL 10. ug/l 8260B 12/21/12 1 Benzene BDL 1.0 ug/l 8260B 12/21/12 1 Bromobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 12/21/12 1 Bromoform BDL 1.0 ug/l 8260B 12/21/12 1 Bromomethane BDL 5.0 ug/l 8260B 12/21/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 12/21/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 12/21/12 1 Chloroethane BDL 5.0 ug/l 8260B 12/21/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 12/21/12 1 Chloroform 16. 5.0 ug/l 8260B 12/21/12 1 Chloromethane BDL 2.5 ug/l 8260B 12/21/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 12/21/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 12/21/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 12/21/12 1 Dibromomethane BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 12/21/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 cis-1,2-Dichloroethene 10. 1.0 ug/l 8260B 12/21/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 12/21/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 12/21/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 12/21/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 6 of 43

Reference 45 Page 221

Page 222: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-03 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : MW-8

Project # : 1024-1003-01 Collected By : Collection Date : 12/18/12 15:50

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 12/21/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 12/21/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 12/21/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 12/21/12 1 Naphthalene BDL 5.0 ug/l 8260B 12/21/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Styrene BDL 1.0 ug/l 8260B 12/21/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 12/21/12 1 Tetrachloroethene 39. 1.0 ug/l 8260B 12/21/12 1 Toluene BDL 5.0 ug/l 8260B 12/21/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,1,1-Trichloroethane 1.3 1.0 ug/l 8260B 12/21/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 Trichloroethene 29. 1.0 ug/l 8260B 12/21/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 12/21/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 12/21/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 12/21/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 12/21/12 1

Surrogate Recovery Toluene-d8 103. % Rec. 8260B 12/21/12 1 Dibromofluoromethane 96.5 % Rec. 8260B 12/21/12 1 4-Bromofluorobenzene 105. % Rec. 8260B 12/21/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 12/27/12 14:54 Printed: 12/27/12 14:55

Page 7 of 43

Reference 45 Page 222

Page 223: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-04 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : MW-11

Project # : 1024-1003-01 Collected By : Collection Date : 12/19/12 09:10

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 12/21/12 1 Acrolein BDL 50. ug/l 8260B 12/21/12 1 Acrylonitrile BDL 10. ug/l 8260B 12/21/12 1 Benzene BDL 1.0 ug/l 8260B 12/21/12 1 Bromobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 12/21/12 1 Bromoform BDL 1.0 ug/l 8260B 12/21/12 1 Bromomethane BDL 5.0 ug/l 8260B 12/21/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 12/21/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 12/21/12 1 Chloroethane BDL 5.0 ug/l 8260B 12/21/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 12/21/12 1 Chloroform BDL 5.0 ug/l 8260B 12/21/12 1 Chloromethane BDL 2.5 ug/l 8260B 12/21/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 12/21/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 12/21/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 12/21/12 1 Dibromomethane BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 12/21/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 12/21/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 12/21/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 12/21/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 8 of 43

Reference 45 Page 223

Page 224: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-04 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : MW-11

Project # : 1024-1003-01 Collected By : Collection Date : 12/19/12 09:10

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 12/21/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 12/21/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 12/21/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 12/21/12 1 Naphthalene BDL 5.0 ug/l 8260B 12/21/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Styrene BDL 1.0 ug/l 8260B 12/21/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 12/21/12 1 Tetrachloroethene 3.9 1.0 ug/l 8260B 12/21/12 1 Toluene BDL 5.0 ug/l 8260B 12/21/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,1,1-Trichloroethane 1.7 1.0 ug/l 8260B 12/21/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 Trichloroethene 23. 1.0 ug/l 8260B 12/21/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 12/21/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 12/21/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 12/21/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 12/21/12 1

Surrogate Recovery Toluene-d8 103. % Rec. 8260B 12/21/12 1 Dibromofluoromethane 104. % Rec. 8260B 12/21/12 1 4-Bromofluorobenzene 107. % Rec. 8260B 12/21/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 12/27/12 14:54 Printed: 12/27/12 14:55

Page 9 of 43

Reference 45 Page 224

Page 225: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-05 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : PMW-1

Project # : 1024-1003-01 Collected By : Collection Date : 12/18/12 11:15

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 12/21/12 1 Acrolein BDL 50. ug/l 8260B 12/21/12 1 Acrylonitrile BDL 10. ug/l 8260B 12/21/12 1 Benzene BDL 1.0 ug/l 8260B 12/21/12 1 Bromobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 12/21/12 1 Bromoform BDL 1.0 ug/l 8260B 12/21/12 1 Bromomethane BDL 5.0 ug/l 8260B 12/21/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 12/21/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 12/21/12 1 Chloroethane BDL 5.0 ug/l 8260B 12/21/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 12/21/12 1 Chloroform BDL 5.0 ug/l 8260B 12/21/12 1 Chloromethane BDL 2.5 ug/l 8260B 12/21/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 12/21/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 12/21/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 12/21/12 1 Dibromomethane BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 12/21/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 12/21/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 12/21/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 12/21/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 10 of 43

Reference 45 Page 225

Page 226: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-05 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : PMW-1

Project # : 1024-1003-01 Collected By : Collection Date : 12/18/12 11:15

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 12/21/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 12/21/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 12/21/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 12/21/12 1 Naphthalene BDL 5.0 ug/l 8260B 12/21/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Styrene BDL 1.0 ug/l 8260B 12/21/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 12/21/12 1 Tetrachloroethene 16. 1.0 ug/l 8260B 12/21/12 1 Toluene BDL 5.0 ug/l 8260B 12/21/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 Trichloroethene 6.4 1.0 ug/l 8260B 12/21/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 12/21/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 12/21/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 12/21/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 12/21/12 1

Surrogate Recovery Toluene-d8 104. % Rec. 8260B 12/21/12 1 Dibromofluoromethane 111. % Rec. 8260B 12/21/12 1 4-Bromofluorobenzene 105. % Rec. 8260B 12/21/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 12/27/12 14:54 Printed: 12/27/12 14:55

Page 11 of 43

Reference 45 Page 226

Page 227: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-06 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : MW-10

Project # : 1024-1003-01 Collected By : Collection Date : 12/19/12 09:40

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 12/21/12 1 Acrolein BDL 50. ug/l 8260B 12/21/12 1 Acrylonitrile BDL 10. ug/l 8260B 12/21/12 1 Benzene BDL 1.0 ug/l 8260B 12/21/12 1 Bromobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 12/21/12 1 Bromoform BDL 1.0 ug/l 8260B 12/21/12 1 Bromomethane BDL 5.0 ug/l 8260B 12/21/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 12/21/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 12/21/12 1 Chloroethane BDL 5.0 ug/l 8260B 12/21/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 12/21/12 1 Chloroform 12. 5.0 ug/l 8260B 12/21/12 1 Chloromethane BDL 2.5 ug/l 8260B 12/21/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 12/21/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 12/21/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 12/21/12 1 Dibromomethane BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 12/21/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 12/21/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 12/21/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 12/21/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 12 of 43

Reference 45 Page 227

Page 228: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-06 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : MW-10

Project # : 1024-1003-01 Collected By : Collection Date : 12/19/12 09:40

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 12/21/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 12/21/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 12/21/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 12/21/12 1 Naphthalene BDL 5.0 ug/l 8260B 12/21/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Styrene BDL 1.0 ug/l 8260B 12/21/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 12/21/12 1 Tetrachloroethene 12. 1.0 ug/l 8260B 12/21/12 1 Toluene BDL 5.0 ug/l 8260B 12/21/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 Trichloroethene 6.2 1.0 ug/l 8260B 12/21/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 12/21/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 12/21/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 12/21/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 12/21/12 1

Surrogate Recovery Toluene-d8 104. % Rec. 8260B 12/21/12 1 Dibromofluoromethane 106. % Rec. 8260B 12/21/12 1 4-Bromofluorobenzene 106. % Rec. 8260B 12/21/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 12/27/12 14:54 Printed: 12/27/12 14:55

Page 13 of 43

Reference 45 Page 228

Page 229: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-07 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : MW-9

Project # : 1024-1003-01 Collected By : Collection Date : 12/19/12 10:10

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 12/21/12 1 Acrolein BDL 50. ug/l 8260B 12/21/12 1 Acrylonitrile BDL 10. ug/l 8260B 12/21/12 1 Benzene BDL 1.0 ug/l 8260B 12/21/12 1 Bromobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 12/21/12 1 Bromoform BDL 1.0 ug/l 8260B 12/21/12 1 Bromomethane BDL 5.0 ug/l 8260B 12/21/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 12/21/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 12/21/12 1 Chloroethane BDL 5.0 ug/l 8260B 12/21/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 12/21/12 1 Chloroform BDL 5.0 ug/l 8260B 12/21/12 1 Chloromethane BDL 2.5 ug/l 8260B 12/21/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 12/21/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 12/21/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 12/21/12 1 Dibromomethane BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 12/21/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 cis-1,2-Dichloroethene 2.6 1.0 ug/l 8260B 12/21/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 12/21/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 12/21/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 12/21/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 14 of 43

Reference 45 Page 229

Page 230: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-07 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : MW-9

Project # : 1024-1003-01 Collected By : Collection Date : 12/19/12 10:10

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 12/21/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 12/21/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 12/21/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 12/21/12 1 Naphthalene BDL 5.0 ug/l 8260B 12/21/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Styrene BDL 1.0 ug/l 8260B 12/21/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 12/21/12 1 Tetrachloroethene 48. 1.0 ug/l 8260B 12/21/12 1 Toluene BDL 5.0 ug/l 8260B 12/21/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 Trichloroethene 13. 1.0 ug/l 8260B 12/21/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 12/21/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 12/21/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 12/21/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 12/21/12 1

Surrogate Recovery Toluene-d8 104. % Rec. 8260B 12/21/12 1 Dibromofluoromethane 105. % Rec. 8260B 12/21/12 1 4-Bromofluorobenzene 101. % Rec. 8260B 12/21/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 12/27/12 14:54 Printed: 12/27/12 14:55

Page 15 of 43

Reference 45 Page 230

Page 231: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-08 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : PMW-6

Project # : 1024-1003-01 Collected By : Collection Date : 12/18/12 13:05

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 12/21/12 1 Acrolein BDL 50. ug/l 8260B 12/21/12 1 Acrylonitrile BDL 10. ug/l 8260B 12/21/12 1 Benzene BDL 1.0 ug/l 8260B 12/21/12 1 Bromobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 12/21/12 1 Bromoform BDL 1.0 ug/l 8260B 12/21/12 1 Bromomethane BDL 5.0 ug/l 8260B 12/21/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Carbon tetrachloride 1.9 1.0 ug/l 8260B 12/21/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 12/21/12 1 Chloroethane BDL 5.0 ug/l 8260B 12/21/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 12/21/12 1 Chloroform 6.0 5.0 ug/l 8260B 12/21/12 1 Chloromethane BDL 2.5 ug/l 8260B 12/21/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 12/21/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 12/21/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 12/21/12 1 Dibromomethane BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 12/21/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 12/21/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 12/21/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 12/21/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 16 of 43

Reference 45 Page 231

Page 232: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-08 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : PMW-6

Project # : 1024-1003-01 Collected By : Collection Date : 12/18/12 13:05

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 12/21/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 12/21/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 12/21/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 12/21/12 1 Naphthalene BDL 5.0 ug/l 8260B 12/21/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Styrene BDL 1.0 ug/l 8260B 12/21/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 12/21/12 1 Tetrachloroethene 8.6 1.0 ug/l 8260B 12/21/12 1 Toluene BDL 5.0 ug/l 8260B 12/21/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,1,1-Trichloroethane 2.4 1.0 ug/l 8260B 12/21/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 Trichloroethene 52. 1.0 ug/l 8260B 12/21/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 12/21/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 12/21/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 12/21/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 12/21/12 1

Surrogate Recovery Toluene-d8 103. % Rec. 8260B 12/21/12 1 Dibromofluoromethane 104. % Rec. 8260B 12/21/12 1 4-Bromofluorobenzene 106. % Rec. 8260B 12/21/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 12/27/12 14:54 Printed: 12/27/12 14:55

Page 17 of 43

Reference 45 Page 232

Page 233: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27, 2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-09 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : MW-12

Project # : 1024-1003-01 Collected By : Collection Date : 12/18/12 10:10

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 12/21/12 1 Acrolein BDL 50. ug/l 8260B 12/21/12 1 Acrylonitrile BDL 10. ug/l 8260B 12/21/12 1 Benzene BDL 1.0 ug/l 8260B 12/21/12 1 Bromobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 12/21/12 1 Bromoform BDL 1.0 ug/l 8260B 12/21/12 1 Bromomethane BDL 5.0 ug/l 8260B 12/21/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Carbon tetrachloride 1.3 1.0 ug/l 8260B 12/21/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 12/21/12 1 Chloroethane BDL 5.0 ug/l 8260B 12/21/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 12/21/12 1 Chloroform 5.3 5.0 ug/l 8260B 12/21/12 1 Chloromethane BDL 2.5 ug/l 8260B 12/21/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 12/21/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 12/21/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 12/21/12 1 Dibromomethane BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 12/21/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 12/21/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 12/21/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 12/21/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 18 of 43

Reference 45 Page 233

Page 234: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27, 2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-09 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : MW-12

Project # : 1024-1003-01 Collected By : Collection Date : 12/18/12 10:10

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 12/21/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 12/21/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 12/21/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 12/21/12 1 Naphthalene BDL 5.0 ug/l 8260B 12/21/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Styrene BDL 1.0 ug/l 8260B 12/21/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 12/21/12 1 Tetrachloroethene 18. 1.0 ug/l 8260B 12/21/12 1 Toluene BDL 5.0 ug/l 8260B 12/21/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 Trichloroethene 9.7 1.0 ug/l 8260B 12/21/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 12/21/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 12/21/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 12/21/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 12/21/12 1

Surrogate Recovery Toluene-d8 104. % Rec. 8260B 12/21/12 1 Dibromofluoromethane 106. % Rec. 8260B 12/21/12 1 4-Bromofluorobenzene 105. % Rec. 8260B 12/21/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 12/27/12 14:54 Printed: 12/27/12 14:55

Page 19 of 43

Reference 45 Page 234

Page 235: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27, 2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-10 Date Received : December 20, 2012 Description : Component Machine

Site ID : COMPONENT MACHINE Sample ID : MW-12 MS

Project # : 1024-1003-01 Collected By : Collection Date : 12/18/12 10:10

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Matrix Spike See QC Report for % Rec. and RPD

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 12/27/12 14:54 Printed: 12/27/12 14:55

Page 20 of 43

Reference 45 Page 235

Page 236: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-11 Date Received : December 20, 2012 Description : Component Machine

Site ID : COMPONENT MACHINE Sample ID : MW-12 MSD

Project # : 1024-1003-01 Collected By : Collection Date : 12/18/12 10:10

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics MSD See QC Report for % Rec and RPD

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 12/27/12 14:54 Printed: 12/27/12 14:55

Page 21 of 43

Reference 45 Page 236

Page 237: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-12 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : MW-13

Project # : 1024-1003-01 Collected By : Collection Date : 12/19/12 12:50

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 12/22/12 1 Acrolein BDL 50. ug/l 8260B 12/22/12 1 Acrylonitrile BDL 10. ug/l 8260B 12/22/12 1 Benzene BDL 1.0 ug/l 8260B 12/22/12 1 Bromobenzene BDL 1.0 ug/l 8260B 12/22/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 12/22/12 1 Bromoform BDL 1.0 ug/l 8260B 12/22/12 1 Bromomethane BDL 5.0 ug/l 8260B 12/22/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 12/22/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 12/22/12 1 Chloroethane BDL 5.0 ug/l 8260B 12/22/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 12/22/12 1 Chloroform 20. 5.0 ug/l 8260B 12/22/12 1 Chloromethane BDL 2.5 ug/l 8260B 12/22/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 12/22/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 12/22/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 12/22/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 12/22/12 1 Dibromomethane BDL 1.0 ug/l 8260B 12/22/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 12/22/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 12/22/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 12/22/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 12/22/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/22/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/22/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 12/22/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 12/22/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 12/22/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/22/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/22/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 12/22/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 12/22/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 12/22/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 12/22/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 22 of 43

Reference 45 Page 237

Page 238: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-12 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : MW-13

Project # : 1024-1003-01 Collected By : Collection Date : 12/19/12 12:50

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 12/22/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 12/22/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 12/22/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 12/22/12 1 Naphthalene BDL 5.0 ug/l 8260B 12/22/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 Styrene BDL 1.0 ug/l 8260B 12/22/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/22/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/22/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 12/22/12 1 Tetrachloroethene 4.2 1.0 ug/l 8260B 12/22/12 1 Toluene BDL 5.0 ug/l 8260B 12/22/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 12/22/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 12/22/12 1 Trichloroethene 3.6 1.0 ug/l 8260B 12/22/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 12/22/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 12/22/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 12/22/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 12/22/12 1

Surrogate Recovery Toluene-d8 103. % Rec. 8260B 12/22/12 1 Dibromofluoromethane 106. % Rec. 8260B 12/22/12 1 4-Bromofluorobenzene 102. % Rec. 8260B 12/22/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 12/27/12 14:54 Printed: 12/27/12 14:55

Page 23 of 43

Reference 45 Page 238

Page 239: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-13 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : MW-14

Project # : 1024-1003-01 Collected By : Collection Date : 12/19/12 11:55

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 12/22/12 1 Acrolein BDL 50. ug/l 8260B 12/22/12 1 Acrylonitrile BDL 10. ug/l 8260B 12/22/12 1 Benzene BDL 1.0 ug/l 8260B 12/22/12 1 Bromobenzene BDL 1.0 ug/l 8260B 12/22/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 12/22/12 1 Bromoform BDL 1.0 ug/l 8260B 12/22/12 1 Bromomethane BDL 5.0 ug/l 8260B 12/22/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 12/22/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 12/22/12 1 Chloroethane BDL 5.0 ug/l 8260B 12/22/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 12/22/12 1 Chloroform BDL 5.0 ug/l 8260B 12/22/12 1 Chloromethane BDL 2.5 ug/l 8260B 12/22/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 12/22/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 12/22/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 12/22/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 12/22/12 1 Dibromomethane BDL 1.0 ug/l 8260B 12/22/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 12/22/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 12/22/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 12/22/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 12/22/12 1 cis-1,2-Dichloroethene 1.1 1.0 ug/l 8260B 12/22/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/22/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 12/22/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 12/22/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 12/22/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/22/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/22/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 12/22/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 12/22/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 12/22/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 12/22/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 24 of 43

Reference 45 Page 239

Page 240: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-13 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : MW-14

Project # : 1024-1003-01 Collected By : Collection Date : 12/19/12 11:55

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 12/22/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 12/22/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 12/22/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 12/22/12 1 Naphthalene BDL 5.0 ug/l 8260B 12/22/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 Styrene BDL 1.0 ug/l 8260B 12/22/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/22/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/22/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 12/22/12 1 Tetrachloroethene 48. 1.0 ug/l 8260B 12/22/12 1 Toluene BDL 5.0 ug/l 8260B 12/22/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,1,1-Trichloroethane 2.8 1.0 ug/l 8260B 12/22/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 12/22/12 1 Trichloroethene 55. 1.0 ug/l 8260B 12/22/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 12/22/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 12/22/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 12/22/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 12/22/12 1

Surrogate Recovery Toluene-d8 104. % Rec. 8260B 12/22/12 1 Dibromofluoromethane 119. % Rec. 8260B 12/22/12 1 4-Bromofluorobenzene 101. % Rec. 8260B 12/22/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 12/27/12 14:54 Printed: 12/27/12 14:55

Page 25 of 43

Reference 45 Page 240

Page 241: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-14 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : MW-15

Project # : 1024-1003-01 Collected By : Collection Date : 12/19/12 11:20

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 12/22/12 1 Acrolein BDL 50. ug/l 8260B 12/22/12 1 Acrylonitrile BDL 10. ug/l 8260B 12/22/12 1 Benzene BDL 1.0 ug/l 8260B 12/22/12 1 Bromobenzene BDL 1.0 ug/l 8260B 12/22/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 12/22/12 1 Bromoform BDL 1.0 ug/l 8260B 12/22/12 1 Bromomethane BDL 5.0 ug/l 8260B 12/22/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 12/22/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 12/22/12 1 Chloroethane BDL 5.0 ug/l 8260B 12/22/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 12/22/12 1 Chloroform BDL 5.0 ug/l 8260B 12/22/12 1 Chloromethane BDL 2.5 ug/l 8260B 12/22/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 12/22/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 12/22/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 12/22/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 12/22/12 1 Dibromomethane BDL 1.0 ug/l 8260B 12/22/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 12/22/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 12/22/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 12/22/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 12/22/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/22/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/22/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 12/22/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 12/22/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 12/22/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/22/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/22/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 12/22/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 12/22/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 12/22/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 12/22/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 26 of 43

Reference 45 Page 241

Page 242: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-14 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : MW-15

Project # : 1024-1003-01 Collected By : Collection Date : 12/19/12 11:20

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 12/22/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 12/22/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 12/22/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 12/22/12 1 Naphthalene BDL 5.0 ug/l 8260B 12/22/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 Styrene BDL 1.0 ug/l 8260B 12/22/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/22/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/22/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 12/22/12 1 Tetrachloroethene 76. 1.0 ug/l 8260B 12/22/12 1 Toluene BDL 5.0 ug/l 8260B 12/22/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,1,1-Trichloroethane 3.8 1.0 ug/l 8260B 12/22/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 12/22/12 1 Trichloroethene 66. 1.0 ug/l 8260B 12/22/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 12/22/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 12/22/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 12/22/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 12/22/12 1

Surrogate Recovery Toluene-d8 101. % Rec. 8260B 12/22/12 1 Dibromofluoromethane 94.7 % Rec. 8260B 12/22/12 1 4-Bromofluorobenzene 104. % Rec. 8260B 12/22/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 12/27/12 14:54 Printed: 12/27/12 14:55

Page 27 of 43

Reference 45 Page 242

Page 243: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-15 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : MW-16

Project # : 1024-1003-01 Collected By : Collection Date : 12/19/12 10:45

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 12/22/12 1 Acrolein BDL 50. ug/l 8260B 12/22/12 1 Acrylonitrile BDL 10. ug/l 8260B 12/22/12 1 Benzene BDL 1.0 ug/l 8260B 12/22/12 1 Bromobenzene BDL 1.0 ug/l 8260B 12/22/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 12/22/12 1 Bromoform BDL 1.0 ug/l 8260B 12/22/12 1 Bromomethane BDL 5.0 ug/l 8260B 12/22/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 12/22/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 12/22/12 1 Chloroethane BDL 5.0 ug/l 8260B 12/22/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 12/22/12 1 Chloroform BDL 5.0 ug/l 8260B 12/22/12 1 Chloromethane BDL 2.5 ug/l 8260B 12/22/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 12/22/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 12/22/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 12/22/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 12/22/12 1 Dibromomethane BDL 1.0 ug/l 8260B 12/22/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 12/22/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 12/22/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 12/22/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 12/22/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/22/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/22/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 12/22/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 12/22/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 12/22/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/22/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/22/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 12/22/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 12/22/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 12/22/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 12/22/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 28 of 43

Reference 45 Page 243

Page 244: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-15 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : MW-16

Project # : 1024-1003-01 Collected By : Collection Date : 12/19/12 10:45

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 12/22/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 12/22/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 12/22/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 12/22/12 1 Naphthalene BDL 5.0 ug/l 8260B 12/22/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 Styrene BDL 1.0 ug/l 8260B 12/22/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/22/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/22/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 12/22/12 1 Tetrachloroethene 3.5 1.0 ug/l 8260B 12/22/12 1 Toluene BDL 5.0 ug/l 8260B 12/22/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,1,1-Trichloroethane 11. 1.0 ug/l 8260B 12/22/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 12/22/12 1 Trichloroethene 84. 1.0 ug/l 8260B 12/22/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 12/22/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 12/22/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 12/22/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 12/22/12 1

Surrogate Recovery Toluene-d8 102. % Rec. 8260B 12/22/12 1 Dibromofluoromethane 107. % Rec. 8260B 12/22/12 1 4-Bromofluorobenzene 103. % Rec. 8260B 12/22/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 12/27/12 14:54 Printed: 12/27/12 14:55

Page 29 of 43

Reference 45 Page 244

Page 245: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-16 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : DUP

Project # : 1024-1003-01 Collected By : Collection Date : 12/18/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 12/22/12 1 Acrolein BDL 50. ug/l 8260B 12/22/12 1 Acrylonitrile BDL 10. ug/l 8260B 12/22/12 1 Benzene BDL 1.0 ug/l 8260B 12/22/12 1 Bromobenzene BDL 1.0 ug/l 8260B 12/22/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 12/22/12 1 Bromoform BDL 1.0 ug/l 8260B 12/22/12 1 Bromomethane BDL 5.0 ug/l 8260B 12/22/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 12/22/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 12/22/12 1 Chloroethane BDL 5.0 ug/l 8260B 12/22/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 12/22/12 1 Chloroform BDL 5.0 ug/l 8260B 12/22/12 1 Chloromethane BDL 2.5 ug/l 8260B 12/22/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 12/22/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 12/22/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 12/22/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 12/22/12 1 Dibromomethane BDL 1.0 ug/l 8260B 12/22/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 12/22/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 12/22/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 12/22/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 12/22/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/22/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/22/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 12/22/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 12/22/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 12/22/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/22/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/22/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 12/22/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 12/22/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 12/22/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 12/22/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

Page 30 of 43

Reference 45 Page 245

Page 246: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-16 Date Received : December 20, 2012 Description : Component Machine

Site ID : Sample ID : DUP

Project # : 1024-1003-01 Collected By : Collection Date : 12/18/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 12/22/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 12/22/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 12/22/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 12/22/12 1 Naphthalene BDL 5.0 ug/l 8260B 12/22/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 Styrene BDL 1.0 ug/l 8260B 12/22/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/22/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/22/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 12/22/12 1 Tetrachloroethene 17. 1.0 ug/l 8260B 12/22/12 1 Toluene BDL 5.0 ug/l 8260B 12/22/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 12/22/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 12/22/12 1 Trichloroethene 6.7 1.0 ug/l 8260B 12/22/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 12/22/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 12/22/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 12/22/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 12/22/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 12/22/12 1

Surrogate Recovery Toluene-d8 103. % Rec. 8260B 12/22/12 1 Dibromofluoromethane 104. % Rec. 8260B 12/22/12 1 4-Bromofluorobenzene 101. % Rec. 8260B 12/22/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 12/27/12 14:54 Printed: 12/27/12 14:55

Page 31 of 43

Reference 45 Page 246

Page 247: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-17 Date Received : December 20, 2012 Description : Component Machine

Site ID : COMPONENT MACHINE Sample ID : TRIPBLANK

Project # : 1024-1003-01 Collected By : Collection Date : 12/18/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

Volatile Organics Acetone BDL 50. ug/l 8260B 12/21/12 1 Acrolein BDL 50. ug/l 8260B 12/21/12 1 Acrylonitrile BDL 10. ug/l 8260B 12/21/12 1 Benzene BDL 1.0 ug/l 8260B 12/21/12 1 Bromobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Bromodichloromethane BDL 1.0 ug/l 8260B 12/21/12 1 Bromoform BDL 1.0 ug/l 8260B 12/21/12 1 Bromomethane BDL 5.0 ug/l 8260B 12/21/12 1 n-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 sec-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 tert-Butylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Carbon tetrachloride BDL 1.0 ug/l 8260B 12/21/12 1 Chlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Chlorodibromomethane BDL 1.0 ug/l 8260B 12/21/12 1 Chloroethane BDL 5.0 ug/l 8260B 12/21/12 1 2-Chloroethyl vinyl ether BDL 50. ug/l 8260B 12/21/12 1 Chloroform BDL 5.0 ug/l 8260B 12/21/12 1 Chloromethane BDL 2.5 ug/l 8260B 12/21/12 1 2-Chlorotoluene BDL 1.0 ug/l 8260B 12/21/12 1 4-Chlorotoluene BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dibromo-3-Chloropropane BDL 5.0 ug/l 8260B 12/21/12 1 1,2-Dibromoethane BDL 1.0 ug/l 8260B 12/21/12 1 Dibromomethane BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,3-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,4-Dichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 Dichlorodifluoromethane BDL 5.0 ug/l 8260B 12/21/12 1 1,1-Dichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 cis-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 trans-1,2-Dichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 1,2-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 1,1-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 1,3-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 cis-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 trans-1,3-Dichloropropene BDL 1.0 ug/l 8260B 12/21/12 1 2,2-Dichloropropane BDL 1.0 ug/l 8260B 12/21/12 1 Di-isopropyl ether BDL 1.0 ug/l 8260B 12/21/12 1 Ethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Hexachloro-1,3-butadiene BDL 1.0 ug/l 8260B 12/21/12 1 Isopropylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 p-Isopropyltoluene BDL 1.0 ug/l 8260B 12/21/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL)

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12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970

REPORT OF ANALYSIS Mrs. Wendy Milejczak December 27,2012 Acuity Environmental Solutions 7965 East 106th St. Suite 128 Fishers, IN 46038

ESC Sample # : L612291-17 Date Received : December 20, 2012 Description : Component Machine

Site ID : COMPONENT MACHINE Sample ID : TRIPBLANK

Project # : 1024-1003-01 Collected By : Collection Date : 12/18/12 00:00

Parameter Result Det. Limit Units Method Date Dil.

2-Butanone (MEK) BDL 10. ug/l 8260B 12/21/12 1 Methylene Chloride BDL 5.0 ug/l 8260B 12/21/12 1 4-Methyl-2-pentanone (MIBK) BDL 10. ug/l 8260B 12/21/12 1 Methyl tert-butyl ether BDL 1.0 ug/l 8260B 12/21/12 1 Naphthalene BDL 5.0 ug/l 8260B 12/21/12 1 n-Propylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Styrene BDL 1.0 ug/l 8260B 12/21/12 1 1,1,1,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2,2-Tetrachloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2-Trichlorotrifluoroethane BDL 1.0 ug/l 8260B 12/21/12 1 Tetrachloroethene BDL 1.0 ug/l 8260B 12/21/12 1 Toluene BDL 5.0 ug/l 8260B 12/21/12 1 1,2,3-Trichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,2,4-Trichlorobenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,1,1-Trichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 1,1,2-Trichloroethane BDL 1.0 ug/l 8260B 12/21/12 1 Trichloroethene BDL 1.0 ug/l 8260B 12/21/12 1 Trichlorofluoromethane BDL 5.0 ug/l 8260B 12/21/12 1 1,2,3-Trichloropropane BDL 2.5 ug/l 8260B 12/21/12 1 1,2,4-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,2,3-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 1,3,5-Trimethylbenzene BDL 1.0 ug/l 8260B 12/21/12 1 Vinyl chloride BDL 1.0 ug/l 8260B 12/21/12 1 Xylenes, Total BDL 3.0 ug/l 8260B 12/21/12 1

Surrogate Recovery Toluene-d8 103. % Rec. 8260B 12/21/12 1 Dibromofluoromethane 101. % Rec. 8260B 12/21/12 1 4-Bromofluorobenzene 103. % Rec. 8260B 12/21/12 1

BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. . Reported: 12/27/12 14:54 Printed: 12/27/12 14:55

Page 33 of 43

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Attachment AList of Analytes with QC Qualifiers

Sample Work Sample Run Number Group Type Analyte ID Qualifier ________________ ___________ _______ ________________________________________ __________ __________

L612291-09 WG629303 SAMP 2-Chloroethyl vinyl ether R2492362 J6J3

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Attachment BExplanation of QC Qualifier Codes

Qualifier Meaning __________________ _______________________________________________________________________________

J3 The associated batch QC was outside the established quality control rangefor precision.

J6 The sample matrix interfered with the ability to make any accuratedetermination; spike value is low

Qualifier Report Information

ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program andas required by most certifying bodies including NELAC. In addition to the EPA qualifiers adoptedby ESC, we have implemented ESC qualifiers to provide more information pertaining to our analyticalresults. Each qualifier is designated in the qualifier explanation as either EPA or ESC.Data qualifiers are intended to provide the ESC client with more detailed information concerningthe potential bias of reported data. Because of the wide range of constituents and variety ofmatrices incorporated by most EPA methods,it is common for some compounds to fall outside ofestablished ranges. These exceptions are evaluated and all reported data is valid and useable"unless qualified as 'R' (Rejected)."

DefinitionsAccuracy - The relationship of the observed value of a known sample to the

true value of a known sample. Represented by percent recovery andrelevant to samples such as: control samples, matrix spike recoveries,surrogate recoveries, etc.

Precision - The agreement between a set of samples or between duplicate samples.Relates to how close together the results are and is represented byRelative Percent Differrence.

Surrogate - Organic compounds that are similar in chemical composition, extraction,and chromotography to analytes of interest. The surrogates are used todetermine the probable response of the group of analytes that are chem-ically related to the surrogate compound. Surrogates are added to thesample and carried through all stages of preparation and analyses.

TIC - Tentatively Identified Compound: Compounds detected in samples that arenot target compounds, internal standards, system monitoring compounds,or surrogates.

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Summary of Remarks For Samples Printed12/27/12 at 14:55:34

TSR Signing Reports: 364

Quarterly sampling, always log with QC4 per standing order from client.

Sample: L612291-01 Account: SEABREFIN Received: 12/20/12 10:00 Due Date: 12/28/12 00:00 RPT Date: 12/27/12 14:54 QC4Sample: L612291-02 Account: SEABREFIN Received: 12/20/12 10:00 Due Date: 12/28/12 00:00 RPT Date: 12/27/12 14:54

Sample: L612291-03 Account: SEABREFIN Received: 12/20/12 10:00 Due Date: 12/28/12 00:00 RPT Date: 12/27/12 14:54

Sample: L612291-04 Account: SEABREFIN Received: 12/20/12 10:00 Due Date: 12/28/12 00:00 RPT Date: 12/27/12 14:54

Sample: L612291-05 Account: SEABREFIN Received: 12/20/12 10:00 Due Date: 12/28/12 00:00 RPT Date: 12/27/12 14:54

Sample: L612291-06 Account: SEABREFIN Received: 12/20/12 10:00 Due Date: 12/28/12 00:00 RPT Date: 12/27/12 14:54

Sample: L612291-07 Account: SEABREFIN Received: 12/20/12 10:00 Due Date: 12/28/12 00:00 RPT Date: 12/27/12 14:54

Sample: L612291-08 Account: SEABREFIN Received: 12/20/12 10:00 Due Date: 12/28/12 00:00 RPT Date: 12/27/12 14:54

Sample: L612291-09 Account: SEABREFIN Received: 12/20/12 10:00 Due Date: 12/28/12 00:00 RPT Date: 12/27/12 14:54 MS/MSD this sampleSample: L612291-10 Account: SEABREFIN Received: 12/20/12 10:00 Due Date: 12/28/12 00:00 RPT Date: 12/27/12 14:54

Sample: L612291-11 Account: SEABREFIN Received: 12/20/12 10:00 Due Date: 12/28/12 00:00 RPT Date: 12/27/12 14:54

Sample: L612291-12 Account: SEABREFIN Received: 12/20/12 10:00 Due Date: 12/28/12 00:00 RPT Date: 12/27/12 14:54

Sample: L612291-13 Account: SEABREFIN Received: 12/20/12 10:00 Due Date: 12/28/12 00:00 RPT Date: 12/27/12 14:54

Sample: L612291-14 Account: SEABREFIN Received: 12/20/12 10:00 Due Date: 12/28/12 00:00 RPT Date: 12/27/12 14:54

Sample: L612291-15 Account: SEABREFIN Received: 12/20/12 10:00 Due Date: 12/28/12 00:00 RPT Date: 12/27/12 14:54

Sample: L612291-16 Account: SEABREFIN Received: 12/20/12 10:00 Due Date: 12/28/12 00:00 RPT Date: 12/27/12 14:54

Sample: L612291-17 Account: SEABREFIN Received: 12/20/12 10:00 Due Date: 12/28/12 00:00 RPT Date: 12/27/12 14:54

Reference 45 Page 251

Page 252: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 December 27, 2012

L612291

Laboratory BlankAnalyte Result Units % Rec Limit Batch Date Analyzed

1,1,1,2-Tetrachloroethane < .001 mg/l WG629303 12/21/12 17:26 1,1,1-Trichloroethane < .001 mg/l WG629303 12/21/12 17:26 1,1,2,2-Tetrachloroethane < .001 mg/l WG629303 12/21/12 17:26 1,1,2-Trichloroethane < .001 mg/l WG629303 12/21/12 17:26 1,1,2-Trichlorotrifluoroethane < .001 mg/l WG629303 12/21/12 17:26 1,1-Dichloroethane < .001 mg/l WG629303 12/21/12 17:26 1,1-Dichloroethene < .001 mg/l WG629303 12/21/12 17:26 1,1-Dichloropropene < .001 mg/l WG629303 12/21/12 17:26 1,2,3-Trichlorobenzene < .001 mg/l WG629303 12/21/12 17:26 1,2,3-Trichloropropane < .001 mg/l WG629303 12/21/12 17:26 1,2,3-Trimethylbenzene < .001 mg/l WG629303 12/21/12 17:26 1,2,4-Trichlorobenzene < .001 mg/l WG629303 12/21/12 17:26 1,2,4-Trimethylbenzene < .001 mg/l WG629303 12/21/12 17:26 1,2-Dibromo-3-Chloropropane < .005 mg/l WG629303 12/21/12 17:26 1,2-Dibromoethane < .001 mg/l WG629303 12/21/12 17:26 1,2-Dichlorobenzene < .001 mg/l WG629303 12/21/12 17:26 1,2-Dichloroethane < .001 mg/l WG629303 12/21/12 17:26 1,2-Dichloropropane < .001 mg/l WG629303 12/21/12 17:26 1,3,5-Trimethylbenzene < .001 mg/l WG629303 12/21/12 17:26 1,3-Dichlorobenzene < .001 mg/l WG629303 12/21/12 17:26 1,3-Dichloropropane < .001 mg/l WG629303 12/21/12 17:26 1,4-Dichlorobenzene < .001 mg/l WG629303 12/21/12 17:26 2,2-Dichloropropane < .001 mg/l WG629303 12/21/12 17:26 2-Butanone (MEK) < .01 mg/l WG629303 12/21/12 17:26 2-Chloroethyl vinyl ether < .05 mg/l WG629303 12/21/12 17:26 2-Chlorotoluene < .001 mg/l WG629303 12/21/12 17:26 4-Chlorotoluene < .001 mg/l WG629303 12/21/12 17:26 4-Methyl-2-pentanone (MIBK) < .01 mg/l WG629303 12/21/12 17:26 Acetone < .05 mg/l WG629303 12/21/12 17:26 Acrolein < .025 mg/l WG629303 12/21/12 17:26 Acrylonitrile < .01 mg/l WG629303 12/21/12 17:26 Benzene < .001 mg/l WG629303 12/21/12 17:26 Bromobenzene < .001 mg/l WG629303 12/21/12 17:26 Bromodichloromethane < .001 mg/l WG629303 12/21/12 17:26 Bromoform < .001 mg/l WG629303 12/21/12 17:26 Bromomethane < .005 mg/l WG629303 12/21/12 17:26 Carbon tetrachloride < .001 mg/l WG629303 12/21/12 17:26 Chlorobenzene < .001 mg/l WG629303 12/21/12 17:26 Chlorodibromomethane < .001 mg/l WG629303 12/21/12 17:26 Chloroethane < .005 mg/l WG629303 12/21/12 17:26 Chloroform < .005 mg/l WG629303 12/21/12 17:26 Chloromethane < .0025 mg/l WG629303 12/21/12 17:26 cis-1,2-Dichloroethene < .001 mg/l WG629303 12/21/12 17:26 cis-1,3-Dichloropropene < .001 mg/l WG629303 12/21/12 17:26 Di-isopropyl ether < .001 mg/l WG629303 12/21/12 17:26 Dibromomethane < .001 mg/l WG629303 12/21/12 17:26 Dichlorodifluoromethane < .005 mg/l WG629303 12/21/12 17:26 Ethylbenzene < .001 mg/l WG629303 12/21/12 17:26 Hexachloro-1,3-butadiene < .001 mg/l WG629303 12/21/12 17:26 Isopropylbenzene < .001 mg/l WG629303 12/21/12 17:26 Methyl tert-butyl ether < .001 mg/l WG629303 12/21/12 17:26 Methylene Chloride < .005 mg/l WG629303 12/21/12 17:26 n-Butylbenzene < .001 mg/l WG629303 12/21/12 17:26 n-Propylbenzene < .001 mg/l WG629303 12/21/12 17:26 Naphthalene < .005 mg/l WG629303 12/21/12 17:26 p-Isopropyltoluene < .001 mg/l WG629303 12/21/12 17:26 sec-Butylbenzene < .001 mg/l WG629303 12/21/12 17:26 Styrene < .001 mg/l WG629303 12/21/12 17:26 tert-Butylbenzene < .001 mg/l WG629303 12/21/12 17:26

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 36 of 43

Reference 45 Page 252

Page 253: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 December 27, 2012

L612291

Laboratory BlankAnalyte Result Units % Rec Limit Batch Date Analyzed

Tetrachloroethene < .001 mg/l WG629303 12/21/12 17:26 Toluene < .005 mg/l WG629303 12/21/12 17:26 trans-1,2-Dichloroethene < .001 mg/l WG629303 12/21/12 17:26 trans-1,3-Dichloropropene < .001 mg/l WG629303 12/21/12 17:26 Trichloroethene < .001 mg/l WG629303 12/21/12 17:26 Trichlorofluoromethane < .005 mg/l WG629303 12/21/12 17:26 Vinyl chloride < .001 mg/l WG629303 12/21/12 17:26 Xylenes, Total < .003 mg/l WG629303 12/21/12 17:26 4-Bromofluorobenzene % Rec. 100.9 82-120 WG629303 12/21/12 17:26 Dibromofluoromethane % Rec. 99.41 82-126 WG629303 12/21/12 17:26 Toluene-d8 % Rec. 104.1 92-112 WG629303 12/21/12 17:26

Laboratory Control SampleAnalyte Units Known Val Result % Rec Limit Batch

1,1,1,2-Tetrachloroethane mg/l .025 0.0264 106. 77-128 WG629303 1,1,1-Trichloroethane mg/l .025 0.0256 103. 71-126 WG629303 1,1,2,2-Tetrachloroethane mg/l .025 0.0260 104. 78-130 WG629303 1,1,2-Trichloroethane mg/l .025 0.0264 106. 81-121 WG629303 1,1,2-Trichlorotrifluoroethane mg/l .025 0.0252 101. 53-143 WG629303 1,1-Dichloroethane mg/l .025 0.0261 105. 73-123 WG629303 1,1-Dichloroethene mg/l .025 0.0247 98.9 54-134 WG629303 1,1-Dichloropropene mg/l .025 0.0248 99.1 67-127 WG629303 1,2,3-Trichlorobenzene mg/l .025 0.0286 114. 77-130 WG629303 1,2,3-Trichloropropane mg/l .025 0.0282 113. 68-130 WG629303 1,2,3-Trimethylbenzene mg/l .025 0.0268 107. 77-126 WG629303 1,2,4-Trichlorobenzene mg/l .025 0.0288 115. 76-127 WG629303 1,2,4-Trimethylbenzene mg/l .025 0.0269 107. 77-129 WG629303 1,2-Dibromo-3-Chloropropane mg/l .025 0.0250 100. 55-142 WG629303 1,2-Dibromoethane mg/l .025 0.0266 107. 78-124 WG629303 1,2-Dichlorobenzene mg/l .025 0.0273 109. 82-121 WG629303 1,2-Dichloroethane mg/l .025 0.0251 100. 69-128 WG629303 1,2-Dichloropropane mg/l .025 0.0270 108. 77-121 WG629303 1,3,5-Trimethylbenzene mg/l .025 0.0269 108. 78-127 WG629303 1,3-Dichlorobenzene mg/l .025 0.0277 111. 77-127 WG629303 1,3-Dichloropropane mg/l .025 0.0260 104. 78-117 WG629303 1,4-Dichlorobenzene mg/l .025 0.0259 104. 79-117 WG629303 2,2-Dichloropropane mg/l .025 0.0246 98.5 63-130 WG629303 2-Butanone (MEK) mg/l .125 0.110 88.1 58-144 WG629303 2-Chloroethyl vinyl ether mg/l .125 0.211 169. 26-172 WG629303 2-Chlorotoluene mg/l .025 0.0269 108. 78-123 WG629303 4-Chlorotoluene mg/l .025 0.0274 110. 78-122 WG629303 4-Methyl-2-pentanone (MIBK) mg/l .125 0.138 111. 58-147 WG629303 Acetone mg/l .125 0.110 88.1 49-153 WG629303 Acrolein mg/l .125 0.0873 69.8 10-181 WG629303 Acrylonitrile mg/l .125 0.130 104. 53-153 WG629303 Benzene mg/l .025 0.0253 101. 72-119 WG629303 Bromobenzene mg/l .025 0.0265 106. 76-121 WG629303 Bromodichloromethane mg/l .025 0.0265 106. 75-127 WG629303 Bromoform mg/l .025 0.0256 103. 61-136 WG629303 Bromomethane mg/l .025 0.0261 104. 42-172 WG629303 Carbon tetrachloride mg/l .025 0.0233 93.1 63-129 WG629303 Chlorobenzene mg/l .025 0.0267 107. 78-123 WG629303 Chlorodibromomethane mg/l .025 0.0257 103. 73-128 WG629303 Chloroethane mg/l .025 0.0254 101. 52-164 WG629303 Chloroform mg/l .025 0.0262 105. 76-122 WG629303 Chloromethane mg/l .025 0.0263 105. 50-141 WG629303 cis-1,2-Dichloroethene mg/l .025 0.0267 107. 75-121 WG629303 cis-1,3-Dichloropropene mg/l .025 0.0271 108. 74-124 WG629303

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 37 of 43

Reference 45 Page 253

Page 254: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 December 27, 2012

L612291

Laboratory Control SampleAnalyte Units Known Val Result % Rec Limit Batch

Di-isopropyl ether mg/l .025 0.0266 106. 66-129 WG629303 Dibromomethane mg/l .025 0.0268 107. 77-124 WG629303 Dichlorodifluoromethane mg/l .025 0.0235 94.1 33-173 WG629303 Ethylbenzene mg/l .025 0.0267 107. 77-124 WG629303 Hexachloro-1,3-butadiene mg/l .025 0.0278 111. 71-134 WG629303 Isopropylbenzene mg/l .025 0.0264 106. 74-126 WG629303 Methyl tert-butyl ether mg/l .025 0.0264 106. 67-127 WG629303 Methylene Chloride mg/l .025 0.0255 102. 67-122 WG629303 n-Butylbenzene mg/l .025 0.0274 110. 74-130 WG629303 n-Propylbenzene mg/l .025 0.0268 107. 77-125 WG629303 Naphthalene mg/l .025 0.0277 111. 70-134 WG629303 p-Isopropyltoluene mg/l .025 0.0271 108. 77-132 WG629303 sec-Butylbenzene mg/l .025 0.0266 107. 77-130 WG629303 Styrene mg/l .025 0.0282 113. 69-145 WG629303 tert-Butylbenzene mg/l .025 0.0266 107. 76-131 WG629303 Tetrachloroethene mg/l .025 0.0255 102. 69-131 WG629303 Toluene mg/l .025 0.0260 104. 75-114 WG629303 trans-1,2-Dichloroethene mg/l .025 0.0258 103. 63-127 WG629303 trans-1,3-Dichloropropene mg/l .025 0.0281 112. 69-124 WG629303 Trichloroethene mg/l .025 0.0268 107. 69-131 WG629303 Trichlorofluoromethane mg/l .025 0.0250 100. 53-161 WG629303 Vinyl chloride mg/l .025 0.0257 103. 55-142 WG629303 Xylenes, Total mg/l .075 0.0802 107. 77-123 WG629303 4-Bromofluorobenzene 102.3 82-120 WG629303 Dibromofluoromethane 96.28 82-126 WG629303 Toluene-d8 104.5 92-112 WG629303

Laboratory Control Sample DuplicateAnalyte Units Result Ref %Rec Limit RPD Limit Batch

1,1,1,2-Tetrachloroethane mg/l 0.0244 0.0264 98.0 77-128 7.99 20 WG629303 1,1,1-Trichloroethane mg/l 0.0245 0.0256 98.0 71-126 4.61 20 WG629303 1,1,2,2-Tetrachloroethane mg/l 0.0254 0.0260 101. 78-130 2.40 20 WG629303 1,1,2-Trichloroethane mg/l 0.0246 0.0264 98.0 81-121 6.87 20 WG629303 1,1,2-Trichlorotrifluoroethane mg/l 0.0240 0.0252 96.0 53-143 5.17 20 WG629303 1,1-Dichloroethane mg/l 0.0259 0.0261 104. 73-123 0.970 20 WG629303 1,1-Dichloroethene mg/l 0.0242 0.0247 97.0 54-134 2.27 20 WG629303 1,1-Dichloropropene mg/l 0.0239 0.0248 96.0 67-127 3.59 20 WG629303 1,2,3-Trichlorobenzene mg/l 0.0264 0.0286 106. 77-130 7.92 20 WG629303 1,2,3-Trichloropropane mg/l 0.0272 0.0282 109. 68-130 3.45 20 WG629303 1,2,3-Trimethylbenzene mg/l 0.0244 0.0268 98.0 77-126 9.32 20 WG629303 1,2,4-Trichlorobenzene mg/l 0.0265 0.0288 106. 76-127 8.43 20 WG629303 1,2,4-Trimethylbenzene mg/l 0.0250 0.0269 100. 77-129 7.35 20 WG629303 1,2-Dibromo-3-Chloropropane mg/l 0.0245 0.0250 98.0 55-142 2.12 20 WG629303 1,2-Dibromoethane mg/l 0.0251 0.0266 100. 78-124 5.91 20 WG629303 1,2-Dichlorobenzene mg/l 0.0256 0.0273 102. 82-121 6.39 20 WG629303 1,2-Dichloroethane mg/l 0.0251 0.0251 100. 69-128 0.140 20 WG629303 1,2-Dichloropropane mg/l 0.0257 0.0270 103. 77-121 5.03 20 WG629303 1,3,5-Trimethylbenzene mg/l 0.0249 0.0269 100. 78-127 7.54 20 WG629303 1,3-Dichlorobenzene mg/l 0.0264 0.0277 106. 77-127 4.62 20 WG629303 1,3-Dichloropropane mg/l 0.0247 0.0260 99.0 78-117 4.97 20 WG629303 1,4-Dichlorobenzene mg/l 0.0234 0.0259 94.0 79-117 9.99 20 WG629303 2,2-Dichloropropane mg/l 0.0260 0.0246 104. 63-130 5.29 20 WG629303 2-Butanone (MEK) mg/l 0.116 0.110 93.0 58-144 5.22 20 WG629303 2-Chloroethyl vinyl ether mg/l 0.197 0.211 157. 26-172 7.09 22 WG629303 2-Chlorotoluene mg/l 0.0251 0.0269 100. 78-123 6.94 20 WG629303 4-Chlorotoluene mg/l 0.0253 0.0274 101. 78-122 8.18 20 WG629303 4-Methyl-2-pentanone (MIBK) mg/l 0.139 0.138 111. 58-147 0.290 20 WG629303 Acetone mg/l 0.121 0.110 97.0 49-153 9.87 21 WG629303

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 38 of 43

Reference 45 Page 254

Page 255: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 December 27, 2012

L612291

Laboratory Control Sample DuplicateAnalyte Units Result Ref %Rec Limit RPD Limit Batch

Acrolein mg/l 0.0982 0.0873 78.0 10-181 11.8 30 WG629303 Acrylonitrile mg/l 0.137 0.130 110. 53-153 5.40 20 WG629303 Benzene mg/l 0.0245 0.0253 98.0 72-119 3.37 20 WG629303 Bromobenzene mg/l 0.0249 0.0265 99.0 76-121 6.35 20 WG629303 Bromodichloromethane mg/l 0.0251 0.0265 100. 75-127 5.30 20 WG629303 Bromoform mg/l 0.0254 0.0256 102. 61-136 0.860 20 WG629303 Bromomethane mg/l 0.0252 0.0261 101. 42-172 3.40 20 WG629303 Carbon tetrachloride mg/l 0.0229 0.0233 92.0 63-129 1.75 20 WG629303 Chlorobenzene mg/l 0.0243 0.0267 97.0 78-123 9.08 20 WG629303 Chlorodibromomethane mg/l 0.0242 0.0257 97.0 73-128 5.78 20 WG629303 Chloroethane mg/l 0.0251 0.0254 100. 52-164 1.00 20 WG629303 Chloroform mg/l 0.0257 0.0262 103. 76-122 1.88 20 WG629303 Chloromethane mg/l 0.0250 0.0263 100. 50-141 5.06 20 WG629303 cis-1,2-Dichloroethene mg/l 0.0261 0.0267 104. 75-121 2.17 20 WG629303 cis-1,3-Dichloropropene mg/l 0.0251 0.0271 100. 74-124 7.54 20 WG629303 Di-isopropyl ether mg/l 0.0261 0.0266 104. 66-129 1.90 20 WG629303 Dibromomethane mg/l 0.0257 0.0268 103. 77-124 4.28 20 WG629303 Dichlorodifluoromethane mg/l 0.0227 0.0235 91.0 33-173 3.64 20 WG629303 Ethylbenzene mg/l 0.0247 0.0267 99.0 77-124 7.87 20 WG629303 Hexachloro-1,3-butadiene mg/l 0.0249 0.0278 100. 71-134 10.7 20 WG629303 Isopropylbenzene mg/l 0.0243 0.0264 97.0 74-126 8.28 20 WG629303 Methyl tert-butyl ether mg/l 0.0264 0.0264 106. 67-127 0.230 20 WG629303 Methylene Chloride mg/l 0.0250 0.0255 100. 67-122 2.00 20 WG629303 n-Butylbenzene mg/l 0.0250 0.0274 100. 74-130 9.32 20 WG629303 n-Propylbenzene mg/l 0.0248 0.0268 99.0 77-125 8.10 20 WG629303 Naphthalene mg/l 0.0263 0.0277 105. 70-134 5.16 20 WG629303 p-Isopropyltoluene mg/l 0.0253 0.0271 101. 77-132 6.69 20 WG629303 sec-Butylbenzene mg/l 0.0249 0.0266 100. 77-130 6.61 20 WG629303 Styrene mg/l 0.0263 0.0282 105. 69-145 7.00 20 WG629303 tert-Butylbenzene mg/l 0.0254 0.0266 101. 76-131 4.86 20 WG629303 Tetrachloroethene mg/l 0.0235 0.0255 94.0 69-131 8.08 20 WG629303 Toluene mg/l 0.0241 0.0260 96.0 75-114 7.67 20 WG629303 trans-1,2-Dichloroethene mg/l 0.0256 0.0258 102. 63-127 0.510 20 WG629303 trans-1,3-Dichloropropene mg/l 0.0263 0.0281 105. 69-124 6.55 20 WG629303 Trichloroethene mg/l 0.0252 0.0268 101. 69-131 6.15 20 WG629303 Trichlorofluoromethane mg/l 0.0239 0.0250 95.0 53-161 4.72 20 WG629303 Vinyl chloride mg/l 0.0242 0.0257 97.0 55-142 5.85 20 WG629303 Xylenes, Total mg/l 0.0737 0.0802 98.0 77-123 8.43 20 WG629303 4-Bromofluorobenzene 100.7 82-120 WG629303 Dibromofluoromethane 99.19 82-126 WG629303 Toluene-d8 104.2 92-112 WG629303

Matrix SpikeAnalyte Units MS Res Ref Res TV % Rec Limit Ref Samp Batch

1,1,1,2-Tetrachloroethane mg/l 0.0244 0 .025 97.4 71-130 L612291-09 WG629303 1,1,1-Trichloroethane mg/l 0.0263 0 .025 105. 58-137 L612291-09 WG629303 1,1,2,2-Tetrachloroethane mg/l 0.0238 0 .025 95.3 64-149 L612291-09 WG629303 1,1,2-Trichloroethane mg/l 0.0235 0 .025 93.9 73-128 L612291-09 WG629303 1,1,2-Trichlorotrifluoroethane mg/l 0.0262 0 .025 105. 36-159 L612291-09 WG629303 1,1-Dichloroethane mg/l 0.0244 0 .025 97.4 58-133 L612291-09 WG629303 1,1-Dichloroethene mg/l 0.0237 0 .025 94.9 32-152 L612291-09 WG629303 1,1-Dichloropropene mg/l 0.0238 0 .025 95.3 50-140 L612291-09 WG629303 1,2,3-Trichlorobenzene mg/l 0.0258 0 .025 103. 68-135 L612291-09 WG629303 1,2,3-Trichloropropane mg/l 0.0245 0 .025 97.9 74-137 L612291-09 WG629303 1,2,3-Trimethylbenzene mg/l 0.0241 0 .025 96.3 67-133 L612291-09 WG629303 1,2,4-Trichlorobenzene mg/l 0.0271 0 .025 108. 67-133 L612291-09 WG629303 1,2,4-Trimethylbenzene mg/l 0.0257 0 .025 103. 62-141 L612291-09 WG629303 1,2-Dibromo-3-Chloropropane mg/l 0.0218 0 .025 87.2 55-148 L612291-09 WG629303

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 39 of 43

Reference 45 Page 255

Page 256: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 December 27, 2012

L612291

Matrix SpikeAnalyte Units MS Res Ref Res TV % Rec Limit Ref Samp Batch

1,2-Dibromoethane mg/l 0.0231 0 .025 92.3 71-129 L612291-09 WG629303 1,2-Dichlorobenzene mg/l 0.0249 0 .025 99.5 75-125 L612291-09 WG629303 1,2-Dichloroethane mg/l 0.0223 0 .025 89.2 59-135 L612291-09 WG629303 1,2-Dichloropropane mg/l 0.0239 0 .025 95.6 68-126 L612291-09 WG629303 1,3,5-Trimethylbenzene mg/l 0.0255 0 .025 102. 67-136 L612291-09 WG629303 1,3-Dichlorobenzene mg/l 0.0263 0 .025 105. 69-131 L612291-09 WG629303 1,3-Dichloropropane mg/l 0.0228 0 .025 91.1 70-122 L612291-09 WG629303 1,4-Dichlorobenzene mg/l 0.0238 0 .025 95.0 70-123 L612291-09 WG629303 2,2-Dichloropropane mg/l 0.0258 0 .025 103. 51-141 L612291-09 WG629303 2-Butanone (MEK) mg/l 0.0769 0 .125 61.5 51-149 L612291-09 WG629303 2-Chloroethyl vinyl ether mg/l 0.0570 0 .125 45.6 10-161 L612291-09 WG629303 2-Chlorotoluene mg/l 0.0256 0 .025 102. 65-133 L612291-09 WG629303 4-Chlorotoluene mg/l 0.0259 0 .025 103. 67-129 L612291-09 WG629303 4-Methyl-2-pentanone (MIBK) mg/l 0.121 0 .125 97.1 53-154 L612291-09 WG629303 Acetone mg/l 0.0552 0 .125 44.1 34-146 L612291-09 WG629303 Acrolein mg/l 0.107 0 .125 86.0 10-189 L612291-09 WG629303 Acrylonitrile mg/l 0.117 0 .125 93.7 49-162 L612291-09 WG629303 Benzene mg/l 0.0234 0 .025 93.6 51-134 L612291-09 WG629303 Bromobenzene mg/l 0.0244 0 .025 97.6 64-130 L612291-09 WG629303 Bromodichloromethane mg/l 0.0236 0 .025 94.5 67-132 L612291-09 WG629303 Bromoform mg/l 0.0233 0 .025 93.3 59-137 L612291-09 WG629303 Bromomethane mg/l 0.0215 0 .025 85.8 23-177 L612291-09 WG629303 Carbon tetrachloride mg/l 0.0248 0.00130 .025 94.0 49-140 L612291-09 WG629303 Chlorobenzene mg/l 0.0246 0 .025 98.3 69-126 L612291-09 WG629303 Chlorodibromomethane mg/l 0.0229 0 .025 91.8 68-130 L612291-09 WG629303 Chloroethane mg/l 0.0229 0 .025 91.6 32-177 L612291-09 WG629303 Chloroform mg/l 0.0293 0.00530 .025 95.9 64-130 L612291-09 WG629303 Chloromethane mg/l 0.0219 0 .025 87.6 27-155 L612291-09 WG629303 cis-1,2-Dichloroethene mg/l 0.0244 0 .025 97.4 54-137 L612291-09 WG629303 cis-1,3-Dichloropropene mg/l 0.0238 0 .025 95.0 63-127 L612291-09 WG629303 Di-isopropyl ether mg/l 0.0242 0 .025 96.9 58-133 L612291-09 WG629303 Dibromomethane mg/l 0.0228 0 .025 91.2 68-131 L612291-09 WG629303 Dichlorodifluoromethane mg/l 0.0236 0 .025 94.2 16-188 L612291-09 WG629303 Ethylbenzene mg/l 0.0252 0 .025 101. 64-135 L612291-09 WG629303 Hexachloro-1,3-butadiene mg/l 0.0277 0 .025 111. 64-140 L612291-09 WG629303 Isopropylbenzene mg/l 0.0261 0 .025 104. 62-134 L612291-09 WG629303 Methyl tert-butyl ether mg/l 0.0233 0 .025 93.2 55-136 L612291-09 WG629303 Methylene Chloride mg/l 0.0227 0 .025 90.7 52-130 L612291-09 WG629303 n-Butylbenzene mg/l 0.0277 0 .025 111. 62-142 L612291-09 WG629303 n-Propylbenzene mg/l 0.0265 0 .025 106. 62-137 L612291-09 WG629303 Naphthalene mg/l 0.0243 0 .025 97.4 65-140 L612291-09 WG629303 p-Isopropyltoluene mg/l 0.0271 0 .025 108. 64-142 L612291-09 WG629303 sec-Butylbenzene mg/l 0.0269 0 .025 108. 67-139 L612291-09 WG629303 Styrene mg/l 0.0262 0 .025 105. 58-152 L612291-09 WG629303 tert-Butylbenzene mg/l 0.0268 0 .025 107. 66-139 L612291-09 WG629303 Tetrachloroethene mg/l 0.0417 0.0180 .025 94.9 56-139 L612291-09 WG629303 Toluene mg/l 0.0239 0 .025 95.4 61-126 L612291-09 WG629303 trans-1,2-Dichloroethene mg/l 0.0235 0 .025 93.8 45-137 L612291-09 WG629303 trans-1,3-Dichloropropene mg/l 0.0248 0 .025 99.0 59-130 L612291-09 WG629303 Trichloroethene mg/l 0.0333 0.00970 .025 94.4 40-155 L612291-09 WG629303 Trichlorofluoromethane mg/l 0.0248 0 .025 99.2 35-177 L612291-09 WG629303 Vinyl chloride mg/l 0.0230 0 .025 92.0 32-159 L612291-09 WG629303 Xylenes, Total mg/l 0.0753 0 .075 100. 64-133 L612291-09 WG629303 4-Bromofluorobenzene 102.5 82-120 WG629303 Dibromofluoromethane 98.63 82-126 WG629303 Toluene-d8 103.5 92-112 WG629303

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

Page 40 of 43

Reference 45 Page 256

Page 257: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 December 27, 2012

L612291

Matrix Spike DuplicateAnalyte Units MSD Ref %Rec Limit RPD Limit Ref Samp Batch

1,1,1,2-Tetrachloroethane mg/l 0.0255 0.0244 102. 71-130 4.73 20 L612291-09 WG629303 1,1,1-Trichloroethane mg/l 0.0284 0.0263 114. 58-137 7.92 20 L612291-09 WG629303 1,1,2,2-Tetrachloroethane mg/l 0.0252 0.0238 101. 64-149 5.82 20 L612291-09 WG629303 1,1,2-Trichloroethane mg/l 0.0251 0.0235 100. 73-128 6.53 20 L612291-09 WG629303 1,1,2-Trichlorotrifluoroethane mg/l 0.0285 0.0262 114. 36-159 8.56 21 L612291-09 WG629303 1,1-Dichloroethane mg/l 0.0271 0.0244 108. 58-133 10.8 20 L612291-09 WG629303 1,1-Dichloroethene mg/l 0.0263 0.0237 105. 32-152 10.2 20 L612291-09 WG629303 1,1-Dichloropropene mg/l 0.0267 0.0238 107. 50-140 11.2 20 L612291-09 WG629303 1,2,3-Trichlorobenzene mg/l 0.0272 0.0258 109. 68-135 5.20 20 L612291-09 WG629303 1,2,3-Trichloropropane mg/l 0.0268 0.0245 107. 74-137 8.95 20 L612291-09 WG629303 1,2,3-Trimethylbenzene mg/l 0.0253 0.0241 101. 67-133 4.82 20 L612291-09 WG629303 1,2,4-Trichlorobenzene mg/l 0.0285 0.0271 114. 67-133 4.92 20 L612291-09 WG629303 1,2,4-Trimethylbenzene mg/l 0.0268 0.0257 107. 62-141 3.99 20 L612291-09 WG629303 1,2-Dibromo-3-Chloropropane mg/l 0.0236 0.0218 94.2 55-148 7.74 22 L612291-09 WG629303 1,2-Dibromoethane mg/l 0.0249 0.0231 99.4 71-129 7.41 20 L612291-09 WG629303 1,2-Dichlorobenzene mg/l 0.0262 0.0249 105. 75-125 5.34 20 L612291-09 WG629303 1,2-Dichloroethane mg/l 0.0252 0.0223 101. 59-135 12.2 20 L612291-09 WG629303 1,2-Dichloropropane mg/l 0.0260 0.0239 104. 68-126 8.30 20 L612291-09 WG629303 1,3,5-Trimethylbenzene mg/l 0.0271 0.0255 108. 67-136 6.01 20 L612291-09 WG629303 1,3-Dichlorobenzene mg/l 0.0276 0.0263 110. 69-131 5.15 20 L612291-09 WG629303 1,3-Dichloropropane mg/l 0.0244 0.0228 97.6 70-122 6.86 20 L612291-09 WG629303 1,4-Dichlorobenzene mg/l 0.0249 0.0238 99.8 70-123 4.87 20 L612291-09 WG629303 2,2-Dichloropropane mg/l 0.0292 0.0258 117. 51-141 12.4 20 L612291-09 WG629303 2-Butanone (MEK) mg/l 0.0922 0.0769 73.8 51-149 18.2 22 L612291-09 WG629303 2-Chloroethyl vinyl ether mg/l 0.00793 0.0570 6.34* 10-161 151.* 40 L612291-09 WG629303 2-Chlorotoluene mg/l 0.0270 0.0256 108. 65-133 5.37 20 L612291-09 WG629303 4-Chlorotoluene mg/l 0.0272 0.0259 109. 67-129 5.24 20 L612291-09 WG629303 4-Methyl-2-pentanone (MIBK) mg/l 0.133 0.121 106. 53-154 8.93 21 L612291-09 WG629303 Acetone mg/l 0.0630 0.0552 50.4 34-146 13.3 22 L612291-09 WG629303 Acrolein mg/l 0.122 0.107 97.5 10-189 12.5 30 L612291-09 WG629303 Acrylonitrile mg/l 0.134 0.117 107. 49-162 13.3 20 L612291-09 WG629303 Benzene mg/l 0.0257 0.0234 103. 51-134 9.30 20 L612291-09 WG629303 Bromobenzene mg/l 0.0260 0.0244 104. 64-130 6.24 20 L612291-09 WG629303 Bromodichloromethane mg/l 0.0254 0.0236 101. 67-132 7.11 20 L612291-09 WG629303 Bromoform mg/l 0.0254 0.0233 102. 59-137 8.63 20 L612291-09 WG629303 Bromomethane mg/l 0.0236 0.0215 94.4 23-177 9.59 21 L612291-09 WG629303 Carbon tetrachloride mg/l 0.0276 0.0248 105. 49-140 10.7 20 L612291-09 WG629303 Chlorobenzene mg/l 0.0258 0.0246 103. 69-126 4.79 20 L612291-09 WG629303 Chlorodibromomethane mg/l 0.0246 0.0229 98.4 68-130 6.98 20 L612291-09 WG629303 Chloroethane mg/l 0.0252 0.0229 101. 32-177 9.71 21 L612291-09 WG629303 Chloroform mg/l 0.0321 0.0293 107. 64-130 9.25 20 L612291-09 WG629303 Chloromethane mg/l 0.0236 0.0219 94.5 27-155 7.58 20 L612291-09 WG629303 cis-1,2-Dichloroethene mg/l 0.0266 0.0244 106. 54-137 8.80 20 L612291-09 WG629303 cis-1,3-Dichloropropene mg/l 0.0253 0.0238 101. 63-127 6.36 20 L612291-09 WG629303 Di-isopropyl ether mg/l 0.0268 0.0242 107. 58-133 9.93 20 L612291-09 WG629303 Dibromomethane mg/l 0.0251 0.0228 100. 68-131 9.55 20 L612291-09 WG629303 Dichlorodifluoromethane mg/l 0.0261 0.0236 104. 16-188 10.2 22 L612291-09 WG629303 Ethylbenzene mg/l 0.0268 0.0252 107. 64-135 6.16 20 L612291-09 WG629303 Hexachloro-1,3-butadiene mg/l 0.0290 0.0277 116. 64-140 4.70 20 L612291-09 WG629303 Isopropylbenzene mg/l 0.0274 0.0261 109. 62-134 4.70 20 L612291-09 WG629303 Methyl tert-butyl ether mg/l 0.0261 0.0233 104. 55-136 11.5 20 L612291-09 WG629303 Methylene Chloride mg/l 0.0251 0.0227 100. 52-130 10.1 20 L612291-09 WG629303 n-Butylbenzene mg/l 0.0291 0.0277 116. 62-142 4.69 20 L612291-09 WG629303 n-Propylbenzene mg/l 0.0279 0.0265 112. 62-137 5.17 20 L612291-09 WG629303 Naphthalene mg/l 0.0265 0.0243 106. 65-140 8.59 20 L612291-09 WG629303 p-Isopropyltoluene mg/l 0.0286 0.0271 114. 64-142 5.46 20 L612291-09 WG629303 sec-Butylbenzene mg/l 0.0281 0.0269 112. 67-139 4.18 20 L612291-09 WG629303 Styrene mg/l 0.0276 0.0262 110. 58-152 5.34 20 L612291-09 WG629303 tert-Butylbenzene mg/l 0.0279 0.0268 112. 66-139 4.01 20 L612291-09 WG629303 Tetrachloroethene mg/l 0.0433 0.0417 101. 56-139 3.70 20 L612291-09 WG629303

* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

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Reference 45 Page 257

Page 258: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 December 27, 2012

L612291

Matrix Spike DuplicateAnalyte Units MSD Ref %Rec Limit RPD Limit Ref Samp Batch

Toluene mg/l 0.0254 0.0239 101. 61-126 6.04 20 L612291-09 WG629303 trans-1,2-Dichloroethene mg/l 0.0258 0.0235 103. 45-137 9.49 20 L612291-09 WG629303 trans-1,3-Dichloropropene mg/l 0.0266 0.0248 106. 59-130 7.24 20 L612291-09 WG629303 Trichloroethene mg/l 0.0355 0.0333 103. 40-155 6.35 20 L612291-09 WG629303 Trichlorofluoromethane mg/l 0.0278 0.0248 111. 35-177 11.4 23 L612291-09 WG629303 Vinyl chloride mg/l 0.0254 0.0230 102. 32-159 9.93 21 L612291-09 WG629303 Xylenes, Total mg/l 0.0791 0.0753 106. 64-133 4.97 20 L612291-09 WG629303 4-Bromofluorobenzene 102.3 82-120 WG629303 Dibromofluoromethane 102.4 82-126 WG629303 Toluene-d8 103.6 92-112 WG629303

Batch number /Run number / Sample number cross reference

WG629303: R2492362: L612291-01 02 03 04 05 06 07 08 09 10 11 12 13 14 15 16 17

* * Calculations are performed prior to rounding of reported values.* Performance of this Analyte is outside of established criteria.For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'

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Reference 45 Page 258

Page 259: ACUITY ENVIRONMENTAL SOLUTIONS, ANNUAL PROGRESS …18, 2010 Groundwater Remediation Pilot Test Plan) consisting of a groundwater recirculation system with a chemical oxidizer (permanganate)

12065 Lebanon Rd.Mt. Juliet, TN 37122(615) 758-58581-800-767-5859Fax (615) 758-5859

Tax I.D. 62-0814289

Est. 1970Acuity Environmental Solutions Mrs. Wendy Milejczak 7965 East 106th St. Suite 128 Quality Assurance Report

Level IIFishers, IN 46038 December 27, 2012

L612291

The data package includes a summary of the analytic results of the qualitycontrol samples required by the SW-846 or CWA methods. The quality controlsamples include a method blank, a laboratory control sample, and the matrixspike/matrix spike duplicate analysis. If a target parameter is outsidethe method limits, every sample that is effected is flagged with theappropriate qualifier in Appendix B of the analytic report.

Method Blank - an aliquot of reagent water carried through theentire analytic process. The method blank results indicate ifany possible contamination exposure during the sample handling,digestion or extraction process, and analysis. Concentrations oftarget analytes above the reporting limit in the method blank arequalified with the "B" qualifier.

Laboratory Control Sample - is a sample of known concentrationthat is carried through the digestion/extraction and analysisprocess. The percent recovery, expressed as a percentage of thetheoretical concentration, has statistical control limitsindicating that the analytic process is "in control". If atarget analyte is outside the control limits for the laboratorycontrol sample or any other control sample, the parameter isflagged with a "J4" qualifier for all effected samples.

Matrix Spike and Matrix Spike Duplicate - is two aliquots of anenvironmental sample that is spiked with known concentrations oftarget analytes. The percent recovery of the target analytesalso has statistical control limits. If any recoveries that areoutside the method control limits, the sample that was selectedfor matrix spike/matrix spike duplicate analysis is flagged witheither a "J5" or a "J6". The relative percent difference (%RPD)between the matrix spike and the matrix spike duplicaterecoveries is all calculated. If the RPD is above the methodlimit, the effected samples are flagged with a "J3" qualifier.

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