alliance analytical laboratories, inc. · 4/23/2019  · heavy metals kratom arsenic 0.738 ppm...

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CUSTOMER GAIA Ethnobotanical LLC/MitraGaia 2752 Botticelli Dr. Henderson, NV 89052 Phone: 904-551-9009 Email: [email protected]; REFERENCE NUMBER 190158: 1915813.01 Customer PO SAMPLE DATE 4/23/2019 DATE RECEIVED 5/8/2019 TEMPERATURE AT RECEIVING SAMPLE DESCRIPTION Lot 04232019 Green MD SD 4/23/19 Test Method Test Requested Start Date Ref Number Results Cobalt ICP-AES < 0.500 ppm 5/14 12:00 PM Internal File Analyst: 23 Heavy Metals Kratom Analyst: 23 Arsenic 0.586 ppm Internal File 5/14 12:00 PM Analyst: 23 Chromium 1.322 ppm Internal File 5/14 12:00 PM Analyst: 23 Lead 1.611 ppm Internal File 5/14 12:00 PM Analyst: 23 Nickel 1.407 ppm Internal File 5/14 12:00 PM Analyst: 23 Vanadium < 0.500 ppm Internal File 5/14 12:00 PM Analyst: 23 Sample Comment: Supplement to report 1915813 5/1 An Date: 5/16/2019 Page 1 of 1 THIS DOCUMENT CONTAINS TRADE SECRET/CONFIDENTIAL INFORMATION PURSUANT TO 5 U.S.C.(b)(4) This report must not be reproduced, except in full, without written approval of the laboratory. It is the customer's responsibility to evaluate the compliance of these results to any regulatory requirement. Test results apply to the sample as received. Reviewed and Approved by: Date: 5/16/2019 Andrea Balduck - Laboratory Manager Alliance Analytical Laboratories, Inc. 179 West Randall Street Coopersville, MI 49404 Phone: (616) 837-7670 Fax: (616) 837-7701 Test methods marked with ^ are accredited under the laboratory's ISO/IEC 17025 accreditation issued by ANSI-ASQ National Accreditation Board. Refer to certificate and scope of accreditation AT-2044 TEST RESULTS REPORT

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Page 1: Alliance Analytical Laboratories, Inc. · 4/23/2019  · Heavy Metals Kratom Arsenic 0.738 ppm Internal File 5/7 12:00 PM Analyst: 23 Chromium 1.075 ppm Internal File 5/7 12:00 PM

CUSTOMER GAIA Ethnobotanical LLC/MitraGaia2752 Botticelli Dr.Henderson, NV 89052Phone: 904-551-9009Email: [email protected];

REFERENCE NUMBER 190158: 1915813.01 Customer PO

SAMPLE DATE 4/23/2019

DATE RECEIVED 5/8/2019

TEMPERATURE AT RECEIVING

SAMPLE DESCRIPTION Lot 04232019 Green MDSD 4/23/19

Test MethodTest Requested Start DateRef NumberResultsCobalt ICP-AES < 0.500 ppm 5/14 12:00 PMInternal File

Analyst: 23

Heavy Metals Kratom Analyst: 23

Arsenic 0.586 ppm Internal File 5/14 12:00 PMAnalyst: 23

Chromium 1.322 ppm Internal File 5/14 12:00 PMAnalyst: 23

Lead 1.611 ppm Internal File 5/14 12:00 PMAnalyst: 23

Nickel 1.407 ppm Internal File 5/14 12:00 PMAnalyst: 23

Vanadium < 0.500 ppm Internal File 5/14 12:00 PMAnalyst: 23

Sample Comment:Supplement to report 1915813

5/1An

Date: 5/16/2019 Page 1 of 1

THIS DOCUMENT CONTAINS TRADE SECRET/CONFIDENTIAL INFORMATIONPURSUANT TO 5 U.S.C.(b)(4)

This report must not be reproduced, except in full, without written approval of the laboratory.

It is the customer's responsibility to evaluate the compliance of these results to any regulatory requirement.Test results apply to the sample as received.

Reviewed and Approved by: Date: 5/16/2019Andrea Balduck - Laboratory Manager

Alliance Analytical Laboratories, Inc.179 West Randall StreetCoopersville, MI 49404Phone: (616) 837-7670

Fax: (616) 837-7701

Test methods marked with ^ are accredited under the laboratory's ISO/IEC 17025

accreditation issued by ANSI-ASQ National Accreditation Board. Refer to certificate and

scope of accreditation AT-2044

TEST RESULTSREPORT

Page 2: Alliance Analytical Laboratories, Inc. · 4/23/2019  · Heavy Metals Kratom Arsenic 0.738 ppm Internal File 5/7 12:00 PM Analyst: 23 Chromium 1.075 ppm Internal File 5/7 12:00 PM

CUSTOMER GAIA Ethnobotanical LLC/MitraGaia2752 Botticelli Dr.Henderson, NV 89052Phone: 904-551-9009Email: [email protected];

REFERENCE NUMBER 190158: 1915809 Customer PO

SAMPLE DATE

DATE RECEIVED 5/8/2019

TEMPERATURE AT RECEIVING

SAMPLE DESCRIPTION Green MD Lot 05012019SD NA

Test MethodTest Requested Start DateRef NumberResultsBAM:Aerobic Plate Count ^BAM Ch.3 87000 cfu/g 5/10 2:46 PMLog: 4.9

Analyst: 39

BAM:Mold ^BAM Ch. 18 1900 cfu/g 5/9 5:02 PMLog: 3.2Analyst: 34

BAM:Yeast ^BAM Ch. 18 <100 cfu/g 5/9 5:02 PMLog: <2.0Analyst: 34

Coliform ^AOAC 991.14 200 cfu/g 5/9 3:43 PMLog: 2.3Analyst: 34

Escherichia coli - Generic:USP 2022

USP 2022 Negative/25g 5/9 11:09 AM

Analyst: 39

Salmonella:AOAC 011404 AOAC 011404 Negative/25g 5/9 11:09 AMKit Lot Number: SSp-359Analyst: 39

5/1An

Date: 5/15/2019 Page 1 of 1

THIS DOCUMENT CONTAINS TRADE SECRET/CONFIDENTIAL INFORMATIONPURSUANT TO 5 U.S.C.(b)(4)

This report must not be reproduced, except in full, without written approval of the laboratory.

It is the customer's responsibility to evaluate the compliance of these results to any regulatory requirement.Test results apply to the sample as received.

Reviewed and Approved by: Date: 5/15/2019Andrea Balduck - Laboratory Manager

Alliance Analytical Laboratories, Inc.179 West Randall StreetCoopersville, MI 49404Phone: (616) 837-7670

Fax: (616) 837-7701

Test methods marked with ^ are accredited under the laboratory's ISO/IEC 17025

accreditation issued by ANSI-ASQ National Accreditation Board. Refer to certificate and

scope of accreditation AT-2044

TEST RESULTSREPORT

Page 3: Alliance Analytical Laboratories, Inc. · 4/23/2019  · Heavy Metals Kratom Arsenic 0.738 ppm Internal File 5/7 12:00 PM Analyst: 23 Chromium 1.075 ppm Internal File 5/7 12:00 PM

CUSTOMER GAIA Ethnobotanical LLC/MitraGaia2752 Botticelli Dr.Henderson, NV 89052Phone: 904-551-9009Email: [email protected];

REFERENCE NUMBER 190158: 1915809.01 Customer PO

SAMPLE DATE

DATE RECEIVED 5/8/2019

TEMPERATURE AT RECEIVING

SAMPLE DESCRIPTION Green MD Lot 05012019SD NA

Test MethodTest Requested Start DateRef NumberResultsCobalt ICP-AES < 0.500 ppm 5/14 12:00 PMInternal File

Analyst: 23

Heavy Metals Kratom Analyst: 23

Arsenic 0.620 ppm Internal File 5/14 12:00 PMAnalyst: 23

Chromium 1.026 ppm Internal File 5/14 12:00 PMAnalyst: 23

Lead 1.416 ppm Internal File 5/14 12:00 PMAnalyst: 23

Nickel 1.414 ppm Internal File 5/14 12:00 PMAnalyst: 23

Vanadium < 0.500 ppm Internal File 5/14 12:00 PMAnalyst: 23

Sample Comment:Supplement to report 1915809

5/1An

Date: 5/16/2019 Page 1 of 1

THIS DOCUMENT CONTAINS TRADE SECRET/CONFIDENTIAL INFORMATIONPURSUANT TO 5 U.S.C.(b)(4)

This report must not be reproduced, except in full, without written approval of the laboratory.

It is the customer's responsibility to evaluate the compliance of these results to any regulatory requirement.Test results apply to the sample as received.

Reviewed and Approved by: Date: 5/16/2019Andrea Balduck - Laboratory Manager

Alliance Analytical Laboratories, Inc.179 West Randall StreetCoopersville, MI 49404Phone: (616) 837-7670

Fax: (616) 837-7701

Test methods marked with ^ are accredited under the laboratory's ISO/IEC 17025

accreditation issued by ANSI-ASQ National Accreditation Board. Refer to certificate and

scope of accreditation AT-2044

TEST RESULTSREPORT

Page 4: Alliance Analytical Laboratories, Inc. · 4/23/2019  · Heavy Metals Kratom Arsenic 0.738 ppm Internal File 5/7 12:00 PM Analyst: 23 Chromium 1.075 ppm Internal File 5/7 12:00 PM

CUSTOMER GAIA Ethnobotanical LLC/MitraGaia2752 Botticelli Dr.Henderson, NV 89052Phone: 904-551-9009Email: [email protected];

REFERENCE NUMBER 190150: 1915004 Customer PO

SAMPLE DATE

DATE RECEIVED 5/1/2019

TEMPERATURE AT RECEIVING

SAMPLE DESCRIPTION Green MD Lot 041619SD NA

Test MethodTest Requested Start DateRef NumberResultsBAM:Aerobic Plate Count ^BAM Ch.3 210000 cfu/g 5/2 2:16 PMLog: 5.3

Analyst: 34

BAM:Mold ^BAM Ch. 18 40000 cfu/g 5/2 2:16 PMLog: 4.6Analyst: 34

BAM:Yeast ^BAM Ch. 18 <100 cfu/g 5/2 2:16 PMLog: <2.0Analyst: 34

Cobalt ICP-AES < 0.500 ppm 5/7 12:00 PMInternal FileAnalyst: 23

Coliform ^AOAC 991.14 3100 cfu/g 5/2 1:08 PMLog: 3.4Analyst: 34

Escherichia coli - Generic:USP 2022

USP 2022 Negative/25g 5/2 12:28 PM

Analyst: 34

Heavy Metals Kratom Arsenic 0.738 ppm Internal File 5/7 12:00 PM

Analyst: 23Chromium 1.075 ppm Internal File 5/7 12:00 PM

Analyst: 23Lead 1.095 ppm Internal File 5/7 12:00 PM

Analyst: 23

Date: 5/23/2019 Page 1 of 2

THIS DOCUMENT CONTAINS TRADE SECRET/CONFIDENTIAL INFORMATIONPURSUANT TO 5 U.S.C.(b)(4)

This report must not be reproduced, except in full, without written approval of the laboratory.

It is the customer's responsibility to evaluate the compliance of these results to any regulatory requirement.Test results apply to the sample as received.

Reviewed and Approved by: Date: 5/23/2019Audrey Monroe - Laboratory Director

Alliance Analytical Laboratories, Inc.179 West Randall StreetCoopersville, MI 49404Phone: (616) 837-7670

Fax: (616) 837-7701

Test methods marked with ^ are accredited under the laboratory's ISO/IEC 17025

accreditation issued by ANSI-ASQ National Accreditation Board. Refer to certificate and

scope of accreditation AT-2044

TEST RESULTSREPORT

Page 5: Alliance Analytical Laboratories, Inc. · 4/23/2019  · Heavy Metals Kratom Arsenic 0.738 ppm Internal File 5/7 12:00 PM Analyst: 23 Chromium 1.075 ppm Internal File 5/7 12:00 PM

REFERENCE NUMBER 190150: 1915007 Customer PO

SAMPLE DATE

DATE RECEIVED 5/1/2019

TEMPERATURE AT RECEIVING

SAMPLE DESCRIPTION Green MD Lot 030419 SD NA

Test MethodTest Requested Start DateRef NumberResultsLead 1.378 ppm Internal File 5/7 12:00 PM

Analyst: 23Nickel 1.591 ppm Internal File 5/7 12:00 AM

Analyst: 23Vanadium < 0.500 ppm Internal File 5/7 12:00 AM

Analyst: 23

Salmonella:AOAC 011404 AOAC 011404 Negative/25g 5/2 12:29 PMKit Lot Number: SSp-359Analyst: 34

5/1Au

Date: 5/16/2019 Page 2 of 2

THIS DOCUMENT CONTAINS TRADE SECRET/CONFIDENTIAL INFORMATIONPURSUANT TO 5 U.S.C.(b)(4)

This report must not be reproduced, except in full, without written approval of the laboratory.

It is the customer's responsibility to evaluate the compliance of these results to any regulatory requirement.Test results apply to the sample as received.

Reviewed and Approved by: Date: 5/16/2019Audrey Monroe - Laboratory Director

Alliance Analytical Laboratories, Inc.179 West Randall StreetCoopersville, MI 49404Phone: (616) 837-7670

Fax: (616) 837-7701

Test methods marked with ^ are accredited under the laboratory's ISO/IEC 17025

accreditation issued by ANSI-ASQ National Accreditation Board. Refer to certificate and

scope of accreditation AT-2044

TEST RESULTSREPORT

Page 6: Alliance Analytical Laboratories, Inc. · 4/23/2019  · Heavy Metals Kratom Arsenic 0.738 ppm Internal File 5/7 12:00 PM Analyst: 23 Chromium 1.075 ppm Internal File 5/7 12:00 PM

CUSTOMER GAIA Ethnobotanical LLC/MitraGaia2752 Botticelli Dr.Henderson, NV 89052Phone: 904-551-9009Email: [email protected];

REFERENCE NUMBER 190150: 1915007 Customer PO

SAMPLE DATE

DATE RECEIVED 5/1/2019

TEMPERATURE AT RECEIVING

SAMPLE DESCRIPTION Green MD Lot 030419 SD NA

Test MethodTest Requested Start DateRef NumberResultsBAM:Aerobic Plate Count ^BAM Ch.3 330000 cfu/g 5/2 2:17 PMLog: 5.5

Analyst: 34

BAM:Mold ^BAM Ch. 18 20000 cfu/g 5/2 2:17 PMLog: 4.3Analyst: 34

BAM:Yeast ^BAM Ch. 18 <100 cfu/g 5/2 2:17 PMLog: <2.0Analyst: 34

Cobalt ICP-AES < 0.500 ppm 5/7 12:00 PMInternal FileAnalyst: 23

Coliform ^AOAC 991.14 5800 cfu/g 5/2 1:08 PMLog: 3.7Analyst: 34

Escherichia coli - Generic:USP 2022

USP 2022 Negative/25g 5/2 12:29 PM

Analyst: 34

Heavy Metals Kratom Analyst: 23

Arsenic < 0.500 ppm Internal File 5/7 12:00 PMAnalyst: 23

Cadmium < 0.500 ppm Internal File 5/7 12:00 PMAnalyst: 23

Date: 5/16/2019 Page 1 of 2

THIS DOCUMENT CONTAINS TRADE SECRET/CONFIDENTIAL INFORMATIONPURSUANT TO 5 U.S.C.(b)(4)

This report must not be reproduced, except in full, without written approval of the laboratory.

It is the customer's responsibility to evaluate the compliance of these results to any regulatory requirement.Test results apply to the sample as received.

Reviewed and Approved by: Date: 5/16/2019Audrey Monroe - Laboratory Director

Alliance Analytical Laboratories, Inc.179 West Randall StreetCoopersville, MI 49404Phone: (616) 837-7670

Fax: (616) 837-7701

Test methods marked with ^ are accredited under the laboratory's ISO/IEC 17025

accreditation issued by ANSI-ASQ National Accreditation Board. Refer to certificate and

scope of accreditation AT-2044

TEST RESULTSREPORT

Page 7: Alliance Analytical Laboratories, Inc. · 4/23/2019  · Heavy Metals Kratom Arsenic 0.738 ppm Internal File 5/7 12:00 PM Analyst: 23 Chromium 1.075 ppm Internal File 5/7 12:00 PM

REFERENCE NUMBER 190150: 1915010 Customer PO

SAMPLE DATE

DATE RECEIVED 5/1/2019

TEMPERATURE AT RECEIVING

SAMPLE DESCRIPTION Green MD Lot 030819SD NA

Test MethodTest Requested Start DateRef NumberResultsNickel 1.426 ppm Internal File 5/7 12:00 PM

Analyst: 23Vanadium < 0.500 ppm Internal File 5/7 12:00 PM

Analyst: 23

Salmonella:AOAC 011404 AOAC 011404 Negative/25g 5/2 12:30 PMKit Lot Number: SSp-359Analyst: 34

5/2Au

Date: 5/23/2019 Page 2 of 2

THIS DOCUMENT CONTAINS TRADE SECRET/CONFIDENTIAL INFORMATIONPURSUANT TO 5 U.S.C.(b)(4)

This report must not be reproduced, except in full, without written approval of the laboratory.

It is the customer's responsibility to evaluate the compliance of these results to any regulatory requirement.Test results apply to the sample as received.

Reviewed and Approved by: Date: 5/23/2019Audrey Monroe - Laboratory Director

Alliance Analytical Laboratories, Inc.179 West Randall StreetCoopersville, MI 49404Phone: (616) 837-7670

Fax: (616) 837-7701

Test methods marked with ^ are accredited under the laboratory's ISO/IEC 17025

accreditation issued by ANSI-ASQ National Accreditation Board. Refer to certificate and

scope of accreditation AT-2044

TEST RESULTSREPORT

Page 8: Alliance Analytical Laboratories, Inc. · 4/23/2019  · Heavy Metals Kratom Arsenic 0.738 ppm Internal File 5/7 12:00 PM Analyst: 23 Chromium 1.075 ppm Internal File 5/7 12:00 PM

CUSTOMER GAIA Ethnobotanical LLC/MitraGaia2752 Botticelli Dr.Henderson, NV 89052Phone: 904-551-9009Email: [email protected];

REFERENCE NUMBER 190158: 1915809 Customer PO

SAMPLE DATE

DATE RECEIVED 5/8/2019

TEMPERATURE AT RECEIVING

SAMPLE DESCRIPTION Green MD Lot 05012019SD NA

Test MethodTest Requested Start DateRef NumberResultsBAM:Aerobic Plate Count ^BAM Ch.3 87000 cfu/g 5/10 2:46 PMLog: 4.9

Analyst: 39

BAM:Mold ^BAM Ch. 18 1900 cfu/g 5/9 5:02 PMLog: 3.2Analyst: 34

BAM:Yeast ^BAM Ch. 18 <100 cfu/g 5/9 5:02 PMLog: <2.0Analyst: 34

Coliform ^AOAC 991.14 200 cfu/g 5/9 3:43 PMLog: 2.3Analyst: 34

Escherichia coli - Generic:USP 2022

USP 2022 Negative/25g 5/9 11:09 AM

Analyst: 39

Salmonella:AOAC 011404 AOAC 011404 Negative/25g 5/9 11:09 AMKit Lot Number: SSp-359Analyst: 39

5/1An

Date: 5/15/2019 Page 1 of 1

THIS DOCUMENT CONTAINS TRADE SECRET/CONFIDENTIAL INFORMATIONPURSUANT TO 5 U.S.C.(b)(4)

This report must not be reproduced, except in full, without written approval of the laboratory.

It is the customer's responsibility to evaluate the compliance of these results to any regulatory requirement.Test results apply to the sample as received.

Reviewed and Approved by: Date: 5/15/2019Andrea Balduck - Laboratory Manager

Alliance Analytical Laboratories, Inc.179 West Randall StreetCoopersville, MI 49404Phone: (616) 837-7670

Fax: (616) 837-7701

Test methods marked with ^ are accredited under the laboratory's ISO/IEC 17025

accreditation issued by ANSI-ASQ National Accreditation Board. Refer to certificate and

scope of accreditation AT-2044

TEST RESULTSREPORT

Page 9: Alliance Analytical Laboratories, Inc. · 4/23/2019  · Heavy Metals Kratom Arsenic 0.738 ppm Internal File 5/7 12:00 PM Analyst: 23 Chromium 1.075 ppm Internal File 5/7 12:00 PM

CUSTOMER GAIA Ethnobotanical LLC/MitraGaia2752 Botticelli Dr.Henderson, NV 89052Phone: 904-551-9009Email: [email protected];

REFERENCE NUMBER 190158: 1915809.01 Customer PO

SAMPLE DATE

DATE RECEIVED 5/8/2019

TEMPERATURE AT RECEIVING

SAMPLE DESCRIPTION Green MD Lot 05012019SD NA

Test MethodTest Requested Start DateRef NumberResultsCobalt ICP-AES < 0.500 ppm 5/14 12:00 PMInternal File

Analyst: 23

Heavy Metals Kratom Analyst: 23

Arsenic 0.620 ppm Internal File 5/14 12:00 PMAnalyst: 23

Chromium 1.026 ppm Internal File 5/14 12:00 PMAnalyst: 23

Lead 1.416 ppm Internal File 5/14 12:00 PMAnalyst: 23

Nickel 1.414 ppm Internal File 5/14 12:00 PMAnalyst: 23

Vanadium < 0.500 ppm Internal File 5/14 12:00 PMAnalyst: 23

Sample Comment:Supplement to report 1915809

5/1An

Date: 5/16/2019 Page 1 of 1

THIS DOCUMENT CONTAINS TRADE SECRET/CONFIDENTIAL INFORMATIONPURSUANT TO 5 U.S.C.(b)(4)

This report must not be reproduced, except in full, without written approval of the laboratory.

It is the customer's responsibility to evaluate the compliance of these results to any regulatory requirement.Test results apply to the sample as received.

Reviewed and Approved by: Date: 5/16/2019Andrea Balduck - Laboratory Manager

Alliance Analytical Laboratories, Inc.179 West Randall StreetCoopersville, MI 49404Phone: (616) 837-7670

Fax: (616) 837-7701

Test methods marked with ^ are accredited under the laboratory's ISO/IEC 17025

accreditation issued by ANSI-ASQ National Accreditation Board. Refer to certificate and

scope of accreditation AT-2044

TEST RESULTSREPORT

Page 10: Alliance Analytical Laboratories, Inc. · 4/23/2019  · Heavy Metals Kratom Arsenic 0.738 ppm Internal File 5/7 12:00 PM Analyst: 23 Chromium 1.075 ppm Internal File 5/7 12:00 PM

CUSTOMER GAIA Ethnobotanical LLC/MitraGaia2752 Botticelli Dr.Henderson, NV 89052Phone: 904-551-9009Email: [email protected];

REFERENCE NUMBER 190158: 1915813.01 Customer PO

SAMPLE DATE 4/23/2019

DATE RECEIVED 5/8/2019

TEMPERATURE AT RECEIVING

SAMPLE DESCRIPTION Lot 04232019 Green MDSD 4/23/19

Test MethodTest Requested Start DateRef NumberResultsCobalt ICP-AES < 0.500 ppm 5/14 12:00 PMInternal File

Analyst: 23

Heavy Metals Kratom Analyst: 23

Arsenic 0.586 ppm Internal File 5/14 12:00 PMAnalyst: 23

Chromium 1.322 ppm Internal File 5/14 12:00 PMAnalyst: 23

Lead 1.611 ppm Internal File 5/14 12:00 PMAnalyst: 23

Nickel 1.407 ppm Internal File 5/14 12:00 PMAnalyst: 23

Vanadium < 0.500 ppm Internal File 5/14 12:00 PMAnalyst: 23

Sample Comment:Supplement to report 1915813

5/1An

Date: 5/16/2019 Page 1 of 1

THIS DOCUMENT CONTAINS TRADE SECRET/CONFIDENTIAL INFORMATIONPURSUANT TO 5 U.S.C.(b)(4)

This report must not be reproduced, except in full, without written approval of the laboratory.

It is the customer's responsibility to evaluate the compliance of these results to any regulatory requirement.Test results apply to the sample as received.

Reviewed and Approved by: Date: 5/16/2019Andrea Balduck - Laboratory Manager

Alliance Analytical Laboratories, Inc.179 West Randall StreetCoopersville, MI 49404Phone: (616) 837-7670

Fax: (616) 837-7701

Test methods marked with ^ are accredited under the laboratory's ISO/IEC 17025

accreditation issued by ANSI-ASQ National Accreditation Board. Refer to certificate and

scope of accreditation AT-2044

TEST RESULTSREPORT

Page 11: Alliance Analytical Laboratories, Inc. · 4/23/2019  · Heavy Metals Kratom Arsenic 0.738 ppm Internal File 5/7 12:00 PM Analyst: 23 Chromium 1.075 ppm Internal File 5/7 12:00 PM

CUSTOMER GAIA Ethnobotanical LLC/MitraGaia2752 Botticelli Dr.Henderson, NV 89052Phone: 904-551-9009Email: [email protected];

REFERENCE NUMBER 190150: 1915004 Customer PO

SAMPLE DATE

DATE RECEIVED 5/1/2019

TEMPERATURE AT RECEIVING

SAMPLE DESCRIPTION Green MD Lot 041619SD NA

Test MethodTest Requested Start DateRef NumberResultsBAM:Aerobic Plate Count ^BAM Ch.3 210000 cfu/g 5/2 2:16 PMLog: 5.3

Analyst: 34

BAM:Mold ^BAM Ch. 18 40000 cfu/g 5/2 2:16 PMLog: 4.6Analyst: 34

BAM:Yeast ^BAM Ch. 18 <100 cfu/g 5/2 2:16 PMLog: <2.0Analyst: 34

Cobalt ICP-AES < 0.500 ppm 5/7 12:00 PMInternal FileAnalyst: 23

Coliform ^AOAC 991.14 3100 cfu/g 5/2 1:08 PMLog: 3.4Analyst: 34

Escherichia coli - Generic:USP 2022

USP 2022 Negative/25g 5/2 12:28 PM

Analyst: 34

Heavy Metals Kratom Arsenic 0.738 ppm Internal File 5/7 12:00 PM

Analyst: 23Chromium 1.075 ppm Internal File 5/7 12:00 PM

Analyst: 23Lead 1.095 ppm Internal File 5/7 12:00 PM

Analyst: 23

Date: 5/23/2019 Page 1 of 2

THIS DOCUMENT CONTAINS TRADE SECRET/CONFIDENTIAL INFORMATIONPURSUANT TO 5 U.S.C.(b)(4)

This report must not be reproduced, except in full, without written approval of the laboratory.

It is the customer's responsibility to evaluate the compliance of these results to any regulatory requirement.Test results apply to the sample as received.

Reviewed and Approved by: Date: 5/23/2019Audrey Monroe - Laboratory Director

Alliance Analytical Laboratories, Inc.179 West Randall StreetCoopersville, MI 49404Phone: (616) 837-7670

Fax: (616) 837-7701

Test methods marked with ^ are accredited under the laboratory's ISO/IEC 17025

accreditation issued by ANSI-ASQ National Accreditation Board. Refer to certificate and

scope of accreditation AT-2044

TEST RESULTSREPORT

Page 12: Alliance Analytical Laboratories, Inc. · 4/23/2019  · Heavy Metals Kratom Arsenic 0.738 ppm Internal File 5/7 12:00 PM Analyst: 23 Chromium 1.075 ppm Internal File 5/7 12:00 PM

REFERENCE NUMBER 190150: 1915007 Customer PO

SAMPLE DATE

DATE RECEIVED 5/1/2019

TEMPERATURE AT RECEIVING

SAMPLE DESCRIPTION Green MD Lot 030419 SD NA

Test MethodTest Requested Start DateRef NumberResultsLead 1.378 ppm Internal File 5/7 12:00 PM

Analyst: 23Nickel 1.591 ppm Internal File 5/7 12:00 AM

Analyst: 23Vanadium < 0.500 ppm Internal File 5/7 12:00 AM

Analyst: 23

Salmonella:AOAC 011404 AOAC 011404 Negative/25g 5/2 12:29 PMKit Lot Number: SSp-359Analyst: 34

5/1Au

Date: 5/16/2019 Page 2 of 2

THIS DOCUMENT CONTAINS TRADE SECRET/CONFIDENTIAL INFORMATIONPURSUANT TO 5 U.S.C.(b)(4)

This report must not be reproduced, except in full, without written approval of the laboratory.

It is the customer's responsibility to evaluate the compliance of these results to any regulatory requirement.Test results apply to the sample as received.

Reviewed and Approved by: Date: 5/16/2019Audrey Monroe - Laboratory Director

Alliance Analytical Laboratories, Inc.179 West Randall StreetCoopersville, MI 49404Phone: (616) 837-7670

Fax: (616) 837-7701

Test methods marked with ^ are accredited under the laboratory's ISO/IEC 17025

accreditation issued by ANSI-ASQ National Accreditation Board. Refer to certificate and

scope of accreditation AT-2044

TEST RESULTSREPORT

Page 13: Alliance Analytical Laboratories, Inc. · 4/23/2019  · Heavy Metals Kratom Arsenic 0.738 ppm Internal File 5/7 12:00 PM Analyst: 23 Chromium 1.075 ppm Internal File 5/7 12:00 PM

CUSTOMER GAIA Ethnobotanical LLC/MitraGaia2752 Botticelli Dr.Henderson, NV 89052Phone: 904-551-9009Email: [email protected];

REFERENCE NUMBER 190150: 1915007 Customer PO

SAMPLE DATE

DATE RECEIVED 5/1/2019

TEMPERATURE AT RECEIVING

SAMPLE DESCRIPTION Green MD Lot 030419 SD NA

Test MethodTest Requested Start DateRef NumberResultsBAM:Aerobic Plate Count ^BAM Ch.3 330000 cfu/g 5/2 2:17 PMLog: 5.5

Analyst: 34

BAM:Mold ^BAM Ch. 18 20000 cfu/g 5/2 2:17 PMLog: 4.3Analyst: 34

BAM:Yeast ^BAM Ch. 18 <100 cfu/g 5/2 2:17 PMLog: <2.0Analyst: 34

Cobalt ICP-AES < 0.500 ppm 5/7 12:00 PMInternal FileAnalyst: 23

Coliform ^AOAC 991.14 5800 cfu/g 5/2 1:08 PMLog: 3.7Analyst: 34

Escherichia coli - Generic:USP 2022

USP 2022 Negative/25g 5/2 12:29 PM

Analyst: 34

Heavy Metals Kratom Analyst: 23

Arsenic < 0.500 ppm Internal File 5/7 12:00 PMAnalyst: 23

Cadmium < 0.500 ppm Internal File 5/7 12:00 PMAnalyst: 23

Date: 5/16/2019 Page 1 of 2

THIS DOCUMENT CONTAINS TRADE SECRET/CONFIDENTIAL INFORMATIONPURSUANT TO 5 U.S.C.(b)(4)

This report must not be reproduced, except in full, without written approval of the laboratory.

It is the customer's responsibility to evaluate the compliance of these results to any regulatory requirement.Test results apply to the sample as received.

Reviewed and Approved by: Date: 5/16/2019Audrey Monroe - Laboratory Director

Alliance Analytical Laboratories, Inc.179 West Randall StreetCoopersville, MI 49404Phone: (616) 837-7670

Fax: (616) 837-7701

Test methods marked with ^ are accredited under the laboratory's ISO/IEC 17025

accreditation issued by ANSI-ASQ National Accreditation Board. Refer to certificate and

scope of accreditation AT-2044

TEST RESULTSREPORT

Page 14: Alliance Analytical Laboratories, Inc. · 4/23/2019  · Heavy Metals Kratom Arsenic 0.738 ppm Internal File 5/7 12:00 PM Analyst: 23 Chromium 1.075 ppm Internal File 5/7 12:00 PM

REFERENCE NUMBER 190150: 1915010 Customer PO

SAMPLE DATE

DATE RECEIVED 5/1/2019

TEMPERATURE AT RECEIVING

SAMPLE DESCRIPTION Green MD Lot 030819SD NA

Test MethodTest Requested Start DateRef NumberResultsNickel 1.426 ppm Internal File 5/7 12:00 PM

Analyst: 23Vanadium < 0.500 ppm Internal File 5/7 12:00 PM

Analyst: 23

Salmonella:AOAC 011404 AOAC 011404 Negative/25g 5/2 12:30 PMKit Lot Number: SSp-359Analyst: 34

5/2Au

Date: 5/23/2019 Page 2 of 2

THIS DOCUMENT CONTAINS TRADE SECRET/CONFIDENTIAL INFORMATIONPURSUANT TO 5 U.S.C.(b)(4)

This report must not be reproduced, except in full, without written approval of the laboratory.

It is the customer's responsibility to evaluate the compliance of these results to any regulatory requirement.Test results apply to the sample as received.

Reviewed and Approved by: Date: 5/23/2019Audrey Monroe - Laboratory Director

Alliance Analytical Laboratories, Inc.179 West Randall StreetCoopersville, MI 49404Phone: (616) 837-7670

Fax: (616) 837-7701

Test methods marked with ^ are accredited under the laboratory's ISO/IEC 17025

accreditation issued by ANSI-ASQ National Accreditation Board. Refer to certificate and

scope of accreditation AT-2044

TEST RESULTSREPORT