1l 1h nmr (400 mhz, cdcl3 · 1l. 13. c nmr (100 mhz, cdcl. 3) hn s o o i s. electronic...

1l 1H NMR (400 MHz, CDCl3)

HNS

O

O

I

S

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

1l 13C NMR (100 MHz, CDCl3)

HNS

O

O

I

S

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

Copies of 1H and 13C NMR

3a 1H NMR (400 MHz, CDCl3)

NN

I

CH3

Ts

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3a 13C NMR (100 MHz, CDCl3)

NN

I

CH3

Ts

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3b 1H NMR (400 MHz, CDCl3)

NN

I

F

Ms

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3b 13C NMR (100 MHz, CDCl3)

NN

I

F

Ms

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3c 1H NMR (400 MHz, CDCl3)

NN

I

Cl

Ms

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3c 13C NMR (100 MHz, CDCl3)

NN

I

Cl

Ms

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3d 1H NMR (400 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3d 13C NMR (100 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3e 1H NMR (400 MHz, CDCl3)

NN

I

F

Ts

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3e 13C NMR (100 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3f 1H NMR (400 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3f 13C NMR (100 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3g 1H NMR (400 MHz, CDCl3)

NN

I

Cl

Ts

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3g 13C NMR (100 MHz, CDCl3)

NN

I

Cl

Ts

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3h 1H NMR (400 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3h 13C NMR (100 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3i 1H NMR (400 MHz, CDCl3)

NN

I

CH3

S OO

S

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3i 13C NMR (100 MHz, CDCl3)

NN

I

CH3

S OO

S

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3j 1H NMR (400 MHz, CDCl3)

NN

I

S OO

S

F

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3j 13C NMR (100 MHz, CDCl3)

NN

I

S OO

S

F

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3k 1H NMR (400 MHz, CDCl3)

NN

I

S OO

S

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3k 13C NMR (100 MHz, CDCl3)

NN

I

S OO

S

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3l 1H NMR (400 MHz, CDCl3)

NN

I

CH3

Ms

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3l 13C NMR (100 MHz, CDCl3)

NN

I

CH3

Ms

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3m 1H NMR (400 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3m 13C NMR (100 MHz, CDCl3)

NN

I

F

Ms

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3n 1H NMR (400 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3n 13C NMR (100 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3o 1H NMR (400 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3o 13C NMR (100 MHz, CDCl3)

NN

I

Me

Ts

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3p 1H NMR (400 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3p 13C NMR (100 MHz, CDCl3)

NN

I

F

Ts

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3q 1H NMR (400 MHz, CDCl3)

NN

I

Cl

Ts

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3q 13C NMR (100 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3r 1H NMR (400 MHz, CDCl3)

NN

I

Br

Ts

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3r 13C NMR (100 MHz, CDCl3)

NN

I

Br

Ts

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3s 1H NMR (400 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3s 13C NMR (100 MHz, CDCl3)

NBn

N

I

Ts

F

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3t 1H NMR (400 MHz, CDCl3)

N NN

I

F

Ts

Cl

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3t 13C NMR (100 MHz, CDCl3)

N NN

I

F

Ts

Cl

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3u 1H NMR (400 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3u 13C NMR (100 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3v1H NMR (400 MHz, CDCl3)

NN

O2N

S OO

I

F

S

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3v 13C NMR (100 MHz, CDCl3)

NN

O2N

S OO

I

F

S

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3w 1H NMR (400 MHz, CDCl3)

NN

S OO

Br

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

3w 13C NMR (100 MHz, CDCl3)

NN

S OO

Br

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4a 1H NMR (400 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4a 13C NMR (100 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4b 1H NMR (400 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4b 13C NMR (100 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4c 1H NMR (400 MHz, CDCl3)

NN

Ms

Cl

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4c 1H NMR (400 MHz, CDCl3)

NN

Ms

Cl

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4d 1H NMR (400 MHz, CDCl3)

NN

Ms

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4d 13C NMR (100 MHz, CDCl3)

NN

Ms

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4e 1H NMR (400 MHz, CDCl3)

NN

Ts

F

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4e 13C NMR (100 MHz, CDCl3)

NN

Ts

F

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4f 1H NMR (400 MHz, CDCl3)

NN

Ts

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4f 13C NMR (100 MHz, CDCl3)

NN

Ts

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4g 1H NMR (400 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4g 13C NMR (100 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4h 1H NMR (400 MHz, CDCl3)

NN

Ts

Br

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4h 13C NMR (100 MHz, CDCl3)

NN

Ts

Br

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4i 1H NMR (400 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4i 13C NMR (100 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4j 1H NMR (400 MHz, CDCl3)

NN

S OO

S

F

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4j 13C NMR (100 MHz, CDCl3)

NN

S OO

S

F

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4k 1H NMR (400 MHz, CDCl3)

NN

S OO

S

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4k 13C NMR (100 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4l 1H NMR (400 MHz, CDCl3)

N NMs

CH3

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4l 13C NMR (100 MHz, CDCl3)

N NMs

CH3

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4m 1H NMR (400 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4m 13C NMR (100 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4n 1H NMR (400 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4n 13C NMR (100 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4o 1H NMR (400 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4o 13C NMR (100 MHz, CDCl3)

N NTs

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4p 1H NMR (400 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4p 13C NMR (100 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4q 1H NMR (400 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4q 13C NMR (100 MHz, CDCl3)

N NTs

Cl

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4r 1H NMR (400 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4r 13C NMR (100 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4s 1H NMR (400 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4s 13C NMR (100 MHz, CDCl3)

NN

Ts

F

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4t 1H NMR (400 MHz, CDCl3)

N NN

Ts

F

Cl

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4t 13C NMR (100 MHz, CDCl3)

N NN

Ts

F

Cl

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4u 1H NMR (400 MHz, CDCl3)

N

MeO

NS O

O

S

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4u 13C NMR (100 MHz, CDCl3)

N

MeO

NS O

O

S

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4v 1H NMR (400 MHz, CDCl3)

N

O2N

N

F

S OO

S

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013

4v 13C NMR (100 MHz, CDCl3)

Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013