appendix g flysheets 4th qtr 2008 - boeing · d 0.00000182 78.0 17 - 15713c-ocdf ocdf n d...

TestAmerica 61

101

TestAmerica 62

102

TestAmerica 63

103

TestAmerica 64

104

TestAmerica 65

105

TestAmerica 66

106

TestAmerica 67

107

TestAmerica 68

108

TestAmerica 69

109

TestAmerica 70

110

TestAmerica 71

111

TestAmerica 72

112

TestAmerica 73

113

TestAmerica 74

114

115

116

117

118

119

120

121

122

123

124

125

126

127

128

129

130

TestAmerica St. Louis

LOT # F8L170177-REV 1 1 of 13

131

TestAmerica St. Louis

LOT # F8L170177-REV 1 2 of 13

132

TestAmerica St. Louis

LOT # F8L170177-REV 1 3 of 13

133

TestAmerica St. Louis

LOT # F8L170177-REV 1 4 of 13

134

TestAmerica St. Louis

LOT # F8L170177-REV 1 5 of 13

135

TestAmerica St. Louis

LOT # F8L170177-REV 1 6 of 13

136

TestAmerica St. Louis

LOT # F8L170177-REV 1 7 of 13

137

TestAmerica St. Louis

LOT # F8L170177-REV 1 8 of 13

138

TestAmerica St. Louis

LOT # F8L170177-REV 1 9 of 13

139

TestAmerica St. Louis

LOT # F8L170177-REV 1 10 of 13

140

TestAmerica St. Louis

LOT # F8L170177-REV 1 11 of 13

141

TestAmerica St. Louis

LOT # F8L170177-REV 1 12 of 13

142

TestAmerica St. Louis

LOT # F8L170177-REV 1 13 of 13

143

144

Section I: Sample Inventory ReportDate Received:

Vista Lab. ID Client Sample ID

12/17/2008

31268-001 IRL1714-01

Project 31268 Page 2 of 217

145

SECTION II

Project 31268 Page 3 of 217

146

EPA

Met

hod

1613

Met

hod

Bla

nk

Mat

rix:

Sam

ple

Size

:

Lab

Sam

ple:

QC

Bat

ch N

o.:

Dat

e Ex

tract

ed:

Aqu

eous

17-D

ec-0

81.

00 L

0-M

B00

1

Dat

e A

naly

zed

DB

-5:

18-D

ec-0

8D

ate

Ana

lyze

d D

B-2

25:

NA

1770

Qua

lifie

rsD

LA

nal y

teL

abel

ed S

tand

ard

%R

LC

L-U

CL

Qua

lifie

rsE

MPC

bd

(ug/

L)

aC

onc.

2,3,

7,8-

TCD

DN

D0.

0000

0095

894

.025

- 16

4IS

13C

-2,3

,7,8

-TC

DD

1,2,

3,7,

8-Pe

CD

DN

D0.

0000

0250

101

25 -

181

13C

-1,2

,3,7

,8-P

eCD

D1,

2,3,

4,7,

8-H

xCD

DN

D0.

0000

0182

84.4

32 -

141

13C

-1,2

,3,4

,7,8

-HxC

DD

1,2,

3,6,

7,8-

HxC

DD

ND

0.00

0001

7195

.728

- 13

013

C-1

,2,3

,6,7

,8-H

xCD

D1,

2,3,

7,8,

9-H

xCD

DN

D0.

0000

0164

89.5

23 -

140

13C

-1,2

,3,4

,6,7

,8-H

pCD

D1,

2,3,

4,6,

7,8-

HpC

DD

ND

0.00

0002

7974

.117

- 15

713

C-O

CD

DO

CD

DN

D0.

0000

0430

92.8

24 -

169

13C

-2,3

,7,8

-TC

DF

2,3,

7,8-

TCD

FN

D0.

0000

0088

790

.124

- 18

513

C-1

,2,3

,7,8

-PeC

DF

1,2,

3,7,

8-Pe

CD

FN

D0.

0000

0118

97.0

21 -

178

13C

-2,3

,4,7

,8-P

eCD

F2,

3,4,

7,8-

PeC

DF

ND

0.00

0001

0791

.126

- 15

213

C-1

,2,3

,4,7

,8-H

xCD

F1,

2,3,

4,7,

8-H

xCD

FN

D0.

0000

0051

285

.926

- 12

313

C-1

,2,3

,6,7

,8-H

xCD

F1,

2,3,

6,7,

8-H

xCD

FN

D0.

0000

0059

286

.928

- 13

613

C-2

,3,4

,6,7

,8-H

xCD

F2,

3,4,

6,7,

8-H

xCD

FN

D0.

0000

0069

689

.929

- 14

713

C-1

,2,3

,7,8

,9-H

xCD

F1,

2,3,

7,8,

9-H

xCD

FN

D0.

0000

0105

80.2

28 -

143

13C

-1,2

,3,4

,6,7

,8-H

pCD

F1,

2,3,

4,6,

7,8-

HpC

DF

ND

0.00

0001

5383

.226

- 13

813

C-1

,2,3

,4,7

,8,9

-HpC

DF

1,2,

3,4,

7,8,

9-H

pCD

FN

D0.

0000

0182

78.0

17 -

157

13C

-OC

DF

OC

DF

ND

0.00

0001

5995

.035

- 19

7C

RS

37C

l-2,3

,7,8

-TC

DD

Tot

als

Foot

note

s

Tota

l TC

DD

ND

0.00

0000

958

a. S

ampl

e sp

ecifi

c es

timat

ed d

etec

tion

limit.

Tota

l PeC

DD

ND

0.00

0002

50b.

Est

imat

ed m

axim

um p

ossi

ble

conc

entra

tion.

Tota

l HxC

DD

ND

0.00

0001

72c.

Met

hod

dete

ctio

n lim

it.

Tota

l HpC

DD

ND

0.00

0002

79d.

Low

er c

ontro

l lim

it - u

pper

con

trol l

imit.

Tota

l TC

DF

ND

0.00

0000

887

Tota

l PeC

DF

ND

0.00

0002

18To

tal H

xCD

FN

D0.

0000

0069

2To

tal H

pCD

FN

D0.

0000

0166

App

rove

d B

y:A

naly

st:

MA

SW

illia

m J.

Luk

sem

burg

1

9-D

ec-2

008

11:1

3

Proj

ect3

1268

Page

4of

217

147

EPA

Met

hod

1613

OPR

Res

ults

Mat

rix:

1.00

LSa

mpl

e Si

ze:

Aqu

eous

1770

QC

Bat

ch N

o.:

Dat

e Ex

tract

ed:

17-D

ec-0

8

Lab

Sam

ple:

0-O

PR00

1

Dat

e A

naly

zed

DB

-5:

18-D

ec-0

8D

ate

Ana

lyze

d D

B-2

25:

NA

Con

c. (n

g/m

L)

Ana

l yte

Lab

eled

Sta

ndar

d%

RL

CL

-UC

LSp

ike

Con

c.O

PR L

imits

Qua

lifie

r2,

3,7,

8-TC

DD

8.63

89.2

25 -

164

IS10

.06.

7 - 1

5.8

13C

-2,3

,7,8

-TC

DD

1,2,

3,7,

8-Pe

CD

D47

.896

.725

- 18

150

.035

- 71

13C

-1,2

,3,7

,8-P

eCD

D1,

2,3,

4,7,

8-H

xCD

D46

.877

.132

- 14

150

.035

- 82

13C

-1,2

,3,4

,7,8

-HxC

DD

1,2,

3,6,

7,8-

HxC

DD

46.3

91.1

28 -

130

50.0

38 -

6713

C-1

,2,3

,6,7

,8-H

xCD

D1,

2,3,

7,8,

9-H

xCD

D45

.784

.023

- 14

050

.032

- 81

13C

-1,2

,3,4

,6,7

,8-H

pCD

D1,

2,3,

4,6,

7,8-

HpC

DD

46.3

67.9

17 -

157

50.0

35 -

7013

C-O

CD

DO

CD

D95

.688

.624

- 16

910

078

- 14

413

C-2

,3,7

,8-T

CD

F2,

3,7,

8-TC

DF

8.58

88.4

24 -

185

10.0

7.5

- 15.

813

C-1

,2,3

,7,8

-PeC

DF

1,2,

3,7,

8-Pe

CD

F46

.791

.121

- 17

850

.040

- 67

13C

-2,3

,4,7

,8-P

eCD

F2,

3,4,

7,8-

PeC

DF

48.7

88.6

26 -

152

50.0

34 -

8013

C-1

,2,3

,4,7

,8-H

xCD

F1,

2,3,

4,7,

8-H

xCD

F45

.281

.126

- 12

350

.036

- 67

13C

-1,2

,3,6

,7,8

-HxC

DF

1,2,

3,6,

7,8-

HxC

DF

47.5

81.0

28 -

136

50.0

42 -

6513

C-2

,3,4

,6,7

,8-H

xCD

F2,

3,4,

6,7,

8-H

xCD

F45

.783

.529

- 14

750

.035

- 78

13C

-1,2

,3,7

,8,9

-HxC

DF

1,2,

3,7,

8,9-

HxC

DF

46.6

74.7

28 -

143

50.0

39 -

6513

C-1

,2,3

,4,6

,7,8

-HpC

DF

1,2,

3,4,

6,7,

8-H

pCD

F45

.079

.526

- 13

850

.041

- 61

13C

-1,2

,3,4

,7,8

,9-H

pCD

F1,

2,3,

4,7,

8,9-

HpC

DF

44.9

73.1

17 -

157

50.0

39 -

6913

C-O

CD

FO

CD

F89

.584

.035

- 19

7C

RS

100

63 -

170

37C

l-2,3

,7,8

-TC

DD

Ana

lyst

:M

AS

Will

iam

J. L

ukse

mbu

rg

19-

Dec

-200

8 11

:13

App

rove

d B

y:

Proj

ect3

1268

Page

5of

217

148

Sam

ple

ID:

IRL

1714

-01

EPA

Met

hod

1613

Clie

nt D

ata

Nam

e:Pr

ojec

t:D

ate

Col

lect

ed:

Sam

ple

Dat

a

Mat

rix:

Sam

ple

Size

:

Lab

orat

ory

Dat

a

Lab

Sam

ple:

QC

Bat

ch N

o.:

Dat

e R

ecei

ved:

Dat

e Ex

tract

ed:

Aqu

eous

17-D

ec-0

817

-Dec

-08

15-D

ec-0

81.

02 L

3126

8-00

1IR

L171

4

Dat

e A

naly

zed

DB

-5:

18-D

ec-0

8D

ate

Ana

lyze

d D

B-2

25:

NA

Test

Am

eric

a-Ir

vine

, CA

1770

Tim

e C

olle

cted

:11

30

Qua

lifie

rsD

LA

naly

teL

abel

ed S

tand

ard

%R

LC

L-U

CL

Qua

lifie

rsE

MPC

ab

d (u

g/L

)C

onc.

2,3,

7,8-

TCD

DN

D0.

0000

0069

310

825

- 16

4IS

13C

-2,3

,7,8

-TC

DD

1,2,

3,7,

8-Pe

CD

DN

D0.

0000

0208

114

25 -

181

13C

-1,2

,3,7

,8-P

eCD

D1,

2,3,

4,7,

8-H

xCD

DN

D0.

0000

0409

98.2

32 -

141

13C

-1,2

,3,4

,7,8

-HxC

DD

1,2,

3,6,

7,8-

HxC

DD

ND

0.00

0003

9910

528

- 13

013

C-1

,2,3

,6,7

,8-H

xCD

D1,

2,3,

7,8,

9-H

xCD

DN

D0.

0000

0375

99.9

23 -

140

13C

-1,2

,3,4

,6,7

,8-H

pCD

D1,

2,3,

4,6,

7,8-

HpC

DD

0.00

0011

4J

82.3

17 -

157

13C

-OC

DD

OC

DD

0.00

0171

106

24 -

169

13C

-2,3

,7,8

-TC

DF

2,3,

7,8-

TCD

FN

D0.

0000

0057

711

024

- 18

513

C-1

,2,3

,7,8

-PeC

DF

1,2,

3,7,

8-Pe

CD

FN

D0.

0000

0132

106

21 -

178

13C

-2,3

,4,7

,8-P

eCD

F2,

3,4,

7,8-

PeC

DF

ND

0.00

0001

5010

826

- 15

213

C-1

,2,3

,4,7

,8-H

xCD

F1,

2,3,

4,7,

8-H

xCD

FN

D0.

0000

0088

395

.126

- 12

313

C-1

,2,3

,6,7

,8-H

xCD

F1,

2,3,

6,7,

8-H

xCD

FN

D0.

0000

0110

95.6

28 -

136

13C

-2,3

,4,6

,7,8

-HxC

DF

2,3,

4,6,

7,8-

HxC

DF

ND

0.00

0001

3410

129

- 14

713

C-1

,2,3

,7,8

,9-H

xCD

F1,

2,3,

7,8,

9-H

xCD

FN

D0.

0000

0198

94.3

28 -

143

13C

-1,2

,3,4

,6,7

,8-H

pCD

F1,

2,3,

4,6,

7,8-

HpC

DF

ND

0.00

0002

6092

.426

- 13

813

C-1

,2,3

,4,7

,8,9

-HpC

DF

1,2,

3,4,

7,8,

9-H

pCD

FN

D0.

0000

0183

84.5

17 -

157

13C

-OC

DF

OC

DF

0.00

0005

16J

89.7

35 -

197

CR

S37

Cl-2

,3,7

,8-T

CD

D

Tot

als

Foot

note

s

a. S

ampl

e sp

ecifi

c es

timat

ed d

etec

tion

limit.

Tota

l TC

DD

ND

0.00

0000

693

b. E

stim

ated

max

imum

pos

sibl

e co

ncen

tratio

n.To

tal P

eCD

DN

D0.

0000

0208

c. M

etho

d de

tect

ion

limit.

Tota

l HxC

DD

ND

0.00

0003

94d.

Low

er c

ontro

l lim

it - u

pper

con

trol l

imit.

Tota

l HpC

DD

0.00

0027

0To

tal T

CD

FN

D0.

0000

0057

7To

tal P

eCD

FN

D0.

0000

0202

Tota

l HxC

DF

ND

0.00

0002

63To

tal H

pCD

FN

D0.

0000

0543

Will

iam

J. L

ukse

mbu

r g

19-

Dec

-200

8 11

:13

App

rove

d B

y:A

naly

st:

MA

S

Proj

ect3

1268

Page

6of

217

149

APPENDIX

Project 31268 Page 7 of 217

150