o me 4 6 ho 5 - pdfs.semanticscholar.org€¦figure 3 13c-nmr (125 mhz) spectrum of moscatilin...

Figure 1 1H-NMR (500 MHz) spectrum of Moscatilin (acetone-d6)

Figure 2 1H-NMR (500 MHz) spectrum of Moscatilin (acetone-d6)

MeO

HO

OMe

OMe

OH

1

2

3

45

6

1'

2'

3'

4'

5'

6'

'

MeO

HO

OMe

OMe

OH

1

2

3

45

6

1'

2'

3'

4'

5'

6'

'

Figure 3 13C-NMR (125 MHz) spectrum of Moscatilin (acetone-d6)

Figure 4 1H-NMR (300 MHz) spectrum of Flavanthrinin (CDCl3)

MeO

HO

OMe

OMe

OH

1

2

3

45

6

1'

2'

3'

4'

5'

6'

'

HO OH

MeO

1

2

34

4a4b

56

7

8 8a

9 10

10a

Figure 5 NOSEY spectrum of Flavanthrinin

Figure 6 13C-NMR (75 MHz) spectrum of Flavanthrinin (CDCl3)

HO OH

MeO

1

2

34

4a4b

56

7

8 8a

9 10

10a

HO OH

MeO

1

2

34

4a4b

56

7

8 8a

9 10

10a

Figure 7 1H-NMR (500 MHz) spectrum of Gigantol (acetone-d6)

Figure 8 1H-NMR (500 MHz) spectrum of Gigantol (acetone-d6)

MeO

OH

OMe

OH

1

2

3

4

5

6

1'

2'3'

4'

5'

6'

'

MeO

OH

OMe

OH

1

2

3

4

5

6

1'

2'3'

4'

5'

6'

'

Figure 9 13C-NMR (125 MHz) spectrum of Gigantol (acetone-d6)

Figure 10 NOESY spectrum of compound Gigantol (acetone-d6)

MeO

OH

OMe

OH

1

2

3

4

5

6

1'

2'3'

4'

5'

6'

'

MeO

OH

OMe

OH

1

2

3

4

5

6

1'

2'3'

4'

5'

6'

'

Figure 11 DEPT 135 spectrum of Gigantol (acetone-d6)

Figure 12 1H-NMR (500 MHz) spectrum of Lusianthridin (acetone-d6)

MeO

OH

OMe

OH

1

2

3

4

5

6

1'

2'3'

4'

5'

6'

'

HO OMe

HO

1

2

3456

7

8a 10a8

9 10

4a4b

Figure 13 NOESY spectrum of Lusianthridin (acetone-d6)

Figure 14 13C-NMR (125 MHz) spectrum of Lusianthridin (acetone-d6)

HO OMe

HO

1

2

3456

7

8a 10a8

9 10

4a4b

Figure 15 1H-NMR (500 MHz) spectrum of Nobilone (acetone-d6)

OH

MeO

HO

O

1

2

34

4b 4a

56

7

88a

9 9a

Figure 16 13C-NMR (125 MHz) spectrum of Nobilone (acetone-d6)

Figure 17 HMBC spectrum of Nobilone (acetone-d6)

OH

MeO

HO

O

1

2

34

4b 4a

56

7

88a

9 9a

OH

MeO

HO

O

1

2

34

4b 4a

56

7

88a

9 9a

Figure 18 NOESY spectrum of Nobilone (acetone-d6)

Figure 19 1H-NMR (500 MHz) spectrum of Dendroflorin (acetone-d6)

OH

MeO

HO

O

1

2

34

4b 4a

56

7

88a

9 9a

OH

MeO

O

1

2

34

4b 4a

56

7

8 8a9 9a

HO

OH

Figure 20 1H-NMR (500 MHz) spectrum of Dendroflorin (acetone-d6)

Figure 21 NOESY spectrum of Dendroflorin (acetone-d6)

OH

MeO

O

1

2

34

4b 4a

56

7

8 8a9 9a

HO

OH

OH

MeO

O

1

2

34

4b 4a

56

7

8 8a9 9a

HO

OH

Figure 22 13C-NMR (125 MHz) spectrum of Dendroflorin (acetone-d6)

Figure 23 1H-NMR (300 MHz) spectrum of Denchrysan B (acetone-d6)

OH

MeO

O

1

2

34

4b 4a

56

7

8 8a9 9a

HO

OH

OH

MeOOH

HO

1

34

4a4b

56

7

8 8a 9 9a

2

Figure 24 13C-NMR (75 MHz) spectrum of Denchrysan B (acetone-d6)

Figure 25 HMBC spectrum of Denchrysan B (acetone-d6)

OH

MeOOH

HO

1

34

4a4b

56

7

8 8a 9 9a

2

OH

MeOOH

HO

1

34

4a4b

56

7

8 8a 9 9a

2

Figure 26 1H-NMR (300 MHz) spectrum of Tristin (acetone-d6)

Figure 27 13C-NMR (75 MHz) spectrum of Tristin (acetone-d6)

OH

OMe

OH

1

2

3

45

6

1'

2'

3'

4'

5'

6'

'

HO

OH

OMe

OH

1

2

3

45

6

1'

2'

3'

4'

5'

6'

'

HO

Figure 28 HMBC spectrum of Tristin (acetone-d6)

Figure 29 NOESY spectrum of Tristin (acetone-d6)

OH

OMe

OH

1

2

3

45

6

1'

2'

3'

4'

5'

6'

'

HO

OH

OMe

OH

1

2

3

45

6

1'

2'

3'

4'

5'

6'

'

HO