analytical data reports antrim iron works site … · 2020. 8. 27. · thall ium vanadium zinc f s...

H Q 0 0 0 0 0 4 0

ANALYTICAL DATA REPORTS

ANTRIM IRON WORKS SITE

VOLUME II

MARCH, 1988

ENVIRONMENTAL & SAFETY DESIGNS. INC.

Memphis, TN

EPA Region 5 Records Ctr.

209184

TABLE OF CONTENTS

TAB 1 - INTRODUCTION AND DATA SUMMARY

TAB 2 - CASE 1 DATA PACKAGE

TAB 3 - CASE 2 DATA PACKAGE

ANALYTICAL RESULTS FROMTHE ANTRIM IRON WORKS SITE

(aka TAR LAKE)VOLUME II

INTRODUCTIONThe following are the raw data reports from CompuChemLaboratories for sampling events conducted as part of the RI/FSfor the Antrim Iron Works Site. The sampling was conducted byEnvironmental & Safety Designs, Inc. on behalf of Fifty-SixthCentury Antrim Iron Co., New York, NY. This volume containsresults of analyses for metals and cyanide. Volatile andsemi-volatile results are reported in Volume I.

SAMPLING HISTORYThe data is organized as two sampling cases as reported by thelaboratory. Case 1 (Tab 2) contains samples collected onJanuary 27, 1988 and includes Monitoring Wells 15 and 16. Case2 (Tab 3) contains samples collected on January 20, 1988,January 25, 1988 and February 3, 1988 and includes MonitoringWells 6, 7, 11, 12, 13, 14, and a field blank. In additionthere is an identified duplicate of Well 14, called Well-14-DUP,and a blind duplicate of monitoring well 11. The blindduplicate is identifed as well 21. The table belowcross-references field identification numbers, laboratorynumbers, and sampling locations.

Sampling Location Cro»s-R«f«r«nce

FIELD IDNUMBER

LABORATORYID NUMBER

DATESAMPLED

SAMPLINGLOCATION

CASE 1:MW-15MW-16

CASE 2:0188110188120188210188FB2WELL-6WELL-7WELL-13WELL-14WELL-14-DUP

177713 1/27/88 Monitoring Well 15177707 1/27/88 Monitoring Well 16

176659 1/20/88 Monitoring Well 11176666 1/20/88 Monitoring Well 12176668 1/20/88 Blind duplicate Well 11176670 1/20/88 Field Blank177380 1/25/88 Monitoring Well 6177381 1/25/88 Monitoring Well 7179006 2/03/88 Monitoring Well 13179007 2/03/88 Monitoring Well 14179008 2/03/88 Duplicate - Well 14

The following tables summarize the results reported in thisvolume. A complete QA/QC review by EPA, DNR, and EnSafe will beperformed prior to use of this data.

[Note: The Sampling PLan and Quality Assurance Plan for thissampling event specified that Monitoring Well 10 would besampled and analyzed for metals and cyanide also. However thewell was found to be dry and Monitoring Well 13 was substitutedfor Monitoring Well 10. This substitution was reviewed andapproved in the field by the Tar Lake Remedial Project Manager.]

RESULTS OF THE ANALYSES

SUMMARY OF INORGANICS DATA

ANTRIM IRON WORKS SITE

(ug/l)

PARAMETER WELL 6 WELL 7 WELL 11 WELL 11 WELL 12 WELL 13

(DUP)

Aluminum H70 430 [119] C1121 [87] 430

Antimony 5311 53U 53U 53U 53U 530

Arsenic 14 [2.1] [8.7] 19 1.50 [6.0]

Barium [25]E [22]E [13)E [11]E [33]E [361E

••rylltum 1.00 1.0U 1.0U t.OU C1.21 LOU

Cadmium 5.00 5.0U 5.0U 5.0U 5. 00 5.00

Calcium 81200 87900 108000 113000 92900 92700

Chromium 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U

Cobalt [8.4] 5.00 [9.4] [9.4] [7.2] [6.3]

Copper [21] 26 26 26 20U 20U

Iron 7700 1190 2130 1810 280 3150

Lead 6.2 [4.9] 2.5U 2.5U 2.5U 5.5

Magnesium 12600 13400 8310 8740 19500 12600

Manganese 334E 439E 107E 106E 2.0UE 317E

Mercury 0.20U 0.20U 0.20U 0.20U 0.20U 0.20U

Nickel 39U 39U 39U 39U 39U 39U

Potassium 34000 24000 24000 24000 21100 7590

Selenium 6.50 N 1.3O N 6.5U N 6.5U N [9.1] N 1.30 N

Silver 8.0U S.Oo 8.00 8.00 8. 00 8.00

Sodium [3450] 8460 [3380] [3520] [3930] [2970]

Thallium 2.20 2.20 2.2U 2.20 2.20 2.20

Vanadium [9.4] 3.0O [7.8] [8.2] [5.0] [4.4]

Zinc 1070 268 72 123 134 134

Cyanide 100 100 100 100 66 100

NOTES:

WELL 14

1530

53U

1.50

[191E

1.005.00

59100

C9.3]

[9.2]

26

2650

7.4

12300

80E

0.200

39U

24000

1.30 N

a. oo(30301

2.20

[6.31

646

100

(1 = A value is reported in brackets if the result is a value greater than the

less than the CLP's contract-required detection limit.

E = Indicates a value estimated or not reported due to the presence

cover sheet.

0 = Indicates element was analyzed for but not detected. Value is

N = Indicates sample spike recovery is not within control limits.

S = Indicates value determined by method of standard additions.

* = Indicates duplicate analysis is not within control limits.

WELL 14

(OOP)

828

53U

1.50

[141E

1.00

5.00

52900

[6.0]

5.00

200

1620

[5.0]

10900

49E

0.200

390

24000

6.50 N

21

C2190I

2.20

3.00

587

100

WELL 15 WELL 16

2040 N* 4320 N*

53U 53U

[5.4] [3.4]

[20] [27]

1.00 1.0U

5.00 5.00

78600 90700*

C7.6] 14

[5.2] [6.4]

200 200

4220 6130

[4.5] 32 S

13300 24600

198 246

0.200N 0.200N

390 390

[4430] 24000

6.50 EN 6.50 EN

8.00 8.00

[2620] [4280]

2.20 2.20

[8.61 [11]

751 • 6410 *

178 100

instrument detetction limit

of interference. See explanatory note

FIELD

BLNK

43U

53U

1.50

M.71E

I.Ou

S.Ou

[841]

5.00

[6.9]

20U

[75]

2.5U

[535]

2.00E

0.200

390

24000

1.30N

8.00

[3040]

2.2U

[3.3]

77

100

but

on

the instrument detetction l imit.

c

\ I•X VX

LiGCND

o Snoilo* Or-&te Well Lxotto

• Sfxmow Off '&te Well Locott

(ft Oeep Or-Stte Wttl Locotion

ANTRIM IRON WORKS SITE' ' '

GOMPUCHEMLABORATORIES

Mr. Phil CoopEnsafe5705 Stage Rd./Suite 212Memphis TN 381J4

March 15, 1988

MI60B

Subject: Report of Data - Account Number 178202

Dear Mr. Coop:

Enclosed herewith are the results of analytical work performed inaccordance with the referenced account number.

This report covers 2 sample(s) and Quality Control Data receivedby CompuChem@ on January 28, 1988.

If you have any questions regarding this package, please contact yourservice representative at 1-919-549-8263.

Sincerely,

Mary M/tchel lSupervisor, Report Del iverables

Enclosurescw

Sample ID: MU-16, MW-15

C/C Numbers: 177707, 177713

cc: Accounting (cover letter only)

COMF'UCHFMl ABOHATORIFS INC P O Rox 1 ?65? 3308 rrmpel Hill < Nelson Highway Research Ti anglp P.iffc NC 27709 [919| *>49-fl?63

OOMPUCHEMLABORATORIES

March 15, 1988

Mr. Phil CoopEnsafe5705 Stage Rd./Suite 212Memphis TN 38134

Subject: Report of Data - Account Number 178202

Dear Mr. Coop:

Enclosed herewith are the results of analytical work performed inaccordance with the referenced account number.

This report covers 2 sample(s) and Quality Control Data receivedby CompuChemta on January 28, 1988.

If you have any questions regarding this package, please contact yourservice representative at 1-919-549-8263.

Sincerely,

Mary M/tchellSupervisor, Report Deliverables

Enclosurescw

Sample ID: MW-16, MW-15

C/C Numbers: 177707, 177713

cc: Accounting (cover letter only)

COMPUCHEM LABORATORIES INC P O Box 12652 3308 Criapel Hill/Nelson Highway Research Triangle Park, NC 27709 (9191549-8263

S. EPA Contract Laboratory Programimple Management OfficeO. Box 818 - Alexandria, VA 22313'••/557-2490 FTS: 8-557-2490 Date 3/ 2/88

COVER PAGEINORGANIC ANALYSES DATA PACKAGE

ib Name CompuChem Labora to_r ies

)W No. 785

Case No. 13562

Q.C. Report No. 13562A

Receipt Date 01/28/88

Sample Numbers

'A No.

,#-16

Lab ID No.

177707

177713

EPA No. Lab ID No.

imments : Mercury :

Cyanide :

177708177709177710177711177712

SSD

LC!SS

177707)177713)

177707 )D( 177707 )

interelement and Backgroundcorrection!; appl ied?yes, corrections applied before _X__ or after

Yes X Nogeneration ol raw data

lotnotes :< - Notirml :\lue -

required by contract at this time

If the result is a value greater than or equal to the instrumentdetection limit but less than the contract-required detection limit,report the value in brackets (i.e., [10]). Indicate the analyticalmethod used with P (for ICP), A (for Flame AA), or F (for Furnace AA)Indicates element was analyzed for but not detected. Report with theinstrument detection l i m i t value (e.g., 10U).Indicates a value estimated or not reported due to the presence ofinterference. Explanatory note included on cover page.Indicates value determined by Method of Standard Addition.Indicates spike sample recovery is not within control limits.Indicates duplicate analysis is not within control limits.Indicates the correlation coefficient for method of standard additioris less than 0.995Indicates duplicate injection results exceeded control limits.

idicate method used: P for ICP; A for Flame AA and F for Furnace

FORM I

U ; . EPA CONTRACT LABORATORY PROGRAMS 1PLE MANAGEMENT OFFICEP ). BOX 818 - ALEXANDRIA, VA 223137

FORM I

U i. EPA CONTRACT LABORATORY PROGRAMS IPLE MANAGEMENT OFFICEP ). BOX 818 - ALEXANDRIA, VA 223137 !/557-2490 FTS: 8-557-2490

EPA SAMPLE NO.MW-16

DATE 3/ 2/88

INORGANIC ANALYSIS DATA SHEET

L 1 NAME: COMPUCHEM LABORATORIES CASE NO: 13562

s

L.

/ NO: 785

1 SAMPLE ID. NO 177707

Lab Recei

QC REPORT

pt Date

NO 1

01/28/88

3562A

ELEMENTS IDENTIFIED AND MEASURED

C

M

111

C

F

JCENTRATION:

'RIX: WATER

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperI ronLead

mide

)tnotes : For re

LOW XXX

XXX SOIL

( ug/1 )or

4320 N*53U

[3.4][27]1 .OU5.0U

90700 *14

[6.4]20u

613032 S

10U

porting resul

MEDIUM

SLUDGE OTHER

mg/kg

penpFPPPP (J"'PPPPF

ts to

DRY

1314151617181920212223

EPA,

WEIGHT (circle one)

. Magnesium 24600

. Manganese

. Mercury fl/T)

. Nickel

. Potassium

. Selenium f̂

. Silver

. Sodium

. Thallium

. Vanadium

. Zinc J~

Percent Solids(

standard result

246.20U39u

2400U6.5Ufl.Ou

[ 4280 ]2.2U[H]

6410

%)

PP

N CVPP

EN PPPFP

* P

qualifiers are usedas defined on Cover Page. Additional flags or footnotes explainingresults are encouraged. Definitions of such flags must be explicitand contained on Cover Page, however.

C iments:CLOUDY, LIGHT BROWN

LAB MANAGER

Form II

NAME

Q. C. Report No. 13625B

INITIAL AND CONTINUING CALIBRATION VERIFICATION (3)

COMPUCHEM LABORATORIES CASE NO. 13562

Page 1

SOW NO. 785

3/ 2/88 UNITS: ug/L

C »pound initial Calib.(l) Continuing Calibrat ion( 2 )

M :als:1 AluminumZ Antimony3 Arsenic4 Barium5 Beryllium6 Cadmium7 Calcium0 Chromium9 Cobalt1 Copper1 I ron1 LeadT Magnesium1 Manganese1 Me r cu ry1 Nickel1 Potassium1 Seleni um1 Si Ive r2 Sodium2 Thallium2 Vanadium2 . Zinc0 »e r :

C mide

TrueValue

101047.01980

481 .0489.049800506.0474 . 0542.0199039.2

25000513.05.20

496.050200104.0509.05070038.9

511.03100

210.0

Found20021006

- 4 9 . 41921

494 .6492. 150760486.1491 .0527 . 1197141.3

25640506.5TTW476.249320rosvei

~4T9T9~51630~35.T513.63000

%RT0~l10010597

10310110296

1CF49799

[ 10510399949698

;~nrr96

1029T

10197

i

221 . 3 105

TrueValue10000100047.0100010001000

100000100010001000

1000039.2

10000010005.201000

100000104 .01000

10000038.910001000

210.0

Found10250101648.9

906. 410601032

101900101410101013

1003039.0'

10270010014.SS1039

103900ni .cr1023

10310038.610591026

225.6

%RT0*21021049910610310210110110110099

103100941041041HT710210399106103

107

Found" 10340

102649.2986.610551047

940401014101610211006036.9

9^67010064.5B1014

97170106 .71032

96730

10671035

221 . 3

&10310599

10610594

101102102101949610189

10197

1031039T

107104

105

(4)Method

PPFPPPPPPPPFPPCVPPFPPFPP

CN

1 nitial Calibration Source EPA/ERA 2 Continuing Calibration Source EPA/ER/

3 :ontrol Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115

4 ndicate Analytical Method Used: P - ICP; A - Flame AA; F - Furnace AAA

Form II

L i NAME

D 'E




SOW NO.

UNITS:

Page 2

785

3/ 2/88

initial Calib.(l)

ug/L

Continuing Calibration(2)

M a 1 s :1 Aluminum2 Antimony3 Arsenic4 Barium5 Beryllium6 Cadmium7 Calcium8 Chromium9 Cobalt1 Copper1 I ron1 Lead1 Magnesium1 Manganese1 Mercury1 Nickel1 Potassium1 Selenium1 Silver2 Sodium2 Thallium2 Vanadium2 Zinc0 i e r :

C mide

TrueValue Found %R

TrueVaTueTWOO1000

100010001000

100000100010001000

loooolOOOOOj

10005 .201000

100000

1000100000

10001000

210.0

Found~ro? o"o

1037

992 .210561057

101200101210231026

10.140

10360010164 .751014

104200

1068104000

10751044

214.9

%R104104

99106106101101102103101

10410292

101104

107104

108104

102

Found102301025

972.71031103B

1022001002

998.7IOCS9891

104300991 . 1

1015104900

1031104400

10521015

206.4

%RTU2102

971

103104102100

L 10010199

10499

102105

103104

105102

98

MethodPP

PPPP iP !PPP

PPCVP jP

PP

PP

CN

1 :nitial Calibration Source EPA/ERA 2 Continuing Calibration Source EPA/ER/

3 'ontrol Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115


Form II

L 1 NAME




SOW NO. 785

UNITS:

Page 3

3/ 2/88

Initial Calib.(1)

ug/L

Continuing Calibration(2)

M als:1 Aluminum2 Antimony3 Arsenic4 Barium5 Beryllium6 Cadmium7 Calcium8 Chromium9 Cobalt1 Copper1 I ron1 Lead1 Magnesium1 Manganese1 Mercury1 Nickel1 Potassium1 Selenium1 Silver2 Sodium2 Thallium2 Vanadium2 ZincO ler :

C \nide

TrueValue Found %R

TrueValue100001000

100010001000

1000001000row1000

10000

1000001000

1000IfJOOOO

1000100000

10001000

ZlO.O

1Found103701031

983. 510411038

1023001009100110209975

104000996.9

1018104400

1034104200

10581020

2IO.>

%RTr34103

98104104102101100102100

104100

102104

103104

106102

107-

Found %R(4)

MethodPP

PPPppPPP

PP

PP

PP

PP

CM

1 nitial Calibration Source EPA/ERA 2 Continuing Calibration Source EPA/ER/

3 :ontrol Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115


K T A I L Of OC'» UStO

yC frpurl Mu / .."_ gc frpurt »u«^» V— O r>\ o.... f V.,. _

. t

KV-M-l-J/sf

IC1A2, !iCv-3 ;icu-l } y

^_. •. /~i 1 1 , , ̂ *

{5&k 1

iiii;

i

iiiiiitii

iiitii

v

ii

:

i

* !

!xj

i

I" i

i

ijiii

i

i

j

iiijii

i

iirl

y_

_n

X

/•»

X

3»l«

r-

X

*9 '4 ,̂ /

_

x̂ *

^

) C^-\'•

^

^

VVD S

X

X

V/Vi ,XA,

S-~ 1lk>kl

X

J

•o *^•

A

r^4*%J

J

)C

/

\Jf^

I

;7Ti

•iii

x!{jiii:

J iiiI

;

»

l;i

i

i

i•

i

•

X X

Cn

f

X

2 -«

L. 1 NAME

D. ^E 3/ 2/88

Form III


BLANKS

COMPUCHEM LABORATORIES CASE NO.

Units:

Page 1

13562

ug/L

Initial| Blank Value

Continuing CalibrationT 3 4

rrr~Preparation Blank*| WATER \ SOLID

C ipoundM . a 1 s :1 Aluminum2 Antimony3 Arsenic4 Barium5 Beryllium6 Cadmium7 Calciumfl Chromium9 Cobalt1 Copper1 I ron1 Lead1 Magnesium1 Manganese1 Mercury1 Nickel1 Potassium1 Selenium1 Silver2 Sodium2 Thallium2 Vanadium2 ZincO ler :

C mide

43U53U

1.5U1 .OUl.OU5.0u67U

5.0U5.0U20U

4.0U2.5U180U2.0U.20U39U

2400U1.3U8.0U

1690U2.2U3.0U4 . OU

10U

43U53U

1.5u1 .OUl.OU5.0U67U

5.0U5.0U20u

4 .OU2.5UIflOu2.0u.20U39U

2400u1.3U8 . Ou1690U[2.2]3.0U4 .OU

10U

43U53U

[1.8]1 .OU1 .Ou5.0U67U? .OU5.0U20U

4 . OU2.5u180U2.0u.20u39U

2400u1.3U8 .OU1690U

3.0U4 . OU

10U

43U53U

1 .OU1 .OU5.0u67U

5. OU5.0U20u

4.0U

180u2.0u.20u39U

2400u

8.0U1690U

3.0U4 . OU

10U

43U53U

1 .OU1 .Ou5.0U67U5.0U5.0U20u4.0U

IflOu2.0U

39U2400U

8 .OU1690U

3.0u4 . OU

iou

l

43U53U

1.5Ul.OUl.Ou5.0U67U

5.0U5.0U20U4.0U2.5UIflOu2.0U.20U39U

2400U1 . 3U8.0U1690U2.2U3.0u

[9.0]

VOU.

2

( Reporting Units: aqueous, ug/L; solid, mg/kg

L 1 NAME

D ^E 3/ 2/88

Form III


BLANKS

COMPUCHEM LABORATORIES CASE NO.

Units:

Page 2

13562

ug/L

(1)BlankInitial

Blank ValueContinuing Calibration

^ T 3 4Preparation

|" WATER SOLIDC ipoundM :als :1 Aluminum2 Antimony3 Arsenic4 Barium5 Beryllium6 Cadmium7 Calcium8 Chromium9 Cobalt1 Copper1 I ron1 Lead1 . Magnesium1 Manganese1 Mercury1 Nickel1 Potassium1 Selenium1 Si Ive r2 Sodium2 Thallium2 Vanadium2 ZincO ler :

C mide

43U53U

1 . OU[1.1]5 . OU67U5.0U5.0U20U

4 .OU

180U2.0U

39U2400U

B.OU1690U

3 .OU4.0U

IOU.

1 2

Reporting Units: aqueous, ug/L; solid, mg/kg

Form IV

L l NAME


ICP INTERFERENCE CHECK SAMPLE


3/ 1/88

Check Sample I.D. ICS (0387 )

Check Sample Source EPA

Units: ug/L

C ipoundM als:1 Aluminum2 Antimony3 Arsenic4 Barium5 Beryllium6 Cadmium7 Calcium8 Chromium9 Cobalt1 Copper1 Iron1 Lead1 Magnesium1 Manganese1 Mercury1 Nickel1 Potassium1 Selenium1 Silver2 Sodium2 Thallium2 Vanadium2 zinc0 ler :

ControlMean

. Limi tslStd . Dev . True2

508000

483474909

516000513478534

203000,413̂ 0

[S09000531

916

993

1475973

InitialObserved

49540053u

463.5481 .1955.7489800494.9516.9530.4181100

4808503200523. 5

900.62400U

967.7[ 4209]

531.5904.1

%R

98

9610110595961089989999999

98

97

11293

FinalObserved

49320053U

455.7467.8948.5481600487.8508.2528.6177800

4751501700515.0

881.82400U

963.9[4859]

523.4894 . 3

%R

97

94i 991049395

TO 69988

~9~B999"7

96

97

11092

1 Mean value based on n

2 "rue Value of EPA ICP Interference Check Sample or contractor standard.

Form V

Q. C. Report No. 13562A

SAMPLE SPIKE RECOVERY

L ! NAME COMPUCHEM LABORATORIES CASE NO. 13562

EPA Sample N. MW-16

3/ 2/88

Matrix

Lab Sample ID No. 177708

Units: uq/LWATER

ipoundal s :AluminumAnt imonyArsenicBariumBeryll IumCadmiumCalciumChromiumCobaltCopperI ronLeadMagnesiumManganeseMercury

. NickelPotassiumSeleniumSilverSodiumThall iumVanadiumZinc

ie r :

tnide

Control Limit%R

75-125"

"

11

11

ii

n

n

11

11

"n

11

n

II

ib

fl

II

"n

Spiked SampleResult (SSR)

5723454 .921.1187151 .242 . 3

197.2477.3248.1696450 .5

449.5.680

387 .2

1 . 3U47.4

47.0 -478.07056

SampleResult (SR)

431753U

3.4127.2l.OU5.0U

14.0[6.39

20U612532. 5

245.9.20U39U

6.5U8.0U

2.2U[11.26406

lOu

SpikedAdded (SA)

200050020

20005050*

200500250

100020*

2001

400*

1050*

50500200

100

(1)%R

7091889210̂85NR9294998490NR1026897NR0

95NR9493325

N

N

N

CM1I7T5"5"7F9"rrrrTrrTrr

o

%R - [ (SSR - SR)/SA] x 100"N" - out of control'NR" - Not Required""" - Sample result (SR) exceeds.'omments: *No Spike Required.

spike added (SA) by a factor of 4 or more

Form V

L.


SAMPLE SPIKE RECOVERY

NAME COMPUCHEM LABORATORIES CASE NO. 13562

EPA Sample N. MW-16

3/ 2/88

Matrix WATER


Units: ug/L

C ipoundM ;als:1 Aluminum2 Antimony3 Arsenic4 Barium5 Beryllium6 Cadmium7 Calcium8 Chromium9 Cobalt1 Copper1 Iron1 Lead1 Magnesium1 Manganese1 Mercury1 Nickel1 Potassium1 Se len ium1 Silver2 Sodium2 Thallium2 Vanadium2 ZincO icr :

C tnide

Control Limit%R

75-125 ."

II

"

"

"

11

l!

"

"

n

n

rr

M

11

n

ii

ir11

iin

niiii

Spiked SampleResult (SSR)

-

"

~"~~"

~

~

106.4

SampleResult (SR)

43175lu

[3.41[27.2

1 .OU5.0U

14.0[6.39]

20U612532.5

245.9.20U39U

6. 5U8.0U

2.2u[11.2]6406

10U

SpikedAdded (SA)

200050020

20005050*

200500250

100020*

2001

400*

1050*

50500200

100

(1)%R

106

%R - [ (SSR - SR)/SA] x 100"N" - out of control'NR" - Not Required""" - Sample result (SR) exceeds:omments: *No Spike Required.

spike added (SA) by a factor of 4 or more.

Form VI


DUPLICATES

PAGE |

L l NAME COMPUCHEM LABORATORIES

3/ 2/88

CASE NO. 13562

EPA Sample No. MW-15

Matrix WATER

Lab Sample ID No.

Units: ug/L

177709

ipound:als :AluminumAntimonyArsenicBa r iumBeryll iumCadmiumCalciumChromiumCobaltCopperI ronLeadMagnesiumManganeseMe ccuryNickelPotassiumSeleniumSilve rSodiumThall iumVanadiumZinc

ier :

mide

Control Limi t ( 1 )

+/- 20% RPD

+/- 20% RPD

+/- 20% RPD

+/- CRDL-t-/- 20% RPD

+/- 20% RPD

Sample ( S )

203853U

[5.4]20]

1 .OU5.0U

786107.6'5.~y20U

42204.5]

13260198.1

. 20U39U

[ 44306.5U8 .OU

[ 2620]2.2U[8.6]

750.7

178 .0

Duplicate( D)

162953U

[6.0J21l.ot5.0U

971705.0U[6.720U

4282[4.7 ,

16420240.9. 31039U

71286.5UB.OU

[ 39802.2U .[11

938.2

No Data

RPD(2)

22NCNCNCNCNC21NCNCNC1.5NC2119NCNCNCNCNCNCNCNC22

NC

*

*

*

c_M177T*6"7tf9"1rrrrrrrTr

I7o

(N

Out of controlTo be added at a later dateRPD - (|S - D|/((S + D)/2] x 100

- Non-calculable RPD due to value(s) less than CRDL

Form VI


DUPLICATES

L 1 NAME COMPUCHEM LABORATORIES CASE NO. 13562

PAG El,


D ?E 3/ 2/88

Matrix WATER


Units: ug/L

C ipoundM . a 1 s :1 Aluminum2 Antimony3 Arsenic4 Barium5 Beryllium6 Cadmium7 Calcium8 Chromium9 Cobalt1 Copper1 Iron1 Lead1 Magnesium1 Manganese1 Mercury1 Nickel1 Potassium1 Selenium1 Silver2 Sodium2 Thallium2 Vanadium2 ZincO >er :

C tnide

Control Limit(l) Sample ( S )

431753U

[ 3.4[271 .OU5 . OU

9065014.0[6.4

20U612532.5

24590245.9

.20U39U

2400U6 .5U8 .OU

[ 4280]2.2U[11

6406

10U

Duplicate(D)

NO DataNo DataNo DataNo DataNo DataNo DataNo DataNo DataNo DataNo DataNo DataNo DataNo DataNo DataNo DataNo DataNo DataNo DataNo DataNo DataNo DataNo DataNo Data

10U Mo Pat a**

RPD(2)

NCNCNCNCNCNCNCNCNCNCNCNCNCNCNCNCNCNCNCNCNCNCNC

NC

((N

Out of control1 To be added at a later date1 RPD - [|S - D|/((S + D)/2] x 100- Non-calculable RPD due to valuei s) less than CRDL

Form VII


INSTRUMENT DETECTION LIMITS AND

LABORATORY CONTROL SAMPLE

L 5 NAME;CompuChem Laboratories CASE NO.: 13562

Page 1

DATE 3/ 2/E

1(Required Detection

ipound (Limits (CRDD-ug/1

1| Instrument| Limits| ICP/AAI ID# 3

Detection(IDD-ug/1

FurnaceIDi 2

LCS NO. 17771

1 1| Lab Control Sample |I (uq/L) mg/kg |j (circle one) || True Found %R |

M .als:1 Aluminum2 Antimony3 Arsenic4 Barium5 Beryllium6 Cadmium7 CalciumB Chromium9 Cobalt1 Copper1 I ron1 Lead1 Magnesium1 Manganese1 Mercury1 .Nickel1 Potassium1 Selenium1 Silver2 Sodium2 Thallium2 Vanadium2 Zinc0 le r :

C mide

2006010

20055

5000105025

1005

500015

0.240

50005

105000

105020

10

4353

1.01 .05.0675.05. 020

4 . 0

1802.0

392400

S.O1690

3.04.0

(2) 1.5

(2) 2.5

(1) 0.13

(2) 1.3

(2) 2.2

(4) 10

1000010000100.010000100001000010000010000100001000010000100.010000010000NR10000

100000100.01000

100000100.01000010000

150.0

104501034086.6102001114010420997SO10310103801032010340

., 82. 310070010360NR10300101000

84.5981.010120085.71025010530

146.8

104103 |8̂ 7102111 |104 |10010310410310382101104 |NR103101849810186

102105

98

((A

N - Not Required

Video 12 (Cold Vapor technique)Video 22/755Jarrell-Ash 1100Technicon

Form VIII

L 1 NAME

D ^E 3/ 2/88


STANDARD ADDITION RESULTS

COHPUCHEM LABORATORIES CASE NO.

Units:

13562

ug/L

EPASample 1

M' -16ElemPB

(1)Matrix

LA

0 ADDABS..0320

1CON.10.0

ADDABS.. 0550

2CON.20.0

ADDABS..0690

3CON.30. 0

ADDABS..0940

(3)FINALCON.32.5

r*.995

,

( i Matrix abbreviations: Low Solid, LS; Medium Solid, MS; Low Aqueous, LA;Aqueous, MA.

( > CON is the concentration added, ABS. is the instrument readout inabsorbance concentration.

( ' Concentration as determined by MSA.

" '" is the correlation coefficient." ' Final concentration (3) has been multiplied by dilution factor.

Form IX


ICP SERIAL DILUTIONS

PAGE

L 1 NAME COMPUCHEM LABORATORIES

D ?E 3/ 2/88

CASE NO. 13562



UnitsMatrix WATER

ug/L

C ipound

M a 1 6 :1 Aluminum1 Antimony3 Arsenic4 Barium5 Beryllium6 Cadmium7 Calcium8 Chromium9 Cobalt1 Copper1 Iron1 Lead1 . Magnesium1 Manganese1 Nickel1 Potassium1 Selenium1 Silver1 Sodium2 Thallium2 Vanadium2 Z i nc0 icr :

Initial SampleConcent rat ion( I )

431753 .OU

[27.2]l.OOU5.00U

9065014.0[6.39]20. OU6125

24590245.939. OU2400U

8.00U[ 4283]

[11.2]6406

Serial Dilution(l)ResulUS )

4281

[25.8]

89640

6057

25540244 .5

6514

% Difference* 2)

.83NRNA

5.1NRNR

1.1NRNRNR

1. 1NA

3.9.57NRNRNANRNRNANR

1.7

NN.

i Diluted Sample concentration corrected for 1:5 dilution (See Exhibit D)i Percent Difference - |I - S| x 100

I- Not Required, initial sample concentration less than 10 time IDL- Not Applicable, analyte not determined by ICP

Form X

QC Report No. 13562A

HOLDING TIMES

\B NAME CompuChem Laboratories

\TE 3/ 2/88 CASE NO. 13562

EPASample No.

MW-16MW-15

Matrix

WATERWATER

DateReceived

01/28/8801/28/88

MercuryPrep Date

02/09/BS02/09/88

MercuryHoldingTime( 1 )(days)

1212

CN PrepDate

02/05/8802/05/88

CNHoldingTime(l)(days)

88

.(Holding time is defined as number of days between the date received and trimple preparation date.

For* XI (Quarterly)XMTRVMINT MTICTION LIMITS

UJ KAMI ConpuChem Laboratories. Inc . _ DAlI January 1988,f—\ J*rr«11-Ash'jCFYFi*B€ AA (Clrclt Ow) Kedtl »u»t>tr nnn Iun«ci AA Uu»b«r

Eltatot

1. AIuMlDua

2. ActicscT

3. Artc&lc

*. lirlu='

5. Ber-»i:iu=

f. C»i=J —

7 . C j l c i ' . r

£ . r-r :-u^

9. C c b i l :

1C. Ccr -e r

11. I rc r

12 . L « i ^

Vcv«lta|th(B»)

302.2

206.8

193.6

493.4

313.0

228.8

315.8

2 6 7 . 7

2 2 S . 6

324 .7

259 .9

2 2 0 . 3

CXDL(ui/L)

200

•0

10

2CO

5

3

soc?

J C

3C

2?

I O C

3

XDLt«f/i)

43

53

203

1

1

5

« 15

5

20

4

42

Iltwnt

13. lUnetiu*

14. lUafinctt

13* Kcreurr

16. Nleki!

1?. Pot lMlUC

11. Sclcr.lu:

119. Si lver

2 T . Sc

Farm XI (Quarterly)ZNSTKUMIKT DlTlCTIOtJ LIMITS

LAJ KA>W.I CompuChem Laboratories, Inc .

'ICFYFlame AA (Circle One) Modal •»-*-» Video

January 1988

Eltaent

1. AJualnua

2. Aztl«3CT

3. Aric&lc

4. liriur

5. Ier»::ius

t . Cai^u-

V*v«ltBgth(na)

189.0 B

CXDL(vc/L)

200

40

10

200

3

XDL(ut/L)

1.5

XltMAt

13. lUntilm

14. MjBfifitti

IS. Ktreurr

16. Nlckc!

1?. Fertdlur

I t . Selerlue

Vav«ltB|th(BC)

196.0 B

OCL( u f / l )

30GC

1J

0.2

iO

3 C C D

*

:?.f t / / L

i . :

7. c«:;iu=

«. Ort^.r

9. Cetil:

1C. Ccrrer

11. Ircr

IT. L«»d 283.3 B

*o:c

1C

3C

2?

IOC

3

1

2.5

119. Silver

2:. Sc

Fora XI (Quarterly)DETECTION LIMITS

*r ConpuChen Laboratories, Inc.

(Clrclt One) Model Busbar V1de°

DATI January 1988

Furuce AA Mu*b

Fora III (Quar te r ly ;

1C? Intcrelcoc&t Correction factors

LABORATORY ICF Modtl Hurtcr.J^rrfll-ftsh I I PC

f

Aaalyte

1. Art looey

2. ArttBie

3. larlua

4. Bcr?lliu9

3. Cadelua

6. ChroKlue

7. Cobalt

1. Cepotr

9. Laad

10. K*=r»ce«e

11. M«rcur»

12. Rlckal

13. Vota i t lus

14. Sclcalus

13. Silver

16. Sodlu*

17. Thallluo

11. Tanadlun

19. Zinc

AaalytaVavelanjth

(n=)

lO'r.S

l ^ l i . i r^3,43 i 3 , OZTJB-ft2-(t\-l^^^32.4,1'

2. 2O. 51^-7. (̂

• ^li .C/

7L'tf,4

i^r3Z§0

320, "Z.1%-S7.^.^

7. 1 3 . ft

Intaralaaaat Corracsloc Factorsfor

AI

o.oc3eif

o.ocrxa)

^.con.\

"k Cooo"}

Ca Ft

: "oo\3

LvOcnilc.roaOr nrr.u:

oDnrr,5

^ OOOH

ccom

rt oooiS

ooooc^

Mf

o.0om5

n.cKn4

V- C. 00744-

c.atiS

0003(c)

•Cio^rf

CrD.CIT-^

O.DCIlfC

t.Ofr*)

).POCi6

o ores 2

/Is

O.no^

Cc!

IO.DOZI"?

Lab Manager,1 - 1 9

inttrtleaeat Correctloa Factors

ICP M:i , **. \\ -\\ < \ .DAT! snndfiru /9/?8

7

Analyta

I. I*OK-

j..Ao*Twom3. ~Z-IK.C-

4. fobftlf

3.

6.

7.

1.

f.

10.

11.

12.

13.

14.

13.

16.

17.

IS.

19.

AiulytaWavelength

(ts)

z^.°t3C3.-Z-

2.1"-.. B

2-Zft.^

•

lataralaoaat Correction Factorsfor

AU

0 OOOl1^

•

\;

•o.ortld

AJ;

&.

For* XIII (Qutrterly)ICP Linear Langcs

LAI KA>£

DATE

Lobs XCF Modal Kuaber

7*

Atalyte

1. AluslauB

2. AatlBony

3. Arieaic

4. ItrluB

3. >errlllu«

6. Cidtlus

7. Calciua

8. Chrooiua

9. Cobalt

10. Coooer

11. Iron

12. Lead

Integration71 M

(Seconds )

*\c.f^ntTC

lGOcT'CJi"._

(CXV>'/.

-4Cc^ci O'- r/ ~-- '

Footnotes:

COJttlNTS:

• Indicate eleaents oot analysed by ICP with the no ta t ion *,V.

/I

Lab

1 - 2 1

WiT^nwR/i-)Vtf

BURN # 1ICV ICV-

LV277L-.u

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25.71Su

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13 22:03

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25.6471, 1

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33 22:03

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25.546

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S3 22:05

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25.637I I

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3.005"

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CM C p50 . 322 .436x4

MI 'f.47:1:3 43.034

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50.733 .43322MI H

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K-1 .730

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CALIBRATE-: ASTD CONG0 00.OO1 40.00y 20. oo3 05.004 60. 00

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00. 0039. 5020. 01

O4. t I6O. 09

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SN- OOOOOOC onrMeanP/HConeMpanP/H

MeanSDPSD

SN = 1'8 o n rMeanP /HConeMeanP/H

M panSI.)RSD

SN^ 1C onrMeanP/HC onrMeanP /H

MeansoRSD

SN- 1'.". nn rf 1 panP /H1 ! o n rMeanP /H

MeanSDRSD

SN- 1.' oneM f- a nV f H1 '. o n rM e -i nP/H

MeanSDRSD

1 00. OBOO. 08-0. 001

2 -OO. 16-OO. 040. OOO

p b - y T i-00. 0400. J 7

DIG HIPb-S T]

7/71O1 15. 37

15. 3 70. J 63

2 17.5516. 460. 257

f'b-S 'i 116. 46..01 . K'409. 36

Pb-S Tl7/7101 27.92

27. 920. 37B

2 25.>3326. 870. 239

P b - CJ> "I ]26. 3701. 1 BO5. 49Ph-S 1 !

7 y •'•:>/1 2 5 . 0 5

25. 050.31 3

2 33. r3126. 930. 391Pb-5 Tl26. 9302. 6609. 07

P h - - "' 1v /•,-)-/

1 31. 273 ' . """7

(». 3c-lt?

2 71 3 . «1 132. .7-: 40. 41 1

Pb-S 7)32. 340 1.5104. 6/

Ol . >')70 1 . 07O. OO401. 3701. 22O. OO 3-D01. -'.-''00. f' 11 .'.37

-D

1 6 . "/ : "-i16. 7'i'). 1 /41 7 . 5 ''I17. 140. 24 3

-D17.1 400.. 5R'7)3. 37-D

37. J 237. 12O. 4 ';>'•i.-j. y.'t37. ~" >O. 7113'-D

377. ooOO. 1 ''7-1 0. 4 5b

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1 H, 2"'I B . 2 ''o. '^ ::•.'0. 1 L;.1^.31•3. 23;3-D

1 9 . 2 L01. 2306. '5!

4

Pb-S Tl-DSN= I/7708Cone 1 52. 13 47. 37Mean 53. 13 47. 37P/H 0.578 0.515Conr 2 48.BB 46.30Mean 50.50 47.03P/H 0.421 0.438

Pb-S Tl-DMean 50.50 47.03SD 02. 30 00. 713RSD 04 .55 OO.70

Pb-S " l 1 - - DSN- 177709Cone 1 04.39 00.81Mean 04.39 OO.SIP/H 0.064 0. OO2Cone 2 05.03 O1.49Mean O4. 71, Ol . 1 5P/H 0. 061 O. OO.J

Pb-S Tl-DMean 04. 71 Ol. 15SD 00. 45 00. 48RSD 09.59 41.7^

Pb-S Tl-DSN= 177709Conr 1 16. 16 22. 07Mean 16.16 22.07P/H 0.228 0.2̂ 9Cone 2 14.BB 21.20Mean 1 5. 52 21 . 673P/H O. 2 IB O. 292

Pb-S 71 -DMean 15.52 21.63SD 00.91 00.62RSD 05.83 02.84

Pb-S Tl-DSN= 177713Cone 1 O4, 1 6 01 . c.5Moan 04.16 01.55P/H O. 047 0. O03Cone ;_' O4.32 01.85Mean O4. 49 01 . 70 .P/H O.077 O.OO4

Pb-S Tl-DMean 04.49 Ol.7OSD 00.47 00.21RSD 10.37 12.47

Pb-S Tl-DSN= 17 '71 3' . one 1 1 5. 04 23. 59Mean 1 ' - > . O4 2 J. ':>'>P /H 0. 1 fri/1 0. 2/HCnnr :-_' 14. 52 22. 62 ^

Mean 1 4 . 7 8 23.10 ~V I G '^P/H 0. 14O 0. 219

P h - S T l - DMean 14. 73 23.1CSU 00.37 00.69RSD 02. 48 0.2. 96

Pb-S Tl -DSN= 000004ConeMeanP/HConeMeanP/H

MeanSDRSD

1 36. 5736. 570. 478

2 41.4839. 020. 457

Pb-S Tl39. 0203. 4708. B9

Pb-S 71

37. 3637. 360. 44939. 8938. 620. 384

-D3G. 6201 . 79O/K 62-D

SN= O00099C, o n eMeanP/HC o n rMeanP/H

MeanSDRSD

SN =AbsP /HSN~Ab sP/HSN ^AbsP /HSN-Ab ̂F' / H

SN =C. o n eMeanP/HConeMeanP / H

Tie anSDPSD

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Pb-S177707

O. 032o. 127

00001 0O. 055O. 268

OOO O2 O0. O6O . 3 1 "t

UOOO3Oo. 0̂ 4O. 45O

Pb-S000004

1 34.9034. 900.451

? 38. 8636. f^B0. 501

H b - S36. 3: 3

02. 9007. 59

02. 0502. 050. OO4O2. 3702. 21O. 009-DO2. 21OO. 2310. 22

\O1 ''•̂

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0' 00X00

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Pb-SMean -O0.41SD 00. 30RSD -74.14

CCfe

CompuChem Laboratories Inc.

ELEMENTS

FURNACE AAS RUN LOG

12

3

4

5

6

7

8

9

10

1

2

3

4

5

6

7

8

9

10

Date

Operator:

rile Naae:

Case Name;

POS. NO.

|

SAMPLE NO. | COMMENTS

icv i KV-^ r.||POS. NO. | SAMPLE NO.

M CCB i r c p.

COMMENTS

I ICB

I PREP BLANK

im/o.

.!_-/3?-U5-.i-±i&Mi ccv i |C\M

CCB

CCV

8

9

10

CCV

CCB

M — D

RM, DBFl.:. Rread Se--SLi OU OO1 3O OO:-: os ooII J.:'t:7l OO•4 -4O OO

Ol 2 sMb -7

O OOOO. O37'n nnsO O2 b.O O-4'H

'-it atsec

rts-DOO OO-4Ci OOin noLi'c:- ML1r.-iO OO

#10

ooouo

1

Mb ^OOOi 33OF, T1 ~"'.\L7OiH

Se-S As-DSN= 020887Cone 1 CON HI 24.84Mean CON HI 24.34 ivr^** (cy'~>P/H 0.253 0.399Cone 2 CON HI 24.6GMean CON HI 24.72P/H 0.281 0.492

Se-S As-DMean CON HI 24.72SD 00.RSD 00.

Se-S As-D3N= OO0002Cone 1 22.86 12.06Mean 22.86 12.06P/H 0.133 O.209Cone 2 20.69 12.55Mean 21.77 , 12.3OP/H O.124 O.242

Se-S As-DMean 21. 77 12.JOSD 01.53 OO.35RSD 07.O4 O2.ai

Se-S A s - DSN- OOOOOOC one 1 'JO. OS 00. 95Mt-dn OO. O8 O0.95P/H 0. 001 0.

analytical data reports antrim iron works site … · 2020. 8. 27. · thall ium vanadium zinc f s...

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