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APPENDIX C CHEMICAL TEST CERTIFICATES P/2015/00220 Received 09/02/15

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Page 1: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

APPENDIX C

CHEMICAL TEST

CERTIFICATES

P/2015/00220

Received 09/02/15

Page 2: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

James May QTS Environmental Ltd

Lustre Consulting Ltd Unit 1

Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Kent

ME17 2JNt: 01622 850410

[email protected]

Site Reference: K & N Distribution Depot - Draycott-in-the-Clay

Project / Job Ref: 1309

Order No: None Supplied

Sample Receipt Date: 11/07/2014

Sample Scheduled Date: 14/07/2014

Report Issue Number: 1

Reporting Date: 18/07/2014

Authorised by: Authorised by:

Russell Jarvis Kevin OldDirector Director

On behalf of QTS Environmental Ltd On behalf of QTS Environmental Ltd

Admiral's Offices

The Historic Dockyard

Chatham

Kent

ME4 4TZ

QTS Environmental Report No: 14-22971

QTS Environmental Ltd - Registered in England No 06620874 Page 1 of 21

Page 3: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

09/07/14 09/07/14 09/07/14 09/07/14 09/07/14

None Supplied None Supplied None Supplied None Supplied None Supplied

AWS01 AWS01 AWS02 AWS03 AWS03

Topsoil Clay / Silt Clay / Silt Fill Clay / Silt

0.20 0.50 0.90 0.35 0.70

110722 110723 110725 110727 110728

Determinand Unit RL Accreditation

Asbestos Screen N/a N/a ISO17025 Not Detected Not Detected Not Detected Not Detected Not Detected

pH pH Units N/a MCERTS 9.4 8.0 7.5 7.4

Total Cyanide mg/kg < 2 NONE < 2 < 2 < 2 < 2

W/S Sulphate as SO4 (2:1) g/l < 0.01 MCERTS 0.01 0.04 0.05 0.03

Total Organic Carbon (TOC) % < 0.1 NONE 1.7 0.7 0.8 0.2

Arsenic (As) mg/kg < 2 MCERTS 5 < 2 < 2 6

W/S Boron mg/kg < 1 NONE < 1 < 1 < 1 < 1

Cadmium (Cd) mg/kg < 0.5 MCERTS 1.1 < 0.5 < 0.5 < 0.5

Chromium (Cr) mg/kg < 2 MCERTS 29 35 37 32

Chromium (hexavalent) mg/kg < 2 NONE < 2 < 2 < 2 < 2

Copper (Cu) mg/kg < 4 MCERTS 19 15 22 9

Lead (Pb) mg/kg < 3 MCERTS 23 14 15 8

Mercury (Hg) mg/kg < 1 NONE < 1 < 1 < 1 < 1

Nickel (Ni) mg/kg < 3 MCERTS 30 33 35 33

Selenium (Se) mg/kg < 3 NONE < 3 < 3 < 3 < 3

Zinc (Zn) mg/kg < 3 MCERTS 76 65 89 58

Total Phenols (monohydric) mg/kg < 2 NONE < 2 < 2 < 2 < 2

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

This report refers to samples as received, and QTS Environmental Ltd, takes no responsibility for the accuracy or competence of sampling by others.

The material description shall be regarded as tentative and is not included in our scope of UKAS Accreditation.

Opinions and interpretations expressed herein are outside the scope of UKAS Accreditation.

Asbestos Analyst: Graham Revell

RL: Reporting Limit

Pinch Test: Where pinch test is positive it is reported “Loose Fibres - PT” with type(s).

Subcontracted analysis (S)

QTS Environmental Ltd ' Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis CertificateQTS Environmental Report No: 14-22971 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: K & N Distribution Depot - Draycott-

in-the-Clay

TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

Reporting Date: 18/07/2014 QTSE Sample No

Analysis carried out on the dried sample is corrected for the stone content

The samples have been examined to identify the presence of asbestiform minerals by polarising light microscopy and dispersion staining technique to In-House Procedures QTSE600 Determination of Asbestos in Bulk

Materials; Asbestos in Soils/Sediments (fibre screening and identification)

QTS Environmental Ltd - Registered in England No 06620874 Page 2 of 21

Page 4: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

09/07/14 09/07/14 09/07/14 09/07/14 09/07/14

None Supplied None Supplied None Supplied None Supplied None Supplied

AWS04 AWS04 AWS05 AWS05 AWS06

Fill Clay / Silt MG Clay / Silt Fill

0.32 0.70 0.20 0.75 0.50

110729 110730 110731 110732 110733

Determinand Unit RL Accreditation

Asbestos Screen N/a N/a ISO17025 Not Detected Not Detected Not Detected Not Detected Not Detected

pH pH Units N/a MCERTS 7.6 7.4 7.2

Total Cyanide mg/kg < 2 NONE < 2 < 2 < 2

W/S Sulphate as SO4 (2:1) g/l < 0.01 MCERTS 0.01 0.02 0.02

Total Organic Carbon (TOC) % < 0.1 NONE 0.1 1 0.8

Arsenic (As) mg/kg < 2 MCERTS 4 2 < 2

W/S Boron mg/kg < 1 NONE < 1 < 1 < 1

Cadmium (Cd) mg/kg < 0.5 MCERTS < 0.5 1.6 < 0.5

Chromium (Cr) mg/kg < 2 MCERTS 35 23 31

Chromium (hexavalent) mg/kg < 2 NONE < 2 < 2 < 2

Copper (Cu) mg/kg < 4 MCERTS 7 74 20

Lead (Pb) mg/kg < 3 MCERTS 8 67 11

Mercury (Hg) mg/kg < 1 NONE < 1 < 1 < 1

Nickel (Ni) mg/kg < 3 MCERTS 31 29 30

Selenium (Se) mg/kg < 3 NONE < 3 < 3 < 3

Zinc (Zn) mg/kg < 3 MCERTS 58 132 72

Total Phenols (monohydric) mg/kg < 2 NONE < 2 < 2 < 2

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

This report refers to samples as received, and QTS Environmental Ltd, takes no responsibility for the accuracy or competence of sampling by others.

The material description shall be regarded as tentative and is not included in our scope of UKAS Accreditation.

Opinions and interpretations expressed herein are outside the scope of UKAS Accreditation.

Asbestos Analyst: Graham Revell

RL: Reporting Limit

Pinch Test: Where pinch test is positive it is reported “Loose Fibres - PT” with type(s).

Subcontracted analysis (S)

QTS Environmental Ltd ' Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis CertificateQTS Environmental Report No: 14-22971 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: K & N Distribution Depot - Draycott-

in-the-Clay

TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

Reporting Date: 18/07/2014 QTSE Sample No

Analysis carried out on the dried sample is corrected for the stone content

The samples have been examined to identify the presence of asbestiform minerals by polarising light microscopy and dispersion staining technique to In-House Procedures QTSE600 Determination of Asbestos in Bulk

Materials; Asbestos in Soils/Sediments (fibre screening and identification)

QTS Environmental Ltd - Registered in England No 06620874 Page 3 of 21

Page 5: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

09/07/14 10/07/14 10/07/14 10/07/14 10/07/14

None Supplied None Supplied None Supplied None Supplied None Supplied

AWS06 AWS07 AWS07 AWS08 AWS08

Clay / Silt Fill MG Clay / Silt Clay / Silt

1.50 0.30 0.60 0.20 0.60

110734 110735 110736 110738 110739

Determinand Unit RL Accreditation

Asbestos Screen N/a N/a ISO17025 Not Detected Not Detected Not Detected Not Detected Not Detected

pH pH Units N/a MCERTS 7.1 7.7 7.4

Total Cyanide mg/kg < 2 NONE < 2 < 2 < 2

W/S Sulphate as SO4 (2:1) g/l < 0.01 MCERTS 0.02 0.07 0.03

Total Organic Carbon (TOC) % < 0.1 NONE 0.1 < 0.1 0.6

Arsenic (As) mg/kg < 2 MCERTS 13 22 2

W/S Boron mg/kg < 1 NONE < 1 < 1 < 1

Cadmium (Cd) mg/kg < 0.5 MCERTS < 0.5 0.7 < 0.5

Chromium (Cr) mg/kg < 2 MCERTS 43 20 33

Chromium (hexavalent) mg/kg < 2 NONE < 2 < 2 < 2

Copper (Cu) mg/kg < 4 MCERTS 12 52 11

Lead (Pb) mg/kg < 3 MCERTS 13 44 17

Mercury (Hg) mg/kg < 1 NONE < 1 < 1 < 1

Nickel (Ni) mg/kg < 3 MCERTS 50 36 32

Selenium (Se) mg/kg < 3 NONE < 3 < 3 < 3

Zinc (Zn) mg/kg < 3 MCERTS 74 64 72

Total Phenols (monohydric) mg/kg < 2 NONE < 2 < 2 < 2

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

This report refers to samples as received, and QTS Environmental Ltd, takes no responsibility for the accuracy or competence of sampling by others.

The material description shall be regarded as tentative and is not included in our scope of UKAS Accreditation.

Opinions and interpretations expressed herein are outside the scope of UKAS Accreditation.

Asbestos Analyst: Graham Revell

RL: Reporting Limit

Pinch Test: Where pinch test is positive it is reported “Loose Fibres - PT” with type(s).

Subcontracted analysis (S)

QTS Environmental Ltd ' Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis CertificateQTS Environmental Report No: 14-22971 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: K & N Distribution Depot - Draycott-

in-the-Clay

TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

Reporting Date: 18/07/2014 QTSE Sample No

Analysis carried out on the dried sample is corrected for the stone content

The samples have been examined to identify the presence of asbestiform minerals by polarising light microscopy and dispersion staining technique to In-House Procedures QTSE600 Determination of Asbestos in Bulk

Materials; Asbestos in Soils/Sediments (fibre screening and identification)

QTS Environmental Ltd - Registered in England No 06620874 Page 4 of 21

Page 6: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

10/07/14 10/07/14 10/07/14 10/07/14 10/07/14

None Supplied None Supplied None Supplied None Supplied None Supplied

AWS09 AWS09 AWS10 AWS11 AWS12

Fill MG Topsoil Ash MG

0.20 0.40 0.10 0.50 0.20

110740 110741 110742 110743 110744

Determinand Unit RL Accreditation

Asbestos Screen N/a N/a ISO17025 Not Detected Not Detected Not Detected Not Detected Not Detected

pH pH Units N/a MCERTS 7.3 7.1 7.6 7.5

Total Cyanide mg/kg < 2 NONE < 2 < 2 < 2 < 2

W/S Sulphate as SO4 (2:1) g/l < 0.01 MCERTS 0.03 0.03 0.10 0.35

Total Organic Carbon (TOC) % < 0.1 NONE 0.5 3.7 3 3.4

Arsenic (As) mg/kg < 2 MCERTS 3 4 16 5

W/S Boron mg/kg < 1 NONE < 1 < 1 < 1 < 1

Cadmium (Cd) mg/kg < 0.5 MCERTS < 0.5 < 0.5 < 0.5 < 0.5

Chromium (Cr) mg/kg < 2 MCERTS 29 25 19 22

Chromium (hexavalent) mg/kg < 2 NONE < 2 < 2 < 2 < 2

Copper (Cu) mg/kg < 4 MCERTS 21 18 90 38

Lead (Pb) mg/kg < 3 MCERTS 15 34 20 51

Mercury (Hg) mg/kg < 1 NONE < 1 < 1 < 1 < 1

Nickel (Ni) mg/kg < 3 MCERTS 25 25 60 36

Selenium (Se) mg/kg < 3 NONE < 3 < 3 < 3 < 3

Zinc (Zn) mg/kg < 3 MCERTS 88 87 186 87

Total Phenols (monohydric) mg/kg < 2 NONE < 2 < 2 < 2 < 2

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

This report refers to samples as received, and QTS Environmental Ltd, takes no responsibility for the accuracy or competence of sampling by others.

The material description shall be regarded as tentative and is not included in our scope of UKAS Accreditation.

Opinions and interpretations expressed herein are outside the scope of UKAS Accreditation.

Asbestos Analyst: Graham Revell

RL: Reporting Limit

Pinch Test: Where pinch test is positive it is reported “Loose Fibres - PT” with type(s).

Subcontracted analysis (S)

QTS Environmental Ltd ' Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis CertificateQTS Environmental Report No: 14-22971 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: K & N Distribution Depot - Draycott-

in-the-Clay

TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

Reporting Date: 18/07/2014 QTSE Sample No

Analysis carried out on the dried sample is corrected for the stone content

The samples have been examined to identify the presence of asbestiform minerals by polarising light microscopy and dispersion staining technique to In-House Procedures QTSE600 Determination of Asbestos in Bulk

Materials; Asbestos in Soils/Sediments (fibre screening and identification)

QTS Environmental Ltd - Registered in England No 06620874 Page 5 of 21

Page 7: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

10/07/14

None Supplied

AWS12

Clay / Silt

0.50

110745

Determinand Unit RL Accreditation

Asbestos Screen N/a N/a ISO17025 Not Detected

pH pH Units N/a MCERTS 7.6

Total Cyanide mg/kg < 2 NONE < 2

W/S Sulphate as SO4 (2:1) g/l < 0.01 MCERTS 0.08

Total Organic Carbon (TOC) % < 0.1 NONE 0.1

Arsenic (As) mg/kg < 2 MCERTS 6

W/S Boron mg/kg < 1 NONE < 1

Cadmium (Cd) mg/kg < 0.5 MCERTS < 0.5

Chromium (Cr) mg/kg < 2 MCERTS 39

Chromium (hexavalent) mg/kg < 2 NONE < 2

Copper (Cu) mg/kg < 4 MCERTS 12

Lead (Pb) mg/kg < 3 MCERTS 12

Mercury (Hg) mg/kg < 1 NONE < 1

Nickel (Ni) mg/kg < 3 MCERTS 41

Selenium (Se) mg/kg < 3 NONE < 3

Zinc (Zn) mg/kg < 3 MCERTS 72

Total Phenols (monohydric) mg/kg < 2 NONE < 2

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

This report refers to samples as received, and QTS Environmental Ltd, takes no responsibility for the accuracy or competence of sampling by others.

The material description shall be regarded as tentative and is not included in our scope of UKAS Accreditation.

Opinions and interpretations expressed herein are outside the scope of UKAS Accreditation.

Asbestos Analyst: Graham Revell

RL: Reporting Limit

Pinch Test: Where pinch test is positive it is reported “Loose Fibres - PT” with type(s).

Subcontracted analysis (S)

QTS Environmental Ltd ' Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Depth (m)

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis CertificateQTS Environmental Report No: 14-22971 Date Sampled

Lustre Consulting Ltd Time Sampled

Reporting Date: 18/07/2014 QTSE Sample No

Analysis carried out on the dried sample is corrected for the stone content

The samples have been examined to identify the presence of asbestiform minerals by polarising light microscopy and dispersion staining technique to In-House Procedures QTSE600 Determination of Asbestos in Bulk

Materials; Asbestos in Soils/Sediments (fibre screening and identification)

Site Reference: K & N Distribution Depot - Draycott-

in-the-Clay

TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: None Supplied

QTS Environmental Ltd - Registered in England No 06620874 Page 6 of 21

Page 8: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

09/07/14 09/07/14 09/07/14 09/07/14 09/07/14

None Supplied None Supplied None Supplied None Supplied None Supplied

AWS01 AWS01 AWS02 AWS03 AWS04

Topsoil Clay / Silt Clay / Silt Clay / Silt Clay / Silt

0.20 0.50 0.90 0.70 0.70

110722 110723 110725 110728 110730

Determinand Unit RL Accreditation

Naphthalene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Acenaphthylene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Acenaphthene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Fluorene mg/kg < 0.1 MCERTS < 0.1 0.20 < 0.1 < 0.1 < 0.1

Phenanthrene mg/kg < 0.1 MCERTS < 0.1 0.55 < 0.1 < 0.1 < 0.1

Anthracene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Fluoranthene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Pyrene mg/kg < 0.1 MCERTS < 0.1 0.39 < 0.1 < 0.1 < 0.1

Benzo(a)anthracene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Chrysene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Benzo(b)fluoranthene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Benzo(k)fluoranthene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Benzo(a)pyrene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Indeno(1,2,3-cd)pyrene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Dibenz(a,h)anthracene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Benzo(ghi)perylene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Total EPA-16 PAHs mg/kg < 1.6 MCERTS < 1.6 < 1.6 < 1.6 < 1.6 < 1.6

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate - Speciated PAHsQTS Environmental Report No: 14-22971 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: K & N Distribution Depot -

Draycott-in-the-Clay

TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

Reporting Date: 18/07/2014 QTSE Sample No

QTS Environmental Ltd - Registered in England No 06620874 Page 7 of 21

Page 9: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

09/07/14 09/07/14 09/07/14 10/07/14 10/07/14

None Supplied None Supplied None Supplied None Supplied None Supplied

AWS05 AWS05 AWS06 AWS07 AWS08

MG Clay / Silt Clay / Silt MG Clay / Silt

0.20 0.75 1.50 0.60 0.20

110731 110732 110734 110736 110738

Determinand Unit RL Accreditation

Naphthalene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Acenaphthylene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Acenaphthene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Fluorene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Phenanthrene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Anthracene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Fluoranthene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Pyrene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Benzo(a)anthracene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Chrysene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Benzo(b)fluoranthene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Benzo(k)fluoranthene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Benzo(a)pyrene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Indeno(1,2,3-cd)pyrene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Dibenz(a,h)anthracene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Benzo(ghi)perylene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Total EPA-16 PAHs mg/kg < 1.6 MCERTS < 1.6 < 1.6 < 1.6 < 1.6 < 1.6

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

Reporting Date: 18/07/2014 QTSE Sample No

Soil Analysis Certificate - Speciated PAHsQTS Environmental Report No: 14-22971 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: K & N Distribution Depot -

Draycott-in-the-Clay

TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

QTS Environmental Ltd - Registered in England No 06620874 Page 8 of 21

Page 10: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

10/07/14 10/07/14 10/07/14 10/07/14 10/07/14

None Supplied None Supplied None Supplied None Supplied None Supplied

AWS09 AWS10 AWS11 AWS12 AWS12

MG Topsoil Ash MG Clay / Silt

0.40 0.10 0.50 0.20 0.50

110741 110742 110743 110744 110745

Determinand Unit RL Accreditation

Naphthalene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Acenaphthylene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Acenaphthene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Fluorene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Phenanthrene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 0.30 < 0.1

Anthracene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Fluoranthene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 0.72 < 0.1

Pyrene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 0.67 < 0.1

Benzo(a)anthracene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 0.33 < 0.1

Chrysene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 0.36 < 0.1

Benzo(b)fluoranthene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 0.45 < 0.1

Benzo(k)fluoranthene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 0.14 < 0.1

Benzo(a)pyrene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 0.32 < 0.1

Indeno(1,2,3-cd)pyrene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 0.19 < 0.1

Dibenz(a,h)anthracene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Benzo(ghi)perylene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 0.18 < 0.1

Total EPA-16 PAHs mg/kg < 1.6 MCERTS < 1.6 < 1.6 < 1.6 3.6 < 1.6

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

Soil Analysis Certificate - Speciated PAHsQTS Environmental Report No: 14-22971

Project / Job Ref: 1309 Additional Refs

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

Order No: None Supplied Depth (m)

Reporting Date: 18/07/2014 QTSE Sample No

Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: K & N Distribution Depot -

Draycott-in-the-Clay

TP / BH No

QTS Environmental Ltd - Registered in England No 06620874 Page 9 of 21

Page 11: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

09/07/14 09/07/14 09/07/14 09/07/14 09/07/14

None Supplied None Supplied None Supplied None Supplied None Supplied

AWS01 AWS01 AWS01 AWS02 AWS02

Topsoil Clay / Silt Clay / Silt Clay / Silt Clay / Silt

0.20 0.50 1.50 0.90 2.30

110722 110723 110724 110725 110726

Determinand Unit RL Accreditation

Aliphatic >C5 - C6 mg/kg < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Aliphatic >C6 - C8 mg/kg < 0.05 NONE < 0.05 < 0.05 < 0.05 < 0.05 < 0.05

Aliphatic >C8 - C10 mg/kg < 1 NONE < 1 3 < 1 < 1 < 1

Aliphatic >C10 - C12 mg/kg < 1 NONE < 1 31 < 1 < 1 < 1

Aliphatic >C12 - C16 mg/kg < 1 NONE < 1 201 < 1 < 1 < 1

Aliphatic >C16 - C21 mg/kg < 1 NONE < 1 246 < 1 < 1 < 1

Aliphatic >C21 - C34 mg/kg < 6 NONE < 6 47 < 6 < 6 < 6

Aliphatic (C5 - C34) mg/kg < 12 NONE < 12 527 < 12 < 12 < 12

Aromatic >C5 - C7 mg/kg < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Aromatic >C7 - C8 mg/kg < 0.05 NONE < 0.05 < 0.05 < 0.05 < 0.05 < 0.05

Aromatic >C8 - C10 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aromatic >C10 - C12 mg/kg < 1 NONE < 1 11 < 1 < 1 < 1

Aromatic >C12 - C16 mg/kg < 1 NONE < 1 105 < 1 < 1 < 1

Aromatic >C16 - C21 mg/kg < 1 NONE < 1 188 < 1 < 1 < 1

Aromatic >C21 - C35 mg/kg < 6 NONE < 6 34 < 6 < 6 < 6

Aromatic (C5 - C35) mg/kg < 12 NONE < 12 338 < 12 < 12 < 12

Total >C5 - C35 mg/kg < 24 NONE < 24 865 < 24 < 24 < 24

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate - TPH CWG BandedQTS Environmental Report No: 14-22971 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: K & N Distribution Depot -

Draycott-in-the-Clay

TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

Reporting Date: 18/07/2014 QTSE Sample No

QTS Environmental Ltd - Registered in England No 06620874 Page 10 of 21

Page 12: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

09/07/14 09/07/14 09/07/14 09/07/14 09/07/14

None Supplied None Supplied None Supplied None Supplied None Supplied

AWS03 AWS04 AWS05 AWS05 AWS06

Clay / Silt Clay / Silt MG Clay / Silt Clay / Silt

0.70 0.70 0.20 0.75 1.50

110728 110730 110731 110732 110734

Determinand Unit RL Accreditation

Aliphatic >C5 - C6 mg/kg < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Aliphatic >C6 - C8 mg/kg < 0.05 NONE < 0.05 < 0.05 < 0.05 < 0.05 < 0.05

Aliphatic >C8 - C10 mg/kg < 1 NONE < 1 < 1 < 1 < 1 51

Aliphatic >C10 - C12 mg/kg < 1 NONE < 1 < 1 < 1 < 1 127

Aliphatic >C12 - C16 mg/kg < 1 NONE < 1 < 1 < 1 < 1 87

Aliphatic >C16 - C21 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aliphatic >C21 - C34 mg/kg < 6 NONE < 6 < 6 < 6 < 6 < 6

Aliphatic (C5 - C34) mg/kg < 12 NONE < 12 < 12 < 12 < 12 266

Aromatic >C5 - C7 mg/kg < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Aromatic >C7 - C8 mg/kg < 0.05 NONE < 0.05 < 0.05 < 0.05 < 0.05 < 0.05

Aromatic >C8 - C10 mg/kg < 1 NONE < 1 < 1 < 1 < 1 10

Aromatic >C10 - C12 mg/kg < 1 NONE < 1 < 1 < 1 < 1 49

Aromatic >C12 - C16 mg/kg < 1 NONE < 1 < 1 < 1 < 1 46

Aromatic >C16 - C21 mg/kg < 1 NONE < 1 < 1 < 1 < 1 3

Aromatic >C21 - C35 mg/kg < 6 NONE < 6 < 6 < 6 < 6 < 6

Aromatic (C5 - C35) mg/kg < 12 NONE < 12 < 12 < 12 < 12 107

Total >C5 - C35 mg/kg < 24 NONE < 24 < 24 < 24 < 24 373

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate - TPH CWG BandedQTS Environmental Report No: 14-22971 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: K & N Distribution Depot -

Draycott-in-the-Clay

TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

Reporting Date: 18/07/2014 QTSE Sample No

QTS Environmental Ltd - Registered in England No 06620874 Page 11 of 21

Page 13: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

10/07/14 10/07/14 10/07/14 10/07/14 10/07/14

None Supplied None Supplied None Supplied None Supplied None Supplied

AWS07 AWS07 AWS08 AWS09 AWS10

MG Clay / Silt Clay / Silt MG Topsoil

0.60 1.40 0.20 0.40 0.10

110736 110737 110738 110741 110742

Determinand Unit RL Accreditation

Aliphatic >C5 - C6 mg/kg < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Aliphatic >C6 - C8 mg/kg < 0.05 NONE < 0.05 < 0.05 < 0.05 < 0.05 < 0.05

Aliphatic >C8 - C10 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aliphatic >C10 - C12 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aliphatic >C12 - C16 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aliphatic >C16 - C21 mg/kg < 1 NONE < 1 < 1 < 1 2 < 1

Aliphatic >C21 - C34 mg/kg < 6 NONE < 6 < 6 < 6 < 6 < 6

Aliphatic (C5 - C34) mg/kg < 12 NONE < 12 < 12 < 12 < 12 < 12

Aromatic >C5 - C7 mg/kg < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Aromatic >C7 - C8 mg/kg < 0.05 NONE < 0.05 < 0.05 < 0.05 < 0.05 < 0.05

Aromatic >C8 - C10 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aromatic >C10 - C12 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aromatic >C12 - C16 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aromatic >C16 - C21 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aromatic >C21 - C35 mg/kg < 6 NONE < 6 < 6 < 6 < 6 < 6

Aromatic (C5 - C35) mg/kg < 12 NONE < 12 < 12 < 12 < 12 < 12

Total >C5 - C35 mg/kg < 24 NONE < 24 < 24 < 24 < 24 < 24

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate - TPH CWG BandedQTS Environmental Report No: 14-22971 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: K & N Distribution Depot -

Draycott-in-the-Clay

TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

Reporting Date: 18/07/2014 QTSE Sample No

QTS Environmental Ltd - Registered in England No 06620874 Page 12 of 21

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10/07/14 10/07/14 10/07/14

None Supplied None Supplied None Supplied

AWS11 AWS12 AWS12

Ash MG Clay / Silt

0.50 0.20 0.50

110743 110744 110745

Determinand Unit RL Accreditation

Aliphatic >C5 - C6 mg/kg < 0.01 NONE < 0.01 < 0.01 < 0.01

Aliphatic >C6 - C8 mg/kg < 0.05 NONE < 0.05 < 0.05 < 0.05

Aliphatic >C8 - C10 mg/kg < 1 NONE < 1 < 1 < 1

Aliphatic >C10 - C12 mg/kg < 1 NONE < 1 < 1 < 1

Aliphatic >C12 - C16 mg/kg < 1 NONE < 1 < 1 < 1

Aliphatic >C16 - C21 mg/kg < 1 NONE < 1 < 1 < 1

Aliphatic >C21 - C34 mg/kg < 6 NONE < 6 8 < 6

Aliphatic (C5 - C34) mg/kg < 12 NONE < 12 < 12 < 12

Aromatic >C5 - C7 mg/kg < 0.01 NONE < 0.01 < 0.01 < 0.01

Aromatic >C7 - C8 mg/kg < 0.05 NONE < 0.05 < 0.05 < 0.05

Aromatic >C8 - C10 mg/kg < 1 NONE < 1 < 1 < 1

Aromatic >C10 - C12 mg/kg < 1 NONE < 1 < 1 < 1

Aromatic >C12 - C16 mg/kg < 1 NONE < 1 < 1 < 1

Aromatic >C16 - C21 mg/kg < 1 NONE < 1 9 < 1

Aromatic >C21 - C35 mg/kg < 6 NONE < 6 15 < 6

Aromatic (C5 - C35) mg/kg < 12 NONE < 12 24 < 12

Total >C5 - C35 mg/kg < 24 NONE < 24 32 < 24

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate - TPH CWG BandedQTS Environmental Report No: 14-22971 Date Sampled

Lustre Consulting Ltd Time Sampled

Reporting Date: 18/07/2014 QTSE Sample No

Site Reference: K & N Distribution Depot -

Draycott-in-the-Clay

TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

QTS Environmental Ltd - Registered in England No 06620874 Page 13 of 21

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09/07/14 09/07/14 09/07/14 09/07/14 09/07/14

None Supplied None Supplied None Supplied None Supplied None Supplied

AWS01 AWS01 AWS01 AWS02 AWS02

Topsoil Clay / Silt Clay / Silt Clay / Silt Clay / Silt

0.20 0.50 1.50 0.90 2.30

110722 110723 110724 110725 110726

Determinand Unit RL Accreditation

Benzene ug/kg < 2 MCERTS < 2 < 2 < 2 < 2 < 2

Toluene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Ethylbenzene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

p & m-xylene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

o-xylene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

MTBE ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate - BTEX / MTBEQTS Environmental Report No: 14-22971 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: K & N Distribution Depot -

Draycott-in-the-Clay

TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

Reporting Date: 18/07/2014 QTSE Sample No

QTS Environmental Ltd - Registered in England No 06620874 Page 14 of 21

Page 16: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

09/07/14 09/07/14 09/07/14 09/07/14 09/07/14

None Supplied None Supplied None Supplied None Supplied None Supplied

AWS03 AWS04 AWS05 AWS05 AWS06

Clay / Silt Clay / Silt MG Clay / Silt Clay / Silt

0.70 0.70 0.20 0.75 1.50

110728 110730 110731 110732 110734

Determinand Unit RL Accreditation

Benzene ug/kg < 2 MCERTS < 2 < 2 < 2 < 2 < 2

Toluene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Ethylbenzene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 191

p & m-xylene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 53

o-xylene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 16

MTBE ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate - BTEX / MTBEQTS Environmental Report No: 14-22971 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: K & N Distribution Depot -

Draycott-in-the-Clay

TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

Reporting Date: 18/07/2014 QTSE Sample No

QTS Environmental Ltd - Registered in England No 06620874 Page 15 of 21

Page 17: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

10/07/14 10/07/14 10/07/14 10/07/14 10/07/14

None Supplied None Supplied None Supplied None Supplied None Supplied

AWS07 AWS07 AWS08 AWS09 AWS10

MG Clay / Silt Clay / Silt MG Topsoil

0.60 1.40 0.20 0.40 0.10

110736 110737 110738 110741 110742

Determinand Unit RL Accreditation

Benzene ug/kg < 2 MCERTS < 2 < 2 < 2 < 2 < 2

Toluene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Ethylbenzene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

p & m-xylene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

o-xylene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

MTBE ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate - BTEX / MTBEQTS Environmental Report No: 14-22971 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: K & N Distribution Depot -

Draycott-in-the-Clay

TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

Reporting Date: 18/07/2014 QTSE Sample No

QTS Environmental Ltd - Registered in England No 06620874 Page 16 of 21

Page 18: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

10/07/14 10/07/14 10/07/14

None Supplied None Supplied None Supplied

AWS11 AWS12 AWS12

Ash MG Clay / Silt

0.50 0.20 0.50

110743 110744 110745

Determinand Unit RL Accreditation

Benzene ug/kg < 2 MCERTS < 2 < 2 < 2

Toluene ug/kg < 5 MCERTS < 5 < 5 < 5

Ethylbenzene ug/kg < 10 MCERTS < 10 < 10 < 10

p & m-xylene ug/kg < 10 MCERTS < 10 < 10 < 10

o-xylene ug/kg < 10 MCERTS < 10 < 10 < 10

MTBE ug/kg < 5 MCERTS < 5 < 5 < 5

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate - BTEX / MTBEQTS Environmental Report No: 14-22971 Date Sampled

Lustre Consulting Ltd Time Sampled

Reporting Date: 18/07/2014 QTSE Sample No

Site Reference: K & N Distribution Depot -

Draycott-in-the-Clay

TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

QTS Environmental Ltd - Registered in England No 06620874 Page 17 of 21

Page 19: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

09/07/14 09/07/14 10/07/14 10/07/14

None Supplied None Supplied None Supplied None Supplied

AWS05 AWS06 AWS07 AWS09

Clay / Silt Clay / Silt MG MG

0.75 1.50 0.60 0.40

110732 110734 110736 110741

Determinand Unit RL Accreditation

Dichlorodifluoromethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

Vinyl Chloride ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

Chloromethane ug/kg < 10 MCERTS < 10 < 10 < 10 < 10

Chloroethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

Bromomethane ug/kg < 10 MCERTS < 10 < 10 < 10 < 10

Trichlorofluoromethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

1,1-Dichloroethene ug/kg < 5 ISO17025 < 5 < 5 < 5 < 5

MTBE ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

trans-1,2-Dichloroethene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

1,1-Dichloroethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

cis-1,2-Dichloroethene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

2,2-Dichloropropane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

Chloroform ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

Bromochloromethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

1,1,1-Trichloroethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

1,1-Dichloropropene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10

Carbon Tetrachloride ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

1,2-Dichloroethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

Benzene ug/kg < 2 MCERTS < 2 < 2 < 2 < 2

1,2-Dichloropropane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

Trichloroethene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

Bromodichloromethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

Dibromomethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

TAME ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

cis-1,3-Dichloropropene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

Toluene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

trans-1,3-Dichloropropene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

1,1,2-Trichloroethane ug/kg < 10 MCERTS < 10 < 10 < 10 < 10

1,3-Dichloropropane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

Tetrachloroethene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

Dibromochloromethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

1,2-Dibromoethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

Chlorobenzene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

1,1,1,2-Tetrachloroethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

Ethyl Benzene ug/kg < 10 MCERTS < 10 191 < 10 < 10

m,p-Xylene ug/kg < 10 MCERTS < 10 53 < 10 < 10

o-Xylene ug/kg < 10 MCERTS < 10 16 < 10 < 10

Styrene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

Bromoform ug/kg < 10 MCERTS < 10 < 10 < 10 < 10

Isopropylbenzene ug/kg < 5 MCERTS < 5 293 < 5 < 5

1,1,2,2-Tetrachloroethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

1,2,3-Trichloropropane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

n-Propylbenzene ug/kg < 5 MCERTS < 5 551 < 5 < 5

Bromobenzene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

2-Chlorotoluene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

1,3,5-Trimethylbenzene ug/kg < 5 MCERTS < 5 1180 < 5 < 5

4-Chlorotoluene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

tert-Butylbenzene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

1,2,4-Trimethylbenzene ug/kg < 5 MCERTS < 5 1670 < 5 < 5

sec-Butylbenzene ug/kg < 5 MCERTS < 5 559 < 5 < 5

p-Isopropyltoluene ug/kg < 5 MCERTS < 5 1439 < 5 < 5

1,3-Dichlorobenzene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

1,4-Dichlorobenzene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

n-Butylbenzene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

1,2-Dichlorobenzene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

1,2-Dibromo-3-chloropropane ug/kg < 10 MCERTS < 10 < 10 < 10 < 10

Hexachlorobutadiene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate - Volatile Organic Compounds (VOC)QTS Environmental Report No: 14-22971 Date Sampled

Lustre Consulting Ltd Time Sampled

Reporting Date: 18/07/2014 QTSE Sample No

Site Reference: K & N Distribution Depot -

Draycott-in-the-Clay

TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

QTS Environmental Ltd - Registered in England No 06620874 Page 18 of 21

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09/07/14 09/07/14 10/07/14 10/07/14

None Supplied None Supplied None Supplied None Supplied

AWS05 AWS06 AWS07 AWS09

Clay / Silt Clay / Silt MG MG

0.75 1.50 0.60 0.40

110732 110734 110736 110741

Determinand Unit RL Accreditation

Phenol mg/kg < 0.1 NONE < 0.1 < 0.1 < 0.1 < 0.1

1,2,4-Trichlorobenzene mg/kg < 0.1 ISO17025 < 0.1 < 0.1 < 0.1 < 0.1

2-Nitrophenol mg/kg < 0.1 NONE < 0.1 < 0.1 < 0.1 < 0.1

Nitrobenzene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1

0-Cresol mg/kg < 0.1 NONE < 0.1 < 0.1 < 0.1 < 0.1

bis(2-chloroethoxy)methane mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1

bis(2-chloroethyl)ether mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1

2,4-Dichlorophenol mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1

2-Chlorophenol mg/kg < 0.1 ISO17025 < 0.1 < 0.1 < 0.1 < 0.1

1,3-Dichlorobenzene mg/kg < 0.1 ISO17025 < 0.1 < 0.1 < 0.1 < 0.1

1,4-Dichlorobenzene mg/kg < 0.1 ISO17025 < 0.1 < 0.1 < 0.1 < 0.1

1,2-Dichlorobenzene mg/kg < 0.1 ISO17025 < 0.1 < 0.1 < 0.1 < 0.1

2,4-Dimethylphenol mg/kg < 0.15 ISO17025 < 0.15 < 0.15 < 0.15 < 0.15

Isophorone mg/kg < 0.1 NONE < 0.1 < 0.1 < 0.1 < 0.1

Hexachloroethane mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1

p-Cresol mg/kg < 0.15 MCERTS < 0.15 < 0.15 < 0.15 < 0.15

2,4,6-Trichlorophenol mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1

2,4,5-Trichlorophenol mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1

2-Nitroaniline mg/kg < 0.1 NONE < 0.1 < 0.1 < 0.1 < 0.1

4-Chloro-3-methylphenol mg/kg < 0.1 NONE < 0.1 < 0.1 < 0.1 < 0.1

2-Methylnaphthalene mg/kg < 0.1 MCERTS < 0.1 0.4 < 0.1 < 0.1

Hexachlorocyclopentadiene mg/kg < 0.1 NONE < 0.1 < 0.1 < 0.1 < 0.1

Hexachlorobutadiene mg/kg < 0.1 ISO17025 < 0.1 < 0.1 < 0.1 < 0.1

2,6-Dinitrotoluene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1

Dimethyl phthalate mg/kg < 0.1 NONE < 0.1 < 0.1 < 0.1 < 0.1

2-Chloronaphthalene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1

4-Chloroanaline mg/kg < 0.2 NONE < 0.2 < 0.2 < 0.2 < 0.2

4-Nitrophenol mg/kg < 0.1 NONE < 0.1 < 0.1 < 0.1 < 0.1

4-Chlorophenyl phenyl ether mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1

3-Nitroaniline mg/kg < 0.1 NONE < 0.1 0.1 < 0.1 < 0.1

4-Nitroaniline mg/kg < 0.1 NONE < 0.1 < 0.1 < 0.1 < 0.1

4-Bromophenyl phenyl ether mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1

Hexachlorobenzene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1

2,4-Dinitrotoluene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1

Diethyl phthalate mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1

Dibenzofuran mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1

Azobenzene mg/kg < 0.1 NONE < 0.1 < 0.1 < 0.1 < 0.1

Dibutyl phthalate mg/kg < 0.15 ISO17025 < 0.15 < 0.15 < 0.15 < 0.15

Carbazole mg/kg < 0.1 ISO17025 < 0.1 < 0.1 < 0.1 < 0.1

bis(2-ethylhexyl)phthalate mg/kg < 0.2 MCERTS < 0.2 < 0.2 < 0.2 < 0.2

Benzyl butyl phthalate mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1

Di-n-octyl phthalate mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate - Semi Volatile Organic Compounds (SVOC)QTS Environmental Report No: 14-22971 Date Sampled

Lustre Consulting Ltd Time Sampled

Reporting Date: 18/07/2014 QTSE Sample No

Site Reference: K & N Distribution Depot -

Draycott-in-the-Clay

TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

QTS Environmental Ltd - Registered in England No 06620874 Page 19 of 21

Page 21: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

QTSE Sample No TP / BH No Additional Refs Depth (m)Moisture

Content (%) 110722 AWS01 Topsoil 0.20 11.8

110723 AWS01 Clay / Silt 0.50 16.9

110724 AWS01 Clay / Silt 1.50 18.1

110725 AWS02 Clay / Silt 0.90 17

110726 AWS02 Clay / Silt 2.30 15.2

110728 AWS03 Clay / Silt 0.70 8.3

110730 AWS04 Clay / Silt 0.70 14.2

110731 AWS05 MG 0.20 10

110732 AWS05 Clay / Silt 0.75 15.4

110734 AWS06 Clay / Silt 1.50 17.9

110736 AWS07 MG 0.60 11

110737 AWS07 Clay / Silt 1.40 19.2

110738 AWS08 Clay / Silt 0.20 16.5

110741 AWS09 MG 0.40 16.1

110742 AWS10 Topsoil 0.10 24

110743 AWS11 Ash 0.50 24.6

110744 AWS12 MG 0.20 9.4

110745 AWS12 Clay / Silt 0.50 13.5

Moisture content is part of procedure E003 & is not an accredited testInsufficient Sample

I/S

Unsuitable Sample U/S

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate - Sample DescriptionsQTS Environmental Report No: 14-22971

Lustre Consulting Ltd

Site Reference: K & N Distribution Depot - Draycott-in-the-Clay

Project / Job Ref: 1309

Order No: None Supplied

Reporting Date: 18/07/2014

Sample Matrix Description

Light brown clayey gravel with vegetation and rubble

Light brown clay

Light brown clayLight brown clay

Light brown clay

Light brown clay

Light brown clay

Light brown clayey gravel with rubble and vegetation

Light brown clay

Brown gravelly clay with rubble and vegetation

Brown clayey gravel with concrete and vegetation

Light brown clay

Light brown clay

Light brown gravelly clay with rubble and stones

Light brown clayey gravel

Light brown clayey gravel with vegetation

Light brown clay with stones and vegetation

Light brown clayey sand with vegetation

QTS Environmental Ltd - Registered in England No 06620874 Page 20 of 21

Page 22: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Matrix Analysed

On

Determinand Brief Method Description Method

NoSoil D Boron - Water Soluble Determination of water soluble boron in soil by 2:1 hot water extract followed by ICP-OES E012

Soil AR BTEX Determination of BTEX by headspace GC-MS E001

Soil D Cations Determination of cations in soil by aqua-regia digestion followed by ICP-OES E002

Soil D Chloride - Water Soluble (2:1) Determination of chloride by extraction with water & analysed by ion chromatography E009

Soil AR Chromium - HexavalentDetermination of hexavalent chromium in soil by extraction in water then by acidification, addition of

1,5 diphenylcarbazide followed by colorimetryE016

Soil AR Cyanide - Complex Determination of complex cyanide by distillation followed by colorimetry E015

Soil AR Cyanide - Free Determination of free cyanide by distillation followed by colorimetry E015

Soil AR Cyanide - Total Determination of total cyanide by distillation followed by colorimetry E015

Soil D Cyclohexane Extractable Matter (CEM) Gravimetrically determined through extraction with cyclohexane E011

Soil AR Diesel Range Organics (C10 - C24) Determination of hexane/acetone extractable hydrocarbons by GC-FID E004

Soil AR Electrical ConductivityDetermination of electrical conductivity by addition of saturated calcium sulphate followed by

electrometric measurementE022

Soil AR Electrical Conductivity Determination of electrical conductivity by addition of water followed by electrometric measurement E023

Soil D Elemental Sulphur Determination of elemental sulphur by solvent extraction followed by GC-MS E020

Soil AR EPH (C10 – C40) Determination of acetone/hexane extractable hydrocarbons by GC-FID E004

Soil AR EPH Product ID Determination of acetone/hexane extractable hydrocarbons by GC-FID E004

Soil AR EPH TEXAS Determination of acetone/hexane extractable hydrocarbons by GC-FID E004

Soil D Fluoride - Water Soluble Determination of Fluoride by extraction with water & analysed by ion chromatography E009

Soil D FOC (Fraction Organic Carbon)Determination of fraction of organic carbon by oxidising with potassium dichromate followed by

titration with iron (II) sulphateE010

Soil D Loss on Ignition @ 450oCDetermination of loss on ignition in soil by gravimetrically with the sample being ignited in a muffle

furnaceE019

Soil D Magnesium - Water Soluble Determination of water soluble magnesium by extraction with water followed by ICP-OES E025

Soil D Metals Determination of metals by aqua-regia digestion followed by ICP-OES E002

Soil AR Mineral Oil (C10 - C40) Determination of hexane/acetone extractable hydrocarbons by GC-FID fractionating with SPE cartridge E004

Soil AR Moisture Content Moisture content; determined gravimetrically E003

Soil D Nitrate - Water Soluble (2:1) Determination of nitrate by extraction with water & analysed by ion chromatography E009

Soil D Organic MatterDetermination of organic matter by oxidising with potassium dichromate followed by titration with iron

(II) sulphateE010

Soil AR PAH - Speciated (EPA 16)Determination of PAH compounds by extraction in acetone and hexane followed by GC-MS with the

use of surrogate and internal standardsE005

Soil AR PCB - 7 Congeners Determination of PCB by extraction with acetone and hexane followed by GC-MS E008

Soil D Petroleum Ether Extract (PEE) Gravimetrically determined through extraction with petroleum ether E011

Soil AR pH Determination of pH by addition of water followed by electrometric measurement E007

Soil AR Phenols - Total (monohydric) Determination of phenols by distillation followed by colorimetry E021

Soil D Phosphate - Water Soluble (2:1) Determination of phosphate by extraction with water & analysed by ion chromatography E009

Soil D Sulphate (as SO4) - Total Determination of total sulphate by extraction with 10% HCl followed by ICP-OES E013

Soil D Sulphate (as SO4) - Water Soluble (2:1) Determination of sulphate by extraction with water & analysed by ion chromatography E009

Soil D Sulphate (as SO4) - Water Soluble (2:1) Determination of water soluble sulphate by extraction with water followed by ICP-OES E014

Soil AR Sulphide Determination of sulphide by distillation followed by colorimetry E018

Soil D Sulphur - Total Determination of total sulphur by extraction with aqua-regia followed by ICP-OES E024

Soil AR SVOCDetermination of semi-volatile organic compounds by extraction in acetone and hexane followed by

GC-MSE006

Soil AR Thiocyanate (as SCN)Determination of thiocyanate by extraction in caustic soda followed by acidification followed by

addition of ferric nitrate followed by colorimetryE017

Soil D Toluene Extractable Matter (TEM) Gravimetrically determined through extraction with toluene E011

Soil D Total Organic Carbon (TOC)Determination of organic matter by oxidising with potassium dichromate followed by titration with iron

(II) sulphateE010

Soil AR TPH CWG Determination of hexane/acetone extractable hydrocarbons by GC-FID fractionating with SPE cartridge E004

Soil AR TPH LQM Determination of hexane/acetone extractable hydrocarbons by GC-FID fractionating with SPE cartridge E004

Soil AR VOCs Determination of volatile organic compounds by headspace GC-MS E001

Soil AR VPH (C6 - C10) Determination of hydrocarbons C6-C10 by headspace GC-MS E001

D Dried

AR As Received

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Order No: None Supplied

Reporting Date: 18/07/2014

Tel : 01622 850410 '

Soil Analysis Certificate - Methodology & Miscellaneous InformationQTS Environmental Report No: 14-22971

Lustre Consulting Ltd

Site Reference: K & N Distribution Depot - Draycott-in-the-Clay

Project / Job Ref: 1309

QTS Environmental Ltd - Registered in England No 06620874 Page 21 of 21

Page 23: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

James May QTS Environmental Ltd

Lustre Consulting Ltd Unit 1

Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Kent

ME17 2JNt: 01622 850410

[email protected]

Site Reference: Draycott in the Clay

Project / Job Ref: 1309

Order No: None Supplied

Sample Receipt Date: 17/07/2014

Sample Scheduled Date: 17/07/2014

Report Issue Number: 2

Reporting Date: 23/07/2014

Authorised by: Authorised by:

Russell Jarvis Kevin OldDirector Director

On behalf of QTS Environmental Ltd On behalf of QTS Environmental Ltd

Admiral's Offices

The Historic Dockyard

Chatham

Kent

ME4 4TZ

QTS Environmental Report No: 14-23129

QTS Environmental Ltd - Registered in England No 06620874 Page 1 of 11

Page 24: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

None Supplied None Supplied None Supplied None Supplied None Supplied

None Supplied None Supplied None Supplied None Supplied None Supplied

AWS02 AWS03 AWS04 AWS06 AWS07

None Supplied None Supplied None Supplied None Supplied None Supplied

None Supplied None Supplied None Supplied None Supplied None Supplied

111381 111382 111383 111384 111385

Determinand Unit RL Accreditation

pH pH Units N/a ISO17025 7.5 7.1 7.1 7.4 7.7

Total Cyanide ug/l < 5 NONE < 5 < 5 < 5 < 5 < 5

Sulphate as SO4 mg/l < 1 ISO17025 84 280 214 73 87

Total Organic Carbon (TOC) mg/l < 0.1 NONE 6.3 3.6 7.1 11.8 2.6

Arsenic (dissolved) ug/l < 10 NONE < 10 < 10 < 10 < 10 < 10

Boron (dissolved) ug/l < 50 NONE 121 88 60 < 50 182

Cadmium (dissolved) ug/l < 0.5 NONE < 0.5 < 0.5 < 0.5 < 0.5 < 0.5

Chromium (dissolved) ug/l < 5 NONE < 5 < 5 < 5 < 5 6

Chromium (hexavalent) ug/l < 5 NONE < 5 < 5 < 5 < 5 < 5

Copper (dissolved) ug/l < 10 NONE < 10 22 20 < 10 < 10

Lead (dissolved) ug/l < 5 NONE 8 7 14 < 5 10

Mercury (dissolved) ug/l < 0.05 NONE < 0.05 < 0.05 < 0.05 < 0.05 < 0.05

Nickel (dissolved) ug/l < 7 NONE < 7 < 7 < 7 < 7 < 7

Selenium (dissolved) ug/l < 5 NONE < 5 < 5 < 5 < 5 6

Zinc (dissolved) ug/l < 5 NONE 20 28 33 7 39

Total Phenols ug/l < 0.5 NONE < 0.5 < 0.5 < 0.5 < 0.5 < 0.5

EPH (C10 - C40) ug/l < 10 NONE 36 < 10 76 791 < 10

Subcontracted analysis (S)

Insufficient sample I/S

Unsuitable Sample U/S

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410

Water Analysis CertificateQTS Environmental Report No: 14-23129 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: Draycott in the Clay TP / BH NoProject / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

Reporting Date: 23/07/2014 QTSE Sample No

QTS Environmental Ltd - Registered in England No 06620874 Page 2 of 11

Page 25: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

None Supplied

None Supplied

AWS11

None Supplied

None Supplied

111386

Determinand Unit RL Accreditation

pH pH Units N/a ISO17025 7.1

Total Cyanide ug/l < 5 NONE < 5

Sulphate as SO4 mg/l < 1 ISO17025 954

Total Organic Carbon (TOC) mg/l < 0.1 NONE 3.5

Arsenic (dissolved) ug/l < 10 NONE 13

Boron (dissolved) ug/l < 50 NONE 141

Cadmium (dissolved) ug/l < 0.5 NONE < 0.5

Chromium (dissolved) ug/l < 5 NONE < 5

Chromium (hexavalent) ug/l < 5 NONE < 5

Copper (dissolved) ug/l < 10 NONE 22

Lead (dissolved) ug/l < 5 NONE < 5

Mercury (dissolved) ug/l < 0.05 NONE < 0.05

Nickel (dissolved) ug/l < 7 NONE < 7

Selenium (dissolved) ug/l < 5 NONE < 5

Zinc (dissolved) ug/l < 5 NONE 38

Total Phenols ug/l < 0.5 NONE < 0.5

EPH (C10 - C40) ug/l < 10 NONE < 10

Subcontracted analysis (S)

Insufficient sample I/S

Unsuitable Sample U/S

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410

Water Analysis CertificateQTS Environmental Report No: 14-23129 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: Draycott in the Clay TP / BH NoProject / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

Reporting Date: 23/07/2014 QTSE Sample No

QTS Environmental Ltd - Registered in England No 06620874 Page 3 of 11

Page 26: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

None Supplied None Supplied None Supplied None Supplied None Supplied

None Supplied None Supplied None Supplied None Supplied None Supplied

AWS02 AWS03 AWS04 AWS06 AWS07

None Supplied None Supplied None Supplied None Supplied None Supplied

None Supplied None Supplied None Supplied None Supplied None Supplied

111381 111382 111383 111384 111385

Determinand Unit RL Accreditation

Naphthalene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Acenaphthylene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Acenaphthene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 0.19 < 0.01

Fluorene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 0.25 < 0.01

Phenanthrene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 0.13 < 0.01

Anthracene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Fluoranthene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Pyrene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Benzo(a)anthracene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Chrysene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Benzo(b)fluoranthene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Benzo(k)fluoranthene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Benzo(a)pyrene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Indeno(1,2,3-cd)pyrene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Dibenz(a,h)anthracene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Benzo(ghi)perylene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Total EPA-16 PAHs ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 0.57 < 0.01

-

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410

Water Analysis Certificate - Speciated PAHQTS Environmental Report No: 14-23129 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: Draycott in the Clay TP / BH NoProject / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

Reporting Date: 23/07/2014 QTSE Sample No

QTS Environmental Ltd - Registered in England No 06620874 Page 4 of 11

Page 27: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

None Supplied

None Supplied

AWS11

None Supplied

None Supplied

111386

Determinand Unit RL Accreditation

Naphthalene ug/l < 0.01 NONE < 0.01

Acenaphthylene ug/l < 0.01 NONE < 0.01

Acenaphthene ug/l < 0.01 NONE < 0.01

Fluorene ug/l < 0.01 NONE < 0.01

Phenanthrene ug/l < 0.01 NONE < 0.01

Anthracene ug/l < 0.01 NONE < 0.01

Fluoranthene ug/l < 0.01 NONE < 0.01

Pyrene ug/l < 0.01 NONE < 0.01

Benzo(a)anthracene ug/l < 0.01 NONE < 0.01

Chrysene ug/l < 0.01 NONE < 0.01

Benzo(b)fluoranthene ug/l < 0.01 NONE < 0.01

Benzo(k)fluoranthene ug/l < 0.01 NONE < 0.01

Benzo(a)pyrene ug/l < 0.01 NONE < 0.01

Indeno(1,2,3-cd)pyrene ug/l < 0.01 NONE < 0.01

Dibenz(a,h)anthracene ug/l < 0.01 NONE < 0.01

Benzo(ghi)perylene ug/l < 0.01 NONE < 0.01

Total EPA-16 PAHs ug/l < 0.01 NONE < 0.01

-

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410

Water Analysis Certificate - Speciated PAHQTS Environmental Report No: 14-23129 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: Draycott in the Clay TP / BH NoProject / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

Reporting Date: 23/07/2014 QTSE Sample No

QTS Environmental Ltd - Registered in England No 06620874 Page 5 of 11

Page 28: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

None Supplied None Supplied None Supplied None Supplied None Supplied

None Supplied None Supplied None Supplied None Supplied None Supplied

AWS02 AWS03 AWS04 AWS06 AWS07

None Supplied None Supplied None Supplied None Supplied None Supplied

None Supplied None Supplied None Supplied None Supplied None Supplied

111381 111382 111383 111384 111385

Determinand Unit RL Accreditation

Aliphatic >C5 - C6 ug/l < 10 NONE 195 < 10 < 10 < 10 < 10

Aliphatic >C6 - C8 ug/l < 10 NONE 530 < 10 4680 < 10 < 10

Aliphatic >C8 - C10 ug/l < 10 NONE 23 < 10 < 10 50 < 10

Aliphatic >C10 - C12 ug/l < 10 NONE < 10 < 10 < 10 72 < 10

Aliphatic >C12 - C16 ug/l < 10 NONE < 10 < 10 < 10 25 < 10

Aliphatic >C16 - C21 ug/l < 10 NONE < 10 < 10 < 10 < 10 < 10

Aliphatic >C21 - C34 ug/l < 10 NONE < 10 < 10 < 10 < 10 < 10

Aliphatic (C5 - C34) ug/l < 70 NONE 748 < 70 4680 147 < 70

Aromatic >C5 - C7 ug/l < 10 NONE < 10 < 10 < 10 < 10 < 10

Aromatic >C7 - C8 ug/l < 10 NONE < 10 < 10 < 10 < 10 < 10

Aromatic >C8 - C10 ug/l < 10 NONE < 10 < 10 < 10 130 < 10

Aromatic >C10 - C12 ug/l < 10 NONE < 10 < 10 < 10 418 < 10

Aromatic >C12 - C16 ug/l < 10 NONE < 10 < 10 14 146 < 10

Aromatic >C16 - C21 ug/l < 10 NONE < 10 < 10 10 < 10 < 10

Aromatic >C21 - C35 ug/l < 10 NONE < 10 < 10 < 10 < 10 < 10

Aromatic (C5 - C35) ug/l < 70 NONE < 70 < 70 < 70 693 < 70

Total >C5 - C35 ug/l < 140 NONE 748 < 140 4705 840 < 140

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410

Water Analysis Certificate - TPH CWG BandedQTS Environmental Report No: 14-23129 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: Draycott in the Clay TP / BH NoProject / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

Reporting Date: 23/07/2014 QTSE Sample No

QTS Environmental Ltd - Registered in England No 06620874 Page 6 of 11

Page 29: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

None Supplied

None Supplied

AWS11

None Supplied

None Supplied

111386

Determinand Unit RL Accreditation

Aliphatic >C5 - C6 ug/l < 10 NONE < 10

Aliphatic >C6 - C8 ug/l < 10 NONE < 10

Aliphatic >C8 - C10 ug/l < 10 NONE < 10

Aliphatic >C10 - C12 ug/l < 10 NONE < 10

Aliphatic >C12 - C16 ug/l < 10 NONE < 10

Aliphatic >C16 - C21 ug/l < 10 NONE < 10

Aliphatic >C21 - C34 ug/l < 10 NONE < 10

Aliphatic (C5 - C34) ug/l < 70 NONE < 70

Aromatic >C5 - C7 ug/l < 10 NONE < 10

Aromatic >C7 - C8 ug/l < 10 NONE < 10

Aromatic >C8 - C10 ug/l < 10 NONE < 10

Aromatic >C10 - C12 ug/l < 10 NONE < 10

Aromatic >C12 - C16 ug/l < 10 NONE < 10

Aromatic >C16 - C21 ug/l < 10 NONE < 10

Aromatic >C21 - C35 ug/l < 10 NONE < 10

Aromatic (C5 - C35) ug/l < 70 NONE < 70

Total >C5 - C35 ug/l < 140 NONE < 140

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410

Water Analysis Certificate - TPH CWG BandedQTS Environmental Report No: 14-23129 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: Draycott in the Clay TP / BH NoProject / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

Reporting Date: 23/07/2014 QTSE Sample No

QTS Environmental Ltd - Registered in England No 06620874 Page 7 of 11

Page 30: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

None Supplied None Supplied None Supplied None Supplied None Supplied

None Supplied None Supplied None Supplied None Supplied None Supplied

AWS02 AWS03 AWS04 AWS06 AWS07

None Supplied None Supplied None Supplied None Supplied None Supplied

None Supplied None Supplied None Supplied None Supplied None Supplied

111381 111382 111383 111384 111385

Determinand Unit RL Accreditation

Benzene ug/l < 1 ISO17025 < 1 < 1 < 1 < 1 < 1

Toluene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

Ethylbenzene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

p & m-xylene ug/l < 10 ISO17025 < 10 < 10 < 10 < 10 < 10

o-xylene ug/l < 5 ISO17025 < 5 < 5 < 5 31 < 5

MTBE ug/l < 10 ISO17025 195 < 10 < 10 < 10 < 10

.

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410

Water Analysis Certificate - BTEX / MTBEQTS Environmental Report No: 14-23129 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: Draycott in the Clay TP / BH NoProject / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

Reporting Date: 23/07/2014 QTSE Sample No

QTS Environmental Ltd - Registered in England No 06620874 Page 8 of 11

Page 31: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

None Supplied

None Supplied

AWS11

None Supplied

None Supplied

111386

Determinand Unit RL Accreditation

Benzene ug/l < 1 ISO17025 < 1

Toluene ug/l < 5 ISO17025 < 5

Ethylbenzene ug/l < 5 ISO17025 < 5

p & m-xylene ug/l < 10 ISO17025 < 10

o-xylene ug/l < 5 ISO17025 < 5

MTBE ug/l < 10 ISO17025 < 10

.

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410

Water Analysis Certificate - BTEX / MTBEQTS Environmental Report No: 14-23129 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: Draycott in the Clay TP / BH NoProject / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

Reporting Date: 23/07/2014 QTSE Sample No

QTS Environmental Ltd - Registered in England No 06620874 Page 9 of 11

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None Supplied None Supplied None Supplied

None Supplied None Supplied None Supplied

AWS02 AWS04 AWS07

None Supplied None Supplied None Supplied

None Supplied None Supplied None Supplied

111381 111383 111385

Determinand Unit RL Accreditation

Dichlorodifluoromethane ug/l < 5 ISO17025 < 5 < 5 < 5

Vinyl Chloride ug/l < 5 ISO17025 < 5 < 5 < 5

Chloromethane ug/l < 5 ISO17025 < 5 < 5 < 5

Chloroethane ug/l < 5 ISO17025 < 5 < 5 < 5

Bromomethane ug/l < 5 ISO17025 < 5 < 5 < 5

Trichlorofluoromethane ug/l < 5 ISO17025 < 5 < 5 < 5

1,1-Dichloroethene ug/l < 5 ISO17025 < 5 < 5 < 5

MTBE ug/l < 10 ISO17025 195 < 10 < 10

trans-1,2-Dichloroethene ug/l < 5 ISO17025 < 5 < 5 < 5

1,1-Dichloroethane ug/l < 5 ISO17025 < 5 < 5 < 5

cis-1,2-Dichloroethene ug/l < 5 ISO17025 < 5 < 5 < 5

2,2-Dichloropropane ug/l < 5 ISO17025 < 5 < 5 < 5

Chloroform ug/l < 5 ISO17025 < 5 < 5 < 5

Bromochloromethane ug/l < 10 ISO17025 < 10 < 10 < 10

1,1,1-Trichloroethane ug/l < 5 ISO17025 < 5 < 5 < 5

1,1-Dichloropropene ug/l < 5 ISO17025 < 5 < 5 < 5

Carbon Tetrachloride ug/l < 5 ISO17025 < 5 < 5 < 5

1,2-Dichloroethane ug/l < 10 ISO17025 < 10 < 10 < 10

Benzene ug/l < 1 ISO17025 < 1 < 1 < 1

1,2-Dichloropropane ug/l < 5 ISO17025 < 5 < 5 < 5

Trichloroethene ug/l < 5 ISO17025 < 5 4680 < 5

Bromodichloromethane ug/l < 5 ISO17025 < 5 < 5 < 5

Dibromomethane ug/l < 5 ISO17025 < 5 < 5 < 5

TAME ug/l < 5 ISO17025 530 < 5 < 5

cis-1,3-Dichloropropene ug/l < 5 ISO17025 < 5 < 5 < 5

Toluene ug/l < 5 ISO17025 < 5 < 5 < 5

trans-1,3-Dichloropropene ug/l < 5 ISO17025 < 5 < 5 < 5

1,1,2-Trichloroethane ug/l < 10 ISO17025 < 10 < 10 < 10

1,3-Dichloropropane ug/l < 5 ISO17025 < 5 < 5 < 5

Tetrachloroethene ug/l < 5 ISO17025 < 5 < 5 < 5

Dibromochloromethane ug/l < 5 ISO17025 < 5 < 5 < 5

1,2-Dibromoethane ug/l < 5 ISO17025 < 5 < 5 < 5

Chlorobenzene ug/l < 5 ISO17025 < 5 < 5 < 5

1,1,1,2-Tetrachloroethane ug/l < 5 ISO17025 < 5 < 5 < 5

Ethyl Benzene ug/l < 5 ISO17025 < 5 < 5 < 5

m,p-Xylene ug/l < 10 ISO17025 < 10 < 10 < 10

o-Xylene ug/l < 5 ISO17025 < 5 < 5 < 5

Styrene ug/l < 5 ISO17025 < 5 < 5 < 5

Bromoform ug/l < 10 ISO17025 < 10 < 10 < 10

Isopropylbenzene ug/l < 5 ISO17025 < 5 < 5 < 5

1,1,2,2-Tetrachloroethane ug/l < 10 ISO17025 < 10 < 10 < 10

1,2,3-Trichloropropane ug/l < 5 ISO17025 < 5 < 5 < 5

n-Propylbenzene ug/l < 5 ISO17025 < 5 < 5 < 5

Bromobenzene ug/l < 5 ISO17025 < 5 < 5 < 5

2-Chlorotoluene ug/l < 5 ISO17025 < 5 < 5 < 5

1,3,5-Trimethylbenzene ug/l < 5 ISO17025 < 5 < 5 < 5

4-Chlorotoluene ug/l < 5 ISO17025 < 5 < 5 < 5

tert-Butylbenzene ug/l < 5 ISO17025 < 5 < 5 < 5

1,2,4-Trimethylbenzene ug/l < 5 ISO17025 < 5 < 5 < 5

sec-Butylbenzene ug/l < 5 ISO17025 < 5 < 5 < 5

p-Isopropyltoluene ug/l < 5 ISO17025 < 5 < 5 < 5

1,3-Dichlorobenzene ug/l < 5 ISO17025 < 5 < 5 < 5

1,4-Dichlorobenzene ug/l < 5 ISO17025 < 5 < 5 < 5

n-Butylbenzene ug/l < 5 ISO17025 < 5 < 5 < 5

1,2-Dichlorobenzene ug/l < 5 ISO17025 < 5 < 5 < 5

1,2-Dibromo-3-chloropropane ug/l < 10 ISO17025 < 10 < 10 < 10

Hexachlorobutadiene ug/l < 5 ISO17025 < 5 < 5 < 5

-

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410

Water Analysis Certificate - Volatile Organic Compounds (VOC)QTS Environmental Report No: 14-23129 Date Sampled

Lustre Consulting Ltd Time Sampled

Reporting Date: 23/07/2014 QTSE Sample No

Site Reference: Draycott in the Clay TP / BH NoProject / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

QTS Environmental Ltd - Registered in England No 06620874 Page 10 of 11

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Matrix Analysed

On

Determinand Brief Method Description Method

No

Water UF AlkalinityDetermination of alkalinity by titration against hydrochloric acid using bromocresol green as the end

pointE103

Water UF BTEX Determination of BTEX by headspace GC-MS E101

Water F Cations Determination of cations by filtration followed by ICP-MS E102

Water UF Chemical Oxygen Demand (COD) Determination using a COD reactor followed by colorimetry E112

Water F Chloride Determination of chloride by filtration & analysed by ion chromatography E109

Water F Chromium - Hexavalent Determination of hexavalent chromium by acidification, addition of 1,5 diphenylcarbazide followed by colorimetryE116

Water UF Cyanide - Complex Determination of complex cyanide by distillation followed by colorimetry E115

Water UF Cyanide - Free Determination of free cyanide by distillation followed by colorimetry E115

Water UF Cyanide - Total Determination of total cyanide by distillation followed by colorimetry E115

Water UF Cyclohexane Extractable Matter (CEM) Gravimetrically determined through liquid:liquid extraction with cyclohexane E111

Water F Diesel Range Organics (C10 - C24) Determination of liquid:liquid extraction with hexane followed by GI-FID E104

Water F Dissolved Organic Content (DOC) Determination of DOC by filtration followed by low heat with persulphate addition followed by IR detectionE110

Water UF Electrical Conductivity Determination of electrical conductivity by electrometric measurement E123

Water F EPH (C10 – C40) Determination of liquid:liquid extraction with hexane followed by GI-FID E104

Water F EPH TEXAS Determination of liquid:liquid extraction with hexane followed by GI-FID E104

Water F Fluoride Determination of Fluoride by filtration & analysed by ion chromatography E109

Water F Hardness Determination of Ca and Mg by ICP-MS followed by calculation E102

Leachate F Leachate Preparation - NRA Based on National Rivers Authority leaching test 1994 E301

Leachate F Leachate Preparation - WAC Based on BS EN 12457 Pt1, 2, 3 E302

Water F Metals Determination of metals by filtration followed by ICP-MS E102

Water F Mineral Oil (C10 - C40) Determination of liquid:liquid extraction with hexane followed by GI-FID E104

Water F Nitrate Determination of nitrate by filtration & analysed by ion chromatography E109

Water UF Monohydric Phenol Determination of phenols by distillation followed by colorimetry E121

Water F PAH - Speciated (EPA 16)Determination of PAH compounds by concentration through SPE cartridge, collection in

dichloromethane followed by GC-MSE105

Water F PCB - 7 Congeners Determination of PCB compounds by concentration through SPE cartridge, collection in dichloromethane followed by GC-MSE108

Water UF Petroleum Ether Extract (PEE) Gravimetrically determined through liquid:liquid extraction with petroleum ether E111

Water UF pH Determination of pH by electrometric measurement E107

Water F Phosphate Determination of phosphate by filtration & analysed by ion chromatography E109

Water UF Redox Potential Determination of redox potential by electrometric measurement E113

Water F Sulphate (as SO4) Determination of sulphate by filtration & analysed by ion chromatography E109

Water UF Sulphide Determination of sulphide by distillation followed by colorimetry E118

Water F SVOCDetermination of semi-volatile organic compounds by concentration through SPE cartridge, collection

in dichloromethane followed by GC-MSE106

Water UF Toluene Extractable Matter (TEM) Gravimetrically determined through liquid:liquid extraction with toluene E111

Water UF Total Organic Carbon (TOC) Low heat with persulphate addition followed by IR detection E110

Water F TPH CWG Determination of liquid:liquid extraction with hexane, fractionating with SPE followed by GC-FID E104

Water F TPH LQM Determination of liquid:liquid extraction with hexane, fractionating with SPE followed by GC-FID E104

Water UF VOCs Determination of volatile organic compounds by headspace GC-MS E101

Water UF VPH (C6 - C10) Determination of hydrocarbons C6-C10 by headspace GC-MS E101

Key

F Filtered

UF Unfiltered

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Order No: None Supplied

Reporting Date: 23/07/2014

Tel : 01622 850410 '

Soil Analysis Certificate - Methodology & Miscellaneous InformationQTS Environmental Report No: 14-23129

Lustre Consulting Ltd

Site Reference: Draycott in the Clay

Project / Job Ref: 1309

QTS Environmental Ltd - Registered in England No 06620874 Page 11 of 11

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Page 35: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS
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Page 37: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Matthew Larkin QTS Environmental Ltd

Lustre Consulting Ltd Unit 1

Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Kent

ME17 2JNt: 01622 850410

[email protected]

Site Reference: Draycott in the Clay

Project / Job Ref: 1309

Order No: None Supplied

Sample Receipt Date: 17/07/2014

Sample Scheduled Date: 31/07/2014

Report Issue Number: 1

Reporting Date: 04/08/2014

Authorised by: Authorised by:

Russell Jarvis Kevin OldDirector Director

On behalf of QTS Environmental Ltd On behalf of QTS Environmental Ltd

Admiral's Offices

The Historic Dockyard

Chatham

Kent

ME4 4TZ

QTS Environmental Report No: 14-23462

QTS Environmental Ltd - Registered in England No 06620874 Page 1 of 2

Page 38: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

None Supplied None Supplied None Supplied

None Supplied None Supplied None Supplied

AWS06 BH1 BH3

None Supplied None Supplied None Supplied

None Supplied None Supplied None Supplied

112751 112752 112753

Determinand Unit RL Accreditation

EPH (>C8 - C10) % < 1 NONE 15 1 6

EPH (>C10 - C12) % < 1 NONE 46 5 12

EPH (>C12 - C16) % < 1 NONE 29 32 36

EPH (>C16 - C21) % < 1 NONE 7 47 39

EPH (>C21 - C40) % < 1 NONE 3 15 7

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410

Oil Analysis Certificate - EPH BandedQTS Environmental Report No: 14-23462 Date Sampled

Lustre Consulting Ltd Time Sampled

Reporting Date: 04/08/2014 QTSE Sample No

Site Reference: Draycott in the Clay TP / BH NoProject / Job Ref: 1309 Additional Refs

Order No: None Supplied Depth (m)

QTS Environmental Ltd - Registered in England No 06620874 Page 2 of 2

Page 39: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Amy Khan QTS Environmental Ltd

Lustre Consulting Ltd Unit 1

Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Kent

ME17 2JN

t: 01622 [email protected]

Site Reference: K & N Distribution Depot, Derby

Project / Job Ref: 1309

Order No: 1309

Sample Receipt Date: 16/10/2014

Sample Scheduled Date: 16/10/2014

Report Issue Number: 1

Reporting Date: 22/10/2014

Authorised by: Authorised by:

Russell Jarvis Kevin Old

Director Director

On behalf of QTS Environmental Ltd On behalf of QTS Environmental Ltd

Admiral's Offices

The Historic Dockyard

Chatham

Kent

ME4 4TZ

QTS Environmental Report No: 14-25663

QTS Environmental Ltd - Registered in England No 06620874 Page 1 of 28

Page 40: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

10/09/14 09/09/14 09/09/14 10/09/14 10/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

SP1 TP1 TP2 TP3 TP3

None Supplied None Supplied None Supplied None Supplied None Supplied

0.50 0.30 - 0.50 0.10 - 0.30 0.05 0.50

121787 121788 121789 121790 121791

Determinand Unit RL Accreditation

Asbestos Screen N/a N/a ISO17025 Not Detected Not Detected Not Detected Not Detected

pH pH Units N/a MCERTS 9.1 8.1 7.8 7.6

Total Cyanide mg/kg < 2 NONE < 2 < 2 < 2

Total Sulphate as SO4 mg/kg < 200 NONE 1228

W/S Sulphate as SO4 (2:1) g/l < 0.01 MCERTS 0.09 0.10 0.09 0.14

Total Sulphur mg/kg < 200 NONE 595

Total Organic Carbon (TOC) % < 0.1 NONE 1.1 3.7 2.1

Ammonium as NH4 mg/kg < 0.5 NONE 4.2

W/S Chloride (2:1) mg/kg < 1 MCERTS 10

Water Soluble Nitrate (2:1) as NO3 mg/kg < 3 MCERTS < 3

Arsenic (As) mg/kg < 2 MCERTS 4 18 5

W/S Boron mg/kg < 1 NONE < 1 < 1 < 1

Cadmium (Cd) mg/kg < 0.5 MCERTS 1 0.5 < 0.5

Chromium (Cr) mg/kg < 2 MCERTS 30 30 34

Chromium (hexavalent) mg/kg < 2 NONE < 2 < 2 < 2

Copper (Cu) mg/kg < 4 MCERTS 39 75 19

Lead (Pb) mg/kg < 3 MCERTS 52 76 35

W/S Magnesium g/l < 0.0001 NONE 0.0267

Mercury (Hg) mg/kg < 1 NONE < 1 < 1 < 1

Nickel (Ni) mg/kg < 3 MCERTS 34 45 32

Selenium (Se) mg/kg < 3 NONE < 3 < 3 < 3

Zinc (Zn) mg/kg < 3 MCERTS 165 126 113

Total Phenols (monohydric) mg/kg < 2 NONE < 2 < 2 < 2

EPH (C10 - C40) mg/kg < 6 MCERTS

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

This report refers to samples as received, and QTS Environmental Ltd, takes no responsibility for the accuracy or competence of sampling by others.

The material description shall be regarded as tentative and is not included in our scope of UKAS Accreditation.

Opinions and interpretations expressed herein are outside the scope of UKAS Accreditation.

Asbestos Analyst: Graham Revell

RL: Reporting Limit

Pinch Test: Where pinch test is positive it is reported “Loose Fibres - PT” with type(s).

Subcontracted analysis (S)

Site Reference: K & N Distribution Depot, Derby TP / BH No

Project / Job Ref: 1309 Additional Refs

Tel : 01622 850410 '

Soil Analysis Certificate

QTS Environmental Report No: 14-25663 Date Sampled

Lustre Consulting Ltd Time Sampled

QTS Environmental Ltd '

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Reporting Date: 22/10/2014 QTSE Sample No

Analysis carried out on the dried sample is corrected for the stone content

The samples have been examined to identify the presence of asbestiform minerals by polarising light microscopy and dispersion staining technique to In-House Procedures QTSE600 Determination of Asbestos in Bulk

Materials; Asbestos in Soils/Sediments (fibre screening and identification)

Order No: 1309 Depth (m)

QTS Environmental Ltd - Registered in England No 06620874 Page 2 of 28

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10/09/14 10/09/14 10/09/14 09/09/14 09/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

TP4 TP5 TP6 TP9 TP10

None Supplied None Supplied None Supplied None Supplied None Supplied

0.20 0.50 & BB 0.20 0.20 0.10 - 0.30

121792 121793 121794 121795 121796

Determinand Unit RL Accreditation

Asbestos Screen N/a N/a ISO17025 Not Detected Not Detected Not Detected Not Detected Not Detected

pH pH Units N/a MCERTS 7.6 7.8 7.9 7.7

Total Cyanide mg/kg < 2 NONE < 2 < 2 < 2 < 2

Total Sulphate as SO4 mg/kg < 200 NONE

W/S Sulphate as SO4 (2:1) g/l < 0.01 MCERTS 0.07 0.03 1.09 0.67

Total Sulphur mg/kg < 200 NONE

Total Organic Carbon (TOC) % < 0.1 NONE 1.8 0.2 1 1.6

Ammonium as NH4 mg/kg < 0.5 NONE

W/S Chloride (2:1) mg/kg < 1 MCERTS

Water Soluble Nitrate (2:1) as NO3 mg/kg < 3 MCERTS

Arsenic (As) mg/kg < 2 MCERTS 4 3 4 4

W/S Boron mg/kg < 1 NONE < 1 < 1 1.5 < 1

Cadmium (Cd) mg/kg < 0.5 MCERTS < 0.5 < 0.5 0.6 0.9

Chromium (Cr) mg/kg < 2 MCERTS 31 16 21 27

Chromium (hexavalent) mg/kg < 2 NONE < 2 < 2 < 2 < 2

Copper (Cu) mg/kg < 4 MCERTS 19 7 35 51

Lead (Pb) mg/kg < 3 MCERTS 24 52 33 122

W/S Magnesium g/l < 0.0001 NONE

Mercury (Hg) mg/kg < 1 NONE < 1 < 1 < 1 < 1

Nickel (Ni) mg/kg < 3 MCERTS 36 22 12 24

Selenium (Se) mg/kg < 3 NONE < 3 < 3 < 3 < 3

Zinc (Zn) mg/kg < 3 MCERTS 83 49 129 323

Total Phenols (monohydric) mg/kg < 2 NONE < 2 < 2 < 2 < 2

EPH (C10 - C40) mg/kg < 6 MCERTS < 6

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

This report refers to samples as received, and QTS Environmental Ltd, takes no responsibility for the accuracy or competence of sampling by others.

The material description shall be regarded as tentative and is not included in our scope of UKAS Accreditation.

Opinions and interpretations expressed herein are outside the scope of UKAS Accreditation.

Asbestos Analyst: Graham Revell

RL: Reporting Limit

Pinch Test: Where pinch test is positive it is reported “Loose Fibres - PT” with type(s).

Subcontracted analysis (S)

Reporting Date: 22/10/2014 QTSE Sample No

Analysis carried out on the dried sample is corrected for the stone content

The samples have been examined to identify the presence of asbestiform minerals by polarising light microscopy and dispersion staining technique to In-House Procedures QTSE600 Determination of Asbestos in Bulk

Materials; Asbestos in Soils/Sediments (fibre screening and identification)

Site Reference: K & N Distribution Depot, Derby TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: 1309 Depth (m)

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate

QTS Environmental Report No: 14-25663 Date Sampled

Lustre Consulting Ltd Time Sampled

QTS Environmental Ltd '

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

QTS Environmental Ltd - Registered in England No 06620874 Page 3 of 28

Page 42: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

09/09/14 09/09/14 09/09/14 09/09/14 09/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

TP11 TP12 TP15 TP16 TP16

None Supplied None Supplied None Supplied None Supplied None Supplied

0.30 0.10 - 0.20 0.60 - 0.70 GL - 0.10 0.20 - 0.30

121797 121798 121799 121800 121801

Determinand Unit RL Accreditation

Asbestos Screen N/a N/a ISO17025 Not Detected Not Detected Not Detected Not Detected Not Detected

pH pH Units N/a MCERTS 7.5 7.4 9.0 8.1

Total Cyanide mg/kg < 2 NONE < 2 < 2 < 2 < 2

Total Sulphate as SO4 mg/kg < 200 NONE

W/S Sulphate as SO4 (2:1) g/l < 0.01 MCERTS 0.18 0.09 1.12 0.55

Total Sulphur mg/kg < 200 NONE

Total Organic Carbon (TOC) % < 0.1 NONE 2 1.8 2.4 1.7

Ammonium as NH4 mg/kg < 0.5 NONE

W/S Chloride (2:1) mg/kg < 1 MCERTS

Water Soluble Nitrate (2:1) as NO3 mg/kg < 3 MCERTS

Arsenic (As) mg/kg < 2 MCERTS 3 6 14 10

W/S Boron mg/kg < 1 NONE < 1 < 1 2.5 1.3

Cadmium (Cd) mg/kg < 0.5 MCERTS < 0.5 < 0.5 1 0.7

Chromium (Cr) mg/kg < 2 MCERTS 35 30 24 15

Chromium (hexavalent) mg/kg < 2 NONE < 2 < 2 < 2 < 2

Copper (Cu) mg/kg < 4 MCERTS 23 18 57 31

Lead (Pb) mg/kg < 3 MCERTS 34 43 53 28

W/S Magnesium g/l < 0.0001 NONE

Mercury (Hg) mg/kg < 1 NONE < 1 < 1 < 1 < 1

Nickel (Ni) mg/kg < 3 MCERTS 35 29 44 25

Selenium (Se) mg/kg < 3 NONE < 3 < 3 < 3 < 3

Zinc (Zn) mg/kg < 3 MCERTS 100 210 202 97

Total Phenols (monohydric) mg/kg < 2 NONE < 2 < 2 < 2 < 2

EPH (C10 - C40) mg/kg < 6 MCERTS

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

This report refers to samples as received, and QTS Environmental Ltd, takes no responsibility for the accuracy or competence of sampling by others.

The material description shall be regarded as tentative and is not included in our scope of UKAS Accreditation.

Opinions and interpretations expressed herein are outside the scope of UKAS Accreditation.

Asbestos Analyst: Graham Revell

RL: Reporting Limit

Pinch Test: Where pinch test is positive it is reported “Loose Fibres - PT” with type(s).

Subcontracted analysis (S)

QTSE Sample No

Analysis carried out on the dried sample is corrected for the stone content

The samples have been examined to identify the presence of asbestiform minerals by polarising light microscopy and dispersion staining technique to In-House Procedures QTSE600 Determination of Asbestos in Bulk

Materials; Asbestos in Soils/Sediments (fibre screening and identification)

Site Reference: K & N Distribution Depot, Derby TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: 1309 Depth (m)

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate

QTS Environmental Report No: 14-25663 Date Sampled

Lustre Consulting Ltd Time Sampled

QTS Environmental Ltd '

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Reporting Date: 22/10/2014

QTS Environmental Ltd - Registered in England No 06620874 Page 4 of 28

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09/09/14 06/09/14 06/09/14 06/09/14 06/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

TP17 WS501 WS501 WS502 WS503

None Supplied None Supplied None Supplied None Supplied None Supplied

0.10 0.10 - 0.20 1.80 - 1.90 0.30 - 0.40 0.60 - 0.70

121802 121803 121804 121805 121806

Determinand Unit RL Accreditation

Asbestos Screen N/a N/a ISO17025 Not Detected Not Detected Not Detected Not Detected

pH pH Units N/a MCERTS 7.8 7.6 7.5 7.6

Total Cyanide mg/kg < 2 NONE < 2 < 2 < 2

Total Sulphate as SO4 mg/kg < 200 NONE 3321

W/S Sulphate as SO4 (2:1) g/l < 0.01 MCERTS 0.73 0.40 0.12 0.08

Total Sulphur mg/kg < 200 NONE 1122

Total Organic Carbon (TOC) % < 0.1 NONE 0.5 1.8 1.4

Ammonium as NH4 mg/kg < 0.5 NONE 13.2

W/S Chloride (2:1) mg/kg < 1 MCERTS 10

Water Soluble Nitrate (2:1) as NO3 mg/kg < 3 MCERTS < 3

Arsenic (As) mg/kg < 2 MCERTS 6 4 7

W/S Boron mg/kg < 1 NONE 1.4 1.1 < 1

Cadmium (Cd) mg/kg < 0.5 MCERTS < 0.5 < 0.5 2.4

Chromium (Cr) mg/kg < 2 MCERTS 48 35 29

Chromium (hexavalent) mg/kg < 2 NONE < 2 < 2 < 2

Copper (Cu) mg/kg < 4 MCERTS 32 27 45

Lead (Pb) mg/kg < 3 MCERTS 27 63 74

W/S Magnesium g/l < 0.0001 NONE 0.0331

Mercury (Hg) mg/kg < 1 NONE < 1 < 1 < 1

Nickel (Ni) mg/kg < 3 MCERTS 21 31 43

Selenium (Se) mg/kg < 3 NONE < 3 < 3 < 3

Zinc (Zn) mg/kg < 3 MCERTS 102 136 123

Total Phenols (monohydric) mg/kg < 2 NONE < 2 < 2 < 2

EPH (C10 - C40) mg/kg < 6 MCERTS < 6

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

This report refers to samples as received, and QTS Environmental Ltd, takes no responsibility for the accuracy or competence of sampling by others.

The material description shall be regarded as tentative and is not included in our scope of UKAS Accreditation.

Opinions and interpretations expressed herein are outside the scope of UKAS Accreditation.

Asbestos Analyst: Graham Revell

RL: Reporting Limit

Pinch Test: Where pinch test is positive it is reported “Loose Fibres - PT” with type(s).

Subcontracted analysis (S)

Analysis carried out on the dried sample is corrected for the stone content

The samples have been examined to identify the presence of asbestiform minerals by polarising light microscopy and dispersion staining technique to In-House Procedures QTSE600 Determination of Asbestos in Bulk

Materials; Asbestos in Soils/Sediments (fibre screening and identification)

Site Reference: K & N Distribution Depot, Derby TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: 1309 Depth (m)

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate

QTS Environmental Report No: 14-25663 Date Sampled

Lustre Consulting Ltd Time Sampled

QTS Environmental Ltd '

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Reporting Date: 22/10/2014 QTSE Sample No

QTS Environmental Ltd - Registered in England No 06620874 Page 5 of 28

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06/09/14 06/09/14 06/09/14 07/09/14 07/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

WS504 WS504 WS504 WS505 WS506

None Supplied None Supplied None Supplied None Supplied None Supplied

0.35 - 0.45 0.70 - 1.00 1.60 - 1.80 0.30 - 0.50 0.60 - 0.70

121807 121808 121809 121810 121811

Determinand Unit RL Accreditation

Asbestos Screen N/a N/a ISO17025 Not Detected Not Detected Not Detected Not Detected

pH pH Units N/a MCERTS 7.9 7.8

Total Cyanide mg/kg < 2 NONE < 2 < 2

Total Sulphate as SO4 mg/kg < 200 NONE

W/S Sulphate as SO4 (2:1) g/l < 0.01 MCERTS 0.05 2.24

Total Sulphur mg/kg < 200 NONE

Total Organic Carbon (TOC) % < 0.1 NONE < 0.1 0.8

Ammonium as NH4 mg/kg < 0.5 NONE

W/S Chloride (2:1) mg/kg < 1 MCERTS

Water Soluble Nitrate (2:1) as NO3 mg/kg < 3 MCERTS

Arsenic (As) mg/kg < 2 MCERTS 3 23

W/S Boron mg/kg < 1 NONE < 1 1.1

Cadmium (Cd) mg/kg < 0.5 MCERTS < 0.5 0.6

Chromium (Cr) mg/kg < 2 MCERTS 28 26

Chromium (hexavalent) mg/kg < 2 NONE < 2 < 2

Copper (Cu) mg/kg < 4 MCERTS 6 49

Lead (Pb) mg/kg < 3 MCERTS 10 46

W/S Magnesium g/l < 0.0001 NONE

Mercury (Hg) mg/kg < 1 NONE < 1 < 1

Nickel (Ni) mg/kg < 3 MCERTS 26 42

Selenium (Se) mg/kg < 3 NONE < 3 < 3

Zinc (Zn) mg/kg < 3 MCERTS 67 78

Total Phenols (monohydric) mg/kg < 2 NONE < 2 < 2

EPH (C10 - C40) mg/kg < 6 MCERTS < 6

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

This report refers to samples as received, and QTS Environmental Ltd, takes no responsibility for the accuracy or competence of sampling by others.

The material description shall be regarded as tentative and is not included in our scope of UKAS Accreditation.

Opinions and interpretations expressed herein are outside the scope of UKAS Accreditation.

Asbestos Analyst: Graham Revell

RL: Reporting Limit

Pinch Test: Where pinch test is positive it is reported “Loose Fibres - PT” with type(s).

Subcontracted analysis (S)

Analysis carried out on the dried sample is corrected for the stone content

The samples have been examined to identify the presence of asbestiform minerals by polarising light microscopy and dispersion staining technique to In-House Procedures QTSE600 Determination of Asbestos in Bulk

Materials; Asbestos in Soils/Sediments (fibre screening and identification)

Site Reference: K & N Distribution Depot, Derby TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: 1309 Depth (m)

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate

QTS Environmental Report No: 14-25663 Date Sampled

Lustre Consulting Ltd Time Sampled

QTS Environmental Ltd '

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Reporting Date: 22/10/2014 QTSE Sample No

QTS Environmental Ltd - Registered in England No 06620874 Page 6 of 28

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07/09/14 07/09/14 07/09/14 07/09/14 07/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

WS507 WS507 WS507 WS508 WS509

None Supplied None Supplied None Supplied None Supplied None Supplied

0.20 - 0.50 0.80 - 0.90 1.20 - 1.30 0.50 - 0.60 0.50 - 0.80

121812 121813 121814 121816 121817

Determinand Unit RL Accreditation

Asbestos Screen N/a N/a ISO17025 Not Detected Not Detected Not Detected Not Detected

pH pH Units N/a MCERTS 8.4 8.3 8.2 8.0

Total Cyanide mg/kg < 2 NONE < 2 < 2 < 2

Total Sulphate as SO4 mg/kg < 200 NONE 682

W/S Sulphate as SO4 (2:1) g/l < 0.01 MCERTS 0.55 0.07 0.07 0.07

Total Sulphur mg/kg < 200 NONE 241

Total Organic Carbon (TOC) % < 0.1 NONE 0.2 0.3 0.4

Ammonium as NH4 mg/kg < 0.5 NONE 5.2

W/S Chloride (2:1) mg/kg < 1 MCERTS 8

Water Soluble Nitrate (2:1) as NO3 mg/kg < 3 MCERTS 4

Arsenic (As) mg/kg < 2 MCERTS 6 12 3

W/S Boron mg/kg < 1 NONE < 1 < 1 < 1

Cadmium (Cd) mg/kg < 0.5 MCERTS < 0.5 < 0.5 < 0.5

Chromium (Cr) mg/kg < 2 MCERTS 26 23 34

Chromium (hexavalent) mg/kg < 2 NONE < 2 < 2 < 2

Copper (Cu) mg/kg < 4 MCERTS 8 31 10

Lead (Pb) mg/kg < 3 MCERTS 9 31 11

W/S Magnesium g/l < 0.0001 NONE 0.0222

Mercury (Hg) mg/kg < 1 NONE < 1 < 1 < 1

Nickel (Ni) mg/kg < 3 MCERTS 26 34 32

Selenium (Se) mg/kg < 3 NONE < 3 < 3 < 3

Zinc (Zn) mg/kg < 3 MCERTS 45 73 78

Total Phenols (monohydric) mg/kg < 2 NONE < 2 < 2 < 2

EPH (C10 - C40) mg/kg < 6 MCERTS

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

This report refers to samples as received, and QTS Environmental Ltd, takes no responsibility for the accuracy or competence of sampling by others.

The material description shall be regarded as tentative and is not included in our scope of UKAS Accreditation.

Opinions and interpretations expressed herein are outside the scope of UKAS Accreditation.

Asbestos Analyst: Graham Revell

RL: Reporting Limit

Pinch Test: Where pinch test is positive it is reported “Loose Fibres - PT” with type(s).

Subcontracted analysis (S)

The samples have been examined to identify the presence of asbestiform minerals by polarising light microscopy and dispersion staining technique to In-House Procedures QTSE600 Determination of Asbestos in Bulk

Materials; Asbestos in Soils/Sediments (fibre screening and identification)

Site Reference: K & N Distribution Depot, Derby TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: 1309 Depth (m)

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate

QTS Environmental Report No: 14-25663 Date Sampled

Lustre Consulting Ltd Time Sampled

QTS Environmental Ltd '

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Reporting Date: 22/10/2014 QTSE Sample No

Analysis carried out on the dried sample is corrected for the stone content

QTS Environmental Ltd - Registered in England No 06620874 Page 7 of 28

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07/09/14 07/09/14 07/09/14 07/09/14 08/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

WS510 WS510 WS511 WS511 WS513

None Supplied None Supplied None Supplied None Supplied None Supplied

0.06 - 0.14 0.14 - 0.20 0.45 - 0.55 0.60 - 0.80 0.30 - 0.40

121818 121819 121820 121821 121823

Determinand Unit RL Accreditation

Asbestos Screen N/a N/a ISO17025 Not Detected Not Detected Not Detected Not Detected

pH pH Units N/a MCERTS 7.7 7.7 7.7

Total Cyanide mg/kg < 2 NONE < 2 < 2 < 2

Total Sulphate as SO4 mg/kg < 200 NONE

W/S Sulphate as SO4 (2:1) g/l < 0.01 MCERTS 0.19 0.11 1.13

Total Sulphur mg/kg < 200 NONE

Total Organic Carbon (TOC) % < 0.1 NONE 1.6 1.1 2.7

Ammonium as NH4 mg/kg < 0.5 NONE

W/S Chloride (2:1) mg/kg < 1 MCERTS

Water Soluble Nitrate (2:1) as NO3 mg/kg < 3 MCERTS

Arsenic (As) mg/kg < 2 MCERTS 5 22 8

W/S Boron mg/kg < 1 NONE < 1 < 1 < 1

Cadmium (Cd) mg/kg < 0.5 MCERTS 1.6 1 0.8

Chromium (Cr) mg/kg < 2 MCERTS 19 19 22

Chromium (hexavalent) mg/kg < 2 NONE < 2 < 2 < 2

Copper (Cu) mg/kg < 4 MCERTS 35 29 42

Lead (Pb) mg/kg < 3 MCERTS 48 101 37

W/S Magnesium g/l < 0.0001 NONE

Mercury (Hg) mg/kg < 1 NONE < 1 < 1 < 1

Nickel (Ni) mg/kg < 3 MCERTS 27 27 35

Selenium (Se) mg/kg < 3 NONE < 3 < 3 < 3

Zinc (Zn) mg/kg < 3 MCERTS 184 60 56

Total Phenols (monohydric) mg/kg < 2 NONE < 2 < 2 < 2

EPH (C10 - C40) mg/kg < 6 MCERTS < 6 26

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

This report refers to samples as received, and QTS Environmental Ltd, takes no responsibility for the accuracy or competence of sampling by others.

The material description shall be regarded as tentative and is not included in our scope of UKAS Accreditation.

Opinions and interpretations expressed herein are outside the scope of UKAS Accreditation.

Asbestos Analyst: Graham Revell

RL: Reporting Limit

Pinch Test: Where pinch test is positive it is reported “Loose Fibres - PT” with type(s).

Subcontracted analysis (S)

Reporting Date: 22/10/2014 QTSE Sample No

Site Reference: K & N Distribution Depot, Derby TP / BH No

Project / Job Ref: 1309 Additional Refs

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate

QTS Environmental Report No: 14-25663 Date Sampled

Lustre Consulting Ltd Time Sampled

QTS Environmental Ltd '

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Analysis carried out on the dried sample is corrected for the stone content

The samples have been examined to identify the presence of asbestiform minerals by polarising light microscopy and dispersion staining technique to In-House Procedures QTSE600 Determination of Asbestos in Bulk

Materials; Asbestos in Soils/Sediments (fibre screening and identification)

Order No: 1309 Depth (m)

QTS Environmental Ltd - Registered in England No 06620874 Page 8 of 28

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08/09/14 08/09/14 08/09/14 08/09/14 08/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

WS513 WS514 WS515 WS515 WS515

None Supplied None Supplied None Supplied None Supplied None Supplied

3.60 - 3.70 0.10 - 0.50 0.30 - 0.60 0.90 - 1.00 1.00 - 1.30

121824 121825 121826 121827 121828

Determinand Unit RL Accreditation

Asbestos Screen N/a N/a ISO17025 Not Detected Not Detected Not Detected

pH pH Units N/a MCERTS 7.8 8.1 7.9 7.2 7.1

Total Cyanide mg/kg < 2 NONE < 2 < 2 < 2

Total Sulphate as SO4 mg/kg < 200 NONE 881 1803

W/S Sulphate as SO4 (2:1) g/l < 0.01 MCERTS 0.15 0.45 0.34 0.25 0.16

Total Sulphur mg/kg < 200 NONE 299 832

Total Organic Carbon (TOC) % < 0.1 NONE 0.9 1 1.2

Ammonium as NH4 mg/kg < 0.5 NONE 3.5 51

W/S Chloride (2:1) mg/kg < 1 MCERTS 9 9

Water Soluble Nitrate (2:1) as NO3 mg/kg < 3 MCERTS < 3 5

Arsenic (As) mg/kg < 2 MCERTS 7 7 < 2

W/S Boron mg/kg < 1 NONE 1.7 1.5 1.5

Cadmium (Cd) mg/kg < 0.5 MCERTS 1.2 0.9 < 0.5

Chromium (Cr) mg/kg < 2 MCERTS 17 14 31

Chromium (hexavalent) mg/kg < 2 NONE < 2 < 2 < 2

Copper (Cu) mg/kg < 4 MCERTS 31 37 20

Lead (Pb) mg/kg < 3 MCERTS 75 106 26

W/S Magnesium g/l < 0.0001 NONE 0.0120 0.0267

Mercury (Hg) mg/kg < 1 NONE < 1 < 1 < 1

Nickel (Ni) mg/kg < 3 MCERTS 15 17 30

Selenium (Se) mg/kg < 3 NONE < 3 < 3 < 3

Zinc (Zn) mg/kg < 3 MCERTS 347 276 87

Total Phenols (monohydric) mg/kg < 2 NONE < 2 < 2 < 2

EPH (C10 - C40) mg/kg < 6 MCERTS

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

This report refers to samples as received, and QTS Environmental Ltd, takes no responsibility for the accuracy or competence of sampling by others.

The material description shall be regarded as tentative and is not included in our scope of UKAS Accreditation.

Opinions and interpretations expressed herein are outside the scope of UKAS Accreditation.

Asbestos Analyst: Graham Revell

RL: Reporting Limit

Pinch Test: Where pinch test is positive it is reported “Loose Fibres - PT” with type(s).

Subcontracted analysis (S)

Reporting Date: 22/10/2014 QTSE Sample No

Analysis carried out on the dried sample is corrected for the stone content

The samples have been examined to identify the presence of asbestiform minerals by polarising light microscopy and dispersion staining technique to In-House Procedures QTSE600 Determination of Asbestos in Bulk

Materials; Asbestos in Soils/Sediments (fibre screening and identification)

Site Reference: K & N Distribution Depot, Derby TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: 1309 Depth (m)

QTS Environmental Ltd '

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate

QTS Environmental Report No: 14-25663 Date Sampled

Lustre Consulting Ltd Time Sampled

QTS Environmental Ltd - Registered in England No 06620874 Page 9 of 28

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10/09/14 09/09/14 10/09/14 10/09/14 10/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

SP1 TP1 TP3 TP4 TP5

None Supplied None Supplied None Supplied None Supplied None Supplied

0.50 0.30 - 0.50 0.05 0.20 0.50 & BB

121787 121788 121790 121792 121793

Determinand Unit RL Accreditation

Naphthalene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Acenaphthylene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Acenaphthene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Fluorene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Phenanthrene mg/kg < 0.1 MCERTS < 0.1 0.12 < 0.1 0.31 < 0.1

Anthracene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Fluoranthene mg/kg < 0.1 MCERTS < 0.1 0.37 0.18 0.56 < 0.1

Pyrene mg/kg < 0.1 MCERTS < 0.1 0.33 0.16 0.46 < 0.1

Benzo(a)anthracene mg/kg < 0.1 MCERTS < 0.1 0.12 < 0.1 0.20 < 0.1

Chrysene mg/kg < 0.1 MCERTS < 0.1 0.18 < 0.1 0.26 < 0.1

Benzo(b)fluoranthene mg/kg < 0.1 MCERTS < 0.1 0.16 < 0.1 0.28 < 0.1

Benzo(k)fluoranthene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 0.12 < 0.1

Benzo(a)pyrene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 0.19 < 0.1

Indeno(1,2,3-cd)pyrene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 0.13 < 0.1

Dibenz(a,h)anthracene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Benzo(ghi)perylene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 0.12 < 0.1

Total EPA-16 PAHs mg/kg < 1.6 MCERTS < 1.6 < 1.6 < 1.6 2.6 < 1.6

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

Lustre Consulting Ltd Time Sampled

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Reporting Date: 22/10/2014 QTSE Sample No

Site Reference: K & N Distribution Depot,

Derby

TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: 1309 Depth (m)

Tel : 01622 850410 '

Soil Analysis Certificate - Speciated PAHs

QTS Environmental Report No: 14-25663 Date Sampled

QTS Environmental Ltd - Registered in England No 06620874 Page 10 of 28

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09/09/14 09/09/14 09/09/14 09/09/14 09/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

TP9 TP10 TP11 TP12 TP15

None Supplied None Supplied None Supplied None Supplied None Supplied

0.20 0.10 - 0.30 0.30 0.10 - 0.20 0.60 - 0.70

121795 121796 121797 121798 121799

Determinand Unit RL Accreditation

Naphthalene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Acenaphthylene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Acenaphthene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Fluorene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Phenanthrene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 0.11 < 0.1

Anthracene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Fluoranthene mg/kg < 0.1 MCERTS 0.19 < 0.1 < 0.1 0.56 < 0.1

Pyrene mg/kg < 0.1 MCERTS 0.16 < 0.1 < 0.1 0.49 < 0.1

Benzo(a)anthracene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 0.24 < 0.1

Chrysene mg/kg < 0.1 MCERTS 0.11 < 0.1 < 0.1 0.27 < 0.1

Benzo(b)fluoranthene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 0.25 < 0.1

Benzo(k)fluoranthene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 0.11 < 0.1

Benzo(a)pyrene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 0.21 < 0.1

Indeno(1,2,3-cd)pyrene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Dibenz(a,h)anthracene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Benzo(ghi)perylene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 0.11 < 0.1

Total EPA-16 PAHs mg/kg < 1.6 MCERTS < 1.6 < 1.6 < 1.6 2.4 < 1.6

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

Project / Job Ref: 1309 Additional Refs

Order No: 1309 Depth (m)

Reporting Date: 22/10/2014 QTSE Sample No

Soil Analysis Certificate - Speciated PAHs

QTS Environmental Report No: 14-25663 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: K & N Distribution Depot,

Derby

TP / BH No

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

QTS Environmental Ltd - Registered in England No 06620874 Page 11 of 28

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09/09/14 09/09/14 06/09/14 06/09/14 06/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

TP16 TP17 WS502 WS503 WS504

None Supplied None Supplied None Supplied None Supplied None Supplied

0.20 - 0.30 0.10 0.30 - 0.40 0.60 - 0.70 1.60 - 1.80

121801 121802 121805 121806 121809

Determinand Unit RL Accreditation

Naphthalene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Acenaphthylene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Acenaphthene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Fluorene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Phenanthrene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 0.15 < 0.1

Anthracene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Fluoranthene mg/kg < 0.1 MCERTS < 0.1 0.16 < 0.1 0.31 < 0.1

Pyrene mg/kg < 0.1 MCERTS < 0.1 0.15 < 0.1 0.27 < 0.1

Benzo(a)anthracene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Chrysene mg/kg < 0.1 MCERTS < 0.1 0.13 < 0.1 0.13 < 0.1

Benzo(b)fluoranthene mg/kg < 0.1 MCERTS < 0.1 0.12 < 0.1 < 0.1 < 0.1

Benzo(k)fluoranthene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Benzo(a)pyrene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Indeno(1,2,3-cd)pyrene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Dibenz(a,h)anthracene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Benzo(ghi)perylene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Total EPA-16 PAHs mg/kg < 1.6 MCERTS < 1.6 < 1.6 < 1.6 < 1.6 < 1.6

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: K & N Distribution Depot,

Derby

TP / BH No

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate - Speciated PAHs

QTS Environmental Report No: 14-25663

Order No: 1309 Depth (m)

Reporting Date: 22/10/2014 QTSE Sample No

Project / Job Ref: 1309 Additional Refs

QTS Environmental Ltd - Registered in England No 06620874 Page 12 of 28

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07/09/14 07/09/14 07/09/14 07/09/14 07/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

WS506 WS507 WS508 WS509 WS510

None Supplied None Supplied None Supplied None Supplied None Supplied

0.60 - 0.70 0.80 - 0.90 0.50 - 0.60 0.50 - 0.80 0.14 - 0.20

121811 121813 121816 121817 121819

Determinand Unit RL Accreditation

Naphthalene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Acenaphthylene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Acenaphthene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Fluorene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Phenanthrene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Anthracene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Fluoranthene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Pyrene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Benzo(a)anthracene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Chrysene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Benzo(b)fluoranthene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Benzo(k)fluoranthene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Benzo(a)pyrene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Indeno(1,2,3-cd)pyrene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Dibenz(a,h)anthracene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Benzo(ghi)perylene mg/kg < 0.1 MCERTS < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Total EPA-16 PAHs mg/kg < 1.6 MCERTS < 1.6 < 1.6 < 1.6 < 1.6 < 1.6

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

Reporting Date: 22/10/2014 QTSE Sample No

Site Reference: K & N Distribution Depot,

Derby

TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: 1309 Depth (m)

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate - Speciated PAHs

QTS Environmental Report No: 14-25663 Date Sampled

Lustre Consulting Ltd Time Sampled

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

QTS Environmental Ltd - Registered in England No 06620874 Page 13 of 28

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07/09/14 08/09/14 08/09/14 08/09/14 08/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

WS511 WS513 WS514 WS515 WS515

None Supplied None Supplied None Supplied None Supplied None Supplied

0.45 - 0.55 0.30 - 0.40 0.10 - 0.50 0.30 - 0.60 0.90 - 1.00

121820 121823 121825 121826 121827

Determinand Unit RL Accreditation

Naphthalene mg/kg < 0.1 MCERTS 0.40 < 0.1 < 0.1 < 0.1 < 0.1

Acenaphthylene mg/kg < 0.1 MCERTS 0.27 < 0.1 < 0.1 < 0.1 < 0.1

Acenaphthene mg/kg < 0.1 MCERTS 0.50 < 0.1 < 0.1 < 0.1 < 0.1

Fluorene mg/kg < 0.1 MCERTS 2.99 < 0.1 < 0.1 < 0.1 < 0.1

Phenanthrene mg/kg < 0.1 MCERTS 3.41 1.90 < 0.1 0.55 < 0.1

Anthracene mg/kg < 0.1 MCERTS 0.31 0.16 < 0.1 0.11 < 0.1

Fluoranthene mg/kg < 0.1 MCERTS 0.18 5.70 < 0.1 0.46 < 0.1

Pyrene mg/kg < 0.1 MCERTS 0.60 4.41 < 0.1 0.52 < 0.1

Benzo(a)anthracene mg/kg < 0.1 MCERTS < 0.1 2.55 < 0.1 0.46 < 0.1

Chrysene mg/kg < 0.1 MCERTS < 0.1 3.48 < 0.1 0.42 < 0.1

Benzo(b)fluoranthene mg/kg < 0.1 MCERTS < 0.1 4.19 0.15 0.31 < 0.1

Benzo(k)fluoranthene mg/kg < 0.1 MCERTS < 0.1 1.51 < 0.1 < 0.1 < 0.1

Benzo(a)pyrene mg/kg < 0.1 MCERTS < 0.1 2.51 < 0.1 0.21 < 0.1

Indeno(1,2,3-cd)pyrene mg/kg < 0.1 MCERTS < 0.1 1.62 < 0.1 < 0.1 < 0.1

Dibenz(a,h)anthracene mg/kg < 0.1 MCERTS < 0.1 0.33 < 0.1 < 0.1 < 0.1

Benzo(ghi)perylene mg/kg < 0.1 MCERTS < 0.1 1.29 < 0.1 0.17 < 0.1

Total EPA-16 PAHs mg/kg < 1.6 MCERTS 8.7 29.7 < 1.6 3.2 < 1.6

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

Project / Job Ref: 1309 Additional Refs

Order No: 1309 Depth (m)

Reporting Date: 22/10/2014 QTSE Sample No

Soil Analysis Certificate - Speciated PAHs

QTS Environmental Report No: 14-25663 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: K & N Distribution Depot,

Derby

TP / BH No

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

QTS Environmental Ltd - Registered in England No 06620874 Page 14 of 28

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10/09/14 09/09/14 10/09/14 10/09/14 10/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

SP1 TP1 TP3 TP4 TP5

None Supplied None Supplied None Supplied None Supplied None Supplied

0.50 0.30 - 0.50 0.05 0.20 0.50 & BB

121787 121788 121790 121792 121793

Determinand Unit RL Accreditation

Aliphatic >C5 - C6 mg/kg < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Aliphatic >C6 - C8 mg/kg < 0.05 NONE < 0.05 < 0.05 < 0.05 < 0.05 < 0.05

Aliphatic >C8 - C10 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aliphatic >C10 - C12 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aliphatic >C12 - C16 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aliphatic >C16 - C21 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aliphatic >C21 - C34 mg/kg < 6 NONE < 6 < 6 < 6 < 6 < 6

Aliphatic (C5 - C34) mg/kg < 12 NONE < 12 < 12 < 12 < 12 < 12

Aromatic >C5 - C7 mg/kg < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Aromatic >C7 - C8 mg/kg < 0.05 NONE < 0.05 < 0.05 < 0.05 < 0.05 < 0.05

Aromatic >C8 - C10 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aromatic >C10 - C12 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aromatic >C12 - C16 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aromatic >C16 - C21 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aromatic >C21 - C35 mg/kg < 6 NONE < 6 < 6 < 6 < 6 < 6

Aromatic (C5 - C35) mg/kg < 12 NONE < 12 < 12 < 12 < 12 < 12

Total >C5 - C35 mg/kg < 24 NONE < 24 < 24 < 24 < 24 < 24

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

Lustre Consulting Ltd Time Sampled

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Reporting Date: 22/10/2014 QTSE Sample No

Site Reference: K & N Distribution Depot,

Derby

TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: 1309 Depth (m)

Tel : 01622 850410 '

Soil Analysis Certificate - TPH CWG Banded

QTS Environmental Report No: 14-25663 Date Sampled

QTS Environmental Ltd - Registered in England No 06620874 Page 15 of 28

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09/09/14 09/09/14 09/09/14 09/09/14 09/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

TP9 TP10 TP11 TP12 TP15

None Supplied None Supplied None Supplied None Supplied None Supplied

0.20 0.10 - 0.30 0.30 0.10 - 0.20 0.60 - 0.70

121795 121796 121797 121798 121799

Determinand Unit RL Accreditation

Aliphatic >C5 - C6 mg/kg < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Aliphatic >C6 - C8 mg/kg < 0.05 NONE < 0.05 < 0.05 < 0.05 < 0.05 < 0.05

Aliphatic >C8 - C10 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aliphatic >C10 - C12 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aliphatic >C12 - C16 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aliphatic >C16 - C21 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aliphatic >C21 - C34 mg/kg < 6 NONE < 6 < 6 < 6 < 6 < 6

Aliphatic (C5 - C34) mg/kg < 12 NONE < 12 < 12 < 12 < 12 < 12

Aromatic >C5 - C7 mg/kg < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Aromatic >C7 - C8 mg/kg < 0.05 NONE < 0.05 < 0.05 < 0.05 < 0.05 < 0.05

Aromatic >C8 - C10 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aromatic >C10 - C12 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aromatic >C12 - C16 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aromatic >C16 - C21 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aromatic >C21 - C35 mg/kg < 6 NONE < 6 < 6 < 6 < 6 < 6

Aromatic (C5 - C35) mg/kg < 12 NONE < 12 < 12 < 12 < 12 < 12

Total >C5 - C35 mg/kg < 24 NONE < 24 < 24 < 24 < 24 < 24

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

Project / Job Ref: 1309 Additional Refs

Order No: 1309 Depth (m)

Reporting Date: 22/10/2014 QTSE Sample No

Soil Analysis Certificate - TPH CWG Banded

QTS Environmental Report No: 14-25663 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: K & N Distribution Depot,

Derby

TP / BH No

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

QTS Environmental Ltd - Registered in England No 06620874 Page 16 of 28

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09/09/14 09/09/14 06/09/14 06/09/14 06/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

TP16 TP17 WS502 WS503 WS504

None Supplied None Supplied None Supplied None Supplied None Supplied

0.20 - 0.30 0.10 0.30 - 0.40 0.60 - 0.70 1.60 - 1.80

121801 121802 121805 121806 121809

Determinand Unit RL Accreditation

Aliphatic >C5 - C6 mg/kg < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Aliphatic >C6 - C8 mg/kg < 0.05 NONE < 0.05 < 0.05 < 0.05 < 0.05 < 0.05

Aliphatic >C8 - C10 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aliphatic >C10 - C12 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aliphatic >C12 - C16 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aliphatic >C16 - C21 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aliphatic >C21 - C34 mg/kg < 6 NONE < 6 < 6 < 6 < 6 < 6

Aliphatic (C5 - C34) mg/kg < 12 NONE < 12 < 12 < 12 < 12 < 12

Aromatic >C5 - C7 mg/kg < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Aromatic >C7 - C8 mg/kg < 0.05 NONE < 0.05 < 0.05 < 0.05 < 0.05 < 0.05

Aromatic >C8 - C10 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aromatic >C10 - C12 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aromatic >C12 - C16 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aromatic >C16 - C21 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aromatic >C21 - C35 mg/kg < 6 NONE < 6 < 6 < 6 < 6 < 6

Aromatic (C5 - C35) mg/kg < 12 NONE < 12 < 12 < 12 < 12 < 12

Total >C5 - C35 mg/kg < 24 NONE < 24 < 24 < 24 < 24 < 24

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: K & N Distribution Depot,

Derby

TP / BH No

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate - TPH CWG Banded

QTS Environmental Report No: 14-25663

Order No: 1309 Depth (m)

Reporting Date: 22/10/2014 QTSE Sample No

Project / Job Ref: 1309 Additional Refs

QTS Environmental Ltd - Registered in England No 06620874 Page 17 of 28

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07/09/14 07/09/14 07/09/14 07/09/14 07/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

WS506 WS507 WS508 WS509 WS510

None Supplied None Supplied None Supplied None Supplied None Supplied

0.60 - 0.70 0.80 - 0.90 0.50 - 0.60 0.50 - 0.80 0.14 - 0.20

121811 121813 121816 121817 121819

Determinand Unit RL Accreditation

Aliphatic >C5 - C6 mg/kg < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Aliphatic >C6 - C8 mg/kg < 0.05 NONE < 0.05 < 0.05 < 0.05 < 0.05 < 0.05

Aliphatic >C8 - C10 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aliphatic >C10 - C12 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aliphatic >C12 - C16 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aliphatic >C16 - C21 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aliphatic >C21 - C34 mg/kg < 6 NONE < 6 < 6 < 6 < 6 < 6

Aliphatic (C5 - C34) mg/kg < 12 NONE < 12 < 12 < 12 < 12 < 12

Aromatic >C5 - C7 mg/kg < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Aromatic >C7 - C8 mg/kg < 0.05 NONE < 0.05 < 0.05 < 0.05 < 0.05 < 0.05

Aromatic >C8 - C10 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aromatic >C10 - C12 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aromatic >C12 - C16 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aromatic >C16 - C21 mg/kg < 1 NONE < 1 < 1 < 1 < 1 < 1

Aromatic >C21 - C35 mg/kg < 6 NONE < 6 < 6 < 6 < 6 < 6

Aromatic (C5 - C35) mg/kg < 12 NONE < 12 < 12 < 12 < 12 < 12

Total >C5 - C35 mg/kg < 24 NONE < 24 < 24 < 24 < 24 < 24

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

Reporting Date: 22/10/2014 QTSE Sample No

Site Reference: K & N Distribution Depot,

Derby

TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: 1309 Depth (m)

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate - TPH CWG Banded

QTS Environmental Report No: 14-25663 Date Sampled

Lustre Consulting Ltd Time Sampled

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

QTS Environmental Ltd - Registered in England No 06620874 Page 18 of 28

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07/09/14 08/09/14 08/09/14 08/09/14 08/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

WS511 WS513 WS514 WS515 WS515

None Supplied None Supplied None Supplied None Supplied None Supplied

0.45 - 0.55 0.30 - 0.40 0.10 - 0.50 0.30 - 0.60 0.90 - 1.00

121820 121823 121825 121826 121827

Determinand Unit RL Accreditation

Aliphatic >C5 - C6 mg/kg < 0.01 NONE 0.06 < 0.01 < 0.01 < 0.01 < 0.01

Aliphatic >C6 - C8 mg/kg < 0.05 NONE 8.90 0.28 < 0.05 < 0.05 < 0.05

Aliphatic >C8 - C10 mg/kg < 1 NONE 105 3 < 1 < 1 < 1

Aliphatic >C10 - C12 mg/kg < 1 NONE 302 < 1 < 1 < 1 < 1

Aliphatic >C12 - C16 mg/kg < 1 NONE 1626 < 1 < 1 8 < 1

Aliphatic >C16 - C21 mg/kg < 1 NONE 1850 < 1 < 1 12 < 1

Aliphatic >C21 - C34 mg/kg < 6 NONE 560 < 6 < 6 41 < 6

Aliphatic (C5 - C34) mg/kg < 12 NONE 4453 < 12 < 12 61 < 12

Aromatic >C5 - C7 mg/kg < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Aromatic >C7 - C8 mg/kg < 0.05 NONE < 0.05 < 0.05 < 0.05 < 0.05 < 0.05

Aromatic >C8 - C10 mg/kg < 1 NONE 10 < 1 < 1 < 1 < 1

Aromatic >C10 - C12 mg/kg < 1 NONE 130 < 1 < 1 < 1 < 1

Aromatic >C12 - C16 mg/kg < 1 NONE 1134 1 < 1 2 < 1

Aromatic >C16 - C21 mg/kg < 1 NONE 1270 19 < 1 10 < 1

Aromatic >C21 - C35 mg/kg < 6 NONE 423 79 < 6 31 < 6

Aromatic (C5 - C35) mg/kg < 12 NONE 2967 100 < 12 43 < 12

Total >C5 - C35 mg/kg < 24 NONE 7420 104 < 24 104 < 24

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

Project / Job Ref: 1309 Additional Refs

Order No: 1309 Depth (m)

Reporting Date: 22/10/2014 QTSE Sample No

Soil Analysis Certificate - TPH CWG Banded

QTS Environmental Report No: 14-25663 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: K & N Distribution Depot,

Derby

TP / BH No

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

QTS Environmental Ltd - Registered in England No 06620874 Page 19 of 28

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10/09/14 09/09/14 10/09/14 10/09/14 10/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

SP1 TP1 TP3 TP4 TP5

None Supplied None Supplied None Supplied None Supplied None Supplied

0.50 0.30 - 0.50 0.05 0.20 0.50 & BB

121787 121788 121790 121792 121793

Determinand Unit RL Accreditation

Benzene ug/kg < 2 MCERTS < 2 < 2 < 2 < 2 < 2

Toluene ug/kg < 5 MCERTS < 5 7 < 5 < 5 < 5

Ethylbenzene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

p & m-xylene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

o-xylene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

MTBE ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

Lustre Consulting Ltd Time Sampled

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Reporting Date: 22/10/2014 QTSE Sample No

Site Reference: K & N Distribution Depot,

Derby

TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: 1309 Depth (m)

Tel : 01622 850410 '

Soil Analysis Certificate - BTEX / MTBE

QTS Environmental Report No: 14-25663 Date Sampled

QTS Environmental Ltd - Registered in England No 06620874 Page 20 of 28

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09/09/14 09/09/14 09/09/14 09/09/14 09/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

TP9 TP10 TP11 TP12 TP15

None Supplied None Supplied None Supplied None Supplied None Supplied

0.20 0.10 - 0.30 0.30 0.10 - 0.20 0.60 - 0.70

121795 121796 121797 121798 121799

Determinand Unit RL Accreditation

Benzene ug/kg < 2 MCERTS < 2 < 2 < 2 < 2 < 2

Toluene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Ethylbenzene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

p & m-xylene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

o-xylene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

MTBE ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

Project / Job Ref: 1309 Additional Refs

Order No: 1309 Depth (m)

Reporting Date: 22/10/2014 QTSE Sample No

Soil Analysis Certificate - BTEX / MTBE

QTS Environmental Report No: 14-25663 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: K & N Distribution Depot,

Derby

TP / BH No

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

QTS Environmental Ltd - Registered in England No 06620874 Page 21 of 28

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09/09/14 09/09/14 06/09/14 06/09/14 06/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

TP16 TP17 WS502 WS503 WS504

None Supplied None Supplied None Supplied None Supplied None Supplied

0.20 - 0.30 0.10 0.30 - 0.40 0.60 - 0.70 1.60 - 1.80

121801 121802 121805 121806 121809

Determinand Unit RL Accreditation

Benzene ug/kg < 2 MCERTS < 2 < 2 < 2 < 2 < 2

Toluene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Ethylbenzene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

p & m-xylene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

o-xylene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

MTBE ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: K & N Distribution Depot,

Derby

TP / BH No

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate - BTEX / MTBE

QTS Environmental Report No: 14-25663

Order No: 1309 Depth (m)

Reporting Date: 22/10/2014 QTSE Sample No

Project / Job Ref: 1309 Additional Refs

QTS Environmental Ltd - Registered in England No 06620874 Page 22 of 28

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07/09/14 07/09/14 07/09/14 07/09/14 07/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

WS506 WS507 WS508 WS509 WS510

None Supplied None Supplied None Supplied None Supplied None Supplied

0.60 - 0.70 0.80 - 0.90 0.50 - 0.60 0.50 - 0.80 0.14 - 0.20

121811 121813 121816 121817 121819

Determinand Unit RL Accreditation

Benzene ug/kg < 2 MCERTS < 2 < 2 < 2 < 2 < 2

Toluene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Ethylbenzene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

p & m-xylene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

o-xylene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

MTBE ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

Reporting Date: 22/10/2014 QTSE Sample No

Site Reference: K & N Distribution Depot,

Derby

TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: 1309 Depth (m)

Kent ME17 2JN

Tel : 01622 850410 '

Soil Analysis Certificate - BTEX / MTBE

QTS Environmental Report No: 14-25663 Date Sampled

Lustre Consulting Ltd Time Sampled

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

QTS Environmental Ltd - Registered in England No 06620874 Page 23 of 28

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07/09/14 08/09/14 08/09/14 08/09/14 08/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

WS511 WS513 WS514 WS515 WS515

None Supplied None Supplied None Supplied None Supplied None Supplied

0.45 - 0.55 0.30 - 0.40 0.10 - 0.50 0.30 - 0.60 0.90 - 1.00

121820 121823 121825 121826 121827

Determinand Unit RL Accreditation

Benzene ug/kg < 2 MCERTS < 2 < 2 < 2 < 2 < 2

Toluene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Ethylbenzene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

p & m-xylene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

o-xylene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

MTBE ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

Project / Job Ref: 1309 Additional Refs

Order No: 1309 Depth (m)

Reporting Date: 22/10/2014 QTSE Sample No

Soil Analysis Certificate - BTEX / MTBE

QTS Environmental Report No: 14-25663 Date Sampled

Lustre Consulting Ltd Time Sampled

Site Reference: K & N Distribution Depot,

Derby

TP / BH No

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

QTS Environmental Ltd - Registered in England No 06620874 Page 24 of 28

Page 63: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

06/09/14 07/09/14 07/09/14 07/09/14 07/09/14

None Supplied None Supplied None Supplied None Supplied None Supplied

WS503 WS506 WS508 WS509 WS511

None Supplied None Supplied None Supplied None Supplied None Supplied

0.60 - 0.70 0.60 - 0.70 0.20 - 0.40 0.50 - 0.80 0.45 - 0.55

121806 121811 121815 121817 121820

Determinand Unit RL Accreditation

Dichlorodifluoromethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Vinyl Chloride ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Chloromethane ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

Chloroethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Bromomethane ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

Trichlorofluoromethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

1,1-Dichloroethene ug/kg < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

MTBE ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

trans-1,2-Dichloroethene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

1,1-Dichloroethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

cis-1,2-Dichloroethene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

2,2-Dichloropropane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Chloroform ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Bromochloromethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

1,1,1-Trichloroethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

1,1-Dichloropropene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

Carbon Tetrachloride ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

1,2-Dichloroethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Benzene ug/kg < 2 MCERTS < 2 < 2 < 2 < 2 < 2

1,2-Dichloropropane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Trichloroethene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Bromodichloromethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Dibromomethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

TAME ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

cis-1,3-Dichloropropene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Toluene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

trans-1,3-Dichloropropene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

1,1,2-Trichloroethane ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

1,3-Dichloropropane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Tetrachloroethene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Dibromochloromethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

1,2-Dibromoethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Chlorobenzene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

1,1,1,2-Tetrachloroethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Ethyl Benzene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

m,p-Xylene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

o-Xylene ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

Styrene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Bromoform ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

Isopropylbenzene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 87

1,1,2,2-Tetrachloroethane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

1,2,3-Trichloropropane ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

n-Propylbenzene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 143

Bromobenzene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

2-Chlorotoluene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

1,3,5-Trimethylbenzene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

4-Chlorotoluene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

tert-Butylbenzene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

1,2,4-Trimethylbenzene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 1616

sec-Butylbenzene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 168

p-Isopropyltoluene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 209

1,3-Dichlorobenzene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

1,4-Dichlorobenzene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

n-Butylbenzene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 522

1,2-Dichlorobenzene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

1,2-Dibromo-3-chloropropane ug/kg < 10 MCERTS < 10 < 10 < 10 < 10 < 10

Hexachlorobutadiene ug/kg < 5 MCERTS < 5 < 5 < 5 < 5 < 5

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

Reporting Date: 22/10/2014 QTSE Sample No

Order No: 1309 Depth (m)

Site Reference: K & N Distribution Depot,

Derby

TP / BH No

Project / Job Ref: 1309 Additional Refs

Tel : 01622 850410 '

Soil Analysis Certificate - Volatile Organic Compounds (VOC)

QTS Environmental Report No: 14-25663 Date Sampled

Lustre Consulting Ltd Time Sampled

Kent ME17 2JN

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

QTS Environmental Ltd - Registered in England No 06620874 Page 25 of 28

Page 64: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

07/09/14 08/09/14

None Supplied None Supplied

WS511 WS513

None Supplied None Supplied

0.60 - 0.80 0.30 - 0.40

121821 121823

Determinand Unit RL Accreditation

Dichlorodifluoromethane ug/kg < 5 MCERTS < 5 < 5

Vinyl Chloride ug/kg < 5 MCERTS < 5 < 5

Chloromethane ug/kg < 10 MCERTS < 10 < 10

Chloroethane ug/kg < 5 MCERTS < 5 < 5

Bromomethane ug/kg < 10 MCERTS < 10 < 10

Trichlorofluoromethane ug/kg < 5 MCERTS < 5 < 5

1,1-Dichloroethene ug/kg < 5 ISO17025 < 5 < 5

MTBE ug/kg < 5 MCERTS < 5 < 5

trans-1,2-Dichloroethene ug/kg < 5 MCERTS < 5 < 5

1,1-Dichloroethane ug/kg < 5 MCERTS < 5 < 5

cis-1,2-Dichloroethene ug/kg < 5 MCERTS < 5 < 5

2,2-Dichloropropane ug/kg < 5 MCERTS < 5 < 5

Chloroform ug/kg < 5 MCERTS < 5 < 5

Bromochloromethane ug/kg < 5 MCERTS < 5 < 5

1,1,1-Trichloroethane ug/kg < 5 MCERTS < 5 < 5

1,1-Dichloropropene ug/kg < 10 MCERTS < 10 < 10

Carbon Tetrachloride ug/kg < 5 MCERTS < 5 < 5

1,2-Dichloroethane ug/kg < 5 MCERTS < 5 < 5

Benzene ug/kg < 2 MCERTS < 2 < 2

1,2-Dichloropropane ug/kg < 5 MCERTS < 5 < 5

Trichloroethene ug/kg < 5 MCERTS < 5 276

Bromodichloromethane ug/kg < 5 MCERTS < 5 < 5

Dibromomethane ug/kg < 5 MCERTS < 5 < 5

TAME ug/kg < 5 MCERTS < 5 < 5

cis-1,3-Dichloropropene ug/kg < 5 MCERTS < 5 < 5

Toluene ug/kg < 5 MCERTS < 5 < 5

trans-1,3-Dichloropropene ug/kg < 5 MCERTS < 5 < 5

1,1,2-Trichloroethane ug/kg < 10 MCERTS < 10 < 10

1,3-Dichloropropane ug/kg < 5 MCERTS < 5 < 5

Tetrachloroethene ug/kg < 5 MCERTS < 5 < 5

Dibromochloromethane ug/kg < 5 MCERTS < 5 < 5

1,2-Dibromoethane ug/kg < 5 MCERTS < 5 < 5

Chlorobenzene ug/kg < 5 MCERTS < 5 < 5

1,1,1,2-Tetrachloroethane ug/kg < 5 MCERTS < 5 < 5

Ethyl Benzene ug/kg < 10 MCERTS < 10 < 10

m,p-Xylene ug/kg < 10 MCERTS < 10 < 10

o-Xylene ug/kg < 10 MCERTS < 10 < 10

Styrene ug/kg < 5 MCERTS < 5 < 5

Bromoform ug/kg < 10 MCERTS < 10 < 10

Isopropylbenzene ug/kg < 5 MCERTS < 5 < 5

1,1,2,2-Tetrachloroethane ug/kg < 5 MCERTS < 5 < 5

1,2,3-Trichloropropane ug/kg < 5 MCERTS < 5 < 5

n-Propylbenzene ug/kg < 5 MCERTS < 5 < 5

Bromobenzene ug/kg < 5 MCERTS < 5 < 5

2-Chlorotoluene ug/kg < 5 MCERTS < 5 < 5

1,3,5-Trimethylbenzene ug/kg < 5 MCERTS < 5 < 5

4-Chlorotoluene ug/kg < 5 MCERTS < 5 < 5

tert-Butylbenzene ug/kg < 5 MCERTS < 5 < 5

1,2,4-Trimethylbenzene ug/kg < 5 MCERTS < 5 < 5

sec-Butylbenzene ug/kg < 5 MCERTS < 5 < 5

p-Isopropyltoluene ug/kg < 5 MCERTS < 5 < 5

1,3-Dichlorobenzene ug/kg < 5 MCERTS < 5 < 5

1,4-Dichlorobenzene ug/kg < 5 MCERTS < 5 < 5

n-Butylbenzene ug/kg < 5 MCERTS < 5 < 5

1,2-Dichlorobenzene ug/kg < 5 MCERTS < 5 < 5

1,2-Dibromo-3-chloropropane ug/kg < 10 MCERTS < 10 < 10

Hexachlorobutadiene ug/kg < 5 MCERTS < 5 < 5

Analytical results are expressed on a dry weight basis where samples are dried at less than 30OC

QTS Environmental Report No: 14-25663 Date Sampled

Lustre Consulting Ltd Time Sampled

Project / Job Ref: 1309 Additional Refs

Order No: 1309 Depth (m)

Reporting Date: 22/10/2014 QTSE Sample No

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Kent ME17 2JN

Tel : 01622 850410 '

Site Reference: K & N Distribution Depot,

Derby

TP / BH No

Soil Analysis Certificate - Volatile Organic Compounds (VOC)

QTS Environmental Ltd - Registered in England No 06620874 Page 26 of 28

Page 65: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

QTSE Sample No TP / BH No Additional Refs Depth (m)Moisture

Content (%)

$ 121787 SP1 None Supplied 0.50 13.1

$ 121788 TP1 None Supplied 0.30 - 0.50 22.2

$ 121790 TP3 None Supplied 0.05 21

$ 121791 TP3 None Supplied 0.50 15.6

$ 121792 TP4 None Supplied 0.20 17.4

$ 121793 TP5 None Supplied 0.50 & BB 3.9

$ 121794 TP6 None Supplied 0.20 15.4

$ 121795 TP9 None Supplied 0.20 9.2

$ 121796 TP10 None Supplied 0.10 - 0.30 17.9

$ 121797 TP11 None Supplied 0.30 23.5

$ 121798 TP12 None Supplied 0.10 - 0.20 14.5

$ 121799 TP15 None Supplied 0.60 - 0.70 13.9

$ 121801 TP16 None Supplied 0.20 - 0.30 13.7

$ 121802 TP17 None Supplied 0.10 9.4

$ 121804 WS501 None Supplied 1.80 - 1.90 19.7

$ 121805 WS502 None Supplied 0.30 - 0.40 18.7

$ 121806 WS503 None Supplied 0.60 - 0.70 14

$ 121808 WS504 None Supplied 0.70 - 1.00 2.8

$ 121809 WS504 None Supplied 1.60 - 1.80 15.3

$ 121811 WS506 None Supplied 0.60 - 0.70 11.6

$ 121813 WS507 None Supplied 0.80 - 0.90 13.8

$ 121814 WS507 None Supplied 1.20 - 1.30 12.7

$ 121815 WS508 None Supplied 0.20 - 0.40 5.5

$ 121816 WS508 None Supplied 0.50 - 0.60 10.7

$ 121817 WS509 None Supplied 0.50 - 0.80 16.3

$ 121819 WS510 None Supplied 0.14 - 0.20 12.7

$ 121820 WS511 None Supplied 0.45 - 0.55 14.4

$ 121821 WS511 None Supplied 0.60 - 0.80 18.2

$ 121823 WS513 None Supplied 0.30 - 0.40 13.5

$ 121824 WS513 None Supplied 3.60 - 3.70 17.9

$ 121825 WS514 None Supplied 0.10 - 0.50 13.1

$ 121826 WS515 None Supplied 0.30 - 0.60 12.3

$ 121827 WS515 None Supplied 0.90 - 1.00 20.8

$ 121828 WS515 None Supplied 1.00 - 1.30 21.3

Moisture content is part of procedure E003 & is not an accredited test

Insufficient Sample I/S

Unsuitable Sample U/S

$ samples exceeded recommended holding times

Brown clay

Red clay

Grey loamy gravel with brick and rubble

Red clay

Grey loamy gravel with rubble

Brown loamy gravel with rubble

Brown sandy clay

Red loamy gravel with rubble and oil / petroleum

Red sandy clay with rubble

Red clayey loam with brick and rubble

Light brown sandy gravel with rubble

Red clayey loam

Red loamy gravel with brick and stones

Red clayey loam

Red sandy clay

Red clayey gravel

Red loamy gravel with rubble

Red clay

Brown loam with concrete and vegetation

Brown clayey loam with brick and vegetation

Red clayey loam

Red sandy clay with rubble and vegetation

Light brown clayey gravel with rubble

Red clayey loam with vegetation

Grey loamy gravel with rubble

Brown loamy gravel with vegetation

Red clayey loam with vegetation

Red clayey loam with vegetation

Grey loamy gravel

Red loamy gravel with rubble

Grey loamy gravel with rubble

Red clayey loam

Tel : 01622 850410 '

Soil Analysis Certificate - Sample Descriptions

QTS Environmental Report No: 14-25663

Lustre Consulting Ltd

Site Reference: K & N Distribution Depot, Derby

Project / Job Ref: 1309

Order No: 1309

Reporting Date: 22/10/2014

Sample Matrix Description

Red clayey loam with stones

Grey loamy gravel with rubble

Kent ME17 2JN

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

QTS Environmental Ltd - Registered in England No 06620874 Page 27 of 28

Page 66: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Matrix Analysed

On

Determinand Brief Method Description Method

No

Soil D Boron - Water Soluble Determination of water soluble boron in soil by 2:1 hot water extract followed by ICP-OES E012

Soil AR BTEX Determination of BTEX by headspace GC-MS E001

Soil D Cations Determination of cations in soil by aqua-regia digestion followed by ICP-OES E002

Soil D Chloride - Water Soluble (2:1) Determination of chloride by extraction with water & analysed by ion chromatography E009

Soil AR Chromium - HexavalentDetermination of hexavalent chromium in soil by extraction in water then by acidification, addition of 1,5

diphenylcarbazide followed by colorimetryE016

Soil AR Cyanide - Complex Determination of complex cyanide by distillation followed by colorimetry E015

Soil AR Cyanide - Free Determination of free cyanide by distillation followed by colorimetry E015

Soil AR Cyanide - Total Determination of total cyanide by distillation followed by colorimetry E015

Soil D Cyclohexane Extractable Matter (CEM) Gravimetrically determined through extraction with cyclohexane E011

Soil AR Diesel Range Organics (C10 - C24) Determination of hexane/acetone extractable hydrocarbons by GC-FID E004

Soil AR Electrical ConductivityDetermination of electrical conductivity by addition of saturated calcium sulphate followed by

electrometric measurementE022

Soil AR Electrical Conductivity Determination of electrical conductivity by addition of water followed by electrometric measurement E023

Soil D Elemental Sulphur Determination of elemental sulphur by solvent extraction followed by GC-MS E020

Soil AR EPH (C10 – C40) Determination of acetone/hexane extractable hydrocarbons by GC-FID E004

Soil AR EPH Product ID Determination of acetone/hexane extractable hydrocarbons by GC-FID E004

Soil AR EPH TEXAS Determination of acetone/hexane extractable hydrocarbons by GC-FID E004

Soil D Fluoride - Water Soluble Determination of Fluoride by extraction with water & analysed by ion chromatography E009

Soil D FOC (Fraction Organic Carbon)Determination of fraction of organic carbon by oxidising with potassium dichromate followed by titration

with iron (II) sulphateE010

Soil D Loss on Ignition @ 450oCDetermination of loss on ignition in soil by gravimetrically with the sample being ignited in a muffle

furnaceE019

Soil D Magnesium - Water Soluble Determination of water soluble magnesium by extraction with water followed by ICP-OES E025

Soil D Metals Determination of metals by aqua-regia digestion followed by ICP-OES E002

Soil AR Mineral Oil (C10 - C40) Determination of hexane/acetone extractable hydrocarbons by GC-FID fractionating with SPE cartridge E004

Soil AR Moisture Content Moisture content; determined gravimetrically E003

Soil D Nitrate - Water Soluble (2:1) Determination of nitrate by extraction with water & analysed by ion chromatography E009

Soil D Organic MatterDetermination of organic matter by oxidising with potassium dichromate followed by titration with iron

(II) sulphateE010

Soil AR PAH - Speciated (EPA 16)Determination of PAH compounds by extraction in acetone and hexane followed by GC-MS with the use

of surrogate and internal standardsE005

Soil AR PCB - 7 Congeners Determination of PCB by extraction with acetone and hexane followed by GC-MS E008

Soil D Petroleum Ether Extract (PEE) Gravimetrically determined through extraction with petroleum ether E011

Soil AR pH Determination of pH by addition of water followed by electrometric measurement E007

Soil AR Phenols - Total (monohydric) Determination of phenols by distillation followed by colorimetry E021

Soil D Phosphate - Water Soluble (2:1) Determination of phosphate by extraction with water & analysed by ion chromatography E009

Soil D Sulphate (as SO4) - Total Determination of total sulphate by extraction with 10% HCl followed by ICP-OES E013

Soil D Sulphate (as SO4) - Water Soluble (2:1) Determination of sulphate by extraction with water & analysed by ion chromatography E009

Soil D Sulphate (as SO4) - Water Soluble (2:1) Determination of water soluble sulphate by extraction with water followed by ICP-OES E014

Soil AR Sulphide Determination of sulphide by distillation followed by colorimetry E018

Soil D Sulphur - Total Determination of total sulphur by extraction with aqua-regia followed by ICP-OES E024

Soil AR SVOCDetermination of semi-volatile organic compounds by extraction in acetone and hexane followed by GC-

MSE006

Soil AR Thiocyanate (as SCN)Determination of thiocyanate by extraction in caustic soda followed by acidification followed by addition

of ferric nitrate followed by colorimetryE017

Soil D Toluene Extractable Matter (TEM) Gravimetrically determined through extraction with toluene E011

Soil D Total Organic Carbon (TOC)Determination of organic matter by oxidising with potassium dichromate followed by titration with iron

(II) sulphateE010

Soil AR TPH CWG Determination of hexane/acetone extractable hydrocarbons by GC-FID fractionating with SPE cartridge E004

Soil AR TPH LQM Determination of hexane/acetone extractable hydrocarbons by GC-FID fractionating with SPE cartridge E004

Soil AR VOCs Determination of volatile organic compounds by headspace GC-MS E001

Soil AR VPH (C6 - C10) Determination of hydrocarbons C6-C10 by headspace GC-MS E001

D Dried

AR As Received

Order No: 1309

Reporting Date: 22/10/2014

Tel : 01622 850410 '

Soil Analysis Certificate - Methodology & Miscellaneous Information

QTS Environmental Report No: 14-25663

Lustre Consulting Ltd

Site Reference: K & N Distribution Depot, Derby

Project / Job Ref: 1309

Kent ME17 2JN

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

QTS Environmental Ltd - Registered in England No 06620874 Page 28 of 28

Page 67: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

James May QTS Environmental Ltd

Lustre Consulting Ltd Unit 1

Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Kent

ME17 2JN

t: 01622 [email protected]

Site Reference: K+N Distribution Depot

Project / Job Ref: 1309

Order No: 1309

Sample Receipt Date: 27/10/2014

Sample Scheduled Date: 27/10/2014

Report Issue Number: 1

Reporting Date: 31/10/2014

Authorised by: Authorised by:

Russell Jarvis Kevin Old

Director Director

On behalf of QTS Environmental Ltd On behalf of QTS Environmental Ltd

Admiral's Offices

The Historic Dockyard

Chatham

Kent

ME4 4TZ

QTS Environmental Report No: 14-26026

QTS Environmental Ltd - Registered in England No 06620874 Page 1 of 8

Page 68: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

24/10/14 24/10/14 24/10/14 24/10/14 24/10/14

None Supplied None Supplied None Supplied None Supplied None Supplied

WS501 WS502 WS503 WS507 WS513

None Supplied None Supplied None Supplied None Supplied None Supplied

None Supplied None Supplied None Supplied None Supplied None Supplied

123555 123556 123557 123558 123559

Determinand Unit RL Accreditation

pH pH Units N/a ISO17025 7.1 7.3 7.3 8.5 7.6

Total Cyanide ug/l < 5 NONE < 5 < 5 < 5 < 5 < 5

Sulphate as SO4 mg/l < 1 ISO17025 962 77 63 55 33

Total Organic Carbon (TOC) mg/l < 0.1 NONE 36 60.8 64.6 9.6 59.5

Carbonate as CaCO3 (S) mg/l < 10 NONE 290 370 350 130 340

Arsenic (dissolved) ug/l < 10 NONE < 10 < 10 < 10 15 < 10

Boron (dissolved) ug/l < 50 NONE 161 159 157 115 114

Cadmium (dissolved) ug/l < 0.5 NONE < 0.5 < 0.5 < 0.5 < 0.5 < 0.5

Chromium (dissolved) ug/l < 5 NONE < 5 < 5 7 8 9

Chromium (hexavalent) ug/l < 5 NONE < 5 < 5 < 5 < 5 < 5

Copper (dissolved) ug/l < 10 NONE < 10 < 10 < 10 < 10 < 10

Lead (dissolved) ug/l < 5 NONE < 5 < 5 < 5 < 5 < 5

Mercury (dissolved) ug/l < 0.05 NONE < 0.05 < 0.05 < 0.05 < 0.05 < 0.05

Nickel (dissolved) ug/l < 7 NONE < 7 < 7 < 7 < 7 < 7

Selenium (dissolved) ug/l < 5 NONE < 5 < 5 < 5 < 5 < 5

Zinc (dissolved) ug/l < 5 NONE 8 < 5 < 5 < 5 < 5

Total Phenols ug/l < 0.5 NONE < 0.5 < 0.5 < 0.5 < 0.5 < 0.5

EPH (C10 - C40) ug/l < 10 NONE < 10 < 10 < 10 < 10 < 10

Subcontracted analysis (S)

Insufficient sample I/S

Unsuitable Sample U/S

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Site Reference: K+N Distribution Depot TP / BH No

Project / Job Ref: 1309 Additional Refs

Tel : 01622 850410

Water Analysis Certificate

QTS Environmental Report No: 14-26026 Date Sampled

Lustre Consulting Ltd Time Sampled

Kent ME17 2JN

Reporting Date: 31/10/2014 QTSE Sample No

Order No: 1309 Depth (m)

QTS Environmental Ltd - Registered in England No 06620874 Page 2 of 8

Page 69: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

24/10/14 24/10/14

None Supplied None Supplied

WS514 WS517

None Supplied None Supplied

None Supplied None Supplied

123560 123561

Determinand Unit RL Accreditation

pH pH Units N/a ISO17025 7.8 7.5

Total Cyanide ug/l < 5 NONE < 5 < 5

Sulphate as SO4 mg/l < 1 ISO17025 248 140

Total Organic Carbon (TOC) mg/l < 0.1 NONE 26.7 47.5

Carbonate as CaCO3 (S) mg/l < 10 NONE 180 260

Arsenic (dissolved) ug/l < 10 NONE < 10 < 10

Boron (dissolved) ug/l < 50 NONE 131 183

Cadmium (dissolved) ug/l < 0.5 NONE < 0.5 < 0.5

Chromium (dissolved) ug/l < 5 NONE 14 6

Chromium (hexavalent) ug/l < 5 NONE < 5 < 5

Copper (dissolved) ug/l < 10 NONE < 10 < 10

Lead (dissolved) ug/l < 5 NONE < 5 < 5

Mercury (dissolved) ug/l < 0.05 NONE < 0.05 < 0.05

Nickel (dissolved) ug/l < 7 NONE < 7 < 7

Selenium (dissolved) ug/l < 5 NONE < 5 < 5

Zinc (dissolved) ug/l < 5 NONE < 5 < 5

Total Phenols ug/l < 0.5 NONE < 0.5 < 0.5

EPH (C10 - C40) ug/l < 10 NONE < 10 < 10

Subcontracted analysis (S)

Insufficient sample I/S

Unsuitable Sample U/S

Kent ME17 2JN

Tel : 01622 850410

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Site Reference: K+N Distribution Depot TP / BH No

Water Analysis Certificate

QTS Environmental Report No: 14-26026 Date Sampled

Lustre Consulting Ltd Time Sampled

Project / Job Ref: 1309 Additional Refs

Order No: 1309 Depth (m)

Reporting Date: 31/10/2014 QTSE Sample No

QTS Environmental Ltd - Registered in England No 06620874 Page 3 of 8

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24/10/14 24/10/14 24/10/14 24/10/14 24/10/14

None Supplied None Supplied None Supplied None Supplied None Supplied

WS501 WS502 WS503 WS507 WS513

None Supplied None Supplied None Supplied None Supplied None Supplied

None Supplied None Supplied None Supplied None Supplied None Supplied

123555 123556 123557 123558 123559

Determinand Unit RL Accreditation

Naphthalene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Acenaphthylene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Acenaphthene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Fluorene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Phenanthrene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Anthracene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Fluoranthene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Pyrene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Benzo(a)anthracene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Chrysene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Benzo(b)fluoranthene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Benzo(k)fluoranthene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Benzo(a)pyrene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Indeno(1,2,3-cd)pyrene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Dibenz(a,h)anthracene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Benzo(ghi)perylene ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Total EPA-16 PAHs ug/l < 0.01 NONE < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

-

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Site Reference: K+N Distribution

Depot

TP / BH No

Project / Job Ref: 1309 Additional Refs

Tel : 01622 850410

Water Analysis Certificate - Speciated PAH

QTS Environmental Report No: 14-26026 Date Sampled

Lustre Consulting Ltd Time Sampled

Kent ME17 2JN

Reporting Date: 31/10/2014 QTSE Sample No

Order No: 1309 Depth (m)

QTS Environmental Ltd - Registered in England No 06620874 Page 4 of 8

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24/10/14 24/10/14

None Supplied None Supplied

WS514 WS517

None Supplied None Supplied

None Supplied None Supplied

123560 123561

Determinand Unit RL Accreditation

Naphthalene ug/l < 0.01 NONE < 0.01 < 0.01

Acenaphthylene ug/l < 0.01 NONE < 0.01 < 0.01

Acenaphthene ug/l < 0.01 NONE < 0.01 < 0.01

Fluorene ug/l < 0.01 NONE < 0.01 < 0.01

Phenanthrene ug/l < 0.01 NONE < 0.01 < 0.01

Anthracene ug/l < 0.01 NONE < 0.01 < 0.01

Fluoranthene ug/l < 0.01 NONE < 0.01 < 0.01

Pyrene ug/l < 0.01 NONE < 0.01 < 0.01

Benzo(a)anthracene ug/l < 0.01 NONE < 0.01 < 0.01

Chrysene ug/l < 0.01 NONE < 0.01 < 0.01

Benzo(b)fluoranthene ug/l < 0.01 NONE < 0.01 < 0.01

Benzo(k)fluoranthene ug/l < 0.01 NONE < 0.01 < 0.01

Benzo(a)pyrene ug/l < 0.01 NONE < 0.01 < 0.01

Indeno(1,2,3-cd)pyrene ug/l < 0.01 NONE < 0.01 < 0.01

Dibenz(a,h)anthracene ug/l < 0.01 NONE < 0.01 < 0.01

Benzo(ghi)perylene ug/l < 0.01 NONE < 0.01 < 0.01

Total EPA-16 PAHs ug/l < 0.01 NONE < 0.01 < 0.01

-

Kent ME17 2JN

Tel : 01622 850410

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Site Reference: K+N Distribution

Depot

TP / BH No

Water Analysis Certificate - Speciated PAH

QTS Environmental Report No: 14-26026 Date Sampled

Lustre Consulting Ltd Time Sampled

Project / Job Ref: 1309 Additional Refs

Order No: 1309 Depth (m)

Reporting Date: 31/10/2014 QTSE Sample No

QTS Environmental Ltd - Registered in England No 06620874 Page 5 of 8

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24/10/14 24/10/14 24/10/14 24/10/14 24/10/14

None Supplied None Supplied None Supplied None Supplied None Supplied

WS501 WS502 WS503 WS507 WS513

None Supplied None Supplied None Supplied None Supplied None Supplied

None Supplied None Supplied None Supplied None Supplied None Supplied

123555 123556 123557 123558 123559

Determinand Unit RL Accreditation

Dichlorodifluoromethane ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

Vinyl Chloride ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

Chloromethane ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

Chloroethane ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

Bromomethane ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

Trichlorofluoromethane ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

1,1-Dichloroethene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

MTBE ug/l < 10 ISO17025 < 10 < 10 < 10 < 10 < 10

trans-1,2-Dichloroethene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

1,1-Dichloroethane ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

cis-1,2-Dichloroethene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

2,2-Dichloropropane ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

Chloroform ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

Bromochloromethane ug/l < 10 ISO17025 < 10 < 10 < 10 < 10 < 10

1,1,1-Trichloroethane ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

1,1-Dichloropropene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

Carbon Tetrachloride ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

1,2-Dichloroethane ug/l < 10 ISO17025 < 10 < 10 < 10 < 10 < 10

Benzene ug/l < 1 ISO17025 < 1 < 1 < 1 < 1 < 1

1,2-Dichloropropane ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

Trichloroethene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

Bromodichloromethane ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

Dibromomethane ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

TAME ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

cis-1,3-Dichloropropene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

Toluene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

trans-1,3-Dichloropropene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

1,1,2-Trichloroethane ug/l < 10 ISO17025 < 10 < 10 < 10 < 10 < 10

1,3-Dichloropropane ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

Tetrachloroethene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

Dibromochloromethane ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

1,2-Dibromoethane ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

Chlorobenzene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

1,1,1,2-Tetrachloroethane ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

Ethyl Benzene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

m,p-Xylene ug/l < 10 ISO17025 < 10 < 10 < 10 < 10 < 10

o-Xylene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

Styrene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

Bromoform ug/l < 10 ISO17025 < 10 < 10 < 10 < 10 < 10

Isopropylbenzene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

1,1,2,2-Tetrachloroethane ug/l < 10 ISO17025 < 10 < 10 < 10 < 10 < 10

1,2,3-Trichloropropane ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

n-Propylbenzene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

Bromobenzene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

2-Chlorotoluene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

1,3,5-Trimethylbenzene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

4-Chlorotoluene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

tert-Butylbenzene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

1,2,4-Trimethylbenzene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

sec-Butylbenzene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

p-Isopropyltoluene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

1,3-Dichlorobenzene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

1,4-Dichlorobenzene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

n-Butylbenzene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

1,2-Dichlorobenzene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

1,2-Dibromo-3-chloropropane ug/l < 10 ISO17025 < 10 < 10 < 10 < 10 < 10

Hexachlorobutadiene ug/l < 5 ISO17025 < 5 < 5 < 5 < 5 < 5

-

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Site Reference: K+N Distribution Depot TP / BH No

Project / Job Ref: 1309 Additional Refs

Tel : 01622 850410

Water Analysis Certificate - Volatile Organic Compounds (VOC)

QTS Environmental Report No: 14-26026 Date Sampled

Lustre Consulting Ltd Time Sampled

Kent ME17 2JN

Reporting Date: 31/10/2014 QTSE Sample No

Order No: 1309 Depth (m)

QTS Environmental Ltd - Registered in England No 06620874 Page 6 of 8

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24/10/14 24/10/14

None Supplied None Supplied

WS514 WS517

None Supplied None Supplied

None Supplied None Supplied

123560 123561

Determinand Unit RL Accreditation

Dichlorodifluoromethane ug/l < 5 ISO17025 < 5 < 5

Vinyl Chloride ug/l < 5 ISO17025 < 5 < 5

Chloromethane ug/l < 5 ISO17025 < 5 < 5

Chloroethane ug/l < 5 ISO17025 < 5 < 5

Bromomethane ug/l < 5 ISO17025 < 5 < 5

Trichlorofluoromethane ug/l < 5 ISO17025 < 5 < 5

1,1-Dichloroethene ug/l < 5 ISO17025 < 5 < 5

MTBE ug/l < 10 ISO17025 < 10 < 10

trans-1,2-Dichloroethene ug/l < 5 ISO17025 < 5 < 5

1,1-Dichloroethane ug/l < 5 ISO17025 < 5 < 5

cis-1,2-Dichloroethene ug/l < 5 ISO17025 < 5 < 5

2,2-Dichloropropane ug/l < 5 ISO17025 < 5 < 5

Chloroform ug/l < 5 ISO17025 < 5 < 5

Bromochloromethane ug/l < 10 ISO17025 < 10 < 10

1,1,1-Trichloroethane ug/l < 5 ISO17025 < 5 < 5

1,1-Dichloropropene ug/l < 5 ISO17025 < 5 < 5

Carbon Tetrachloride ug/l < 5 ISO17025 < 5 < 5

1,2-Dichloroethane ug/l < 10 ISO17025 < 10 < 10

Benzene ug/l < 1 ISO17025 < 1 < 1

1,2-Dichloropropane ug/l < 5 ISO17025 < 5 < 5

Trichloroethene ug/l < 5 ISO17025 < 5 < 5

Bromodichloromethane ug/l < 5 ISO17025 < 5 < 5

Dibromomethane ug/l < 5 ISO17025 < 5 < 5

TAME ug/l < 5 ISO17025 < 5 < 5

cis-1,3-Dichloropropene ug/l < 5 ISO17025 < 5 < 5

Toluene ug/l < 5 ISO17025 < 5 < 5

trans-1,3-Dichloropropene ug/l < 5 ISO17025 < 5 < 5

1,1,2-Trichloroethane ug/l < 10 ISO17025 < 10 < 10

1,3-Dichloropropane ug/l < 5 ISO17025 < 5 < 5

Tetrachloroethene ug/l < 5 ISO17025 < 5 < 5

Dibromochloromethane ug/l < 5 ISO17025 < 5 < 5

1,2-Dibromoethane ug/l < 5 ISO17025 < 5 < 5

Chlorobenzene ug/l < 5 ISO17025 < 5 < 5

1,1,1,2-Tetrachloroethane ug/l < 5 ISO17025 < 5 < 5

Ethyl Benzene ug/l < 5 ISO17025 < 5 < 5

m,p-Xylene ug/l < 10 ISO17025 < 10 < 10

o-Xylene ug/l < 5 ISO17025 < 5 < 5

Styrene ug/l < 5 ISO17025 < 5 < 5

Bromoform ug/l < 10 ISO17025 < 10 < 10

Isopropylbenzene ug/l < 5 ISO17025 < 5 < 5

1,1,2,2-Tetrachloroethane ug/l < 10 ISO17025 < 10 < 10

1,2,3-Trichloropropane ug/l < 5 ISO17025 < 5 < 5

n-Propylbenzene ug/l < 5 ISO17025 < 5 < 5

Bromobenzene ug/l < 5 ISO17025 < 5 < 5

2-Chlorotoluene ug/l < 5 ISO17025 < 5 < 5

1,3,5-Trimethylbenzene ug/l < 5 ISO17025 < 5 < 5

4-Chlorotoluene ug/l < 5 ISO17025 < 5 < 5

tert-Butylbenzene ug/l < 5 ISO17025 < 5 < 5

1,2,4-Trimethylbenzene ug/l < 5 ISO17025 < 5 < 5

sec-Butylbenzene ug/l < 5 ISO17025 < 5 < 5

p-Isopropyltoluene ug/l < 5 ISO17025 < 5 < 5

1,3-Dichlorobenzene ug/l < 5 ISO17025 < 5 < 5

1,4-Dichlorobenzene ug/l < 5 ISO17025 < 5 < 5

n-Butylbenzene ug/l < 5 ISO17025 < 5 < 5

1,2-Dichlorobenzene ug/l < 5 ISO17025 < 5 < 5

1,2-Dibromo-3-chloropropane ug/l < 10 ISO17025 < 10 < 10

Hexachlorobutadiene ug/l < 5 ISO17025 < 5 < 5

-

Kent ME17 2JN

Tel : 01622 850410

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Site Reference: K+N Distribution Depot TP / BH No

Water Analysis Certificate - Volatile Organic Compounds (VOC)

QTS Environmental Report No: 14-26026 Date Sampled

Lustre Consulting Ltd Time Sampled

Project / Job Ref: 1309 Additional Refs

Order No: 1309 Depth (m)

Reporting Date: 31/10/2014 QTSE Sample No

QTS Environmental Ltd - Registered in England No 06620874 Page 7 of 8

Page 74: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Matrix Analysed

On

Determinand Brief Method Description Method

No

Water UF Alkalinity Determination of alkalinity by titration against hydrochloric acid using bromocresol green as the end point E103

Water UF BTEX Determination of BTEX by headspace GC-MS E101

Water F Cations Determination of cations by filtration followed by ICP-MS E102

Water UF Chemical Oxygen Demand (COD) Determination using a COD reactor followed by colorimetry E112

Water F Chloride Determination of chloride by filtration & analysed by ion chromatography E109

Water F Chromium - Hexavalent Determination of hexavalent chromium by acidification, addition of 1,5 diphenylcarbazide followed by colorimetryE116

Water UF Cyanide - Complex Determination of complex cyanide by distillation followed by colorimetry E115

Water UF Cyanide - Free Determination of free cyanide by distillation followed by colorimetry E115

Water UF Cyanide - Total Determination of total cyanide by distillation followed by colorimetry E115

Water UF Cyclohexane Extractable Matter (CEM) Gravimetrically determined through liquid:liquid extraction with cyclohexane E111

Water F Diesel Range Organics (C10 - C24) Determination of liquid:liquid extraction with hexane followed by GI-FID E104

Water F Dissolved Organic Content (DOC) Determination of DOC by filtration followed by low heat with persulphate addition followed by IR detection E110

Water UF Electrical Conductivity Determination of electrical conductivity by electrometric measurement E123

Water F EPH (C10 – C40) Determination of liquid:liquid extraction with hexane followed by GI-FID E104

Water F EPH TEXAS Determination of liquid:liquid extraction with hexane followed by GI-FID E104

Water F Fluoride Determination of Fluoride by filtration & analysed by ion chromatography E109

Water F Hardness Determination of Ca and Mg by ICP-MS followed by calculation E102

Leachate F Leachate Preparation - NRA Based on National Rivers Authority leaching test 1994 E301

Leachate F Leachate Preparation - WAC Based on BS EN 12457 Pt1, 2, 3 E302

Water F Metals Determination of metals by filtration followed by ICP-MS E102

Water F Mineral Oil (C10 - C40) Determination of liquid:liquid extraction with hexane followed by GI-FID E104

Water F Nitrate Determination of nitrate by filtration & analysed by ion chromatography E109

Water UF Monohydric Phenol Determination of phenols by distillation followed by colorimetry E121

Water F PAH - Speciated (EPA 16)Determination of PAH compounds by concentration through SPE cartridge, collection in dichloromethane

followed by GC-MSE105

Water F PCB - 7 Congeners Determination of PCB compounds by concentration through SPE cartridge, collection in dichloromethane followed by GC-MSE108

Water UF Petroleum Ether Extract (PEE) Gravimetrically determined through liquid:liquid extraction with petroleum ether E111

Water UF pH Determination of pH by electrometric measurement E107

Water F Phosphate Determination of phosphate by filtration & analysed by ion chromatography E109

Water UF Redox Potential Determination of redox potential by electrometric measurement E113

Water F Sulphate (as SO4) Determination of sulphate by filtration & analysed by ion chromatography E109

Water UF Sulphide Determination of sulphide by distillation followed by colorimetry E118

Water F SVOCDetermination of semi-volatile organic compounds by concentration through SPE cartridge, collection in

dichloromethane followed by GC-MSE106

Water UF Toluene Extractable Matter (TEM) Gravimetrically determined through liquid:liquid extraction with toluene E111

Water UF Total Organic Carbon (TOC) Low heat with persulphate addition followed by IR detection E110

Water F TPH CWG Determination of liquid:liquid extraction with hexane, fractionating with SPE followed by GC-FID E104

Water F TPH LQM Determination of liquid:liquid extraction with hexane, fractionating with SPE followed by GC-FID E104

Water UF VOCs Determination of volatile organic compounds by headspace GC-MS E101

Water UF VPH (C6 - C10) Determination of hydrocarbons C6-C10 by headspace GC-MS E101

Key

F Filtered

UF Unfiltered

Kent ME17 2JN

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Order No: 1309

Reporting Date: 31/10/2014

Tel : 01622 850410 '

Soil Analysis Certificate - Methodology & Miscellaneous Information

QTS Environmental Report No: 14-26026

Lustre Consulting Ltd

Site Reference: K+N Distribution Depot

Project / Job Ref: 1309

QTS Environmental Ltd - Registered in England No 06620874 Page 8 of 8

Page 75: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Amy Khan QTS Environmental Ltd

Lustre Consulting Ltd Unit 1

Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Kent

ME17 2JN

t: 01622 [email protected]

Site Reference: K & N Distribution Depot

Project / Job Ref: 1309

Order No: 1309

Sample Receipt Date: 08/10/2014

Sample Scheduled Date: 06/11/2014

Report Issue Number: 1

Reporting Date: 28/11/2014

Authorised by: Authorised by:

Russell Jarvis Kevin Old

Director Director

On behalf of QTS Environmental Ltd On behalf of QTS Environmental Ltd

Admiral's Offices

The Historic Dockyard

Chatham

Kent

ME4 4TZ

QTS Environmental Report No: 14-26360

QTS Environmental Ltd - Registered in England No 06620874 Page 1 of 2

Page 76: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

None Supplied None Supplied None Supplied

None Supplied None Supplied None Supplied

BH1 BH2 BH3

None Supplied None Supplied None Supplied

None Supplied None Supplied None Supplied

124965 124966 124967

Determinand Unit RL Accreditation

Tentative Petroleum Type N/a N/a NONETypical of

weathered diesel

range organics

Typical of

weathered diesel

range organics

Typical of

weathered diesel

range organics

Subcontracted analysis (S)

Kent ME17 2JN

QTS Environmental Ltd

Unit 1, Rose Lane Industrial Estate

Rose Lane

Lenham Heath

Maidstone

Tel : 01622 850410

Oil Analysis Certificate

QTS Environmental Report No: 14-26360 Date Sampled

Lustre Consulting Ltd Time Sampled

Reporting Date: 28/11/2014 QTSE Sample No

Site Reference: K & N Distribution Depot TP / BH No

Project / Job Ref: 1309 Additional Refs

Order No: 1309 Depth (m)

QTS Environmental Ltd - Registered in England No 06620874 Page 2 of 2

Page 77: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

APPENDIX D

GEOTECHNICAL TEST

CERTIFICATES

Page 78: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Project Name: Samples Received:

Project Started:

Client: Testing Started:

Project No: Our job/report no: Date Reported:

Borehole

No:

Sample

No:

Depth

(m)

Moisture

content

(%)

Liquid

Limit

(%)

Plastic

Limit

(%)

Plasticity

Index

(%)

Passing

0.425

mm (%)

WS5031.20 -

2.0019 38 18 20 94

WS5053.40 -

3.7026 43 22 21 100

WS5072.50 -

3.0015 29 19 10 100

WS508.60 -

1.0013 29 18 11 100

WS5102.00 -

2.4023 35 19 16 100

WS5121.20 -

1.5024 39 23 16 100

WS5131.60 -

1.9019 28 15 13 100

WS5133.70 -

4.0025 34 20 14 100

WS5142.50 -

2.8018 26 16 10 100

WS5161.60 -

2.0022 31 18 13 100

WS5171.45 -

2.0023 38 20 18 100

WS518.50 -

1.0017 40 20 20 100

Summary of Test ResultsInitials: K.P

BS 1377 : Part 2 : Clause 5 : 1990 Determination of the plastic limit and plasticity index. Date: 04/11/2014

2519 BS 1377 : Part 2 : Clause 3.2 : 1990 Determination of the moisture content by the oven-drying method.

Test Report by K4 SOILS LABORATORY Unit 8 Olds Close Olds Approach Watford Herts WD18 9RU

Test Results relate only to the sample numbers shown above. Approved Signatories: K.Phaure (Tech.Mgr) J.Phaure (Lab.Mgr)

All samples connected with this report ,incl any on 'hold' will be stored and disposed off according to Company policy.Acopy of this policy is available on request. MSF-11/R2

Medium strength reddish brown slightly sandy silty CLAY with

fine mudstone fragments

K4 SOILS

Remarks

14/10/2014

15/10/2014

27/10/2014

04/11/2014

K&N Distribution Depot, Derby

Lustre Consulting

176441309

BS 1377 : Part 2 : Clause 4.4 : 1990 Determination of the liquid limit by the cone penetrometer method.

Description

Very high strength brown slightly gravelly silty CLAY

occasional with black flecks (gravel is fm and sub-angular)

Medium strength reddish brown slightly sandy silty CLAY

High strength reddish brown slightly fine sandy silty CLAY

Reddish brown and occasional pale grey silty CLAY

Medium strength reddish brown silty CLAY

Reddish brown silty CLAY

Reddish brown silty CLAY

High strength fissured reddish brown silty CLAY

Medium strength reddish brown mottled pale blue grey silty

CLAY

Medium strength reddish brown slightly sandy silty CLAY with

fine mudstone fragments

Checked and

Approved

Reddish brown and occasional pale grey silty CLAY

Page 79: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Approved Signatories:

Initials: kp

Test results relate only to the sample numbers shown above Date:

All samples connected with this report, incl any on 'hold' will be disposed off according to company policy. A copy of this policy is available on request. Sheet 3/3 MSF-11/R9

BS 1377 : Part 2 : 1990 : Clause 9

K4 SOILS

Location K&N Distribution Depot, Derby

Borehole / Trial

Pit No:

PARTICLE SIZE DISTRIBUTIONOur Report No:

0.025 58

90

75

100

100

-

WS507

Depth 1.50 - 2.00 m

17644

Project No: 1309

Visual Soil

Description

Reddish brown slightly sandy silty CLAY with traces of fine

mudstone fragments Sample Type/No

Sieving Sedimentation Test Method

Particle Size

mm% Passing

Particle Size

mm% Passing

BS 1377 : Part 2 : 1990

Sieving Clause 9.2

0.018 53

0.01450 100

Sedimentation Clause 9.5

63 100

0.035 65

125 100 0.049 71

0.010 42

Cobbles 0.0

28 100 0.007

48

37.5 100

14 100

37

0.005 32

0.004 28

10 100 0.003 25

20 100

0.001 236.3 100

5 98

3.35

81

D60870.3

1.18 94

0.6 91

0.425 89

97

0.212 83

Unit 8 Olds Close Olds Approach

Watford Herts WD18 9RU.

E-mail: [email protected]

N/A

0.15

D10

2 96

K.Phaure(Tech.Mgr) J.Phaure(Lab.Mgr)

Uniformity Coefficient0.063 73

K4 SOILS LABORATORY

Suitable Amount Of

Sample ReceivedYes

13/11/2014

Checked and Approved

2519

Grading Analysis

D100 125.0

Clay 23.9

Silt 48.7

Gravel 4.2

Sand 23.2

Sample Proportions

0.0

02

0.0

06

0.0

3

0.0

6

0.2

0.6

2

6

20

60

200

0

10

20

30

40

50

60

70

80

90

100

Perc

en

tag

e P

assin

g -

%

Particle Size - mm

CLAYSILT SAND GRAVEL

COBBLESFine Medium Coarse Fine Medium Coarse Fine Medium Coarse

Page 80: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Approved Signatories:

Initials: kp

Test results relate only to the sample numbers shown above Date:

All samples connected with this report, incl any on 'hold' will be disposed off according to company policy. A copy of this policy is available on request. Sheet 3/3 MSF-11/R9

BS 1377 : Part 2 : 1990 : Clause 9

K4 SOILS

Location K&N Distribution Depot, Derby

Borehole / Trial

Pit No:

PARTICLE SIZE DISTRIBUTIONOur Report No:

0.026 34

90

75

100

100

-

WS514

Depth 3.60 - 4.00 m

17644

Project No: 1309

Visual Soil

Description

Reddish brown sandy clayey SILT with occasional fm

mudstone fragments Sample Type/No

Sieving Sedimentation Test Method

Particle Size

mm% Passing

Particle Size

mm% Passing

BS 1377 : Part 2 : 1990

Sieving Clause 9.2

0.019 30

0.01450 100

Sedimentation Clause 9.5

63 100

0.037 37

125 100 0.051 41

0.010 25

Cobbles 0.0

28 100 0.007

27

37.5 100

14 100

21

0.005 17

0.004 13

10 98 0.003 13

20 100

0.002 116.3 94

5 91

3.35

48

D60580.3

1.18 80

0.6 70

0.425 65

88

0.212 51

Unit 8 Olds Close Olds Approach

Watford Herts WD18 9RU.

E-mail: [email protected]

N/A

0.15

D10

2 85

K.Phaure(Tech.Mgr) J.Phaure(Lab.Mgr)

Uniformity Coefficient0.063 42

K4 SOILS LABORATORY

Suitable Amount Of

Sample ReceivedYes

13/11/2014

Checked and Approved

2519

Grading Analysis

0.3

D100 125.0

Clay 11.8

Silt 29.7

Gravel 15.4

Sand 43.1

Sample Proportions

0.0

02

0.0

06

0.0

3

0.0

6

0.2

0.6

2

6

20

60

200

0

10

20

30

40

50

60

70

80

90

100

Perc

en

tag

e P

assin

g -

%

Particle Size - mm

CLAYSILT SAND GRAVEL

COBBLESFine Medium Coarse Fine Medium Coarse Fine Medium Coarse

Page 81: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Approved Signatories:

Initials: kp

Test results relate only to the sample numbers shown above Date:

All samples connected with this report, incl any on 'hold' will be disposed off according to company policy. A copy of this policy is available on request. Sheet 3/3 MSF-11/R9

BS 1377 : Part 2 : 1990 : Clause 9

K4 SOILS

Location K&N Distribution Depot, Derby

Borehole / Trial

Pit No:

PARTICLE SIZE DISTRIBUTIONOur Report No:

0.026 34

90

75

100

100

-

WS514

Depth 3.60 - 4.00 m

17644

Project No: 1309

Visual Soil

Description

Reddish brown sandy clayey SILT with occasional fm

mudstone fragments Sample Type/No

Sieving Sedimentation Test Method

Particle Size

mm% Passing

Particle Size

mm% Passing

BS 1377 : Part 2 : 1990

Sieving Clause 9.2

0.019 30

0.01450 100

Sedimentation Clause 9.5

63 100

0.037 37

125 100 0.051 41

0.010 25

Cobbles 0.0

28 100 0.007

27

37.5 100

14 100

21

0.005 17

0.004 13

10 98 0.003 13

20 100

0.002 116.3 94

5 91

3.35

48

D60580.3

1.18 80

0.6 70

0.425 65

88

0.212 51

Unit 8 Olds Close Olds Approach

Watford Herts WD18 9RU.

E-mail: [email protected]

N/A

0.15

D10

2 85

K.Phaure(Tech.Mgr) J.Phaure(Lab.Mgr)

Uniformity Coefficient0.063 42

K4 SOILS LABORATORY

Suitable Amount Of

Sample ReceivedYes

13/11/2014

Checked and Approved

2519

Grading Analysis

0.3

D100 125.0

Clay 11.8

Silt 29.7

Gravel 15.4

Sand 43.1

Sample Proportions

0.0

02

0.0

06

0.0

3

0.0

6

0.2

0.6

2

6

20

60

200

0

10

20

30

40

50

60

70

80

90

100

Perc

en

tag

e P

assin

g -

%

Particle Size - mm

CLAYSILT SAND GRAVEL

COBBLESFine Medium Coarse Fine Medium Coarse Fine Medium Coarse

Page 82: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Approved Signatories:

Initials: kp

Test results relate only to the sample numbers shown above Date:

All samples connected with this report, incl any on 'hold' will be disposed off according to company policy. A copy of this policy is available on request. Sheet 3/3 MSF-11/R9

BS 1377 : Part 2 : 1990 : Clause 9

K4 SOILS

Location K&N Distribution Depot, Derby

Borehole / Trial

Pit No:

PARTICLE SIZE DISTRIBUTIONOur Report No:

0.025 77

90

75

100

100

-

WS515

Depth 2.50 - 3.00 m

17644

Project No: 1309

Visual Soil

Description

Reddish brown slightly sandy very silty CLAY with traces of

fine mudstone fragments Sample Type/No

Sieving Sedimentation Test Method

Particle Size

mm% Passing

Particle Size

mm% Passing

BS 1377 : Part 2 : 1990

Sieving Clause 9.2

0.018 70

0.01350 100

Sedimentation Clause 9.5

63 100

0.034 85

125 100 0.048 89

0.010 55

Cobbles 0.0

28 100 0.007

62

37.5 100

14 100

48

0.005 39

0.004 34

10 100 0.003 29

20 100

0.001 256.3 100

5 100

3.35

93

D60990.3

1.18 100

0.6 100

0.425 100

100

0.212 96

Unit 8 Olds Close Olds Approach

Watford Herts WD18 9RU.

E-mail: [email protected]

N/A

0.15

D10

2 100

K.Phaure(Tech.Mgr) J.Phaure(Lab.Mgr)

Uniformity Coefficient0.063 91

K4 SOILS LABORATORY

Suitable Amount Of

Sample ReceivedYes

13/11/2014

Checked and Approved

2519

Grading Analysis

D100 125.0

Clay 26.7

Silt 63.8

Gravel 0.1

Sand 9.4

Sample Proportions

0.0

02

0.0

06

0.0

3

0.0

6

0.2

0.6

2

6

20

60

200

0

10

20

30

40

50

60

70

80

90

100

Perc

en

tag

e P

assin

g -

%

Particle Size - mm

CLAYSILT SAND GRAVEL

COBBLESFine Medium Coarse Fine Medium Coarse Fine Medium Coarse

Page 83: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Approved Signatories:

Initials: kp

Test results relate only to the sample numbers shown above Date:

All samples connected with this report, incl any on 'hold' will be disposed off according to company policy. A copy of this policy is available on request. Sheet 3/3 MSF-11/R9

BS 1377 : Part 2 : 1990 : Clause 9

K4 SOILS

Location K&N Distribution Depot, Derby

Borehole / Trial

Pit No:

PARTICLE SIZE DISTRIBUTIONOur Report No:

0.025 51

90

75

100

100

-

WS516

Depth 1.60 - 2.00 m

17644

Project No: 1309

Visual Soil

Description

Medium strength reddish brown sandy very silty CLAY with

traces of fine mudstone fragments Sample Type/No

Sieving Sedimentation Test Method

Particle Size

mm% Passing

Particle Size

mm% Passing

BS 1377 : Part 2 : 1990

Sieving Clause 9.2

0.018 45

0.01350 100

Sedimentation Clause 9.5

63 100

0.035 55

125 100 0.048 60

0.010 36

Cobbles 0.0

28 100 0.007

40

37.5 100

14 100

31

0.005 26

0.004 22

10 100 0.003 18

20 100

0.001 166.3 100

5 100

3.35

73

D60880.3

1.18 100

0.6 98

0.425 93

100

0.212 81

Unit 8 Olds Close Olds Approach

Watford Herts WD18 9RU.

E-mail: [email protected]

N/A

0.15

D10

2 100

K.Phaure(Tech.Mgr) J.Phaure(Lab.Mgr)

Uniformity Coefficient0.063 62

K4 SOILS LABORATORY

Suitable Amount Of

Sample ReceivedYes

13/11/2014

Checked and Approved

2519

Grading Analysis

D100 125.0

Clay 17.3

Silt 44.6

Gravel 0.0

Sand 38.1

Sample Proportions

0.0

02

0.0

06

0.0

3

0.0

6

0.2

0.6

2

6

20

60

200

0

10

20

30

40

50

60

70

80

90

100

Perc

en

tag

e P

assin

g -

%

Particle Size - mm

CLAYSILT SAND GRAVEL

COBBLESFine Medium Coarse Fine Medium Coarse Fine Medium Coarse

Page 84: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Approved Signatories:

Initials: kp

Test results relate only to the sample numbers shown above Date:

All samples connected with this report, incl any on 'hold' will be disposed off according to company policy. A copy of this policy is available on request. Sheet 3/3 MSF-11/R9

BS 1377 : Part 2 : 1990 : Clause 9

K4 SOILS

Location K&N Distribution Depot, Derby

Borehole / Trial

Pit No:

PARTICLE SIZE DISTRIBUTIONOur Report No:

0.024 82

90

75

100

100

-

WS517

Depth 1.45 - 2.00 m

17644

Project No: 1309

Visual Soil

Description

Reddish brown slightly sandy very silty CLAY with traces of

fm mudstone fragments Sample Type/No

Sieving Sedimentation Test Method

Particle Size

mm% Passing

Particle Size

mm% Passing

BS 1377 : Part 2 : 1990

Sieving Clause 9.2

0.017 77

0.01350 100

Sedimentation Clause 9.5

63 100

0.033 88

125 100 0.046 93

0.009 66

Cobbles 0.0

28 100 0.007

71

37.5 100

14 98

60

0.005 51

0.003 45

10 98 0.002 40

20 100

0.001 366.3 98

5 98

3.35

97

D60970.3

1.18 98

0.6 98

0.425 97

98

0.212 97

Unit 8 Olds Close Olds Approach

Watford Herts WD18 9RU.

E-mail: [email protected]

N/A

0.15

D10

2 98

K.Phaure(Tech.Mgr) J.Phaure(Lab.Mgr)

Uniformity Coefficient0.063 95

K4 SOILS LABORATORY

Suitable Amount Of

Sample ReceivedYes

13/11/2014

Checked and Approved

2519

Grading Analysis

D100 125.0

Clay 37.9

Silt 56.8

Gravel 2.5

Sand 2.8

Sample Proportions

0.0

02

0.0

06

0.0

3

0.0

6

0.2

0.6

2

6

20

60

200

0

10

20

30

40

50

60

70

80

90

100

Perc

en

tag

e P

assin

g -

%

Particle Size - mm

CLAYSILT SAND GRAVEL

COBBLESFine Medium Coarse Fine Medium Coarse Fine Medium Coarse

Page 85: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Client : Our Job/report no: Samples Rec : Testing Started:

Project name: Project No: Project Started: Date reported:

WS503

WS505

WS507

WS512

WS513

WS514

WS516

WS518

Initials

Test Report by K4 SOILS LABORATORY Unit 8 Olds Close Olds Approach Watford WD18 9RU Approved Signatories: K.Phaure (Tech.Mgr) J.Phaure (Lab.Mgr)

1.60 - 2.00Medium strength reddish brown slightly sandy silty CLAY with fine

mudstone fragments 28 1.99 1.56 32

NA1.94 20 5.2 179 Brittle 90

18.5 131 Plastic 66 NA

Checked and

approved

kp

Brittle 99 NA

1.54 24

1.96 50 4.0 198

5.1 142 Brittle 71 NA

NA

1.68 50

2519

Summary of Undrained Triaxial Compression Testing

BS 1377 : Part 7 : Clause 8 : 1990

Test Results relate only to the sample numbers shown above. All samples connected with this report, incl any on 'hold' will be stored and disposed off according to company policy. A copy of this policy is available on request.

3.40 - 3.70 Medium strength reddish brown slightly sandy silty CLAY 25 2.20 1.77

K4 SOILS

1.20 - 1.50 Medium strength reddish brown silty CLAY 24 1.92

16 2.26

3.70 - 4.00 Medium strength reddish brown mottled pale blue grey silty CLAY 25 2.15

BH / TP

No

Sample no /

ref

2.50 - 3.00

68 11.3 133

2.50 - 2.80Medium strength reddish brown slightly sandy silty CLAY with fine

mudstone fragments 20 2.02 19 107

1.72 74 18.4 88

.50 - 1.00 High strength fissured reddish brown silty CLAY 19 2.31

9.4241.68211.20 - 2.00

High strength reddish brown slightly fine sandy silty CLAY

2.02Very high strength brown slightly gravelly silty CLAY occasional with black

flecks (gravel is fm and sub-angular)

Compound

Compound

Plastic

Moisture

content

(%)

Lustre Consulting

K&N Distribution Depot, Derby

Dry density

(Mg/m3)

Bulk Density

(Mg/m3)

17644

Strain at

failure (%)

1309

Phi (deg)

Shear

Strength

(kPa)

Cell

Pressure

(kPa)

Mode of

failure

Max Deviator

Stress (kPa)

04/11/2014-

Sample

depth (m)Description

NA207Compound414

14/10/2014 27/10/2014

67 NA

44

54 NA

Page 86: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Project name: Samples Received:

Project Started:

Client: Testing Started:

Project no: Our job /report no: Date Reported:

Sample no: Depth (m):

Specimen

Approved Signatories: K.Phaure(Tech.Mgr)

Initials: kp

Test results relate only to the sample numbers shown above Date:

All samples connected with this report, incl any on 'hold' will be disposed off according to Company Policy. A copy of this policy is available on request. MSF-11/R9 Sheet 2/2

Shear Strength

Parameters

C 207 kPa

Phi 0.0 °

Sample Condition Undisturbed

1Sample Details

Height mm 168.0

Diameter mm

Dry Density Mg/m³ 1.68

84.0

Moisture Content % 21

Cell Pressure kPa 24

Rate of Axial Displacement %/min 2.00

Membrane Correction kPa 0.51

Membrane Thickness mm 0.2

kPa 207

Maximum Deviator Stress kPa 414

Strain at Failure % 9.4

K4 SOILS Report of Undrained Triaxial Compression Test

BS 1377 : Part 7 : 1990 Clause 8.0

14/10/2014

15/10/2014

K&N Distribution Depot, Derby

Po

sitio

n a

nd

ori

en

tatio

n w

ith

in

the

ori

gin

al sa

mp

le

Test Details

Bulk Density Mg/m³ 2.02

27/10/2014

J.Phaure(Lab.Mgr)

Checked and Approved

Soil Description:

BH / TP no:

Lustre Consulting

1309 17644 04/11/2014

2519

Very high strength brown slightly gravelly silty CLAY occasional with black flecks (gravel is fm and sub-angular)

1.20

K4 SOILS LABORATORYUnit 8, Olds Close, Watford, Herts, WD18 9RU.

Tel:01923711288 Fax:01923711311

E-mail: [email protected] 04/11/2014

WS503

Mode of Failure Compound

Shear Strength

-50

0

50

100

150

200

250

300

350

400

450

0 2 4 6 8 10 12 14

Devia

tor

Str

ess

- k

Pa

Strain - %

Specimen 1

0

100

200

300

400

500

0 100 200 300 400 500 600 700 800 900 1000

Sh

ear

Str

ess -

kP

a

Normal Stress - kPa

Page 87: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Project name: Samples Received:

Project Started:

Client: Testing Started:

Project no: Our job /report no: Date Reported:

Sample no: Depth (m):

Specimen

Approved Signatories: K.Phaure(Tech.Mgr)

Initials: kp

Test results relate only to the sample numbers shown above Date:

All samples connected with this report, incl any on 'hold' will be disposed off according to Company Policy. A copy of this policy is available on request. MSF-11/R9 Sheet 2/2

Shear Strength

Parameters

C 66 kPa

Phi 0.0 °

Sample Condition Undisturbed

1Sample Details

Height mm 100.0

Diameter mm

Dry Density Mg/m³ 1.77

50.0

Moisture Content % 25

Cell Pressure kPa 68

Rate of Axial Displacement %/min 2.00

Membrane Correction kPa 0.99

Membrane Thickness mm 0.2

kPa 66

Maximum Deviator Stress kPa 133

Strain at Failure % 11.3

K4 SOILS Report of Undrained Triaxial Compression Test

BS 1377 : Part 7 : 1990 Clause 8.0

14/10/2014

15/10/2014

K&N Distribution Depot, Derby

Po

sitio

n a

nd

ori

en

tatio

n w

ith

in

the

ori

gin

al sa

mp

le

Test Details

Bulk Density Mg/m³ 2.20

28/10/2014

J.Phaure(Lab.Mgr)

Checked and Approved

Soil Description:

BH / TP no:

Lustre Consulting

1309 17644 04/11/2014

2519

Medium strength reddish brown slightly sandy silty CLAY

3.40

K4 SOILS LABORATORYUnit 8, Olds Close, Watford, Herts, WD18 9RU.

Tel:01923711288 Fax:01923711311

E-mail: [email protected] 04/11/2014

WS505

Mode of Failure Compound

Shear Strength

-20

0

20

40

60

80

100

120

140

0 2 4 6 8 10 12 14 16

Devia

tor

Str

ess

- k

Pa

Strain - %

Specimen 1

0

50

100

150

200

250

0 50 100 150 200 250 300 350 400 450 500

Sh

ear

Str

ess -

kP

a

Normal Stress - kPa

Page 88: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Project name: Samples Received:

Project Started:

Client: Testing Started:

Project no: Our job /report no: Date Reported:

Sample no: Depth (m):

Specimen

Approved Signatories: K.Phaure(Tech.Mgr)

Initials: kp

Test results relate only to the sample numbers shown above Date:

All samples connected with this report, incl any on 'hold' will be disposed off according to Company Policy. A copy of this policy is available on request. MSF-11/R9 Sheet 2/2

Shear Strength

Parameters

C 66 kPa

Phi 0.0 °

Sample Condition Undisturbed

1Sample Details

Height mm 100.0

Diameter mm

Dry Density Mg/m³ 1.77

50.0

Moisture Content % 25

Cell Pressure kPa 68

Rate of Axial Displacement %/min 2.00

Membrane Correction kPa 0.99

Membrane Thickness mm 0.2

kPa 66

Maximum Deviator Stress kPa 133

Strain at Failure % 11.3

K4 SOILS Report of Undrained Triaxial Compression Test

BS 1377 : Part 7 : 1990 Clause 8.0

14/10/2014

15/10/2014

K&N Distribution Depot, Derby

Po

sitio

n a

nd

ori

en

tatio

n w

ith

in

the

ori

gin

al sa

mp

le

Test Details

Bulk Density Mg/m³ 2.20

28/10/2014

J.Phaure(Lab.Mgr)

Checked and Approved

Soil Description:

BH / TP no:

Lustre Consulting

1309 17644 04/11/2014

2519

Medium strength reddish brown slightly sandy silty CLAY

3.40

K4 SOILS LABORATORYUnit 8, Olds Close, Watford, Herts, WD18 9RU.

Tel:01923711288 Fax:01923711311

E-mail: [email protected] 04/11/2014

WS505

Mode of Failure Compound

Shear Strength

-20

0

20

40

60

80

100

120

140

0 2 4 6 8 10 12 14 16

Devia

tor

Str

ess

- k

Pa

Strain - %

Specimen 1

0

50

100

150

200

250

0 50 100 150 200 250 300 350 400 450 500

Sh

ear

Str

ess -

kP

a

Normal Stress - kPa

Page 89: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Project name: Samples Received:

Project Started:

Client: Testing Started:

Project no: Our job /report no: Date Reported:

Sample no: Depth (m):

Specimen

Approved Signatories: K.Phaure(Tech.Mgr)

Initials: kp

Test results relate only to the sample numbers shown above Date:

All samples connected with this report, incl any on 'hold' will be disposed off according to Company Policy. A copy of this policy is available on request. MSF-11/R9 Sheet 2/2

Shear Strength

Parameters

C 99 kPa

Phi 0.0 °

Sample Condition Undisturbed

1Sample Details

Height mm 112.0

Diameter mm

Dry Density Mg/m³ 1.96

58.0

Moisture Content % 16

Cell Pressure kPa 50

Rate of Axial Displacement %/min 2.00

Membrane Correction kPa 0.37

Membrane Thickness mm 0.2

kPa 99

Maximum Deviator Stress kPa 198

Strain at Failure % 4.0

K4 SOILS Report of Undrained Triaxial Compression Test

BS 1377 : Part 7 : 1990 Clause 8.0

14/10/2014

15/10/2014

K&N Distribution Depot, Derby

Po

sitio

n a

nd

ori

en

tatio

n w

ith

in

the

ori

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al sa

mp

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Test Details

Bulk Density Mg/m³ 2.26

28/10/2014

J.Phaure(Lab.Mgr)

Checked and Approved

Soil Description:

BH / TP no:

Lustre Consulting

1309 17644 04/11/2014

2519

High strength reddish brown slightly fine sandy silty CLAY

2.50

K4 SOILS LABORATORYUnit 8, Olds Close, Watford, Herts, WD18 9RU.

Tel:01923711288 Fax:01923711311

E-mail: [email protected] 04/11/2014

WS507

Mode of Failure Brittle

Shear Strength

-50

0

50

100

150

200

250

0 1 2 3 4 5 6 7

Devia

tor

Str

ess

- k

Pa

Strain - %

Specimen 1

0

50

100

150

200

250

0 50 100 150 200 250 300 350 400 450 500

Sh

ear

Str

ess -

kP

a

Normal Stress - kPa

Page 90: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Project name: Samples Received:

Project Started:

Client: Testing Started:

Project no: Our job /report no: Date Reported:

Sample no: Depth (m):

Specimen

Approved Signatories: K.Phaure(Tech.Mgr)

Initials: kp

Test results relate only to the sample numbers shown above Date:

All samples connected with this report, incl any on 'hold' will be disposed off according to Company Policy. A copy of this policy is available on request. MSF-11/R9 Sheet 2/2

27/10/2014

J.Phaure(Lab.Mgr)

Checked and Approved

Soil Description:

BH / TP no:

Lustre Consulting

1309 17644 04/11/2014

2519

Medium strength reddish brown silty CLAY

1.20

K4 SOILS LABORATORYUnit 8, Olds Close, Watford, Herts, WD18 9RU.

Tel:01923711288 Fax:01923711311

E-mail: [email protected] 04/11/2014

WS512

Mode of Failure Brittle

Shear Strength

K4 SOILS Report of Undrained Triaxial Compression Test

BS 1377 : Part 7 : 1990 Clause 8.0

14/10/2014

15/10/2014

K&N Distribution Depot, Derby

Po

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Test Details

Bulk Density Mg/m³ 1.92

kPa 71

Maximum Deviator Stress kPa 142

Strain at Failure % 5.1

Cell Pressure kPa 24

Rate of Axial Displacement %/min 2.00

Membrane Correction kPa 0.36

Membrane Thickness mm 0.2

Height mm 146.0

Diameter mm

Dry Density Mg/m³ 1.54

73.0

Moisture Content % 24

Sample Condition Undisturbed

1Sample Details

Shear Strength

Parameters

C 71 kPa

Phi 0.0 °

-20

0

20

40

60

80

100

120

140

160

0 1 2 3 4 5 6 7

Devia

tor

Str

ess

- k

Pa

Strain - %

Specimen 1

0

50

100

150

200

250

0 50 100 150 200 250 300 350 400 450 500

Sh

ear

Str

ess -

kP

a

Normal Stress - kPa

Page 91: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Project name: Samples Received:

Project Started:

Client: Testing Started:

Project no: Our job /report no: Date Reported:

Sample no: Depth (m):

Specimen

Approved Signatories: K.Phaure(Tech.Mgr)

Initials: kp

Test results relate only to the sample numbers shown above Date:

All samples connected with this report, incl any on 'hold' will be disposed off according to Company Policy. A copy of this policy is available on request. MSF-11/R9 Sheet 2/2

27/10/2014

J.Phaure(Lab.Mgr)

Checked and Approved

Soil Description:

BH / TP no:

Lustre Consulting

1309 17644 04/11/2014

2519

Medium strength reddish brown mottled pale blue grey silty CLAY

3.70

K4 SOILS LABORATORYUnit 8, Olds Close, Watford, Herts, WD18 9RU.

Tel:01923711288 Fax:01923711311

E-mail: [email protected] 04/11/2014

WS513 -

Mode of Failure Compound

Shear Strength

K4 SOILS Report of Undrained Triaxial Compression Test

BS 1377 : Part 7 : 1990 Clause 8.0

14/10/2014

15/10/2014

K&N Distribution Depot, Derby

Po

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nd

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in

the

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al sa

mp

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Test Details

Bulk Density Mg/m³ 2.15

kPa 44

Maximum Deviator Stress kPa 88

Strain at Failure % 18.4

Cell Pressure kPa 74

Rate of Axial Displacement %/min 2.00

Membrane Correction kPa 1.18

Membrane Thickness mm 0.2

Height mm 122.0

Diameter mm

Dry Density Mg/m³ 1.72

61.0

Moisture Content % 25

Sample Condition Undisturbed

1Sample Details

Shear Strength

Parameters

C 44 kPa

Phi 0.0 °

-10

0

10

20

30

40

50

60

70

80

90

100

0 5 10 15 20 25

Devia

tor

Str

ess

- k

Pa

Strain - %

Specimen 1

0

50

100

150

200

250

0 50 100 150 200 250 300 350 400 450 500

Sh

ear

Str

ess -

kP

a

Normal Stress - kPa

Page 92: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Project name: Samples Received:

Project Started:

Client: Testing Started:

Project no: Our job /report no: Date Reported:

Sample no: Depth (m):

Specimen

Approved Signatories: K.Phaure(Tech.Mgr)

Initials: kp

Test results relate only to the sample numbers shown above Date:

All samples connected with this report, incl any on 'hold' will be disposed off according to Company Policy. A copy of this policy is available on request. MSF-11/R9 Sheet 2/2

27/10/2014

J.Phaure(Lab.Mgr)

Checked and Approved

Soil Description:

BH / TP no:

Lustre Consulting

1309 17644 04/11/2014

2519

Medium strength reddish brown mottled pale blue grey silty CLAY

3.70

K4 SOILS LABORATORYUnit 8, Olds Close, Watford, Herts, WD18 9RU.

Tel:01923711288 Fax:01923711311

E-mail: [email protected] 04/11/2014

WS513 -

Mode of Failure Compound

Shear Strength

K4 SOILS Report of Undrained Triaxial Compression Test

BS 1377 : Part 7 : 1990 Clause 8.0

14/10/2014

15/10/2014

K&N Distribution Depot, Derby

Po

sitio

n a

nd

ori

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tatio

n w

ith

in

the

ori

gin

al sa

mp

le

Test Details

Bulk Density Mg/m³ 2.15

kPa 44

Maximum Deviator Stress kPa 88

Strain at Failure % 18.4

Cell Pressure kPa 74

Rate of Axial Displacement %/min 2.00

Membrane Correction kPa 1.18

Membrane Thickness mm 0.2

Height mm 122.0

Diameter mm

Dry Density Mg/m³ 1.72

61.0

Moisture Content % 25

Sample Condition Undisturbed

1Sample Details

Shear Strength

Parameters

C 44 kPa

Phi 0.0 °

-10

0

10

20

30

40

50

60

70

80

90

100

0 5 10 15 20 25

Devia

tor

Str

ess

- k

Pa

Strain - %

Specimen 1

0

50

100

150

200

250

0 50 100 150 200 250 300 350 400 450 500

Sh

ear

Str

ess -

kP

a

Normal Stress - kPa

Page 93: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Project name: Samples Received:

Project Started:

Client: Testing Started:

Project no: Our job /report no: Date Reported:

Sample no: Depth (m):

Specimen

Approved Signatories: K.Phaure(Tech.Mgr)

Initials: kp

Test results relate only to the sample numbers shown above Date:

All samples connected with this report, incl any on 'hold' will be disposed off according to Company Policy. A copy of this policy is available on request. MSF-11/R9 Sheet 2/2

27/10/2014

J.Phaure(Lab.Mgr)

Checked and Approved

Soil Description:

BH / TP no:

Lustre Consulting

1309 17644 04/11/2014

2519

Medium strength reddish brown slightly sandy silty CLAY with fine mudstone fragments

1.60

K4 SOILS LABORATORYUnit 8, Olds Close, Watford, Herts, WD18 9RU.

Tel:01923711288 Fax:01923711311

E-mail: [email protected] 04/11/2014

WS516 -

Mode of Failure Plastic

Shear Strength

K4 SOILS Report of Undrained Triaxial Compression Test

BS 1377 : Part 7 : 1990 Clause 8.0

14/10/2014

15/10/2014

K&N Distribution Depot, Derby

Po

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nd

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in

the

ori

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al sa

mp

le

Test Details

Bulk Density Mg/m³ 1.99

kPa 65

Maximum Deviator Stress kPa 131

Strain at Failure % 18.5

Cell Pressure kPa 32

Rate of Axial Displacement %/min 2.00

Membrane Correction kPa 0.97

Membrane Thickness mm 0.2

Height mm 142.0

Diameter mm

Dry Density Mg/m³ 1.56

74.0

Moisture Content % 28

Sample Condition Undisturbed

1Sample Details

Shear Strength

Parameters

C 65 kPa

Phi 0.0 °

-20

0

20

40

60

80

100

120

140

0 5 10 15 20 25

Devia

tor

Str

ess

- k

Pa

Strain - %

Specimen 1

0

50

100

150

200

250

0 50 100 150 200 250 300 350 400 450 500

Sh

ear

Str

ess -

kP

a

Normal Stress - kPa

Page 94: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Project name: Samples Received:

Project Started:

Client: Testing Started:

Project no: Our job /report no: Date Reported:

Sample no: Depth (m):

Specimen

Approved Signatories: K.Phaure(Tech.Mgr)

Initials: kp

Test results relate only to the sample numbers shown above Date:

All samples connected with this report, incl any on 'hold' will be disposed off according to Company Policy. A copy of this policy is available on request. MSF-11/R9 Sheet 2/2

Shear Strength

Parameters

C 90 kPa

Phi 0.0 °

Sample Condition Undisturbed

1Sample Details

Height mm 160.0

Diameter mm

Dry Density Mg/m³ 1.94

80.0

Moisture Content % 19

Cell Pressure kPa 20

Rate of Axial Displacement %/min 2.00

Membrane Correction kPa 0.33

Membrane Thickness mm 0.2

kPa 90

Maximum Deviator Stress kPa 179

Strain at Failure % 5.2

K4 SOILS Report of Undrained Triaxial Compression Test

BS 1377 : Part 7 : 1990 Clause 8.0

14/10/2014

15/10/2014

K&N Distribution Depot, Derby

Po

sitio

n a

nd

ori

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tatio

n w

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in

the

ori

gin

al sa

mp

le

Test Details

Bulk Density Mg/m³ 2.31

27/10/2014

J.Phaure(Lab.Mgr)

Checked and Approved

Soil Description:

BH / TP no:

Lustre Consulting

1309 17644 04/11/2014

2519

High strength fissured reddish brown silty CLAY

0.50

K4 SOILS LABORATORYUnit 8, Olds Close, Watford, Herts, WD18 9RU.

Tel:01923711288 Fax:01923711311

E-mail: [email protected] 04/11/2014

WS518

Mode of Failure Brittle

Shear Strength

-20

0

20

40

60

80

100

120

140

160

180

200

0 1 2 3 4 5 6 7

Devia

tor

Str

ess

- k

Pa

Strain - %

Specimen 1

0

50

100

150

200

250

0 50 100 150 200 250 300 350 400 450 500

Sh

ear

Str

ess -

kP

a

Normal Stress - kPa

Page 95: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Project name: Samples Received:

Project Started:

Client: Testing Started:

Project no: Our job /report no: Date Reported:

Sample no: Depth (m):

Specimen

Approved Signatories: K.Phaure(Tech.Mgr)

Initials: kp

Test results relate only to the sample numbers shown above Date:

All samples connected with this report, incl any on 'hold' will be disposed off according to Company Policy. A copy of this policy is available on request. MSF-11/R9 Sheet 2/2

Shear Strength

Parameters

C 90 kPa

Phi 0.0 °

Sample Condition Undisturbed

1Sample Details

Height mm 160.0

Diameter mm

Dry Density Mg/m³ 1.94

80.0

Moisture Content % 19

Cell Pressure kPa 20

Rate of Axial Displacement %/min 2.00

Membrane Correction kPa 0.33

Membrane Thickness mm 0.2

kPa 90

Maximum Deviator Stress kPa 179

Strain at Failure % 5.2

K4 SOILS Report of Undrained Triaxial Compression Test

BS 1377 : Part 7 : 1990 Clause 8.0

14/10/2014

15/10/2014

K&N Distribution Depot, Derby

Po

sitio

n a

nd

ori

en

tatio

n w

ith

in

the

ori

gin

al sa

mp

le

Test Details

Bulk Density Mg/m³ 2.31

27/10/2014

J.Phaure(Lab.Mgr)

Checked and Approved

Soil Description:

BH / TP no:

Lustre Consulting

1309 17644 04/11/2014

2519

High strength fissured reddish brown silty CLAY

0.50

K4 SOILS LABORATORYUnit 8, Olds Close, Watford, Herts, WD18 9RU.

Tel:01923711288 Fax:01923711311

E-mail: [email protected] 04/11/2014

WS518

Mode of Failure Brittle

Shear Strength

-20

0

20

40

60

80

100

120

140

160

180

200

0 1 2 3 4 5 6 7

Devia

tor

Str

ess

- k

Pa

Strain - %

Specimen 1

0

50

100

150

200

250

0 50 100 150 200 250 300 350 400 450 500

Sh

ear

Str

ess -

kP

a

Normal Stress - kPa

Page 96: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

APPENDIX E

ENVIRONMENTAL

ASSESSMENT

Page 97: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

SOM = 1% SOM = 1% 10 0 0 0 0 0 0 0 0 0 0 0 0.007

HUMAN HEALTH QUANTITATIVE RISK ASSESSMENT - SOILS SOM = 2.5%SOM = 2.5%

MADE GROUND SOM = 6%

1309 2.784762

K&N Distribution Depot, Draycott in the Clay SOM = 2.5%

AWS030.35 AWS040.32 AWS050.20 AWS060.50 AWS070.30 AWS070.60 AWS090.20 AWS090.40 AWS110.50 AWS120.20 SP10.50 TP10.30 - 0.50

AWS03 AWS04 AWS05 AWS06 AWS07 AWS07 AWS09 AWS09 AWS11 AWS12 SP1 TP1

0.35 0.32 0.20 0.50 0.30 0.60 0.20 0.40 0.50 0.20 0.50 0.30 - 0.50

Asbestos Screen N/A N/A N/A N/A 34 Detected 0 Not Detected Not Detected Not Detected Not Detected Not Detected Not Detected Not Detected Not Detected Not Detected Not Detected Not Detected Not Detected

pH no units 7.30 7.84 9.10 24 No Criteria 0 - - 7.4 - - 7.7 - 7.3 7.6 7.5 9.1 8.1

Total Cyanide mg/kg <LOD <LOD <LOD 22 53.00 0 - - < 2 - - < 2 - < 2 < 2 < 2 < 2 < 2

Total Organic Carbon (TOC) mg/kg 0.30 1.62 3.70 22 No Criteria 0 - - 1 - - < 0.1 - 0.5 3 3.4 1.1 3.7

37 Arsenic mg/kg 2.00 9.36 23.00 22 37.00 0 - - 2 - - 22 - 3 16 5 4 18

Water Soluble Sulphate as SO4 (2:1) mg/kg 0.02 0.35 2.24 24 No Criteria 0 - - 0.02 - - 0.07 - 0.03 0.1 0.35 0.09 0.1

26 Cadmium mg/kg 0.50 1.06 2.40 22 26.00 0 - - 1.6 - - 0.7 - < 0.5 < 0.5 < 0.5 1 0.5

Chromium mg/kg 14.00 24.45 35.00 22 3000.00 0 - - 23 - - 20 - 29 19 22 30 30

Copper mg/kg 10.00 40.95 90.00 22 2330.00 0 - - 74 - - 52 - 21 90 38 39 75

200 Lead mg/kg 11.00 53.95 122.00 22 200.00 0 - - 67 - - 44 - 15 20 51 52 76

Mercury mg/kg <LOD <LOD <LOD 22 170.00 0 - - < 1 - - < 1 - < 1 < 1 < 1 < 1 < 1

Nickel mg/kg 15.00 33.00 60.00 22 130.00 0 - - 29 - - 36 - 25 60 36 34 45

Selenium mg/kg <LOD <LOD <LOD 22 350.00 0 - - < 3 - - < 3 - < 3 < 3 < 3 < 3 < 3

Zinc mg/kg 56.00 144.27 347.00 22 3750.00 0 - - 132 - - 64 - 88 186 87 165 126

Naphthalene mg/kg 0.40 0.40 0.40 22 3.70 0 - - < 0.1 - - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Acenaphthylene mg/kg 0.27 0.27 0.27 22 400.00 0 - - < 0.1 - - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Acenaphthene mg/kg 0.50 0.50 0.50 22 480.00 0 - - < 0.1 - - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Fluorene mg/kg 2.99 2.99 2.99 22 380.00 0 - - < 0.1 - - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Phenanthrene mg/kg 0.11 0.86 3.41 22 200.00 0 - - < 0.1 - - < 0.1 - < 0.1 < 0.1 0.3 < 0.1 0.12

Anthracene mg/kg 0.11 0.19 0.31 22 4900.00 0 - - < 0.1 - - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Fluoranthene mg/kg 0.18 1.11 5.70 22 460.00 0 - - < 0.1 - - < 0.1 - < 0.1 < 0.1 0.72 < 0.1 0.37

Pyrene mg/kg 0.27 0.97 4.41 22 1000.00 0 - - < 0.1 - - < 0.1 - < 0.1 < 0.1 0.67 < 0.1 0.33

Benzo(a)anthracene mg/kg 0.12 0.65 2.55 22 4.70 0 - - < 0.1 - - < 0.1 - < 0.1 < 0.1 0.33 < 0.1 0.12

Chrysene mg/kg 0.13 0.73 3.48 22 8.00 0 - - < 0.1 - - < 0.1 - < 0.1 < 0.1 0.36 < 0.1 0.18

Benzo(b)fluoranthene mg/kg 0.15 0.83 4.19 22 6.50 0 - - < 0.1 - - < 0.1 - < 0.1 < 0.1 0.45 < 0.1 0.16

Benzo(k)fluoranthene mg/kg 0.11 0.47 1.51 22 9.60 0 - - < 0.1 - - < 0.1 - < 0.1 < 0.1 0.14 < 0.1 < 0.1

5 Benzo(a)pyrene mg/kg 0.19 0.69 2.51 22 5.00 0 - - < 0.1 - - < 0.1 - < 0.1 < 0.1 0.32 < 0.1 < 0.1

Indeno(1,2,3-cd)pyrene mg/kg 0.13 0.65 1.62 22 3.90 0 - - < 0.1 - - < 0.1 - < 0.1 < 0.1 0.19 < 0.1 < 0.1

Di-benzo(a,h)anthracene mg/kg 0.33 0.33 0.33 22 0.86 0 - - < 0.1 - - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Benzo(ghi)perylene mg/kg 0.11 0.37 1.29 22 46.00 0 - - < 0.1 - - < 0.1 - < 0.1 < 0.1 0.18 < 0.1 < 0.1

TPH CWG - Aliphatic >C5 - C6 mg/kg 0.06 0.06 0.06 22 55.00 0 - - < 0.01 - - < 0.01 - < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

TPH CWG - Aliphatic >C6 - C8 mg/kg 0.28 4.59 8.90 22 160.00 0 - - < 0.05 - - < 0.05 - < 0.05 < 0.05 < 0.05 < 0.05 < 0.05

TPH CWG - Aliphatic >C8 - C10 mg/kg 3.00 54.00 105.00 22 46.00 1 - - < 1 - - < 1 - < 1 < 1 < 1 < 1 < 1

TPH CWG - Aliphatic >C10 - C12 mg/kg 302.00 302.00 302.00 22 230.00 1 - - < 1 - - < 1 - < 1 < 1 < 1 < 1 < 1

TPH CWG - Aliphatic >C12 - C16 mg/kg 8.00 817.00 1626.00 22 1700.00 0 - - < 1 - - < 1 - < 1 < 1 < 1 < 1 < 1

TPH CWG - Aliphatic >C16 - C21 mg/kg 2.00 621.33 1850.00 22 64000.00 0 - - < 1 - - < 1 - 2 < 1 < 1 < 1 < 1

TPH CWG - Aliphatic >C21 - C34 mg/kg 8.00 203.00 560.00 22 64000.00 0 - - < 6 - - < 6 - < 6 < 6 8 < 6 < 6

TPH CWG - Aromatic >C5 - C7 mg/kg <LOD <LOD <LOD 22 130.00 0 - - < 0.01 - - < 0.01 - < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

TPH CWG - Aromatic >C7 - C8 mg/kg <LOD <LOD <LOD 22 270.00 0 - - < 0.05 - - < 0.05 - < 0.05 < 0.05 < 0.05 < 0.05 < 0.05

TPH CWG - Aromatic >C8 - C10 mg/kg 10.00 10.00 10.00 22 65.00 0 - - < 1 - - < 1 - < 1 < 1 < 1 < 1 < 1

TPH CWG - Aromatic >C10 - C12 mg/kg 130.00 130.00 130.00 22 160.00 0 - - < 1 - - < 1 - < 1 < 1 < 1 < 1 < 1

TPH CWG - Aromatic >C12 - C16 mg/kg 1.00 379.00 1134.00 22 310.00 1 - - < 1 - - < 1 - < 1 < 1 < 1 < 1 < 1

TPH CWG - Aromatic >C16 - C21 mg/kg 9.00 327.00 1270.00 22 480.00 1 - - < 1 - - < 1 - < 1 < 1 9 < 1 < 1

TPH CWG - Aromatic >C21 - C35 mg/kg 15.00 137.00 423.00 22 1100.00 0 - - < 6 - - < 6 - < 6 < 6 15 < 6 < 6

0.9 Benzene mg/kg <LOD <LOD <LOD 22 0.87 0 - - < 2 - - < 2 - < 2 < 2 < 2 < 2 < 2

Toluene mg/kg 0.01 0.01 0.01 22 610.00 0 - - < 5 - - < 5 - < 5 < 5 < 5 < 5 0.007

Ethylbenzene mg/kg <LOD <LOD <LOD 22 350.00 0 - - < 10 - - < 10 - < 10 < 10 < 10 < 10 < 10

m & p-xylene mg/kg <LOD <LOD <LOD 22 230.00 0 - - < 10 - - < 10 - < 10 < 10 < 10 < 10 < 10

o-Xylene mg/kg <LOD <LOD <LOD 22 250.00 0 - - < 10 - - < 10 - < 10 < 10 < 10 < 10 < 10

Monohydric Phenols mg/kg <LOD <LOD <LOD 22 420.00 0 - - < 2 - - < 2 - < 2 < 2 < 2 < 2 < 2

Dichlorodifluoromethane mg/kg <LOD <LOD <LOD 8 No Criteria 0 - - - - - < 5 - < 5 - - - -

Vinyl Chloride mg/kg <LOD <LOD <LOD 8 0.00 0 - - - - - < 5 - < 5 - - - -

Chloromethane mg/kg <LOD <LOD <LOD 8 0.01 0 - - - - - < 10 - < 10 - - - -

Chloroethane mg/kg <LOD <LOD <LOD 8 11.00 0 - - - - - < 5 - < 5 - - - -

Bromomethane mg/kg <LOD <LOD <LOD 8 No Criteria 0 - - - - - < 10 - < 10 - - - -

Trichlorofluoromethane mg/kg <LOD <LOD <LOD 8 No Criteria 0 - - - - - < 5 - < 5 - - - -

1,1-Dichloroethene mg/kg <LOD <LOD <LOD 8 0.40 0 - - - - - < 5 - < 5 - - - -

MTBE mg/kg <LOD <LOD <LOD 22 84.00 0 - - < 5 - - < 5 - < 5 < 5 < 5 < 5 < 5

trans-1,2-Dichloroethene mg/kg <LOD <LOD <LOD 8 0.34 0 - - - - - < 5 - < 5 - - - -

1,1-Dichloroethane mg/kg <LOD <LOD <LOD 8 3.90 0 - - - - - < 5 - < 5 - - - -

cis-1,2-Dichloroethene mg/kg <LOD <LOD <LOD 8 0.19 0 - - - - - < 5 - < 5 - - - -

2,2-Dichloropropane mg/kg <LOD <LOD <LOD 8 No Criteria 0 - - - - - < 5 - < 5 - - - -

Chloroform mg/kg <LOD <LOD <LOD 8 1.30 0 - - - - - < 5 - < 5 - - - -

SGVs & GACs

Residential

SGVs, GACs & C4SLs

SOM = 2.5%

Assessment Criteria Source:

Soil Organic Matter (%):

Assessment Scenario:

ASSESSMENT

CRITERIA

No. >

ACDETERMINAND MINIMUM AVERAGE MAXIMUM

No. of

TESTSUNITS

Page 98: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

HUMAN HEALTH QUANTITATIVE RISK ASSESSMENT - SOILS SOM = 2.5%SOM = 2.5%

MADE GROUND SOM = 6%

1309 2.784762

K&N Distribution Depot, Draycott in the Clay SOM = 2.5%

AWS030.35 AWS040.32 AWS050.20 AWS060.50 AWS070.30 AWS070.60 AWS090.20 AWS090.40 AWS110.50 AWS120.20 SP10.50 TP10.30 - 0.50

AWS03 AWS04 AWS05 AWS06 AWS07 AWS07 AWS09 AWS09 AWS11 AWS12 SP1 TP1

0.35 0.32 0.20 0.50 0.30 0.60 0.20 0.40 0.50 0.20 0.50 0.30 - 0.50

SGVs & GACs

Residential

SGVs, GACs & C4SLs

SOM = 2.5%

Assessment Criteria Source:

Soil Organic Matter (%):

Assessment Scenario:

ASSESSMENT

CRITERIA

No. >

ACDETERMINAND MINIMUM AVERAGE MAXIMUM

No. of

TESTSUNITS

Bromochloromethane mg/kg <LOD <LOD <LOD 8 No Criteria 0 - - - - - < 5 - < 5 - - - -

1,1,1-Trichloroethane mg/kg <LOD <LOD <LOD 8 13.00 0 - - - - - < 5 - < 5 - - - -

1,1-Dichloropropene mg/kg <LOD <LOD <LOD 8 No Criteria 0 - - - - - < 10 - < 10 - - - -

Carbon Tetrachloride mg/kg <LOD <LOD <LOD 8 0.04 0 - - - - - < 5 - < 5 - - - -

1,2-Dichloroethane mg/kg <LOD <LOD <LOD 8 0.01 0 - - - - - < 5 - < 5 - - - -

Benzene mg/kg <LOD <LOD <LOD 22 0.33 0 - - < 2 - - < 2 - < 2 < 2 < 2 < 2 < 2

1,2-Dichloropropane mg/kg <LOD <LOD <LOD 8 0.04 0 - - - - - < 5 - < 5 - - - -

Trichloroethene mg/kg 0.28 0.28 0.28 8 0.22 1 - - - - - < 5 - < 5 - - - -

Bromodichloromethane mg/kg <LOD <LOD <LOD 8 0.03 0 - - - - - < 5 - < 5 - - - -

Dibromomethane mg/kg <LOD <LOD <LOD 8 No Criteria 0 - - - - - < 5 - < 5 - - - -

TAME mg/kg <LOD <LOD <LOD 8 No Criteria 0 - - - - - < 5 - < 5 - - - -

cis-1,3-Dichloropropene mg/kg <LOD <LOD <LOD 8 No Criteria 0 - - - - - < 5 - < 5 - - - -

Toluene mg/kg 0.01 0.01 0.01 22 610.00 0 - - < 5 - - < 5 - < 5 < 5 < 5 < 5 0.007

trans-1,3-Dichloropropene mg/kg <LOD <LOD <LOD 8 No Criteria 0 - - - - - < 5 - < 5 - - - -

1,1,2-Trichloroethane mg/kg <LOD <LOD <LOD 8 1.20 0 - - - - - < 10 - < 10 - - - -

1,3-Dichloropropane mg/kg <LOD <LOD <LOD 8 No Criteria 0 - - - - - < 5 - < 5 - - - -

Tetrachloroethene mg/kg <LOD <LOD <LOD 8 2.10 0 - - - - - < 5 - < 5 - - - -

Dibromochloromethane mg/kg <LOD <LOD <LOD 8 No Criteria 0 - - - - - < 5 - < 5 - - - -

1,2-Dibromoethane mg/kg <LOD <LOD <LOD 8 No Criteria 0 - - - - - < 5 - < 5 - - - -

Chlorobenzene mg/kg <LOD <LOD <LOD 8 0.73 0 - - - - - < 5 - < 5 - - - -

1,1,1,2-Tetrachloroethane mg/kg <LOD <LOD <LOD 8 2.10 0 - - - - - < 5 - < 5 - - - -

Ethyl Benzene mg/kg <LOD <LOD <LOD 8 350.00 0 - - - - - < 10 - < 10 - - - -

m,p-Xylene mg/kg <LOD <LOD <LOD 8 230.00 0 - - - - - < 10 - < 10 - - - -

o-Xylene mg/kg <LOD <LOD <LOD 22 250.00 0 - - < 10 - - < 10 - < 10 < 10 < 10 < 10 < 10

Styrene mg/kg <LOD <LOD <LOD 8 19.00 0 - - - - - < 5 - < 5 - - - -

Bromoform mg/kg <LOD <LOD <LOD 8 5.90 0 - - - - - < 10 - < 10 - - - -

Isopropylbenzene mg/kg 0.09 0.09 0.09 8 27.00 0 - - - - - < 5 - < 5 - - - -

1,1,2,2-Tetrachloroethane mg/kg <LOD <LOD <LOD 8 2.90 0 - - - - - < 5 - < 5 - - - -

1,2,3-Trichloropropane mg/kg <LOD <LOD <LOD 8 No Criteria 0 - - - - - < 5 - < 5 - - - -

n-Propylbenzene mg/kg 0.14 0.14 0.14 8 82.00 0 - - - - - < 5 - < 5 - - - -

Bromobenzene mg/kg <LOD <LOD <LOD 8 2.00 0 - - - - - < 5 - < 5 - - - -

2-Chlorotoluene mg/kg <LOD <LOD <LOD 8 No Criteria 0 - - - - - < 5 - < 5 - - - -

1,3,5-Trimethylbenzene mg/kg <LOD <LOD <LOD 8 No Criteria 0 - - - - - < 5 - < 5 - - - -

4-Chlorotoluene mg/kg <LOD <LOD <LOD 8 No Criteria 0 - - - - - < 5 - < 5 - - - -

tert-Butylbenzene mg/kg <LOD <LOD <LOD 8 No Criteria 0 - - - - - < 5 - < 5 - - - -

1,2,4-Trimethylbenzene mg/kg 1.62 1.62 1.62 8 0.85 1 - - - - - < 5 - < 5 - - - -

sec-Butylbenzene mg/kg 0.17 0.17 0.17 8 No Criteria 0 - - - - - < 5 - < 5 - - - -

p-Isopropyltoluene mg/kg 0.21 0.21 0.21 8 No Criteria 0 - - - - - < 5 - < 5 - - - -

1,3-Dichlorobenzene mg/kg <LOD <LOD <LOD 8 0.70 0 - - - - - < 5 - < 5 - - - -

1,4-Dichlorobenzene mg/kg <LOD <LOD <LOD 8 72.00 0 - - - - - < 5 - < 5 - - - -

n-Butylbenzene mg/kg 0.52 0.52 0.52 8 No Criteria 0 - - - - - < 5 - < 5 - - - -

1,2-Dichlorobenzene mg/kg <LOD <LOD <LOD 8 39.00 0 - - - - - < 5 - < 5 - - - -

1,2-Dibromo-3-chloropropane mg/kg <LOD <LOD <LOD 8 No Criteria 0 - - - - - < 10 - < 10 - - - -

Hexachlorobutadiene mg/kg <LOD <LOD <LOD 8 0.51 0 - - - - - < 5 - < 5 - - - -

1,2,4-Trichlorobenzene mg/kg <LOD <LOD <LOD 2 4.50 0 - - - - - < 0.1 - < 0.1 - - - -

2-Nitrophenol mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - < 0.1 - < 0.1 - - - -

Nitrobenzene mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - < 0.1 - < 0.1 - - - -

0-Cresol mg/kg <LOD <LOD <LOD 2 180.00 0 - - - - - < 0.1 - < 0.1 - - - -

bis(2-chloroethoxy)methane mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - < 0.1 - < 0.1 - - - -

bis(2-chloroethyl)ether mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - < 0.1 - < 0.1 - - - -

2,4-Dichlorophenol mg/kg <LOD <LOD <LOD 2 2.00 0 - - - - - < 0.1 - < 0.1 - - - -

2-Chlorophenol mg/kg <LOD <LOD <LOD 2 2.00 0 - - - - - < 0.1 - < 0.1 - - - -

1,3-Dichlorobenzene mg/kg <LOD <LOD <LOD 8 0.70 0 - - - - - < 5 - < 5 - - - -

1,4-Dichlorobenzene mg/kg <LOD <LOD <LOD 8 72.00 0 - - - - - < 5 - < 5 - - - -

1,2-Dichlorobenzene mg/kg <LOD <LOD <LOD 8 39.00 0 - - - - - < 5 - < 5 - - - -

2,4-Dimethylphenol mg/kg <LOD <LOD <LOD 2 43.00 0 - - - - - < 0.15 - < 0.15 - - - -

Isophorone mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - < 0.1 - < 0.1 - - - -

Hexachloroethane mg/kg <LOD <LOD <LOD 2 0.48 0 - - - - - < 0.1 - < 0.1 - - - -

p-Cresol mg/kg <LOD <LOD <LOD 2 180.00 0 - - - - - < 0.15 - < 0.15 - - - -

2,4,6-Trichlorophenol mg/kg <LOD <LOD <LOD 2 2.00 0 - - - - - < 0.1 - < 0.1 - - - -

2,4,5-Trichlorophenol mg/kg <LOD <LOD <LOD 2 2.00 0 - - - - - < 0.1 - < 0.1 - - - -

2-Nitroaniline mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - < 0.1 - < 0.1 - - - -

4-Chloro-3-methylphenol mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - < 0.1 - < 0.1 - - - -

2-Methylnaphthalene mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - < 0.1 - < 0.1 - - - -

Page 99: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

HUMAN HEALTH QUANTITATIVE RISK ASSESSMENT - SOILS SOM = 2.5%SOM = 2.5%

MADE GROUND SOM = 6%

1309 2.784762

K&N Distribution Depot, Draycott in the Clay SOM = 2.5%

AWS030.35 AWS040.32 AWS050.20 AWS060.50 AWS070.30 AWS070.60 AWS090.20 AWS090.40 AWS110.50 AWS120.20 SP10.50 TP10.30 - 0.50

AWS03 AWS04 AWS05 AWS06 AWS07 AWS07 AWS09 AWS09 AWS11 AWS12 SP1 TP1

0.35 0.32 0.20 0.50 0.30 0.60 0.20 0.40 0.50 0.20 0.50 0.30 - 0.50

SGVs & GACs

Residential

SGVs, GACs & C4SLs

SOM = 2.5%

Assessment Criteria Source:

Soil Organic Matter (%):

Assessment Scenario:

ASSESSMENT

CRITERIA

No. >

ACDETERMINAND MINIMUM AVERAGE MAXIMUM

No. of

TESTSUNITS

Hexachlorocyclopentadiene mg/kg <LOD <LOD <LOD 2 46.00 0 - - - - - < 0.1 - < 0.1 - - - -

Hexachlorobutadiene mg/kg <LOD <LOD <LOD 8 0.51 0 - - - - - < 5 - < 5 - - - -

2,6-Dinitrotoluene mg/kg <LOD <LOD <LOD 2 1.70 0 - - - - - < 0.1 - < 0.1 - - - -

Dimethyl phthalate mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - < 0.1 - < 0.1 - - - -

2-Chloronaphthalene mg/kg <LOD <LOD <LOD 2 9.20 0 - - - - - < 0.1 - < 0.1 - - - -

4-Chloroaniline mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - < 0.2 - < 0.2 - - - -

4-Nitrophenol mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - < 0.1 - < 0.1 - - - -

4-Chlorophenyl phenyl ether mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - < 0.1 - < 0.1 - - - -

3-Nitroaniline mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - < 0.1 - < 0.1 - - - -

4-Nitroaniline mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - < 0.1 - < 0.1 - - - -

4-Bromophenyl phenyl ether mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - < 0.1 - < 0.1 - - - -

Hexachlorobenzene mg/kg <LOD <LOD <LOD 2 46.00 0 - - - - - < 0.1 - < 0.1 - - - -

2,4-Dinitrotoluene mg/kg <LOD <LOD <LOD 2 3.20 0 - - - - - < 0.1 - < 0.1 - - - -

Diethyl phthalate mg/kg <LOD <LOD <LOD 2 260.00 0 - - - - - < 0.1 - < 0.1 - - - -

Dibenzofuran mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - < 0.1 - < 0.1 - - - -

Azobenzene mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - < 0.1 - < 0.1 - - - -

Dibutyl phthalate mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - < 0.15 - < 0.15 - - - -

Carbazole mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - < 0.1 - < 0.1 - - - -

bis(2-ethylhexyl)phthalate mg/kg <LOD <LOD <LOD 2 610.00 0 - - - - - < 0.2 - < 0.2 - - - -

Benzyl butyl phthalate mg/kg <LOD <LOD <LOD 2 3300.00 0 - - - - - < 0.1 - < 0.1 - - - -

Di-n-octyl phthalate mg/kg <LOD <LOD <LOD 2 2800.00 0 - - - - - < 0.1 - < 0.1 - - - -

Page 100: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

HUMAN HEALTH QUANTITATIVE RISK ASSESSMENT - SOILS

MADE GROUND

1309

K&N Distribution Depot, Draycott in the Clay

Asbestos Screen

pH

Total Cyanide

Total Organic Carbon (TOC)

Arsenic

Water Soluble Sulphate as SO4 (2:1)

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Selenium

Zinc

Naphthalene

Acenaphthylene

Acenaphthene

Fluorene

Phenanthrene

Anthracene

Fluoranthene

Pyrene

Benzo(a)anthracene

Chrysene

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(a)pyrene

Indeno(1,2,3-cd)pyrene

Di-benzo(a,h)anthracene

Benzo(ghi)perylene

TPH CWG - Aliphatic >C5 - C6

TPH CWG - Aliphatic >C6 - C8

TPH CWG - Aliphatic >C8 - C10

TPH CWG - Aliphatic >C10 - C12

TPH CWG - Aliphatic >C12 - C16

TPH CWG - Aliphatic >C16 - C21

TPH CWG - Aliphatic >C21 - C34

TPH CWG - Aromatic >C5 - C7

TPH CWG - Aromatic >C7 - C8

TPH CWG - Aromatic >C8 - C10

TPH CWG - Aromatic >C10 - C12

TPH CWG - Aromatic >C12 - C16

TPH CWG - Aromatic >C16 - C21

TPH CWG - Aromatic >C21 - C35

Benzene

Toluene

Ethylbenzene

m & p-xylene

o-Xylene

Monohydric Phenols

Dichlorodifluoromethane

Vinyl Chloride

Chloromethane

Chloroethane

Bromomethane

Trichlorofluoromethane

1,1-Dichloroethene

MTBE

trans-1,2-Dichloroethene

1,1-Dichloroethane

cis-1,2-Dichloroethene

2,2-Dichloropropane

Chloroform

DETERMINAND

0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

TP20.10 - 0.30 TP30.50 TP40.20 TP60.20 TP100.10 - 0.30 TP120.10 - 0.20 TP150.60 - 0.70 TP16GL - 0.10 TP160.20 - 0.30 WS5010.10 - 0.20WS5020.30 - 0.40WS5030.60 - 0.70WS5040.35 - 0.45WS5040.70 - 1.00WS5050.30 - 0.50WS5060.60 - 0.70WS5070.20 - 0.50

TP2 TP3 TP4 TP6 TP10 TP12 TP15 TP16 TP16 WS501 WS502 WS503 WS504 WS504 WS505 WS506 WS507

0.10 - 0.30 0.50 0.20 0.20 0.10 - 0.30 0.10 - 0.20 0.60 - 0.70 GL - 0.10 0.20 - 0.30 0.10 - 0.20 0.30 - 0.40 0.60 - 0.70 0.35 - 0.45 0.70 - 1.00 0.30 - 0.50 0.60 - 0.70 0.20 - 0.50

Not Detected - Not Detected Not Detected Not Detected Not Detected Not Detected Not Detected Not Detected Not Detected Not Detected Not Detected Not Detected - Not Detected Not Detected Not Detected

- 7.6 7.6 - 7.7 7.4 9 - 8.1 - 7.5 7.6 - - - 7.8 -

- - < 2 - < 2 < 2 < 2 - < 2 - < 2 < 2 - - - < 2 -

- - 1.8 - 1.6 1.8 2.4 - 1.7 - 1.8 1.4 - - - 0.8 -

- - 4 - 4 6 14 - 10 - 4 7 - - - 23 -

- 0.14 0.07 - 0.67 0.09 1.12 - 0.55 - 0.12 0.08 - - - 2.24 -

- - < 0.5 - 0.9 < 0.5 1 - 0.7 - < 0.5 2.4 - - - 0.6 -

- - 31 - 27 30 24 - 15 - 35 29 - - - 26 -

- - 19 - 51 18 57 - 31 - 27 45 - - - 49 -

- - 24 - 122 43 53 - 28 - 63 74 - - - 46 -

- - < 1 - < 1 < 1 < 1 - < 1 - < 1 < 1 - - - < 1 -

- - 36 - 24 29 44 - 25 - 31 43 - - - 42 -

- - < 3 - < 3 < 3 < 3 - < 3 - < 3 < 3 - - - < 3 -

- - 83 - 323 210 202 - 97 - 136 123 - - - 78 -

- - < 0.1 - < 0.1 < 0.1 < 0.1 - < 0.1 - < 0.1 < 0.1 - - - < 0.1 -

- - < 0.1 - < 0.1 < 0.1 < 0.1 - < 0.1 - < 0.1 < 0.1 - - - < 0.1 -

- - < 0.1 - < 0.1 < 0.1 < 0.1 - < 0.1 - < 0.1 < 0.1 - - - < 0.1 -

- - < 0.1 - < 0.1 < 0.1 < 0.1 - < 0.1 - < 0.1 < 0.1 - - - < 0.1 -

- - 0.31 - < 0.1 0.11 < 0.1 - < 0.1 - < 0.1 0.15 - - - < 0.1 -

- - < 0.1 - < 0.1 < 0.1 < 0.1 - < 0.1 - < 0.1 < 0.1 - - - < 0.1 -

- - 0.56 - < 0.1 0.56 < 0.1 - < 0.1 - < 0.1 0.31 - - - < 0.1 -

- - 0.46 - < 0.1 0.49 < 0.1 - < 0.1 - < 0.1 0.27 - - - < 0.1 -

- - 0.2 - < 0.1 0.24 < 0.1 - < 0.1 - < 0.1 < 0.1 - - - < 0.1 -

- - 0.26 - < 0.1 0.27 < 0.1 - < 0.1 - < 0.1 0.13 - - - < 0.1 -

- - 0.28 - < 0.1 0.25 < 0.1 - < 0.1 - < 0.1 < 0.1 - - - < 0.1 -

- - 0.12 - < 0.1 0.11 < 0.1 - < 0.1 - < 0.1 < 0.1 - - - < 0.1 -

- - 0.19 - < 0.1 0.21 < 0.1 - < 0.1 - < 0.1 < 0.1 - - - < 0.1 -

- - 0.13 - < 0.1 < 0.1 < 0.1 - < 0.1 - < 0.1 < 0.1 - - - < 0.1 -

- - < 0.1 - < 0.1 < 0.1 < 0.1 - < 0.1 - < 0.1 < 0.1 - - - < 0.1 -

- - 0.12 - < 0.1 0.11 < 0.1 - < 0.1 - < 0.1 < 0.1 - - - < 0.1 -

- - < 0.01 - < 0.01 < 0.01 < 0.01 - < 0.01 - < 0.01 < 0.01 - - - < 0.01 -

- - < 0.05 - < 0.05 < 0.05 < 0.05 - < 0.05 - < 0.05 < 0.05 - - - < 0.05 -

- - < 1 - < 1 < 1 < 1 - < 1 - < 1 < 1 - - - < 1 -

- - < 1 - < 1 < 1 < 1 - < 1 - < 1 < 1 - - - < 1 -

- - < 1 - < 1 < 1 < 1 - < 1 - < 1 < 1 - - - < 1 -

- - < 1 - < 1 < 1 < 1 - < 1 - < 1 < 1 - - - < 1 -

- - < 6 - < 6 < 6 < 6 - < 6 - < 6 < 6 - - - < 6 -

- - < 0.01 - < 0.01 < 0.01 < 0.01 - < 0.01 - < 0.01 < 0.01 - - - < 0.01 -

- - < 0.05 - < 0.05 < 0.05 < 0.05 - < 0.05 - < 0.05 < 0.05 - - - < 0.05 -

- - < 1 - < 1 < 1 < 1 - < 1 - < 1 < 1 - - - < 1 -

- - < 1 - < 1 < 1 < 1 - < 1 - < 1 < 1 - - - < 1 -

- - < 1 - < 1 < 1 < 1 - < 1 - < 1 < 1 - - - < 1 -

- - < 1 - < 1 < 1 < 1 - < 1 - < 1 < 1 - - - < 1 -

- - < 6 - < 6 < 6 < 6 - < 6 - < 6 < 6 - - - < 6 -

- - < 2 - < 2 < 2 < 2 - < 2 - < 2 < 2 - - - < 2 -

- - < 5 - < 5 < 5 < 5 - < 5 - < 5 < 5 - - - < 5 -

- - < 10 - < 10 < 10 < 10 - < 10 - < 10 < 10 - - - < 10 -

- - < 10 - < 10 < 10 < 10 - < 10 - < 10 < 10 - - - < 10 -

- - < 10 - < 10 < 10 < 10 - < 10 - < 10 < 10 - - - < 10 -

- - < 2 - < 2 < 2 < 2 - < 2 - < 2 < 2 - - - < 2 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 10 - - - < 10 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 10 - - - < 10 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - < 5 - < 5 < 5 < 5 - < 5 - < 5 < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

Page 101: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

HUMAN HEALTH QUANTITATIVE RISK ASSESSMENT - SOILS

MADE GROUND

1309

K&N Distribution Depot, Draycott in the Clay

DETERMINAND

Bromochloromethane

1,1,1-Trichloroethane

1,1-Dichloropropene

Carbon Tetrachloride

1,2-Dichloroethane

Benzene

1,2-Dichloropropane

Trichloroethene

Bromodichloromethane

Dibromomethane

TAME

cis-1,3-Dichloropropene

Toluene

trans-1,3-Dichloropropene

1,1,2-Trichloroethane

1,3-Dichloropropane

Tetrachloroethene

Dibromochloromethane

1,2-Dibromoethane

Chlorobenzene

1,1,1,2-Tetrachloroethane

Ethyl Benzene

m,p-Xylene

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,2,3-Trichloropropane

n-Propylbenzene

Bromobenzene

2-Chlorotoluene

1,3,5-Trimethylbenzene

4-Chlorotoluene

tert-Butylbenzene

1,2,4-Trimethylbenzene

sec-Butylbenzene

p-Isopropyltoluene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

n-Butylbenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-chloropropane

Hexachlorobutadiene

1,2,4-Trichlorobenzene

2-Nitrophenol

Nitrobenzene

0-Cresol

bis(2-chloroethoxy)methane

bis(2-chloroethyl)ether

2,4-Dichlorophenol

2-Chlorophenol

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

2,4-Dimethylphenol

Isophorone

Hexachloroethane

p-Cresol

2,4,6-Trichlorophenol

2,4,5-Trichlorophenol

2-Nitroaniline

4-Chloro-3-methylphenol

2-Methylnaphthalene

TP20.10 - 0.30 TP30.50 TP40.20 TP60.20 TP100.10 - 0.30 TP120.10 - 0.20 TP150.60 - 0.70 TP16GL - 0.10 TP160.20 - 0.30 WS5010.10 - 0.20WS5020.30 - 0.40WS5030.60 - 0.70WS5040.35 - 0.45WS5040.70 - 1.00WS5050.30 - 0.50WS5060.60 - 0.70WS5070.20 - 0.50

TP2 TP3 TP4 TP6 TP10 TP12 TP15 TP16 TP16 WS501 WS502 WS503 WS504 WS504 WS505 WS506 WS507

0.10 - 0.30 0.50 0.20 0.20 0.10 - 0.30 0.10 - 0.20 0.60 - 0.70 GL - 0.10 0.20 - 0.30 0.10 - 0.20 0.30 - 0.40 0.60 - 0.70 0.35 - 0.45 0.70 - 1.00 0.30 - 0.50 0.60 - 0.70 0.20 - 0.50

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 10 - - - < 10 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - < 2 - < 2 < 2 < 2 - < 2 - < 2 < 2 - - - < 2 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - < 5 - < 5 < 5 < 5 - < 5 - < 5 < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 10 - - - < 10 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 10 - - - < 10 -

- - - - - - - - - - - < 10 - - - < 10 -

- - < 10 - < 10 < 10 < 10 - < 10 - < 10 < 10 - - - < 10 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 10 - - - < 10 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 10 - - - < 10 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

Page 102: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

HUMAN HEALTH QUANTITATIVE RISK ASSESSMENT - SOILS

MADE GROUND

1309

K&N Distribution Depot, Draycott in the Clay

DETERMINAND

Hexachlorocyclopentadiene

Hexachlorobutadiene

2,6-Dinitrotoluene

Dimethyl phthalate

2-Chloronaphthalene

4-Chloroaniline

4-Nitrophenol

4-Chlorophenyl phenyl ether

3-Nitroaniline

4-Nitroaniline

4-Bromophenyl phenyl ether

Hexachlorobenzene

2,4-Dinitrotoluene

Diethyl phthalate

Dibenzofuran

Azobenzene

Dibutyl phthalate

Carbazole

bis(2-ethylhexyl)phthalate

Benzyl butyl phthalate

Di-n-octyl phthalate

TP20.10 - 0.30 TP30.50 TP40.20 TP60.20 TP100.10 - 0.30 TP120.10 - 0.20 TP150.60 - 0.70 TP16GL - 0.10 TP160.20 - 0.30 WS5010.10 - 0.20WS5020.30 - 0.40WS5030.60 - 0.70WS5040.35 - 0.45WS5040.70 - 1.00WS5050.30 - 0.50WS5060.60 - 0.70WS5070.20 - 0.50

TP2 TP3 TP4 TP6 TP10 TP12 TP15 TP16 TP16 WS501 WS502 WS503 WS504 WS504 WS505 WS506 WS507

0.10 - 0.30 0.50 0.20 0.20 0.10 - 0.30 0.10 - 0.20 0.60 - 0.70 GL - 0.10 0.20 - 0.30 0.10 - 0.20 0.30 - 0.40 0.60 - 0.70 0.35 - 0.45 0.70 - 1.00 0.30 - 0.50 0.60 - 0.70 0.20 - 0.50

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - < 5 - - - < 5 -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

Page 103: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

HUMAN HEALTH QUANTITATIVE RISK ASSESSMENT - SOILS

MADE GROUND

1309

K&N Distribution Depot, Draycott in the Clay

Asbestos Screen

pH

Total Cyanide

Total Organic Carbon (TOC)

Arsenic

Water Soluble Sulphate as SO4 (2:1)

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Selenium

Zinc

Naphthalene

Acenaphthylene

Acenaphthene

Fluorene

Phenanthrene

Anthracene

Fluoranthene

Pyrene

Benzo(a)anthracene

Chrysene

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(a)pyrene

Indeno(1,2,3-cd)pyrene

Di-benzo(a,h)anthracene

Benzo(ghi)perylene

TPH CWG - Aliphatic >C5 - C6

TPH CWG - Aliphatic >C6 - C8

TPH CWG - Aliphatic >C8 - C10

TPH CWG - Aliphatic >C10 - C12

TPH CWG - Aliphatic >C12 - C16

TPH CWG - Aliphatic >C16 - C21

TPH CWG - Aliphatic >C21 - C34

TPH CWG - Aromatic >C5 - C7

TPH CWG - Aromatic >C7 - C8

TPH CWG - Aromatic >C8 - C10

TPH CWG - Aromatic >C10 - C12

TPH CWG - Aromatic >C12 - C16

TPH CWG - Aromatic >C16 - C21

TPH CWG - Aromatic >C21 - C35

Benzene

Toluene

Ethylbenzene

m & p-xylene

o-Xylene

Monohydric Phenols

Dichlorodifluoromethane

Vinyl Chloride

Chloromethane

Chloroethane

Bromomethane

Trichlorofluoromethane

1,1-Dichloroethene

MTBE

trans-1,2-Dichloroethene

1,1-Dichloroethane

cis-1,2-Dichloroethene

2,2-Dichloropropane

Chloroform

DETERMINAND

0 0 0 0 0 0 0 0 0

WS5080.20 - 0.40WS5080.50 - 0.60WS5090.50 - 0.80WS5100.14 - 0.20WS5110.45 - 0.55WS5130.30 - 0.40WS5133.60 - 3.70WS5140.10 - 0.50WS5150.30 - 0.60

WS508 WS508 WS509 WS510 WS511 WS513 WS513 WS514 WS515

0.20 - 0.40 0.50 - 0.60 0.50 - 0.80 0.14 - 0.20 0.45 - 0.55 0.30 - 0.40 3.60 - 3.70 0.10 - 0.50 0.30 - 0.60

- Not Detected Not Detected Not Detected Not Detected Not Detected - Not Detected Not Detected

- 8.2 8 7.7 7.7 7.7 7.8 8.1 7.9

- < 2 < 2 < 2 < 2 < 2 - < 2 < 2

- 0.3 0.4 1.6 1.1 2.7 - 0.9 1

- 12 3 5 22 8 - 7 7

- 0.07 0.07 0.19 0.11 1.13 0.15 0.45 0.34

- < 0.5 < 0.5 1.6 1 0.8 - 1.2 0.9

- 23 34 19 19 22 - 17 14

- 31 10 35 29 42 - 31 37

- 31 11 48 101 37 - 75 106

- < 1 < 1 < 1 < 1 < 1 - < 1 < 1

- 34 32 27 27 35 - 15 17

- < 3 < 3 < 3 < 3 < 3 - < 3 < 3

- 73 78 184 60 56 - 347 276

- < 0.1 < 0.1 < 0.1 0.4 < 0.1 - < 0.1 < 0.1

- < 0.1 < 0.1 < 0.1 0.27 < 0.1 - < 0.1 < 0.1

- < 0.1 < 0.1 < 0.1 0.5 < 0.1 - < 0.1 < 0.1

- < 0.1 < 0.1 < 0.1 2.99 < 0.1 - < 0.1 < 0.1

- < 0.1 < 0.1 < 0.1 3.41 1.9 - < 0.1 0.55

- < 0.1 < 0.1 < 0.1 0.31 0.16 - < 0.1 0.11

- < 0.1 < 0.1 < 0.1 0.18 5.7 - < 0.1 0.46

- < 0.1 < 0.1 < 0.1 0.6 4.41 - < 0.1 0.52

- < 0.1 < 0.1 < 0.1 < 0.1 2.55 - < 0.1 0.46

- < 0.1 < 0.1 < 0.1 < 0.1 3.48 - < 0.1 0.42

- < 0.1 < 0.1 < 0.1 < 0.1 4.19 - 0.15 0.31

- < 0.1 < 0.1 < 0.1 < 0.1 1.51 - < 0.1 < 0.1

- < 0.1 < 0.1 < 0.1 < 0.1 2.51 - < 0.1 0.21

- < 0.1 < 0.1 < 0.1 < 0.1 1.62 - < 0.1 < 0.1

- < 0.1 < 0.1 < 0.1 < 0.1 0.33 - < 0.1 < 0.1

- < 0.1 < 0.1 < 0.1 < 0.1 1.29 - < 0.1 0.17

- < 0.01 < 0.01 < 0.01 0.06 < 0.01 - < 0.01 < 0.01

- < 0.05 < 0.05 < 0.05 8.9 0.28 - < 0.05 < 0.05

- < 1 < 1 < 1 105 3 - < 1 < 1

- < 1 < 1 < 1 302 < 1 - < 1 < 1

- < 1 < 1 < 1 1626 < 1 - < 1 8

- < 1 < 1 < 1 1850 < 1 - < 1 12

- < 6 < 6 < 6 560 < 6 - < 6 41

- < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 - < 0.01 < 0.01

- < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 - < 0.05 < 0.05

- < 1 < 1 < 1 10 < 1 - < 1 < 1

- < 1 < 1 < 1 130 < 1 - < 1 < 1

- < 1 < 1 < 1 1134 1 - < 1 2

- < 1 < 1 < 1 1270 19 - < 1 10

- < 6 < 6 < 6 423 79 - < 6 31

- < 2 < 2 < 2 < 2 < 2 - < 2 < 2

- < 5 < 5 < 5 < 5 < 5 - < 5 < 5

- < 10 < 10 < 10 < 10 < 10 - < 10 < 10

- < 10 < 10 < 10 < 10 < 10 - < 10 < 10

- < 10 < 10 < 10 < 10 < 10 - < 10 < 10

- < 2 < 2 < 2 < 2 < 2 - < 2 < 2

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

< 10 - < 10 - < 10 < 10 - - -

< 5 - < 5 - < 5 < 5 - - -

< 10 - < 10 - < 10 < 10 - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

- < 5 < 5 < 5 < 5 < 5 - < 5 < 5

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

Page 104: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

HUMAN HEALTH QUANTITATIVE RISK ASSESSMENT - SOILS

MADE GROUND

1309

K&N Distribution Depot, Draycott in the Clay

DETERMINAND

Bromochloromethane

1,1,1-Trichloroethane

1,1-Dichloropropene

Carbon Tetrachloride

1,2-Dichloroethane

Benzene

1,2-Dichloropropane

Trichloroethene

Bromodichloromethane

Dibromomethane

TAME

cis-1,3-Dichloropropene

Toluene

trans-1,3-Dichloropropene

1,1,2-Trichloroethane

1,3-Dichloropropane

Tetrachloroethene

Dibromochloromethane

1,2-Dibromoethane

Chlorobenzene

1,1,1,2-Tetrachloroethane

Ethyl Benzene

m,p-Xylene

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,2,3-Trichloropropane

n-Propylbenzene

Bromobenzene

2-Chlorotoluene

1,3,5-Trimethylbenzene

4-Chlorotoluene

tert-Butylbenzene

1,2,4-Trimethylbenzene

sec-Butylbenzene

p-Isopropyltoluene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

n-Butylbenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-chloropropane

Hexachlorobutadiene

1,2,4-Trichlorobenzene

2-Nitrophenol

Nitrobenzene

0-Cresol

bis(2-chloroethoxy)methane

bis(2-chloroethyl)ether

2,4-Dichlorophenol

2-Chlorophenol

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

2,4-Dimethylphenol

Isophorone

Hexachloroethane

p-Cresol

2,4,6-Trichlorophenol

2,4,5-Trichlorophenol

2-Nitroaniline

4-Chloro-3-methylphenol

2-Methylnaphthalene

WS5080.20 - 0.40WS5080.50 - 0.60WS5090.50 - 0.80WS5100.14 - 0.20WS5110.45 - 0.55WS5130.30 - 0.40WS5133.60 - 3.70WS5140.10 - 0.50WS5150.30 - 0.60

WS508 WS508 WS509 WS510 WS511 WS513 WS513 WS514 WS515

0.20 - 0.40 0.50 - 0.60 0.50 - 0.80 0.14 - 0.20 0.45 - 0.55 0.30 - 0.40 3.60 - 3.70 0.10 - 0.50 0.30 - 0.60

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

< 10 - < 10 - < 10 < 10 - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

- < 2 < 2 < 2 < 2 < 2 - < 2 < 2

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 0.276 - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

- < 5 < 5 < 5 < 5 < 5 - < 5 < 5

< 5 - < 5 - < 5 < 5 - - -

< 10 - < 10 - < 10 < 10 - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

< 10 - < 10 - < 10 < 10 - - -

< 10 - < 10 - < 10 < 10 - - -

- < 10 < 10 < 10 < 10 < 10 - < 10 < 10

< 5 - < 5 - < 5 < 5 - - -

< 10 - < 10 - < 10 < 10 - - -

< 5 - < 5 - 0.087 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - 0.143 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - 1.616 < 5 - - -

< 5 - < 5 - 0.168 < 5 - - -

< 5 - < 5 - 0.209 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - 0.522 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

< 10 - < 10 - < 10 < 10 - - -

< 5 - < 5 - < 5 < 5 - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

< 5 - < 5 - < 5 < 5 - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

Page 105: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

HUMAN HEALTH QUANTITATIVE RISK ASSESSMENT - SOILS

MADE GROUND

1309

K&N Distribution Depot, Draycott in the Clay

DETERMINAND

Hexachlorocyclopentadiene

Hexachlorobutadiene

2,6-Dinitrotoluene

Dimethyl phthalate

2-Chloronaphthalene

4-Chloroaniline

4-Nitrophenol

4-Chlorophenyl phenyl ether

3-Nitroaniline

4-Nitroaniline

4-Bromophenyl phenyl ether

Hexachlorobenzene

2,4-Dinitrotoluene

Diethyl phthalate

Dibenzofuran

Azobenzene

Dibutyl phthalate

Carbazole

bis(2-ethylhexyl)phthalate

Benzyl butyl phthalate

Di-n-octyl phthalate

WS5080.20 - 0.40WS5080.50 - 0.60WS5090.50 - 0.80WS5100.14 - 0.20WS5110.45 - 0.55WS5130.30 - 0.40WS5133.60 - 3.70WS5140.10 - 0.50WS5150.30 - 0.60

WS508 WS508 WS509 WS510 WS511 WS513 WS513 WS514 WS515

0.20 - 0.40 0.50 - 0.60 0.50 - 0.80 0.14 - 0.20 0.45 - 0.55 0.30 - 0.40 3.60 - 3.70 0.10 - 0.50 0.30 - 0.60

- - - - - - - - -

< 5 - < 5 - < 5 < 5 - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

- - - - - - - - -

Page 106: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

HUMAN HEALTH QUANTITATIVE RISK ASSESSMENT - SOILS SOM = 1% SOM = 1%

NATURAL GROUND SOM = 2.5%

1309 SOM = 6%

K&N Distribution Depot, Draycott in the Clay 1.774316

SOM = 1% AWS010.20 AWS010.50 AWS011.50 AWS020.90 AWS022.30 AWS030.70 AWS040.70 AWS050.75 AWS061.50 AWS071.40 AWS080.20 AWS080.60

AWS01 AWS01 AWS01 AWS02 AWS02 AWS03 AWS04 AWS05 AWS06 AWS07 AWS08 AWS08

0.20 0.50 1.50 0.90 2.30 0.70 0.70 0.75 1.50 1.40 0.20 0.60

Asbestos Screen N/A N/A N/A N/A 22 Detected 0 Not Detected Not Detected - Not Detected - Not Detected Not Detected Not Detected Not Detected - Not Detected Not Detected

pH no units 6.80 7.63 9.40 23 No Criteria 0 9.4 8 - 7.5 - 7.4 7.6 7.2 7.1 - 7.4 -

Total Cyanide mg/kg <LOD <LOD <LOD 20 53.00 0 < 2 < 2 - < 2 - < 2 < 2 < 2 < 2 - < 2 -

Total Organic Carbon (TOC) mg/kg 0.10 1.03 3.70 20 No Criteria 0 1.7 0.7 - 0.8 - 0.2 0.1 0.8 0.1 - 0.6 -

37 Arsenic mg/kg 2.00 5.31 13.00 20 37.00 0 5 < 2 - < 2 - 6 4 < 2 13 - 2 -

Water Soluble Sulphate as SO4 (2:1) mg/kg 0.01 0.18 1.09 23 No Criteria 0 0.01 0.04 - 0.05 - 0.03 0.01 0.02 0.02 - 0.03 -

26 Cadmium mg/kg 0.60 0.85 1.10 20 26.00 0 1.1 < 0.5 - < 0.5 - < 0.5 < 0.5 < 0.5 < 0.5 - < 0.5 -

Chromium mg/kg 16.00 32.30 48.00 20 3000.00 0 29 35 - 37 - 32 35 31 43 - 33 -

Copper mg/kg 6.00 17.70 39.00 20 2330.00 0 19 15 - 22 - 9 7 20 12 - 11 -

200 Lead mg/kg 8.00 20.60 52.00 20 200.00 0 23 14 - 15 - 8 8 11 13 - 17 -

Mercury mg/kg <LOD <LOD <LOD 20 170.00 0 < 1 < 1 - < 1 - < 1 < 1 < 1 < 1 - < 1 -

Nickel mg/kg 12.00 30.70 50.00 20 130.00 0 30 33 - 35 - 33 31 30 50 - 32 -

Selenium mg/kg <LOD <LOD <LOD 20 350.00 0 < 3 < 3 - < 3 - < 3 < 3 < 3 < 3 - < 3 -

Zinc mg/kg 45.00 78.80 129.00 20 3750.00 0 76 65 - 89 - 58 58 72 74 - 72 -

Naphthalene mg/kg <LOD <LOD <LOD 20 1.50 0 < 0.1 < 0.1 - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 -

Acenaphthylene mg/kg <LOD <LOD <LOD 20 170.00 0 < 0.1 < 0.1 - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 -

Acenaphthene mg/kg <LOD <LOD <LOD 20 210.00 0 < 0.1 < 0.1 - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 -

Fluorene mg/kg 0.20 0.20 0.20 20 160.00 0 < 0.1 0.2 - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 -

Phenanthrene mg/kg 0.55 0.55 0.55 20 92.00 0 < 0.1 0.55 - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 -

Anthracene mg/kg <LOD <LOD <LOD 20 2300.00 0 < 0.1 < 0.1 - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 -

Fluoranthene mg/kg 0.16 0.18 0.20 20 260.00 0 < 0.1 < 0.1 - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 -

Pyrene mg/kg 0.15 0.20 0.39 20 560.00 0 < 0.1 0.39 - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 -

Benzo(a)anthracene mg/kg <LOD <LOD <LOD 20 3.10 0 < 0.1 < 0.1 - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 -

Chrysene mg/kg 0.11 0.12 0.13 20 6.00 0 < 0.1 < 0.1 - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 -

Benzo(b)fluoranthene mg/kg 0.12 0.12 0.12 20 5.60 0 < 0.1 < 0.1 - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 -

Benzo(k)fluoranthene mg/kg <LOD <LOD <LOD 20 6.50 0 < 0.1 < 0.1 - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 -

5 Benzo(a)pyrene mg/kg <LOD <LOD <LOD 20 5.00 0 < 0.1 < 0.1 - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 -

Indeno(1,2,3-cd)pyrene mg/kg <LOD <LOD <LOD 20 3.20 0 < 0.1 < 0.1 - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 -

Di-benzo(a,h)anthracene mg/kg <LOD <LOD <LOD 20 0.76 0 < 0.1 < 0.1 - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 -

Benzo(ghi)perylene mg/kg <LOD <LOD <LOD 20 44.00 0 < 0.1 < 0.1 - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 -

TPH CWG - Aliphatic >C5 - C6 mg/kg <LOD <LOD <LOD 23 30.00 0 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 -

TPH CWG - Aliphatic >C6 - C8 mg/kg <LOD <LOD <LOD 23 73.00 0 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 -

TPH CWG - Aliphatic >C8 - C10 mg/kg 3.00 27.00 51.00 23 19.00 1 < 1 3 < 1 < 1 < 1 < 1 < 1 < 1 51 < 1 < 1 -

TPH CWG - Aliphatic >C10 - C12 mg/kg 31.00 79.00 127.00 23 93.00 1 < 1 31 < 1 < 1 < 1 < 1 < 1 < 1 127 < 1 < 1 -

TPH CWG - Aliphatic >C12 - C16 mg/kg 87.00 144.00 201.00 23 740.00 0 < 1 201 < 1 < 1 < 1 < 1 < 1 < 1 87 < 1 < 1 -

TPH CWG - Aliphatic >C16 - C21 mg/kg 246.00 246.00 246.00 23 45000.00 0 < 1 246 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 -

TPH CWG - Aliphatic >C21 - C34 mg/kg 47.00 47.00 47.00 23 45000.00 0 < 6 47 < 6 < 6 < 6 < 6 < 6 < 6 < 6 < 6 < 6 -

TPH CWG - Aromatic >C5 - C7 mg/kg <LOD <LOD <LOD 23 65.00 0 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 -

TPH CWG - Aromatic >C7 - C8 mg/kg <LOD <LOD <LOD 23 120.00 0 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 -

TPH CWG - Aromatic >C8 - C10 mg/kg 10.00 10.00 10.00 23 27.00 0 < 1 < 1 < 1 < 1 < 1 < 1 < 1 < 1 10 < 1 < 1 -

TPH CWG - Aromatic >C10 - C12 mg/kg 11.00 30.00 49.00 23 69.00 0 < 1 11 < 1 < 1 < 1 < 1 < 1 < 1 49 < 1 < 1 -

TPH CWG - Aromatic >C12 - C16 mg/kg 46.00 75.50 105.00 23 140.00 0 < 1 105 < 1 < 1 < 1 < 1 < 1 < 1 46 < 1 < 1 -

TPH CWG - Aromatic >C16 - C21 mg/kg 3.00 65.67 188.00 23 250.00 0 < 1 188 < 1 < 1 < 1 < 1 < 1 < 1 3 < 1 < 1 -

TPH CWG - Aromatic >C21 - C35 mg/kg 34.00 34.00 34.00 23 890.00 0 < 6 34 < 6 < 6 < 6 < 6 < 6 < 6 < 6 < 6 < 6 -

0.9 Benzene mg/kg <LOD <LOD <LOD 23 0.87 0 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 -

Toluene mg/kg <LOD <LOD <LOD 23 610.00 0 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 -

Ethylbenzene mg/kg 0.19 0.19 0.19 23 350.00 0 < 10 < 10 < 10 < 10 < 10 < 10 < 10 < 10 0.191 < 10 < 10 -

m & p-xylene mg/kg 0.05 0.05 0.05 23 230.00 0 < 10 < 10 < 10 < 10 < 10 < 10 < 10 < 10 0.053 < 10 < 10 -

o-Xylene mg/kg 0.02 0.02 0.02 23 250.00 0 < 10 < 10 < 10 < 10 < 10 < 10 < 10 < 10 0.016 < 10 < 10 -

Monohydric Phenols mg/kg <LOD <LOD <LOD 20 420.00 0 < 2 < 2 - < 2 - < 2 < 2 < 2 < 2 - < 2 -

Dichlorodifluoromethane mg/kg <LOD <LOD <LOD 3 No Criteria 0 - - - - - - - < 5 < 5 - - -

Vinyl Chloride mg/kg <LOD <LOD <LOD 3 0.00 0 - - - - - - - < 5 < 5 - - -

Chloromethane mg/kg <LOD <LOD <LOD 3 0.01 0 - - - - - - - < 10 < 10 - - -

Chloroethane mg/kg <LOD <LOD <LOD 3 8.30 0 - - - - - - - < 5 < 5 - - -

Bromomethane mg/kg <LOD <LOD <LOD 3 No Criteria 0 - - - - - - - < 10 < 10 - - -

Trichlorofluoromethane mg/kg <LOD <LOD <LOD 3 No Criteria 0 - - - - - - - < 5 < 5 - - -

1,1-Dichloroethene mg/kg <LOD <LOD <LOD 3 0.23 0 - - - - - - - < 5 < 5 - - -

MTBE mg/kg <LOD <LOD <LOD 23 49.00 0 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 -

trans-1,2-Dichloroethene mg/kg <LOD <LOD <LOD 3 0.19 0 - - - - - - - < 5 < 5 - - -

1,1-Dichloroethane mg/kg <LOD <LOD <LOD 3 2.40 0 - - - - - - - < 5 < 5 - - -

cis-1,2-Dichloroethene mg/kg <LOD <LOD <LOD 3 0.11 0 - - - - - - - < 5 < 5 - - -

2,2-Dichloropropane mg/kg <LOD <LOD <LOD 3 No Criteria 0 - - - - - - - < 5 < 5 - - -

Chloroform mg/kg <LOD <LOD <LOD 3 0.75 0 - - - - - - - < 5 < 5 - - -

Bromochloromethane mg/kg <LOD <LOD <LOD 3 No Criteria 0 - - - - - - - < 5 < 5 - - -

SGVs & GACs

Assessment Scenario: Residential

Assessment Criteria Source: SGVs, GACs & C4SLs

Soil Organic Matter (%): SOM = 1%

ASSESSMENT

CRITERIA

No. >

ACDETERMINAND UNITS MINIMUM AVERAGE MAXIMUM

No. of

TESTS

Page 107: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

HUMAN HEALTH QUANTITATIVE RISK ASSESSMENT - SOILS SOM = 1% SOM = 1%

NATURAL GROUND SOM = 2.5%

1309 SOM = 6%

K&N Distribution Depot, Draycott in the Clay 1.774316

SOM = 1% AWS010.20 AWS010.50 AWS011.50 AWS020.90 AWS022.30 AWS030.70 AWS040.70 AWS050.75 AWS061.50 AWS071.40 AWS080.20 AWS080.60

AWS01 AWS01 AWS01 AWS02 AWS02 AWS03 AWS04 AWS05 AWS06 AWS07 AWS08 AWS08

0.20 0.50 1.50 0.90 2.30 0.70 0.70 0.75 1.50 1.40 0.20 0.60

SGVs & GACs

Assessment Scenario: Residential

Assessment Criteria Source: SGVs, GACs & C4SLs

Soil Organic Matter (%): SOM = 1%

ASSESSMENT

CRITERIA

No. >

ACDETERMINAND UNITS MINIMUM AVERAGE MAXIMUM

No. of

TESTS

1,1,1-Trichloroethane mg/kg <LOD <LOD <LOD 3 6.20 0 - - - - - - - < 5 < 5 - - -

1,1-Dichloropropene mg/kg <LOD <LOD <LOD 3 No Criteria 0 - - - - - - - < 10 < 10 - - -

Carbon Tetrachloride mg/kg <LOD <LOD <LOD 3 0.02 0 - - - - - - - < 5 < 5 - - -

1,2-Dichloroethane mg/kg <LOD <LOD <LOD 3 0.01 0 - - - - - - - < 5 < 5 - - -

Benzene mg/kg <LOD <LOD <LOD 23 0.33 0 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 < 2 -

1,2-Dichloropropane mg/kg <LOD <LOD <LOD 3 0.02 0 - - - - - - - < 5 < 5 - - -

Trichloroethene mg/kg <LOD <LOD <LOD 3 0.11 0 - - - - - - - < 5 < 5 - - -

Bromodichloromethane mg/kg <LOD <LOD <LOD 3 0.02 0 - - - - - - - < 5 < 5 - - -

Dibromomethane mg/kg <LOD <LOD <LOD 3 No Criteria 0 - - - - - - - < 5 < 5 - - -

TAME mg/kg <LOD <LOD <LOD 3 No Criteria 0 - - - - - - - < 5 < 5 - - -

cis-1,3-Dichloropropene mg/kg <LOD <LOD <LOD 3 No Criteria 0 - - - - - - - < 5 < 5 - - -

Toluene mg/kg <LOD <LOD <LOD 23 610.00 0 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 -

trans-1,3-Dichloropropene mg/kg <LOD <LOD <LOD 3 No Criteria 0 - - - - - - - < 5 < 5 - - -

1,1,2-Trichloroethane mg/kg <LOD <LOD <LOD 3 0.60 0 - - - - - - - < 10 < 10 - - -

1,3-Dichloropropane mg/kg <LOD <LOD <LOD 3 No Criteria 0 - - - - - - - < 5 < 5 - - -

Tetrachloroethene mg/kg <LOD <LOD <LOD 3 0.94 0 - - - - - - - < 5 < 5 - - -

Dibromochloromethane mg/kg <LOD <LOD <LOD 3 No Criteria 0 - - - - - - - < 5 < 5 - - -

1,2-Dibromoethane mg/kg <LOD <LOD <LOD 3 No Criteria 0 - - - - - - - < 5 < 5 - - -

Chlorobenzene mg/kg <LOD <LOD <LOD 3 0.33 0 - - - - - - - < 5 < 5 - - -

1,1,1,2-Tetrachloroethane mg/kg <LOD <LOD <LOD 3 0.90 0 - - - - - - - < 5 < 5 - - -

Ethyl Benzene mg/kg 0.19 0.19 0.19 3 350.00 0 - - - - - - - < 10 0.191 - - -

m,p-Xylene mg/kg 0.05 0.05 0.05 3 230.00 0 - - - - - - - < 10 0.053 - - -

o-Xylene mg/kg 0.02 0.02 0.02 23 250.00 0 < 10 < 10 < 10 < 10 < 10 < 10 < 10 < 10 0.016 < 10 < 10 -

Styrene mg/kg <LOD <LOD <LOD 3 8.10 0 - - - - - - - < 5 < 5 - - -

Bromoform mg/kg <LOD <LOD <LOD 3 2.80 0 - - - - - - - < 10 < 10 - - -

Isopropylbenzene mg/kg 0.29 0.29 0.29 3 11.00 0 - - - - - - - < 5 0.293 - - -

1,1,2,2-Tetrachloroethane mg/kg <LOD <LOD <LOD 3 1.40 0 - - - - - - - < 5 < 5 - - -

1,2,3-Trichloropropane mg/kg <LOD <LOD <LOD 3 No Criteria 0 - - - - - - - < 5 < 5 - - -

n-Propylbenzene mg/kg 0.55 0.55 0.55 3 34.00 0 - - - - - - - < 5 0.551 - - -

Bromobenzene mg/kg <LOD <LOD <LOD 3 0.87 0 - - - - - - - < 5 < 5 - - -

2-Chlorotoluene mg/kg <LOD <LOD <LOD 3 No Criteria 0 - - - - - - - < 5 < 5 - - -

1,3,5-Trimethylbenzene mg/kg 1.18 1.18 1.18 3 No Criteria 0 - - - - - - - < 5 1.18 - - -

4-Chlorotoluene mg/kg <LOD <LOD <LOD 3 No Criteria 0 - - - - - - - < 5 < 5 - - -

tert-Butylbenzene mg/kg <LOD <LOD <LOD 3 No Criteria 0 - - - - - - - < 5 < 5 - - -

1,2,4-Trimethylbenzene mg/kg 1.67 1.67 1.67 3 0.35 1 - - - - - - - < 5 1.67 - - -

sec-Butylbenzene mg/kg 0.56 0.56 0.56 3 No Criteria 0 - - - - - - - < 5 0.559 - - -

p-Isopropyltoluene mg/kg 1.44 1.44 1.44 3 No Criteria 0 - - - - - - - < 5 1.439 - - -

1,3-Dichlorobenzene mg/kg <LOD <LOD <LOD 3 0.29 0 - - - - - - - < 5 < 5 - - -

1,4-Dichlorobenzene mg/kg <LOD <LOD <LOD 3 30.00 0 - - - - - - - < 5 < 5 - - -

n-Butylbenzene mg/kg <LOD <LOD <LOD 3 No Criteria 0 - - - - - - - < 5 < 5 - - -

1,2-Dichlorobenzene mg/kg <LOD <LOD <LOD 3 16.00 0 - - - - - - - < 5 < 5 - - -

1,2-Dibromo-3-chloropropane mg/kg <LOD <LOD <LOD 3 No Criteria 0 - - - - - - - < 10 < 10 - - -

Hexachlorobutadiene mg/kg <LOD <LOD <LOD 3 0.21 0 - - - - - - - < 5 < 5 - - -

1,2,4-Trichlorobenzene mg/kg <LOD <LOD <LOD 2 1.80 0 - - - - - - - < 0.1 < 0.1 - - -

2-Nitrophenol mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - - - < 0.1 < 0.1 - - -

Nitrobenzene mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - - - < 0.1 < 0.1 - - -

0-Cresol mg/kg <LOD <LOD <LOD 2 80.00 0 - - - - - - - < 0.1 < 0.1 - - -

bis(2-chloroethoxy)methane mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - - - < 0.1 < 0.1 - - -

bis(2-chloroethyl)ether mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - - - < 0.1 < 0.1 - - -

2,4-Dichlorophenol mg/kg <LOD <LOD <LOD 2 0.87 0 - - - - - - - < 0.1 < 0.1 - - -

2-Chlorophenol mg/kg <LOD <LOD <LOD 2 0.87 0 - - - - - - - < 0.1 < 0.1 - - -

1,3-Dichlorobenzene mg/kg <LOD <LOD <LOD 3 0.29 0 - - - - - - - < 5 < 5 - - -

1,4-Dichlorobenzene mg/kg <LOD <LOD <LOD 3 30.00 0 - - - - - - - < 5 < 5 - - -

1,2-Dichlorobenzene mg/kg <LOD <LOD <LOD 3 16.00 0 - - - - - - - < 5 < 5 - - -

2,4-Dimethylphenol mg/kg <LOD <LOD <LOD 2 19.00 0 - - - - - - - < 0.15 < 0.15 - - -

Isophorone mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - - - < 0.1 < 0.1 - - -

Hexachloroethane mg/kg <LOD <LOD <LOD 2 0.20 0 - - - - - - - < 0.1 < 0.1 - - -

p-Cresol mg/kg <LOD <LOD <LOD 2 80.00 0 - - - - - - - < 0.15 < 0.15 - - -

2,4,6-Trichlorophenol mg/kg <LOD <LOD <LOD 2 0.87 0 - - - - - - - < 0.1 < 0.1 - - -

2,4,5-Trichlorophenol mg/kg <LOD <LOD <LOD 2 0.87 0 - - - - - - - < 0.1 < 0.1 - - -

2-Nitroaniline mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - - - < 0.1 < 0.1 - - -

4-Chloro-3-methylphenol mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - - - < 0.1 < 0.1 - - -

2-Methylnaphthalene mg/kg 0.00 0.00 0.00 2 No Criteria 0 - - - - - - - < 0.1 0.0004 - - -

Hexachlorocyclopentadiene mg/kg <LOD <LOD <LOD 2 19.00 0 - - - - - - - < 0.1 < 0.1 - - -

Page 108: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

HUMAN HEALTH QUANTITATIVE RISK ASSESSMENT - SOILS SOM = 1% SOM = 1%

NATURAL GROUND SOM = 2.5%

1309 SOM = 6%

K&N Distribution Depot, Draycott in the Clay 1.774316

SOM = 1% AWS010.20 AWS010.50 AWS011.50 AWS020.90 AWS022.30 AWS030.70 AWS040.70 AWS050.75 AWS061.50 AWS071.40 AWS080.20 AWS080.60

AWS01 AWS01 AWS01 AWS02 AWS02 AWS03 AWS04 AWS05 AWS06 AWS07 AWS08 AWS08

0.20 0.50 1.50 0.90 2.30 0.70 0.70 0.75 1.50 1.40 0.20 0.60

SGVs & GACs

Assessment Scenario: Residential

Assessment Criteria Source: SGVs, GACs & C4SLs

Soil Organic Matter (%): SOM = 1%

ASSESSMENT

CRITERIA

No. >

ACDETERMINAND UNITS MINIMUM AVERAGE MAXIMUM

No. of

TESTS

Hexachlorobutadiene mg/kg <LOD <LOD <LOD 3 0.21 0 - - - - - - - < 5 < 5 - - -

2,6-Dinitrotoluene mg/kg <LOD <LOD <LOD 2 0.78 0 - - - - - - - < 0.1 < 0.1 - - -

Dimethyl phthalate mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - - - < 0.1 < 0.1 - - -

2-Chloronaphthalene mg/kg <LOD <LOD <LOD 2 3.70 0 - - - - - - - < 0.1 < 0.1 - - -

4-Chloroaniline mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - - - < 0.2 < 0.2 - - -

4-Nitrophenol mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - - - < 0.1 < 0.1 - - -

4-Chlorophenyl phenyl ether mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - - - < 0.1 < 0.1 - - -

3-Nitroaniline mg/kg 0.00 0.00 0.00 2 No Criteria 0 - - - - - - - < 0.1 0.0001 - - -

4-Nitroaniline mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - - - < 0.1 < 0.1 - - -

4-Bromophenyl phenyl ether mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - - - < 0.1 < 0.1 - - -

Hexachlorobenzene mg/kg <LOD <LOD <LOD 2 19.00 0 - - - - - - - < 0.1 < 0.1 - - -

2,4-Dinitrotoluene mg/kg <LOD <LOD <LOD 2 1.50 0 - - - - - - - < 0.1 < 0.1 - - -

Diethyl phthalate mg/kg <LOD <LOD <LOD 2 120.00 0 - - - - - - - < 0.1 < 0.1 - - -

Dibenzofuran mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - - - < 0.1 < 0.1 - - -

Azobenzene mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - - - < 0.1 < 0.1 - - -

Dibutyl phthalate mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - - - < 0.15 < 0.15 - - -

Carbazole mg/kg <LOD <LOD <LOD 2 No Criteria 0 - - - - - - - < 0.1 < 0.1 - - -

bis(2-ethylhexyl)phthalate mg/kg <LOD <LOD <LOD 2 280.00 0 - - - - - - - < 0.2 < 0.2 - - -

Benzyl butyl phthalate mg/kg <LOD <LOD <LOD 2 1400.00 0 - - - - - - - < 0.1 < 0.1 - - -

Di-n-octyl phthalate mg/kg <LOD <LOD <LOD 2 2300.00 0 - - - - - - - < 0.1 < 0.1 - - -

Page 109: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

HUMAN HEALTH QUANTITATIVE RISK ASSESSMENT - SOILS

NATURAL GROUND

1309

K&N Distribution Depot, Draycott in the Clay

Asbestos Screen

pH

Total Cyanide

Total Organic Carbon (TOC)

Arsenic

Water Soluble Sulphate as SO4 (2:1)

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Selenium

Zinc

Naphthalene

Acenaphthylene

Acenaphthene

Fluorene

Phenanthrene

Anthracene

Fluoranthene

Pyrene

Benzo(a)anthracene

Chrysene

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Benzo(a)pyrene

Indeno(1,2,3-cd)pyrene

Di-benzo(a,h)anthracene

Benzo(ghi)perylene

TPH CWG - Aliphatic >C5 - C6

TPH CWG - Aliphatic >C6 - C8

TPH CWG - Aliphatic >C8 - C10

TPH CWG - Aliphatic >C10 - C12

TPH CWG - Aliphatic >C12 - C16

TPH CWG - Aliphatic >C16 - C21

TPH CWG - Aliphatic >C21 - C34

TPH CWG - Aromatic >C5 - C7

TPH CWG - Aromatic >C7 - C8

TPH CWG - Aromatic >C8 - C10

TPH CWG - Aromatic >C10 - C12

TPH CWG - Aromatic >C12 - C16

TPH CWG - Aromatic >C16 - C21

TPH CWG - Aromatic >C21 - C35

Benzene

Toluene

Ethylbenzene

m & p-xylene

o-Xylene

Monohydric Phenols

Dichlorodifluoromethane

Vinyl Chloride

Chloromethane

Chloroethane

Bromomethane

Trichlorofluoromethane

1,1-Dichloroethene

MTBE

trans-1,2-Dichloroethene

1,1-Dichloroethane

cis-1,2-Dichloroethene

2,2-Dichloropropane

Chloroform

Bromochloromethane

DETERMINAND

AWS100.10 AWS120.50 TP30.05 TP50.50 & BB TP90.20 TP110.30 TP170.10 WS5011.80 - 1.90WS5041.60 - 1.80WS5070.80 - 0.90WS5071.20 - 1.30WS5100.06 - 0.14WS5110.60 - 0.80WS5150.90 - 1.00WS5151.00 - 1.30HP10.15 HP20.10

AWS10 AWS12 TP3 TP5 TP9 TP11 TP17 WS501 WS504 WS507 WS507 WS510 WS511 WS515 WS515 HP1 HP2

0.10 0.50 0.05 0.50 & BB 0.20 0.30 0.10 1.80 - 1.90 1.60 - 1.80 0.80 - 0.90 1.20 - 1.30 0.06 - 0.14 0.60 - 0.80 0.90 - 1.00 1.00 - 1.30 0.15 0.10

Not Detected Not Detected Not Detected Not Detected Not Detected Not Detected Not Detected - Not Detected Not Detected - Not Detected - Not Detected - Not Detected Not Detected

7.1 7.6 7.8 7.8 7.9 7.5 7.8 7.6 7.9 8.4 8.3 - - 7.2 7.1 7 6.8

< 2 < 2 < 2 < 2 < 2 < 2 < 2 - < 2 < 2 - - - < 2 - < 2 < 2

3.7 0.1 2.1 0.2 1 2 0.5 - < 0.1 0.2 - - - 1.2 - 1.5 2.1

4 6 5 3 4 3 6 - 3 6 - - - < 2 - 7 8

0.03 0.08 0.09 0.03 1.09 0.18 0.73 0.4 0.05 0.55 0.07 - - 0.25 0.16 0.02 < 0.01

< 0.5 < 0.5 < 0.5 < 0.5 0.6 < 0.5 < 0.5 - < 0.5 < 0.5 - - - < 0.5 - < 0.5 < 0.5

25 39 34 16 21 35 48 - 28 26 - - - 31 - 32 36

18 12 19 7 35 23 32 - 6 8 - - - 20 - 39 20

34 12 35 52 33 34 27 - 10 9 - - - 26 - 21 10

< 1 < 1 < 1 < 1 < 1 < 1 < 1 - < 1 < 1 - - - < 1 - < 1 < 1

25 41 32 22 12 35 21 - 26 26 - - - 30 - 35 35

< 3 < 3 < 3 < 3 < 3 < 3 < 3 - < 3 < 3 - - - < 3 - < 3 < 3

87 72 113 49 129 100 102 - 67 45 - - - 87 - 87 74

< 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 < 0.1 - - - < 0.1 - < 0.1 < 0.1

< 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 < 0.1 - - - < 0.1 - < 0.1 < 0.1

< 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 < 0.1 - - - < 0.1 - < 0.1 < 0.1

< 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 < 0.1 - - - < 0.1 - < 0.1 < 0.1

< 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 < 0.1 - - - < 0.1 - < 0.1 < 0.1

< 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 < 0.1 - - - < 0.1 - < 0.1 < 0.1

< 0.1 < 0.1 0.18 < 0.1 0.19 < 0.1 0.16 - < 0.1 < 0.1 - - - < 0.1 - < 0.1 0.2

< 0.1 < 0.1 0.16 < 0.1 0.16 < 0.1 0.15 - < 0.1 < 0.1 - - - < 0.1 - < 0.1 0.15

< 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 < 0.1 - - - < 0.1 - < 0.1 < 0.1

< 0.1 < 0.1 < 0.1 < 0.1 0.11 < 0.1 0.13 - < 0.1 < 0.1 - - - < 0.1 - < 0.1 < 0.1

< 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 0.12 - < 0.1 < 0.1 - - - < 0.1 - < 0.1 < 0.1

< 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 < 0.1 - - - < 0.1 - < 0.1 < 0.1

< 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 < 0.1 - - - < 0.1 - < 0.1 < 0.1

< 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 < 0.1 - - - < 0.1 - < 0.1 < 0.1

< 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 < 0.1 - - - < 0.1 - < 0.1 < 0.1

< 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 < 0.1 - - - < 0.1 - < 0.1 < 0.1

< 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 - < 0.01 < 0.01 - - - < 0.01 - < 0.01 < 0.01

< 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 - < 0.05 < 0.05 - - - < 0.05 - < 0.05 < 0.05

< 1 < 1 < 1 < 1 < 1 < 1 < 1 - < 1 < 1 - - - < 1 - < 2 < 2

< 1 < 1 < 1 < 1 < 1 < 1 < 1 - < 1 < 1 - - - < 1 - < 2 < 2

< 1 < 1 < 1 < 1 < 1 < 1 < 1 - < 1 < 1 - - - < 1 - < 3 < 3

< 1 < 1 < 1 < 1 < 1 < 1 < 1 - < 1 < 1 - - - < 1 - < 3 < 3

< 6 < 6 < 6 < 6 < 6 < 6 < 6 - < 6 < 6 - - - < 6 - < 10 < 10

< 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 - < 0.01 < 0.01 - - - < 0.01 - < 0.01 < 0.01

< 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 - < 0.05 < 0.05 - - - < 0.05 - < 0.05 < 0.05

< 1 < 1 < 1 < 1 < 1 < 1 < 1 - < 1 < 1 - - - < 1 - < 2 < 2

< 1 < 1 < 1 < 1 < 1 < 1 < 1 - < 1 < 1 - - - < 1 - < 2 < 2

< 1 < 1 < 1 < 1 < 1 < 1 < 1 - < 1 < 1 - - - < 1 - < 2 < 2

< 1 < 1 < 1 < 1 < 1 < 1 < 1 - < 1 < 1 - - - < 1 - 6 < 3

< 6 < 6 < 6 < 6 < 6 < 6 < 6 - < 6 < 6 - - - < 6 - < 10 < 10

< 2 < 2 < 2 < 2 < 2 < 2 < 2 - < 2 < 2 - - - < 2 - < 2 < 2

< 5 < 5 < 5 < 5 < 5 < 5 < 5 - < 5 < 5 - - - < 5 - < 5 < 5

< 10 < 10 < 10 < 10 < 10 < 10 < 10 - < 10 < 10 - - - < 10 - < 10 < 10

< 10 < 10 < 10 < 10 < 10 < 10 < 10 - < 10 < 10 - - - < 10 - < 10 < 10

< 10 < 10 < 10 < 10 < 10 < 10 < 10 - < 10 < 10 - - - < 10 - < 10 < 10

< 2 < 2 < 2 < 2 < 2 < 2 < 2 - < 2 < 2 - - - < 2 - < 2 < 2

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 10 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 10 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

< 5 < 5 < 5 < 5 < 5 < 5 < 5 - < 5 < 5 - - - < 5 - < 5 < 5

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

Page 110: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

HUMAN HEALTH QUANTITATIVE RISK ASSESSMENT - SOILS

NATURAL GROUND

1309

K&N Distribution Depot, Draycott in the Clay

DETERMINAND

1,1,1-Trichloroethane

1,1-Dichloropropene

Carbon Tetrachloride

1,2-Dichloroethane

Benzene

1,2-Dichloropropane

Trichloroethene

Bromodichloromethane

Dibromomethane

TAME

cis-1,3-Dichloropropene

Toluene

trans-1,3-Dichloropropene

1,1,2-Trichloroethane

1,3-Dichloropropane

Tetrachloroethene

Dibromochloromethane

1,2-Dibromoethane

Chlorobenzene

1,1,1,2-Tetrachloroethane

Ethyl Benzene

m,p-Xylene

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,2,3-Trichloropropane

n-Propylbenzene

Bromobenzene

2-Chlorotoluene

1,3,5-Trimethylbenzene

4-Chlorotoluene

tert-Butylbenzene

1,2,4-Trimethylbenzene

sec-Butylbenzene

p-Isopropyltoluene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

n-Butylbenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-chloropropane

Hexachlorobutadiene

1,2,4-Trichlorobenzene

2-Nitrophenol

Nitrobenzene

0-Cresol

bis(2-chloroethoxy)methane

bis(2-chloroethyl)ether

2,4-Dichlorophenol

2-Chlorophenol

1,3-Dichlorobenzene

1,4-Dichlorobenzene

1,2-Dichlorobenzene

2,4-Dimethylphenol

Isophorone

Hexachloroethane

p-Cresol

2,4,6-Trichlorophenol

2,4,5-Trichlorophenol

2-Nitroaniline

4-Chloro-3-methylphenol

2-Methylnaphthalene

Hexachlorocyclopentadiene

AWS100.10 AWS120.50 TP30.05 TP50.50 & BB TP90.20 TP110.30 TP170.10 WS5011.80 - 1.90WS5041.60 - 1.80WS5070.80 - 0.90WS5071.20 - 1.30WS5100.06 - 0.14WS5110.60 - 0.80WS5150.90 - 1.00WS5151.00 - 1.30HP10.15 HP20.10

AWS10 AWS12 TP3 TP5 TP9 TP11 TP17 WS501 WS504 WS507 WS507 WS510 WS511 WS515 WS515 HP1 HP2

0.10 0.50 0.05 0.50 & BB 0.20 0.30 0.10 1.80 - 1.90 1.60 - 1.80 0.80 - 0.90 1.20 - 1.30 0.06 - 0.14 0.60 - 0.80 0.90 - 1.00 1.00 - 1.30 0.15 0.10

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 10 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

< 2 < 2 < 2 < 2 < 2 < 2 < 2 - < 2 < 2 - - - < 2 - < 2 < 2

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

< 5 < 5 < 5 < 5 < 5 < 5 < 5 - < 5 < 5 - - - < 5 - < 5 < 5

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 10 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 10 - - - -

- - - - - - - - - - - - < 10 - - - -

< 10 < 10 < 10 < 10 < 10 < 10 < 10 - < 10 < 10 - - - < 10 - < 10 < 10

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 10 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 10 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

Page 111: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

HUMAN HEALTH QUANTITATIVE RISK ASSESSMENT - SOILS

NATURAL GROUND

1309

K&N Distribution Depot, Draycott in the Clay

DETERMINAND

Hexachlorobutadiene

2,6-Dinitrotoluene

Dimethyl phthalate

2-Chloronaphthalene

4-Chloroaniline

4-Nitrophenol

4-Chlorophenyl phenyl ether

3-Nitroaniline

4-Nitroaniline

4-Bromophenyl phenyl ether

Hexachlorobenzene

2,4-Dinitrotoluene

Diethyl phthalate

Dibenzofuran

Azobenzene

Dibutyl phthalate

Carbazole

bis(2-ethylhexyl)phthalate

Benzyl butyl phthalate

Di-n-octyl phthalate

AWS100.10 AWS120.50 TP30.05 TP50.50 & BB TP90.20 TP110.30 TP170.10 WS5011.80 - 1.90WS5041.60 - 1.80WS5070.80 - 0.90WS5071.20 - 1.30WS5100.06 - 0.14WS5110.60 - 0.80WS5150.90 - 1.00WS5151.00 - 1.30HP10.15 HP20.10

AWS10 AWS12 TP3 TP5 TP9 TP11 TP17 WS501 WS504 WS507 WS507 WS510 WS511 WS515 WS515 HP1 HP2

0.10 0.50 0.05 0.50 & BB 0.20 0.30 0.10 1.80 - 1.90 1.60 - 1.80 0.80 - 0.90 1.20 - 1.30 0.06 - 0.14 0.60 - 0.80 0.90 - 1.00 1.00 - 1.30 0.15 0.10

- - - - - - - - - - - - < 5 - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

- - - - - - - - - - - - - - - - -

Page 112: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

1

1

1

1

1 TABLE SHOWING PHYTOTOXICITY ASSESSMENT FOR MADE GROUND

1

1

1

Copper mg/kg 10.00 40.95 90.00 22 200.00 0

1

Nickel mg/kg 15.00 33.00 60.00 22 110.00 0

1

Zinc mg/kg 56.00 144.27 347.00 22 300.00 2

1

1 TABLE SHOWING PHYTOTOXICITY ASSESSMENT FOR NATURAL SOILS

1

1

1

Copper mg/kg 6.00 17.70 39.00 20 200.00 0

1

Nickel mg/kg 12.00 30.70 50.00 20 110.00 0

1

Zinc mg/kg 45.00 78.80 129.00 20 300.00 0

1

AWS03 [0.35m

bgl] at -mg/kg,

AWS04 [0.32m

bgl] at -mg/kg,

AWS05 [0.20m

bgl] at

132mg/kg,

AWS06 [0.50m

bgl] at -mg/kg,

AWS07 [0.30m

bgl] at -mg/kg,

AWS07 [0.60m

bgl] at

64mg/kg,

AWS09

[0.20m bgl]

at -mg/kg,

AWS03 [0.35m bgl] at -mg/kg,AWS04 [0.32m bgl] at -mg/kg,AWS05 [0.20m bgl] at 29mg/kg,AWS06 [0.50m bgl] at -mg/kg,AWS07 [0.30m bgl] at -mg/kg,AWS07 [0.60m bgl] at 36mg/kg,AWS09 [0.20m bgl] at -mg/kg,

MINIMUM AVERAGE MAXIMUMNo. of

TESTS

DETERMINAND UNITS MINIMUM AVERAGE MAXIMUMNo. of

TESTS

ASSESSMENT

CRITERIA

No. >

AC

ASSESSMENT

CRITERIA

No. >

ACDETERMINAND UNITS

PHYTOTOXICITY RISK ASSESSMENT

1309

K&N Distribution Depot, Draycott in the Clay

DETAILS

-

-

-

Risk Criteria: British Standard BS 3882:2007 (Specification for topsoil and requirements for

use)

DETAILS

-

-

TP10 [0.10 - 0.30m bgl] at 323mg/kg,WS514 [0.10 - 0.50m bgl] at 347mg/kg

Page 113: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

TABLE SHOWING WATER PIPELINE ASSESSMENT

PE EXCEEDED PVC EXCEEDED

Total VOC (with TICs)* µg/kg 500.00 125.00

BTEX & MTBE µg/kg 100.00 NO 30.00 NO 10.00

**Total SVOC Suite (with TIC) mg/kg 2.00 1.40

Phenols mg/kg 2.00 0.40 <LOD

Cresols & Chlorinated Phenols mg/kg 2.00 0.04

†Ethers mg/kg 0.50 - 1.00 - -

†Nitrobenzene mg/kg 0.50 - 0.40 - -

†Ketones mg/kg 0.50 - 0.02 - -

†Aldehydes mg/kg 0.50 - 0.02 - -

Mineral Oils (C11 to C20) mg/kg 10.00 No effect

Mineral Oils (C21 to C40) mg/kg 500.00 No effect

Conductivity µ2/cm - - - - -

Redox Potential mV - - - - -

pH - - -

†Amines ug/kg N/A - No effect - -

NOTES:

*Minus total concentration of BTEX + MTBE.

**Minus total concentration of phenols, cresols and chlorinated phenols.

†Only required if current or historical site use indicates they may be present.

^Only applicable when selecting suitable barrier pipe (see UKWIR Guidance document)

RISK CRITERIA:

POTABLE WATER PIPELINE RISK ASSESSMENT

1309

K&N Distribution Depot, Draycott in the Clay

UK Water Industry Research (UKWIR). Guidance for the Selection of Water Supply

Pipes to be used in Brownfield Sites. Ref. 10/WM/03/21. 2010

DETERMINAND UNITSMAXIMUM

CONCENTRATION

THRESHOLD THRESHOLD

GROUP 1

GROUP 6

GROUP 2

GROUP 3

GROUP 4

GROUP 5^

Page 114: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

TABLE SHOWING BURIED CONCRETE ASSESSMENT

DETERMINAND UNITS NO. OF TESTS MIN MAXCHARACTERISTIC

VALUEBRE CLASSIFICATION

Water Soluble Sulphate as SO4 g/l 24 0.02 2.24 1.1 DS2

pH - 24 7 9.10 7.4 AC2

Water Soluble Sulphate as SO4 g/l 23 0.01 1.09 0.6 DS2

pH - 23 6.80 9.40 7.0 AC2

NOTES:

DATA CRITERIA:

BRE Special Digest 1:2005, 3rd Edition, ‘Concrete in Aggressive Ground.’

BURIED CONCRETE ASSESSMENT

1309

Where there are >10 results, the Characteristic Value is based on the mean of the highest 20% of values for SO4, or the mean of the lowest

20% of values for pH. Where there are <10 samples, the Characteristic Value is based on lowest pH value / highest SO4.

K&N Distribution Depot, Draycott in the Clay

NATURAL GROUND

MADE GROUND

Page 115: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

CONTROLLED WATERS RISK ASSESSMENT

1309

K&N Distribution Depot, Draycott in the Clay

AWS02 AWS03 AWS04 AWS06 AWS07 AWS11 WS501 WS502 WS503

AWS02 AWS03 AWS04 AWS06 AWS07 AWS11 WS501 WS502 WS503

pH NA 7.10 7.46 8.50 13 No criteria 0 No criteria 0 No criteria 0 7.5 7.1 7.1 7.4 7.7 7.1 7.1 7.3 7.3

Total Cyanide µg/l <LOD <LOD <LOD 13 No criteria 0 No criteria 0 No criteria 0 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5 < 5

Sulphate as SO4 mg/l 33.00 251.54 962.00 13 250.00 3 400.00 2 250.00 3 84 280 214 73 87 954 962 77 63

Sulphide µg/l <LOD <LOD <LOD 0 No criteria 0 0.25 0 No criteria 0

Total Organic Carbon (TOC) µg/l 2.60 26.12 64.60 13 No criteria 0 No criteria 0 No criteria 0 6.3 3.6 7.1 11.8 2.6 3.5 36 60.8 64.6

37 Arsenic (dissolved) µg/l 13.00 14.00 15.00 13 10.00 2 50.00 0 10.00 2 < 10 < 10 < 10 < 10 < 10 13 < 10 < 10 < 10

Boron (dissolved) µg/l 0.06 0.13 0.18 13 1.00 0 2.00 0 0.30 0 0.121 0.088 0.06 < 0050 0.182 0.141 0.161 0.159 0.157

26 Cadmium (dissolved) µg/l <LOD <LOD <LOD 13 5.00 0 5.00 0 3.00 0 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5

Chromium (dissolved) µg/l 6.00 8.33 14.00 13 50.00 0 250.00 0 50.00 0 < 5 < 5 < 5 < 5 6 < 5 < 5 < 5 7

Copper (dissolved) µg/l 20.00 21.33 22.00 13 2000.00 0 28.00 0 2000.00 0 < 10 22 20 < 10 < 10 22 < 10 < 10 < 10

200 Lead (dissolved) µg/l 7.00 9.75 14.00 13 25.00 0 250.00 0 10.00 2 8 7 14 < 5 10 < 5 < 5 < 5 < 5

Mercury (dissolved) µg/l <LOD <LOD <LOD 13 1.00 0 1.00 0 1.00 0 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05

Nickel (dissolved) µg/l <LOD <LOD <LOD 13 20.00 0 50.00 0 20.00 0 < 7 < 7 < 7 < 7 < 7 < 7 < 7 < 7 < 7

Selenium (dissolved) µg/l 6.00 6.00 6.00 13 10.00 0 No criteria 0 10.00 0 < 5 < 5 < 5 < 5 6 < 5 < 5 < 5 < 5

Zinc (dissolved) µg/l 7.00 24.71 39.00 13 5000.00 0 500.00 0 3000.00 0 20 28 33 7 39 38 8 < 5 < 5

Total Phenols µg/l <LOD <LOD <LOD 13 0.50 0 30.00 0 No criteria 0 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5

EPH (C10 - C40) µg/l 36.00 301.00 791.00 13 No criteria 0 No criteria 0 No criteria 0 36 < 10 76 791 < 10 < 10 < 10 < 10 < 10

Naphthalene µg/l <LOD <LOD <LOD 13 No criteria 0 10.00 0 No criteria 0 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Benzo(a)pyrene µg/l <LOD <LOD <LOD 13 0.01 0 No criteria 0 0.70 0 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Total EPA-16 PAHs µg/l 0.57 0.57 0.57 13 No criteria 0 No criteria 0 No criteria 0 < 0.01 < 0.01 < 0.01 0.57 < 0.01 < 0.01 < 0.01 < 0.01 < 0.01

Total >C5 - C35 µg/l <LOD <LOD <LOD 0 No criteria 0 No criteria 0 No criteria 0

Dichlorodifluoromethane µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

Vinyl Chloride µg/l <LOD <LOD <LOD 10 0.50 0 No criteria 0 5.00 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

Chloromethane µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

Chloroethane µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

Bromomethane µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

Trichlorofluoromethane µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

5 1,1-Dichloroethene µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 30.00 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

MTBE µg/l 195.00 195.00 195.00 6 No criteria 0 No criteria 0 No criteria 0 195 < 10 < 10 < 10 < 10 < 10 - - -

trans-1,2-Dichloroethene µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

1,1-Dichloroethane µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

cis-1,2-Dichloroethene µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

2,2-Dichloropropane µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

Chloroform µg/l <LOD <LOD <LOD 10 No criteria 0 12.00 0 200.00 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

Bromochloromethane µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 10 - < 10 - < 10 - < 10 < 10 < 10

1,1,1-Trichloroethane µg/l <LOD <LOD <LOD 10 No criteria 0 100.00 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

1,1-Dichloropropene µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

Carbon Tetrachloride µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

1,2-Dichloroethane µg/l <LOD <LOD <LOD 10 3.00 0 10.00 0 30.00 0 < 10 - < 10 - < 10 - < 10 < 10 < 10

Benzene µg/l <LOD <LOD <LOD 6 1.00 0 30.00 0 10.00 0 < 1 < 1 < 1 < 1 < 1 < 1 - - -

1,2-Dichloropropane µg/l <LOD <LOD <LOD 10 0.10 0 No criteria 0 20.00 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

Trichloroethene µg/l 4680.00 4680.00 4680.00 10 10.00 1 10.00 1 70.00 1 < 5 - 4680 - < 5 - < 5 < 5 < 5

Bromodichloromethane µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

Dibromomethane µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

TAME µg/l 530.00 530.00 530.00 10 No criteria 0 No criteria 0 No criteria 0 530 - < 5 - < 5 - < 5 < 5 < 5

0.9 cis-1,3-Dichloropropene µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

Toluene µg/l <LOD <LOD <LOD 6 No criteria 0 50.00 0 700.00 0 < 5 < 5 < 5 < 5 < 5 < 5 - - -

trans-1,3-Dichloropropene µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

1,1,2-Trichloroethane µg/l <LOD <LOD <LOD 10 No criteria 0 400.00 0 No criteria 0 < 10 - < 10 - < 10 - < 10 < 10 < 10

1,3-Dichloropropane µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

Tetrachloroethene µg/l <LOD <LOD <LOD 10 10.00 0 10.00 0 40.00 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

Dibromochloromethane µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

1,2-Dibromoethane µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

Chlorobenzene µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

1,1,1,2-Tetrachloroethane µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

Ethyl Benzene µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 300.00 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

m,p-Xylene µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 10 - < 10 - < 10 - < 10 < 10 < 10

o-Xylene µg/l 31.00 31.00 31.00 6 No criteria 0 No criteria 0 No criteria 0 < 5 < 5 < 5 31 < 5 < 5 - - -

Styrene µg/l <LOD <LOD <LOD 10 No criteria 0 50.00 0 20.00 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

Bromoform µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 10 - < 10 - < 10 - < 10 < 10 < 10

Isopropylbenzene µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

1,1,2,2-Tetrachloroethane µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 10 - < 10 - < 10 - < 10 < 10 < 10

1,2,3-Trichloropropane µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

n-Propylbenzene µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

DETERMINAND UNITS MINIMUM AVERAGE MAXIMUM UK DWSNo. >

ACWHO

No. of

TESTS

No. >

ACEQS FW

No. >

AC

SGVs & GACsData Source: Environment Agency H1 Environmental Risk

Assessment – Annex J, v2.0, April 2010 & Petroleum

Products in Drinking-Water, WHO

(WHO/SDE/WSH/05.08/123)2 - Environmental Quality Standards Freshwater (EQS FW)

1 - UK Drinking Water Standards (UK DWS)

Water Quality Standard (WQS) Selection Hierarchy:

3 - World Health Organisation (WHO)

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CONTROLLED WATERS RISK ASSESSMENT

1309

K&N Distribution Depot, Draycott in the Clay

AWS02 AWS03 AWS04 AWS06 AWS07 AWS11 WS501 WS502 WS503

AWS02 AWS03 AWS04 AWS06 AWS07 AWS11 WS501 WS502 WS503DETERMINAND UNITS MINIMUM AVERAGE MAXIMUM UK DWS

No. >

ACWHO

No. of

TESTS

No. >

ACEQS FW

No. >

AC

SGVs & GACsData Source: Environment Agency H1 Environmental Risk

Assessment – Annex J, v2.0, April 2010 & Petroleum

Products in Drinking-Water, WHO

(WHO/SDE/WSH/05.08/123)2 - Environmental Quality Standards Freshwater (EQS FW)

1 - UK Drinking Water Standards (UK DWS)

Water Quality Standard (WQS) Selection Hierarchy:

3 - World Health Organisation (WHO)

Bromobenzene µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

2-Chlorotoluene µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

1,3,5-Trimethylbenzene µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

4-Chlorotoluene µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

tert-Butylbenzene µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

1,2,4-Trimethylbenzene µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

sec-Butylbenzene µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

p-Isopropyltoluene µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

1,3-Dichlorobenzene µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

1,4-Dichlorobenzene µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 300.00 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

n-Butylbenzene µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 No criteria 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

1,2-Dichlorobenzene µg/l <LOD <LOD <LOD 10 No criteria 0 No criteria 0 1000.00 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

1,2-Dibromo-3-chloropropane µg/l <LOD <LOD <LOD 10 0.10 0 No criteria 0 1.00 0 < 10 - < 10 - < 10 - < 10 < 10 < 10

Hexachlorobutadiene µg/l <LOD <LOD <LOD 10 No criteria 0 0.10 0 0.60 0 < 5 - < 5 - < 5 - < 5 < 5 < 5

#N/A #N/A #N/A

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Page 117: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

CONTROLLED WATERS RISK ASSESSMENT

1309

K&N Distribution Depot, Draycott in the Clay

pH

Total Cyanide

Sulphate as SO4Sulphide

Total Organic Carbon (TOC)

Arsenic (dissolved)

Boron (dissolved)

Cadmium (dissolved)

Chromium (dissolved)

Copper (dissolved)

Lead (dissolved)

Mercury (dissolved)

Nickel (dissolved)

Selenium (dissolved)

Zinc (dissolved)

Total Phenols

EPH (C10 - C40)

Naphthalene

Benzo(a)pyrene

Total EPA-16 PAHs

Total >C5 - C35

Dichlorodifluoromethane

Vinyl Chloride

Chloromethane

Chloroethane

Bromomethane

Trichlorofluoromethane

1,1-Dichloroethene

MTBE

trans-1,2-Dichloroethene

1,1-Dichloroethane

cis-1,2-Dichloroethene

2,2-Dichloropropane

Chloroform

Bromochloromethane

1,1,1-Trichloroethane

1,1-Dichloropropene

Carbon Tetrachloride

1,2-Dichloroethane

Benzene

1,2-Dichloropropane

Trichloroethene

Bromodichloromethane

Dibromomethane

TAME

cis-1,3-Dichloropropene

Toluene

trans-1,3-Dichloropropene

1,1,2-Trichloroethane

1,3-Dichloropropane

Tetrachloroethene

Dibromochloromethane

1,2-Dibromoethane

Chlorobenzene

1,1,1,2-Tetrachloroethane

Ethyl Benzene

m,p-Xylene

o-Xylene

Styrene

Bromoform

Isopropylbenzene

1,1,2,2-Tetrachloroethane

1,2,3-Trichloropropane

n-Propylbenzene

DETERMINAND

WS507 WS513 WS514 WS517

WS507 WS513 WS514 WS517

8.5 7.6 7.8 7.5 - -

< 5 < 5 < 5 < 5 - -

55 33 248 140 - -

9.6 59.5 26.7 47.5 - -

15 < 10 < 10 < 10 - -

0.115 0.114 0.131 0.183 - -

< 0.5 < 0.5 < 0.5 < 0.5 - -

8 9 14 6 - -

< 10 < 10 < 10 < 10 - -

< 5 < 5 < 5 < 5 - -

< 0.05 < 0.05 < 0.05 < 0.05 - -

< 7 < 7 < 7 < 7 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 0.5 < 0.5 < 0.5 < 0.5 - -

< 10 < 10 < 10 < 10 - -

< 0.01 < 0.01 < 0.01 < 0.01 - -

< 0.01 < 0.01 < 0.01 < 0.01 - -

< 0.01 < 0.01 < 0.01 < 0.01 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

- - - - - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 10 < 10 < 10 < 10 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 10 < 10 < 10 < 10 - -

- - - - - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

- - - - - -

< 5 < 5 < 5 < 5 - -

< 10 < 10 < 10 < 10 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 10 < 10 < 10 < 10 - -

- - - - - -

< 5 < 5 < 5 < 5 - -

< 10 < 10 < 10 < 10 - -

< 5 < 5 < 5 < 5 - -

< 10 < 10 < 10 < 10 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

Page 118: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

CONTROLLED WATERS RISK ASSESSMENT

1309

K&N Distribution Depot, Draycott in the Clay

DETERMINAND

Bromobenzene

2-Chlorotoluene

1,3,5-Trimethylbenzene

4-Chlorotoluene

tert-Butylbenzene

1,2,4-Trimethylbenzene

sec-Butylbenzene

p-Isopropyltoluene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

n-Butylbenzene

1,2-Dichlorobenzene

1,2-Dibromo-3-chloropropane

Hexachlorobutadiene

WS507 WS513 WS514 WS517

WS507 WS513 WS514 WS517

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 5 < 5 < 5 < 5 - -

< 10 < 10 < 10 < 10 - -

< 5 < 5 < 5 < 5 - -

Page 119: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

APPENDIX F

FIELD MONITORING DATA

Page 120: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Water Sampling Log

1

Project Number:

1309 Site

Location: K&N Distribution Depot,

Draycott-in-the-Clay Date: 15/07/2014

Location Reference: AWS02

Weather: Overcast

Condition of headworks: Good

Sampled by: JM

Description of monitoring point (MP)

Ground Level

Depth to LNAPL below MP (m)

0 Thickness of LNAPL (m)

0

Depth to DNAPL below MP (m)

0 Thickness of DNAPL (m)

0

Depth to water below MP (m)

0.94 Total well depth below MP (m)

3.95

Water column in well (m)

2.99 Diameter of well casing (mm)

50mm

Volume of water purged (l)

12 Well volumes Purged Dry

Purging method Bailer

Field Parameters

Time sampling began: 14:46 Time sampling completed:

18:30

Time Colour Temp (0C)

pH Redox (mV)

Odour Conductivity

(ms)

Amount of water purged

(L)

Dissolved Oxygen

14:46 Light Tan 18.7 7.45 -31 Nil 916 12 6.4

18:30 Orangish

Brown 13.4 7.65 39 Nil 933 16 6.3

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Water Sampling Log

2

Project Number:

1309 Site

Location: K&N Distribution Depot,

Draycott-in-the-Clay Date: 15/07/2014

Location Reference: AWS03

Weather: Sun/Cloud

Condition of headworks: Good

Sampled by: JM

Description of monitoring point (MP)

Ground Level

Depth to LNAPL below MP (m)

0 Thickness of LNAPL (m)

0

Depth to DNAPL below MP (m)

0 Thickness of DNAPL (m)

0

Depth to water below MP (m)

1.27 Total well depth below MP (m)

3.95

Water column in well (m)

2.68 Diameter of well casing (mm)

50mm

Volume of water purged (l)

12 Well volumes Purged Dry

Purging method Bailer

Field Parameters

Time sampling began: 15:28 Time sampling completed:

16:00

Time Colour Temp (0C)

pH Redox (mV)

Odour Conductivity

(ms)

Amount of water purged

(L)

Dissolved Oxygen

15:28 Light

Orange 15.5 7.61 74 Nil 1433 12 7.4

16:00 Reddish Brown

15.5 7.60 52 Nil 1325 14 7.4

Page 122: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Water Sampling Log

3

Project Number:

1309 Site

Location: K&N Distribution Depot,

Draycott-in-the-Clay Date: 15&16/7/2014

Location Reference: AWS04

Weather: Sunny

Condition of headworks: Good

Sampled by: JM

Description of monitoring point (MP)

Ground Level

Depth to LNAPL below MP (m)

0 Thickness of LNAPL (m)

0

Depth to DNAPL below MP (m)

0 Thickness of DNAPL (m)

0

Depth to water below MP (m)

1.73 Total well depth below MP (m)

3.95

Water column in well (m)

2.22 Diameter of well casing (mm)

50mm

Volume of water purged (l)

6 Well volumes Purged Dry

Purging method Bailer

Field Parameters

Time sampling began: 09:15 (16/07/2014)

Time sampling completed:

09:20 (16/07/2014)

Time Colour Temp (0C)

pH Redox (mV)

Odour Conductivity

(ms)

Amount of water purged

(L)

Dissolved Oxygen

15/07/2014 17:48

Reddish Brown

15.5 7.47 73 Nil 1429 4 4.2

16/07/2014 09:15

Reddish Brown

15.8 7.4 111 Nil 1309 4 4.1

Page 123: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Water Sampling Log

4

Project Number:

1309 Site

Location: K&N Distribution Depot,

Draycott-in-the-Clay Date: 15&16/7/2014

Location Reference: AWS06

Weather: Sunny

Condition of headworks: Good

Sampled by: JM

Description of monitoring point (MP)

Ground Level

Depth to LNAPL below MP (m)

0 Thickness of LNAPL (m)

0

Depth to DNAPL below MP (m)

0 Thickness of DNAPL (m)

0

Depth to water below MP (m)

2.48 Total well depth below MP (m)

3.75

Water column in well (m)

1.20 Diameter of well casing (mm)

50mm

Volume of water purged (l)

4 Well volumes Dry

Purging method Bailer

Field Parameters

Time sampling began: 09:30 (16/07/2014)

Time sampling completed:

09:45 (16/07/2014)

Time Colour Temp (0C)

pH Redox (mV)

Odour Conductivit

y (ms)

Amount of water purged

(L)

Dissolved Oxygen

08:30 Reddish Brown

15.0 8.1 147 Diesel 1058 4 6.1

9:45 Reddish Brown

15.5 8.0 117 Diesel 1128 2.5 4.3

Page 124: APPENDIX C CHEMICAL TEST CERTIFICATES Application...110722 110723 110725 110727 110728 Determinand Unit RL Accreditation Asbestos Screen N/a ISO17025 Not Detected pH pH Units N/a MCERTS

Water Sampling Log

5

Project Number:

1309 Site

Location: K&N Distribution Depot,

Draycott-in-the-Clay Date: 15&16/7/2014

Location Reference: AWS07

Weather: Sun & Cloud, Slight Wind

Condition of headworks: Good

Sampled by: JM

Description of monitoring point (MP)

Ground Level

Depth to LNAPL below MP (m)

0 Thickness of LNAPL (m)

0

Depth to DNAPL below MP (m)

0 Thickness of DNAPL (m)

0

Depth to water below MP (m)

2.7 Total well depth below MP (m)

3.0

Water column in well (m)

0.3 Diameter of well casing (mm)

50mm

Volume of water purged (l)

3/4 Well volumes Dry

Purging method Bailer

Field Parameters

Time sampling began: 10:30 Time sampling completed:

10:45

Time Colour Temp (0C)

pH Redox (mV)

Odour Conductivit

y (ms)

Amount of water purged

(L)

Dissolved Oxygen

16:09 LIMITED SAMPLE

10:45 LIMITED SAMPLE

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Water Sampling Log

6

Project Number:

1309 Site

Location: K&N Distribution Depot,

Draycott-in-the-Clay Date: 15/7/2014

Location Reference: AWS11

Weather: Sun & Cloud

Condition of headworks: Good

Sampled by: JM

Description of monitoring point (MP)

Ground Level

Depth to LNAPL below MP (m)

0 Thickness of LNAPL (m)

0

Depth to DNAPL below MP (m)

0 Thickness of DNAPL (m)

0

Depth to water below MP (m)

1.10 Total well depth below MP (m)

2.9

Water column in well (m)

1.8 Diameter of well casing (mm)

50

Volume of water purged (l)

8 Well volumes Dry

Purging method Bailer

Field Parameters

Time sampling began: 11:00 Time sampling completed:

11:15

Time Colour Temp (0C)

pH Redox (mV)

Odour Conductivit

y (ms)

Amount of water purged

(L)

Dissolved Oxygen

10:00 Reddish Brown

15.5 7.29 61 Nil 2110 8 6.4

11:00 Reddish Brown

15.5 7.30 82 Nil 2142 4 5.2

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Water Sampling Log

7

Project Number:

1309 Site

Location: K&N Distribution Depot,

Draycott-in-the-Clay Date: 15/7/2014

Location Reference: BH1

Weather: Sunny

Condition of headworks: Good- Historic Borehole

Sampled by: JM

Description of monitoring point (MP)

Ground Level

Depth to LNAPL below MP (m)

1.61 Thickness of LNAPL (m)

0.025

Depth to DNAPL below MP (m)

0 Thickness of DNAPL (m)

0

Depth to water below MP (m)

1.585 Total well depth below MP (m)

-

Water column in well (m)

- Diameter of well casing (mm)

-

Volume of water purged (l)

- Well volumes -

Method Bailer

Time sampling began: 19:20 Time sampling completed:

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Water Sampling Log

8

Project Number:

1309 Site

Location: K&N Distribution Depot,

Draycott-in-the-Clay Date: 15/7/2014

Location Reference: BH3

Weather: Sunny

Condition of headworks: Good- Historic Borehole

Sampled by: JM

Description of monitoring point (MP)

Ground Level

Depth to LNAPL below MP (m)

2.04 Thickness of LNAPL (m)

0.03

Depth to DNAPL below MP (m)

0 Thickness of DNAPL (m)

0

Depth to water below MP (m)

2.01 Total well depth below MP (m)

-

Water column in well (m)

- Diameter of well casing (mm)

-

Volume of water purged (l)

- Well volumes -

Method Bailer

Remarks: Strong Diesel odour

Time sampling began: 19:20 Time sampling completed:

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Borehole Development Log Project Number:

1309 Site Location:

K+N Distribution Depot, Draycott-in-the-Clay

Date of purging:

23/10/14

Method used to purge: Bailer Sampler: Amy Khan

Borehole ID Pre – Purge Post - Purge

WS501

Depth to Water (m bgl) 2.35 DRY

Depth to Base (m bgl) 3.78 3.78

Water purged (l) 6

Recharge Rate: Slow to moderate recharge

WS502

Depth to Water 2.49 DRY

Depth to Base 3.93 3.93

Water purged 8

Recharge Rate: Very slow recharge

WS503

Depth to Water 3.33 DRY

Depth to Base 4.0 4.0

Water Purged 2

Recharge Rate: Very slow recharge

WS507

Depth to Water 1.4 DRY

Depth to Base 3.0 3.0

Water Purged 12

Recharge Rate: Very slow recharge

WS513

Depth to Water 1.98 DRY

Depth to Base 3.93 3.93

Water purged 5

Recharge Rate: Slow recharge

WS515

Depth to Water 2.08 3.89

Depth to Base 4.09 4.09

Water purged 47

Recharge Rate: Rate of 5mm/ 10 seconds

WS514

Depth to Water 1.66 DRY

Depth to Base 3.72 3.72

Water Purged 9

Recharge Rate: Moderate to quick recharge

WS517

Depth to Water 0.55 DRY

Depth to Base 4.05 4.05

Water Purged 17

Recharge Rate: Rate of 1cm/ 15 seconds

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Groundwater Monitoring Log

Project Number:

1309 Site Location:

K&N Distribution Depot, Draycott-in-the-Clay

Date of sampling:

24/10/2014

Location Reference: WS501

Weather: Overcast, dry

Condition of headworks: Good

Sampled by: AK

Description of monitoring point (MP)

Ground Level

Diameter of well casing (mm)

100mm Pipe diameter (mm) 50

Depth to LNAPL below MP (m)

- Thickness of LNAPL (m) -

Depth to DNAPL below MP (m)

- Thickness of DNAPL (m) -

Depth to water below MP (m)

2.61 Total well depth below MP (m)

3.78

Water column in well (m bgl)

1.43 Water column in well after sampling below MP (m)

3.42

Sampling method Bailer

Time sampling began: 1000 Time sampling completed:

1021

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Groundwater Monitoring Log

Project Number:

1309 Site Location:

K&N Distribution Depot, Draycott-in-the-Clay

Date of sampling:

24/10/2014

Location Reference: WS502

Weather: Overcast, dry

Condition of headworks: Good

Sampled by: AK

Description of monitoring point (MP)

Ground Level

Diameter of well casing (mm)

100mm Pipe diameter (mm) 50

Depth to LNAPL below MP (m)

- Thickness of LNAPL (m)

-

Depth to DNAPL below MP (m)

- Thickness of DNAPL (m)

-

Depth to water below MP (m)

2.63 Total well depth below MP (m)

3.93

Water column in well (m bgl)

1.3 Water column in well after sampling below MP (m)

3.67

Sampling method Bailer

Time sampling began: 0940 Time sampling completed:

1000

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Groundwater Monitoring Log

Project Number:

1309 Site Location:

K&N Distribution Depot, Draycott-in-the-Clay

Date of sampling:

24/10/2014

Location Reference: WS503

Weather: Overcast, dry

Condition of headworks: Good

Sampled by: AK

Description of monitoring point (MP)

Ground Level

Diameter of well casing (mm)

100mm Pipe diameter (mm) 50

Depth to LNAPL below MP (m)

- Thickness of LNAPL (m)

-

Depth to DNAPL below MP (m)

- Thickness of DNAPL (m)

-

Depth to water below MP (m)

3.3 Total well depth below MP (m)

4.0

Water column in well (m) 0.7 Water column in well after sampling below MP (m)

3.94

Sampling method Bailer

Time sampling began: 1048 Time sampling completed:

1111

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Groundwater Monitoring Log

Project Number:

1309 Site Location:

K&N Distribution Depot, Draycott-in-the-Clay

Date of sampling:

24/10/2014

Location Reference: WS507

Weather: Overcast, dry

Condition of headworks: Good

Sampled by: AK

Description of monitoring point (MP)

Ground Level

Diameter of well casing (mm)

100mm Pipe diameter (mm) 50

Depth to LNAPL below MP (m)

- Thickness of LNAPL (m)

-

Depth to DNAPL below MP (m)

- Thickness of DNAPL (m)

-

Depth to water below MP (m)

1.59 Total well depth below MP (m)

3.0

Water column in well (m bgl)

1.41 Water column in well after sampling below MP (m)

2.11

Sampling method Bailer

Time sampling began: 1146 Time sampling completed:

1205

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Groundwater Monitoring Log

Project Number:

1309 Site Location:

K&N Distribution Depot, Draycott-in-the-Clay

Date of sampling:

24/10/2014

Location Reference: WS513

Weather: Overcast, dry

Condition of headworks: Good

Sampled by: AK

Description of monitoring point (MP)

Ground Level

Diameter of well casing (mm)

100mm Pipe diameter (mm) 50

Depth to LNAPL below MP (m)

- Thickness of LNAPL (m)

-

Depth to DNAPL below MP (m)

- Thickness of DNAPL (m)

-

Depth to water below MP (m)

2.98 Total well depth below MP (m)

3.93

Water column in well (m bgl)

0.95 Water column in well after sampling below MP (m)

3.86

Sampling method Bailer

Time sampling began: 0920 Time sampling completed:

0940

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Groundwater Monitoring Log

Project Number:

1309 Site Location:

K&N Distribution Depot, Draycott-in-the-Clay

Date of sampling:

24/10/2014

Location Reference: WS515

Weather: Overcast, dry

Condition of headworks: Good

Sampled by: AK

Description of monitoring point (MP)

Ground Level

Diameter of well casing (mm)

100mm Pipe diameter (mm) 50

Depth to LNAPL below MP (m)

- Thickness of LNAPL (m)

-

Depth to DNAPL below MP (m)

- Thickness of DNAPL (m)

-

Depth to water below MP (m)

2.09 Total well depth below MP (m)

4.09

Water column in well (m bgl)

2 Water column in well after sampling below MP (m)

2.31

Sampling method Bailer

Time sampling began: 1113 Time sampling completed:

1125

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Groundwater Monitoring Log

Project Number:

1309 Site Location:

K&N Distribution Depot, Draycott-in-the-Clay

Date of sampling:

24/10/2014

Location Reference: WS514

Weather: Overcast, dry

Condition of headworks: Good

Sampled by: AK

Description of monitoring point (MP)

Ground Level

Diameter of well casing (mm)

100mm Pipe diameter (mm) 50

Depth to LNAPL below MP (m)

- Thickness of LNAPL (m)

-

Depth to DNAPL below MP (m)

- Thickness of DNAPL (m)

-

Depth to water below MP (m)

1.67 Total well depth below MP (m)

3.72

Water column in well (m bgl)

2.05 Water column in well after sampling below MP (m)

2.17

Sampling method Bailer

Time sampling began: 1027 Time sampling completed:

1045

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Groundwater Monitoring Log

Project Number:

1309 Site Location:

K&N Distribution Depot, Draycott-in-the-Clay

Date of sampling:

24/10/2014

Location Reference: WS517

Weather: Overcast, dry

Condition of headworks: Good

Sampled by: AK

Description of monitoring point (MP)

Ground Level

Diameter of well casing (mm)

100mm Pipe diameter (mm) 50

Depth to LNAPL below MP (m)

- Thickness of LNAPL (m)

-

Depth to DNAPL below MP (m)

- Thickness of DNAPL (m)

-

Depth to water below MP (m)

2.29 Total well depth below MP (m)

4.05

Water column in well (m bgl)

1.76 Water column in well after sampling below MP (m)

3.09

Sampling method Bailer

Time sampling began: 1125 Time sampling completed:

1145

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Project

Number:Date:

Pressure

Range

(mb)

Peak Steady Peak Steady Peak Steady Min Steady CO H2S Top Base Peak Steady

AWS02 11.2 1010 0.1 0.1 2 2 0.5 0.5 20 20 4 0 0.94 3.95 0.7 0

AWS03 0 1011 0 0 0 0 0.1 0.1 20.1 20.1 0 0 1.27 3.95 0.9 0.9

AWS04 0 1010 0 0 0 0 0 0 21.4 21.4 0 0 1.73 3.95 18.1 18.1

AWS06 0 1011 4.4 4.4 88 88 1.3 1.3 17.3 17.3 18 0 2.45 3.75 140.1 140.1

AWS07 0 1011 0 0 0 0 1.3 1.3 18.5 18.5 1 0 2.7 3 2.4 2.4

AWS08 0 1012 0 0 0 0 2.7 2.7 18.4 18.5 3 0 Dry 0.9 0.9

AWS11 -1.4 1011 0.1 0 2 0 0.2 0.2 20.9 20.9 19 0 1.1 2.9 0 0

ROUND 1

CO/ H2S Water level (m bgl) PID (ppm)% V\V

% LEL ( Lower

Explosive Limit)% V\V % V\V

Monitoring Point

Reference

Flow Range

(Litres / hr)

Methane Methane Carbon Dioxide Oxygen

SOILS GAS MONITORING

1309 Site Location:K&N Distribution Depot,

Draycott-in-the-clay

Remarks:

Logged By: JM15/07/2014

Atm. Pressure: 1010 to

1011 variable

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Project

Number:Date:

Peak Steady Peak Steady Peak Steady Min Steady CO H2S Top Base Peak Steady

BH1 -0.1 998 1.3 0.2 26 4 13 12.1 0.2 0.9 1 2 2.06 2.06 47.2 47.2

BH2 0 998 14.9 14 298 280 8.2 7.2 10 10.8 4 1 1.61 - 26.1 26.1

BH3 0 998 0.5 0.5 10 10 7.1 7.1 2.9 2.9 0 0 2.39 - 158.8 158.8

WS501 0 995 0 0 0 0 1.4 1.4 19.4 19.4 0 0 2.37 3.79 0.3 0.3

WS502 -3.1 995 0.1 0.1 2 2 0.6 0.5 9.4 9.4 0 0 2.47 3.97 1.3 1.3

WS503 0.1 998 0 0 0 0 2 2 16.5 16.5 0 0 3.3 4 0.3 0.3

WS507 0 995 0 0 0 0 0 0 20 20 0 0 1.1 3 8.1 8.1

WS513 0 995 0 0 0 0 1 1 19 19 0 0 2.8 3.89 5.4 5.4

WS514 0.1 995 0 0 0 0 0.3 0.3 19.4 19.4 3 0 1.72 3.71 10 10

WS515 0 995 0.1 0.1 2 2 1 1 19.8 19.8 0 0 2.15 4.1 6.8 6.8

WS517 0 995 0 0 0 0 3.3 3.3 17.3 17.3 0 0 2.7 4.05 6.4 6.4

AWS02 0.2 985 0 0 0 0 0.6 0.6 20.7 20.7 0 0 0.87 3.98 1.2 1.2

AWS03 0 985 0.1 0 2 0 1 1 20.1 20.1 0 0 1.47 3.9 0.1 0

AWS04 1.7 985 0 0 0 0 6.4 6.4 7.8 7.8 12 0 20.7 - 260 260

AWS06 0.1 985 1.4 1.4 28 28 6.8 6.8 10.6 20.2 5 0 2.76 - 96.8 96.8

AWS07 0.3 985 0 0 0 0 1.8 1.8 9.6 9.6 0 0 2.82 3.05 0.1 0.1

AWS08 0 985 0 0 0 0 4.3 4.3 18.8 18.8 0 0 Dry - 0.5 0.5

AWS11 0.1 984 0 0 0 0 2.5 0.4 16.5 20.2 0 0 1.11 3.04 2 0.5

SOILS GAS MONITORING ROUND 2

1309 Site Location:K&N Distribution Depot,

Draycott-in-the-clay10/10/2014 Logged By: AK

Water level (m bgl) PID (ppm)

Atm. Pressure: 995

Monitoring Point

Reference

Flow Range

(Litres / hr)

Methane Methane Carbon Dioxide Oxygen

CO/ H2S

Remarks: WS17 Soil blockage in gas tap.

% V\V% LEL ( Lower

Explosive Limit)% V\V % V\V

(mb)

Pressure

Range

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Project

Number:Date:

Peak Steady Peak Steady Peak Steady Min Steady CO H2S Top Base Peak Steady

BH1 0 1013 0.4 0.1 8 2 9.2 2.3 7.5 17.6 0 2 2.06 - 4.6 4.6

BH2 0 1013 37.2 34.5 744 690 15.3 14.6 0.8 0.9 0 7 1.71 - 24.1 24.1

BH3 0 1013 3 3 60 60 5 5 0.3 0.3 0 0 2.39 - 108 108

WS501 0.1 1013 0 0 0 0 1.6 1.6 19.1 19.2 0 0 2.35 3.78 1.1 1.1

WS502 2.7 1011 0 0 0 0 3.5 3.5 2.5 2.5 0 0 2.49 3.93 0.2 0.2

WS503 0 1013 0 0 0 0 2.2 2.2 18.2 18.2 0 0 3.31 4 2.4 2.4

WS507 3 1011 0 0 0 0 0 0 17 17 0 0 1.4 3 0.7 0.7

WS513 0 1011 0 0 0 0 1.6 1.6 18.2 18.2 0 0 1.98 3.93 0.6 0.6

WS514 0 1011 0 0 0 0 0.1 0.1 20.2 20.3 0 0 1.66 3.72 0.3 0.3

WS515 0 1011 0 0 0 0 1.4 1.3 19.9 19.9 0 0 2.08 4.09 0.4 0.1

WS517 0 1011 0 0 0 0 4.2 3.9 7.3 7.3 0 0 0.55 4.05 0.7 0.7

AWS02 0.3 1011 0 0 0 0 1.5 1.5 19.2 19.2 0 0 0.89 3.99 0.8 0.8

AWS03 0 1011 0 0 0 0 1 1 19.8 19.8 0 0 1.52 3.89 0.5 0.5

AWS04 -0.1 1013 0.2 0.1 4 2 6.6 6.5 5.9 6 0 0 2.07 - 18.2 18.2

AWS06 0.1 1013 79.7 79.7 >100% >100% 9.3 9.3 0.4 0.4 140 1 2.81 - 131.8 131.8

AWS07 3.6 1011 0 0 0 0 1.6 1.6 11.3 11.3 0 0 2.8 3.05 0.3 0.3

AWS08 0 1013 0 0 0 0 4 4 18.6 18.6 0 0 Dry 3.05 2.1 2.1

AWS11 -1.1 1011 0 0 0 0 1.9 1.9 17.9 18 0 0 1.04 3.03 3.5 3.5

SOILS GAS MONITORING ROUND 3

1309 Site Location:K&N Distribution Depot,

Draycott-in-the-clay22/10/2014 Logged By: AK

Water level (m bgl) PID (ppm)

Atm. Pressure: 1011 to

1013 rising

Monitoring Point

Reference

Flow Range

(Litres / hr)

Methane Methane Carbon Dioxide Oxygen

CO/ H2S% V\V

Remarks: AWS11 had a loose gas bung.

(mb)

Pressure

Range% LEL ( Lower

Explosive Limit)% V\V % V\V

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Project

Number:Date:

Peak Steady Peak Steady Peak Steady Min Steady CO H2S Top Base Peak Steady

BH1 0.1 982 1 0.2 20 4 11.7 2.5 2.1 17.3 0 3 2.06 - 4.5 3

BH2 0 982 43.9 43.9 >100% >100% 15.3 14.9 0.4 0.4 1 7 2.07 - 6.1 -

BH3 0 982 3.2 3.2 64 64 4.8 4.8 0.4 0.4 0 0 2.42 - 70.4 -

WS501 0 981 0 0 0 0 2.5 2.5 18.2 18.2 0 0 2.39 3.78 0.1 0

WS502 0 981 0 0 0 0 4.2 4.2 7.2 7.2 0 0 2.59 3.93 0.1 0

WS503 0 981 0 0 0 0 2.4 2.3 18.9 19 0 0 3.35 4 0.2 0.1

WS507 0 983 0 0 0 0 0.1 0 20.1 20.1 0 0 1.55 3 0.1 0

WS513 0 981 0 0 0 0 1 1 20.1 20.1 0 0 3.26 3.93 - -

WS514 0.1 981 0 0 0 0 0.5 0.5 20.8 20.8 0 0 1.79 3.72 0.1 0.1

WS515 0.1 981 0 0 0 0 0.9 0.8 21.1 21.1 0 0 2.18 4.09 0 0

WS517 0 980 0 0 0 0 4.1 4.1 10.1 10.2 0 0 2.14 4.05 0.1 0

AWS02 -1.1 981 0 0 0 0 1.7 1.6 18.8 19 0 0 0.94 3.99 0.5 0.4

AWS03 0 981 0 0 0 0 1.1 1.1 20.3 20.4 0 0 1.45 3.89 0.2 0.2

AWS04 -0.1 982 0 0 0 0 7 7 4.6 4.6 0 0 2.1 - 14.1 -

AWS06 0.1 982 99 99 - - 9.4 9.4 0.2 0.2 216 0 2.83 - 98.7 98.7

AWS07 -0.7 981 0 0 0 0 1.7 1.7 12.9 12.9 0 0 2.98 3.05 0.1 0.1

AWS08 0 981 0 0 0 0 4.9 4.9 18 18 0 0 Dry 3.05 0.5 0.5

AWS11 0 981 0 0 0 0 6.8 6.8 12.5 12.6 0 0 1.04 3.03 1.4 1.4

SOILS GAS MONITORING ROUND 4

1309 Site Location:K&N Distribution Depot,

Draycott-in-the-clay04/11/2014 Logged By: AK

Atm. Pressure: 982 to 981

falling

Monitoring Point

Reference

Flow Range

(Litres / hr)

Methane Methane Carbon Dioxide Oxygen

CO/ H2S% V\V

Remarks:

(mb)

Pressure

Range

% V\V% V\V% LEL ( Lower

Explosive Limit)

Water level (m bgl) PID (ppm)

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Project

Number:Date:

Peak Steady Peak Steady Peak Steady Min Steady CO H2S Top Base Peak Steady

BH1 0 988 0.3 0 6 0 11.6 1.9 4.5 18.8 0 0 2.01 - 7.2 6.4

BH2 0 988 40.3 40.3 >100% >100% 11.6 11.3 0.1 0.1 19 0 1.31 - 17.5 17.5

BH3 0 988 2.5 2.5 50 50 3.3 3.3 3.7 3.7 3.4 0 2.28 - 66.9 66.9

WS501 0 988 0 0 0 0 2.5 2.5 19.2 19.2 0 0 2.15 - 0.7 0.7

WS502 0 988 0 0 0 0 4.1 4.1 6.4 6.4 0 0 2.26 - 0.7 0.7

WS503 0 988 0 0 0 0 2.2 2.2 19.2 19.4 0 0 3.12 - 0.9 0.9

WS507 0.6 988 0 0 0 0 0 0 19.5 19.5 0 0 1.52 - 0.9 0.9

WS513 0 988 0 0 0 0 1.3 1.3 19.7 19.8 0 0 2.87 - 1.8 1.8

WS514 5 988 0 0 0 0 0.3 0.3 21.1 21.1 0 0 0.78 - 0.7 0.7

WS515 0 988 0 0 0 0 0.8 0.8 21.4 21.4 0 0 1.79 - 0.4 0.4

WS517 7.7 988 0 0 0 0 3.5 3.5 11.1 11.1 0 0 0.36 - 0.7 0.7

AWS02 7.7 988 0 0 0 0 1.2 1.2 19.1 19.1 0 0 0.81 - 1.9 1.9

AWS03 0 988 0 0 0 0 1 1 19.8 19.8 0 0 1.36 - 0.6 0.6

AWS04 0 988 0 0 0 0 5.1 5.1 5.1 5.1 0 0 1.97 - 11.9 11.9

AWS06 0 988 99 99 >100% >100% 9.4 9.4 0.2 0.2 66 0 2.67 - 139.8 -

AWS07 -0.1 988 0 0 0 0 1.5 1.5 13.6 13.6 0 0 2.61 - 0.7 0.7

AWS08 0 988 0 0 0 0 4.6 - 17.9 17.9 0 0 0.8 - 0.3 0.3

AWS11 0 988 0 0 0 0 5.9 5.9 15.3 15.3 0 0 0.88 - 0.3 0.3

Monitoring Point

Reference

Flow Range

(Litres / hr)

Methane Methane Carbon Dioxide Oxygen

CO/ H2S

SOILS GAS MONITORING ROUND 5

1309 Site Location:K&N Distribution Depot,

Draycott-in-the-clay10/11/2014 Logged By: JM

Remarks:

Water level (m bgl) PID (ppm)

Atm. Pressure: 988

steady

% LEL ( Lower

Explosive Limit)% V\V % V\V% V\V

Pressure

Range

(mb)

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Project

Number:Date:

Peak Steady Peak Steady Peak Steady Min Steady CO H2S Top Base Peak Steady

BH1 0 -0.14 1.2 0.9 24 18 9.1 6.5 3.2 8.6 0 0 1.689 - 10.8

BH2 0 0 27.9 27.9 >100% >100% 9.2 9.2 0.5 0.5 49 3 1.35 - 25.8

BH3 0 0 0.8 0.8 16 16 2 2 13 13 35 0 2.005 - 91.7

WS501 -8.78 -0.1 0 0 0 0 2.8 2.8 18.1 18.1 0 0 2.12 - 0.5

WS502 0 0 0 0 0 0 3.9 3 10 10.4 0 0 2.3 - 0.6

WS503 0 -0.03 0 0 0 0 1.7 1.7 19.7 19.7 0 0 3 - 0.9

WS507 -8.59 0.3 0 0 0 0 0 0 18 18 0 0 1.54 - 0.7

WS513 0 -8.63 0 0 0 0 0.6 0.6 21.4 21.4 0 0 1.7 - 0.9

WS514 -0.1 -7.31 0 0 0 0 0.2 0.2 21.6 21.6 0 0 0.55 - 0.9

WS515 0 0.1 0.1 2 2 1.3 1.3 19.6 19.8 0 0 2.77 - 1.7

WS517 0 -4.42 0 0 0 0 3.9 3.9 19.4 19.4 0 0 0.42 - 0.4

AWS02 -2.9 -19.31 0 0 0 0 1 1 20 20 0 0 0.59 - 0.8

AWS03 1.8 3.8 0 0 0 0 1.7 1.7 19.6 19.6 0.1 0 1.1 - 1

AWS04 0 0 0 0 0 0 5.8 5.8 3.5 0 0 0 1.6 - 18.8

AWS06 0 0 99 99 >100% >100% 8.5 8.3 0.3 0.8 86 0 2.4 - 131.3

AWS07 -3.6 0 0.4 0.1 8 2 1.4 1.3 14.4 14.4 0 0 2.62 - 1.5

AWS08 0 -4.86 0.1 0.1 2 2 4.6 4.6 17.1 17.1 0 0 2.78 - 1.1

AWS11 -0.2 -0.97 0.1 0.1 2 2 4.3 1.9 18.9 20.3 0 0 0.93 - 1.2

Water level (m bgl) PID (ppm)% V\V

Atm. Pressure: 1004 to

1005

Monitoring Point

Reference

Flow Range

(Litres / hr)

Methane Methane Carbon Dioxide Oxygen

CO/ H2S% LEL ( Lower

Explosive Limit)% V\V % V\V

Pressure

Range

(mb)

SOILS GAS MONITORING ROUND 6

1309 Site Location:K&N Distribution Depot,

Draycott-in-the-clay01/12/2014 Logged By: JM

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APPENDIX G

NOTES ON LIMITATIONS

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LUSTRE CONSULTING, ENVIRONMENTAL AND GEOTECHNICAL CONSULTANCY SERVICES

NOTES ON LIMITATIONS

General

Lustre Consulting have completed the attached report for the use of the Client detailed on the front cover and those parties with whom a warranty agreement has been executed, or with whom an assignment has been agreed. Third parties should not use or rely upon the contents of the report unless written approval has been gained from Lustre Consulting; (due to legal requirements, a charge may be levied against such approval). Lustre Consulting accepts no responsibility or liability for: a) the consequences of this documentation being used for any purpose or project other than that for

which it was commissioned, and

b) this document to any third party with whom approval for use has not been agreed.

Phase I Environmental Risk Assessments, Desk Studies and Site Audits

The work completed and utilised to provide this report comprises a study of available documentation. The opinions and results presented in this report have been arrived at by utilising the finite amount of data available at the time of writing and are relevant only to the purpose for which the report was commissioned. The data which has been reviewed should not be considered exhaustive and has been accepted in good faith as providing true and representative information pertaining to site conditions. Should additional information become available which may affect the opinions expressed in this report, Lustre Consulting reserves the right to review this information and, if warranted, to modify the opinions presented in the report accordingly. It should be noted that the risks which are identified in this report are perceived risks based on the available information at the time of writing and that the actual risks associated can only be assessed following a physical investigation of the site.

Phase II Site Investigations

The intrusive investigation has been completed to provide information concerning the type and degree of contamination present along with ground and groundwater conditions which facilitates a reasonable risk assessment to be completed. The stated objectives of the ground investigation have been limited to assessing the proven risks which are associated with potential human targets, building materials, the environment (including adjacent land), and to surface and groundwater. The amount of exploratory work, chemical testing and monitoring completed as part of this project has potentially been restricted by the short timescale available, and the locations of exploratory holes undertaken have potentially been restricted to areas unoccupied by buildings(s) and buried services. A more comprehensive post demolition / decommission investigation may be required if the site is to be redeveloped. For these reasons any costs included in relation to site remediation must be considered as tentative only at this time. The exploratory holes investigate only a small volume of the ground in relation to the size of the site and therefore, can only provide a “snap shot” or general indication of ground conditions located on the site. The fact that the site has been investigated does not preclude the existence of localised “hotspots” of contamination where concentrations may be significantly higher than those actually encountered. The risk assessment and opinions provided in this report take into account currently available guidance values relating to acceptable contamination concentrates; no liability can be accepted for the retrospective effects of any future changes or amendments to these values.

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The Admiral’s Offices The Historic Dockyard

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