appendix h - der.wa.gov.au · table 2 sample sample identification date number assessment criteria...
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APPENDIX H
Sample
Identification
Number
Sample
Date
f:cological Investigation Levels ElLs {mg!Kg)
Health Investigation Levels HIL·A (mg/kg)
Analytical Results
Table 1. Soil Analytical Results: Total Metals
Metals (m ikQ) Mercury Arsenic Cadmium Chromium Copper
20 3 400 100
15 100 20 210 1000
Lead Nickel
600 60
300 600
SBOI-1 00 17/2/2010 <0_1 ,, <1 <2 - _ __ , _ __c<__ ,, -"'"5-+- ,, 5801-4.00 17/2/2010 �-' <5 8 , , --- ------� -- -. --1---'' ,_, -S802-t.so --�!'3!2_�-�-� -I-- �'�O>c -�' --4--·•:os_ _ <:__________ _____ 6 -l--�7 -"'·---�---
1-----�-�9��::_�5 __ ___ 1712/2010 <0.1 <5 <1 10 16 20 SB03-1 25 _ _ _ __ ;_���!3� 0c 1'0-f _ _:'0,.::1_ _
<5 <1 11 9 16 -----�-!?_��-��__?'-�--- 171212010 <0.1 <5'--1---'0''--� - ---- -�--------- <5 7
4 3 7 5 •2
Zinc
200
7000
,, ,, <5
SBOS-1.50 1712/2010 <0.1 <5 <1 10 7 11 3 <5 . -- ------ +--""'--'----1-- - - - ��"'-1-- . -- .. ----����-!�-�--- +"1�
71 �21�2, 01�0'-1 <0_1 _____ ________ ::�--+-�-�'--+- 10 5 10 2 <5 ---��!:�� '!'-?!':�_,_g_ <0 1 <5 <1 <='---11-�-<5 -----��------ -�'''---1 ------::�----
SBOS-1 5-�---�- __ 1__?'1212010 <0_1 _______ _::�----1--_:'c' _ _ , ___ 18
----· _____ • '''----1---'8'----l-- __ ----�------j--'::''--1 SBQA 1 17/2/2010 J--�'::0c.1c__J---- <5 <1 ---l--�'2:_ __ _ ____ -------�?---� __ _ <5 <2 ____ ::_�-----����----- 171212010 <0 1 �'C''___j'___:'"-1 -------�------L_C':"5 _ _j'__ 7 ____ - - --- - ----��- <5
Table 2- Soil Analvtical R 'd s esults: Act ulohate Soils Actual Aciditv Potential Aciditv Acid Base AccountinQ
Sample Sample " ldentlfication Date il �
Number � " -% 2 • filz-.I �" rou..'l:' x"' -'2'0 2 �-" >-�"
Assessment Criteria
Analytical Results
��--"'<>Bo_01·0_5o 17/2/2010 c<u0c:>.1-!-' 8801-1.00 171212010 _____ ____ ::0_0_��1--{_:''-''
1----''"'""-o�_:_�-�qg ___ --l---'""121.�g__1_9_ _ _ ___ _ 5.1 ?_?_ __ 1---'"'""'0_1_���<?-�-- -· � -+---''"7/2�?-Q!�---- - -- ---_§_1_ 17
$801-3.50 �-+--'1'-'''"21_?_Q_1,�--- ---- 'C5-'-2 -!�" SB01-4 50 1712/2010 5.0>_j__>31 S801 5 25 171212010 4.9-11-4'>'5 $801·6.00 17/212010 4.9 --l---"'"-'--
1---�S�B,ot-7 _ 00 --1--- -'17 ,, l?l_?g_:l_q___ 4 _g }_5 ____ _ 1----"'"'""01 · 8.00 -l--''"7'?!3g_�Q_______ ·�'"· '-1--_}§____ __ _ __<_S�B,02-075 17/2/2010 5c>o.6'-J-- 4 ---"'"'"""02-1.5·�0---l--1"7"/2�2.Q!�----- - "5."_0 -1-_?_9'
$802-2.00 -�---"17'-'/2/2010 5>c·1'--+-- "' ��--'S,oB.o-02':"3.00 171212010 5 3 26 t- ____ ?_�Q3:_4__ O_{} 1713!��!?-. _ 5.3 17
----�-�9_2_�2_.92_ -- - - - - -�-�-���/20 � _Q_- - - ----l---'-5.;>0 __ 1"' __ _?_4 _____ _ ____ __ --�-�_o__?_�--I� . __ --�!:1-���9.!?_ ----· _ -!--''"'"---- _ ___ :!9 _ _
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__ ?!3_{}?:! _ _?_5 _ __ 1_ 17/2/2010 5.1 20 21
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<0.02 _ _:<�0�0�0�5-1--__<_<"10;_ _ _ ----�2�9.?_ __:_]_Q_� --- __ :2.!_ <0 02 ,-o�-�00�5·_+-_.'�'�0--J-�'<g)g_ _ ____ :_!Q _____ ----� 0 o,, --+-�<0�-�00�5>_+---·<1 0- - - - -- ____ Q,�� - -- 27 -- 11---'-2 -� 0.03 <0.005 <10 _____ Q;Q}__ 18 __ _>1_--j 0.04 <0.005 <10 ___ <tQ;!-____ 27 _,2c_--j
____ Q_._o_�---- ______ , _o. _oo�5---+-�<,,�o,_ o.o�---- ____ J�- ____ l_ _ _ _ Q&?__ _ _ ____ ,o _o _o5 __ 1--__<_<�10'--�- _Q,Q_L __ _____ i�------ ____ _i_
- _ __ Qo._Q_@_ _____ -- _•_0 _00_5 __ -l--�<�10'---i-0.10 60 - - - - �� 0 06 <0.005 <10 ______ Q_,Q_�----- . -- - __ 3_7_____ 3 o.os,_+-�<�O�.o�o�5-I-- __-<!_Q:__ o_os <0.02 <0.005 <10 <0,02 ------ ---- ----0 04 <0.005 <10 0.05 0.04 <0.005 <10 0.04
____ _Q __ Q� .. J--__<_'0�-�00�5>_+-_-<�1�0-j 0 04 o -�03'---J--�<Q�O_QL_ __ _____ __:_1�L-- -�9cQ.L __ o,,.o�''--+-�<o.oo5 _ ____ "'":'!_Q _____ ______ Q_ . .Q� _ _ 006"--+--'<Q,Q�--- -- __ <_1_Q_ - - 0.06 0.03 <Q_._9_9__2__ <10 ______ Q:_Q_L __ 0.03 <0 005 <10 0.03
38 3 ____ ":_I__Q_ - -- - -�- ''---j
29 2 28 2 27 2 19 1 24 2 40 3 20 2
-�2«'2_L__ 2
Table 2
Sample Sample Identification Date
Number
Assessment Criteria
Analytical Results
Soil Anal_vtical Results: Acid Sulphate Soils
g - c \!co Ir o3
Actual Aciditv
;;; 0 � ? -� . � �" 2 -., w rou--� -o E >-�-
� 2 "� ""'""' -f-_"Q(J) ' 0 . _\l::: -c ;g�i): Olt>;:R (!)<(�
Potential Acidltv
� '§ E "" " E .2 u • o-�in ..C�,;:;:-§;;>< o.-1::0+ E:: »GI 0 " -"' "'<!) '2-oO "� �" o • E 00 �"'-
Cont.) Acid Base Accountin!l
m m c -'"-u� �_g) -§ -� '6 c 0 X 0 X o ..,z� . " •z.- �<:r:(.) -�� z-:6� (}_ O>O '9. ·g t: u " ms u 0$ o_ c u "
<(u(l) "'u-P E2o -a>z� -zo '"' � .£' �-r:S Z<C� �·-
Table 3- Groundwater Analytical Results: Oissolved Metals
Sample
Identification
Number
Assessment Crlteria
Drinking Water
long Term \rrigahon
Freshvtaler
DoH (2006)
Sample
Date Units Metals
Arsenic Cadmium Chromium Copper Lead
0_007 ! 0.002 2.0 0_01
0.1 0_01 0.1 0.2 2.0
0.024 0.0002 1 0.0001 0_0014 0.0034
0_07 0.02 20 0 1
Nickel Zinc
0.02 3 0
0.2 2.0
0.011 0_008
0 2 30
M801 171212010 mg/L <0.001 0.0002 <0_001 0.008 0_001 0.009 0.143
MB02 171212010 mg/L
M803
QA1
Table 3- Grotmdwatcr Analytical Re.<iults: Dissolved Metals (cont.)
Sample
ldentlficati 0"
Number
Sample
Date
Assessment Criteria
Drinking Water
Long Term Irrigation
Freshwater
DoH (2006)
MB01 1712/2010
M802 171212010
Units
mgll
mgll
-�3 = ��;���r�� ------ __ ______________ _!,_ _______ __
Metals
Aluminium Manganese Iron
0.2 0 3
5.0 0 2
0.055 300
2 3
0.09 0.114
<0.05
0 71
1.44
Selenium
0 1
0_02
0.00005
<0.01
<0.01
<0.01
Mercury
0.001
0.002
0 00006
0 01
<0.0001 ·---·--
<0.0001
Table 4- Groundwater Analytical Result!i: Nitrates and Phosphorus
Sample Name
DOH Long MB01 MB02 MB03 QA1
Drinking Term Freshwater
{2006) Water Irrigation Sample Date
1712/2010 17/2/2010 1712/2010 17/212010
Ammonia asN 0.16 0.18 0.22 0.16
Nitrite as N 30 <0.01 om -<0.01 0.01 I- �------------- ----------- - - - -
Nitrate as N 500 10 31 0.07 0.06 0.03 0.05 ···- ----------------------- -·�-. "- ----· --------------
Nitrite + Nitrate as N 0.07 0.08 0.03 0.05 r- ·- -·-·�- -----r-�·-· Total Kjeldahl N as N 1.3 1 5 <1_0 1.5
·--------------- ·-···-·· ----------- - -----·· ·
T olal Nitrogen as N 1000 14 16 <1.0 1.6 c-----·-�- ------- ----------- ----------···
Reactive Phosphorus 0.05 0.89 0.17 -<0.10 0.96 ------------------ - ----------
APPENDIX I
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CERTIFICATE OF ANALYSIS Work Onl�r neon\ Contact ,'\C)(�( US�
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. MS GINA PEMBERTON SHOP 1712 SOUTH WESTERN HIGHWAY ARMAOALE WA, AUSTRALIA 6112 [email protected] +61 08 9497 5000
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[email protected] +61-S-9209 7655 +61-8-9209 7600 NEPM 1999 Scheclule 8(3) anct ALS 0CS3 reqwement
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l h1s document has be>?n electro01Cally signr;>d by the au1Mnzed
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poor reactMty of lime. For conversion of Uming Rato from 'llglt d<y weight' to 'kg/m3 ln·zltu zoll', multiply •reportod results' "'wet bulk den5lty of $Oil in tlm3'.
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MS GINA PEMBERTON SHOP H/2 SOUTH VVESTERN HIGHWAY ARMADALE WA. AUSTRALIA6112
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1 0 Hod Way Malaga WA Australia 6090
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iSOIIEC 17025.
Sign atones Tf1;s document h% been BlG<�tronically s.igned by the i!i.i\honzed Signatories <ndicatei'J below. nectror:ic 51911;.ng 11as beer1
c:ilrne<J oc:t :n comphance with procedutes specifte<l in 21 CFF:: P:il:t 1 -;.
$JgnW'XW$ Ctceha Bartels
Leanne Cooper
PoMron
Metals Instrument Chemist
Acid Sullate Sctls Supervisor
Ern•1<oo»n"'nt"'1 Oh.>OSI<>O P<trth Pwt oi lhe Al-'5 Labor "'torq Group
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Laboratory Duplicate (DUP) Report
-:"r-� (fc<eii.l)• centro: :erm L8bo":tc>'y Dur;>lrc21·:,;, reh�;•, 10 -" ;undornly S<>iu:)M l�U�I;;boraWIY spilL L<li)<:XOlt�r)' ctuplrci.ll�·s Pro·o;C:e :niorn:�Vo0 r>'gc.n!•ng rn+Ji':M prec.s:or. �·1d Sc.H1'1Pk: helerog>!r,8>ty Tbc pern"\l'i:d "''"')t'�
(vf' :Ice Rdmrvc< P<Oie<,ni Devt;'Jl:c� (RPDi cf L.cmc<"<J1C�j C:;pl.c��ws are spec.rf:ed m .>\c.S Meth<)(l QWI<C_N.'3S «r� """' der�mkn: on (he m�gnr',"j" ct r<•::wlts i� ::ornpar•�on to th· leoe: ol 1'0ocrtrn>) R<J8dl 1J lq\leS �0? 1\;> urn.!. Ru.<;ult b�·o.v,'x-m 1 c;-<1110 2.0 <.-m�o t.Of<- OY. - so;t,: R">',�lt > Xi 1m1�·s LOR - :J % - 20'(
EPj1Qt027·012 S802 0.75
, EP1101021-033 SSOG 1 00
EAQ33' TM<;table_A_ct�al ACFd!ty__(Z3F) __
' EA033. pHKCI (23A) : EA033' sulfidic- T\lrataPle Actual Ac,cti:y (s---23F)
EA033 Tl\!atable Actual ACid>iy (23F)
EA033' Tttratable Actual Ac,d'.ty (23f)
EAo?.3' pH KCI (23A)
i--- i
-t
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2
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.. .,, __ .;""''"o_1 -.---- "'PHunrt -. .. ..
SA , ..
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i EP1i01027-012
i EPi\01027-033 !
S8C2 0.75
5806 1_00
acidity - Chrcmium Re\l'.1C<ble Sul�ur (a-228)
EA033' Chrofl"iUn\ _Rr;duc�PI� __ Su!iu!J_2_ 28),
(a-228) EA033' Chrctnum Red:'-lC\ble Sulfur (228)
: EA033' acidity- ChrOr'l<Um Reduc•b!e Sulfur (a-226)
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0.0 00
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0 % - 20%
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0%- 20%
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0 % - 20%
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NoLrmtt No Lim<t
'NC"um•t No Lim<\
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EA033' s.ullidic - Ac,d Neutrat.si�g C<Jpacity {s-.1.9A2) '
EA033: ac•d:ty - Ac.d Neutrnl1S1ng Capacity - ! 10 mole H + I \ 2180 , {a-19A2) . ���l'lllli�'l!l!�llll\-lj\Glllllllllllllli0lll'lll\j\10\1W'I/iJ'1j\\llclWllY'clll!c\\ ,ll ' ' ' ' -
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EA033: Net Acidity (sullur units) ,. EA033·. �et Ac.idlty. exctud•','9 ... ANC_{sullur.�!:'ls),
• EA033: Llrmng .. Rste .. EA033 Umll"lg Rate exdudm$.ANC EA033' Net Ac>dity {acidity ur)!�s)
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; EA033 Net ACid>ty e:<dudtng ANC (sultur uMs) EA033; L<!Tiifl>l Rate :· EA033 .. l:'.!!iln.\l. R�ta __ e:<�lu:J.'�g fl:.�c ...
" EA033 .Net Ac.i_dtt,: .. (act.chty �.n . .ts) .. : EA033 Net ACidl�(_e.>(CIUdlng ANC (addity.uMs)
EA033· ANC Fmeness. Factor : EA033: Net fl:c;?ityJ�u.l.f�.r u.':!tsl. i EM33 !;let.A;:id>)'. e.x.::krdtn.g. ANC {:>UIIur.unlts.l_ ' EA033 Li.mm� Rate
; EA033: L>ming_ Rate e�du<:ling ANC EA033· Net Ac>d,ty (ac1dity uMs)
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kg CaC031t . .
<\ c:af'.03it <l 1e H+ l l <1()
% S :J.02 kg CaCQ3,t
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' ·' % S 0.02 % S 0.02
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00
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No llmrt No Lrmt\ No lim'\ No l<m't No L,mrt No L,m,\ No Lm"lft No ltmlt No L1m1\ No L,mlt NOL>mlt No l..<mrt No Lrmit NO Limll NOLil"l1it
No L:mit No um1t NO ltffill NO L!m>t No L>m<t NO \..tm� N0 L1mit NC L.rr\it No L1m'.!
,'-kJ um•t Nc umrt
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SBOS 1.50
EGOOST. Arsemc
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EGOOSI_: Lead
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EGOOST: Chromum
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5 mg!l<$
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D'H>ito•m Rc•uJ! RPD(%) /?�COY�
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0.0 Noumrt
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<2 <2 0.0 No Ltmrt
<5 <5 o_o NO L ;mit
<5 <5 0.0 NO Ltm<t
<5 <5 0.0 No Lrmft
<5 <5 0.0 No Ltmit
q << 0.0 NoLrm<t
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Method Blank (MB) and Laboratory Control Spike (LCS) Report
"n1u qu;JI•'•Y �ontrol \()r;n ;-re:Ctcd :_,lQQr;;:tmy Blank reiors \o •'�' @n<l.lytv :r<ee :n:�l'llX to w'aO'l ull re,;,gcrH m<:o i'!doicd '' the s�rne val\.rr,es or p;cpcrt.on" ,;,s U:k"<i rn st.3nd.iHd s:lrql!� pr,·•f!'-ltnl:on_ T:'c �urpo><c o! 1!11" GC
PL1nJH'd'·" <S to rnorlltUI Pc>tcntl<ll lut.omtwy wnt,\rn,nm<on Tik\ quolr1y eo;mol t�'"' Labcr:Jtory Con:rol S""'Pie tLCS) r0�0rs !:0 -� cer..r!:<:od refB<�n'::e rn<1kH1ll. or u kr:c.wn q�•:'r'"'"•n<:V :rfi:e nBtnx �prke·-1 w;th :;;:rgro\
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Ne\ At:Jd1ty {acrdJty un1ts) " % S
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R�cov�ry LJmiL> ()'.)
"'' " DO
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,06 70 "'
87.4 70 DO
64.2 70 130
85,3 70 t$0
70 ' "
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EP1101027 ACE ENVIRONMENTAL PTY L TO
J010-039
MMhO<i SIMX {MB) R"pml
<S <S <5 <5
61.6 mgl�g 54.7 mglkg
55.5 mg/kg 55.1 mWko
l�bw•<ory Comr"¢1 Spi�" (LCS) l�cpcl'l
R<><:cvery Lm"m ('/,)
·--··--sr.; ... SS-5 ' "
S<o 82.2 1 1 2
98.3 " "' 98.4 " ' " '" se.s " 1 1
' " " ' " 91,9 85.6 "'
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s of 8 EP1101027
ACE ENViRONMENTAL PTY L TO
J010-039
Matrix Spike (MS) Report
'lho q:.�cJi:ty c;cnwl '·"'"' v,·;;;c;;.; S;.WJO i�tS/ mror� w <1:1 lt1\roboormory &plil �·ilmpk sprke.d w::n .� repm�'"'r<;'Jtrv.,; set o: tmgd onalyrc-o. -rvo pVCpi)S(O ot :hi� OC psrwD�r�r ;;, :o m<:>rt<roc potcontiJI m<>�m etr,cts on an>Jiyt<'
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ALS Lal:lloraton.-1 Group ANALYTICAL CrtEr.-11STRY & TESTiNG SERViCES
Environmental Division INTERPRETIVE QUALITY CONTROL REPORT
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,EP1101027 ACE ENVIRONMENTAL PTY LTD MS GiNA PEMBERTON SHOP 17/2 SOUTH WESTERN HIGHWAY ARMADALE WA, AUSTRALIA 6112
[email protected]_au +61 08 9497 5000
J010-039
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Environmental [ljvision Perth Scott James 10 Hod Way Malaga WAAustralia 6090
[email protected] +61-8-9209 7655 +61-8-9209 7600 NEPM 1999 Schedule 8(3) and ALS OCS3 reqwrerr.ent
18-FEB-2011 28-FEB-2011
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d,JM "''tr. th� shortest e<l'.�iytu l�old:ng krrK\ Icc t!!e e·�uro��l�ni ,,orl rr�<:tMd 'fC1cs0 '>Oil Midrng \tn1�·>'> mG. Q;ysruc>l r14 a21ys) M<>;cc:r-y 128 dO\yS) & otlwr m<Otdo \11>0 rWy:;), A rewroe:J a/each \!<'Jf8:or<? dew� not •]Ll<lf¥rt8•o
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QuaUty Control Parameter Frequency Comp!iance Ti�C" foibl'ilh\1 m�ort �Ml'mi'ln·c;�� tho li0•W"ncv c:l lub0ratc!y OC s�n;91<;� �n�IYS'-'d .,.,:r<c: :r:<O a<'ol·;t<CJ.I io\ls·, :n wt•·cl\ tho s,:c,.,.n\Wd ��<v:pl�\0) wos{N10!Q) ;:w.>o�··;su·Cl. Aelu�l rall',· �!10uld !;)(.• (;r0<'lt\l� th<m :x 10qual �0 '""' ¢Xf.l''C!(.)d rCLt"' A J:�"'lcl <Jf bee�"'''"' ::; ;r;w1d<ld m lh-" Su"'"'"'Y ct Outt:er.';,
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Brief Method Summaries Tne ;l.r1alyt.csl ;xcced'"'"' c.>;Bd �y \hie f'wronmei:li>l D1Vi":o� h:wG b,;,c,-, d�'>'IOicp�d from es:eu . ._�.�<!O 1"\"'cna\:onallj rcl>·,ogr;:�e<J proc&dc�rf'� S>JCh �5 U>o�e pu;:.bi"«Cd :C.y \�\G U!.; EPC•, JWC,A AS 'wd NCYM In Mc:se
d<OvdOP<:><I P<oWdJr,% zr<o r,mpiop.� >n the absence 0! Ce<;u:nf:nWd stand�rds. or by c.li<:t:\1 reqw<e$1. fi<<O iollcw:ng IB!X>rl P""'id<es �net <H:rM:r:pt;OilS ,jj \h•J an;-Jiy\<Cal pcor-edc;ros <;rm�loy<ed f.::•r i'%d:o r•l>'<\')1'1nd ·.n �1:1; CW1c·
'14lt0 ot A�Ji)'>·�>. SourcES �cmn wh;c.� ALS r.�,et�ods tmve :010<1n o0v<liO\K'<l 0ro pwv<cGd wnt:<n t'J(; Me�hCd De�;;r,�ttons
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EAciss-to3
EG005T
EG0;.5T
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' ' " .. J\'i<'!.C:'\io\l',;i'J· method covers the determination of Chrom1um Reducible Sulfur (SCR): pHKCI: titratable
, actual acidity (T AA)·, acld Mutralising capacity by bacK titration (ANC): and net acid soluble sulfur (SNAS} which 1ncorporates peroxide sulfur. lt applies to soils and sediments (including sands) derived from coastal regions.
, limi!'IS Rate IS based on results for samples as submitted and incorporates a mmimum safety factor of 1 .5.
SOIL · ! A gr;,;v;ffi'etric PrOcedure baseo on �,vBi9ht lo·s·s oVer ·a 12 .. hoUf ctrYi�g Period at 1oz�'1os d.·
egrees C. This methOd is ...... ' . .;of!lpliant.<JV!Ifl .t:'t:.e':-1 .(2_01.Q .. .Dr�ft) �(;..he�ul� ... �f3L?�cti()n a.��-T<!ble ... 1 .( 1 � .. day ... hol.cJ.ing_ !ime).-.
SOIL ' (APHA 2'\st eel., 3120: USEPA SWS46- 6010) (ICPAES) Metals are determined fo!lowmg an appropriate ac1d , Oiges\lon cf the soil. The ICPAES technique 10nises samples io a plasma, emtlting a characteriStic spectrum : based on metals present Intensities at selected wavelengtl"ls are compared agamst those of matrix matched
_,.!._stanct.ar�s,.J:hio; .. �ethod .. i�.co.f!1pH!i!(I\Yiith.N_EP.� .. P.9�§l . . ?_ched�l� .. 8@....... . ... ...... ... ..... .... .. SOIL , AS 3550, APHA 21sted., 3112 Hg - B (FIOW·inject'on (SnCIZ)(Co!dVapOI.lr generation) AASj FIM-AAS tsan
awtomated flameless atom1c absorption technique. Mercul)' in solids are determmect fo\lowing an appropriate acid d1gestion. Ionic mercul)' is reduced online to atomic mercury vapour by SnCl2 which is then purged ir.to a heated
Quantlflcaflon is by cornparing absorbance against a calibration curve. This method is compliant With
SOIL " r iJsEPA'20o.2' MO'ct. HOt 8i0c1<),cid' bi9est1Qn 1'.cg Of sample 'is heated With Nitric and .. Hydrochloric acids, then
; coolecL Peroxide IS added and samples heated and cooled again before being filtered and bulKed to volume for ; analysis. Digest is appropnate for determination of selected metals in sludge. sediments, and so1ls. This method <s .... r:o.�PJ.iant NEP�t . .f.:� ��.?t'?.��€.?.�!� .... �1.�1...\.�.�!�? .. d ... ?�?L_
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Accred:ted fer ccmptmnce wtth
ISO.'!EC 17025.
Signatories ThiS Oo.:;wnent has he8n e.'lt'ctiCrliCi!lly s1gn.ed bJ-' the a<l\honzed
earned out in co,r-,plronce w1th pro(;edl.ii'8� �peoli;,o.d m 21 CFR Part 1 1 . St!?"·''tcr:t•;· Pos;t.or:
Leanne Cooper Acid Sulfate Soils Supervisor
__________ ________ " __ _ l;;:nv!roi'i'ro"<an�"'' t:::"';�,�•on Partr> p,,, ,�jm,·. AL$ L>>bor<ltory Group
'" "\0.1 """' ,W,(qo N.\ i"->>!<�H�Js-:; T<t. .,� \.,.Ol�� 70!>< '''"· • o \ .. ;.�;-�·) :;,Q.; "'-'""'·''hU�o'>•>l.wm
$�JiliHOit00' rnG�c\led �elow. E!,:ct,·onl( �;gr:mg i)C\"' t..\i.J01';
A"r.rew!cwon CJtC•_()<l''i
Perth ASS
wo M&W@Q&Ni>ltJ!liiWUillMh ,1 Gatt,,.,,,.off Sroo��,-, (.OI''<Od C<;m,><or-y
M@fu 1i1&UMl\ID!ii$\�'', :\!!;,··-----• �
f',"l" Wo!� O•·c\•Ot
<:!,em
F'W)c'G\
2 of26 2Pt 101026 AC2 ENVIRONMENTAL PTY L TO J010-0:I8
Genera! Comments ncJ �n.�!yw;�J pte<:0du�o "sod t!\' \h" C·:�vteOP,mem:::! [),v,son i"o:!ve b-e'·""' di'>•dcp<:o fr,yn CJ%3t·hshcd mtr.·rG.U;:OI\(lily ri,•r;..lg,,led �rcc•.ldwm•; such 1:\'i· ?NJW p�bid1'Cd �y (ioe USEPf1
d·JvdJp�G p;ocud<.<i<o�. :�:.;, <w<p:<:�y0d ''" 1r11" ;m"•Jl!•>: o( (!occmwn;e<! obn<!mde. 'x :''>' d<>:i�t Nq,,•ost
\'Vh<�r<) r�Vt�(<,l'e ''i0hlrD\':'\\11.()� ha-S bO,')h P0'i�)f11",oQ, n.l�',i,ll�; �m '"P<ll'1<Cd Oh a 0:1')' w<l,§l\\ b:,Y.;<> V'i'WI'<l � r�por',CJ<.i iec,s 11\i!n (•':· ""�dr ;s h<glwr '"''.tn n·.0 LOP lh.s rnay o� dwe to prm1«•)' s6rnpk o�traclJC:iJO�lci:C, d,[,;tron ''lnd'ar rns\ifrrert sarr-p:8 jor ar1:a!y�,,
\•\hi>!ll U'"• L()C� C'l 1\ re!Jcr!cd 1\c"llt dt(%r.\ fr07l S(�rlO.:'lrd LOi': t�<S m�y b� due tQ .�<_<:;.� morst�·ce co�t"r' ,ns�ii,�\er:t 'iiV�1tlG {ie<J.::ood "'"'S'·"lt e<:�.<oy�-<:) vr .'1K<1n� 'n"''Yf<H<JnC:!
"""'"A f\S and N:O::i")..l '"' hC'-'6<·�
'h�·''"' sa:n�i·n(,l '""* ,i'fcc:r;c,t>On ,,:. i\01 p10Vtdc:d :1y tl\c' cb<e"� :;mnp!tng li8\0$ :are o�.cwr; wt\ocut lil t.rne <:C.r'i;Jon\Cr11. In thes8 :n$i'i'JnCCS, the 1>mo r..Oil1f>0!101\l h;;o-. 1Jecn J$�Ur10Q tJ·1 111e b�.·<;:(,llC>ry '!G:' pi"J0SSW;J p•.rpo�''''
K(q CAS l'umoor Cc\S mg<�.\cy :',u,;1D<''' \1\)rr\ ct<>t<lb2;<� :':'1\ll(\l;)j(l<)d b'i Chd;ucal 1\ostrac:Ts s,·,rv:c�« Th; ChQilVC�', i\b�ttil,c�s Serv.ce >Sa <liv:s,on of 'llC1 Am�'"'-"" S!'<'rDICal Soc;;,tf
i...OR �n,nt<:,f r�P''rnr.IJ � � T�.:� rroS�lll tS CCIP;>wl'>t: :·ron :�C"''d"ill an�JyK d�·tockm� .�1 '"'' ,,t•<lw tM I�·Wl <Of repmr.,�q
0 ASS Field Screening: NATA accreditation does not cover P<>rlormnncc of this S�<,..,ico.
f �o ,,.,.,;NcO,' {l.•.x.\J,'o\ �"' .. �..._, ('(NIP" "f
h18'' ·t;o·� O;J,,,r
l:!,c'r\ Pm;,Kt
Anatytic<JJ! Resufts
S,;!H,\o:r,xo SOIL
R�action Rata
3 of26 EP11C1026 ACE ENVIRONMENTAL PTY L TO J010-039
C,1.'io'O( samp�t' i0 5601 {l.25
17-FEB-2C·i1 15:00
Slight
$801 0.50
17-FE8-20 1 1 15:0Cl
Slight
SB01 0.75
17-FEB--2.011 1 5 0 0
Slight
SB01 1.00
17-FE8<20tt tSOO
EP1101026-G04
'·'
6.1 Slight
$801 1.25
17-FES-ZO: t 15 00
E?11G1026-0il5
8.8
,_, Strong
A (;,,n•�l!c•,J iJ.'�IIIC.'O L• l•,:<c.l •;y•, Yd >t
g • � " " 0
� ' ";'_ , ...,. :�:N 5; 8
, :::J-m ' .n ' m - • 0 " N N � b --g rn
g.
-' 0 • S: ' u; 0 0
0
N ... •
)> 'G 'Jj $ C. , ' � il " 0 '!! "' ' 0 • ru � -
"' m �
00 w "
F-�u" Wt·:� C<ckr Gl•a·1� PmJ�(:t
Anatytica! R.esu!ts
Sc>t>-1,\;;\nx: SO!L
pH (Fox) Reaction Rare
5 oi 26 EP11 01026 ACE ENVIRONNIENTAL PTY LTD J0\0-0'39
Cl1ent �;,>mple i.G SS01
2.75 17-FES-20 1 1 15.00
Mode raw
SB<l\
3.00 -- 17:F·Ea-.z6'i t 1so6
Modcraw
$801
3.25
17-F£8-201 1 \S.OO
Moderate
$601
3.50 17-FE8-20 1 t tsoo
EP1101026..Q14
\.7
'·'
Slight
$601
3.75
17-FES-2.01 1 15·00
EP11l!1025·015
;_;
'·'
Slight
'' CY.ortoc:, ,-1.-,{''e'" �·,miw Co-">'"';!
P�G0 'li0(� ()�el<O!' C:.0,\ i-'rvi'';:
AnaJyticaf Results SW?Mut�'X' SOIL
R.e&ction. Rate
6 of26 EP110\026 ACE ENV!R0N'I.1ENT AL PTY L T:) J010-039
C/o&Jit $�J":,p/0 ;[; $801
4.00
17-FE6·20 1 1 15.00
Slight
5801
4.25
17-FEB-2011 1S·CO
S801
4.50
17-FEB�20 1 1 15.00
Modnrnt0
5801 $801
4.7$ 5.00
17-FEB-2011 15.00 17-FEB-201 1 1500
EP1101026-ll19 EP1101026-020
'·' '·'
'·' '·'
Moder&t\l Modwat&
h c·.,.,-,_.'"''3"''"-'> ���*''' c�·-"'".""f
i''''J'-' \'""'K Ci<dUI'
Cl1�r,! c··roy'"t
Anafyticai Resu!fs 8c<n .. r,��tr:�; S01L
''Roaction Rato
7 Ol26 EP1101026 ACE ENVIRONMENTAl PTY L TO J010-0'39
C/l&r1{ :;�mp,'�· ,'D SB01
5.25
�7-FEB-2011 15.00
Moderato
5,50
17-FEB-201115.00
Moderato
SS01
5.75
'i7-F.EB-2011 15:oo
Mod<lrato
SB01
6.00
ti-H�:B-2011 1.5 00
EP1101026.024 ---·----'
5.0 5.0
Moduate
SS01
6.25
17-Fi:B-2011 12 CO
EP1t0t02$·02S
'·' '·'
Modorato
A C.·rnipl,c•,f .�.·GC,",,,., �. ,'f,{C'V' c,x, .. ;o,ii>j
Pav� Ww�O .. ci<x C!'�'i" !0ro,�·:U
Anafytical Results ::;,,r,.�,·iitt:l�: SO!L
pH �Fox)
Reaction Rata
8 of 26 EP110tG26 ACE ENVIRONMENTAL PTY LTO J010-03S
0.1
C/•0'11 ;,;gnp!,) !!:;
pHUM
SBG1
6.50
17-f'EB-2.011 12 00
Moderato
6.75
17.FEB-201t t2:oo
"
Modwata
SB01
7.00
17-FES-2011 12.00
Moder3t\l
SB01
7.25
17-FEB-2011 12 00
€?1101026-029
'·'
.., Slight
SB01
7.50
17-FEB-20'. 1 12'00
EP1101026-030 --·-
'·'
'·'
Moderate
A(,,.,�·�·�:,· iJ.·.;;•:M;; i.•n"l''-' (',\·: r•;'""t
'<•;)'." 'A or.\ O'd�·r
(:\,Gr\
i>rc�;,,n
Ana!ytica1 Resv.fts
SCJt>-M<�tnx; SO!L
j ReactiM Rata
g of 26 EPHC1\l.?!l ACE ENIJIRONM2NTA\. PTY LTO J010-03S
Ci'"'"' sample .'D SSC1
7,75
17-FE:S-201\ <2·.oo
Moderate
SB01
8.00
17·FEB-20n 12·00
Moderate
SBG2
0.25
17'-FEB-2011 12 00
Slight
SBOZ
0.50
t?�FES-2011 1260
EP11G1021).034
'·'
'·'
S!igl'lt
SB02
0.75
r 17-FES-201 1 12 oo
Ef>1101021>·03S
'·'
'·'
Shght
A :J,�:,p�c·) [;CAlC\'� '''"'!''-' (,''-''"?Y"f
' "' ' m • � w 0 " "' w • ,:;:- 0 • � N • 0 " 0 0
" ' ';" ' m • m � w 0 0 � w • e 0 •
" it 0 m 0 0
e,,;_, '""'!'·' 0'""'"
,;:t<mt
l"•rJJ-tCl
Analytical Results
s,,p..Mmr·x: SO·IL
pH (Fox)
R<Jaction Rate-
1 1 Of213 E?\101026 ACE :ONVIRONMENTAL PTY L TO J010-039
(.'i,Mt s,;,rf'ple IC $602
2.25
17-FES-201 1 ts·oo
'·'
S!lght
SSG2
2.50
17;FE8-20 1 1 15'00
SBD2
2.75
17-FES-201 1 15:00
Slight
SS02
3.00 17-FEB-2011 1 5 00
EP1101C26-044
'·' '·'
Slight
SB02
3.25
17-FES-20 1 1 15'00
EP110102�·045
'·' u
Slight
A .:;�_,,,�Qr;,\ fcui:,o,·., ;,,/"'"" Co',' I l'<J'.'f
P<'" \''{nr�, 0<'<C: Ci,e:�t �·'IQ)'X.1
Anafyticai Resuits ·.>Q./·,ld!!lo: $0\L
1 2 cf26 EP1101026
ACE ENVIRCN!I.'ENTAL PTY LTD
J010-03'.l
C:r,;n1 �,y,p.'� iD SB02
3.50
17-FES-201� 15:00
Slight
SB02
3.75
17-FES-2011 15·00
SB02
4.00
17-FEB-2011 15.00
Slight
SB02 5602
4.25 4.50
17 -FEB-2011 1 5 00 17-FEB-2011 15'00
EP1101026-04S EPH010Z6·0W -----
'·' '·'
.., ' ' Slight Motl<lrat<>
A (>,,.-,�'-"'') !). �,-,,,., �,-, ,,,-e,.- �-"'.''"'�'•!
f>,,,_,, ..
'/\'<;cK C;.•,·i<J-r
Ci.c>n\
Prc;<>-c:
Analytical Results S"b--M;>l',�: SOIL
pH (Fo�) Reaction Rate
1 3 of26 EP1101026
ACE ENVIRONMENTAL PTY L TO J010-03S
c:.-en� $¥r:;:A:) :0 5602.
4.75
17-FES-2011 15 00
Slight
5802
s.oo 17-FES-2011 t5 00
Moderate
5602.
5.25
17-FES-2011 1 5:CO
Mod<!>rate
5602
5.50
17-FE8-201i 15·00
EP11 C1(ll:�Hl54
•••
'·'
Sligh!
5602
5.75
17-FEB-201 1 1500
EP11010Z6..US5
• ••
'·'
Moderato
A C,;·npC<· '! 3:</i''-" L"'''""' Gc-•c·pJ'>_;
Pd,i,l \-\iol). Co.\•Jr Cl,<:nl P>·q,x-!
Analytical Results Sl.C·I>.bt!.·�: SOlL
14 Of26 EP1104026
ACE ENVIRONMENTAL PTY L 10 .1010-039
C '01>1 S¥!Jp!e ID 6,00
17-�EB-2011 1 5 0 0
6.25
17-FE8·2011 15.00
6.50
n-FEe-zo·-1 'is:oo
SJlght
SB02
6.75
17-FEB-201 1 15'00
E?1101026-05S
'·' '·'
Slight
SS02
7.00
17-FES-20\1 1 5 00
E?1101!1Z6-060 ----·
'·' '·'
Slight
fl, c,,,_.,,;,�d tNI.''"'" �,,,•;:c·� �C.'·""'"I
h1Q0 V',ock C'l-1•'"' c:,ww f·'''*"l
Analytical Results
SCJt,.P,\1':"" S01L
Rea<:tior� Rare
1 5 of 26 EP�1C1026
ACE ENVIRONMENTAL PTY L TO
J01 0"039
Ci,f!,;t s.'!mple !D SSOZ SB02 T'··-·
· SB02 $802 $803
7.25 7.5o 7-75 a.oo o.25
17-FEB-2011 15 00 17-FEB-201 1 15:00 17-FEB-2011 15:00 17-FEB-20i 1 15 00 17-FE8·20� 1 15.00
Slight Slight Sligl>t
E?1101026-0&4
.., '·'
Slight
EP110102$.065
" ,_,
Moderate
'
A C'•'l•;,·t>c•.J £>�·'•c•!O f.-'-'il."iC'•:I <::0>'"W'•f
)> .$ (; :;:: £ (/) I " • " � & " Cc c' " ; • ;:: ! ,, 9 "' A �-• 0 0 " o' 0
• " ru � Q -r :u * £ <4 �
� " ' '" � 0 � ' 00 � 0 • " • 0 0
i: i ' "' ! § � � � " w 0 ' 0 " 0 " : ' � b • 0< • 0 0
m � ] m !i w � � :# • " w I • 0 e • 0 " " " 0 " • � �
" • 0 0
!''�:)'·' Wo<icO•·Jc•'
Cwm� PrO)W;l
Analytical ResuJts
Sui>-Mntnx: SO!L
j Reaction Rate
17 of26 E'Pi101026 ACE ENV!RONMEN1AL P1Y L TO JCt0-039
C:'enr sormo!e IS 1.7$
F-FE8-2o11 1S.c'o
5 5
Slight
SBG3
2.00
"n-FE8-20i\ 1s-o6
5804
0.25
'17-FEi:i."2o1 1 1 5.oo
Moderllt0
SB04 SB04
o.so 0.75
17-FE8-2011 15·oo 17-FEB-2011 1 5 00
EP1101026-li74 EP1101026·075
'" '·'
'·' 5.5
MOde rat& S�gtl\
A G":nro--�,,;; & o<.'>c'"• c,·, •• tc•;l C c"''�"''r
.,.',•·?'-' ','.'�" ()1·.'-•·
C\l';'r',T
""'J"<:i
Analytical Results
i"ic;i:dhit<,x: SOJL
Reaction Rate
< 8 cl26 EP1104026
1\C€ ENVI�ONMENT AL PTY L TO
J010-039
U.t>'m s·.Jmp(e ro
(;),'':!4 .IJ.'ri/J>�·ng 1HA" I im:c
0.' prl Unit
SBCM
1.00
n-FES-201 1 ;;;-oo
M Slight
SB04
1.25 H-FES-201 1 1$·00
s.a·-
Siight
SB04
1.50
17-FEB--201 1 1 5 00
...
Slight
S804
1.75 17-."E8-2Cl 1 t5.00
EP11G102S·G79
.., Slight
S804
2.00
l7�"E6-2Ci1 1 5:00
E?110�02S·OSO --
' ' ..,
Slight
A '""'"Db¢;, 1i.-vl!'"'" c .. · ''""-: ('"";.'"'"
.�'-'·]•'' 'f<'o�:, C<d�: Ci,�·m ,c·,n ·"'�i
Analytical Res:uus :,�_,!) .. �·\Gtl\x: SOIL
pH jFoxl
Ruaetion Rate
19 of 26 EP1 1 01026 ACE EN1/iRONMENTAl "TY L TO J01C-OSS
C'li''''( $Jcr:pie !') SBOS
0.2:$ 17-FEB-2011 15:00
Mo<lerate
SBOS 0<50
17-FEB-2011 1 5 00
Moderate
$805
0.75
17-FES:.2011 15:00
$8()5
1.00
17-FE8-201 1 1 5 CO
EP110102S.·Oe4
'<' '<'
Slight
$805
1.25
17-FEB-2011 15.00
EP1101C25-0BS
,<, ,<,
Slight
A Cli.".•:-·o�;! 6r�lm�> L''""'·" C"·r•:O.n(
,'"'d0� '1\'Uril C·tdG·'
·:·:k(l\
?'C)'''("
Analytical Results
Sc.b-Mi,ifl:<: SO!L
20 of26
EP1101�2&
ACE SNVIRONMENT AL PTY LTD
J01D-039
Ci'")l� ,;.,)."'!;:>.'<! /0 saos
1.50
1!-FES-20;1 jf>·OO
'"
Slight
17-FEB-201 1 15'00 17-FEB-2011 15 oo
' ' Sn911t
saos S806
0.25 0.50
H·FES-201 1 15:00 17-FES-201 1 1 5'00
EP1101026..{)8S EP110102&-090 .. _: ., "' s.o '·'
ModtltM� Moderato
), C,;·.yrM\ (l;W''I'> L"i>J<K' c'•J',O."'l''Y
"·''�" f'Qh, (i,d,>r c.�"'
;">;-o;\0\;,'
Analyticai Results
Sc,b-\htr',�: $0\l..
21 of26 EP1101026 ACE ENV!RONMENT"'-l PTY l TO J010-0:}9
Cl.1;"� �:lmpiC' IS
Chent
SSOG
0.75
" r7-FEB-2.ot't ,·s·o'o
Slight
SBOG
1.00
ti-FEs-<.Cj't tS·o6"
Slight
SS06
1.25
t7-FE6·2.0 1 1 15:00
Ef'11010:U·09l
Slight
SSOG
1,50
'i7-FE8-2ottts.6o
EP110102S-ll94
..,
.., Slight
5806
us
17-FEB-2011 15:00
EP110102S·095
5 6 5.<
Slight
..; c:"·";:t":' '""'""" "'":'.�' c'"":··�nt
hliJC'
'/.JG:k Cl(i•,;c C:.C•r.t f'rQ;CC\
Analytical Res�#ts s,,toA,l:;:m: SOIL
22 0( 26 EP1101026
ACE ENVIRONMENTAL PTY LTD
;010-0::>9
(;,- SBCS
2.00
SB07
0.25 17-FEB-201 1 1 5:00
Slight
SB07 Cl.SO
17-FES-201 1 1 5:00
Slight
$807 SB07
0.75 1.00
17-FEE\-2011 15.00 17-FEB-201 1 15·00
EP11010ZS·OS9 EP11010ZS-100 �
,., '-' <.< '·'
S!�nt Slight
A (';,,,."��;>_,;! ih..\'w,-,, �""''"" 1:uo'"'''-"
r-�0'' 'o\'O'K Ct.;J,or Ci'""' !''fU,<�'"
Analytical Resuits
SuiHv\c·:m�: SO!L
R"act\on Rata
23 of 26 EP1�C1026 ACE ENVIRONMENTAL PTY L TO J010-G3e
C><J'l! S.·Jmp��· ID SB07
1.25
17-FES-20;1 15·00
SliGht
SB07
1.50 17-FE8-2011 15:0c
S!ight
S607 1.75
17-FEB-2011 i 5 00
S!igirlt
SB07 seos
2.1)0 0.25 17-FEC-2011 15 00 17-FES-2011 1 5 00
EP1101G26-104 EP110102S-10S -
'·' '·' '-0 '·'
Moderate Mod(>rate
li [\,",.';0c•\ 3t..,;'.'<;r; i..<.'l 'oiC'G C'·.· :.;'"''1
'""U" Wx� (;;,:tvr (;1;0:'•'
"''1!]\·:·(:\
Analytical Results
2·.,b·>V,Iht: SOlL
Reaction Ra�
24 of 26 EP11D1026 ACE ENVIRONMENTAL PTY LTD J01 0-0:>9
"
Cf,n,,� S$imple :!)
0.50
17-F£8-2011 15:00
Moderato
0.75 17-FES-201 1 1 5.00
..
Slight
uo 17-FEB-201 1 15.00
Slight
SB<l8
1.25
17-FES-20 1 1 1 5 00
EP110102S-1C9
'·' '"
Slight
ssos
t.so 17-FES-201 1 15·00
EP110102S-110
'·' ..
Slight
,; Cwi:,oUvo'; B:uir'"" �"'''""' C•e""""''!
P;;-;;<; 'Aor� ()l(ldt-
Ci.<>;>� \'roJ"''�;
Ana!yticaJ Results
2<Lh-Mmn�: SO!L
pH {Foxl
Rea<;tiorl Rat<>
25 of 26 EP11010;<6
ACE EN'/tRONMENTAL PTY L TO
J010-0%
Chf.'n( s,i!rnp!e .'D
Cus-n1 sarrwirf)q aM" I :rm&
·a.1
sec a 1.75
17-FEB-2011 15:00
·st·i-Eiht
$603
2.00
17-FE8-2Gt l 15'00
'·'
Slight
H-FES-201 1 1 5 00
, , ·--Siisnt
SBQA2
17-FES-201 1 15 00
EP110102S·114
'·'
"' Stlght
SSQA3
17-FEB-2011 1 5 CO EP1101026-11S
"' "'
Snght
A G.,.-,.,u.,;! "''--'1·'"''" : .. .-,;;%' (:.y:qu'-1
p-�,)0 '�""''·''' a,,;,;, ..
C":n� I'''CJC<"-t
Analytical Results
S"o·M.,.Ir•,,: SOIL
26 of 26 EP1101026 ACE ENVIRONMENTAL PTY L TO J010-02S
C!ienl 0!Jrrp!0 iD S8QA4
\7-FES-2011 1�:00
Moderato
SBQA5
Mod&rato
SBQAS
t?:FES-:<61 1 1s:ao"
Moderato
SSQA7
1?-FE8-20;1 ts·oo
E?1HHil2li-119
'·'
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Environmental Division
Work Or<:iur
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[email protected] .,.61 08 9497 5000
J010-039
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Environmental D1vis1on Pertl'\ Scott James 10 Hod Way Malaga WA Australia 6090
perth,[email protected] +6"1-8-9209 7655 +61-8-9209 7600
NEPM 1999 Schedule 6(3) and ALS QCS3 reqwement
18-FEB-2011 22-FEB-201 1
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accordance Wtth NATA
accredrta�on reqvtrements
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ACE 2NViRONMENTAL PTY LTD
J01C-03J
Genera§ Comments
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It No Method Blank {MB) or Laboratory Conttro! Spike (SCS) Results are required to be reported,
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INTERPRETIVE QUALITY CONTROL REPORT
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gma@aceenvironmentat com. au .,.61 08 9497 5000
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Erwironmer\tal �vision Perth Scott James 10 Hod Way Malaga WA Australia 6090
perth.er1viro. services@alsg Jobal. com +61-8-9209 7655 +61-8--9209 7600
NEPM 1999 Schedule 8{3) and ALS QCS3 reqUirement
18-FEB-2011
22-FEB-2011
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$802 - 0.25.
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ACE EN1JIRONMENTA'.. PTY LTD
j010-039
8801 - 2.SO,
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ACE ENVlRON.MENTAL PT'I l TO
J01C-039
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and ALS oc_�-� .r?9�.•r,<;_':l_1,er:t __ .� .. _
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Brief Method Summaries "!'tW i't�,>i;\,<:81 plOCCC\JC�S US<i<' by tt"l \"n,·II'Onm<>niul Cnv<�•on hc\Ve \)Q�rl ctevelc�N; from \CSWllt$'1ed :ntem:;t,on�liy t"�)gn1ZOC prOC�duW:> s�ch 00 lC,CS'.' p:!i:>'l"£.l>ed 'cy �M· ;,)S fp,<,, APH.•';, AS 1\�.(! Nf::Pl/ I� �0',10\; <k·•dC�(·�d prcc<o·j<lt�& �'" i:m;!io;"i:0 '"' tn<o ab�n.�v of dOc�me,;tt>C 1'·l«ndords or oy '�'enl '"�''"�1 TI\G to:tow:n\) nop011 pmv,des bMf de>n<pt,.-,,�1· of th.c :>n�lyuc:,11 procc<i1;f0$ •.Jm�loyc_•d �·x '"''idts '"'POrtee ,n :<w CW(Lic�\0 ot 1\n�;ym;, 6o.1f�'\O� -'TCII\1 wi'"<.t\ ALS �'�'hOd� hiMC b,e•,;1 <.'<-'VdOpGd ,l<'i' p;MidL'<J ,.,,;�:,,� 8\!' !>'\eF;oc Cl\,'i'CCol)bo.�s
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Summary off Outliers
Outliers : Quamy Control Samples
Tr,B icllo·A',n•:• roopoct. h<\l�ll,gt11C, Q,<ti;"'lt li<t<;Jg"'\l ,n �h,, Q"CJl.r) Con�'ol (CC� R"?C<\ SU1tC(p:� r"'cove;y i''11<tS 3rt> S\O�G Jnct b,)Z�<.l en USEPA $;',.V84$ c: ,t,LS-QWi:C,'{/:!,8 {<n ;M acse,.we ct �t!c,c·.t,c \.'SEPA llfl:lh). "'t><s i'"PC·":' Xop�Jy:< CC Ou\llf;(.'< (bn!:l,:nc,·;) cMy.
Dtlp!icates, Method Blenks, L,lborato1)' Control Samples and Matrix Spikes
o For an matrices, rto Method Btanl<. value outliers occur.
0 For all matrices, no Duplicate outliers occur.
e For a!l matrices, no Laboratory Control outliers occur.
e For all rna1rice&, no Matrix Spike outners occur.
Regubr Sample Surrogiltes
e For a�\ regular sample matrici'IS, no surrogate reeovery outliers occur.
OuWers : Analysis Holding Time Comp!iance
Tnr.� rc.,oort d<spic.y� H<:lk�n\(j 1'rmw brwnch0> only. Only 1M; re,,p0d1ve Ex;r�d.tcn ! Pre��lriltVl <lnd:ar 4-.Mr.i'tt;,•, �<Jr:'.:IOM;nt 1s:nr" diSPbY'-':i
o No Analysis Holding Time Oulliers exist
Outliers : Frequency of Quality Comrot Samples
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AUSTRALIAN lABORATORY SERVICES PIL EP1101327
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ALS Laborator4 Group ANALYTICAL CHEt.11STRY & TESTI�iG SERViCES
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Wcri< Order
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f'.fri:J:J
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ACE ENVIRONMENTAL PTY LTD
MS GINA PEMBERTON SHOP 1712 SOUTH WESTERN HIGHWAY ARMADALE WA. AUSTRAUA 6112 [email protected] +61 08 9497 5000
J010-039
G P
EP-163-10 BQ
CERTIFICATE OF ANALYSIS P<>U"
Ldx>r�tor;
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1 of 4
Environmental Division Perth Scott James 1 0 Hod Way Malaga WAAustralia 6090
perth.enviro .seTYices@aJsglobal. com +61-8-9209 7655 +61·8·9209 7600 NEPM 1999 Schedule 8(3) and ALS QCS3 reqwement
04-MAR-2011 22-MAR-2011
'"c cl so.rnples re\Xlwcd 4 :-/o_ of �;:un;::l�s <J:Vllys�d 4
Tt11s repo1� wpersed8S any prevt(IUS wpcc(s) w:tl: U1\s r"lerer.ce. Results apply to :rte sample{s) as release.
pc:ges of \h1s f(:port have oeen cnec�.ed em: 3pprovet: kr
1'11iS C0rM:caw of f\nalys1�, coflli'l:llS (M folloWII\(; m!ormation·
o General Comments e AnalytiC81 r�esults
NATA Accredited laboratory 825 Signatories
NATA Ths dccument <S issued 1n accordance w1th NATA
accreddatiOn requ1rements
ThiS document has been electronically Signed by the <lllthorize<:l signa((;ries :ndiCilled below. IC:IectrC111c scgrung has oe10n
carne(i out ,D comp!lcmce wtlh procedcires specifi'8d v-1 21 CFR Part 11.
>'loJ>!"� Hl·�i)"�>'>J.O ACCl'lf!tl�TA"nO!<i
Accrochted fer compl•anceWJth iSOilEC 17025.
_, ___ _____ _
S;,m!ii!ones Chas Tucker C1cetm Bartels
PCSIIIOO
Inorganic Chemist Metals Instrument Chemist
En<.Hronm@nt"'! I:W.>l:;:>on P•ntil p-�c; �� lh<O ALSO L.M::""�"'ton.J o.-oup
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Ac;ctc·di!atJ::>n C<w;gory Perth tnorganics Perth lnorgar11Cs
P�·)0
'o\Qrk Q,;t.;,r Ch'n(
,D".))�ct
2 of 4 EP1101327 Amendment 1
ACE ENVIRONMENTAL PTY L TO
.!010-039
Genera! Comments
-�hcc aM<ytr.:<tl wcc�:qures l;WG oy th� Enwontr�cntc;l Dr�'�"c'' hiM> lloi'�· de-,,oloped tl'0"' es:.ohi·,snco.-:t rnbrn;wcnal!y rvcog:l'.lM procedure.� �uct-. <IS �n:x;oe pcroir•;hM Cy tn0 US!;:PA A?HA AS M\d NEPM In !'ou��
(I<N0i<:po0 ;n:xwdc.n,� me- <:rq/oyc\1 "' tne ol,�<onm ol doc,:·l'�·mc•d S'i<''>dmds ot OJ ci!%t wqcr'1'\-
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V'.,l:\eto � ruported 1-��'� t:L�n (<i ,,,·�dt rs �Jgi\H th:on th<J lOR :nts may tm <:<uf! to pr,rrs>'f sam pi� extrsct/0:(l�·statu �;t<Jno� and: or ;no.,, mont 2arn�:u fer �na!y�iiO.
Wlwru the I.OR ot a '"�orted '"'�"it d:trers frcm �tandard LOR th's rn1:1 l:le di,1l to �:gi: mcts:ur� ccnter.1, "l�d.'.c;�nt smnpiD it2\'J\,C0d VNrgr,t anplo:;ed\ cc mn�nx tntsr'tc•:unce
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K':y c_,>.s hwml'�'' c;;,s r<;,g,�uy number (l(lrn datab:;.s� <n'!l.rntwn<d by C:Mrv::�l Abs:ra·�bl s,,,..,,c-cs H•e cn,_nncui Abs�rocts s�rvrc�· ts :> dr·,,�,:_r� of the Amcr:c�n CMr"rJCal Socr"'�Y
LCR � Lomll ct' �-�part,l'G
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A C.t·CJp0"'! &oVWo �''''''"" CvYC;W•f
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Analytical Results ,,.,,i' .. --N.Jt•>x: WATER
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3 of 4 EP110l327 Amendment 1 ACE 2r>;VIRONMENT AL PTY L TO J0'0·03S
M801
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4 of 4
EPO�G1327 Amendment 1
ACE ENVIRONMENTAl PTY l TO
.'010-039
04-MAR-2011 1 5 00
QA1
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ALS Lal:loraton.o� Group ANr,LYTICAl CHEMISTRY & TEST!�G SERVICES
Environmental Division
QUALITY CONTROL REPORT
WorkOrdw Am"n<lmonr
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Contact ''"dre:ss
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, EP1101327 j ACE ENVIRONMENTAL PrY LTD
MS GINA PEMBERTON
SHOP 1712 SOUTH WESTERN HIGHWAY
ARMADALE WA, AUSTRAUA 6 1 1 2
[email protected] +61 08 9497 5000
J010-039
G P
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Pag.;:
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Cor.tact Addwso
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T �l0oho0\'� Faco .. m·l0 QC l.evcl
Dt<'-" SJmpk�> Ribr.e•ved
b�(lG Date:
1 of 7
Environmental Div'tsion Perth Scolt James 1 0 Hod Way Malaga WA Australia 6090
perth.env:ro [email protected] .,.61-8-9209 7655
+61 -8-9209 7600
NEPM 1999 Schedule 8(3} and ALS QCS3 requirement
04-MAR-2011
22-MAR-2011
No. of s&mpl�� l0Cet;0ct 4 N<;. oi �a.rnpl% anulyoc•ct 4
Tr<i� report supe1sedes any pn:.vious f(Cpott(S) with Hlis referi�rtGe Re-su:ts ar>ply to the s.:�mple-(s) as su\1r:1it\ed. ,;11 pages (Jj thiS repo1t �1:.we bec�r1 (�necked and :Jpprowd lor
rdlc'�\Sf<. Tl'o�s Quality Control Report contw:s the foilowtng 1nlormation ·
¢> l.N,cm10'y C!':p\ic&\e (OU?r i<D)-Jor":: Rel<.1wte P01C<;:(l1c>ge \J,rtsrence (?..PO; ami ACC('P1l1f1C0 L n\its
® Me:tnod bl:,1nk (Mb) :md L::�t>cr.oto:y (:(>n:roi Sp<kt· (LCSi Rq:>ort R0,:ov-�'Y .gnd Acc<lPtanco UMs
IGI :;1iltr�x Spt<e i.\1S) Ro0oart: Recov''IY ;v-,c Acceop\i.lnce Lmt,ts '"'"'''"'''"'�'•'� '"'�'''"�"-''�--�---•�• """-�--·-•"•-ww�··•-••n*--""'-'--�·-'•,>M_M_ """"""""-"'""'-'"'"'-"''--'"""""--��""-�-•·---" •••·--'-•"""""'-�"'"" """""'�""'"'""'-""-""""' ___ "_"_"""'"'" '"' "-"""""""""���-"""" •
NATA NO'<·•' �!'�O�NI�•f'? ACCR!l:C�TATlON
NATA Accred<ted Lat>cn>tor,• 825
Th's document 's issued tn
accor<Jance with NATA
accredTtallon req\h·renwnt;;,
Acefed:ted fer compliance Mth
ISO/IEC 17025.
Signatories Ttits (J<)Cument ras been 10kcttcnicaliy signed by t�e authonx.ed $1\)natones mdLCaled bdovv. Eiedron:c St(Jn1ng has been
carried out in compliarv;;e with procedures spec1fled in 21 CFR Part 1 L
fN;f!l"��·ni•S Chas Tucker Cicelia Bartels
Po�'�'OI" Inorganic CMmist Metals Instrument Chem1st
;:.ccwd,win;m Ca1eqcx; Perth lnorganics Penh 1norgan1c.s
I'';Jq"'
'A<xK O<J.;r c:,cn:
i"rowcl
2 of 7 EP11C1'0-27 Amendmen1 1
ACE ENVIRONMENTAL. PTY LT:J J010·039
Genera! Comments T�f! :l11il';1<·;,$) ,?.·oa;;dwe� c<S0() o·1 the! E�Y-<<>n;n<:rl;>i Cw'�'o" �:<.1-Jt' b�en devdq,,ed !'I<Jm e�t;Jbld>ed <r<te!Mtlonol!y recogn,zcd ::Orcctodur.c�, guch «s :t,oc·,e p"f.lid1ed :;;y 1he L.'SEPt•. F·i"HA 1\S ;,r\'Cl !':O'Y)� h r·,o��\\
<JI!VdopcJd f!I'Oe<o•dcrr�s �'� �rnr.•luyc-<1 11'1 \lve Oli�Vnct> o( dOCUI'I<irnl�d t<l��d�r<JS Oi' by <::i,�·nl f'il(J�O-�t
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W�<OW \M LOR or <l reporkC:: r"su:t dl�h;n; \rcrn 'i:\andNd lOR. th<S :nay be (']''"' 1.0 'WJ�\ '1\Ciiltufb CGnkr:t. :ns"t:':G:"'nt S;Jm;-,!<J (roo:uoed w<:"i)h\ employ cO! or m<:l'nx ,n,ecf.,.�n:r>C'-'
K·,1y Ar,<l"'l'nO'.!O ·" Ruf,;,;� '<l S<ttn�>ic-� wh:Gh '""'-' not s:;,,c,h:a;ly p�!1 of tlw; WJI'k orctor l>ul (<:,:r�,1d pG<'t oi �11� QC prcceos 1'-11 c,:,s IJ""m"r '·' Ci\S 'O(Ttt\ti'Y �umbe1· fro"l �:>tBbil.><O n'-'l1nt�:l1ed o; GMm,�<>l Ah��m.ct& Serv<Gf�!l. TM Ctwn'''""l (\ilstwGt� Sc:r�IG� � � a d;vo'i,<0<1 ct tn� ,-".m<�>lC�n Ch"'rnc�l So,-,,,.�1 \.OR " L1�1,; of re;:>CI�W.g
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for �11(· !'��l.atrw.> P,"rC•"�( Dc>:·<rC>�:cn (Rf>Di :of L.ai:orntcry 0\:picJ:os ,,,.,, s�r;,::t'IG·d u1 '"LS Methed OV·il--Et\:38w:cl 8fel depcnden\ on In<.> nugn:lc,dCl ot c.c·:.u::·o :n c:C"fop,;r:v:�n �o �!-,e it':vCI ot ro[Xlrnrq :��zc.l1 'iQ l:mc•; l.CR �,;o "'"a:. ?;cv.::, b0tW<>'-ln ',() "/� 20 �""'"·' l.OR.- G-,.�. · �O-% f�C%1t ,, <:O t>rh"t' �OR.- G%- 2(h'< ..
EP1101324-0C2 Anortymcus
, EGOZOA·F· Arser11C ' EG020A-F: Chrom;um
EG020A-F Copper EG020A-F lo�d EG020A-F _Manl!an:Sl:l
, EG020A-F· N<C>;el . EG020A-F· Zmc
EG020A-F· Alummium EG020A-F. Selen1um
:·EGOzoA·F· !ron 'EGozoA:·f. Cadm1um
EG020A-F. Arnemc EG020A-F: Chrcmrum
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7440-43-9! ; ..
7440-38-2 i ..
7440-47-$''"'
0.001 mg/L 0.001 mgiL 0.001 mgiL 0.001 mg;L
06' mg!L 0.005 mgA. O.G1 mg/L 0.01 mg/L
0.05 mgiL
0.0001 mgll 0.001 mgiL
0.001 mg/L
L,,l<ot�l�ry D�plicMe (I./UP) R�pon.
6.54 '·" 0% " 20% 4.14 07 0%" 2.0%
0%- 20% 13�0 17.:; 0%" 20%
,, 0.0 No L'm't
" 00 No L1m1l
,, 0.0 No Lrm1t ,, 0.0 No Limn
" 0.0 0 % " 50% eo; ' 0 0%- 20%
" SA 0 % - 20% <1 00 No Lim•t
" 0%- ZO% "' o.s 0%- 20%
<0. 0001 0 0 No L<m'� <0,001 <0.001 o.o No Lim<l
<0,001 "<o.'O'oi" o.o No Lim't �o oo1 <O_Q01 o.o NoL,m;t <0.001 <0.001 00 No Ll1'l1Jl 0.007 0.007 00 No Llmrt
<0.001 <0.001 0_() No Lnut
<0.005 <0.005 00 Nolimft
0 02 0.02 00 No Llmlt
<0.01 <0.01 o o No Um1t
<O.OS <0.05 00 No b-mt
<O.OW1 <(!.COOt M NOL<mrl
<0.001 <0.001 0.0 No L<mrt
<0.001 <0.001 00 No Limrt
A c."· 'P'-"''-' 6ui,\cc; u"''""' C•. n�""Y
;�:.·y" 1Nor� OldcJ
C!·cm """'"''" 4 of 7 EP1101327 Amendment 1 ACE': ENVIRONMENTAL PTY L TO .lOt0-039
EG020A-F .
EG020A-F: Manganese EG020A·F: N<ckel EG020A-F Z1�C EG020A-F. Al<.!mrnrum
Ar�en<c EG020A-f· Chromium
EGC20f\.F: Copper ' EG02�A-F· �ead
EG020A-F _Manganese EG020A-F. Nlckel EG020A-F Zrnc
EG020A-F' Al<.!mrn<um
EG020A-F- Seler-1um
7�39-96-5 :· 0.001
7440-{)2-0 0.001 ' 7440-€6·6 0.005
7429-90-5 ' 0.01
C.001
0.001
7439-96-s !· c.oai
7440--02-C i 0 001
7440-6&-6 0.005
7429-90·51
7762-49-2 ' I
0,01
0.01
mgil mgiL
m•c
mgiL
mgrL
mg1L mg/L mg/L mgiL mgiL
<0.001 <0.001 0.013 0.02
<0,01
<0.05
<0.001
0.00&
<'0,00�
0.061
0.005
0,076
<Q.Q1
<Q_Q1
' EG020A-F' !ron 7439-89-B i 0.05 mgJL <O.OS
-l&r&lll\�llilRI.W'i'Vill-lll�llfll!lill!��l�lll' llllli''''IIW\IlWIIi'.WI/1TI'ill"'il!:C\1\II' '' ' '' •··· Wii&liiii:&'RI.�, liilllllllll)l\itl\llll1ltJill.B.\\'l&\1!Jiii'lif,,W\ . ik\iil '.1!kit1k\(,QIQ-\)fiL\io1�l)l(�>:-.¥:s-WN;\_;:_!)\i' ._., . . · '·'··
74�9--97-6} 0.0001 , mg/L -<0.000\ ... ' ''"'"\"li"�'II'�111W!i!IW�W'&''"!I''"'""'I'��'!'''''""' ·w , · � Willilli@lJl; Wif]KU11 •lf1ll)fiHil0 . \\;!· \ l\-)fft' �!�). '-''\'&'k! FiY1U>'·y, ,..,,_ ,.-.. __. ... • d4 ,. , ,K * . . �0 Hi) ·";:J},).ii M!it (,,,,�\1,,,,,,, '"''"""'"'"� ........ ,-c.· .. -EP110t324-00i Artcnymous EK05SG. Ammor1a as N 7064--41-7! o.ot mg1L 0.05
7664-41-7!
"'0.001
<Q.OD\ 0 ,01 3 0.02
<0.01
�0.05
0.0001
-<0.001
<0 001
0 009
<O.V01
OJ)$0
o_oos
0,075
<:0.01
�0.01
<0.05
<0.0001
0.04
0.12
9.07
a.os
0 9
1.5
"'"Q.'i.i' ' ·a,x: "2o%
0.0 N0 L1mt 0.0 No;_:mLI 00 �u L<m•t
0.0 Noum't 0 0 No L•mt
0 0 r--;o L,mt
0.0 NCl>mrt
00 No L:mt\ 0.0 No Lrm1r 0.0 NoL:mr\ 0 0 NOL1m1t 0.0 No L;mn
1.9 0%- 20% 0.0 No Lim<!
00 0%- SO%
0 0 NO Lim1t
0 0 NO L1m1t 00 No L;m:t
0.0 No Lim•\
0.0 No LLm<1
30.0 0 % . 50%
0.0 No L•mrt
0 0 No l>m>t
1A 0%- 20% o o No L<m,t
0.0 No L1m·t
0.0 0%- 50%
0.0 No Llmd
1()_6 0% - 50%
A (;".copiN.'l ih\'w;; L '>"!t'-J (;c,'''P�>''>'
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5 of 7 t:Pt101327 AmeMm(mt 1 ACE EN\IIRONMIS'\JT AL PTY l TO
J010-039
Method Biank {MB) and Laboratory Controi Spike [LC$) Report
! '"·'' qcwli\V c<;n'.rOI 1c;""' �,\,·;t;od L,JIJO'Gtmy 81;mk rd.:::•� to Jtr\ C<:HIVIc !:ee m.Jtrox 10 w�1,GI'\ all r<la')or·,O, ��·Q 3ddc;ct m \he g�rne •mivm<l� or ;;coprt:ons �$ UG�il ,n %'<M.J:<I M'l'?b prcopc,cnt:ot. Tiw fl"rPQ!'k d t:·:> CC p.,lr8n'"''": ;(, (V "nGrno: p(>ior:,-�1 !c1b<:nW,'t) C<lnWrnln:>\IOI'L 1't1� q;J.o!,ty GVt'ctrul t<?rm L,J.bO;<>tny C</\(rol Somplu n.CS; wrer� to a Cd1dl'io:l <U:Bc''"'c"' rnmen!.1!. 01 o. known ;nt.c,c,,,er,o.' tro<.'" rna�rv. o.p:�iJd '''"' '·'-''�;s•\ :.cn�l)';os. ·;·ne P'•<'PV''" o: \111� GC p!.lriln1e'k;' �� lo mon;tO( n'i>�Md ,-,,.;;c,s<or and nc,;,>raot t'ld.:Op�n,�ent o( sa:n9k mMnx. Dyn.'H'fl<C R'OGO·owy '-"POt:< are Mo.e·ct en swm;trc;JI ilVUiiJ<liton cf Pro-.c:.�>():l LCS. 3ur-�r,LW·x; WATER
C:aclm,um 7446.-13�'9 ' O.COC1 Chrom1um 7440-47-3 0.001
Co.oper 7440-50-8 0.001 0.001 0.001 o·:cm
Sclen<Um 7?82-49-2 :· 0.01
!EG020A-F' CadffiHJm 7440-43-$ 0.0001
:'2G02CA·F. Chromtum 7440-47-3 0.001 ;EG020A-f Coppfrf 7443-50-8 o:Oo1
"""""'"""'" '"'"'""''""""-"' '''"""'""'-"'" ''""" '"" "'" L,1�<>mmry Cor,r;ol SpiJ,·o (LCS) R�por: Sp�h R�C<>v<'fY (%j Raov'"Y �'"'"" (%!
" ;30
79.8 ij6
88.1 " "'
'70"" DO
e5 13.0
il:l."S" 7S ;so
" " "' . .
88.2 73 ; ; ; mgJL <0.0001 0.1000 mgiL " ' n 109
mgiL <O.OCi 0.100 rngiL "' " ; ; ; """ <0.001 0.100 mgll 97.8 73 \ 1 j
mgiL <0.001 0.100 mg/L 88.9 " '" mgiL <0.001 o.�OO mg/L "' 7? 107
mgJL <0 001 0.100 mg/L " ' 7S no mg'C ;,:c·:o; 0.10 mg/L 96.8 76 "'
" ' n 115 99.7 " "'
88.1 " "' 87.7 " ; ; ;
mgll �0.0001 0.1000 mg/L S6.5 n '" """ <O.GC1 0.100 m;;/L 006 75 ; ; ; ""
0.\00'fngll."
- <0.001 S8.6 " 1 1 1
-·--·-··--�-----�··---· ··------·-----· A C.1'n;>l'-�' i�·d."!�iO '-"''.!<'" C•Y"'P""I
P;y;<e Wct'r, ;)"okr Ci.cnt ."'m,vc.'
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6 of7 EP\ 101327 Mmet\dmcnt � ACE ENVIRONMENTAl- PTY L TO
J010-%'9
98,1
'" '" ' "
"'
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"
B7.$
"
"
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123
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124
1.24
1$0
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p;,.y, 'f·,0rk C,J..,r (;l,•gq
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7 ol7 EP1-t01327 Amendment 1 ACE ENVIRONMENTAL PTY l TO
J0�0-03$
Matrix. Spike (MS) Reporl
'i're 'l'-'dld)' ccM'OI \\.<rrr; �\:;r�� S).>\k\� (rc1S) nd.,rs :o e<n n1ir->bborutory !,p\:l ''"''">Pk ;;p:ke<O w:1r, " <epno<>ent.:lt<VC. o�t (�1 t:J")N 8l1iJiyt�·�. Th� pu;po<;o ol tnr,; Z)C pnmmetor c$ \iJ mc�oW< potQn'.:i.\1 ,-:,?.tr�x utf·2c:� Or> OJ!\CJiyt,i• ru�'""'"-'''"�' Stat:c R•lO.WC.'"' l •• m:t� �' per iCJbor�:0;y ;')ilta Qual•:Y OD;'lc:w,,s .;:;cOs) lcWJI rc,cov�·ry r;mgu·.', ;;\3Hct m�y br.• war;·erJ >n e1o e�0N of NJ.�1pk m�tr<.� ;nt0rl¢k�C"
S�o-Matr;x: WATER
EG02CA-F Cadmn.rm
:EG020A-F: ChN,mium EG020A-F. Cop?e,r .. ,
....... 7446-so-s EG020A·F· Lead 7439-92-1 EG020A-F: Manganese -i4iS:S6·�s.
• " """"""" """"'' " '"'" " " '"""···· Mcc,c,C"C'.,"··,·,
,.,,.
{MIC
'II if
i C,·,"··,··,
"·""" '
o_zo'O' mg.il 0.2:i0 mgll 0.200m�IL
"' "' 9'5 ' " "' 95.1
EGOZC.".·f. N>CI;el 7440-02-0 0.200 mg/L 113 EG020A·F. Zmc 7440-66-6 , O . .:Wo mgiL j22 "1!1�1' ����g •. , 'il'l"w'll. �"1!1""''1"�·����,��1'&'''·1""''"'''"'''' ,. •····" >;� ' !m�lii! j • ' {{)\! !M(! � 'i'UI 11 '�M)'i' il<!• -��< '"'l '-·\h':J<; ,:,·.·:. .. ·,· 1' '®liiMl ' : · . . &1/ If\", l•iJi\rit&JL,11fi•l\tc\,·\\SH\i1fiLi·,,\iX:\\ <>L< · . . EP1101327-003 M803 :EG020A·F. Arsenic 7440.38-2 ' 0.2?0mg/.L 104
, EG020A-F: Ca\lm<L>m 7440-43-S 0.0500 mg/L 103 •EGC20A-f· O.romrurn
.. ..... i<i4i:i-47�3----· o:206 n1�C 86':$ EG020A·F: Copper
lead Man£lar>es_e
7440-50-8 7438-9:?.-1
"74s9:9e-s"
0.200 mg/L O.zoomgiL 0.266 mg1L
1Ci9 "' 75.9 1 \ 3 9!3.5
' "
80'3
·ns
'02
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f!�C<>v�ry LJmJW (%}
" no
" m
70 130 " 130 70 ' " 70 no " no 70 130 70 '" 70 no
70 130 " no " 130 70 '" 70 '" " '" " '" 70 130
70 "'
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ALS Lalborator4 Group /\NALYTICAL CHEMISTRY & TESTiNG SERVICES
Environmental Division
INTERPRETIVE QUALITY CONTROL REPORT
Wor� Ordor Ame,Himent
Ci<<'n\ Contac\ Addr()S'i
S-rn;:hi
1d€p1G0'>
F�<;•;rn111n
, EP1101327 1 ACE ENVIRONMENTAL PTY LTD MS GINA PEMBERTON SHOP 17/2 SOUTH WESTERN H!GHWAY ARMADALE WA, AUSTRALIA 6112
gina@aceenvironmen\al.Com.au ,.61 08 9497 5001}
l't.ge
Lw:!orato:y
Ccr�tacl A¢c'rt:%
E.n'.Od Te\Gp!1cne
"'ncsrmi<O
1 of 8
Environmental Division Perth Scott James 10 Hod Way Malaga WA Australia 6090
[email protected] ,.61-8-9209 7655 +61-8-9209 7600
!iJ!Il\\''Yi'!N"pm ____ _
PrO;�GI J010-039 oc �"''d NEPM 1999 Schedule B(3) and ALS QCS3 requirement S<�<o C-0·C mi·:TI0"'
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o�o:;,:, nurn�d
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I%Uii tlJI<l 04-MAR-2011 22-MAR-2011
No. <;J! .SDr:1;1)('"$ 10C01Vild 4
No. of sarnples unal�s;,:,d 4 Tn<e; '"'port s�p�'<c<('d0� uny provrou� I'<JP(lrl($) w;ti; r.n<� r.o(erenc<!. l�e>ol�� �WIY to tiK s'>mp!o(sj <>S �ubnwi1·�J. All p<>�<c5 "' �h,s !'€Pot: "'"'"' biJ0G cM,ck,;oo ill\d @pprovcd !or rdei.\�''
Thro1 lnt<'rpr;,;rwr Ocral,ty Control Report con�,ogns th'� 1oi!o-.,;ng ,nfo�cnatron
e Ar<lly"� Hoidsng Trnoe Comptr;,nce
e ·:hlt�dy Cop:n:li »11r:m1�'l'Y Freqw<cc.cy Complton<.:c
41 3nd M?:,ryod Sim·:manl':s
111 S\lmrllary of Ootii?<S
<Snut�o"'""'nt.J>I O>v•slon P.,rtn P:."1 d llk' AI.S L.:>bo�a:ton-< Group
: ') hO') ft�)' j.j,>[,�J 'NA AC')'iJkL 1/#J ;�\ <•t1.o,1CWYIM> FA< •0'·9· \;•O<, /';00 """"'·�'"'"'"""""'
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3 of8 EP1101327 Amendment 1 ACE ENViRONMENTAl PTY LTD
J01C-03S
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01-APR-2011 OS..MAR-201 1
06-MAR-2011 \ 0:4·MAR·201 1
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J(lt0-Q3.S
Quality Controf Parameter Frequency CompJiance bt< :cl\cw;ng report <-ut'nr�:otno·.e� lC•& '""'�''�-�.C/ -:>\ 'abo: &toy CC �v;mpi<;s erwi;��eo ntt111n t�e aPolyt,cal lot(�,} "' wl\:ch the $�tbrnt:�·d s:>rrpi0\5) w:·J�I,wlwr�:) ptOC0%�d Act•Jal mle st:o"IC oe \VeDtcc �lwn or '"'<"ill to :hu
c<pL<;1�d '"1()_ A h>�-ng al oru;c>•o'.< t•1 prov1d�d rn \M Seit'nfn�r"f o( Oeiti>ers �:<>t<cx: WATER
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f.v�l�atr-cn � ·' Quc:�Uy Conl.rcl ;cequsncy not wrlhrq specrtrCil\IOn - Ct:<li•�Y Ccr:<r-�i fr,!<qur,ncy w.tf,,n sp,,(·(;c;...>�,,�,
�$.2 11.1 U3
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6 oi 8 EP1101327 Amendment 1
ACE ENVIRONMENTAL PTY LTO JOi0-039
Brief Method Summaries 'I" no Ofl.,liy\;·�:.1 p;cced\JCcs c·5cd 'c:i tt'->J En,rcnrn<JnDI Dtwo.or; r.ave bt<';ll <hOW-ioped from e•;,wbk.hn<l \f",bn13hcn<�Hv '"cogn,zed prcccc:ut,;os �'uch �� tho>'J P'J\:>L�l,cd �y \C\C US f:ro;, .c,PHc\, AS unci Ni:'.'' :Jl. in '>OCIS" 'k"''"lop<Jd ti'0(.�\1�180. ;,w <OmpicJy"d ''1 lho �b;x,ncc of ctc<;.uno(-m\<c·J �l:lnd;;,r¢s ex l)y Gi''''"' '�"i\H%1. "lhe !i)lioW;ni) 1epor! pr,:,vi<J,';S bn\;! d%cnptwns '!I \�c an<>IJ(IC'�I pmC,l(il.,rc:; o·l<"rp!CVed ''Y :o·,,),L; ''�;:.::rwd ,n \!1(; t;,•rt;t<cnl� ot An-;,ly���. Sc'"".::e\ I rom \Nh,cn /oLS fMthOds haw Oe&n d\lV8Ioped ilr<:l pmv1:.>ed w•tllm trw Mot0Cd 00SC:<9-:;Ms
, Total D1ssolved Sol:ds (High Level) '
'i AlKalinity by PC Titrator
i AC1d1ty as CalCIUm Carbonate
: Sulfate (Turbidimetric) as $04 2- by · Discrete Analyser
: ChiOncte· n;;· Dis.Crete AKiar/S
.er
..
.i iiSsotveii Metals bY 1CP-MS :s·u-ii·e A ...
t·o'issOiVed .. MerCury bY 'F1Ms
Arnmon1a as N by DIScrete analyser
Nitrite as N by Discrete Analyser
i'Nitiate as N by· Discrete Analyser
J Nitn\e and N;traie as N (i-!Ox) by Discrete (.Analy.ser i Total KJeldahl Nitrogen as N By Discrete :', At1.a1yser
--·EAot$1-l E0037-P
E003$
ED04lG
... Ec'64sG ...
EG020A-F
EGO:iSF
EKOS5G
E"Ko57G EKOS8G
EKOS9G 'EKos�G ..
WATER
WATER
WATER
WATER
WATER
4500 H+ B. Th1s procedure de!erm:nes oH oi water samo!es bv automated ISE . . • . coffipli,al1t INJtt: .. !:IE.P.M .. (1.9�.9) .':'.ch��ul!":.f3@. (�pp��: .. 2l.... · APHA 21st ed .. 2540C A gravimetric procedure that determines the amount of "filterable' residue in an aqueous . sample. A well-mixed sample is filtered through a glass fibre filter (12um). Ttle filtrate :s evaporated to dryness : .and dried to col)stant weight at 1 8.0""/:SC. This m<)lhod IS compl1ant with NEP¥ (1999) Schedule B(3) (Appdx. 2)
APHA 21st ed .. 2320 B This procedure determines alkalinity by automated measurement (e.g. PC Titrate) using ' pH 4.5 for indicating the total alkalinity end-point. This metnoct ts compliant with NEPM (1999) Schedule B(3) .. _\Appdx .. 2) .. . ... . . .. .. . . ... . . .. . , APHA 21st ed., 2310 B ACidl\Y is determ:ned by titra\lon with a standardiSed alkali to an end-potnt ph of $.3. ThiS , [llet);?_d)�-C�fnplia0t.�t�_N.J::f>".'! {19.�9)..Sch�dl;llf0. i?.\.3) .\1\PP.?:<·_ 2). i APHA21st ed., 4500-S04 Sulfate l(lns are C<lnvertecl to a barium sulfate suspens1on in an ace\!c acid med1um
w1\h barium chloride. light absorbance of the Ba$04 suspension is measured by a photometer and the $04-2 concentration is determined by comparison of the reading With a standard curve_ This method is compliant Wllh
.. L,_N �1;'10 ... \1.�?9L�<:�ed.�Je.f?;£3)_{jl,pp�:<.:.2) ..... -_...... ....... . ........ . ..... .... - .............. - ..... .... ... - .. . .. � APHA 21st ed., 4500 C!- G. The thtocyanate tOn is liberated from mercunc th10cyanate through sequestration ol i mercury by the chloride ion to iorm non·ionisect nwrcuric chloride.in the presence of ferne 1ons the libra ted ' thiocynate forms highly-coloured ferric thiocynate which is measured at 480 nm APHA 21st edition seal method 2
.... _·: CI.17:.1.:L.�p�1.20,{}3 """"""""'""'"'""""'""'" _,_ .. ....... - "·-·--....... ----................ - ......... ""' ......... ' ""' ....... '"'"'" '"'" """ """ "' '" "
WATER , (APHA 21st ed., 3125', USEPA SW846 - 6020, ALS QWI-ENJEG020): Sa:T.ples are 0.45 um filtered pr10r to ana!yS.1s. The ICPMS technique utilizes a highly eff1cient argon plasma to ionize selected elements. lo11s are then passed into a high vacuum mass spectrometer, Which separates tne analytes based on their distinct mass to
WATER
WATER
WATER
WAT.ER
WATER
WATER
�h<l[S.e,rati(l.S P.r.l?rYU��i.r_f!l_e<lsu.r_�.m.,,nt ,'Dy_ <�-�-i�.<;�et�.?Yr\,O_de_,ior� .. �etecto.�. .. ..... ..... ..... ... ... ·- .. , AS 3550. APHA21st ed. 3112 Hg - B (Flow-inJection (SnC\2)(Cold Vapour geflera\lon) AAS) Samples are 0.45 um filtered prior to analysis. FIM-AAS is an automated flameless atom1c absorption tecflnique. A bromate/bromide
' reagent is used to oxidise any organic mercury compounds in the filtered sample. The ion1c mercury IS reduced : online to atomic mercury vapour by SnCI2 which is then purged into a heated quartz celL Quantification is by ' compar'1ng absorbance against a calibration curve. Th1s method IS compliant with NEPM (199g) Sciledute 6(3) , {Appdx. 2) .... .... ..... .... .... .. .... ... .. . .. .. .. ... .. ... .. ·- . · APHA 21st ed., 450Q.-NH3 G Ammonia IS determined 'r:rj direct colorimetry by Discrete Analyser. This method is
...... co.rnpti�!lt..'J>i_�h.�N!�O_f'?.¥ .. �1-�?9L�S::t:�OlJJ�.§Q.l_ .. (Appdx.:..f) .............. � - ...... ....... .. .. .... .. .. .... ... . , APHA 21st ed .. 4500-NOZ- B. Nitrite is determined by direct co\ounmetry by Dtscrete Analyser. This method is
.compliant wrth. NEP.M (199.9) .S:chectule. B{_3) .(Appdx . . �l APHA 21st ed .. 4500-NO:.O- F. Nitrate IS reduced to nitrite by way of a cadmium reduCtiOn column followed by
' quantification by Discrete Analyser. Nitrite is determined seperately by direct colounmetry and result for Nitrate 1 calculated as the difference between the two results. This method is compliant w\th NEPM {1999) Schedule 8(3) : (Appdx. 2). ·- .... ... . .. . . . .. .. .. ... . . .. . ... .. .. .. .. . . ... .. .... ... .. : APHA 21st eel., 45DO-N03- F. Comtmed oxidised Nitrogen (N02+N03) is determined by Cadmium Reduction and
. _!, .dir.ec:t,c.ol�uri.l!lelrY..bY..Pis_cre.t<;J.h!1al�.e�._ .. T�.i_:> .. rll�\.h?� .. is. -�crr;pli,aD�V{i.th .t'/.EP.":l. _\ 1.?9?) ... �.c.he.�.ul.e ... B.@ \App�.x._.2) . APHA 21st ed., 4500-Norg D. 25ml water samples are d1gested using a traditional Kjeldaht digestion followed by ·. determination by .Discrete. Ana!ysl'!r, .. This me.thod is .compliant with NEPM .(1�99).Schedule 6(3). (Appdx. 2)
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7 ol8 EP1101327 Ame'tdmen\ 1
ACE ENVIRONMENTAL PTY L TO
J01C.039
Phosphorus as P By Discrete --Analyser
EKC67G WATER APHA 21st ed., 4500-P B&F ·n.;;s--prOcedure involves sulphuric acid digestion of a 100ml sample to break
; phosphorus down to orthophosphate. The orthophosphate reacts with ammoruum molybdate and ant1mony ' potassium tartrate to form a complex which is then reduced and its concentrat10n measured at 880nm usmg ... SJ.i��!�.t�_fy:�!y_��-: · .. I���-m�i�2�.!-� .... �?!0e!i_S:0� ... ��h���!:�J].�?91..?.�-�-�9.�.1� __ !3_\0l. (�Pp_t!x ••. . '.!..�········· ......... .
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2)
Schedule
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8 of8
EP1 1 C1327 Amendment 1
ACE ENVIRONMENTAL PTY lTD
JCi0-039
Summary of Out!iers
Outiiers : Quality Control Samples
1'1··u lol:ow,n<) 1�po11 l'lgtll'911ts -�utl:ers ti'19JO..:< !1 \i'k a�u!:ty Contcoi :OCj Rl.'po�'- Surro�n:e r<!Co""''l i1mns "'"' �,t;t,-� 2>1'\d ;:>a sod on USfPA S'fi8413 or ·"'L.S-Q'iVI!ECJ/3S (rn :n� c:t!s"'''�"' ct s��;;;,(lc USEPA � rc-.t�r T•,,s
Fti!)01\ (li>'J)ia�� OC C\l�h"s (biC::ilC��s.', or,Jy
D(iplfcates, Method Blanks, Labomto1y Control Samples and Matrix Spikes
Oe<ermmed MS recovery not detcrminm;J, background lov!ll greatllr than or <X;ual to 4:<: spike
"-•- ,_,,,,,,,..,,,,,,.,_,,_ ..... �.-· '""'' , , ,�, .. ..__,_, .. ,,.,, ,., -· '"""""'"'" ,, ,,, .. ... ......... ,_,.,.,,,, __ .. ................. "''"'"'"'-�'""""' �-.. -� .. --- " , . .................... ,,,� ................. '" , """' .......... "" '"""' , , ... __ .... _l?�.0��-, "''�·-- ,
0 For a!J matrices, no Method Blank vaJue- outliers occur,
s Fer aU matrices, no Duplicate o-utliers occur,
G For all matrices, no Laboratory Control outHers occur.
Regular Sample Surrogates
o For all regular sample matrices, no surrogate recovery ouWers occur.
OuWers : Anafysis HoJding Time CompJiance
Tr:;$ rqJ():1 1iWb·n Ho:dng T"'"' Ql'ec'>CG�·s <;dy Cnl·; 1hu n,sp()Ct•V\1 e.xU&ctron I PrupC<IG.(IO:.r· il:1r;J:or •O,r\�lys.s car:-·-�cMm i:<tu.nJ i:li�piC>ye�.
Mi\ti'Ot: WATER
Outliers : Frequency of Quality Control Samples
Tn,,• tolk:.-w1ng <'.Opon h>;f:i.gnts �omad:eC' :n (h" Fwqu�ncy of OuGil\; Contn;t S�mpl;;l'.
o No Quallty Control Sample Frequancy Outliers c;:o;lst.
.,,,-., "'' ;J,p, ·l>' .. li,'<c'(/ :;"•- '<-n :,,•p.-! Day.<
08-MAR.-;<011 04·MAR-20i 1 '
A C.;:r•!--'-"·' tbi!>t•,; (,,'""'"' C'c"C'P.ii\y
APPENDIX J