aspects of intrinsic josephson...
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Microelectronics and Nanoscience, Chalmers University of Technology and Göteborg UniversityS-412 96 Göteborg, Sweden, e-mail: [email protected]
GOTHENBURG UNIVERSITY
Aspects ofIntrinsic Josephson Tunneling
Aspects ofIntrinsic Josephson Tunneling
D. Winkler,1,2 A. Yurgens,1 V.M. Krasnov,1 Y.S. Sudershan,1 T.Claeson,1 E. J. Tarte,3 M.G. Blamire3
• Chalmers University of Technology and Göteborg UniversityDepartment of Microelectronics and Nanoscience,SE-412 96 Göteborg, Sweden
2) Imego InstituteAschebergsg 46, Building 11, SE-411 33 Göteborg, Sweden
3) IRC in Superconductivity, University of CambridgeMadingley Rd, Cambridge, CB3 0HE, UK
Microelectronics and Nanoscience, Chalmers University of Technology and Göteborg UniversityS-412 96 Göteborg, Sweden, e-mail: [email protected]
Microelectronics and Nanoscience, Chalmers University of Technology and Göteborg UniversityS-412 96 Göteborg, Sweden, e-mail: [email protected]
GOTHENBURG UNIVERSITY
Contents
• Background and the system• Ways of making small junctions• The experimental ”toolbox”• Recent work and some understanding• The pseudogap
vs. superconducting gap and T, H, HgBr2
• Interlayer coupling and pressure• Bi2212 films• Conclusions
Microelectronics and Nanoscience, Chalmers University of Technology and Göteborg UniversityS-412 96 Göteborg, Sweden, e-mail: [email protected]
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KLEINER AND MÜLLER
Microelectronics and Nanoscience, Chalmers University of Technology and Göteborg UniversityS-412 96 Göteborg, Sweden, e-mail: [email protected]
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INTRINSIC JOSEPHSON JUNCTIONS
q
Josephson effectintrinsic CuO
Ca
SrOBiOBiOSrOCuO
CuO
CuOCa
intrinsic junctions
I V
I
AB
Bi2212 single crystal 'large'
mesa
stacks
S
S
S
S'S'
S'
S'S'
a) b)
-300 -200 -100 0 100 200 300
VOLTAGE (mV)
CU
RR
ENT
(mA
)
4
6
2
0
-2
-4
-6
Microelectronics and Nanoscience, Chalmers University of Technology and Göteborg UniversityS-412 96 Göteborg, Sweden, e-mail: [email protected]
GOTHENBURG UNIVERSITYMESA STRUCTURES- using photolithography
height ~ 15 - 300 Å(in situ controlled)
Advantages:•specifiednumber ofjunctions•smallvolume•less defects•less heating
area ~ 200-600 µm^2
Ar ion etching orChemical etching (EDTA) Appl. Phys. Lett. 70, 1760 (1997)
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CROSS-BARPHOTOLITHOGRAPHY
photoresist
gold
CaF2
CaF2
CaF2
gold
photoresist
photoresistgold
Bi2212
Bi2212
Bi2212
FIB track
Microelectronics and Nanoscience, Chalmers University of Technology and Göteborg UniversityS-412 96 Göteborg, Sweden, e-mail: [email protected]
GOTHENBURG UNIVERSITYGOTHENBURG UNIVERSITY
FABRICATION OF MESAS OF Bi2212 INTRINSICJOSEPHSON JUNCTIONS USING A FOCUSSED ION BEAM
Microelectronics and Nanoscience, Chalmers University of Technology and Göteborg UniversityS-412 96 Göteborg, Sweden, e-mail: [email protected]
GOTHENBURG UNIVERSITYFABRICATION OF MESAS OF Bi2212 INTRINSIC JOSEPHSONJUNCTIONS USING A FOCUSSED ION BEAM
Microelectronics and Nanoscience, Chalmers University of Technology and Göteborg UniversityS-412 96 Göteborg, Sweden, e-mail: [email protected]
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The experimental ”toolbox”
! Charge transport, current-voltage! Temperature! Magnetic field! Pressure! Intercalation! Irradiation with heavy ions! Light and microwaves! Number of Cu-O planes
Microelectronics and Nanoscience, Chalmers University of Technology and Göteborg UniversityS-412 96 Göteborg, Sweden, e-mail: [email protected]
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RECENT WORK ON Bi2212 INTRINSIC JUNCTIONS
! Pseudogap in the c-axis tunneling! Interlayer coupling theory and intrinsic Josephson
effects! A pressure-induced increase of 2 – 3 times in Ic of both Bi2212
and Bi2201- single crystals in contrast to 2-6% increase of Tc
! Vortex dynamics related work! The c-axis magnetoresistance peak effect in Bi2212 determined
by the zero-field sub-gap current-voltage characteristics. 60-foldincrease at 6 T.
! Mapping the vortex magnetic phase diagram from I-V! The influence of 5 GeV Pb+ ion radiation was studied. Ic has a
peak at 1/3 of the matching field Bφφφφ
! Multiple valued critical current! Zero-voltage-state lifetime measurements! Critical current switching distribution! Phase-locking between junctions in a stack! Comparison to numerical simulations
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Microelectronics and Nanoscience, Chalmers University of Technology and Göteborg UniversityS-412 96 Göteborg, Sweden, e-mail: [email protected]
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PSEUDOGAP versus theSUPERCONDUCTING GAP – two scenarios...
(From J.L. Tallon and J.W. Loram)
Microelectronics and Nanoscience, Chalmers University of Technology and Göteborg UniversityS-412 96 Göteborg, Sweden, e-mail: [email protected]
GOTHENBURG UNIVERSITYPSEUDOGAP
(Krasnov et al. PRL84, 5860 (2000))
Microelectronics and Nanoscience, Chalmers University of Technology and Göteborg UniversityS-412 96 Göteborg, Sweden, e-mail: [email protected]
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PSEUDOGAP
(Winkler et al., Supercond. Sci. Technol. 12, 1013-1015 (1999))
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Tord Claeson
about one week at 230-240 C
Jin-Ho Choy, Seong-Ju Hwang, and Nam-Gyu Park
J. Am. Chem. Soc. 119, 1624 (1997)
HgBr2 intercalation
less heating
Decrease ofthe c-axis
criticalcurrent
Microelectronics and Nanoscience, Chalmers University of Technology and Göteborg UniversityS-412 96 Göteborg, Sweden, e-mail: [email protected]
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PSEUDOGAP
(Krasnov et al. PRL84, 5860 (2000))
Microelectronics and Nanoscience, Chalmers University of Technology and Göteborg UniversityS-412 96 Göteborg, Sweden, e-mail: [email protected]
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Tord Claeson
-1.5
-1.0
-0.5
0.0
0.5
1.0
1.5
-1600 -800 0 800 1600
I(m
V)
V(mV)
(HgBr2) Bi-2212T = 4.2 K
-0.1
0
0.1
-300 -200 -100 0 100 200 300
I(m
A)
V(mV)
2
468
10
I (m
A)
The intercalation does not changethe quality of I-V's
10 intrinsic Josephson junctions
10 intrinsic Josephson junctions
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Tord Claeson
0
5
10
15
20
25
-300 -200 -100 0 100 200 3000
10
20
30
40
50
60
V/10 (mV)
4.2 K
38 K
50 K
92 K
174 K
dI/d
V (m
S)Tc = 66 K
dI/d
V (p
S)
0
5
10
15
20
25
30
-60 -40 -20 0 20 40 60
dI/d
V (m
S)
V (mV)
dI/dV(kΩ-1) = 1.068e-3 V(mV) 2.5 + 0.426
3% of data presented
0 50 100 150 200 250 300
RES
ISTA
NC
ETEMPERATURE (K)
Tc = 66K
Microelectronics and Nanoscience, Chalmers University of Technology and Göteborg UniversityS-412 96 Göteborg, Sweden, e-mail: [email protected]
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Tord Claeson
0
5
10
15
20
25
-50 0 50 100 150 200
dI/d
V (m
S)
V(mV)
Tc = 66 K29 K
50 K
56 K
65 K81 K
0
1
2
3
-200 0 200 400 600 800 1000 1200
0 50 100 150
dI/d
V (m
S)
V(mV)
110 K78 K
66 K
60 K
50 KTc = 65-68 K
0
0.2
0.4
0.6
0.8
1
1.2
0 10 20 30 40 50 60 70 80
∆(Τ)
/∆(4
.2)
∆(Τ)
/∆(4
.2)
∆(Τ)
/∆(4
.2)
∆(Τ)
/∆(4
.2)
TEMPERATURE (K)
HgBr2-Bi2212;
∆(4.2) = 31 meV
pristine Bi2212;∆
1(4,2) = 12.5 meV
∆2(4,2) = 18.5 meV
BCS
Superconducting &pseudogap structures
Two intercalated samples
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Magnetic field dependence H || I || c for Bi2212
-0.6 -0.4 -0.2 0.0 0.2 0.4 0.60
10
20
30
40Bi2212 (S875b) H=0T H=14T
T=80K
T=72K
T=60K
T=40K
V (Volt)
dI/d
V (m
S)
Superconducting gap
and
pseudogap
(Krasnov et al. cond-mat/0006479, 29 June 2000)
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Intercalated HgBr2- Bi2212 mesa at 4.2 K
0.2 0.4 0.6 0.80
2
4
6
8
10
HgBr2-Bi2212
H=0TH=2TH=4TH=6TH=10TH=14T
dI/d
V (m
S)
V (Volt)
640
660 a)
T=4.2KV s (m
V)
H (T)
0 2 4 6 8 10 12 140
10
20
30
40
b)
I=0
σ(H
)- σ(0
) (µS
)
H (T)
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H || I || c – pure Bi2212
0.1 0.2 0.3 0.4 0.5 0.6
5
10
H=0TH=1TH=2TH=4TH=7TH=10TH=12TH=14T
a) T =72K S875b
dI/d
V (m
S)
0.1 0.2 0.3 0.4 0.5 0.6
5
10H=0TH=1TH=2TH=4TH=6TH=10TH=14T
b) T =80K Bi2212
dI/d
V (m
S)V (Volt)
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INTERLAYER COUPLING AND PRESSURE
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PENETRATION DEPTH
cc Js
c2
0
8πλ Φ=
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PRESSURE
1-
1-
GPa%6.0
GPa%2.0
=
==
cc
bb
aa
δ
δδ
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HIGH PRESSURE CELL
Opt i on #1 #2 #3Pr e s s ur e r a nge , GPa 1. 0 2. 0 3. 0Out e r di a me t e r , mm 30 40 60I nne r di a me t e r , mm 8 6 6Wor ki ng vol ume a tma x pr e s s ur e , c c m
1 0. 35 0. 35
We i ght , k g 1. 0 1. 7 2. 7
I ns t i t ut e f or Hi gh Pr e s s ur e Phys i c s Te l . ( 7- 095) 3340582142092 TROI TSK Mos c ow Re g. RUSSI A Fa x. ( 7- 095) 3340012
10/25/00 27Microelectronics and Nanoscience, Chalmers University of Technology and Göteborg UniversityS-412 96 Göteborg, Sweden, e-mail: [email protected]
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Tord Claeson
-12
-8
-4
0
4
8
12CU
RREN
T (m
A)
VOLTAGE
T = 30 K
50 mV
P = 0
P = 0.8 GPa
(a)
-0.3
-0.2
-0.1
0.0
0.1
0.2
0.3
VOLTAGE
2 mV
0.85 GPa
0.04 GPa
T = 4.2 K
(b)
No change in shape of I-V´s
Bi-2201Bi-2212
TWO OR ONE PLANE
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INTERLAYER COUPLING AND PRESSURE
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PRESSURE EFFECTS
0.0
0.1
0.2
4 5 6 7 8
0.04 GPa
0.85 GPa
-1
0
1
2
3
4
5
0 0.2 0.4 0.6 0.8 1
(1-T
c/Tc0
) (%
)
PRESSURE (GPa)
Bi-2201
Bi-2212
(b)
0
1
2
3
4
5
6
7
8
0 20 40 60 80
Ic (m
A)
TEMPERATURE (K)
0.80.60.40.10.0
P(GPa)
The pressure affects the c-axis transport but not the superconducting transition
Bi-2201Bi-2212
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INTERLAYERCOUPLING
ANDPRESSURE
Bi2212
Ic goes up with pressure,but Tc remains about thesame
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CONCLUSIONS
! Fabrication – several methods
! Pseudogap and the superconducting gap seem tocoexist – T, H, HgBr2, pressure,...
! No evidence for the interlayer coupling theory forHTS from experiments on Bi2212 and Bi2201
! Intrinsic Josephson effect and vortex matter
! Multiple valued critical current
Microelectronics and Nanoscience, Chalmers University of Technology and Göteborg UniversityS-412 96 Göteborg, Sweden, e-mail: [email protected]
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REFERENCES AND FURTHER READING
• Yurgens, ”Intrinsic Josephson Junctions - Recent Developments” Supercond. Sci. Technol. 13, R85-100 (2000).
• D. Winkler, Niklas Mros, August Yurgens, and Vladimir M. Krasnov, Edward J. Tarte, David T. Foord,Wilfred E. Booij, and Mark G. Blamire “Intrinsic Josephson effects in submicrometer Bi2212 mesasfabricated by using focussed ion beam etching”, Supercond. Sci. and Technol. 12, 1013-1015 (1999).
• A. Yurgens, D. Winkler, T. Claeson, T. Murayama, and Y. Ando, “Interlayer coupling andsuperconducting critical temperature of Bi2Sr1.5La0.5CuO6+δ and Bi2Sr2CaCu2O8+δ: Incommensurateeffects of pressure” scheduled for Phys. Rev. Lett. 82, 3148-3151(1999).
• V.M.Krasnov, A.Yurgens, D.Winkler, P.Delsing and T.Claeson, "Evidence for Coexistence of theSuperconducting Gap and the Pseudogap in Bi-2212 from Intrinsic Tunneling Spectroscopy”,Phys.Rev.Lett. 84, 5860 (2000)
• V.M.Krasnov, A.E.Kovalev, A.Yurgens, D.Winkler, "Discrimination between the superconducting gapand the pseudo-gap in Bi2212 from intrinsic tunneling spectroscopy in magnetic field" cond-mat/0006479 (subm. to PRL, title "Magnetic field dependence of the superconducting gap and thepseudogap in Bi2212 studied by intrinsic tunneling spectroscopy")
• http://fy.chalmers.se/~winkler/
• http://fy.chalmers.se/~yurgens/ijj.html
• http://fy.chalmers.se/~krasnov/