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LABORATORY SOFTWARE PROCESS AUTOMATION ATR-F Refractometer With ultrafast temperature regulation ATR-B

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Page 1: ATR-B ATR-F Refractometers_all... · Temperature measurement NTC sensor for measurement of sample temperature placed inside the prism Technical data Peltier-thermostat Temperature

LABORATORY

SOFT WARE

PROCESS

AUTOMATION

ATR-F RefractometerWith ultrafast temperature

regulation

ATR-B

Page 2: ATR-B ATR-F Refractometers_all... · Temperature measurement NTC sensor for measurement of sample temperature placed inside the prism Technical data Peltier-thermostat Temperature

SPECIFICATIONS ATR-B ATR-F

Measuring scalesRefractive Index (RI), Sucrose (%Brix) Standard scales included

Measuring range 1.29000 - 1.58000 RI / 100% Brix 1.32000 - 1.7000 RI / 100% Brix

Resolution 0.00001 RI / 0.01% Brix 0.00001 RI / 0.01% Brix

Precision ± 0,00002 RI / ± 0.02% Brix ± 0,00002 RI / ± 0.02% Brix

Reproducibility ± 0.00001 RI / ± 0.01% Brix ± 0.00001 RI / ± 0.01% Brix

Ambient temperature + 10° to + 40°C

Automatic temperature compensation + 5° to + 50°C + 5° to + 100°C

Temperature measurement NTC sensor for measurement of sample temperature placed inside the prism

Technical data Peltier-thermostat Temperature control prism / sample by build-in solid state Peltier-thermostat

Temperature rangeResolution

PrecisionReproducibility

+ 5°C / + 80°C0,01°C± 0.03°C± 0.02°C

+ 5°C / + 100°C

Measurement mode Single sample or flow through measurement

Prism Sapphire YAG

Light source / wavelength LED, interference filter 589 nm

Display L-Display (7” Touchscreen, 800 x 480 Pixel, 16 Bit colors)

Operation Touchscreen, keyboard**, mouse**, barcode reader**, remote via PC**

Interfaces1 x RS232 C serial, 3 x USB (A), 1 x USB (B), 1 x Ethernet, Easy connection of keyboard, mouse, printer, barcode reader, PC and network

Conformity International Pharmacopoea, ASTM, AOAC, DIN, FDA, ICUMSA and others

Highlights

Robust enclosure for rough environments; High performance and accuracy; Continuous measurement; ESH¹ chamber; MBS² as stand alone or with PC; Easy calibration; LED light source; Very low noise; GLP/GMP;Maintenance friendly by remote diagnostic; Intuitive user handling guided OP system; Installation wizard; Full traceability of records; Ext. LIMS integration; Huge storage for 1000 products each with 1000 methods; 21 CFR part 11 ready conformity³1 Easy sample handling; ² Modular build-in-system; ³ Optional software module for the L-Display

Weight / dimensionsMeasuring Head: 4.9 kg; 210 x 210 x 160 mm (width x depth x height)L-Display: 3.0 kg; 240 x 190 x 150 mm (width x depth x height)

Schmidt + Haensch GmbH & Co.Waldstraße 80-81, 13403 Berlin, GermanyTel: + 49 (0 30) 417072-0, Fax: + 49 (0 30) [email protected], www.schmidt-haensch.com

* Standard conditions (589 nm, 20°C)** Optional

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ISO 9001: 2008

Refractometer applicationsThe applications of Refractometers are highly diverse.

Applications often used• Determination of refractive index• Determination of dry substance• Determination of mass percent• Brix measurement• Standard scales (Brix, Oechsle, Zeiss, Fat, Honey) with automatic temperature compensation• Qualitative analysis – identification of samples• Quantitative analysis of dissolved solids in water or other solvents

Typical applications of the models• Pharmaceutical (CFR 21)• Food, beverage• Cosmetic (e.g. shampoo, toothpaste, etc.)• Ketchup• Sweets• Marmelade• Chemical• Petrochemical

Page 3: ATR-B ATR-F Refractometers_all... · Temperature measurement NTC sensor for measurement of sample temperature placed inside the prism Technical data Peltier-thermostat Temperature

LABORATORY

SOFT WARE

PROCESS

AUTOMATION

ATR-F RefractometerWith ultrafast temperature

regulation

ATR-B

Page 4: ATR-B ATR-F Refractometers_all... · Temperature measurement NTC sensor for measurement of sample temperature placed inside the prism Technical data Peltier-thermostat Temperature

SPECIFICATIONS ATR-B ATR-F

Measuring scalesRefractive Index (RI), Sucrose (%Brix) Standard scales included

Measuring range 1.29000 - 1.58000 RI / 100% Brix 1.32000 - 1.7000 RI / 100% Brix

Resolution 0.00001 RI / 0.01% Brix 0.00001 RI / 0.01% Brix

Precision ± 0,00002 RI / ± 0.02% Brix ± 0,00002 RI / ± 0.02% Brix

Reproducibility ± 0.00001 RI / ± 0.01% Brix ± 0.00001 RI / ± 0.01% Brix

Ambient temperature + 10° to + 40°C

Automatic temperature compensation + 5° to + 50°C + 5° to + 100°C

Temperature measurement NTC sensor for measurement of sample temperature placed inside the prism

Technical data Peltier-thermostat Temperature control prism / sample by build-in solid state Peltier-thermostat

Temperature rangeResolution

PrecisionReproducibility

+ 5°C / + 80°C0,01°C± 0.03°C± 0.02°C

+ 5°C / + 100°C

Measurement mode Single sample or flow through measurement

Prism Sapphire YAG

Light source / wavelength LED, interference filter 589 nm

Display L-Display (7” Touchscreen, 800 x 480 Pixel, 16 Bit colors)

Operation Touchscreen, keyboard**, mouse**, barcode reader**, remote via PC**

Interfaces1 x RS232 C serial, 3 x USB (A), 1 x USB (B), 1 x Ethernet, Easy connection of keyboard, mouse, printer, barcode reader, PC and network

Conformity International Pharmacopoea, ASTM, AOAC, DIN, FDA, ICUMSA and others

Highlights

Robust enclosure for rough environments; High performance and accuracy; Continuous measurement; ESH¹ chamber; MBS² as stand alone or with PC; Easy calibration; LED light source; Very low noise; GLP/GMP;Maintenance friendly by remote diagnostic; Intuitive user handling guided OP system; Installation wizard; Full traceability of records; Ext. LIMS integration; Huge storage for 1000 products each with 1000 methods; 21 CFR part 11 ready conformity³1 Easy sample handling; ² Modular build-in-system; ³ Optional software module for the L-Display

Weight / dimensionsMeasuring Head: 4.9 kg; 210 x 210 x 160 mm (width x depth x height)L-Display: 3.0 kg; 240 x 190 x 150 mm (width x depth x height)

Schmidt + Haensch GmbH & Co.Waldstraße 80-81, 13403 Berlin, GermanyTel: + 49 (0 30) 417072-0, Fax: + 49 (0 30) [email protected], www.schmidt-haensch.com

* Standard conditions (589 nm, 20°C)** Optional

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ISO 9001: 2008

Refractometer applicationsThe applications of Refractometers are highly diverse.

Applications often used• Determination of refractive index• Determination of dry substance• Determination of mass percent• Brix measurement• Standard scales (Brix, Oechsle, Zeiss, Fat, Honey) with automatic temperature compensation• Qualitative analysis – identification of samples• Quantitative analysis of dissolved solids in water or other solvents

Typical applications of the models• Pharmaceutical (CFR 21)• Food, beverage• Cosmetic (e.g. shampoo, toothpaste, etc.)• Ketchup• Sweets• Marmelade• Chemical• Petrochemical

Page 5: ATR-B ATR-F Refractometers_all... · Temperature measurement NTC sensor for measurement of sample temperature placed inside the prism Technical data Peltier-thermostat Temperature

LABORATORY

SOFTWARE

PROCESS

AUTOMATION

ATR-P Refractometer

Page 6: ATR-B ATR-F Refractometers_all... · Temperature measurement NTC sensor for measurement of sample temperature placed inside the prism Technical data Peltier-thermostat Temperature

SPECIFICATIONS ATR-P

Measuring scalesRefractive Index (RI), Sucrose (%Brix) Up to 1000 scales freely definable

Measuring range 1.33200 - 1.54000 RI / 100% Brix

Resolution 0.00001 RI / 0.01% Brix

Precision ± 0,00002 RI / ± 0.02% Brix

Reproducibility ± 0.00001 RI / ± 0.01% Brix

Ambient temperature + 10° to + 40°C

Automatic temperature compensation + 5° to + 50°C

Temperature measurement NTC sensor for measurement of sample temperature placed inside the prism

Temperature controlTemperature range

Temperature control prism / sample by external water bath5°C / 50°C

Measurement mode Single sample or flow through measurement / horizontal or vertical usage

Prism Sapphire

Light source / wavelength LED, interference filter 589 nm

Display 7" Touchscreen, 800 x 480 Pixel, 16 Bit colors

Operation Touchscreen, keyboard**, mouse**, barcode reader**, remote via PC**

Interfaces1 x RS232 C serial, 3 x USB (A), 1 x USB (B), 1 x Ethernet, Easy connection of keyboard, mouse, printer, barcode reader, PC and network

Conformity International Pharmacopoea, ASTM, AOAC, DIN, FDA, ICUMSA and others

Highlights

Robust stainless steel measuring head for rough enviroments; High performance and accuracy; Continuous measurement; ESH¹ chamber; MBS² as stand alone with L-Display or polarimeter; Easy calibration; GLP/GMP; With the L-Display: Maintenance friendly by remote diagnostic; Intuitive user handling guided OP system; Installation wizard; Full traceability of records; Ext. LIMS integration; Huge storage for 1000 products each with 1000 methods; 21 CFR part 11 ready conformity³1 Easy sample handling; ² Modular build-in-system; 3 Optional software module for the L-Display

Weight / dimensionsMeasuring Head: 4.5 kg; 200 x 160 x 135 mm (width x depth x height)L-Display: 3.0 kg; 240 x 190 x 150 mm (width x depth x height)

Schmidt + Haensch GmbH & Co.Waldstraße 80-81, 13403 Berlin, GermanyTel: + 49 (0 30) 417072-0, Fax: + 49 (0 30) [email protected], www.schmidt-haensch.com

* Standard conditions (589 nm, 20°C)** Optional

Refractometer applicationsThe applications of Refractometers are highly diverse.

Applications often used•Determination of refractive index•Determination of dry substance•Determination of mass percent• Brix measurement• Standard scale (Brix)•with automatic temperature compensation•Qualitative analysis – identification of samples•Quantitative analysis of dissolved solids in water or other solvents•Quantitative analysis of sugars, solves, glycol, oechsle…

Typical applications of the model• Sugar industry (main application)• Beverages (juices with pulp)• Samples with suspended particles• Food (oil from palm, corn, sunflower, soya)

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ISO 9001: 2008

Page 7: ATR-B ATR-F Refractometers_all... · Temperature measurement NTC sensor for measurement of sample temperature placed inside the prism Technical data Peltier-thermostat Temperature

LABORATORY

SOFTWARE

PROCESS

AUTOMATION

ATR-C Refractometer

Page 8: ATR-B ATR-F Refractometers_all... · Temperature measurement NTC sensor for measurement of sample temperature placed inside the prism Technical data Peltier-thermostat Temperature

SPECIFICATIONS ATR-C

Measuring scalesRefractive Index (RI), Sucrose (%Brix) 10 standard scales can be reloaded via PC: Inverted Sugar (%), Fructose (%), Glucose (%), Honey (% water), Phenol (%), Acetic Acid (%), Oechsle (°Oe), Propylene Glycol (%), Zeiss, H2O2 (%)

Measuring range 1.3200 - 1.5800 RI / 100% Brix

Resolution 0.0001 RI / 0.05% Brix

Precision ± 0,0001 RI / ± 0.05% Brix

Reproducibility ± 0.0001 RI / ± 0.05% Brix

Ambient temperature + 10° to + 40°C

Automatic temperature compensation + 5° to + 50°C

Temperature measurement NTC sensor for measurement of sample temperature placed inside the prism

Temperature controlTemperature range¹

Standard version without Peltier-thermostat / Optional with integrated Peltier-thermostat¹20°C / 25°C

Measurement mode Single sample

Prism YAG

Light source / wavelength LED, interference filter 589 nm

Display Two lines

Operation Continous measurement, start-up, configuration, calibration via external PC

Interfaces 1 x RS232, 1 x USB (B)

Standard modelsATR-C 100: without sample temperature maintaining ATR-C 110: with Peltier driven temperature control

Conformity International Pharmacopoea, ASTM, AOAC, DIN, FDA, ICUMSA and others

Highlights

Robust enclosure for rough enviroments; High performance and accuracy; Continuous measurement; ESH¹ chamber; MBS² as stand alone or with PC; Easy calibration; GLP/GMP; 21 CFR part 11 ready³; LED light source; Very low noise; Maintenance friendly by remote diagnostic; TFT touchscreen; Intuitive user handling guided OP system; Installation wizzard; Full traceability of records; Ext. LIMS integration; Huge storage for 1000 products each with 1000 methods1 Easy sample handling; ² Modular build-in-system; ³ Optional software module

Schmidt + Haensch GmbH & Co.Waldstraße 80-81, 13403 Berlin, GermanyTel: + 49 (0 30) 417072-0, Fax: + 49 (0 30) [email protected], www.schmidt-haensch.com

* Standard conditions (589 nm, 20°C)** Optional

Refractometer applicationsThe applications of Refractometers are highly diverse.

Applications often usedDetermination of refractive indexDetermination of dry substanceDetermination of mass percentBrix measurementStandard scales (Brix, Oechsle, Zeiss, Fat, Honey)

with automatic temperature compensationQualitative analysis – identification of samplesQuantitative analysis of dissolved solids in water or other solvents

Typical applications of the modelStandard measurement of known solutionsFood and beverageDairy products (e.g. flavoured yoghurt, ice cream, etc.)Fruit juiceJam, marmaladeCocoaAnd many more

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ISO 9001: 2008

Page 9: ATR-B ATR-F Refractometers_all... · Temperature measurement NTC sensor for measurement of sample temperature placed inside the prism Technical data Peltier-thermostat Temperature
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Page 11: ATR-B ATR-F Refractometers_all... · Temperature measurement NTC sensor for measurement of sample temperature placed inside the prism Technical data Peltier-thermostat Temperature
Page 12: ATR-B ATR-F Refractometers_all... · Temperature measurement NTC sensor for measurement of sample temperature placed inside the prism Technical data Peltier-thermostat Temperature
Page 13: ATR-B ATR-F Refractometers_all... · Temperature measurement NTC sensor for measurement of sample temperature placed inside the prism Technical data Peltier-thermostat Temperature

ATR-Series

SCHMIDT + HAENSCHOpto-electronic measuring device since 1864

Page 14: ATR-B ATR-F Refractometers_all... · Temperature measurement NTC sensor for measurement of sample temperature placed inside the prism Technical data Peltier-thermostat Temperature

ATR-Controllerinnovation

Laboratory Refractometer ATR-Series

Modular concept of the new ATR Refractometer series is just one of the innovative features, allowing the selection of instruments according to the customers needs. Depending on the application the measuring head can be integrated in the controller (ATR ST) or is housed in a sepa-rate stainless steel water proofed body (ATR SW/W1/W2). Additional advantage is the intuitive, user friendly operation.Same menu structure of the software allows easy compre-hension of all Refractometer models.Unique software features of the instrument software per-form important statistical evaluation of results, individual programming of method’s and selection of predefined scales with speed and ease.

Incorporating the GLP requirements, the software meetsthe particular needs of laboratories in chemical and phar-maceutical industries.

Built-in temperature control features of the ATR SW andATR W1/W2 refractometer ensures correct measurements even in case of external temperature variation.The separate stainless steel housing is extremely robust, chemically resistant against most aggressive media and external temperature variation. It is water resistant andair-tight (ATR SW).

For more than 140 years SCHMIDT+HAENSCH is committed to high performance and exceptional quality.A unique new development is the DSR-λ, a multiple wave-length Refractometer for the automatic dispersion meas-urement and measuring the ABBE number simultaneously. Please, ask for special leaflet DSR-λ.

Page 15: ATR-B ATR-F Refractometers_all... · Temperature measurement NTC sensor for measurement of sample temperature placed inside the prism Technical data Peltier-thermostat Temperature

+

+

Refractometer ATR- ST / ST plus / ST S plus Automatic critical angle Refractometer in a single box design.The spacious sample room allows the measurement of fluidor solid substances. For aggressive samples or samples witha low density we recommend the PTFE insert (see picture). The shown Brix result is temperature corrected.The measuring prism is aligned with the sample room for easy cleaning and application of solid samples.

Example for application: A soft drink company wants tomeasure the Brix concentration in syrups or its final product.A Refractometer with a precision of ± 0.05 Brix is needed. The budget is limited. Advantages: The customer gets a very compact designed instrument with an exceptional price performance ratio. The user participates in the high level of quality and easy operation of SCHMIDT+HAENSCH instruments. Alternative: In case a higher precision or extended meas-uring range is needed choice of models like the ATR ST plus or ATR ST S plus.

Refractometer ATR SW / ATR SW plusAutomatic critical angle Refractometer with a very high pre-cision and a separated measuring head for liquid samples. For individual measurement or continuous measurement different sample chambers are available. The measuring head can be turned around to be used in continuous or single measurement mode.

Example for application: A company processing citrus fruits and wants to control the production by taking samplesregularly. A Refractometer is needed for the fast measure-ment of similar samples with a high precision of<± 0.02 Brix. Advantages: The ATR SW is an instrument which allows a very high throughput of samples with high precision. The sample room is designed to flush out the previous sample completely. No intermediate cleaning of the prism is needed. The programming of up to 10 scales allows the direct read out of concentrations of different products.In addition a separate thermostat can be attached.The high thermal mass of the sample room will lead to a fast temperature adaptation of the sample. Alternative: In case a higher precision or extended meas-uring range is needed choice of models like the ATR SW plus.

Refractometer ATR- W1 / W2 / W1 plus / W2 plusAutomatic critical angle Refractometer with a very highprecision, separate measuring head for liquid and solid media with integrated Peltier thermostatisation.

Example of application: The test lab wants to analyse the constituents of cosmetics. The temperature needed must be exactly 70°C because the substance will become solid below 65°C. No additional thermostat is needed.The customer wants to be sure that the temperature of the sample remains stable within a very small variation (0,01°C). The determination of the melting point is addi-tional information by automatically running a temperature ramp.Advantages: The ATR W1 / W2 is a Refractometer of high-est precision with Peltier driven temperature control in the range of 10°C to 80°C over the whole ABBE range (only W2).Also 10 individual scales can be programmed. Alternative: If a higher precision needed our modularconcept of instruments offers the plus models.

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Refractometer applications

The application of Refractometers is very versatile. Application often used:

• Determination of refractive index• Determination of dry substance• Determination of mass percent• Brix measurement• Standard scales (Oechsle, Zeiss, Fat, Honey) are implemented• Standard methods according to ASTM 1218, 1747 and others• Qualitative analysis - identification of samples• Quantitative analysis of dissolved solids in water or other solvents• Quantitative analysis of sugars, solves, glycol, fat, oechsle...

Refractometrie is used in:

• Food industry• Medicine / pharmaceutical industry• Cosmetic industry• Chemical- and petrochemical industry

For monitoring liquids in production with inline Refractometer please see our leaflet on Process Refractometer iPR.

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SCHMIDT+HAENSCH GmbH & Co.Waldstraße 80/81D-13403 BerlinGermanyPhone: +49 30 / 41 70 72-0Fax: +49 30 / 41 70 72-99e-mail: [email protected]

Refractometer SCHMIDT+HAENSCH

SCHMIDT + HAENSCHOpto-electronic measuring device since 1864

ST

1.3320-1.5320 RI0 - 95 Brix

0.0001 RI0.05 Brix

±0.0001 RI±0.05 Brix

+5 to +50°C

no

no

ST plus

1.3300-1.5500 RI0 - 100 Brix

0.00002 RI0.02 Brix

±0.00005 nRI±0.03 Brix

+5 to +50°C

no

no

SW

1.3320-1.5320 RI0 - 95 Brix

0.00002 RI0.02 Brix

±0.00004 RI±0.04 Brix

+5 to +50°C

external watercirculator (opt.)

Flow through compartmentdoor (opt.)

SW plus

1.3000-1.5500 RI0 - 100 Brix

0.00001 RI0.01 Brix

±0.00002 RI±0.02 Brix

+5 to +50°C

external watercirculator (opt.)

Flow through compartmentdoor (opt.)

W1/W2

1.3320-1.5320 RI0 - 95 Brix (W1)

1.3320-1.7000 RI0 - 95 Brix (W2)

0.00002 RI0.02 Brix

±0.00004 RI±0.04 Brix

+10 to +80°C

internal Peltierthermostat

no

W1 plus/W2 plus

1.3320-1.5320 RI0 - 95 Brix (W1+)

1.3320-1.7000 RI0 - 100 Brix (W2+)

0.00001 RI0.01 Brix

±0.00002 RI±0.02 Brix

+10 to +80°C

internal Peltierthermostat

no

ST S plus

1.2800-1.5500 RI0 - 100 Brix

0.00001 RI0.01 Brix

±0.00003 RI±0.02 Brix

+5 to +50°C

no

no

Model: ATR-

Measuring range

Resolution

Precision

Workingtemperature

Thermostatisat.of sample

Flow throughmeasurement

Page 17: ATR-B ATR-F Refractometers_all... · Temperature measurement NTC sensor for measurement of sample temperature placed inside the prism Technical data Peltier-thermostat Temperature

LABORATORY

SOFTWARE

PROCESS

AUTOMATION

ATR-LRefractometerSpectral-Refractometer for automatic dispersion measurement

Page 18: ATR-B ATR-F Refractometers_all... · Temperature measurement NTC sensor for measurement of sample temperature placed inside the prism Technical data Peltier-thermostat Temperature

SPECIFICATIONS ATR-L

Measuring scales Refractive index (RI)

Measuring range 1.33200 - 1.70000 RI* / 100% Brix

Resolution 0.00001 RI* / 0.01 Brix

Precision ± 0.00004 RI* / ± 0.03 Brix

Reproducibility ± 0.00004 RI* / ± 0.03 Brix

Measuring time per sample 20 sec for all 7 wavelength after temperature stabilisation; single sample measurement

Ambient temperature + 15° to + 40°C

Automatic temperature compensationOperational temperatureTemperature stabilityTemperature precision

Solid state Peltier-thermostatisation+ 10°C to + 80°C0.01°C± 0.03°C

Detector CCD-linear array with 2048 elements

Sample compartment Used materials: stainless steel, Black Delrin®, Teflon®, Viton®, FFKM sealing

Prism YAG

Light source / Wavelength7 discrete LED's with fixed wavelengths 400, 450, 490, 525, 590, 660, 700 nm (others on request), wavelength accuracy ± 2 nm

Display LCD, 16 x 16 characters, back illuminated

Operation 20 key membrane including function keys

Interfaces /Communication 1 x RS232 C, 1x parallel, USB optional

Standards European and international Pharmacopoeia, various ASTM, ISO and DIN standards

Dimensions / Weight Mesuring head, stainless steel: 260 x 190 x 220 mm (w x h x d); control unit: 220 x 110 x 290 mm (w x h x d); complete unit 8 kg

HighlightsAutomatic dispersion measurement at 7 wavelengths over the full range of visibile light (intermediate values interpo-lated)**; Powerful, internal Peltier temperature control guarantees the fastest measurements with highest accuracy

Schmidt + Haensch GmbH & Co.Waldstraße 80-81, 13403 Berlin, GermanyPhone: + 49 (0 30) 417072-0, Fax: + 49 (0 30) [email protected], www.schmidt-haensch.com

* Standard conditions (589 nm, 20°C)** Automatic Abbé number measurement

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ISO 9001: 2008

Refractometer applicationsThe applications of Refractometers are highly diverse for fast and non-destructive determination of refractive index.

Applications often used•Determination of product purity•Quality control• Product fingerprinting•Optical material characterization

Typical applications of the model•Measurement of dispersion and calculation of Abbé number•Measurement of lenses made of plastic or glass•Quality control of hydrophobic and hydrophilic intraocular lenses (IOL)• Standard test method for refractive index and refractive index dispersion determination of hydrocarbon liquids accord. to ASTM 1218• Testing of fiber-optic components•Material engineering of polymer compounds