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    Bars classification Anode load

    WEEK 36

    El Salvador

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    P roject Pu rpose

    Set the bars to be u se as tooling andanode dimensions.

    Detect bars in poor condition and get themou t of prod u ction.

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    P owder MixingPu rpose

    To prepare the tantal u m powder to beprocessed

    To increase the flow of tantal u m powder Check the Mechanical properties of thepowder

    ConditionsRelative h u midity: 40% - 55%Air extraction

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    O bservations

    Why The powder need a Binder?Beca u se this helps the flow of powder

    Aid to l u bricate the tooling

    The mixing process consist in add a Binder to the Virgin powder, thefirst mixing is done man u ally on a stainless steel pot.

    The binder u sed:

    1. Stearic acid ( Tantal u m powder)2. P EG (Niobi u m powder)3. PX (Niobi u m powder)4. PX + Syntamin ( Tantal u m powder)

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    Why we p u t the powder into a blender ?

    Beca u se The V-Blender providehomogeneity to the powder mixt u re.

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    Mesh: P articles Size distrib u tion inside thepowder.

    Scott Density: Determines the ability that hasthe powder to fill a cavity.

    Flow : Meas u re the velocity that has thepowder to flow by the action of the gravity .

    CRUSH STRENGHT: This test determines thebreakage force (kg-F).

    MIXING AQL

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    2. PRESS ING

    Pu rpose:

    To P ress the Tantal u m powder in to anode of defined

    shape u sing a HABERER press.Give a pressing density to the anode

    Conditions

    Temperat u re room: 20C to 25CRelative h u midity: 40% to 55%

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    Description

    P ressing P rocessMechanism poweredby an electric Motor.Tooling can give 3anodes per cycle.The Haberer gives 156

    anodes per min u te.

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    O BSERVATI O NSThe low press u re line indicates the zone where the anode

    is str u ctu rally weak.

    how we can decrease the effects of low

    pressu

    re line?It mu st be between (50% -75%) of the length of theanode.

    To minimize the effects of low-press u re line is necessary toens u re that the wire crossesthe line.

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    P ressing AQL

    Visu al test with a microscope: search s u rface defectsand wire damage.Anode weight ControlVerification of dimensions of anodes with Shadowgraph:Low press u re line u sing Ultraso u nd: Check the Locationof line.

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    WA SH DE- LUB E

    Pu rpose

    Remove the stearic acid.

    MachinesAUTO WASH DE-LUBE (M O RRIS AUT O MATIO N)

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    O BSERVATI O NS

    The process of WASH de -LUBE consist in sevenwashes.The water m u st be at 85C +/- 5C, the temperat u re aidsto dil u te the binder.

    Wash Sol u tion

    First and Second Ca u stic soda 32%Third and Fo u rth Des-ionized water Fifth Nitric acid 17%

    Sixth and Seventh Des-ionized water

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    O bservations

    Why is necessary to remove the binder?Beca u se the binder isn't a raw material, is an imp u rity tothe process.

    Why are the anodes treated with care after washing?Beca u se the anodes are extremely fragile after washing.

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    Drying ovenPu rpose

    Remove the moist u re of the anodes from WASH DE-LUBE

    Why is it important to remove moist u re from the anodes?

    Beca u se water has oxygen and it wo u ld be extremely

    dangero u s by temperat u res inside the sinter, co u ld bein flames.

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    Description

    This process bring to the anodes 120C of temperat u redu ring six and half ho u rs if we u se static oven and 3

    hou

    rs and 15 minu

    tes if weu

    se vacuu

    m oven.

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    The stearic acid has carbon in his internal composition,this is why it sho u ld make evidence of carbon to

    determine if the levels are in the range of permissible.This test shows u s the effectiveness of o u r wash.

    Drying oven AQL

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    S IN TER

    Pu rposesCreate a micro str u ctu re sponge inside the anode.

    P rovide a thin oxide s u rface to anodes to protect

    against the environment.

    Machinery req u iredLinear Sinter ( P yramid Engineer, Centorr)

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    O bservations

    Inside the sinter they a are transported by a metal bandmade of T u ngsten that enters the oven that hastemperat u res ranging between 1600C and 2100C.

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    Why the sinter need a vac uu m chamber?to remove all the oxygen from the anodes

    What is the f u nction of the Argon gas inside theLinear Sinter?create an inert atmosphere inside the f u rnace, and moveimp u rities before the sinter.

    P revent flames b u rn in the anodes by the high

    temperat u re.

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    Why is critical the temperatu

    re in the sintering?Beca u se a very high temperat u re shrink too the anodeand lose CV

    A low-temperat u re will give me Weak sinter- necks anddoes not hold high-voltage

    Why is important the passivation?

    Beca u se it provides a layer of oxide that protects theanodes of an u ncontrolled oxidation

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    SINTER AQL

    Review anode dimensions( for

    determinate the Sinter density)

    O xygen test for Sinter effectiveness.

    Wetscan to determine CV .

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    ANO DO S LO AD

    Pu rposesWeld anodes to a stainless steel strip.

    Machinery req u iredHIMECHAWALDENBURGER

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    O BSERVATI O NS

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    Anodos Load AQL

    To end the process of anode load, it is necessary to

    pass welding test, which consists of an anode bend 90degrees and ret u rn to its original position.

    Verification of height and spacing of anodes, this testis done by meas u ring the distance between anode andsteel strip, this test is vital for the following processes,since these meas u res depend on the proper handlingthe anode.