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Technical Report SL-96-15 September 1996 US Army Corps of Engineers Waterways Experiment Station Workability of Mass Concrete Report 2 Supplemental Proportioning Parameters by Billy D. Neeley, Michael K. Lloyd 19970113 104 Approved for Public Release; Distribution is Unlimited Prepared for Headquarters, U.S. Army Corps of Engineers DTIC QUALIYY II,,-S(,ECTED I

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Page 1: by Billy D. Neeley, Michael K. Lloyd · the Portland Cement Association (PCA), and the CE to assist the contractor in completing a successful placement: Aggregate gradings - "Mass

Technical Report SL-96-15September 1996

US Army Corpsof EngineersWaterways ExperimentStation

Workability of Mass Concrete

Report 2Supplemental Proportioning Parameters

by Billy D. Neeley, Michael K. Lloyd

19970113 104

Approved for Public Release; Distribution is Unlimited

Prepared for Headquarters, U.S. Army Corps of Engineers DTIC QUALIYY II,,-S(,ECTED I

Page 2: by Billy D. Neeley, Michael K. Lloyd · the Portland Cement Association (PCA), and the CE to assist the contractor in completing a successful placement: Aggregate gradings - "Mass

The contents of this report are not to be used for advertising,publication, or promotional purposes. Citation of trade namesdoes not constitute an official endorsement or approval of the useof such commercial products.

@ PRINTED ON RECYCLED PAPER

Page 3: by Billy D. Neeley, Michael K. Lloyd · the Portland Cement Association (PCA), and the CE to assist the contractor in completing a successful placement: Aggregate gradings - "Mass

Technical Report SL-96-15September 1996

Workability of Mass Concrete

Report 2Supplemental Proportioning Parameters

by Billy D. Neeley, Michael K. Lloyd

U.S. Army Corps of EngineersWaterways Experiment Station3909 Halls Ferry RoadVicksburg, MS 39180-6199

Report 2 of a SeriesApproved for public release; distribution is unlimited

Prepared for U.S. Army Corps of EngineersWashington, DC 20314-1000

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US Army Corpsof EngineersWaterways Experiment N

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Includes bibliographic references.Report 2 of a series.1. Concrete -- Evaluation. 2. Paste. 3. Mortar. 4. Concrete -- Additives.

I. Lloyd, Michael K. II. United States. Army. Corps of Engineers. Ill. U.S. ArmyEngineer Waterways Experiment Station. IV. Structures Laboratory (U.S. ArmyEngineer Waterways Experiment Station) V. Title. VI. Title: Supplementalproportioning parameters. VII. Series: Technical report (U.S. Army EngineerWaterways Experiment Station) ; SL-96-15 rept.2.TA7 W34 no.SL-96-1 5 rept.2

Page 5: by Billy D. Neeley, Michael K. Lloyd · the Portland Cement Association (PCA), and the CE to assist the contractor in completing a successful placement: Aggregate gradings - "Mass

Contents

Preface ............................................ v

1- Introduction ....................................... 1

Background ....................................... 1M ortar Content ..................................... 4Paste-M ortar Ratio .................................. 5Objectives ........................................ 6Scope . . . . . .... .. . . .. . . .. . .. . .. . .. .. . . .. . . . .. . .. . . 6

2--Concrete M ixtures ................................... 7

Review of Recent Mass Concrete Mixtures ................... 737.5-mm (1-1/2-in.) NMSA mixtures .................... 775-mm (3-in.) NMSA mixtures ........................ 9

Materials Used in Current Investigation ..................... 11Cem ent ........................................ 11Pozzolan ....................................... 12Aggregates ..................................... 12Adm ixtures ..................................... 12

M ixture Proportions .................................. 1637.5-mm (1-1/2-in.) NMSA mixtures .................... 1675-mm (3-in.) NMSA mixtures ........................ 17

Tests ............................................ 17

3-Discussion and Analysis ............................... 23

37.5-mm (1-1/2-in.) NMSA Mixtures ...................... 23Criteria ........................................ 23Favorable coarse aggregate particle shape .................. 23Less favorable coarse aggregate particle shape ............... 29

75-mm (3-in.) NMSA Mixtures .......................... 32

4-Conclusions and Recommendation ......................... 35

Conclusions ........................................ 35Recommendation ..................................... 36

References ........................................... 38

iii

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Appendix A: Recent Mass Concrete Mixture Information ........... Al

Appendix B: Modified Vebe Test Procedure for Mass Concrete

M ixtures .......................................... B 1

iv

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Preface

This report was prepared by the Structures Laboratory (SL), U.S. ArmyEngineer Waterways Experiment Station (WES), under the sponsorship ofHeadquarters, U.S. Army Corps of Engineers (HQUSACE), as a part of CivilWorks Investigation Studies Work Unit 32768, "Workability of Mass Concrete."

The study was conducted under the general supervision of Messrs. BryantMather, Director, SL, and John Q. Ehrgott, Assistant Director, SL. Directsupervision was provided by Dr. Paul F. Mlakar, Chief, Concrete and MaterialsDivision (CMD), and Mr. Edward F. O'Neil, Acting Chief, EngineeringMechanics Branch (EMB), CMD. Dr. Tony C. Liu, HQUSACE, was theTechnical Monitor. Mr. Billy D. Neeley, EMB, was the Principal Investigator.Messrs. Neeley and Michael K. Lloyd, EMB, prepared this report. The authorsacknowledge the assistance of Messrs. Percy L. Collins, Michael Hedrick, andJimmy W. Hall III, EMB, in preparing and testing the concrete mixtures in thisinvestigation.

At the time of publication of this report, Director of WES was Dr. Robert W.Whalin. Commander was COL Bruce K. Howard, EN.

The contents of this report are not so be used for advertising, publication,or promotional purposes. Otation of trade names does not constitute anofficial endorsement or approval of the use of such commercial products.

V

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1 Introduction

Background

A large percentage of concrete used by the U.S. Army Corps ofEngineers (CE) to construct Civil Works Structures is mass concrete theproportions of which are selected as a result of studies conducted by the divisionlaboratories in accordance with the American Concrete Institute (ACI)Standard 211.1 (ACI 1993b) (CRD-C-99).' In recent years, a number ofcontractor complaints have been received at CE projects regarding poorworkability of mass concrete. In some instances, these complaints have beenfollowed by actual production delay claims. Although the problems associatedwith the workability of the concrete generally appear to be related more to thecontractor's selection of materials, placing operations, or lack of adequatecontractor quality control (CQC) than the Government's mixture proportions, it isoften difficult for the Government to be certain that the mixture itself is not atfault. Civil Works Investigation Studies Work Unit No. 32768, "Workability ofMass Concrete," was initiated to address some of the problems related to theselection of proportions for mass concrete with assurance that the concrete willhave adequate workability.

The initial phase of this study was to obtain information from CE division anddistrict staff members having recent experience with mass concrete construction.Their input was solicited to describe workability complaints as well as thepurported causes of the problems. A survey form was designed to identifypotential problems in five areas that could lead to workability problems or theperception of workability problems. The five areas were (a) materials,(b) mixture proportions, (c) transporting and placing, (d) consolidation, and(e) overall considerations. The results of this survey (Neeley 1993) indicated(a) problems with aggregate grading, usually associated with improper handling atthe job site, (b) improper handling and placement procedures for the freshconcrete, (c) improper consolidation procedures, and (d) frequent adjustments tomixture proportions when taken from the laboratory to the field.

1 CRD-C equivalent in parentheses is from the Handbook for Concrete and Cement,

U.S. Army Engineer Waterways Experiment Station (USAEWES), 1949, Vicksburg, MS.

Chapter 1 Introduction

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Only one of these problem areas is under direct control of the government;i.e., the selection of mixture proportions and adjustments thereof. Aggregategradings are prescribed in the specifications for the work. Handling procedures,transporting, placing, and consolidation are the direct responsibility of thecontractor. Adequate guidance in each of these areas is available from the ACI,the Portland Cement Association (PCA), and the CE to assist the contractor incompleting a successful placement:

Aggregate gradings -

"Mass Concrete," Civil Works Guide Specification 03305 (Headquarters,

U.S. Army Corps of Engineers (HQUSACE) 1992).

"Standard Practice for Concrete for Civil Works Structures," EngineerManual 1110-2-2000 (HQUSACE 1994).

Aggregate handling procedures -

"ACI Manual of Concrete Inspection," SP-2 (ACI 1992).

"Guide for Measuring, Mixing, Transporting, and Placing Concrete,"

ACI 304R (ACI 1993c).

"Design and Control of Concrete Mixtures," (Kosmatka and

Panarese 1988).

Transporting and placing fresh concrete-

"Mass Concrete," Civil Works Guide Specification 03305(HQUSACE 1992).

"Standard Practice for Concrete for Civil Works Structures," EngineerManual 1110-2-2000 (HQUSACE 1994).

"ACI Manual of Concrete Inspection," SP-2 (ACI 1992).

"Guide for Measuring, Mixing, Transporting, and Placing Concrete,"ACI 304R (ACI 1993c).

"Placing Concrete with Belt Conveyors," ACI 304.4R (ACI 1993d).

"Design and Control of Concrete Mixtures," (Kosmatka andPanarese 1988).

Consolidating fresh concrete-

"Mass Concrete," Civil Works Guide Specification 03305(HQUSACE 1992).

2 Chapter 1 Introduction

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"Standard Practice for Concrete for Civil Works Structures," Engineer

Manual 1110-2-2000 (HQUSACE 1994).

"ACI Manual of Concrete Inspection," SP-2 (ACI 1992).

"Guide for Measuring, Mixing, Transporting, and Placing Concrete,"

ACI 304R (ACI 1993c).

"Guide for Consolidation of Concrete," ACI 309R (ACI 1993e).

"Design and Control of Concrete Mixtures," (Kosmatka andPanarese 1988).

Concrete mixture proportions should not be adjusted to avoid complaints if thisinvolves accepting materials that are out of specification or improper transporting,placing, or consolidation procedures. Many complaints of inadequate workabilitycould be eliminated by following proper aggregate handling and fresh concretetransporting, placing, and consolidating procedures. Neeley (1993) alsoconcluded that:

by their nature, mass concrete mixtures are lean and, if not properlyproportioned, can be harsh: It should be recognized that laboratoryconditions where mixtures are proportioned are often nearly idealand always different from the actual field conditions. While CEfield staff members are responsible for assuring that the contractoruses materials that meet specifications and proper procedures to mix,transport, place, and consolidate, the laboratory staff who proportionmass mixtures should do so realizing that field conditions are neverideal. Mixtures should be proportioned in such a way toaccommodate a reasonable amount of field variations without causingexcessively harsh mixtures. The solution may be to increase themortar content by a small enough amount to provide additionalworkability without causing an excessive increase in temperaturerise. This scenario may now be possible with increasing amounts offly ash, or other pozzolan or ground slag constituting thecementitious material.

It was recommended that a laboratory investigation be initiated to examine thefeasibility of suggesting a minimum mortar content in 37.5-mm (1-1/2-in.)nominal maximum size aggregate (NMSA) mass concrete similar to that for75-mm (3-in.) NMSA mass concrete. It was also recommended that a laboratoryinvestigation be initiated to examine the feasibility of suggesting a paste-mortarratio in 37.5-mm (1-1/2-in.) and 75-mm (3-in.) NMSA mass concrete similar tothat for roller-compacted concrete.

As a continuation of this program, this report documents the investigation intothe potential benefits of minimum and maximum mortar contents for 37.5-mm(1-1/2-in.) NMSA mass concrete, and minimum and maximum paste-mortarratios for 37.5-mm (1-1/2-in.) and 75-mm (3-in.) NMSA mass concrete.

Chapter 1 Introduction 3

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Mortar Content

Historically, most mass concretes have contained either 75-mm (3-in.) or150-mm (6-in.) NMSA, and appropriate guidance for proportioning thesemixtures is available. ACI Standard 211, "Standard Practice for SelectingProportions for Normal, Heavyweight, and Mass Concrete," (ACI 1993b)recommends minimum and maximum mortar contents for mass concretes having75-mm (3-in.) and 150-mm (6-in.) NMSA. The Committee 211 report states that"experience has demonstrated that large aggregate mixtures, 75-mm (3-in.) and150-mm (6-in.) NMSA, require a minimum mortar content for suitable placingand workability properties." The minimum mortar content is that which will benecessary to provide adequate workability for placement and consolidation. Themaximum mortar content is suggested to prevent unnecessarily high cementitiouscontents which would generate an undesirable amount of heat and increase thetemperature rise of the mass of concrete.

The Committee 211 report also places emphasis upon the combined grading ofthe coarse aggregates. It states that the individual size groups should be combinedto produce a grading that approaches maximum density. This minimizes voidspace allowing more of the mortar to be available for workability, placability, andfinishability. The parabolic maximum density curve (Eq. 1) originally developedfrom work by Fuller and Thompson (1907) and later modified by others,including Plum (1950), is suggested as a guide for approaching maximum densitywith 75-mm (3-in.) and 150-mm (6-in.) NMSA. The exponents, 0.5 and 0.8, aresuggested based upon the results of numerous dry-rodded weights obtained withvarious types of coarse aggregates (Tynes 1968).

P d X x _ 4.75xP - 47X(1)

D x - 4.75x

where

P = cumulative percent passing the d-size sieved = sieve opening, mmD = NMSA, mmx = exponent (0.5 for rounded and 0.8 for crushed aggregate)4.75 = minimum size aggregate included, mm

It is not expected that the combined grading of the individual aggregate sizegroups match the parabolic maximum density curve perfectly. The grading of theindividual aggregate size groups will be a limiting factor determining how closelythe maximum density grading can be matched. The dry rodded unit weightmethod is suggested for combining individual size groups up to a maximum of37.5-mm (1-1/2-in.) to approach maximum density.

In recent years, an increasing amount of mass concrete has been placed usingsmaller NMSA. The authors have proportioned mass concrete mixtures forconstruction of four hydraulic structures in the CE in the past 10 years which used

4 Chapter 1 Introduction

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37.5-mm (1-1/2-in.) NMSA. The authors have also proportioned mass concretemixtures for structural applications using 19.0-mm (Y4-in.) and 9.5-mm (%-in.)NMSA. Proportioning mass concrete mixtures having adequate workability,placability, and finishability characteristics can sometimes be more difficult withthe smaller NMSA. The smaller aggregate necessitates an increased mortarcontent (water, cementitious material, fine aggregate, air), yet the need to limitheat generated and temperature rise requires the cementitious material be held to aminimum. The practitioner must weigh each of these requirements whenproportioning mass concrete mixtures. Unfortunately, there is little, if any,guidance for minimum mortar contents in concretes having NMSA less than75-mm (3-in.). Therefore, the experience of the person proportioning the massmixtures with smaller NMSA can have a significant impact upon the outcome ofthe mixtures; i.e., has the cementitious content been minimized as much aspossible to reduce the generation of heat, and will the mixtures have adequateworkability, placeability, and finishability when proper procedures are followed.

Another factor that must be considered is material variation in the field.Mixtures are proportioned in the laboratory using a small, presumablyrepresentative sample of materials that have been selected for use. Optimummixtures will be proportioned using these materials. However, caution must beexercised to avoid proportioning the mixtures such as to have barely adequateworkability in the laboratory mixtures. It must be recognized that some materialvariation in the field is normal, especially involving aggregates. If the laboratorymixtures are proportioned with aggregates with a favorable combined grading,and subsequent variations in the field produce a less favorable grading, thenworkability problems can result. The minimum mortar content guidance inACI 211 (ACI 1993b) addresses this concern for mass concrete mixtures having75-mm (3-in.) and 150-mm (6-in.) NMSA. One purpose of this investigation is todetermine if similar principles can also apply to mass concrete mixtures havingsmaller NMSA.

Paste-Mortar Ratio

The ACI Committee 207 report "Roller Compacted Mass Concrete" (ACI1993a) describes several different concepts and procedures for proportioningroller compacted mass concrete (RCC). One of the methods involves determiningthe minimum paste requirement for the proposed fine aggregate after the coarseaggregate grading has been selected. Normally, the void content of fine aggregateranges from 34 to 42 percent. The goal of this method is to determine theminimum paste (water, cementitious material, and air) necessary to fill the voidsbetween the fine aggregate particles and provide some additional paste which willbe needed to ensure necessary workability to the mixture. For RCC, this extrapaste is minimal. For slumpable concretes, a larger amount of extra paste will benecessary. The Committee 207 report states that air-free paste-mortarratios (p/m), by volume, of 0.38 for interior mass concretes and 0.42 for beddingmixtures have generally been found acceptable. Another purpose of thisinvestigation was to determine if similar principles can be applied to slumpable,

Chapter 1 Introduction 5

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mass concrete mixtures to improve their workability, placeability, andfinishability.

Objectives

The objectives of this research were three-fold. The first objective was toexamine the feasibility of requiring a minimum mortar content in 37.5-mm(1-1/2-in.) NMSA mass concrete similar to the requirement for 75-mm (3-in.)NMSA mass concrete. The second and third objectives were to examine thefeasibility of requiring a p/m in 37.5-mm (1-1/2-in.) and 75-mm (3-in.) NMSAmass concretes similar to the requirement for RCC. Concretes having twodifferent 37.5-mm (1-1/2-in.) coarse aggregates were evaluated for mortarcontent and p/m. One was a crushed material consisting primarily of blockyparticles. The other was a crushed material having more flat and elongatedparticles.

Scope

A number of mass concrete mixtures that had been proportioned at theU.S. Army Engineer Waterways Experiment Station (WES), Concrete andMaterials Division (CMD), in recent years were surveyed to determine typicalmortar contents and p/m used. Using these typical values as a starting point, massconcrete mixtures having 37.5-mm (1-1/2-in.) and 75-mm (3-in.) NMSA werethen proportioned having a range of mortar contents and p/m encompassing thehistorical values. The fresh properties of each mixture were evaluated using avariety of test methods. The results were evaluated with consideration given toactual mixtures used in construction which exhibited good workability and othermixtures which were more troublesome during actual field placements. Many ofthe measurements were made in non-SI units and converted to SI units usingconversion values in AmericAn Society for Testing and Materials (ASTM) E 380(ASTM 1993m).

6 Chapter 1 Introduction

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2 Concrete Mixtures

Review of Recent Mass Concrete Mixtures

37.5-mm (1-1/2-in.) NMSA mixtures

A total of 91 mixtures that had been proportioned between the years 1974 and1992 for eleven different projects were examined. Natural sand fine aggregatewas used at 10 of the 11 projects. A manufactured limestone fine aggregate wasused at the remaining project. Coarse aggregates included natural gravel, crushedlimestone, and crushed granite. A complete listing of materials and otherpertinent properties are given in Appendix A, Table Al.

The mortar content and p/m were calculated for each of the mixtures. Allsubsequent references to mortar content are based on a 1-m3 batch.Corresponding mortar contents shown in parentheses are for a 1-yd3 batch. Therelationship between water-cement ratio (w/c) and both mortar content and p/mfor all mixtures are shown in Figures Al and A2, respectively. The relationshipbetween the mortar content and p/m for all mixtures is shown in Figure A3.Averages for each type of coarse aggregate are shown in Figures 1, 2, and 3. Adescription of the acronyms used to identify each type of coarse aggregate in thefigures is given in Appendix A. It can be seen from Figures 1 and 3 that mixturescontaining all crushed coarse aggregates used a higher mortar content thanmixtures which contained natural gravel coarse aggregates or a combination ofcrushed and natural gravel coarse aggregates. Mixtures containing crushed coarseaggregates generally used approximately 0.537 m3 (14.5 ft) of mortar whilemixtures containing natural gravel coarse aggregates used approximately 0.515mi3 (13.9 ft3) of mortar. The mortar content did not appear to be significantlyaffected by the w/c nor the p/in. Figures 2 and 3 indicate that the p/m remainedrelatively constant at 46 to 47 percent, regardless of the w/c and mortar content.

It is suggested from this examination of existing 37.5-mm (1-1/2-in.) NMSAmass concrete mixtures that the p/m remains relatively constant at approximately46 to 47 percent when the slump is generally between 50 and 75 mm. It is alsosuggested that the mortar content ranges from approximately 0.515 m3

(13.9 ft3) for mixtures containing natural gravel coarse aggregates to

Chapter 2 Concrete Mixtures 7

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0.545

0 .5 4 0 . ................................................ ....... ..... .. ...................................... .......

E+o .5 ............... ........ " " ....... " +....... i............... .............. ............... ...............................

L) 0.535I•" ~ ~Crushed granite doarse1" aggregate '

Cuh g Crushed limestone coarse aggrelatea : 0 .5 3 0 . ............... :............... ......... .................... ................................. ............... .............. ............... ............... .0L 0 5 2 .............. ............... .............. ............... ............... .............. i............... ....... ...............

Natural gravel coarse aggregate Crushed granitemD 0 .5 2 0 ..................................... • .. .............. ............................................. . -7 ; a i i ~ 6 ; V,............. ........ .......

V.iC/ and natural gravel0 coarse aggregates

0 .5 1 ............... L.............. ............... .............. ............................... .............. ............... ................................0.515+

0.510 T T 1 r0.25 0.30 0.35 0.40 0.45 0.50 0.55 0.60 0.65 0.70 0.75

WATER/CEM ENT

Figure 1. Average mortar content of 37.5-mm NMSA mass concretemixtures reviewed for historical data

0.500r

0 .4 9 0 -.-.-----------.-. --.-. --------............... .. .............. ............... . .. .............. ............... .............. .............. ................

CC 0 .4 8 0 . .............. ............... .............. ............... ................ .............. .............. ............... .............. ................

CC Natural bravel coarse aggregates Crushed Imestose coarse aggregati0 S0 4 0 .... .... .... ........... ............... ..... ." ............. ................ , .............. .............. ...............

0.470 .~ ......0' .4 6 .................. .............. .............. .......... ÷ ............... ........... .... ...... ........... ............... ..............

Crushedj granite coarse ag~regrates• *rsh rante ani.rsatural gr•al

0 .4 50 . ............... ............... .............. ............................... ............... .............. '. o. . s. . a..... . r g e.s ........

0.440.0.440 t t r i t t

0.25 0.30 0.35 0.40 0.45 0.50 0.55 0.60 0.65 0.70 0.75WATER/CEMENT

Figure 2. Average paste/mortar of 37.5-mm NMSA mass concrete mixturesreviewed for historical data

8 Chapter 2 Concrete Mixtures

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0.480

0 .4 7 5 . ...................................................................................................................................... ..............

Natural gravel coars. .aggregates. .

n -0 .4 7 0 ~~. ............. { .... .... ....................................................... ..................... ......... ....

M 0.470-S.-.Crushed limestone

coarse aggregates

02 0 .4 6 5 . .................. .................. ................... i .................... .................. ................. ....................... ..................0 5Crushed granite and rlatural

4l ; gravel coarse aggregtesW 0- ii Crushed granite

* coarse aggregatesnL 0 .4 6 0 -. . .................. : . ..................... :................... .................. :................... :.. ,...... ..................

....... 0.460...........e............. ..............

0 .4 5 5 . .................... :.................. . ............ ................. ... ... .................................... ...

0.450

0.510 0.515 0.520 05.25 0.530 0.535 0.540 0.545 0.550

VOLUME OF MORTAR, cum

Figure 3. * Relationship of average mortar content and paste/mortar of37.5-mm NMSA mass concrete mixtures reviewed for historicaldata

approximately 0.537 m3 (14.5 ft3) for mixtures containing crushed coarseaggregates. Therefore, it is possible that these two parameters could be effectiveguides to assist in the proportioning of mass concrete mixtures using 37.5-mm(1-1/2-in.) NMSA.

75-mm (3-in.) NMSA mixtures

A total of 17 mixtures that had been proportioned between the years 1974 and1992 for four different projects were examined. Natural sand fine aggregate wasused at three of the four projects. A manufactured limestone fine aggregate wasused at the remaining project. The coarse aggregate was crushed limestone ineach project. A complete listing of materials and other pertinent properties aregiven in Appendix A, Table A2.

The mortar content and p/m were calculated for each of the mixtures. Allsubsequent references to mortar content are based on a 1-m3 batch.Corresponding mortar contents shown in parentheses are for a 1-yd3 batch. Therelationship between w/c and both mortar content and p/m for all mixtures areshown in Figures A4 and AS, respectively. The relationship between the mortarcontent and p/m for all mixtures is shown in Figure A6. Averages are shown inFigures 4, 5, and 6. It can be seen from Figures 4 and 6 that mixtures containingthe manufactured limestone fine aggregate used a higher mortar content thanmixtures which contained natural fine aggregates. Mixtures containing

Chapter 2 Concrete Mixtures 9

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0.480

0.475 . .........: ........

EMa ufacturehi limestorie fine agjregateCrL shed limestone codrse aggregate

0

o Natural fine aggregate

0.450 Cushed limestone coarse aggregate

4.

0.445 r0.25 0.30 03ý5 0.40 0.45 0.50 05ý5 060O 0.65 0.70 0.75

WATER/OEM ENT

Figure 4. Average mortar content of 75-mm NMSA mass concrete mixturesreviewed for historical data

0.520 __ ____- - -____-__ __

0r 0.490 ............ ..........................................n fcu~ ........ . .ama rdlmestohe fine aggregate

Crished limbstone colarse aggil.egateo 0 .4 8 0 ........ .............. ....... i................ ........

Natural line aggregate:0.450 ~.., Crushed limeitane caaheeagrat

0.430 tt i0.25 030O 0.35 0.40 0.45 0.50 0.55 0.60 06ý5 0.70 0.75

WATER/CEMENT

Figure 5. Average paste/mortar of 75-mm NMSA mass concrete mixturesreviewed for historical data

10Chapter 2 Concrete Mixtures

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0.520

0 .5 1 0 . ................................................... i........................... ........................... ................................................

Manufactured limestone fine aggregate

Crushed limestone coarse aggregate

Cc

o0 o ............................I ............................................... I.......................... ....................1............................0 ,0 .4 7 0 . ......................... .................................................... ......................... •............................ ........................

(LJ 0 .4 6 0 . ........................ ........................ ................ ................................... ......................... .........................

0 .4 5 0 ............................................................................ .................... . . . . . . . . .Natur'al fine aggregate

Crushed limestone coarse aggregate0 .4 4 0 . ......................... .................... I .............................. •........................ . ................................ ..................

0.430,

0.430 0.440 0.450 0.460 0.470 0.480 0.490

VOLUME OF MORTAR, cu m

Figure 6. Relationship of average mortar content to paste/mortar of 75-mmNMSA mass concrete mixtures reviewed for historical data

manufactured limestone fine aggregate generally used approximately 0.478 m3

(12.9 ft3) of mortar while mixtures containing natural fine aggregates usedapproximately 0.447 m3 (12.0 ft3) of mortar. As shown in Figures 5 and 6, thepaste/mortar of the mixtures containing manufactured limestone fine aggregatewas also higher than that of the mixtures containing natural fine aggregate;approximately 50 percent versus 44 percent, respectively.

Materials Used In Current Investigation

A listing of the materials used to proportion the 37.5-mm (1-1/2-in.) and75-mm (3-in.) NMSA mass concrete mixtures used in the current investigation isprovided here. The numbers in parenthesis following each material are CTDidentification numbers assigned to all materials used in research programs toensure traceability.

Cement

Portland cement, Type II (940054)

Chapter 2 Concrete Mixtures 11

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Pozzolan

Fly ash, class C (LMK-4 AD-4)

Aggregates

Natural sand fine aggregate (920100)

9.5-mm (3%-in.) nominal maximum size (NMS) crushed limestone coarseaggregate (920337)

19.0-mm (A-in.) NMS crushed limestone coarse aggregate (920048)

37.5-mm (1-1/2-in.) NMS crushed limestone coarse aggregate (CL-2 MG-2)

75-mm (3-in.) NMS crushed limestone coarse aggregate (920322)

19.0-mm (--in.) NMS crushed granite coarse aggregate (940294)

37.5-mm (1-1/2-in.) NMS crushed granite coarse aggregate (940295)

Admixtures

Air-entraining admixture (AEA) (920090)

The sieve analysis (ASTM C 136 (ASTM 1993c)) of each aggregate andvalues of absorption and specific gravity (ASTM C 127 (coarse aggregate) andC 128 (fine aggregate)) (ASTM 1993a,b) are given in Table 1. The portlandcement conformed to Type II requirements of ASTM C 150 (ASTM 19930. Thefly ash conformed to Class F requirements of ASTM C 618 (ASTM 1993k).Physical and chemical properties of the cement and fly ash are given in Tables 2and 3, respectively.

The 19.0-mm (¾-in.) and 37.5-mm (1-1/2-in.) NMS crushed limestone coarseaggregates were generally blocky and were judged to have a favorable particleshape for crushed coarse aggregates. The crushed granite and the 9.5-amm(%-in.) NMS crushed limestone coarse aggregate contained more flat andelongated particles and were judged to have a less favorable particle shape forcrushed coarse aggregates. Particle shape classifications as described in ASTMD 4791 (ASTM 19931) for each of the aggregates listed above are given inTable 4. Natural gravel coarse aggregates were not included in this investigation.However, it can be assumed that they would usually have a more favorableparticle shape than either of the crushed materials. Principles shown to beapplicable to the crushed coarse aggregates could be extended to the natural gravelcoarse aggregates with additional research.

12 Chapter 2 Concrete Mixtures

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Table 1

Aggregate

Cumulative Percent Passing

Coarse Aggregate

Crushed Crushed Crushed Crushed Crushed Crushed FineLimstone Limestone Limestone Limestone Granite Granite Aggregate

Sieve Size 920322 CL-2 MG-2 900048 920337 940295 940294 920100

75 mm 9650 mm 40 100 10037.5 mm 14 96 9125.0 mm 10 29 100 32 9919.0 mm 6 7 97 7 8412.5 mm 3 67 100 1 389.5 mm 3 39 97 1 154.75 mm 2 6 42 1 1002.36 mm 1 8 951.18 mm 81

600 pm 55300 pm 18150 _rn 3

Specific Gravity 2.64 2.74 2.71 2.72 2.63 2.65 2.65

Absorption 2.90 0.3 0.2 0.4 1.0 0.8 0.3

Chapter 2 Concrete Mixtures 13

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Table 2Report of Tests on Hydraulic Cement

TO: FROM:U. S. Army Corps of Engineers

Billy Neeley Waterways Experiment StationStructures Laboratory Engineering Materials Group

3909 Halls Ferry RoadVicksburg, Mississippi 39180-6199

Company: Lone Star Industries Test Report No.: WES-7-94Location: Cape Girardeau, Missouri Program: Single SampleSpecification: ASTM C 150, II, HH* CTD No.: 940054Contract No.: Job No.: ACSAZO81AIS3100Project: Workability of Mass Concrete Date Sampled: 21 Jan 94

Partial test result

3L3/94 Tests complete, material __X does, _ does not meet specification

ASTM C 150Result Retest Spec Limits

Chemical Analysis "Type II"

SiO2, % .......... ................ 21.9 20.0 minA1 2 0 3, % ......... ............... 4.1 6.0 maxFe 2 0 3, % ......... ............... 3.1 6.0 maxCaO, % ........... ................ 62.9MgO, % ........... ................ 3.3 6.0 maxSO 3, % ..... ............... ... .. . 2.6 3.0 maxLoss on ignition, % ... .......... 0.07 0.75 maxNa 2 0, % .............. ... ................ 1. 3.0 maxInsoluble residue,% ....... . ... 0.10K20, % ......... ................ .. 0.7Alkalies-total as Na20, % ....... 0.57 0.60 maxTiO2, % ........ ................ .. 0.26P2 0 5 , % ...... ................ .. 0.10C3A, % ......... ................ .. 7 8 maxC3S, % ......... ................ .. 47C2S, % ......... ................ .. 27C4AF, % ................ ................ 9

Physical Tests

Heat of hydration, 7-day, cal/g . . .. 72* 70 maxSurface area, m2 /kg (air permeability) 392 280 maxAutoclave expansion, % .. ........ 0.07 0.80 maxInitial set, min. (Gillmore) ..... 160 60 minFinal set, min. (Gillmore) ...... 255 600 maxAir content, % ..... ............ .. 8 12 maxCompressive strength, 3-day, psi . . 3,020 1,500, 1,000a minCompressive strength, 7-day, psi . . 4,320 2,500, 1,700a minFalse set (final penetration), % . . - 50 min

REMARKS: aApplies only to heat of hydration cement.

*Heat of hydration tested and reported for information only.

CF:

Melvin C. Sykes

Information given in the report shall not be used in advertising or salespromotion to indicate endorsement of this product by U.S. Government.

14 Chapter 2 Concrete Mixtures

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Table 3Report of Tests on PozzolanTO: Billy Neeley FROM: Structures Laboratory

Structures Laboratory LMIK-4 AD-4 USAE Waterways Experiment StationATTN: Cement and Pozzolan UnitPO Box 631Vicksburg, MISSISSIPPI 39180-631

COMPANY: Gifford-Hill TEST REPORT NO.: 17 Mar 88

LOCATION: Boyce. LA REPORT DATE:

SPECIFICATION: ASTM C 618, Class C DATE SAMPLE:

CONTRACT NO.: Red River Waterway Thermal Study PROGRAM: 3 Mar 88

TEST RESULTS OF THIS SAMPLE SCOMPLYWITH SPECIFICATION LIMITSm__ Do NOT COMPLY

S'0 2 + A120 3 MgO SO 3 AVAILABLE POZZOLANIC AUTOCLAVE

+ Fe 20 3 ALKALIES STRENGTH EXPANSION% (a) (b) % CONTROL (b) %

REQUIREMENTS

MINIMUM MAXIMUM MAXIMUM MINIMUM MAXIMUM

TEST RESULTS

61.3 5.0 2.2 0.0

SAMPLE MOISTURE LOSS OF FINENESS FINENESS LIME WATER DENSITY DENSITY

REQUIREMENTS

IMAXIMUM MAXIMUM MAXIMUM MAXIMUM MAXIMUM MAXIMUM _ IMAXIMUM

TEST RESULTS

1 0.0 0.7 19 0 92 2.53 3

AVERAGE

(a) OPTIONAL REQUIREMENT LABORATORY CEMENT USED:

(b) 28 DAY TEST LABORATORY LIME USED: CHEMSTONE

REMARKS:

Si0 2 : 36.5; Fe 2 0 3 : 6.5: A12 0 3 : 18.2

CQSCL383A1 SR300

Toy S. PooleChief, Cement and Pozzolan Unit

NOtE: THE INFORMATION GIVEN IN THIS REPORT SHALL NOT BE USED IN ADVERTISING OR SALES PROMOTION TOINDICATE EITHER EXPLICITLY OR IMPLICITLY ENDORSEMENT OF THIS PRODUCT BY THE U.S. GOVERNMENT.

FORM EDITION OF 1 SEP 84 IS OBSOLETEWES 1195

R AUG 87

Chapter 2 Concrete Mixtures 15

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Table 4

Coarse Aggregate Particle Shape

Aggregate Not Flat or Elongated, % Flat or Elongated, %

37.5-mm (1-1/2-in.) NMS 97 3crushed limestone

19.0-mm (%-in.) NMS 95 5crushed limestone

9.5-mm (%-in.) NMS 41 59crushed limestone

37.5-mm(1-1/2-in.) NMS 70 30crushed granite

19.0-mm (%-in.) NMS 49 51crushed granite II_ _

Mixture Proportions

37.5-mm (1-1/2-in.) NMSA mixtures

Mixtures having w/c of 0.50 and 0.60, by mass, were proportioned and tested.Thirty-five percent of the cementitious material, by volume, was fly ash. Thecoarse aggregates were separated into two groups, those with a favorable particleshape and those with a less favorable particle shape. The group having afavorable particle shape consisted of the 19.0-mm (A-in.) and 37.5-mm(1-1/2-in.) NMS crushed limestone. The group having a less favorable particleshape consisted of the 9.5-mm (%-in.) NMS crushed limestone and the 19.0-mm('-in.) and 37.5-mm (1-1/2-in.) NMS crushed granite. A range of mortarcontents and p/m were evaluated for each group of coarse aggregate and w/c. Atest matrix is given in Table 5.

Favorable coarse aggregate particle shape. Mixtures containing coarseaggregates with a favorable particle shape were evaluated at mortar contentsranging from 0.504 to 0.548 m3 for a w/c of 0.50, and at mortar contents rangingfrom 0.504 to 0.559 m3 for a w/c of 0.60. Five different p/m's were used at eachmortar content. The combination of coarse aggregates was 53 percent 37.5-mm(1-1/2-in.) NMS crushed limestone and 47 percent 19.0-mm (Y-in.) NMScrushed limestone. The combined grading is shown in Figure 7. A total of 55mixtures were proportioned and tested.

Less favorable coarse aggregate particle shape. Mixtures containing coarseaggregates with a less favorable particle shape were evaluated at mortar contentsranging from 0.515 to 0.548 m3 for a w/c of 0.50, and at mortar contents rangingfrom 0.526 to 0.548 m3 for a w/c of 0.60. Either three or four different p/m'swere used at each mortar content. The combination of coarse aggregates was

16 Chapter 2 Concrete Mixtures

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Table 5Test Matrix

w/c, Mortar Content,Aggregate Shape wt m3 pim

Favorable 0.50 0.504 0.4466 to 0.4966Favorable 0.50 0.515 0.4453 to 0.4953Favorable 0.50 0.526 0.4441 to 0.4941Favorable 0.50 0.537 0.4430 to 0.4030Favorable 0.50 0.548 0.4418 to 0.4918

Favorable 0.60 0.504 0.4228 to 0.4728Favorable 0.60 0.515 0.4215 to 0.4715Favorable 0.60 0.526 0.4202 to 0.4702Favorable 0.60 0.537 0.4190 to 0.4690Favorable 0.60 0.548 0.4178 to 0.4678Favorable 0.60 0.559 0.4167 to 0.4467

Less Favorable 0.50 0.515 0.4591 to 0.4941Less Favorable 0.50 0.526 0.4549 to 0.4949Less Favorable 0.50 0.537 0.4526 to 0.4926Less Favorable 0.50 0.548 0.4512 to 0.4912

Less Favorable 0.60 0.526 0.4315 to 0.4715Less Favorable 0.60 0.537 0.4294 to 0.4694Less Favorable 0.60 0.548 0.4306 to 0.4706

47 percent 37.5-mm (1-1/2-in.) NMS crushed granite, 43 percent 19.0-mm('-in.) NMS crushed granite, and 10 percent 9.5-mm (¾/a-in.) NMS crushedlimestone. The combined grading is also shown in Figure 7. A total of 23mixtures were proportioned and tested.

75-mm (3-in.) NMSA mixtures

Mixtures having w/c of 0.50, by mass, were proportioned and tested. Thirty-five percent of the cementitious material, by volume, was fly ash. The coarseaggregates, consisting of the 19.0-mm (3A-in.), 37.5-mm (1-1/2-in.), and 75-mm(3-in.) NMS crushed limestone, were considered to have a favorable particleshape. The combination of coarse aggregates was 55 percent 75-mm (3-in.) NMScrushed limestone, 23 percent 37.5-mm (1-1/2-in.) NMS crushed limestone, and22 percent 19.0-mm (3A-in.) NMS crushed limestone. The combined grading ofthe coarse aggregates is shown in Figure 8. The mortar content was 0.445 m3

(12.0 f), and p/m ranged from 44.6 to 46.6 percent. Three mixtures wereproportioned and tested.

Tests

Tests performed on the fresh concrete included slump (ASTM C 143) (ASTM1993e), air content' (ASTM C 231) (ASTM 1993h), unit weight (ASTM C 138)

Chapter 2 Concrete Mixtures 17

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100-8090-•' ,,

10.70 ..................(.0 70- ..................................................................

z( 6 0 . ................................................................ •.............. ..

o 40-a:

n..3Q.... ........ ........ ......................2 0 ............................................................................................ .. . . . . .

10 ............................................. . ..............

50 37.5 25 19 12.5 9.5 4.75

SIEVE SIZE, mm

-W- Favorably shaped -- I-- Unfavorably shaped

Figure 7. Combined grading of coarse aggregate used in 37.5-mm (1-1/2-in.)NMSA mixtures

100-

(.9 70..........................z•o 60..........................

a- 50

zo 40..........................ccw

1 0 ..... .... .. .. .. .. .... .. .. .. .. ..... .... .. .. .... ...... ...... .... .. .. .. ..... .... .. .. .. .. .. .. ...... .. .. .. .. ..

7- 5 50 37.5 25 19 12.5 9.5SIEVE SIZE, mm

I Fvorblyshped]

Figure 8. Combined grading of coarse aggregates used in 75-mm (3-in.)NMVSA mixtures

18 Chapter 2 Concrete Mixtures

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(ASTM 1993d), bleed (ASTM C 232) (ASTM 1993i), and a modified Vebe testsimilar to British Standard Method for Determination of Vebe Time (BS 1881:Part 104) (British Standards Institute 1983). The British Vebe test procedure wasmodified to use a larger sample of concrete. Otherwise, the test procedure wasessentially unchanged. The modified test procedure is given in Appendix B. TheVebe test was included in the investigation because it provides a measure of themobility and compactability of concrete under vibration, while the slump testprovides a measure of the consistency of the concrete under static conditions. Thesize of the Vebe apparatus was increased for two reasons: (a) the authorsbelieved that a larger sample might provide a more representative measure of themobility and compactability, and (b) the larger size was necessary to be able totest mixtures having 75-mm (3-in.) NMSA without wet sieving to remove thelarger particles. Test results on wet-sieved material without the large aggregateparticles may not adequately represent the workability and placability of the actualconcrete.

Test results for mixtures containing a 37.5-mm (1-1/2-in.) NMS coarseaggregate of favorable particle shape are given in Table 6. Each result representsthe average from at least two batches of concrete. Test results for mixturescontaining a less favorable 37.5-mm (1-1/2-in.) NMS coarse aggregate particleshape are given in Table 7. Each result represents the average from at least twobatches of concrete. Test results for mixtures containing 75-mm (3-in.) NMSAare given in Table 8.

Chapter 2 Concrete Mixtures 19

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20 Chapter 2 Concrete Mixtures

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Chapter 2 Concrete Mixtures 21

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Table 8Test Results on 75-mm (3-in.) NMSA Mixture with Favorably ShapedCoarse Aggregate

Mortar Water Air Unit VebeMixture Content, Content, Slump, Content, Weight, time,No. m3 p/m kg/mr3 mm % kg/mr3 aec

16 0.445 0.446 92 25 5.4 2,356 47

17 0.445 0.456 95 40 5.6 2,353 62

18 0.445 0.466 98 45 5.5 2,353 60

22 Chapter 2 Concrete Mixtures

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3 Discussion and Analysis

37.5-mm (1-1/2-in.) NMSA Mixtures

Criteria

Consideration was given to actual mixtures used in construction that exhibitedgood workability, and some which were more troublesome, to estimate whatwould be an appropriate Vebe time to describe a mixture easily consolidated. Itwas also noted that historically, 37.5-mm (1-1/2-in) NMSA mass concretemixtures have been proportioned to have slumps ranging from 40 to 75 mm (1-1/2to 3 in.). Using these criteria, it is suggested that a Vebe time of 12 to 20 secondswould indicate that a mixture has adequate workability to be easily placed andconsolidated. The following discussion is based on these assumptions.

Favorable coarse aggregate particle shape

Fifty four mixtures were evaluated as shown in Tables 5 and 6. Plots of p/mversus Vebe time at each mortar content are shown in Figures 9 and 10 for w/c of0.50 and 0.60, respectively. Slump values are indicated on each curve at theappropriate location. The data indicate that for a given p/m, the Vebe timenecessary to consolidate the sample decreases as the mortar content increases. Acorresponding increase in slump is also indicated as the mortar content increasedin the mixtures having a 0.50 w/c. For a given mortar content, the Vebe timenecessary to consolidate the sample decreases as the p/m increases; however, itdoes not appear to be a linear relationship. There appears to be a closerelationship between the p/m and slump. Regardless of the mortar content, theslump increases as the p/m increases. Each of these relationships between themortar content, p/m, slump, and Vebe time were expected. The data providequantification of the relationships.

Mixtures with 0.50 w/c. The data indicate that mixtures having mortarcontents of 0.526 mi3 (14.2 f-0) and less could be judged difficult to consolidatewhen the slump is less than 50 mm (2 in.). Higher p/m were necessary to reducethe Vebe time. While the higher p/m did not necessarily increase the water

Chapter 3 Discussion and Analysis 23

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24 Chapter 3 Discussion and Analysis

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content above that of mixtures having higher mortar contents, the higher p/m didresult in higher slumps. From a visual observation, the mixtures having a lowermortar content and higher p/m appeared to be "wet." Mortar coating the coarseaggregate particles had a noticeable water sheen. Yet these mixtures could bemore difficult to consolidate than other mixtures having a lower p/m but highermortar content. The data indicate that mixtures having mortar contents of0.537 m3 (14.5 fte) and higher required less vibratory effort to consolidate.Lower p/m could be used while maintaining adequate slumps of 40 to 75 mm(1-1/2 to 3 in.). Paste-mortar ratios of approximately 0.45 to 0.46 appeared toresult in slumps between 40 and 75 mmn (1-1/2 to 3 in.).

Muxtures with 0.60 w/c. The data indicate that mixtures having mortarcontents of 0.515 min (13.9 ft') and less could be judged difficult to consolidatewhen the slump is less than 50 mm (2 in.). Higher p/m were necessary to reducethe Vebe time. While the higher p/m did not necessarily increase the watercontent above that of mixtures having higher mortar contents, the higher p/m didresult in higher slumps. From a visual observation, as was the case at a 0.50 w/c,the mixtures having a lower mortar content and higher p/m appeared to be "wet."Mortar coating the coarse aggregate particles had a noticeable water sheen. Yetthese mixtures could be more difficult to consolidate than other mixtures having alower p/m but higher mortar content. The data indicate that mixtures havingmortar contents of 0.526 e9 (14.2 ft3) and higher required less vibratory effort toconsolidate. Lower p/m could be used while maintaining adequate slumps of 40to 75 mm (1-1/2 to 3 in.). Paste-mortar ratios of approximately 0.43 to 0.44appeared to result in slumps between 40 and 75 mm (1-1/2 to 3 in.).

Overall. The data support the statement by ACI Committee 211 that aminimum mortar content is necessary for suitable workability and placeability.While Committee 211 was referring to 75-mm (3-in.) and 150-mm (6-in.) NMSAmass concrete mixtures, the above data suggest that the relationship is alsoapplicable for mass concrete mixtures containing 37.5-mm (1-1/2-in.) NMSA. Aswould be expected, there appears to be a direct relationship between slump andp/re. The resulting increase in water content with an increase in the p/m providesfor an increase in slump. However, the data point out that an increase in slump isnot always the most effective way to make a concrete mixture easier toconsolidate. Perhaps a more desirable approach would be to provide for anadequate proportion of mortar while holding the p/m to the minimum necessary toachieve the required slump at that mortar content. As shown in Figures 11and 12, the Vebe time required to consolidate a mixture at a constant slumpusually decreases as the mortar content increases. For w/c of 0.50 to 0.60, thedata suggest that a mortar content of 0.537 ± 0.007 m3 (14.5 ± 0.2 ft) might bean appropriate mortar content for suitable placing and workability properties in37.5-mm (1-1/2-in.) NMSA mass concrete. Lower mortar contents appear toresult in less workable concretes. Higher mortar contents can result inunnecessarily high cementitious contents. The p/m necessary to produce slumpsbetween 40 and 75 mm (1-1/2 to 3 in.) increased as the w/c decreased due to theincreased cementitious content.

26 Chapter 3 Discussion and Analysis

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Chapter 3 Discussion and Analysis 27

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Less favorable coarse aggregate particle shape

A total of 23 mixtures were evaluated as shown in Tables 5 and 7. Plots ofp/m versus Vebe time at each mortar content are shown in Figures 13 and 14 forw/c of 0.50 and 0.60, respectively. Slump values are superimposed on eachcurve at the appropriate location. As was the case with coarse aggregate having afavorable particle shape, the data indicate that for a given p/m, the Vebe timenecessary to consolidate the sample decreases as the mortar content increases. Acorresponding increase in slump is also indicated as the mortar content increased.For a given mortar content, the Vebe time necessary to consolidate the sampledecreases as the p/m increases, however it does not appear to be a linearrelationship. There appears to be a close relationship between the p/m and slump.Regardless of the mortar content, the slump increases as the p/m increases. Eachof these relationships between the mortar content, p/m, slump, and Vebe timewere expected. However, the data provide quantification the magnitude of therelationships.

Mixtures with 0.50 w/e. The data indicate that mixtures having mortarcontents of 0.537 e 3 (14.5 ft) and less could be judged difficult to consolidatewhen the slump is less than 50 mm (2 in.). Higher p/rn's were necessary toreduce the Vebe time. While the higher p/m did not necessarily increase thewater content above that of mixtures having higher mortar contents, the higherp/m did result in higher slumps. From a visual observation, the mixtures having alower mortar content and higher p/m appeared to be "wet." Mortar coating thecoarse aggregate particles had a noticeable water sheen. Yet these mixtures couldbe more difficult to consolidate than other mixtures having a lower p/m but highermortar content. The data indicate that mixtures having mortar contents of0.548 m` (14.8 fe) required less vibratory effort to consolidate. Mortar contentshigher than those examined in this investigation might have proved beneficial.Lower p/m could be used while maintaining adequate slumps of 40 to 75 mm(1-1/2 to 3 in.). Paste-mortar ratios of approximately 0.47 to 0.48 appeared toresult in slumps between 40 and 75 mm (1-1/2 to 3 in.).

Mixtures with 0.60 w/c. The data indicate that mixtures having mortarcontents of 0.526 mn (14.2 fte) and less could be judged difficult to consolidatewhen the slump is less than 50 mm (2 in.). Higher p/m's were necessary toreduce the Vebe time. While the higher p/m did not necessarily increase thewater content above that of mixtures having higher mortar contents, the higherp/m did result in higher slumps. From a visual observation, the mixtures having alower mortar content and higher p/m appeared to be 'wet." Mortar coating thecoarse aggregate particles had a noticeable water sheen. Yet these mixtures couldbe more difficult to consolidate than other mixtures having a lower p/m but highermortar content. The data indicate that mixtures having mortar contents of0.537 m3 (14.5 ft) and higher required less vibratory effort to consolidate.Mortar contents higher than those examined in this investigation might haveproved beneficial. Lower p/m's could be used while maintaining adequate slumpsof 40 to 75 mm (1-1/2 to 3 in.). Paste-mortar ratios of approximately 0.46 to0.47 appeared to result in slumps between 40 and 75 mm (1-1/2 to 3 in.).

Chapter 3 Discussion and Analysis 29

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Overall. The data describing mixtures having coarse aggregate with a lessfavorable particle shape support similar conclusions as those from mixtures havinga favorable particle shape. There are a few significant differences: (a) a highermortar content is indicated when the coarse aggregate particles have a lessfavorable shape, (b) an increase in mortar content or p/m does not have asdramatic an effect upon Vebe time or slump as is the case with the favorablyshaped coarse aggregate particles, (c) it was difficult to entrain the proper amountof air in mixtures having mortar contents less than 0.537 m'n (14.5 ft), and (d) ahigher p/m was required to produce slumps between 40 and 75 mm (1-1/2 to3 in.). As shown in Figures 15 and 16, the Vebe time required to consolidate amixture at a constant slump usually decreases as the mortar content increases.For w/c of 0.50 to 0.60, the data suggest that a mortar content of 0.548 ±0.007 m' (14.8 ± 0.2 fe) might be an appropriate mortar content for suitableplacing and workability properties in 37.5-mm (1-1/2-in.) NMSA mass concrete.Lower mortar contents appear to result in less workable concretes and possibledifficulty in entraining an appropriate amount of air. Higher mortar contents canresult in unnecessarily high cementitious contents. The p/m necessary to produceslumps between 40 and 75 mm (1-1/2 to 3 in.) increased as the w/c decreased dueto the increased cementitious content.

75-mm (3-in.) NMSA Mixtures

The modified vebe test procedure, which tested the concrete as mixed ratherthan wet-sieved portion, was unable to detect changes in the workablility of75-mm (3-in.) NMSA mass concrete mixtures as successfully as had been the casewith the 37.5-mm (1-112-in.) NMSA mass concrete mixtures. Changes inmixture proportions which should have affected the workability of the concretemixtures did not result in a change measurable by the test procedure. It appearsthat the mold size was not large enough to adequately test a representative sampleof the 75-mm (3-in.) NMSA mass concrete. Increasing the size further wouldhave required two people to handle the mold. Therefore, it was decided not topursue evaluation of the 75-mm (3-in.) NMSA mixtures. Test results for thethree mixtures that were evaluated are given in Table 8.

32V. [ f) o Chapter 3 Discussin and AnalVsis

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34 Chapter 3 Discussion and Analysis

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4 Conclusions andRecommendation

Conclusions

The data indicate that a recommended minimum and maximum mortar contentcould be a useful guide to aid in proportioning workable mass concrete mixturescontaining 37.5-mm NMS coarse aggregate. An approximate minimum andmaximum mortar content was identified for mixtures containing favorably shapedcoarse aggregate particles (primarily blocky with minimal flat and elongated) andfor mixtures containing less favorably shaped coarse aggregate particles (higherpercentage of flat and elongated). All mixtures contained natural fine aggregate.The following mortar contents are suggested for the initial proportioning ofmixtures having slumps of 55 ± 20 mm:

a. Favorably shaped crushed coarse aggregate: 0.537 ± 0.007 m3 (14.5 +0.2 f-t).

b. Less favorably shaped crushed coarse aggregate: increase the minimummortar content by 0.011 m3 (0.3 ft); i.e., 0.548 ± 0.007 n3 (14.8 ±0.2 fe).

These mortar contents appear to be appropriate for mixtures having w/c rangingfrom 0.50 to 0.60. Mixtures having w/c significantly higher or lower than thesecould require mortar contents outside the ranges suggested above. It is reasonableto expect that mortar contents similar to the minimum values suggested forfavorably shaped crushed coarse aggregate, or perhaps somewhat lower, would beappropriate for rounded natural coarse aggregate. It is also reasonable to expectthat higher mortar contents would be necessary if a manufactured fine aggregatewere being used. However, additional research will be necessary to confirm this.

The p/m does not appear to be as useful as the mortar content as a guide toassist in proportioning workable mass concrete mixtures containing 37.5-mmNMS coarse aggregate. The p/m appears to have more impact upon the slump ofthe mixture than upon the amount of vibratory effort required to consolidate theconcrete. The p/m appears to remain relatively constant for a given slump, w/c,

Chapter 4 Conclusions and Recommendation 35

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and type of coarse aggregate, even when the mortar content changes. When theslump increases or the w/c increases, the p/m will necessarily increase also. Itmay, however, be significant that a higher p/m was necessary when the coarseaggregates were less favorably shaped; i.e., those including more flat andelongated particles.

It should also be pointed out that when the coarse aggregate contains asignificant number of flat and elongated particles, it may not be possible toproportion a mixture whose workability will be as good as if the coarse aggregateparticles were more blocky. Even when the mortar content and the p/m wereincreased in the mixtures containing the less favorably shaped aggregate, theslump did not increase nor did the Vebe time decrease as much as when similarchanges were made to the mixtures containing favorably shaped coarse aggregateparticles. EM 1110-2-2000, "Standard Practice for Concrete for Civil WorksStructures," (Headquarters, Department of the Army 1994) states in paragraph2.3, that

"Excessive amounts of flat or elongated particles, or both, inaggregates will severely affect the water demand and finishability.In mass concrete structures, the amount of flat or elongatedparticles, or both, at a 3:1 length-to-width ratio or width-to-thicknessratio is limited to 25 percent in any size group of coarse aggregates."

In view of the data presented in this investigation, this appears to be prudentguidance.

Recommendation

SEM 1110-2-2000, "Standard Practice for Concrete for Civil WorksStructures," (Headquarters, Department of the Army 1994) states in paragraph4.1, that "Proportions for mass concrete or structural concrete are to be selectedin accordance with ACI 211.1 (ACI 1993b) (CRD-C 99) (USAEWES 1949) andother criteria as described in the following paragraphs of this chapter whether thework is done by the Government or the Contractor." It is recommended thatconsideration be given to revising current guidance by adding a subparagraph toparagraph 4.3, "Criteria for Mixture Proportioning," which states the following:

"For mass concretes containing 150-mm (6-in.) and 75-mm (3-in.) NMSA,mortar contents within the range recommended by ACI 211.1 (CRD-C 99) aresuggested for initial mixture proportions. For mass concretes containing 37.5-mm(1½-in.) NMSA, the following mortar contents are suggested for initial mixtureproportions.

a. Primarily blocky shaped crushed coarse aggregate: 0.537 ± 0.007 m3(14.5 ± 0.2 fe).

36 Chapter 4 Conclusions and Recommendation

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b. Crushed coarse aggregate with higher percentages of flat and elongatedparticles: 0.548 ± 0.007 m3 (14.8 ± 0.2 ft3).

These mortar contents appear to be appropriate for mixtures having w/c rangingfrom 0.50 to 0.60 and slumps of 55 ± 20 mm when natural fine aggregates arebeing used. Mixtures having w/c or slumps significantly higher or lower thanthese could require mortar contents outside the ranges suggested above. Use of amanufactured fine aggregate could require mortar contents above the rangessuggested above."

Chapter 4 Conclusions and Recommendation 37

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References

American Concrete Institute Committee 207. (1993a). "Roller compacted massconcrete." ACI manual of concrete practice, Part 1. ACI 207.5R-89,American Concrete Institute, Detroit, MI.

American Concrete Institute Committee 211. (1993b). "Standard practice forselecting proportions for normal, heavyweight, and mass concrete." ACImanual of concrete practice, Part 1. ACI 211.1-91, American ConcreteInstitute, Detroit, MI.

American Concrete Institute Committee 304. (1993c). "Guide for measuring,mixing, transporting, and placing concrete." ACI manual of concretepractice, Part 2. Report Number 304R-89, American Concrete Institute,Detroit, MI.

American Concrete Institute Committee 304. (1993d). Placing concrete with beltconveyors." ACI manual of concrete practice, Part 2. ReportNumber 304.4R-89, American Concrete Institute, Detroit, MI.

American Concrete Institute Committee 309. (1993e). "Guide for consolidationof concrete." AC! manual of concrete practice, Part 2. Report Number309R-87, American Concrete Institute, Detroit, MI.

American Concrete Institute Committee 311. (1992). ACI manual of concreteinspection. Publication SP-2(92), 8th ed., American Concrete Institute,Detroit, MI.

American Society for Testing and Materials. (1993). 1993 Annual Book of ASTMStandards. Philadelphia, PA.

a. Designation C 127-88. "Standard test method for specific gravity andabsorption of coarse aggregate."

b. Designation C 128-88. "Standard test method for specific gravity andabsorption of fine aggregate."

38References

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c. Designation C 136-84. "Standard method for sieve analysis of fine andcoarse aggregate."

d. Designation C 138-81. "Standard test method for unit weight, yield, andair content (gravimetric) of concrete."

e. Designation C 143-90. "Standard test method for slump of portlandcement concrete."

f. Designation C 150-92. "Standard specification for portland cement."

g. Designation C 172-90. "Standard practice for sampling freshly mixedconcrete."

h. Designation C 231-89a. "Standard test method for air content of freshlymixed concrete by the pressure method."

i. Designation C 232-87. "Standard test methods for bleeding of concrete."

j. Designation C 311-92. "Standard test method for sampling and testing flyash or natural pozzolans for use as a mineral admixture in portlandcement concrete."

k. Designation C 618-92. "Standard specification for coal fly ash and raw orcalcined natural pozzolan for use as a mineral admixture in portlandcement concrete."

1. Designation D 4791-89. "Standard test method for flat or elongatedparticles in coarse aggregate."

m. Designation E 380-9 1. "Standard practice for the use of the internationalsystem of units."

British Standards Institute. (1983). "Standard method for determination of vebetime." Testing Concrete. BS 1881: Part 104, London, England.

Fuller, W. B., and Thompson, S. E. (1907). "The laws of proportioningconcrete," Transactions, American Society of Civil Engineers 59, 76-143.

Headquarters, Department of the Army. (1992). "Mass concrete," Civil WorksConstruction Guide Specification CWGS-03305, Washington, D.C.

(1994). "Standard practice for concrete for civil works structures,"Engineer Manual 1110-2-2000, Washington, D.C.

Kosmatka, Steven H., and Panarese, William C. (1988). Design and control ofconcrete mixtures. 13th ed., Portland Cement Association, Skokie, IL.

References 39

Page 47: by Billy D. Neeley, Michael K. Lloyd · the Portland Cement Association (PCA), and the CE to assist the contractor in completing a successful placement: Aggregate gradings - "Mass

Neeley, Billy D. (1993). "Assessing workability complaints in mass concreteconstruction," Miscellaneous Paper SL-93-1, U.S. Army Engineer WaterwaysExperiment Station, Vicksburg, MS.

Plum, N. M. (1950). "The predetermination of water requirement and optimumgrading of concrete," Building Research Studies No. 3, The Danish NationalInstitute of Building Research, Copenhagen, Denmark.

Tynes, William 0. (1968). "Effect of fineness of continuously graded coarseaggregate on properties of concrete," Technical Report No. 6-819, U.S. ArmyEngineer Waterways Experiment Station, Vicksburg, MS.

U.S. Army Engineer Waterways Experiment Station. (1949). Handbook forconcrete and cement (with quarterly supplements), Vicksburg, MS.

40 References

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Appendix ARecent Mass ConcreteMixture Information

Calion L&D Calion Lock and Dam, Ouachita River, ArkansasClarence Cannon Clarence Cannon Dam, Salt River, MissouriCRGNT Crushed granite coarse aggregateCRLS Crushed limestone coarse aggregateL&D 26 - 1st Stage Lock and Dam No. 26, 1st Stage, Mississippi River,

MissouriL&D 26 - 2nd Stage Lock and Dam No. 26, 2nd Stage, Mississippi River,

MissouriMelvin Price L&D Melvin Price Lock and Dam, Mississippi River,

MissouriMLS Manufactured limestone fine aggregateNatural Natural sand fine aggregateNG Natural gravel coarse aggregateOverton L&D Overton Lock and Dam, Red River, LouisianaRed River #3 Lock and Dam No. 3, Red River, LouisianaRed River #4 Lock and Dam No. 4, Red River, LouisianaRed River #5 Lock and Dam No. 5, Red River, LouisianaRed River TS Thermal Study, Red River Locks and Dams, LouisianaTensas Cocodrie Tensas Cocodrie Pumping Plant, Louisiana

Appendix A Recent Mass Concrete Mixture Information Al

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A2 Appendix A Recent Mass Concrete Mixture Information

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A4 Ap eni A Re en Mas Co crt Fitr NnfNrNaNiN

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Appendix A Recent Mass Concrete Mixture Information A5

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A6 Appendix A Recent Mass Concrete Mixture Information

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0.600 . . . . .

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WATER/CEMENT

Z GRNT 4. GRNT/GVL A LS in GVL

Figure Al. Mortar content of 37.5-mm NMSA mass concrete mixturesreviewed for historical data

0.560 -____ ____ ____- - - - - -

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0.25 0.30 0.35 0.40 0.45 0.50 0.55 0.60 0.65 0.70 0.75WATER/CEMENT

X CRGNT + CRGNT/NG A CRLS in NG

Figure A2. Paste/mortar of 37.5-mm NMSA mass concrete mixtures reviewedfor historical data

A8Appendix A Recent Mass Concrete Mixture Information

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0.560-

0 .540 ............:..... ..

AA

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4..

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0.400 r i0.490 0.500 0.510 0.520 0.530 0.540 0.550 0.560 0.570

VOLUME OF MORTAR, cu mX CRGNT .4- CRGNTING A CRLS 0 NG

Figure A3. Relationship of mortar content to paste/mortar of 37.5-mm NMSAmass concrete mixtures reviewed for historical data

0.470- . . .

E 0.465 . ........ ............ ................

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0.520

0 .5 0 0 . ................ ................ .................. I................ ............................ ..................................... .................

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0.400I I

0.44 0.445 0.45 0.455 0.46 0.465 0.47 0.475 0.48 0.485

VOLUME OF MORTAR, cu m

Figure A5. Paste/mortar of 75-mm NMSA mass concrete mixtures reviewedfor historical data

0.470 .

0.465 .......... ...

0 .4 6 0 . ..............0.............. .............. ............... . .............. .. . ........ ................. ............

cc< 0 .4 5 5 . .............. ........ .......... . . . . . .. . . . . . . .!. . .......................... .................. ............ ................ ..............< 0.455" i

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0 .4 3 0 1 .............. ............... ...............- -.............. ............... i.............. ................ .............. ................ I...............

0.425i

0.25 0.30 0.35 0.40 0.45 0.50 0.55 0.60 0.65 0.70 0.75

WATER/CEMENTI C S I

Figure A6. Relationship of mortar contents to paste/mortar of 75-mm NMSAmass concrete mixtures reviewed for historical data

A10Appendix A Recent Mass Concrete Mixture Information

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Appendix BModified Vebe TestProcedure for Mass ConcreteMixtures

The modified list procedure presented below is patterned after the BritishStandard Method for Determination of Vebe Time (BS 1881: Part 104) BritishStandards Institute 1983).'

1. Scope

1.1 This method describes a procedure for determining the consistency ofmass concrete mixtures and is applicable in both the laboratory and the field. It isintended to supplement the slump test.

1.2 This method is considered applicable to concrete containing 50-mm(2-in.) nominal maximum size aggregate or smaller.

2. Applicable Documents

2.1 ASTM StandardsC 143 (ASTM 1993e)1 Method for Slump of Hydraulic Cement

Concrete (CRD-C 5)2

C 172 (ASTM 1993g)' Method of Sampling Freshly MixedConcrete (CRD-C 4)

C 231 (ASTM 1993h)1 Method for Air Content of Freshly MixedConcrete by the Pressure Method (CRD-C 41)

2 References are listed following main text.2 CRD-C equivalents in parentheses are from the Handbook for Concrete and Cement,

U.S. Army Engineer Waterways Experiment, 1949, Vicksburg, MS.

Appendix B Modified Vebe Test Procedure for Mass Concrete Mixtures B1

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2.2 American Concrete Institute StandardACI 211 Standard Practice for selecting proportions for normal,

heavyweight, and mass concrete (CRD-D 99)

2.3 British Standard

BS 1881: Part 104: 1983 Method for Determination of Vebe Time

3. Summary of Method

3.1 This method provides a measure of the consistency of mass concretemixtures. The consistency is measured as the time required to remold andconsolidate a given volume of concrete in a cylindrical mold using externalvibration.

3.2 This method tests a larger sample of concrete than does the BritishStandard 1881, "Method for Determination of Vebe Time."

4. Apparatus

4.1 Cylindrical Mold - The cylindrical mold shall have an inside diameter of356 ± 3 mm and a height of 286 ± 3 mm. The volume of the sample containershall be approximately 0.028 cu m. The cylindrical mold shall be capable ofbeing rigidly clamped to a vibrating table. The top rim of the mold shall besmooth, plane, and parallel to the bottom of the mold.

4.2 Conical Mold - The conical mold shall be 305 ± 3 mm at the base,152 ± 3 mm at the top, and 457 ± 3 mm high. The base and top shall be openand parallel to each other and at right angles to the axis of the cone. The interiorof the cone shall be relatively smooth and free from projections or dents. Theconical mold shall have a clamp which is capable of holding the mold firmly inplace while filling.

4.3 Tamping Rod - The tamping rod shall be a round, straight steel rod16-mm in diameter and approximately 900-mm in length, having the tamping endrounded to a hemispherical tip the diameter of which is 16-mm.

4.4 Surcharge - The surcharge shall be a circular acrylic plate 330 ± 3 mmin diameter and 13 ± 1 mm thick.

4.5 Vibrating Table - A steel vibrating table shall be clamped to a levelconcrete floor or base slab having a mass of at least 50 kg to avoid movementduring vibration. The vibrating table shall produce a sinusoidal vibratory motionwith a frequency of 60 ± 1.7 Hz and an amplitude of 0.70 ± 0.08 mm.

4.6 Miscellaneous Equipment - Also required are a shovel, scoop, andstopwatch.

B2 Appendix B Modified Vebe Test Procedure for Mass Concrete Mixtures

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5. Sampling

5.1 Samples of freshly mixed concrete shall be taken in accordance withASTM C 172.

6. Procedure

6.1 Obtain a representative sample of freshly mixed concrete in accordancewith ASTM C 172, having a minimum mass of 100 kg.

6.2 Remix the sample carefully with a shovel to correct for any segregationthat may exist.

6.3 Dampen the cylindrical and the conical mold. Clamp the cylindrical moldonto the vibrating table. Place the conical mold into the cylindrical mold andclamp into place. From the sample of concrete obtained in accordance withSection 6, immediately fill the conical mold in three layers, each approximatelyone third the volume of the mold.

6.4 Rod each layer with 50 strokes of the tamping rod. Uniformly distributethe strokes over the cross section of each layer. For the bottom layer this willnecessitate incling the rod slightly and making approximately half of the strokesnear the perimeter, and then progressing with vertical strokes spirally toward thecenter. Rod the bottom layer throughout its depth. Rod the second layer and thetop layer each throughout its depth, so that the strokes just penetrate into theunderlying layer.

6.5 In filling and rodding the top layer, heap the concrete above the moldbefore the rodding is started. If the rodding operation results in subsidence of theconcrete below the top edge of the mold, add additional concrete to keep anexcess of concrete above the top of the mold at all times. After the top layer hasbeen rodded, strike off the surface of the concrete by means of a screeding androlling motion of the tamping rod. Carefully remove any excess concrete thatmay have fallen from the top of the cone to the outside of its base inside thecylindrical mold.

6.6 Loosen the clamps holding the conical mold to the cylindrical mold andimmediately remove the conical mold from the concrete by raising it carefully in avertical direction with a steady upward lift with no lateral or torsional motion.The conical mold should be completely removed from the concrete in 5 ±2 seconds.

6.7 Place the surcharge on the sample of concrete so that it is centered overthe cylindrical mold.

6.8 Turn the vibrating table on and begin timing the test. Observe theconcrete underneath the surcharge and around the edge of the surcharge. As thetest progresses, mortar will cover the bottom of the surcharge and migratebetween the surcharge and the wall of the mold. When the bottom of the

Appendix B Modified Vebe Test Procedure for Mass Concrete Mixtures B3

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surcharge has been completely covered with mortar and a ring of mortar hasformed around the periphery of the surcharge, stop the test and determine theelapsed time to the nearest second. Record this as the Vebe Time.

7. Report

7.1 Report the Vebe Time to the nearest second.

8. Precision and Bias

8.1 Precision - The precision of this test method has not been determined.

8.2 Bias - This test method has no bias since Vebe Time is defined only interms of this test method.

B4 Appendix B Modified Vebe Test Procedure for Mass Concrete Mixtures

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REPORT DOCUMENTATION PAGE Form ApprovedOMB No. 0704-0188

Public reporting burftn for this collection of information is estimated to average I hour per response, including the time for reviewing instructions, searching existing data sources, gathering and maintainingthe data needed, and completing and reviewing the collection of information. Send comments regarding this burden estimate or any other aspect of this collection of information, including suggestionsfor reducing this burden, to Washington Headquarters Services, Directorate for Information Operations and Reports, 1215 Jefferson Davis Highway, Suite 1204, Arlington, VA 22202-4302, and to theOffice of Management and Budget, Paperwork Reduction Project (0704-0188), Washington, DC 20503.

1. AGENCY USE ONLY (Leave blank) 2. REPORT DATE 3. REPORT TYPE AND DATES COVEREDSeptember 1996 Report 2 of a Series

4. TITLE AND SUBTITLE 5. FUNDING NUMBERSWorkability of Mass Concrete

Report 2, Supplemental Proportioning Parameters

6. AUTHOR(S)Billy D. Neeley, Michael K. Lloyd

7. PERFORMING ORGANIZATION NAME(S) AND ADDRESS(ES) 8. PERFORMING ORGANIZATION

U.S. Army Engineer Waterways Experiment Station REPORT NUMBER

3909 Halls Ferry Road, Vicksburg, MS 39180-6199 Technical Report SL-96-15

9. SPONSORING/MONITORING AGENCY NAME(S) AND ADDRESS(ES) 10. SPONSORING/MONITORING

Headquarters, U.S. Army Corps of Engineers AGENCY REPORT NUMBER

Washington, D.C. 20310-0000

11. SUPPLEMENTARY NOTES

Available from National Technical Information Service, 5285 Port Royal Road, Springfield, VA 22161.

12a. DISTRIBUTIONWAVAILABILITY STATEMENT 12b. DISTRIBUTION CODE

Approved for public release; distribution is unlimited.

13. ABSTRACT (Maximum 200 words)

This report presents the results of a research program examining the potential benefits of requiring minimum and

maximum mortar contents for 37.5-mm (1-1/2-in.) nominal maximum size aggregate (NMSA) mass concrete and minimumand maximum paste-mortar ratios for 37.5-mm (1-1/2-in.) NMSA mass concrete. The purpose of the research program wasto supplement existing guidance on proportioning mass concrete mixtures.

Two 37.5-mm (1-1/2-in.) nominal maximum size (NMS) coarse aggregates were used. One was a crushed materialconsisting primarily of blocky particles. The other was a crushed material having more flat and elongated particles. All

mixtures contained natural fine aggregate.

The results indicate that a recommended minimum and maximum mortar content could be a useful guide to aid inproportioning workable mass concrete mixtures containing 37.5-mm (1-1/2-in.) NMS coarse aggregate. An approximate

minimum and maximum mortar content was identified for mixtures containing favorably shaped coarse aggregate particles(primarily blocky with minimal flat and elongated) and for mixtures containing less favorably shaped coarse aggregate

particles (higher percentage of flat and elongated). The paste-mortar ratio appears to be less useful.

Recommendations are made to consider supplementing existing guidance on proportioning 37.5-mm (1-1/2-in.) NMSA

mass concrete mixtures with minimum and maximum mortar contents.

14. SUBJECT TERMS 15. NUMBER OF PAGES

Concrete Mass concrete 60Concrete aggregates Mortar content 16. PRICE CODE

Concrete workability Paste-mortar ratio

17. SECURITY CLASSIFICATION 18. SECURITY CLASSIFICATION 19. SECURITY CLASSIFICATION 20. UMITATION OF ABSTRACTOF REPORT OF THIS PAGE OF ABSTRACT

UNCLASSIFIED UNCLASSIFIEDNSN 7540-01-280-5500 Standard Form 298 (Rev. 2-89)

Prescribed by ANSI Std. Z39-1B298-102