case study: resin reactor vent analysis

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Consultancy. Project Delivery. Innovation. Case Study: Resin Reactor Vent Analysis Detailed assessment of reacting two-phase relief Client: Top Tier COMAH Phenolic Resin Manufacturer

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Page 1: Case Study: Resin Reactor Vent Analysis

Consultancy.

Project Delivery.

Innovation.

Case Study: Resin Reactor Vent Analysis

Detailed assessment of reacting two-phase relief

Client: Top Tier COMAH Phenolic Resin Manufacturer

Page 2: Case Study: Resin Reactor Vent Analysis

Who are we?

Process engineering consultancy

Specialising in advanced modelling techniques, to give answers that

are more accurate, reliable and robust

Decades of process and mechanical engineering experience

Combine cutting edge simulation with real world understanding, to

provide you with solutions that are effective and practical.

Core team of eight engineers, supported by a wide network of

associates.

Page 2

Page 3: Case Study: Resin Reactor Vent Analysis

Project Background

Top tier COMAH site

HSE Regulator questions mechanical integrity of reactor emergency vent

system to withstand a full relief event

Original mechanical calculations no longer available

No process flows to support pipe work dynamic assessment, likely to be

two phase reacting flow

Client no longer has access to internal process/mechanical expertise

Flex Process brought in to help address HSE action

Page 3

Page 4: Case Study: Resin Reactor Vent Analysis

Our Responsibilities

Page 4

Site Survey of vessels, pipes and catchment tank

Complete two phase relief calculations to generate process flows

Build pipe stress models for each reactor system and assess against

pipe code (ASME) for thermal, sustained and dynamic cases

Complete vessel nozzle strength calculations

Report findings and agree way forward

Page 5: Case Study: Resin Reactor Vent Analysis

Site Survey

Page 5

General Arrangement

Drawing

Site Measurements

Research Site Data

Records

Page 6: Case Study: Resin Reactor Vent Analysis

Two Phase Flow Modelling

Use own in-house DIERS based software to calculate two

phase flow through vent lines

Use detailed mechanical survey data

Use physical properties for phenol, water, formaldehyde, resin in

calculations

Input actual calorimetry data

Worst case static or dynamic flow outputs

Flows, temperatures and pressures at various points within vent system

to support detailed pipe stress modelling

Page 6

Page 7: Case Study: Resin Reactor Vent Analysis

Process Data Output

Page 7

Page 8: Case Study: Resin Reactor Vent Analysis

Pipe Stress Engineering

Page 8

CAESAR II Simulations

Page 9: Case Study: Resin Reactor Vent Analysis

Main Conclusions

Significant deviations in thermal, sustained and dynamic cases from the

ASME design code. Simple changes not possible.

Original designs had limited pipe stress analysis, some were site run

Insufficient allowance for pipe thermal expansion (e.g. straight runs)

Incorrectly specified pipe bellows

Insufficient pipe supports for dynamic loads, such as disk rupture

Weak nozzles on heat exchangers, reactors and catchment tank

No supporting calculations for catchment tank foundations

Page 9

Page 10: Case Study: Resin Reactor Vent Analysis

Proposal for Redesign

Redesign vent pipe runs to allow for thermal expansion, minimise

bellows on wetted duty

Install new pipe bellows designed to withstand movement on reactor

nozzles

Change heat exchanger heads with stronger nozzles

Install special pipe supports to withstand dynamic loads

Change catchment tank instead of making repairs to weak nozzles and

adopt new centrifugal design for more effective separation

Page 10

Page 11: Case Study: Resin Reactor Vent Analysis

Redesign Proposal

Page 11

Detailed Proposal DrawingsNew Vessel General Arrangement Drawings

Page 12: Case Study: Resin Reactor Vent Analysis

Redesign, Estimate and Programme

Redesign proposal developed in drawings incorporating all the required

changes

Fully checked out proposals through additional site survey, pipe stress

analysis and two phase relief calculations to ensure that relief capacity

not compromised

New, more flexible pipe specification developed that minimises the

requirement for bellows

Detailed capital cost estimate for changes

Installation programme developed, which minimises disruption to

operations

Suggestions made to optimise vent size through further scenario

analysis

Page 12

Page 13: Case Study: Resin Reactor Vent Analysis

Summary

Client had a complex problem involving the HSE

Through a mix of process and mechanical in-house expertise, the

analysis could be completed effectively

Findings were clearly reported and a way forward discussed

Fully checked out redesign completed, costed and installation

programme devised that minimised disruption

Deliverables produced that could be used to support discussions with

HSE regulator

Page 13

Page 14: Case Study: Resin Reactor Vent Analysis

Summary

Page 14

Consultancy.

Project Delivery.

Innovation.

Please get in touch to find out how we can help your

business today.

E: [email protected] W: flexprocess.co.uk

T: +44 1454 629 689