certificate of analysis
TRANSCRIPT
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
08/13/21
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, US
Kaycha LabsOriginal Blueberry 1.5g Pre-Roll
Original BlueberryMatrix: Flower
Certificateof Analysis
Sample:DA10810003-005Harvest/Lot ID: 4258 5425 8382 0926
Cultivation Facility: Tampa CultivationProcessing Facility : Tampa Processing
Seed to Sale# 4258 5425 8382 0926Batch Date: 07/23/21
Batch#: 1829 2772 6022 6080Sample Size Received: 27 gram
Total Weight/Volume: 1214 unitsRetail Product Size: 1.5 gram
Ordered : 08/09/21sampled : 08/09/21
Completed: 08/13/21Sampling Method: SOP.T.20.010
Aug 13, 2021 | FLUENT82 NE 26th streetMiami, FL, 33137, US
PASSEDPage 1 of 4
PRODUCT IMAGE SAFETY RESULTS MISC.
PesticidesPASSED
Heavy MetalsPASSED
MicrobialsPASSED
MycotoxinsPASSED
ResidualsSolvents
NOT TESTED
FilthPASSED
Water ActivityPASSED
MoisturePASSED
TerpenesTESTED
CANNABINOID RESULTS
Total THC
15.703%TOTAL THC/Container :235.557mg
Total CBD
0.044%TOTAL CBD/Container :0.670 mg
Total Cannabinoids
18.365%Total Cannabinoids/Container:275.475 mg
CBDV CBDA CBGA CBG CBD THCV CBN D9-THC D8-THC CBC THCA
% ND 0.0509 0.3530 0.0709 ND ND ND 0.4089 0.0410 ND 17.4400
mg/g ND 0.5100 3.5300 0.7100 ND ND ND 4.0900 0.4100 ND 174.4000
LOD 0.0010 0.0010 0.0010 0.0010 0.0001 0.0010 0.0010 0.0001 0.0010 0.0010 0.0010
% % % % % % % % % % %
Cannabinoid Profile TestAnalyzed by Weight Extraction date : Extracted By :450 0.2305g 08/10/21 01:08:07 2076Analysis Method -SOP.T.40.020, SOP.T.30.050 Reviewed On - 08/11/21 10:54:05 Batch Date : 08/10/21 10:06:48Analytical Batch -DA029737POT Instrument Used : DA-LC-002 Running On : 08/11/21 10:01:38
Reagent Dilution Consums. ID
081021.R50 400 CE0123070621.19 287035261081021.R52 11945-019CD-019C
914C4-914AK929C6-929H
Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 for sample prep andShimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L).
Filth PASSEDAnalyzed By Weight Extraction date Extracted By1879 NA 08/10/21 1879Analyte LOD ResultFilth and Foreign Material 0.1 NDAnalysis Method -SOP.T.40.013 Batch Date : 08/10/21 11:21:52Analytical Batch -DA029752FIL Reviewed On - 08/10/21 17:04:38Instrument Used : Filth/Foreign Material Microscope
This includes but is not limited to hair, insects, feces, packaging contaminants, and manufacturing wasteand by-products. An SH-2B/T Stereo Microscope is use for inspection.
Water Activity PASSEDAnalyte Analyzed by Weight Ext. date LOD A.L ResultWATER ACTIVITY 457 NA 08/10/21 0.01 aw 0.65aw 0.471aWAnalysis Method -Water ActivitySOP.T.40.010 Batch Date : 08/10/21 11:19:38Analytical Batch -DA029751WAT Reviewed On - 08/11/21 09:21:45Instrument Used : DA-028 Rotronic Hygropalm
Moisture PASSEDAnalyte Analyzed by Weight Ext. date LOD A.L ResultMOISTURE CONTENT 1879 0.495g 08/10/21 1 % 15% 9.900%
Analysis Method -MoistureAnalysis SOP.T.40.011 Batch Date : 08/10/21 11:18:56Analytical Batch -DA029750MOI Reviewed On - 08/10/21 17:11:01Instrument Used : DA-003 Moisture Analyzer
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
08/13/21
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, US
Kaycha LabsOriginal Blueberry 1.5g Pre-Roll
Original BlueberryMatrix : Flower
Certificate of Analysis PASSED
82 NE 26th streetMiami, FL, 33137, USTelephone: (305) 900-6266Email: [email protected]
Sample : DA10810003-005Harvest/LOT ID: 4258 5425 8382 0926Batch# : 1829 27726022 6080Sampled : 08/09/21Ordered : 08/09/21
Sample Size Received : 27 gramTotal Weight/Volume : 1214 unitsCompleted : 08/13/21Expires: 08/13/22Sample Method : SOP.T.20.010
Page 2 of 4
Terpenes TESTEDTerpenes LOD(%) mg/g % Result (%)
TOTAL TERPINEOL 0.007 ND NDCAMPHENE 0.007 ND NDBETA-MYRCENE 0.007 2.854 0.285ALPHA-PHELLANDRENE 0.007 ND ND3-CARENE 0.007 ND NDOCIMENE 0.007 ND NDEUCALYPTOL 0.007 ND NDLINALOOL 0.007 0.273 0.027FENCHONE 0.007 ND NDISOPULEGOL 0.007 ND NDISOBORNEOL 0.007 ND NDHEXAHYDROTHYMOL 0.007 ND NDNEROL 0.007 ND NDGERANYL ACETATE 0.007 ND NDBETA-CARYOPHYLLENE 0.007 1.996 0.199VALENCENE 0.007 ND NDCIS-NEROLIDOL 0.007 ND NDCARYOPHYLLENE OXIDE 0.007 ND NDCEDROL 0.007 ND NDFARNESENE 0.007 0.315 0.031ALPHA-BISABOLOL 0.007 0.322 0.032ALPHA-PINENE 0.007 1.094 0.109SABINENE 0.007 ND NDBETA-PINENE 0.007 ND NDALPHA-TERPINENE 0.007 ND NDLIMONENE 0.007 0.729 0.072GAMMA-TERPINENE 0.007 ND NDTERPINOLENE 0.007 ND NDSABINENE HYDRATE 0.007 ND NDFENCHYL ALCOHOL 0.007 ND NDCAMPHOR 0.013 ND ND
Terpenes LOD(%) mg/g % Result (%)
BORNEOL 0.013 ND NDGERANIOL 0.007 ND NDPULEGONE 0.007 ND NDALPHA-CEDRENE 0.007 ND NDALPHA-HUMULENE 0.007 0.526 0.052TRANS-NEROLIDOL 0.007 ND NDGUAIOL 0.007 ND ND
Terpenes TESTED
Analyzed by Weight Extraction date Extracted By1082 1.0133g 08/10/21 12:08:02 1082
Analysis Method -SOP.T.40.090Analytical Batch -DA029685TER Reviewed On - 08/11/21 11:14:35Instrument Used : DA-GCMS-005Running On : 08/09/21 16:12:03Batch Date : 08/09/21 09:22:41
Reagent Dilution Consums. ID
061821.08 10 CE0123CE012313898901
Terpenoid profile screening is performed using GC-MS/MS TQ-8040 with Liquid Injection(Gas Chromatography – Mass Spectrometer Triple Quad) which can screen 37 terpenesusing Method SOP.T.40.090 Terpenoid Analysis Via GC-MS/MS.
Total (%) 0.811
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
08/13/21
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, US
Kaycha LabsOriginal Blueberry 1.5g Pre-Roll
Original BlueberryMatrix : Flower
Certificate of Analysis PASSED
82 NE 26th streetMiami, FL, 33137, USTelephone: (305) 900-6266Email: [email protected]
Sample : DA10810003-005Harvest/LOT ID: 4258 5425 8382 0926Batch# : 1829 27726022 6080Sampled : 08/09/21Ordered : 08/09/21
Sample Size Received : 27 gramTotal Weight/Volume : 1214 unitsCompleted : 08/13/21Expires: 08/13/22Sample Method : SOP.T.20.010
Page 3 of 4
Pesticides PASSEDPesticides LOD Units Action Level ResultABAMECTIN B1A 0.01 ppm 0.1 NDACEPHATE 0.01 ppm 0.1 NDACEQUINOCYL 0.01 ppm 0.1 NDACETAMIPRID 0.01 ppm 0.1 NDALDICARB 0.01 ppm 0.1 NDAZOXYSTROBIN 0.01 ppm 0.1 NDBIFENAZATE 0.01 ppm 0.1 NDBIFENTHRIN 0.01 ppm 0.1 NDBOSCALID 0.01 PPM 0.1 NDCARBARYL 0.05 ppm 0.5 NDCARBOFURAN 0.01 ppm 0.1 NDCHLORANTRANILIPROLE 0.1 ppm 1 NDCHLORMEQUAT CHLORIDE 0.1 ppm 1 NDCHLORPYRIFOS 0.01 ppm 0.1 NDCLOFENTEZINE 0.02 ppm 0.2 NDCOUMAPHOS 0.01 ppm 0.1 NDDAMINOZIDE 0.01 ppm 0.1 NDDIAZINON 0.01 ppm 0.1 NDDICHLORVOS 0.01 ppm 0.1 NDDIMETHOATE 0.01 ppm 0.1 NDETHOPROPHOS 0.01 ppm 0.1 NDETOFENPROX 0.01 ppm 0.1 NDETOXAZOLE 0.01 ppm 0.1 NDFENHEXAMID 0.01 ppm 0.1 NDFENOXYCARB 0.01 ppm 0.1 NDFENPYROXIMATE 0.01 ppm 0.1 NDFIPRONIL 0.01 ppm 0.1 NDFLONICAMID 0.01 ppm 0.1 NDFLUDIOXONIL 0.01 ppm 0.1 NDHEXYTHIAZOX 0.01 ppm 0.1 NDIMAZALIL 0.01 ppm 0.1 NDIMIDACLOPRID 0.04 ppm 0.4 NDKRESOXIM-METHYL 0.01 ppm 0.1 NDMALATHION 0.02 ppm 0.2 NDMETALAXYL 0.01 ppm 0.1 NDMETHIOCARB 0.01 ppm 0.1 NDMETHOMYL 0.01 ppm 0.1 NDMEVINPHOS 0.01 ppm 0.1 NDMYCLOBUTANIL 0.01 ppm 0.1 NDNALED 0.025 ppm 0.25 NDOXAMYL 0.05 ppm 0.5 NDPACLOBUTRAZOL 0.01 ppm 0.1 NDPHOSMET 0.01 ppm 0.1 NDPIPERONYL BUTOXIDE 0.3 ppm 3 NDPRALLETHRIN 0.01 ppm 0.1 NDPROPICONAZOLE 0.01 ppm 0.1 ND
Pesticides LOD Units Action Level ResultPROPOXUR 0.01 ppm 0.1 NDPYRETHRINS 0.05 ppm 0.5 NDPYRIDABEN 0.02 ppm 0.2 NDSPIROMESIFEN 0.01 ppm 0.1 NDSPIROTETRAMAT 0.01 ppm 0.1 NDSPIROXAMINE 0.01 ppm 0.1 NDTEBUCONAZOLE 0.01 ppm 0.1 NDTHIACLOPRID 0.01 ppm 0.1 NDTHIAMETHOXAM 0.05 ppm 0.5 NDTOTAL CONTAMINANT LOAD(PESTICIDES)
0.05 PPM 5 ND
TOTAL DIMETHOMORPH 0.02 PPM 0.2 NDTOTAL PERMETHRIN 0.01 ppm 0.1 NDTOTAL SPINETORAM 0.02 PPM 0.2 NDTOTAL SPINOSAD 0.01 ppm 0.1 NDTRIFLOXYSTROBIN 0.01 ppm 0.1 NDPENTACHLORONITROBENZENE (PCNB)*
0.01 PPM 0.15 ND
PARATHION-METHYL * 0.01 PPM 0.1 NDCAPTAN * 0.025 PPM 0.7 NDCHLORDANE * 0.01 PPM 0.1 NDCHLORFENAPYR * 0.01 PPM 0.1 NDCYFLUTHRIN * 0.01 PPM 0.5 NDCYPERMETHRIN * 0.01 PPM 0.5 ND
Pesticides PASSED
Analyzed by Weight Extraction date Extracted By585 , 1665 0.9854g 08/10/21 02:08:41 2651 , 2651Analysis Method - SOP.T.30.065, SOP.T.40.065, SOP.T.40.066, SOP.T.40.070 , SOP.T.30.065,SOP.T40.070Analytical Batch - DA029728PES , DA029723VOL Reviewed On- 08/10/21
17:04:38Instrument Used : DA-LCMS-003 (PES) , DA-GCMS-001Running On : 08/11/21 16:18:22 Batch Date : 08/10/21 09:56:24
Reagent Dilution Consums. ID080921.R12 25 6524407-03080521.R32080921.R33092820.59081121.R01
Pesticide screen is performed using LC-MS and/or GC-MS which can screen down to below single digit ppbconcentrations for regulated Pesticides. Currently we analyze for 67 Pesticides. (Method: SOP.T.30.060Sample Preparation for Pesticides Analysis via LCMSMS and GCMSMS.SOP.T40.065/SOP.T.40.066/SOP.T.40.070 Procedure for Pesticide Quantification Using LCMS and GCMS). *Volatile Pesticide screening is performed using GC-MS which can screen down to below single digit ppbconcentrations for regulated Pesticides. Analytes marked with an asterisk were tested using GC-MS.
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
08/13/21
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, US
Kaycha LabsOriginal Blueberry 1.5g Pre-Roll
Original BlueberryMatrix : Flower
Certificate of Analysis PASSED
82 NE 26th streetMiami, FL, 33137, USTelephone: (305) 900-6266Email: [email protected]
Sample : DA10810003-005Harvest/LOT ID: 4258 5425 8382 0926Batch# : 1829 27726022 6080Sampled : 08/09/21Ordered : 08/09/21
Sample Size Received : 27 gramTotal Weight/Volume : 1214 unitsCompleted : 08/13/21Expires: 08/13/22Sample Method : SOP.T.20.010
Page 4 of 4
Microbials PASSED
Analyte LOD Result Action LevelESCHERICHIA_COLI_SHIGELLA_SPP not present in 1 gram.SALMONELLA_SPECIFIC_GENE not present in 1 gram.ASPERGILLUS_FLAVUS not present in 1 gram.ASPERGILLUS_FUMIGATUS not present in 1 gram.ASPERGILLUS_TERREUS not present in 1 gram.ASPERGILLUS_NIGER not present in 1 gram.TOTAL YEAST AND MOLD 10 9000 CFU 100000
Analysis Method -SOP.T.40.043 / SOP.T.40.044 / SOP.T.40.041Analytical Batch -DA029722MIC , DA029724TYM Batch Date : 08/10/21, 08/10/21Instrument Used : PathogenDx Scanner DA-111,Running On : 08/11/21, 08/11/21
Analyzed by Weight Extraction date Extracted By1829, 513 1.8455g 08/10/21 513, 513
Reagent Consums. ID Consums. ID Consums. ID Consums. ID071921.R36021921.44
200103-2743110TH093G00410311989-024CC-0242802029
2803035D013D012A17A162807016
28100332B2809006046280403328080102811026
20334227941201126119C009C6-009914C4-914AK929C6-929H
Microbiological testing for Fungal and Bacterial Identification via Polymerase Chain Reaction (PCR) methodconsisting of sample DNA amplified via tandem Polymerase Chain Reaction (PCR) as a crude lysate which avoidspurification. (Method SOP.T.40.043) If a pathogenic Escherichia Coli, Salmonella, Aspergillus fumigatus,Aspergillus flavus, Aspergillus niger, or Aspergillus terreus is detected in 1g of a sample, the sample fails themicrobiological-impurity testing. Pour-plating is used for quantitation and confirmation, Total Yeast and Mold hasan action limit of 100,000 CFU.
Mycotoxins PASSED
Analyte LOD Units Result Action LevelAFLATOXIN G2 0.002 ppm ND 0.02AFLATOXIN G1 0.002 ppm ND 0.02AFLATOXIN B2 0.002 ppm ND 0.02AFLATOXIN B1 0.002 ppm ND 0.02OCHRATOXIN A 0.002 ppm ND 0.02
Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch -DA029729MYC | Reviewed On - 08/12/21 13:01:27Instrument Used : DA-LCMS-003 (MYC)Running On : 08/11/21 16:18:47Batch Date : 08/10/21 09:57:32
Analyzed by Weight Extraction date Extracted By585 g 08/10/21 03:08:10 585
Aflatoxins B1, B2, G1, G2, and Ochratoxins A testing using LC-MS. (Method: SOP.T.30.065 forSample Preparation and SOP.T40.065 Procedure for Mycotoxins Quantification Using LCMS. LOQ 1.0ppb). Aflatoxin B1, B2, G1, and G2 must individually be <20ug/Kg. Ochratoxins must be <20µg/Kg.
Heavy Metals PASSED
Reagent Reagent Reagent Dilution Consums. ID071621.R04080421.R56080421.R57080421.R58072721.R50080921.R04
072721.R51080921.R02080921.R03121020.12080321.R05073021.R32
030420.08050121.01
100 3146-870-00811989-024CC-024
Metal LOD Unit Result Action Level
IODINE 1 ppm ND 20ARSENIC 0.02 PPM <LOQ 0.2CADMIUM 0.02 PPM ND 0.2MERCURY 0.02 PPM ND 0.2LEAD 0.05 PPM ND 0.5
Analyzed by Weight Extraction date Extracted By1879 0.2499g 08/10/21 12:08:52 1879
Analysis Method -SOP.T.40.050, SOP.T.30.052, SOP.T.30.053, SOP.T.40.051Analytical Batch -DA029738HEA | Reviewed On - 08/12/21 09:00:51Instrument Used : DA-ICPMS-003Running On : 08/11/21 15:02:54Batch Date : 08/10/21 10:14:30
Heavy Metals screening is performed using ICP-MS (Inductively Coupled Plasma – MassSpectrometer) using Method SOP.T.30.052, SOP.T.30.053 Sample Preparation for Heavy MetalsAnalysis via ICP-MS and SOP.T.40.050, SOP.T.40.051 Heavy Metals Analysis via ICP-MS.