chemical reaction engineering no. of periods in one ... · chemical reaction engineering subject...

CHEMICAL REACTION ENGINEERING

Subject code04302

No. of periodsin one session60

No. of periods per weekL T P/S3 0 0

Rationals & Objective : Every industrial chemical process designed to produceeconomically a desired product from a variety of starting materials through a successionof treatment steps. The raw materials undergo a number of physical treatment steps to putthem in the form in which they can be reacted chemically. Then they pass through thereactor.Chemical engineering diploma students are required to find the extent and rate of reactionforming the products from reactants. They are also required to handle the chemicalreactors in which reactors occur to form the products.Diploma in chemical engg. Student will learn the various mechanism to find the rate ofvarious type of reactions. They will also learn to get the sufficient information and datafor the design of the chemical reactors.

Sr.No.

Topics - Periods

1. Kineties of lomogeneous Reaction - 62. Analysis and Inerpretation of Batch Reactor data - 63. Reactor Design - 94. Isothermal Reactors for single Reactions - 95. Multiple Reactions - 56. Temperature and pressan affects - 137. Heterogeneous Reactions & Catalysts - 12

60

CHEMICAL REACTION ENGINEERING (2)

1. KINETICS OF HOMOGENEOUS REACTIONS - [6]

1.1 Defining a rate equation and its representation.1.2 Single and multiple reactions.1.3 Elementary and non- elementary reactions.1.4 Molecularity and order of reactions.1.5 Kinetic models for non-elementary reactions.1.6 Searching for a mechanism.1.7 Rate controlling step.

2. ANALYSIS AND INTERPRETATION OF BATCHREACTOR DATA

- [6]

2.1 Constant volume batch reactor.2.1.01 Integral and Differential methods of analysis.2.2 Variable valume batch reactor.2.2.01 Integral and Differential methods of analysis.2.3 Temperature and reaction rate.2.4 The search for a rate equation.

3. REACTOR DESIGN - [9]

3.1 Introduction.3.2 Conversion of mass in reactors.3.3 Performance equation for ideal stirred tank reactor.3.4 Tubular flow reactor.3.5 Space time and space velocity.3.6 Deviation from ideality.

4. ISOTHERMAL REACTORS FOR SINGLEREACTIONS

- [9]

4.1 Batch reactor.4.2 Mixed versus plug flow rectors.4.3 First and second order reactions.4.4 Ceraphical comparisions.4.5 Multiple reactor system.4.6 Plug flow reactors in series and or in parallel.4.7 Equal size mixed reactors in series.4.8 Mixed flow reactors of different size in series.4.9 Recycle reaction (flow batch)4.10 Auto catalytic reactions.

5. MULTIPLE REACTIONS. - [5]

5.1 Parallel reactions.5.2 Series reactions.

6. TEMPERATURE AND PKESSURE EFFECT - [13]

6.1 Heats of reactions from thermodynamics.6.1.1 Effect of temperature on heat of reaction.6.2 Uses of mean molar heat capacities.6.3 Chemical equilibrium.6.3.01 Equilibrium constant from themodynamies.6.3.02 Relation between kp. Kc. And ky. etc.6.3.03 Equilibrium conversion.6.4 General graphical design procedure.6.5 Optimum temperature progression.6.6 Heat effects.6.6.01 Adiabatic operation.6.6.02 Non-adiabatic operation.

7. HETEROGENEOUS REACTIONS & CATALYSIS - [12]

7.01 Heterogeneous reactions- Introduction.7.02 Types of Referoglmous reactions.7.3 Heterogeneous catalysis.7.3.01 The nature of catalytic Reactions.7.3.02 The mechanism of catalytic Reactions.7.3.03 Classification of catalysts.7.3.04 Catalyst preparation.7.3.05 Promotors & Inhi bitors.7.3.06 Poisons (catalyst life)7.4 Adsorption on solid suface.7.4.01 Surface chemistry and adsorption.7.4.02 The Largmuic threatment of adsorption.

Books Recommended

1. Chemical engineering Kinetics by J.M. Smith.2. Reaction Kinetics for chemical engineers by Walas.3. Chemical Reaction Engineering by Octaue Lerenspiel.

Scheme of Examination for Final Examination Full marks –80

Serial No. Topics Marks (%)1 Objective 252 Short Answer 253 Long Answer 50

100

UNIT OPERATION

(Theory)Subject code

04303No. of periodsin one session

60

No. of periods per weekL T P/S3 0 0

Rationals & Objective :Chemical engineering diploma students are lokely to handlevarious tasks in industries related to fluids, its pumping, heat transfer and heat transferequipments so, it is quite essential to have sufficient knowledge of related topics forefficient operation and supervision of the plants.

Sr.No.

Topics - Periods

1. Fluid Statics. - 82. Fluid kinematics. - 83. Dynamics of fluid flow. - 54. Flow Measurement. - 55. Dimensional Analysis. - 76. Pumping of fluids. - 107. Heat Transfer. - 98. Evaporators. - 5

60

CONTENTS

Topic :01 – Fluid Statics - [08]01.01 Definition types and classification of fluid.01.02 Properties of fluid.01.03 Viscosity of order of reactions.01.04 Affect of temperature & presume on viscosity of fluid.01.05 Newtonian & non-newtonian fluids.01.06 Rheological diagram.01.07.01 Simple mano meter.01.07.02 Differential manometer.

Topic :02 – Fluid Kinematies Statics - [08]02.01 General types of fluid flow.02.01.01 Steady and in steady flow.

Topic :03 Dynamics of fluid flow - [08]03.01 Various forms of energy present in fluid flow.03.01.01 Elevation energy kinetic energy, pressune energy .03.01.02 Friction loss of head.03.02.01 General energy equation for steady flow.03.02.02 Burnoullis theorem and its statement.03.02.03 Deviation of Bernoullis equation.03.02.04 Assumption underlying Bernoullis equation.03.02.05 Head & Power – Horse power.03.03 Friction losses in laminer flow through circular tube hagen poiseuille

equation.03.04 Friction losses in turbulent flow fanning equation.03.05 Other energy losses in pipe due to sudden expansion, contraction, pipe

fittings etc.

Topic :04 Flow Measurement - [05]04.01 Variable head meter.04.01.01 Venturimeter.04.01.02 Orificemeter.04.01.03 Pitote tube.04.02 Variable Area meter Rotameter.

Topic :05 Dimensional Analysis - [07]05.01 Methods of Dimensional analysis.05.01.01 Roleigh Method05.01.02 Buckinghams Methods.05.02 Dimensionless Numbers.05.02.01 Reyroldo Number.05.02.02 Frouds Number.05.02.03 Eufer Number.05.02.04 Weber’s Number

Topic :06 Pumping of fluid - [10]06.01 Pipe fittings and joints.06.02 Various values – Gate value, cheek, value, celobe value, safety value06.03 Pumps.06.03.01 Reciproeting Pumps06.03.02 Rotary pumps06.03.03 Centrifugal pumps06.04 Cavifation, water hammer.06.05 NPSH, Priming of a pump.06.06 Study of compressor – single and multistage compressor.

02.01.02 Uniform and non-uniform flow.02.01.03 Laminar & Turbulent flows.02.01.04 Compressible & Incompressible.02.02 Equation of continuity of flow.02.02.01 Equation of continuity for one dimensional flow.02.02.02 Applicability of equation of continuity.

Topic :07 HEAT TRANSFER - [09]07.01 Heat transfer through conduction07.01.01 Mean Area of heat transfer, Am.07.01.02 Conduction through a composite wall and cylinders.07.02 Heat transfer through convection,07.02.01 Film coefficient.07.02.02 Overall heat transfer coefficients.07.02.03 Correlation for calculation of leaf transfer coefficients.07.03 Principle of Radiation07.03.01 Black body radiation07.03.02 Stefan Bolty man law07.03.03 Amissive power, Absorption power.07.04 Heat exchangers07.04.01 Log Mean Temperature coneeft07.04.02 Effect of dirt & fouling factors

Topic :08 Evaporation - [05]08.01 Single effect evaporators.08.02 Parts & accessories.08.03 Principle of worbing of double effect evaporators.

Books Recommended1. Introduction to chemical Engg. Badger & Banchar2. Chemical Engg. Vol- I J.M. Coubors, Rich3. Unit operation Mccabe & Smith4. Heat transfer D. Q. kern

Scheme of ExaminationSl.No.

Topics Marks (%)

1. Objective2. Short Answer3. Long Answer

MASS TRANSFER OPERATION



60

No. of periods per weekL P T3 0 0

Rationals & Objective : An elementary knowledge of mass transfer distillation,aboorption, extration, drying are quite essential to operate and maintain the plants.

The students will be able to learn these basic unit operations which one mostcommon in chemical industries.

Sr.No.

Topics - Periods

1. Mass transfer operation - 062. Distillation - 153. Absorption - 154. Extraction - 125. Drying - 12

60

CONTENTS

Topic :01, Mass Transfer operation - [06]01.01 Introduction01.02 Classification01.03 Diffusion Theory01.04 Molecular diffusion

Topic :02, Distillation - [15]02.01 Vapor liquid equilibria.02.02 Volatility concept.02.03 Methods of distillation.02.03.01 Flask Distillation.02.03.02 Differential Distillation.02.03.03 Rectification.02.04 Material and Energy balance.02.05 Mccabe Theele Material Balance.02.06 Reflux ration and its effects on size of coloumn.02.07 Condenser duty, No of trays.02.08 Plate efficiency

Topic :03, Absorption - [15]03.01 Difinition.03.02 Equilibrium, Solubility of gas in liquid.03.03 Equipment for gas liquid operation.03.03.01 Gas dispersed equipments.03.03.02 Liquid dispersed equipments.03.04 Packed coloumn.03.05 Types of packing.03.06 Characteristics of packing.03.07 Solvent Selection for gas absorption.03.08 Material Balance in Counter current phenomenon.

Topic :04, Extraction - [12]04.01 Principle of Extraction.04.02 Ternary Diagram.04.03 Solvent liquid Extraction.04.04 Liquid-liquid Extraction.04.05 Types of Equipments.

Topic :05, Drying - [12]05.01 Principle05.02 Various terms used.05.03 Rate of drying Calculation.05.04 Study of equipment used for drying.05.04.01 Tray Dryer.05.04.02 Rotary Dryer.05.04.03 Spray Dryer.05.04.04 Drum Dryer.05.04.05 Fluidised bed dryer.Books Recommended1. Introduction to chemical Engg. by Badger & Banchero2. Unit operation by Mccabe & Smith3. Chemical Engg. Vol- II by Coulson & Richardson4. Unit operation by G.G. Brown

Scheme of Examination for final Examination Full marks – 80Sl.No.

Topics Marks (%)

1. Objective 252. Short Answer 253. Long Answer 50

100

MECHANICAL OPERATION



60

No. of periods per weekL T P3 0 0

Rationals & Objective : The subject covers various methods used for treatment of rawmaterials, intermediate and final products to make suitable for use. The study of thissubject highly essential for understanding and operation of various machenis andequipments use for such methods.

The students should learn about the principles and discription ofvarious unit operation methods and equipments and effect of various parameters on theperformance of the equipments.

Sr.No.

Topics - Periods

1. Size Reduction - 112. Size Seperation - 253. Mixing - 094. Crystallisation - 055. Filtration - 10

60

CONTENTS

Topic :01, Size Reduction - [11]01.01 Crushing, grinding and disintegrating equipments for solids. -01.02 Wet and dry grinding. -01.03 Efficiency of Crushing.

Topic :02, Size Seperation - [25]02.01 Methods of seperation of solids based on size.02.02 Grading and the principles involved.02.03 Study of different equipments used in grading. -02.03.01 Grizzlees02.03.02 Trommels02.03.03 Vibrating Screens02.04 Hydraulic Seperation -02.04.01 Settling

Topic :03, Mixing - [09]03.01 Principles involved in mixing. in fluid flow.03.02 Study of equipments used for mixing.03.02.01 Liquids with liquids.03.02.02 Gases with liquids.03.02.03 Viscous Masses -03.02.04 Solids with liquids.03.02.05 Solids with Solids

Topic :04,Crystallisation - [05]04.01 Crystal Forms04.02 Crystal Grocoth04.03 Equipments used for Crystallisation.

Topic :05, Filtration - [10]05.01 Principles of Filtrationnalysis.05.02 Equipments used -05.02.01 Plate & Frame Filter Press05.02.02 Leaf Filters.05.02.03 Vacuum Filters

Books Recommended1. Unit operations in Chemical Engineering by W.L. Mc Cabe and J.C.

Smith (MC Graw –HillBook Company, NewYork.)

2. Introduction to Chemical Engineering by Vol I W.L. Badger and J.T.Banchero.

02.04.02 Sedimentation02.04.03 Flocculation02.04.04 Equipments used02.05 Centrifuging -02.05.01 Basket Centrifuging02.05.02 Critical Speed.02.05.03 Super Centrifuge.

Scheme of Examination for final Examination full marks –80Sl.No.

Topics Marks (%)


100

CHEMICAL ENGINEERING DESIGN& DRAWING



60


Rationals & Objective : A Chemical engg. diploma student should know the details ofstandard equipments in chemical industrials and should be conversant loith drawingsand reading of these equipments.

The students should learn details of various equipments and theircomponents various equipments and their drawings of the same.

Sr.No.

Topics - Periods

1. Fluid Flow - 102. Heat Transfer - 203. Mass Transfer - 30

60

Topic :03, Mass Transfer - [30]03.01 Distillation Coloumn.03.01.01 Height03.01.02 Diameter.03.01.03 No. of stages.03.01.04 Bubble Caps03.02 Absorption Coloumn.

CONTENTS:

Topic :01, Fluid Flow - [10]01.01 H.P. of pump -01.02 Pipe line design

Topic :02, Heat Transfer - [20]02.01 Double Pipe Heat Exchanger.02.02 Shell & Tube Type Heat Exchanger.02.03 Condensers02.04 Evaporators – Single & double effect

03.02.01 Height03.02.02 Diameter03.02.03 No of stages03.02.04 Thickness.

Books Recommended1. Introduction to chemical Engg. by Badger & Banchra2. Unit operations by McCabe & Smith.3. Chemical Engg. Handbook Perry


Topics Marks (%)

1. Free hand sketch 252. Drawing 253. Desegin Long Answer 50

100

CHEMICAL TECHNOLOGY –II



60


Rationals & Objective : The knowledge of process technologies of various chemicalsin chemical industries are most essential for chemical engg. diploma students. Theobjective of the syllabus is to make the students familiar with commercial processes,related parameters and different steps involved. The students are required to understandthe effects of various parameters on production rate, quality and cost.

Sr.No.

Topics - Periods

1. Oils, soap and detergent - 102. Sugar manufacturing - 103. Pulp and Paper - 104. Alcohol and alcohol based products - 135. Polymer Product - 106. Artificial fibre - 07

60

Topic :03, Pulp Paper - [10]03.01 Cellulose03.02 Pulp & Paper manufacture.

Topic :04, Alcohol & Alcohol based Product - [13]04.01 Commercial manufacturing processes.04.01.01 Methanol04.01.02 Ethanol04.01.03 Butanol04.01.04 Denatured Spirit.

CONTENTS:

Topic :01, Oils, Soap and Detergent - [10]01.01 Refining of edible & Non-edible oils01.02 Hydrogenation of oil.01.03 Soap and detergent

Topic :02, Sugar Manufacturing - [10]02.01 Technology.

04.01.05 Acetic Acid.04.01.06 Formic Acid.04.01.07 Ethyl Acetate.04.01.08 Acetone.

Topic :05, Polymers Product - [10]05.01 Commercial manufacturing of high polymers05.01.01 PVC05.01.02 LDPE05.01.03 HDPE05.01.04 PP

Topic :06, Artificial Fibres - [07]06.01 Nylon.06.02 Rayon.06.03 Terylene.

Books Recommended1. Outlines of Chemical Technology by C.E. Dryden2. Chemical Process Industries by H. Shreve3. Chemical Technology by Shukla & Pandey


Topics Marks (%)


100

INDUSTRIAL INSTRUMENTATION &CONTROL



60


Rationals & Objective : Measurement of Various process parameters namelytemperature, pressure, level and flow and properties of various materials like deurity,viscosity, conductivity, PH and composition of mixtures are fundamental requirment forquality control of products and stable operation of the plant. The study of variousmethods instruments for measurements and control and analysis is highly essential.

The student should learn the basic principles, constructions andlooking of emtruments used for measurement and control of various parameters.

Sr.No.

Topics - Periods

1. Measurment - 042. Temperature - 043. Pressure - 054. Level - 075. Flow - 106. Instruments - 087. Control - 12

60

CONTENTS:

Topic :01, Measurment - [04]01.01 Temperature01.02 Pressure01.03 Level01.04 Flow01.05 Humidity01.06 Specific gravety01.07 Viscosity01.08 Conductivity

Topic :02, Temperature - [04]02.01 Temperature scales02.02 Liquid and gas filled thermometers02.03 Bimetallic Thermometers

Topic :03, Prossure - [05]03.01 Manometers.03.02 Pressure Elements03.02.01 Bourdan Tube Bellows03.02.02 Helix03.02.03 Capsule03.03 Measurement of defferential pressure.

Topic :04, Level - [07]04.01 Direct level Measurement.04.01.01 Boband tape.04.01.02 Sight Glass, Floats etc.04.02 Indirect Level Measurement04.02.01 Liquid Head Pressure Type04.02.02 Air trap type Bubbler type etc.04.03 Measures of level based on use of radio active source, sound

inaves, load cells etc.

Topic :05, Flow - [10]05.01 Differential pressure meters05.01.01 Venturimeter05.01.02 Orifice meter05.02 Variable Head Meters05.02.01 Rotameters05.02.02 Valve types meter05.03 Tested Flow Meters.05.03.01 Positive Displacement meters.05.03.02 Velocity meters05.03.03 Integrators

Topic :06, Instruments - [08]06.01 For measuring specific gravity06.02 For measuring specific viscosity06.03 For measuring specific PH06.04 For measuring specific Electircal & thermal conductivity

Topic :07, Control - [12]07.01 Linearisation of model equators07.02 Laplace transforms07.03 Transfer functions and input –output models07.04 Dynamic response to step inputs of first and second order

systems with and without time lags.07.05 Feedback control and effect of proportional, integral and

derivative control.

Books Recommended1. Industrial Instrumentation by Eckman Donald

02.04 Resistance Thermometers.02.05 Pyrometers.

2. Instruments by Kirk & Rimboi


Topics Marks (%)


100

OPERATION & MAINTENANCE OFCHEMICAL ENGG. EQUIPMENTS



50


Rationals & Objective : Diploma in chemical engineering students are supposed to beengaged in industry at operational and supervisory levels. As far as operation isconcerned the operational skills like start up, shut down, normal check up causes offailure and their remedies etc of pump, Compressor, heat exchanger, furnace, Coloumn,filter crusher and dryer are quite essential. The students will learn in details all aboutsthe various operational technics.

Sr.No.

Topics - No. of lectures

1. Pump and compressor - 102. Heat Exchanger - 103. Furnace - 54. Cdoumn - 55. Filter - 56. Crusher - 67. Conveyer - 48. Dryer - 5

50

CONTENTS:

Topic :01, Pump and Compressor - [10]01.01 Preliminary check up after mechanical repair01.02 Start up, shut down, Normal check up01.03 Handing, taking over for mechanical repairs01.04 Possible Causes for failure & their remedied01.05 Safety Precautions.

Topic :02, Heat Exchanger - [10]02.01 Handing, taking over for mechanical repairs.02.02 Commissioning, Decommissioning02.03 Normal check up02.04 Quality Control.02.05 Operational difficulties & their remedies

Topic :03, Furnace - [05]03.01 Commissioning, Decommissioning of gas and oil furnace.03.02 Handing, taking over for mechanical repairs03.03 Safety precautions.03.04 Normal check up03.05 Operational difficulties and their remedies

Topic :04, Coloumn - [05]04.01 Handing, taking over for mechanical repairs.04.02 Commissioning, Decommissioning04.03 Normal Check up.04.04 Quality Control04.05 Operational difficulties & their remedies.

Topic :05, Filter - [05]05.01 Preliminary check up for mechanical repairs.05.02 Commissioning, Decommissioning05.03 Normal checkup.

Topic :06, Crushers - [06]06.01 Start up, Shutdown, Normal checkup06.02 Possible failures and their remedies.06.03 Handing, taking over for mechanical repairs.06.04 Safety precautions.

Topic :07, Conveyers - [04]07.01 Start up, Shutdown, Normal checkup07.02 Possible causes of defects & their remedies07.03 Handing taking over for mechanical repairs07.04 Safety precautions.

Topic :08, Dryers - [05]08.01 Commissioning, Decommissioning08.02 Normal check up08.03 Handing taking over08.04 Possible defects & their remedies08.05 Draft & temperature Controls

Books Recommended1. Pump – operation & Maintenance by G.Hicks

Scheme of Examination for final Examination full marks –80Sr.No.

Topics Marks (%)


100

Fertilizer Technology.(Elective – I)


04310 ANo. of periodsin one session

60


Rationals & Objective

Sl.No.


1. Importance - 032. Nitrogenous Fertilizer - 113. Phosphetic Fertilizer - 114. Potash Fertilizer - 065. Mixed Fertilizer - 116. Micronutrients - 067. Organic Fertilizers - 13

60

Topic :03- Phosphtic Fertilizers - [10]03.01 Single super phosphate.03.02 Treple super phosphate.03.03 Manufacture.

Topic :04- Potash Fertilizers - [06]04.01 Source04.02 Production

CONTENTS:

Topic :01- Importance - [03]01.01 Importance of Fertilizer in agriculture01.02 Sell Fertilizer Interaction

Topic :02- Nitrogenous Fertilizer - [11]02.01 Food stock for synthesis gas production02.02 Process for production of ammonia,02.03 Urea and other nitrogenous fertilizers,02.04 Integrated ammonia-urea plant,02.05 Ammonium Nitrate and other nitrate fertilizer.

Topic :05- Mixed Fertilizer - [11]05.01 Mixed N P K fertilizers.05.02 Granulate fertilizers.05.03 Production & application.

Topic :06-Micro Nutrcents. - [06]06.01 Production.06.02 Applications.

Topic :07-Organic fertilizers. - [13]07.01 Compost and other bio – fertilizers.07.02 Comparative study with synthetic fertilizers.07.03 Intensive agricultural practices ecological effects.

Books Recommended

Scheme of Examination for final Examination Full Marks-80Sr.No.

Topic Marks (%)


100

Bio – Chemical Engineering(Elective – III)


04310 CNo. of periodsin one session

60


Rationals & Objective

Sr.No.


1. Scope and importance of bio-chemical engineering &bio- technology.

- 03

2. Micro organisms - 173. Enzymes - 184. Fermentation - 125. Bio Reactors - 10

60

Topic :03- Enzymes - [18]03.01 Bio Catalysts03.02 Immobilized enayme03.03 Enzyme kinctics03.03.01 Michel’s Menten Equation03.03.02 Sequential enzyme reactions03.03.03 Regulation of enzyme activity03.03.04 Transport phenemena in micro bial systems

CONTENTS:

Topic :01- Scope & importance of bio –chemical engineering &bio-technology

- [03]

01.01 Scope01.02 Importance of bio-chemical Engg.01.03 Importance of bio-technology.

Topic :02- Micro organisms - [17]02.01 Structures.02.02 Composition and activities.02.03 Kinetics of cell growth – monod Equation02.04 Metabolic pathways and bio-energetivs.

Topic :04- Fermentation - [12]04.01 Process parameters.04.02 Sterilization04.03 Process control.

Topic :05- Bio – reactors - [10]05.01 Different types.05.02 Principles of bio-reactor design and scale up.05.03 Cellular manipulation.05.04 Genetic manipulation.05.05 Principles of recombinant05.06 DIM technology.05.07 Important bio – chemical products and processes.

Books Recommended

Scheme of Examination for final Examination Full Marks-80Sr.No.

Topic Marks (%)


100

PETROLEUM REFINING

(Theory, Elective)Subject code

04310 CNo. of periodsin one session

60


Rationals & Objective : The petroleum industry is one of the world’s most importantindustries and one to which serious attention may well be given a set provides scope fora wide Variety of attainments in many fields of endeavour.

The objective of the Course is to attain all a round informationsregarding Petroleum refining. The students would learn basic principles and operationasin related field.

Sr.No.


1. Origin of Petroleum - 062. History of the oil Industry - 043. Properties of Crude oils - 044. Main Petroleum Product - 085. Refining Processes - 336. Location of Refinery - 05

60

Topic :03, Properties of Crude oil - [04]03.01 Constituents03.02 Configuration

Topic :04, Main Petroleum Products - [08]04.01 Liquefied Petroleum Gas04.02 Gasoline

CONTENTS:

Topic :01, Origin of Petroleum - [06]01.01 Hypotheses01.02 Formation of oil01.03 Physical Properties.

Topic :02, History of the oil Industry - [04]02.01 Natural gas.02.02 Transport of oil

04.03 Kerosene04.04 Gas oil04.05 Diesel Fuel04.06 Heavy oils & Residuals04.07 Asphalts or Bitumens04.09 Lubricants & Greases

Topic :05, Refining Processes - [33]05.01 Simplified refining flowsheet05.02 Diagrammatic representation of Crude oil distillation.05.03 Power Requirements05.04 Crude distillation Units.05.05 Solvent Extraction Processes.05.06 Thermal Cracking.05.07 Thermal Reforming.05.08 Alkylation.05.09 Catalytic Cracking

Topic :06, Location of Refinery - [05]06.01 Different factors affecting plant site Location.06.02 Different refineries in India.

Books Recommended1. Petroleum Refining by Nelson2. Petroleum by V.Sokolov3. Handbook of the Petroleum Industry by G. Sell & H.A. Dossett

Scheme of Examination for final ExaminationSr.No.

Topic Marks (%)


100

Chemical Technology-II

( Practical)Subject code


50


Rationals & Objective: Analysis and determination technics of various Constituentsof the chemicals help the technician in design, fabrication, operation, maintenance,marketing etc.

The students will be able to familiarize with the various technics of analysisand doternination which will prove its utility in their professional Career.

[1] To determine the percentage purity of commercial Concentrated suphuricaud[2] Estimation of purity in a sample of iron wire.[3] Determination of total iron in an iron ore ( Haematite, Fe2 O3)[4] Estimation of chlorine in sodium chloride.[5] Preparation of Nitrobenzene.[6] Determination of equivalent weight of an organic acid (Oxalic Acid)[7] Iodine value of fat or oil.[8] Estimation of cane sugar.[9] Estimation of calcium in calcium carbonate.[10] Estimation of Calcium Carbonate in a sample of marble.

List of apparatus for Chemical Technology – II

Sr.No.

Name Specifications No.

1. Burette 100 ml 302. Pipette 100 ml 303. Microburetts 10 ml 304. Conical Hask 250ml,500ml 30,305. Beaker 50ml,400ml 30,306. Volumetric flask 100ml,250ml,500ml 30,30,307. Dessica for 158. Funnel 309. Silica Crucible 3010. Nickelson Hydroane

for30

11. Analytical Balance 1012. Analytical weights box 1013. Digital Balance 114. Winchester bottle 515. Measuring cylinder 5ml,25ml,50ml,100ml,250ml,500ml,1000ml 30 each16. Weighing bottle 5ml 1017. Glas bottle stopper 6018. Separating flask. 100ml,250ml,500ml 30 each

19. Brush and Glass frame 3020. Muffle Furnace (5-1200 c), working temp-1000 c 121. Hot air oven 5-300 c 122. Vacuum Dessicator Dia 16” 123. Vacuum Pump Laboratory Model 1

Industrial Instrumentation & Control lab

(Practical)Subject code


50


Rationals & Objective: Measurement of Various process parameters and properties ofvarious materials are fundamental requirements for quality Control of produced andstable operation of the plant. The study of Various meth instruments for measurements,control and analysis are highly essential.

List of the experiments(At least eight experiments to be performed)

Sr.No.

Name

1. Measurement & Caliberation of thermocouple2. Study of bimetallic thermometer & its use3. Study of pressure gauge and its testing with dead weight tester.4. Measurement of level by air purge method.5. Study of Control valve.6. Caliberation of flow integrator.7. Study of on-line working of conductivity anoter.8. Study of on line working of p H meter.9. Study of online working of pH meter10. Study of online working of pH meter

List of the equipments for Industrial Instrumentation and Control lab

Sr.No.

Name of the equipments No. Specifications

1. Thermocouples 2 Range2. Bimetallic Thermometer 2 Rang 0-500c3. Pressure Gauge 2 0-30 ps4. Dead weight tester 15. Air purge apparatus 1 Storage tank of suitable

size with T shaped tubeinserted in it and this tubeis connected to aircompressor.

6. Control value 1 Inlet & outlet y2”

connection7. Diaphragm value 2 Suitable size8. Flow integrator 2 Taylor model of different.9. Conductivity meter 1

10 to 20 mha/cm0 to 100 mha/cm

10. PH meter 2 0 to 1411. Selica Analyser 1 0 to 0.2 ppm

0 to 30ppm

Unit operation lab

(Practical)Subject code


75


Rationale & Objective:Working experiences with the machenics and equipments like crushers, sieve shaker,grinders, fittings, values, pump heat exchanger dryer, extractor are required for thestudents practical knowledge enrichment. This will assist them in understanding themachnics and equipments as a whole and will be most useful in their professionalCorrears.

List of experiments(At least eight experiments are to be performed).[1] To study the jaw crusher and to determine the energy required[2] To determine the particle size of the ground material by sieve analysis.[3] To determine the power required and critical speed of Ball mill.[4] To study the Plate & Frame Filter press and its characteristics.[5] Demonstration of equipments.

a. Centrifuge.b. Conveyersc. Pumps.d. Valves.e. Heat exchanger models.f. Packings.

[6] To observe the flow Conditions by using the Reynold’s experiments.[7] To study the centrifugal pump and its characteristics.[8] To study the parallel flow counter flow heat transfer patterns in double pipe heat

exchanger and to determine the heat transfer coefficients.[9] To determine the thermal conductivity of a metal rod.[10] To study the tray dryer and to determine the rate of drying for a given wet

sample.

List of Machenis & Equipments for Unit operation lab

Sr.No. Name Specifications Qty.1 Jaw Crusher 0.5 tonne capacity fitted with manganese steel

jaw with 2HP motor.1

2 Ball mill Size – 18” diameter ¼” thick M.S. plakcylindrical cell with 9”x9” charging doordriven by 1 HP motor with speed of 40,20 and10 rpm

1

3 Plate & Frame filterpress

8 plates, a frames of sizes 20cm x 20cm. 1

4 Reynolds Apparatus 2’ diameter corning tube with dye injector anda dye collection tank of 35 x 35 x 50cm

1

5. Sieve Shaker Sieves made of brass with sizes80,100,120,140,150,170,200 and 240 mesh.

1

6. Double Pipe HeatExchanger.

1” diameters pipe with Concentric jacket withprovision of cocurrent, counter current andcross current an angement with suitablemanometer and temperature measuring devices.

1

7. ThermalConductivityapparatus

Metal rod of suitable diameter with steam/oilsupply at one end with temperature measuringdevices along the length of the rod.

1

8. Tray Dryer Drying oven with trays of size 20 x 20 cm (12no) and pan balance.

1

9. FractionalDistillation

1.liter capacity rectifying coloumn with refluxcontrol with heating device, provision forsteam and vacuum distillation.

1

10. Liquid –liquidextractor

Separating funnels, Agitatis, mixers,measuringcylinders

1

11. Centrifuge (Hydro-extractor)

Basket with stable stirror driven by 2 HPmotor.

1

12. Conveyers Belt type Conveyers 12” belt driven by suitablemotor.

1

13. Pumps Gear Pumpcentrifugal pump

11

14. Valves Gate valve 1”Globe valve 1”Non –return valve 1”Diaphragm valve 1”Needle valve 1”

22222

15. Packed Tower Glass Coloumn of 2” dia 3ft hight connectedwith rotameter, distributors

1

16. Packings Pall ringRasching ring.Intel saddles.

Chemical Engg. Design & Drawing

(Sessional)Subject code


75

No. of periods per weekL T S0 0 3

Rationale & Objective:Same as that of chemical Engg. Design and Drawing (Theory), subject code-

Sr.No. Topic - No. of periods1. Flow of fluid - 202. Heat Transfer - 203. Mass Transfer - 35

75

CONTENTS:Same as that of Elementary chemical Engg design & drawing (Theory),Subject code--

Books Recommended[1] Introduction to chemical Engg. by Badger & Banchro[2] Unit Operation by Mccabe & Smith[3] Heat Transfer by D.Q. Kern[4] Chemical Engg. Handbook by J.H. Perry.

Project Work and its Presentation in Seminar

(Sessional)Subject code04316

No. of periodsin one session

50

No. of periods per weekL T S0 0 2

Rationale :Project assignment is important to develop confidence to the problem, tackle it in asystematic way and to prepare a report. Many terms engineers are required to do thesetype of activities in the relevant fields.Objectives :

By working on assigned problem, students must become conversant withtechnological investigation work and remedial measvis . student should prepare detailreport and should present the same before an avedence.

CONTENTSThe project comprises assigning a problem with a view to make the students

conversant with technical investigation work and remedial measures, It could be anactual, live plant problem for a critical & indepth study. The prepared technical reportwould be presented before an audience for sharing, cross examination and evaluation byan expert Committee in the following areas.

[1] Material Balance & Energy Balance to fix up and quantity losses and work outefficiencies.

[2] To find out why the designed capacity and efficency of an equipment or process.[3] To examine the validity of a design date on a particular equipment or process.[4] To defermite specific consumption of raw materials and utilities on given

process for a particular product.[5] Study of problems illustrations application of thermodynamics and kinetics to

find out conversion and yield[6] Study of frequent breakdown/failure of an equipment or process.[7] To sturdy the problem of low product quality.[8] Examples of specific problems:

(a) Cooling water(b) Power(c) Fuel(d) Air requirement for a given duty.

In plant Training & Visit to Works

(Sessional)Subject code


4 weeks

No. of periods per weekL T S

Rationale & Objective:It is quite essential for technical students to get exposed to industrial environments toacquire, practical and professional experiences which improved their understandings allaround.

The duration of training & visit to works will be four weeks in local large scaleand small scale industries. The programme will be decided by the officer incharge (Training) of the organization. The training will be imparted to students after end ofacademic session. After completion of training the students will submit training reportand final evaluation will be done by a committee cousisting of two members, one ofthem should be from industry preferably. There will be no division of marks betweenenternal and external examiners.

One faulty from the institute will monitor the training programmes andhe will maintain liaison with training incharge of the organization.

Scheme of Teaching and Examination for 3-yearsPART-III DIPLOMA in CHEMICAL ENGINEERING

THEORY

Sr.No.

SUBJECTS SUBJECTCODE

TEACHINGSCHEME

EXAMINATION - SCHEME

Periodsper

week

Periodsin one

session(Year)

Hours ofExam.

TerminalExam. (A)

Marks

FinalExam.

(B)Marks

TotalMarks(A+B)

PassMarksFinal

Exam.

PassMarks in

theSubject

1. Professional Studies &Entrepreneurship

00301 03 60 03 20 80 100 26 35

2. Reaction Engineering 04302 03 60 03 20 80 100 26 353. Unit Operation 04303 03 60 03 20 80 100 26 354. Mass Transfer Operation 04304 03 60 03 20 80 100 26 355. Mechanical Operation 04305 03 60 03 20 80 100 26 356. Chemical Engineering Design

& Drawing04306 03 60 03 20 80 100 26 35

7. Chemical Technology -II 04307 03 60 03 20 80 100 26 358. Industrial Instrumentation and

Control04308 02 50 03 20 80 100 26 35

9. Operation and Maintenance ofChemical EngineeringEquipments

04309 02 50 03 20 80 100 26 35

10. Elective 03 60 03 20 80 100 26 35(A) Fertilizer Technology 04310A(B) Bio-Chemical

Engineering04310B

(C) Petroleum Refining 04310CTotal :- 1000

PRACTICAL

Sr.No.


TEACHINGSCHEME

EXAMINATION – SCHEME

Periodsper

week

Periodsin one

session(Year)

Hoursof

Exam.

MarksInternalExam.

(A)

MarksExternalExam.

(B)

TotalMarks(A+B)

PassMarksFinal

Exam.

PassMarks in

theSubject

11. Chemical Technology-II 04311 03 60 03 20 80 100 32 4012. Industrial Instrumentation and

Control04312 03 60 03 10 40 50 16 20

Total :- 150

SESSIONAL

Sr.No.


TEACHINGSCHEME

EXAMINATION - SCHEME

Periodsper week

Periodsin one

session(Year)

Marks ofInternal

Examiner(X)

Marks ofExternal

Examiner(Y)

TotalMarks(X+Y)

PassMarks in

the Subject

13. Unit Operation 04313 03 60 20 30 50 2514. Chemical Engineering Design &

Drawing04314 03 60 20 30 50 25

15. Professional Studies &Entrepreneurship

00315 02 50 20 30 50 25

16. Project Work & its Presentation inSeminar

04316 02 weeks inExtra Hours

40 60 100 50

17. In Plant Training & Visit to Work 04317 04 weeks duringVacation

40 60 100 50

Total :- 350

Total Periods per week = 42 Total Marks = 1500

chemical reaction engineering no. of periods in one ... · chemical reaction engineering subject...

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