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Table of Contents
Preface v
Committees, Sponsors vi
Chapter 1: Technologies of Processing and Manufacturing
Synthesis and Characterization of MoO2 Nanoplates Prepared by Thermal
Evaporation of MoO3 and S Powders
H.Q. Li, Z.J. Peng, J.W. Qian, Z.G. Shen and X.L. Fu.................................................................... 3
Reaction Sintering of Transparent Aluminum Oxynitride (AlON) Ceramics Using
MgO and Y2O3 as Co-Additives
S. Qi, X.J. Mao, B.Y. Chai and L. Zhang ........................................................................................ 7
Effects of Seeding with Nanocrystallites and Addition of Inorganic Alumina Sol on
Crystallization of Alkoxide Alumina Gel
Y. Kobayashi, Y. Mabuchi, M. Hama, K. Yamamura, Y. Yasuda and T. Morita ......................... 12
Preparation and Characteristics of Nanocrystalline Yttria by Microwave-Induced
Solution Combustion Method
Y.S. Zhang, Y.J. Zhang, T. Li and Q.S. Li .................................................................................... 18
Preparation of High-Purity Magnesium Aluminate Spinel Powder by Thermal
Decomposition Method
X.J. Wu, J.S. Li, X.J. Tang, M.Y. Wang and S. Li ........................................................................ 23
Preparation of Amorphous SiOC Ceramic Powders through Precursor Polymer
Pyrolysis
M.B. Ma, H.J. Wang, J.B. Wen, M. Niu, X.Y. Fan and L. Su....................................................... 27
Preparation of Zirconium Diboride Nanopowders Using Different Zirconium
Sources via Sol-Gel Method
X.X. Qin, X.D. Zhao, H.M. Ji and Z. Zhao ................................................................................... 33
Preparation of ZrB2 Powders with Different Morphologies by Pressureless
Reactions
W.X. Hai, Y.H. Huang, Y. Jiang and Z.B. Wei ............................................................................. 39
Preparation of Zirconium Diboride Powder by Carbon Thermal Reduction Method
L. Ma, J.C. Yu, Y.J. Zhang, H.Y. Gong, Q.S. Li and X. Guo ....................................................... 44
Synthesis of Ultra-Fine Zirconium Diboride Powders by Polymer Template Method
Following by Microwave Sintering
Q.H. Deng, Z.H. Ding, X.F. Shen, S.Y. Du and Q. Huang ........................................................... 49
Preparation and Characterization of Ultra-Fine ZrB2 Powders from Inorganic-
Organic Hybrid Precursors via Carbothermal Reduction
B.N. Wang, Y.B. Duan, J. Hu, X.Q. Zhu, K.J. Wang and W.J. Zhang ......................................... 54
Preparation of TiB2 Ultrafine Powders by Carbothermal Reduction
J.C. Yu, L. Ma, Y.J. Zhang, H.Y. Gong and L.W. Zhou ............................................................... 58
Synthesis and Characterization of Asparagine-Modified and Terbium-Doped
Spherical Hydroxyapatite Nanoparticle
X.F. Xing, L.L. Luo, Y.P. Guo, W.M. Gao and L. Hu .................................................................. 62
High-Performance Ceramics IX
x
Preparation of β-CD-HAP Composite Microspheres
L.L. Luo, L. Hu, X.F. Xing, W.M. Gao and Y.P. Guo .................................................................. 67
Improvement of SrAl2O4:Eu2+
, Dy3+
Phosphor via AlN Incorporation
C. Quan, Y.F. Zhou, D.C. Huang and W.T. Xu ............................................................................. 71
Microwave Assisted Preparation of YAG and Yb:YAG Transparent Ceramic
Nanopowders for Laser Crystal
W. Si, C. Xiong, Y.W. Jiang, Z.F. Xing and W. Pan..................................................................... 76
Syntheses and Characterizations of New Eu-Ce Codoped LaSrSiO3N Phosphors for
LEDs
D.C. Huang, Y.F. Zhou, C. Quan and W.T. Xu ............................................................................. 80
BiFeO3 Powders Synthesized by Different Sol-Gel Methods
L. Bao, X.W. Qi, B. Ni, M. Zhang and R.B. Mei .......................................................................... 84
Preparation and Microstructure of (La0.5Sm0.5)2(Zr0.7Ce0.3)2O7 Ceramics Prepared
by Chemical Coprecipitation Method
X.K. Sun, G.H. Wang, S.C. Zhang, H.R. Sun, K. Fang and Y.F. Chen ........................................ 89
Magnetocaloric Properties of Perovskite-Type Manganite La0.65Sr0.2Na0.15MnO3
Q.L. Ji, Z.G. Zou, F. Long and Y. Wu ........................................................................................... 93
La-Doped Nanometer TiO2 Powders Prepared by Sol-Gel Method
Z.C. Duan, G.M. Jiang, X.Q. Rong, J.K. Yan, J.H. Du, G.Y. Gan and J.H. Yi ............................ 97
Preparation Uniform of TiO2 Microporous Ceramic Membrane Supported by Al2O3
X. Zhang, G.Y. Li and J.F. Zhang ............................................................................................... 101
Phase Evolution and Surface Morphology of Niobate Hydrate Template
Nanoparticles Synthesized by Hydrothermal Method
Y.Y. Wang, N.X. Xu, J.Z. Liu, Q.L. Zhang and H. Yang ........................................................... 105
Hydrothermal Synthesis of Bi4Ti3O12/TiO2 Composite
W. Zhao, N.Q. Liu, H.X. Wang, Y.B. Zhang, S.M. Zhang, K.X. Gao, X. Chen
and Z.Y. Fan................................................................................................................................. 109
A Novel Method for Preparing Calcium Carbonate Particles: Thermal
Decomposition from Calcium Hydrogen Carbonate Solution
H.Y. Zeng, Z.L. Yan, M.R. Jiao, D.D. Xu and J.X. Jiang ........................................................... 113
Study on the Pore Structure of Forsterite Insulating Material
J.P. Liu, X.J. Zhang, H.X. Zhu and C.J. Deng ............................................................................. 119
Control of the Spring Back in Rice Husk by Al2O3 Sol
J.J. Liu, Y.B. Li, S.J. Li, Y.W. Li and S.B. Sang ......................................................................... 124
Cellulose-Silica Composite Aerogels Prepared with Sodium Silicate by Freeze
Drying Method
H.Z. Sai, R. Fu, L. Xing, J.H. Xiang, Z.Y. Li, T. Zhang and F.S. Zhang .................................... 129
Pore Forming Mechanism of Forsterite Insulation Materials Synthesized by Molten
Salt Method
Y.F. Song, C.J. Deng, H.X. Zhu and J. Ding ............................................................................... 134
Study on the Gel Casting Process of Silicon Carbide
H. Li, H.Z. Xu, C.L. Zhou and Y.Y. Wang ................................................................................. 138
Bacterial Cellulose Aerogels Skeleton Strengthened by Regenerated Cellulose
R. Fu, H.Z. Sai, L. Xing, J.H. Xiang, Z.Y. Li, T. Zhang and F.S. Zhang .................................... 143
Polysilane as SiC Precursor: Preparation, Catalytic Cure and Pyrolysis
C.J. Huang, Z.H. Wang and M.C. Wang ..................................................................................... 148
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Key Engineering Materials Vol. 697
Zirconyldichloride Modified Polycarbosilazane as Precursors for SiZrCNO
Ceramics
J.J. Han, D. Su, Y. Yu, X.T. Zhao, X.J. Wang, Z.P. Zhao, X. Yan and Z.G. Jin ........................ 153
Preparation of Camphene Carbon/Silicon Carbide Slurry for 3D Printing
X.T. Huang, C.Q. Hu, H.R. Sun, H.L. Liu, Y.L. Huo, H.L. Liang and Y.F. Chen ..................... 159
Preparation of Ti2AlN Porous Ceramics by Organic Foam Impregnation Process
S.S. Shang, X. He, Y. Yang and M. Yan ..................................................................................... 163
Fabrication and Properties of Porous Carbon Preforms for Making Reaction
Formed SiC
C.Q. Hu, X.T. Huang, H.L. Liang, S.G. Chen, Y.L. Huo, H.L. Liu, J. Tang
and Y.F. Chen .............................................................................................................................. 169
Densification Behaviors in the Early Stage of Spark Plasma Sintering of 3Y-TZP
Nanoceramics
Y. Xiong, L. Wang and C. Liu ..................................................................................................... 173
Effect of Sintering Aids on the Properties of Porous YAG Ceramics
M.H. Xu, J.G. Song, R.H. Wang, S.B. Li, N. Wang, S.Y. Yu, H.X. Yan, T.T. Xiao
and F. Chen .................................................................................................................................. 178
Effects of Particle Size on Densification Behavior of Si3N4 Ceramics
L.J. Wang, X. Yang, X.J. Liu, Z. Jiao and Z.R. Huang ............................................................... 182
Effect of Sintering Pressure on Mechanical Properties of BN-Si3N4 Ceramic
Composites Prepared by Spark Plasma Sintering
J.X. An, W.D. Xue, F.R. Zhai, R.M. Xu and J.L. Sun ................................................................. 188
The Influence of Al2O3 and TiO2 Additions on the Sintering Behavior of Partial
Reaction Bonding Silicon Nitride
J. Deng, D.X. Yao, Y.F. Xia, K.H. Zuo, H.Q. Liang and Y.P. Zeng ........................................... 193
Sintering of High Quality Titanium-Doped Zinc Oxide Ceramic Sputtering Target
C.B. Pi, X.X. Cai, C. Xiao, H.P. Yang, J.H. Gao, L. Gao and H.T. Yang .................................. 198
Influence of Hot Pressing Process on the Properties of Cf/SiO2 Composites
C.T. Shao, Q.H. Wei, H.S. Wang, C.H. Wang, Q.L. Zhang and Y.Y. Wang .............................. 203
Fabrication and Properties of W-SiCP/Cu Composites by Hot Pressing Sintering
L.M. Zhang, Y. Liu, C.C. Zhang, G.Q. Luo, H. Liu and Q. Shen ............................................... 207
Effect of Buried Powder Sintering on the Electrical and Piezoelectric Properties of
CuO-Modified (Li,K,Na)(Nb,Sb)O3 Lead-Free Piezoceramics
L.L. Li and Y.H. Zhen ................................................................................................................. 211
Chapter 2: Ceramics for Functional Applications
Preparation and Characterization of Bi2Ti2O7 Microwave Dielectric Ceramics by
Citrate Sol-Gel Method
Y. Zhang, Y.C. Zhang, X.L. Su and M.Q. Xiang ........................................................................ 219
Evidence of Normal to Anti Ferroelectric Phase Transition of PLZT Transparent
Ceramics of Different Zr/Ti Ratio
B. Xia, X.Y. He, D.Z. Sun, W.X. Cheng, P.S. Qiu and X. Zeng ................................................. 223
Using Ferroelectric Thin Film as the Dielectric for Electrowetting-on-Dielectric
J.Q. Niu, Z.K. Xie, Z.X. Yue and W.Q. Wang ............................................................................ 227
High-Performance Ceramics IX
xii
Dielectric Breakdown and Failure of Ferroelectric Films as the Dielectric for
Electrowetting Systems
W.Q. Wang, J.Q. Niu, Z.K. Xie and Z.X. Yue ............................................................................ 231
The Electrical Properties of Epitaxial Grown Sc-Doped (Na0.85K0.15)0.5Bi0.5TiO3 Thin
Film Prepared by Sol-Gel Method
Y.Y. Wu, X.H. Wang, C.F. Zhong and L.T. Li ........................................................................... 235
Influence of (Bi0.5M0.5)TiO3 (M=Li, Na, K, Rb) Addition on the Curie Temperature
and PTC Effect of BaTiO3-Based Ceramics
M.M. Yang, Z.J. Peng, C.B. Wang and X.L. Fu .......................................................................... 239
Effect of Defect Characteristics on the Color of BaTiO3-Based PTC Ceramic
A.M. Yang, J.M. Deng, C.X. Su, W.H. Jia and L.J. Liu.............................................................. 243
Electrode Interface Polarization in BaTiO3-Based PTC Ceramics
A.M. Yang, G.Z. Li, S.Y. Zhen and L.J. Liu ............................................................................... 248
Densification Behavior and Dielectric Properties of CaO-B2O3-SiO2 System Glass-
Ceramics Containing ZrO2
J.Z. Liu, Z.H. Yao, N.X. Xu, Q.L. Zhang and H. Yang............................................................... 253
Phase Evolution and Properties of Li2O-Al2O3-SiO2-Based Glass-Ceramic for LTCC
Applications
Z.J. Qing, B. Li, D.A. Duan, H. Li, Y.X. Li and S.R. Zhang ...................................................... 257
Influence of CeO2-Doping on the Electrical Properties of ZnO-Bi2O3-Based Varistor
Ceramics
Z.C. Cao, L.Y. Zheng, L.H. Cheng, T. Tian and G.R. Li ............................................................ 262
Preparation and Resistivity of Zirconia Oxygen Sensor Probe
B. Zhang, X.Z. Zhang, H. Wang, G.W. Liu, H.C. Shao and G.J. Qiao ....................................... 267
Performance of (Y2O3,V2O5) Co-Doping TiO2 Ceramics
G.M. Jiang, J.K. Yan, G. Yang, Z.C. Duan, K.Y. Kang, J.H. Du, G.Y. Gan and J.H. Yi ........... 271
V2O5-WO3/TiO2 Catalysts for Low Temperature NH3 SCR: Catalytic Activity and
Characterization
Y.X. Deng, X. Chen, R. Shao, L.M. Hu, J. Tang and C.Q. Wang ............................................... 275
Influences of Preparation Parameters of Catalyst Support on the SCR Denitration
Activity of Mn-Ce/TiO2
Y.X. Wu, H.L. Liang, X. Chen, J. Tang, Y.F. Chen and C.L. Zhao ............................................ 279
Photocatalytic Properties of WO3 Particles with Different Grain Sizes
Z.G. Shen, Z.J. Peng, J.W. Qian and X.L. Fu .............................................................................. 284
Effects of Eu and Ca Co-Substitution for the Improvement of Multiferroic
Properties of BiFeO3
X. Xu, Q.F. Yao, S. Peng, L.K. Fang, W.W. Mao, J.P. Yang and X.A. Li ................................. 288
Preparation and Mechanical Properties of BiFeO3 Ceramics
X.Y. Zhang, X.W. Qi, Z.Y. Yang, L. Bao and M. Zhang ............................................................ 293
Hardness and Electromagnetic Properties of YSZ/NiZn Ferrite Composites
L.D. Zhang, Z.X. Qu, Q. Wang and K. Waheed .......................................................................... 297
SiO2-Coated Fe-Ni Alloy Core–Shell Structures Synthesized by a Facile Chemical
Method
G.J. Li, Y.H. Mei and F. Hou....................................................................................................... 303
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Key Engineering Materials Vol. 697
Preparation and Magnetic Properties of Fe80Co20, Fe80Pt20 and Fe80Co20/Fe80Pt20
Bilayer Films
R.K. Pan, C. Zhou, F.L. Zhou and W.Q. Chao ............................................................................ 307
The Role of Aluminium Source (Al2O3/AlN) in the Synthesis of the Ca-α-
SiAlON:Eu2+
Phosphor
T. Pawlik, D. Michalik, M. Sopicka-Lizer, A. Miczek, P. Krzywda and R. Lisiecki ................. 311
Synthesis and Up-Conversion Luminescent Properties of Na(Y1.5Na0.5)F6 Hexagonal
Prism
C.P. Zhong, J.J. Zhang and S.W. Duo ......................................................................................... 318
Phase and Morphology Evolution of Manganese Oxides during Thermal Treatment
Y.C. Zhao, S. Li and C.A. Wang ................................................................................................. 322
Electrical Properties of Y0.06Sr0.94Ti0.6Fe0.4O3-δ-YSZ Composites as Electrode
Materials
K. Shan, X.M. Guo, F.R. Zhai and Z.Z. Yi.................................................................................. 327
Chapter 3: Ceramics for Structural Applications
Preparation and Performance of Monazite Coating on Woven Alumina Ceramic
Cloths
Y.Y. Liang and G.Y. Li ............................................................................................................... 333
Effect of Al Powder Content on Performance of MgO-Al2O3 Composite at 1700°C
under N2 Atmosphere
S.H. Tong, Y. Li, Y. Hong, D.D. Yue and J.J. Ma ...................................................................... 337
Effect of the Addition of Al Power on the Microstructure and Phase Constitution of
Al2O3-MgO Composites Sintered at 1700°C under N2 Atmosphere
J.J. Ma, Y. Li, S.H. Tong, D.D. Yue and Y. Hong ...................................................................... 341
Effect of the Addition of Al Powder on the Microstructure and Phase Constitution
of Magnesia-Spinel Composites Sintered at 1800°C in N2
Y. Hong, Y. Li, S.H. Tong, D.D. Yue and J.J. Ma ...................................................................... 345
Preparation and Characterization of Al-Al2O3 Metal Ceramics via Powder
Metallurgy Methods
D.M. Du, R.H. Wang, J.G. Song, S.Y. Yu, Y.Q. Li, N. Liu, G.L. Cao, S. Dong
and G.C. Ji .................................................................................................................................... 350
Microstructure and Mechanical Properties of Multiscale Zirconia Ceramics
Prepared by Field Assisted Sintering Technique
K. Eltayeb, D.Q. Jin, Y.H. Han, F. Chen, Q. Shen and L.M. Zhang ........................................... 354
Preparation and Characterization of Mullite Fiber-Reinforced Al2O3-SiO2 Aerogel
Composites
H. Chen, X.Y. Sui, C.L. Zhou, C.H. Wang, C.X. Yin and F.T. Liu ............................................ 360
Preparation of Small Size Ceria Stabilized Zirconia Microspheres by External
Gelation: Effect of Vibration Frequency
G.G. Wang, J.T. Ma, Y. Gao, X.Y. Zhao, S.C. Hao and C.S. Deng ............................................ 364
The Effect of Aging Temperature and pH Value of Aging Solution on the
Microstructure of ZrO2-SiO2 Aerogels
Y.C. Qiao, X.L. Li, J. He, H.M. Ji, Z.R. Shen and Z.P. Hu ......................................................... 368
Preparation and Characterization of Al2O3/ZrO2 Composite Ceramics
Y.Y. Ju, X.X. Gan, J.G. Song, F. Wang, W.N. Zhang and W.L. Yang ....................................... 372
High-Performance Ceramics IX
xiv
Thermal Insulation Property of Nanostructured Alumina Coated Zirconia Thermal
Barrier Coating
Z.Z. Yi, K. Shan, F.R. Zhai, H.Y. Sun and Z.P. Xie ................................................................... 377
Effect of the Cooling Ways on the Properties and Microstructure of ZrO2/ZrW2O8
Ceramic Composites
J.P. Li, C. Yang, S.H. Meng, F.J. Yi and Y.H. Li ........................................................................ 381
Influence of Temperature on the Order-Disorder Transition in Gd2Zr2O7
J.L. Shi, Z.X. Qu and Q. Wang .................................................................................................... 386
Synthesis and Characterization of LaMgAl11O19 as Thermal Barrier Coatings
Material
Z.Y. Huang, H.R. Lu and C.A. Wang .......................................................................................... 390
Effect of h-BN on Sintering Behavior, Microstructures and Mechanical Properties
of YAG Bulk Composites
S.B. Li, J.G. Song, H.Y. Ru and X.B. Bai ................................................................................... 395
Synthesis and Characterization of Magnesium Aluminate Spinel Porous Ceramics
by Novel Molten Salt Method
X.G. Deng, J.K. Wang, H.J. Zhang, J.H. Liu and S.W. Zhang.................................................... 399
Preparation and Performance of Neutron Absorbing Dysprosium Oxide Ceramic
Y.B. Zhang, Y.J. Zhang and J.X. Zhao ........................................................................................ 404
Characterization of SiO2 Aerogel/SiO2 Fiber Composites Prepared by Sol-Gel
Method
P. Zhai, X.F. Duan, Q.L. Zhang, H.S. Wang, H.H. Cheng and X.H. Zhang ............................... 409
Mechanically Strong and Hierarchical Porous Silica Ceramics via Gelcasting-
Lyophilization
W. Wan, J. Yang, Y.B. Feng and T. Qiu ..................................................................................... 414
Preparation and Properties of Acupuncture Quartz Fiber Reinforced Quartz-Based
Composites
Y.Y. Wang, Q.H. Wei, H.S. Wang, C.T. Shao, H.H. Cheng and Q.L. Zhang ............................. 419
Effect of Preparation Technology on Properties of Quartz Pore Gradient Materials
Using Low-Grade Quartz Sand
F. Wang, J.G. Song, M.H. Xu, S.B. Li, Y.Q. Li, S.Y. Yu, X. Li, G.L. Cao, S. Dong
and R.J. Liu .................................................................................................................................. 423
Preparation and Properties of Phenolic Resin Impregnated Quartz Fiber Tile
Ablative Composite
Y. Sun, L.P. Shi, C.L. Zhou, C.H. Wang and H.Z. Xu ................................................................ 428
Performance of Nano-Silica Insulation Material Enhanced by High Humidity-
Reinforcement Method
S.C. Zhang, Y.F. Chen, W. Wu, H.R. Sun, G.H. Wang, X.K. Sun, K. Fang
and F. Zhang ................................................................................................................................ 433
Effects of Concentrations of NaCl on the Sintering and Thermal Conductivity of
Forsterite
J. Ding, H.X. Zhu, C.J. Deng, D. Guo and H. Shang ................................................................... 437
The Effect of Particle Size of Expandable Graphite on the Properties of an
Expandable Thermal Insulation Material
K. Fang, Y.F. Chen, S.C. Zhang, H.R. Sun, G.H. Wang and X.K. Sun ...................................... 441
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Key Engineering Materials Vol. 697
Effect of Moisture Absorption on High Temperature Thermal Insulation
Performance of Fiber Insulation Materials
H.R. Sun, S.C. Zhang, S.G. Chen, G.H. Wang, L.S. Tao and Y.F. Chen .................................... 445
Optimized Design of Multilayer Thermal Insulations for Hypersonic Vehicles
G.H. Wang, F. Zhang, X.K. Sun, H.R. Sun, Y.L. Huo, S.C. Zhang and Y.F. Chen ................... 449
Effect of Binders on Preparation of High Temperature Rigid Thermal Insulation
Materials
J. Yang, R.X. Liu, X.Y. Sui, C.L. Zhou, C.H. Wang and W.Y. Zhang ....................................... 453
Influence of Sintering Aids on the Sintering and Conductivity Properties of Si3N4
Composites
Y. Jiang, L.E. Wu and W.X. Hai ................................................................................................. 457
Preparation and Properties of Si3N4-SiC Radar Wave-Absorbing Nanocomposites
P.P. Zhang, H.S. Wang, L. Li, L. Lv and Q.L. Zhang ................................................................. 462
Preparation of Sialon/Si3N4-SiC Composite Refractories Using Kyanite Tailings
M.H. Fang, Z.H. Huang, Y.G. Liu, X. Min and L.N. Zhang ....................................................... 467
Study on the Cause and Control of Defects on Process of CVD SiC
Y.L. Huo, H.L. Liu, C.Q. Hu, X.T. Huang, C.P. Wang, J. Tang and Y.F. Chen......................... 472
Fabrication of Mullite Coating and its Oxidation Protection for Carbon Fiber
Reinforced SiC Composites
K.H. Zeng, Q.S. Ma and L.H. Cai ................................................................................................ 476
Wetting and Interfacial Behavior of Molten Al on Mo-Ni(Co)-Si Coated SiC
Ceramic
S.T. Zhao, X.Z. Zhang, G.W. Liu, H.Y. Xia, Z.Q. Shi and G.J. Qiao ......................................... 481
Effect of Additives on Bond Property for Phenolic Resin-Based Adhesive
F. Zhang, G.H. Wang, Y.F. Chen, C.Q. Hu, H.R. Sun, S.C. Zhang, X.K. Sun
and K. Fang .................................................................................................................................. 485
Preparation and Properties of SiC/Si-B-C-N Ceramic Composites
M.W. Chen, H.P. Qiu and W.J. Xie ............................................................................................. 489
Preparation of B4C-ZrB2 Laminated Composites by Non-Aqueous Tape Casting
and Hot-Press Sintering
W.L. Liu, Z.T. Shi, Y.C. Li and Z.L. Xu ..................................................................................... 494
Structural-Functional Integrative Mullitef/SiBN Composites with Excellent Wave-
Transparent and Mechanical Properties
G.Y. Li, Y.Y. Liang and J.C. Liu ................................................................................................. 498
Effects of Viscosity and Pressure on Microstructure and Properties of Cf/SiC-ZrB2
Composites by PIP Process
K. Jiang, Y.Y. Wang, C.L. Zhou, H. Li and F.H. Yang .............................................................. 506
Microstructure and Mechanical Properties of ZrB2/h-BN Multiphase Ceramics by
Low-Temperature Reactive Sintering
F.R. Zhai, K. Shan, R.M. Xu, M. Lu, Z.Z. Yi and Z.P. Xie ........................................................ 510
Microstructures and Mechanical Properties of β-Sialon-cBN Composites
X.Z. Wu, Y. Wu, J.L. Han and T.Y. Shen ................................................................................... 515
High Pressure and High Temperature Sintered PcBN Using Al, B4C and C as
Sintering Additive
Y. Ma, J. Li, H.L. Wang and R. Zhang ........................................................................................ 521
High-Performance Ceramics IX
xvi
Influence of SiC on the Properties of PcBN Cutting Tools Fabricated by High
Pressure and High Temperature Sintering
S.X. Zhang, J. Li, Y. Ma, H.L. Wang and R. Zhang ................................................................... 526
Effect of Al and Si Additions on the Synthesis of Spark Plasma Sintered Zr2Al4C5
Creamic
Q.L. Guo, J.J. Pei, J.Z. Gan, J.G. Li and L.M. Zhang .................................................................. 530
Microstructure and Ablation Property of TaC-SiC Composite Coatings
Y.R. Niu, H. Pu, L.P. Huang, J. Zhao and X.B. Zheng ............................................................... 535
Preparation and Properties of TiB2-SiC-Si Composites Fabricated by Reaction
Bonding
C.P. Zhang, H.Q. Ru, R.P. He, W.K. Sun, J.H. Zhu, W. Wang and X.Y. Yue ........................... 539
Preparation and Properties of High-Purity Porous Calcium Hexaluminate Material
M.F. Wu, Y.B. Li, S.J. Li, Y.W. Li and S.B. Sang ...................................................................... 547
Gel Casting and Properties of SiCp/Al Composite
H.L. Liu, X.T. Huang, Y.L. Huo, C.Q. Hu, C.P. Wang, H.L. Liang and G.H. Wang ................. 551
Wetting and Interfacial Behaviors of Molten Ag, Cu and Ag-28Cu on WC-8Co
Cemented Carbide
H. Fu, X.Z. Zhang, G.W. Liu, Z.W. Xu, T.Z. Pan and G.J. Qiao ................................................ 555
Preparation of Glass-Ceramics by Reactive Crystallization with Waste Glass and
Mullite
W. Si, Z.Y. Wang, W.Y. Zhang and W. Pan ............................................................................... 561
Phase Equilibria in the BaO-SiO2-Al2O3 Ternary System at 1500 °C
R. Zhang and P. Taskinen ............................................................................................................ 565
Nitridation Isothermal Kinetics of In Situ β-Sialon Bonded Al2O3-C Refractories
X.Q. Yang, N. Peng and C.J. Deng .............................................................................................. 572
Effects of Al Content on the Phase Constitution of Aluminum-Periclase Composites
at 1600°C in N2
D.D. Yue, Y. Li, S.H. Tong, J.J. Ma and Y. Hong ...................................................................... 576
Effect of Spinel Content on the Reaction of Porous Periclase-Spinel Ceramics and
Cement Clinker
X.L. Lin, W. Yan, Q.J. Chen, N. Li, S.B. Ma and W.Y. Zhou .................................................... 581
Influence of Contents of Pre-Synthesized Spinel on the Microstructures and
Mechanical Properties of the Lightweight Corundum-Spinel Refractory Castables
Q.J. Chen, W. Yan, N. Li, X.L. Lin, W.Y. Zhou and L. Wang ................................................... 586
Effect of Sintering Temperature on the Physical Properties and Microstructure of
In Situ Nitrides Bonded MgAl2O4-C Refractories
S.H. Wang, C.J. Deng, H.X. Zhu and W.J. Yuan ........................................................................ 591
Effect of Particle Size Distribution of Raw Materials on Properties of Magnesia-
Alumina Refractory
Z.A. Chai, C.J. Deng, H.X. Zhu, X.J. Zhang and L.Y. Zhou ...................................................... 595
Preparation and Properties of Lightweight, High-Strength Insulation Materials
Using Fly Ash Floating Beads
Y.P. Dai, X.Y. Gu, W.X. Dong and T. Luo ................................................................................. 599
Effect of Zircon Content on the Microstructure and Physical Properties of
Chamotte Refractories
R.F. Xiang, Y.B. Li, S.J. Li, X.Y. Ma, Y.W. Li and S.B. Sang................................................... 604
xvii
Key Engineering Materials Vol. 697
Effects of Short PAN Fiber Contents on Mechanical Properties of Metakaolin-Blast
Furnace Slag Based Geopolymers
X.C. Luo and C.A. Wang ............................................................................................................. 608
Influence of Voltage on the Biological Performance of Micro-Arc Oxide Films Based
on TC4 Titanium Alloy
J.K. Yan, Y. Teng, E.X. Ni, Y.F. Wu, Y.H. Sun, S.M. Fang, Z. Shi and G. Yang ..................... 612
Influence of Voltage on Microstructure of Micro-Arc Oxide Films on TC4 Titanium
Alloy
Y. Teng, W.X. Tang, E.X. Ni, Y.F. Wu, Y.H. Sun, S.M. Fang, Z. Shi, G. Yang
and J.K. Yan ................................................................................................................................. 617
Effect of Thermal Oxidation Temperature on the Properties of Micro-Arc
Oxidation Ceramic Coating on TC4 Alloy
E.X. Ni, J.K. Yan, Y.F. Wu, Y. Teng, Z.C. Duan, G.M. Jiang, Y.H. Sun and G. Yang ............. 623
Chapter 4: Mechanical Properties of Ceramic Materials
The Effect of Thickness on the Fracture Strength and Failure Modes of Zirconia
Crowns
L.X. Zhang, R. Li, Y. Niu and Y.X. Liu ...................................................................................... 629
Effects of Sintering Temperature and Excess Zr on Mechanical Properties of
Reactive Hot-Pressed ZrB2-ZrCx-Zr Cermets
S.Q. Guo ....................................................................................................................................... 633
Mechanical Properties and Microstructure of 2.5D Cf/ZrO2 Composites Prepared
by Precursor Infiltration and Pyrolysis
J.P. Ai, S.S. Luo, W.K. Li, S.W. Wang and G.H. Zhou .............................................................. 639
Effects of Si3N4 Additions on Creep Resistance of Al-Al2O3 Composites
H.N. Shi, Y. Li, C.J. Li, H.X. Qin and J.L. Sun........................................................................... 644
Mechanical Properties of Polymer-Infiltrated-Feldspar for Restorative Composite
CAD/CAM Blocks
B.C. Cui, J. Li, H.N. Wang, Y.H. Lin, Y. Shen, M. Li and C.W. Nan ........................................ 648
Analysis on Low Cycle Fatigue Life and Fatigue Fracture Surface Morphology of
TC25 Titanium Alloy
R.G. Zhao, Y. Yan, Y.Z. Jiang, X.Y. Luo, Q.B. Li, Y.F. Liu, P. Cai and Y. Chen ..................... 652
Analysis on High Cycle Fatigue Properties and Fatigue Damage Evolution of TC25
Titanium Alloy
R.G. Zhao, Y.F. Liu, Y.Z. Jiang, X.Y. Luo, Q.B. Li, Y. Yan, P. Cai and Y. Chen ..................... 658
Research on Transition from Short to Long Fatigue Crack Propagation of
GH4133B Superalloy Used in Turbine Disk of Aero-Engine
R.G. Zhao, Q.B. Li, Y.Z. Jiang, X.Y. Luo, Y.F. Liu, Y. Yan, P. Cai and Y. Chen ..................... 664
Thermal Property of Cu/Ti3SiC2 FGM
Y.L. Chen, J. Li, S.S. Shan, W. Gao, Z.Y. Li and C.W. Zeng..................................................... 670
ZrO2 Ceramic Composite Added with MgAl2O4: Thermal Shock Resistance and
Corrosion Resistance in Molten Uranium
N. Yu, T. Zhang, S. Cai, D.D. Wang and L.P. Luo ..................................................................... 675
The Oxidation Resistance of ZrB2-SiC Composites Fabricated by High Pressure and
High Temperature Sintering
X.T. Zhao, H.L. Wang and R. Zhang ........................................................................................... 680
High-Performance Ceramics IX
xviii
Ablation Behavior of Low Pressure Plasma Sprayed TiB2-MoSi2 Composite
Coatings
L.P. Huang, Y.R. Niu, H. Li, M.S. Ren, X.B. Zheng and J.L. Sun ............................................. 685
Chapter 5: Emerging Inorganic Non-Metallic Materials
Synthesis of Carbon Nanotubes from Phenolic Resin Using Nickel Nitrate as a
Catalyst Precursor
J.K. Wang, X.G. Deng, H.J. Zhang, F.L. Li, C. Tan, L. Han and S.W. Zhang ........................... 691
Effects of Solvent on the Optical Nonlinearities of Multi-Walled Carbon Nanotubes
under the Picosecond Laser Pulses
Q. Chang and X.W. Liu ............................................................................................................... 695
Preparation and Characterization of ZrO2 Nanofibers and Nanobelts by
Electrospinning
Z.L. Liu, M.H. Fang, C. Tang, M. Wang, Y.J. Mao, Z.H. Huang, Y.G. Liu
and X.W. Wu ............................................................................................................................... 701
Preparation and Characterization of Vanadium Pentoxide Hollow Microspheres
with Tunable Sizes
M. Gong and C.A. Wang ............................................................................................................. 706
Synthesis of V6O13 Flowers-Like with Control pH for Li-Ion Battery Cathodes
Z.G. Zou, H.X. Chen, Q. Yuan and Z.L. Hou .............................................................................. 710
Synthesis and Antibacterial Activities of Ag/ZnO Nanoparticles
Y.W. Hu, H.R. He, X. Kong and Y.M. Ma.................................................................................. 714
Effects of Annealing Temperature and Coating Layers on Properties of ZnO Thin
Films Prepared by Sol-Gel Immerse Technique
C. Du, Y.C. Zou, Z.Q. Chen, W.K. Li and S.S. Luo ................................................................... 718
Composition, Structure and Electrical Resistivity of ZnO1-x Films Deposited by RF
Magnetron Sputtering under Various O2/Ar Gas Ratios
Y. Wang, Z.J. Peng, Q. Wang and X.L. Fu ................................................................................. 723
A Single-Phase Full-Color Ca4Si2O7F2:Ce3+
, Tb3+
, Sm3+
Micron Belt Mat for White-
Light Emitting Diode Application
B. Cui, Q.H. Zhang, H.Z. Wang and Y.G. Li .............................................................................. 727
Liquid Phase Deposited TiO2 Films on Stainless Steel Mesh for Corrosion
Resistance Application
T. Zhang, L. Xing, J.H. Xiang, H.Z. Sai, Z.Y. Li and R. Fu ....................................................... 733
A Metastable Ion (III) Oxide Phase (ε-Fe2O3): Preparation and Gas Sensing
Properties
M.J. Wang, H.M. Ji, Y.L. Chen and Q.Q. Jia .............................................................................. 737
Influence of Addition of Fe2O3 and CaO on the Performance of Manual SHS
Welding Slag
Z.Z. Li, F.Q. Han, L.M. Sun, X.F. Han and W.T. Xin ................................................................ 741
Photocatalytic Behaviors Observed in Microstructured PbS under Visible Light
L.N. Qiao, H.C. Wang, Y. Shen, Y.H. Lin and C.W. Nan .......................................................... 745
Immobilization of Laccase in Glycidoxypropyl-Functionalized Magnetic
Mesoporous SiO2/Fe3O4 Hollow Microspheres
P.Y. Wang, Q.Y. Li, Y.L. Zhou, Q. Wei and Z.R. Nie ................................................................ 749
xix
Key Engineering Materials Vol. 697
Control of Preferential Orientation of La1-xSrxMnO3 Thin Films by Pulsed Laser
Deposition
Y.X. Zhu, C.B. Wang, Q. Shen and L.M. Zhang ......................................................................... 756
Study on Zeolite X Complexing Dimethyl Potassium
Y. Hu, N.C. Chen, H. Xu, L.J. Yang, L.L. Ma, C. Wu, S.J. Luo, Y.C. Pei and S.S. Gao ........... 761
Research Progress of Adsorption on Heavy Metals from Aqueous Solutions by
Modified Diatomite
H. Li, Q.L. Xie, N.C. Chen, H. Xu and L.L. Ma ......................................................................... 766
Formation Mechanisms of the Point Defects from the 4H-SiC (0001) Surface to the
Interior Layers: First Principle Calculation
Z.W. Shao, Z.W. Xu, X.Y. Zhang, G.W. Liu, H.H. Li and G.J. Qiao ......................................... 771
Effect of Bias Voltage on Microstructure and Mechanical Properties of CrN
Coatings Prepared by Single Target Magnetron Sputtering
C.G. Luo, H. Zhang, J. Shang and S.W. Duo .............................................................................. 777
Dual-Functional Phase Change Nanocapsules Based on n-Octadecane Core and
Polypyrrole Shell
Y.Y. Yang, H. Wang, G.L. Song and G.Y. Tang ........................................................................ 781
Influence of Pre-Oxidation on the Morphology of Mesocarbon Microbeads
Y.M. Zhu, X.F. Zhao, L.J. Gao, S.Q. Lai and Y.Y. Lian ............................................................ 785
Coalescence of the Fullerenes in SWNT with Bend Junction
K. Zhang, Z.W. Xu, F. Ding, G.W. Liu and G.J. Qiao ................................................................ 789
Chapter 6: Ceramics for Next Generation Nuclear Power
Principle Design of Graphite Components for HTTR and R&D on Nuclear Graphite
for HTGR in JAEA
J. Sumita, T. Shibata, T. Iyoku, M. Ishihara and T. Nishihara .................................................... 797
Sintering of SiC Coating Layer on Graphite Spheres Prepared by Pack
Cementation
P. Zhou, Z.Q. Li, H.S. Zhao, K.H. Zhang, X.X. Liu and B. Liu ................................................. 807
Preparation of Li4SiO4 Ceramic Pebbles by Agar Method Using Li2SiO3 and Li2CO3
as Raw Materials
M.Q. Xiang, Y.C. Zhang, Y. Zhang, C.F. Wang and Y.H. Yu .................................................... 814
Preparation and Characterization of Lithium Orthosilicate Ceramic Pebbles by
Melt Spraying Method
Y.W. Zhai, J. Hu, X.Q. Zhu, K.J. Wang and W.J. Zhang ............................................................ 818
Characterization of the Tracer YSZ/CoO Microspheres with YSZ Ceramic Coating
for HTR Fuel Element
Z.Q. Li, J.T. Ma, X.X. Liu and B. Liu ......................................................................................... 822
Processing and Thermal Properties of Multiwall Carbon Nanotube/Bismuth
Antimony Telluride Composites for Nuclear Energy Applications
K. Ahmad, C.L. Wan, M.A. Al-Eshaikh, A.N. Kadachi, R. Khan and H.S. Abdo ..................... 826
Preparation of UCO Microspheres by Internal Gelation Process
X.Y. Zhao, J.T. Ma, Y. Gao, S.C. Hao, C.S. Deng, B. Liu and Y.P. Tang ................................. 831
Preparation and Performance of Fully Ceramic Fuel Element Using Silicon Carbide
as Coating Layers
R.Z. Liu, M.L. Liu, J.X. Chang, Y.L. Shao, B. Liu and C.S. Deng ............................................. 835
High-Performance Ceramics IX
xx
Preparation of Silicon Carbide Nanowires and Nanochains Using Chemical Vapor
Deposition Method
J.X. Chang, R.Z. Liu, M.L. Liu, Y.L. Shao and B. Liu ............................................................... 841
Preparation of Silicon Carbide Coating Layer by Fluidized Bed Chemical Vapor
Deposition Using a Halogen-Free Precursor
M.L. Liu, R.Z. Liu, J.X. Chang and Y.L. Shao ........................................................................... 846
Effect of PyC Thermal Behavior on the Stress of TRISO-Coated Fuel Particles
R. Li, B. Liu and C.H. Tang ......................................................................................................... 852
Keyword Index ............................................................................................................................... 859
Author Index .................................................................................................................................. 867