conditioning the new bag day 1: 25 feb 2008. particle number concentration (wcpc 3786) lights on at...

29
Conditioning the new bag DAY 1: 25 Feb 2008

Post on 21-Dec-2015

215 views

Category:

Documents


0 download

TRANSCRIPT

Page 1: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

Conditioning the new bag

DAY 1: 25 Feb 2008

Page 2: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

Particle number concentration (wcpc 3786)

Lights on at 15:58

Page 3: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

DMPS after one hour of lights on

Mass = 11 ugm-3 (density 1), mode about 52 nm

Page 4: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

Status at the end of day 1 of cleaning

• After about 2 hours of lights on, 17 ugm-3 of mass (DMPS) were formed in the chamber and particle size mode was about 70 nm. The bag was flushed and post exp procedures were perfumed. The bag was left full of ozone overnight.

Page 5: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

New bag Cleaning: Day 2Tuesday 26 Feb 2008

• Started at 08:50. Bag had 6500 p/cc.

• Flushed the bag

• Started pre-exp procedures

Page 6: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

Particle number dropped to 40p/cc after the first flush

Page 7: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

First fill is complete: 17p/cc

Page 8: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

Completed 3 flush/fill cyclesBag is now in flushed position and being tested for leaks…started test at 09:45 and there was a small increase in number but not close to our

previous problem!

Page 9: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

Ozonolysis increased number dramatically! Lights were turned on at 10:17

Page 10: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

Mass and number after 50min of lights on

9.8 ugm-3 and 1.2e5 p/cc

Page 11: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

CPC problem!!

Page 12: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

• 16:45 lights off (i.e. cleaned for more than 6 hours)

• Post-exp procedures started

• Bag was left full of O3 overnight

Page 13: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

18:11Post-exp procedure completed. The Ozone box thinks there is 720 ppb of O3 in the bag

Page 14: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

New Bag Cleaning

Day 3: 27 Feb 2008

Page 15: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

• Bag was left full of ozone over night

• Flushed the bag and started the pre-exp procedures

• Completed 4 fill/flush cycles

• Ozone at the beginning is 1.2ppm

Page 16: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

Lights on at 10:09

Yellow error sign saying CPC is still in warm up mode (flow range and temp errors)

Page 17: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

Last scan before lights on measured 13 ugm-3!! (note the long DMA scan!!)

Page 18: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

First scan after lights on measured 77 ugm-3!! (note the long DMA scan!!)

DMPS appears to be wet and arcing at high voltages.. The reported mass is wrong

Page 19: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

DMPS, mass=9.08, 1 hour after lights on, no arcing on this scan

Page 20: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

11:49

Page 21: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

End of day 3

• Lights were switched off after 5 hours

• Flushed the bag

• Performed post-exp procedure

• Last fill was done manually with O3 pulsing

• Bag was left with 870 ppb of O3 overnight

C:\elena\Tank_Feb_08

Page 22: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

New Bag Cleaning

Day 4: 28 Feb 2008

Page 23: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

First background Exp

• Flushed the bag from the overnight o3 fill

• Pre-exp procedure to cycle fill/flush for 4 times

• Final fill via humidifier and inject NOx

• Humidifier is NOT working!! Change of plans

• Another harsh cleaning day (O3 + lights)

• 980 ppb O3 according to ozone box

Page 24: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

Bag is flushed and still: note particle number is slightly increasing (could be mixing or small leak)

Most likely it is fresh nucleation! Do it again next time with doors closed

Page 25: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

Immediate response to ozone

Page 26: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

Response to lights (on at 10:49)

Page 27: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

First 10 min after lights on

Page 28: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

Fab!! It is now down to 2.3 ugm-3 after 1 hour of lights on

Page 29: Conditioning the new bag DAY 1: 25 Feb 2008. Particle number concentration (wcpc 3786) Lights on at 15:58

CPC problem appears to be coming back