cooley – main linac - 2008 ilcta 1 summary of the srf materials workshop held 29-31 october at...

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Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab http://meetings.nscl.msu.edu/srfmat sci/ Presented by Lance Cooley SRF Materials Group Leader, Fermilab On behalf of the Program Committee

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Page 1: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 1

Summary of the

SRF Materials Workshop

held 29-31 October at Michigan State Univ.

hosted by MSU, NSCL, and Fermilabhttp://meetings.nscl.msu.edu/srfmats

ci/

Presented by Lance Cooley

SRF Materials Group Leader, Fermilab

On behalf of the Program Committee

Page 2: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 2

Overview

• Fourth in a series of largely domestic workshops in the spirit of the Gordon Conferences

• General themes: end-use pull, industry achievements, materials science, processing innovations, fundamentals and tutorials

• Attendees are 40% Academic, 40% Lab, 20% Industry / Small Business

• Charge: Build connections between fundamental materials science and SRF technology to understand limits, validate processes, and seek breakthroughs inperformance. 

Page 3: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 3

Program

1. Materials R&D Drivers – updates from ILC, TTC, and other recent cavity tests

2. Removing or Avoiding Extrinsic Performance Limits• Focus on possible origins of weld / etch pits: do they originate

from sheet forming? Welding? Electropolishing?

3. Understanding and Achieving Intrinsic Limits• Overviews of atomic layer deposition and flux-line heating

4. Beyond Niobium

5. Processing Science and Innovations

6. Seamless Forming• Tutorial on seamless forming

Page 4: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 4

Program

1. Materials R&D Drivers – updates from ILC, TTC, and other recent cavity tests

2. Removing or Avoiding Extrinsic Performance Limits• Focus on possible origins of weld / etch pits: do they originate

from sheet forming? Welding? Electropolishing?

3. Understanding and Achieving Intrinsic Limits• Overviews of atomic layer deposition and flux-line heating

4. Beyond Niobium

5. Processing Science and Innovations

6. Seamless Forming• Tutorial on seamless forming

Page 5: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 5

Below: Cross-section of defect cut, polished, and imaged by orientation microscopy at Florida State

1 grain

FNAL 3D microscopy

Weld pits have been made in the laboratory

Page 6: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 6

Welding

• Bob Salo – Sciaky• A moving electron gun

may be preferred to a moving work piece

• A 50 µm “defect” is not recognized as a defect in post-weld QA. “Weld porosity” is typically quoted in the 0.2 mm range and higher.

Page 7: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 7Prof. Tom Bieler

Page 8: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 8Tom Bieler

Page 9: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 9C. Reese

Page 10: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 10C. Reese

Page 11: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 11

Program

1. Materials R&D Drivers – updates from ILC, TTC, and other recent cavity tests

2. Removing or Avoiding Extrinsic Performance Limits• Focus on possible origins of weld / etch pits: do they originate

from sheet forming? Welding? Electropolishing?

3. Understanding and Achieving Intrinsic Limits• Overviews of atomic layer deposition and flux-line heating

4. Beyond Niobium

5. Processing Science and Innovations

6. Seamless Forming• Tutorial on seamless forming

Page 12: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 12Ciovatti and Gurevich

Flux “annealing” redistributes hot spotsMore effective in large-grain cavities due to lower pinning

Page 13: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 13

Atomic Layer Deposition appears to work

Page 14: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 14

Permanent cavity coatings?

Page 15: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 15

Explanation of the baking effect?

J. Zasadzinski, T Proslier, M PellinOxygen defects in Nb2O5 are magnetic, break Cooper pairs when close. But they can be annealed away.

Page 16: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 16

Evaluation of flux penetration into a grain boundary

BCP caused a groove to form in the isolated grain boundary, which caused it to admit magnetic flux

Page 17: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 17

A better way to assess roughness

Power spectral density incorporates roughness data from nanometer to millimeter scales

Why is scaling observed over 4 decades?

Data sets taken overdifferent sampling areas

Page 18: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 18

Program

1. Materials R&D Drivers – updates from ILC, TTC, and other recent cavity tests

2. Removing or Avoiding Extrinsic Performance Limits• Focus on possible origins of weld / etch pits: do they originate

from sheet forming? Welding? Electropolishing?

3. Understanding and Achieving Intrinsic Limits• Overviews of atomic layer deposition and flux-line heating

4. Beyond Niobium

5. Processing Science and Innovations

6. Seamless Forming• Tutorial on seamless forming

Page 19: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 19

Seamless cavity forming – avoid welds

Page 20: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 20

Niobium tubes

Page 21: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 21

Page 22: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 22Hartwig – TAMU, Crooks – Black Labs

Page 23: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 23

Summary

Page 24: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 24

C. Reese

Page 25: Cooley – Main Linac - 2008 ILCTA 1 Summary of the SRF Materials Workshop held 29-31 October at Michigan State Univ. hosted by MSU, NSCL, and Fermilab

Cooley – Main Linac - 2008 ILCTA 25

C. Reese