1 BOOKS, REVIEWS & SYMPOSIA

A review on the electron ionization and fast atom bombardment mass spectro-metry of polyphenols naturally occurring in olive wastes and some of theirsynthetic derivativesCapasso R// Univ di Napoli “Federico II”, Dipt Sci Chim-Agr, IT-80055 Por-tici, ItalyPhytochem Anal 1999 10 (6) 299

Special feature: Tutorial - Simulation of ion trajectories in a quadrupole iontrap - A comparison of three simulation programsForbes MW, Sharifi M, Croley T, Lausevic Z, March RE// Trent Univ, DeptChem, Peterborough, Ontario, Canada K9J 7B8J Mass Spectrom 1999 34 (12) 1219

An introduction to the time-of-flight techniqueHakansson P// Angstrom Lab, Div Ion Phys, Box 534, SE-75121 Uppsala,SwedenBraz J Phys 1999 29 (3) 422

Protein folding and interactions revealed by mass spectrometry (Review)Last AM, Robinson CV// Oxford Ctr Mol Sci, Sth Pk Rd, Oxford OX1 3QT,EnglandCurr Opin Chem Biol 1999 3 (5) 564

Mass spectrometry of biomolecules: From PDMS to MALDIMacfarlane RD// Texas A&M Univ, Dept Chem, College Station, Tx 77843,USABraz J Phys 1999 29 (3) 415

Quantitative analysis of pharmacokinetic study samples by liquid chromatog-raphy coupled to tandem mass spectrometry (LC-MS/MS) (Review)Muck M// Bayer AG, Inst Clin Pharmacol, Clin Pharmacokinet, ApratherWeg, GEB 470, DE-42096 Wuppertal, GermanyPharmazie 1999 54 (9) 639

ICP-MS for the determination of trace elements in clinical samples (Mini-Review)Stastna M, Nemvoca I, Zyka J// Charles Univ, Dept Analyt Chem, Albertov2030, CZ-12843 Prague 2, Czech RepublicAnal Lett 1999 32 (13) 2531

Meeting report: The XVIIth Informal Meeting on Mass SpectrometryVekey K// Hungarian Acad Sci, HungaryJ Mass Spectrom 1999 34 (12) 1287

2 INSTRUMENTAL TECHNIQUES & METHODS

Potential sputtering: Desorption from insulator by impact of slow multi-charged ionsAumayr F, Varga P, Winter HP// Vienna Tech Univ, Inst Allgemeine Phys,Wiedner Hauptstr 8-10, AU-1040 Vienna, AustriaInt J Mass Spectrom 1999 192 415

Multiple K- and L-shell ionizations of target atoms by collisions with high-energy heavy ionsAwaya Y, Kambara T, Kanai Y// Musashino Art Univ, Kodaira, Tokyo 1878505, JapanInt J Mass Spectrom 1999 192 49

Laser control of molecular ionization with intense short laser pulsesBandrauk AD, Yu HT// Univ Sherbrooke, Fac Sci, Chim Theor Lab, Sher-brooke, Quebec, Canada J1K 2R1Int J Mass Spectrom 1999 192 379

A design for low-flow sheathless electrospray emittersBarnidge DR, Nilsson S, Markides KE*// *Univ Uppsala, Dept Analyt Chem,Box 531, SE-75121 Uppsala, SwedenAnal Chem 1999 71 (19) 4115

Ion mobility spectrometry: Arriving on site and moving beyond a low profileBaumbach JI, Eiceman GA// Inst Spektrochem & Angew Spektrosk, BunsenKirchhoff Str 11, DE-44139 Dortmund, GermanyAppl Spectrosc 1999 53 (9) A338

Microfabricated polymer devices for automated sample delivery of peptidesfor analysis by electrospray ionization tandem mass spectrometryChan JH, Timperman AT, Qin D, Aebersold R*// *Univ Washington, DeptMol Biotechnol, Box 357730, Seattle, Wa 98195, USAAnal Chem 1999 71 (20) 4437

The use of a porous graphitic carbon column for desalting hydrophilic pep-tides prior to matrix-assisted laser desorption/ionization time-of-flight massspectrometryChin ET, Papac DI// Genentech Inc, 1 DNA Way, Sth San Francisco, Ca94080, USAAnal Biochem 1999 273 (2) 179

Postcolumn introduction of an internal standard for quantitative LC-MS analy-sisChoi BK, Gusev AI, Hercules DM*// *Vanderbilt Univ, Dept Chem, 221Kirkland Hall, Nashville, Tn 37235, USAAnal Chem 1999 71 (18) 4107

Precision and accuracy of lifetimes of metastable levels using the Kingdontrap techniqueChurch DA, Moehs DP, Bhatti MI// Texas A&M Univ, Dept Phys, CollegeStation, Tx 77843, USAInt J Mass Spectrom 1999 192 149

Digital quadrature heterodyne detection for high-resolution Fourier transformion cyclotron resonance mass spectrometryDrader JJ, Shi SDH, Blakney GT, Hendrickson CL, Laude DA, MarshallAG*// *Florida State Univ, Natl High Magnet Field Lab, Ctr InterdisciplinaryMagnet Resonance, Tallahassee, Fl 32310, USAAnal Chem 1999 71 (20) 4758

Thermal energy distribution observed in electrospray ionizationDrahos L, Heeren RMA, Collette C, De Pauw E, Vekey K*// *HungarianAcad Sci, Inst Chem, Pusztaszeri ut 59-67, HU-1025 Budapest, HungaryJ Mass Spectrom 1999 34 (12) 1373

Delayed extraction for improved resolution of ion/surface collision productsby time-of-flight mass spectrometryHaney LL, Riederer DE*// *Univ Missouri, Dept Chem, Columbia, Mo 65211,USAAnal Chim Acta 1999 397 (1-3) 225

Scattering of multiply charged ions from surfacesHatke N, Robin A, Grether M, Narmann A, Heiland W*// *Univ Osnabruck,DE-49069 Osnabruck, GermanyInt J Mass Spectrom 1999 192 393

Advantages of pressurization in capillary electrophoresis/electrospray ioniza-tion mass spectrometryHau J, Roberts M*// *Nestec Ltd, Nestle Res Ctr, Vers Chez Les Blanc, CasePostale 44, CH-1000 Lausanne 26, SwitzerlandAnal Chem 1999 71 (18) 3977

Ligand fishing by mass spectrometryHeck AJR// Utrecht Inst Pharmaceut Sci, Bijvoet Ctr Biomolec Res, Dept Bio-molec Mass Spectrom, Sorbonnelaan 16, NL-3584 CA Utrecht, The Nether-landsSpectrosc Eur 1999 11 (6) 12

Identification of aromatic compounds on a single microparticle by laser de-sorption/ionization ion trap mass spectrometryHong K, Song K*, Cha H, Yang M, Lee J, Lee G// *Korea Atom Energy ResInst, Lab Quantum Opt, Taejon 305600, South KoreaMicrochem J 1999 63 (1) 9

Analysis of product species in capacitively coupled C5F8 plasma by electronattachment mass spectroscopyImai S, Tachibana K// Matsushita Elect Corp, Ulsi Proc Technol Dev Ctr, Mi-nami ku, 19 Nishikujo Kasugacho, Kyoto 601 8413, JapanJpn J Appl Phys Pt 2 1999 38 (8A) L888

Comparison of plasma sample purification by manual liquid-liquid extraction,automated 96-well liquid-liquid extraction and automated 96-well solid-phaseextraction for analysis by high performance liquid chromatography with tan-dem mass spectrometryJemal M, Teitz D, Ouyang Z, Khan S// Bristol Myers Squibb Pharmaceut Res

JOURNAL OF MASS SPECTROMETRYJ. Mass Spectrom. 35, 279–287 (2000)

Current Literature in Mass Spectrometry

(6 weeks journals - Search completed at 24th Nov. 1999)

In order to keep subscribers up-to-date with the latest developments in their field, John Wiley & Sons are providing a current awareness service in each issue of thejournal. The bibliography contains newly published material in the field of mass spectrometry. Each bibliography is divided into 11 sections: 1 Books, Reviews &Symposia; 2 Instrumental Techniques & Methods; 3 Gas Phase Ion Chemistry; 4 Biology/Biochemistry: Amino Acids, Peptides & Proteins; Carbohydrates; Lipids;Nucleic Acids; 5 Pharmacology/Toxicology; 6 Natural Products; 7 Analysis of Organic Compounds; 8 Analysis of Inorganics/Organometallics; 9 Surface Analysis;10 Environmental Analysis; 11 Elemental Analysis. Within each section, articles are listed in alphabetical order with respect to author.

CCC 1076–5174/2000/020279–09 $17.50Copyright © 2000 John Wiley & Sons, Ltd.

Inst, Bioanalyt Res Metab & Pharmacokinet, POB 191, New Brunswick, NJ08903, USAJ Chromatogr B 1999 732 (2) 501

Electron impact ionization in a microion trap mass spectrometerKornienko O, Reilly PTA, Whitten WB, Ramsey JM// Oak Ridge Natl Lab,POB 2008, Oak Ridge, Tn 37831, USARev Sci Instrum 1999 70 (10) 3907

Surface reaction kinetics on the atomic scale: Studies by means of pulsed fielddesorption mass spectrometryKruse N// Free Univ Brussels, CP 243, Campus Plaine, BE-1050 Brussels,BelgiumMater Sci Eng A Struct Mater 1999 270 (1) 75

Desorption and sputtering from solids induced by polyatomic projectilesLe Beyec Y, Baudin K, Brunelle A, Della Negra S, Jacquet D, Pautrat M//Inst Phys Nucl, CNRS, IN2P3, BP 1, FR-91406 Orsay, FranceBraz J Phys 1999 29 (3) 428

Mass spectrometry detection versus flame ionisation detection in pyrolysis-gaschromatography: Spurious pyrolysis peaks and possible errors in estimatingrelative product yieldsLehrle RS, Rollinson M, Dadvand N, Parsons IW// Univ Birmingham, SchChem, POB 363, Birmingham B15 2TT, EnglandPolym Degrad Stabil 1999 66 (2) 221

Size-exclusion chromatography with on-line ultraviolet, proton nuclear mag-netic resonance and mass spectrometric detection and on-line collection foroff-line Fourier transform infrared spectroscopyLudlow M, Louden D, Handley A, Taylor S, Wright B, Wilson ID*// *ZenecaPharmaceut, Alderley Pk, Macclesfield SK10 4TG, EnglandJ Chromatogr A 1999 857 (1-2) 89

Influence of ionization energy on charge-transfer ionization in matrix-assistedlaser desorption/ionization mass spectrometryMacha SF, McCarley TD, Limbach PA*// *Louisiana State Univ, Dept Chem,Baton Rouge, La 70803, USAAnal Chim Acta 1999 397 (1-3) 235

Nature of noise in SIMS depth profiling dataMakarov VV// Copenhagen Univ Observatory, Juliane Maries Vej 30, DK-2100 Copenhagen O, DenmarkSurf Interface Anal 1999 27 (9) 801

Time ordering in fast double ionizationMcGuire JH, Godunov AL, Tolmanov SG, Schmidt-Bocking H, Dorner R,Mergel V, Dreizler R, Shore BW// Tulane Univ, Dept Phys, New Orleans, La70118, USAInt J Mass Spectrom 1999 192 65

Electron cyclotron resonance ion sources of highly charged ions: From classi-cal to superconducting sourcesMelin G// CEA, Dept Rech Fondamentale Mat Condensee, Serv Ions Atoms &Agregats, 17 rue Martyrs, FR-38054 Grenoble 9, FranceInt J Mass Spectrom 1999 192 87

Fully relativistic calculations of cross sections for electron impact ionisation ofcarbon-like uranium ionsMoores DL// UCL, Dept Phys & Astron, Gower St, London WC1E 6BT, Eng-landInt J Mass Spectrom 1999 192 23

State-of-the-art in liquid chromatography-mass spectrometryNiessen WMA// Hyphen Mass Spec Consultancy, De Wetstr 8, NL-2332 XTLeiden, The NetherlandsJ Chromatogr A 1999 856 (1-2) 179

Detection of reaction selectivity on catalyst libraries by spatially resolvedmass spectrometryOrschel M, Klein J, Schmidt HW, Maier WF*// *Max Planck Inst Kohlen-forsch, DE-45470 Mulheim, GermanyAngew Chem Int Ed 1999 38 (18) 2791

Species selective analysis by microcolumn multicapillary gas chromatographywith inductively coupled plasma mass spectrometric detectionRodriguez I, Mounicou S, Lobinski R, Sidelnikov V, Patrushev Y, YamanakaM// CNRS EP132, 2 Ave Pr Angot, Helioparc, FR-64053 Pau, FranceAnal Chem 1999 71 (20) 4534

Mass spectrometry in identification and characterization of biopolymersRoepstorff P// Odense Univ, Dept Mol Biol, Campusvej 55, DK-5230 OdenseM, DenmarkBraz J Phys 1999 29 (3) 440

High-throughput testing of heterogeneous catalyst libraries using array mi-croreactors and mass spectrometrySenkan S, Krantz K, Ozturk S, Zengin V, Onal I// UCLA, Dept Chem Engn,Los Angeles, Ca 90095, USAAngew Chem Int Ed 1999 38 (18) 2794

Capillary column supercritical fluid chromatography-atmospheric pressureionisation mass spectrometry: Interface performance of atmospheric pressurechemical ionisation and electrospray ionisationSjoberg PJR, Markides KE*// *Univ Uppsala, Inst Chem, Dept Analyt Chem,POB 531, SE-75121 Uppsala, SwedenJ Chromatogr A 1999 855 (1) 317

Superheated heavy water as the eluent for HPLC-NMR and HPLC-NMR-MS

of model drugsSmith RM, Chienthavorn O, Wilson ID, Wright B, Taylor SD// LoughboroughUniv Technol, Dept Chem, Loughborough LE11 3TU, EnglandAnal Chem 1999 71 (20) 4493

Liquid chromatography-inductively coupled plasma mass spectrometrySutton KL, Caruso JA// Univ Cincinnati, Dept Chem, PO Box 172, Cincinnati,Oh 45221, USAJ Chromatogr A 1999 856 (1-2) 243

Multiple ionization of negative and positive ions, neutral atoms, and moleculesunder electron impact: Data and databasesTawara H, Shevelko VP// Natl Inst Fus Sci, 322-6 Oroshi-cho, Toki-shi 5095292, JapanInt J Mass Spectrom 1999 192 75

Photon observations on excited multiply charged ionsTrabert E// Ruhr Univ, DE-44780 Bochum, GermanyInt J Mass Spectrom 1999 192 347

Packed column supercritical fluid chromatography/mass spectrometry for highthroughput analysis. Part IIVentura MC, Farrell WP, Aurigemma CM, Greig MJ*// *Alanex Corp, 3550Gen Atom Court, San Diego, Ca 92121, USAAnal Chem 1999 71 (19) 4223

Temperature as a sample preparation tool in the analysis of materials by GC-MSWampler TP// Cos Analyt Inc, 465 Limestone Rd, Oxford, Pa 19363, USALC GC-Mag Separation Sci 1999 17 (9 Suppl) S14

Kinetically labile equilibrium shifts induced by the electrospray processWang HJ, Agnes GR*// *Simon Fraser Univ, Dept Chm, Burnaby, Brit Co-lumbia, Canada V5A 1S6Anal Chem 1999 71 (19) 4166

The state of the art in thin-layer chromatography-mass spectrometry: A criticalappraisalWilson ID// Zeneca Pharmaceut, Dept Safety Med, Macclesfield SK10 4TG,EnglandJ Chromatogr A 1999 856 (1-2) 429

Kinetic electron emission in the near-threshold region studied for differentprojectile chargesWinter HP, Eder H, Aumayr F// Tech Univ Vienna, Inst Allgemeine Phys,AU-1060 Vienna, AustriaInt J Mass Spectrom 1999 192 407

Determination of the sensitivity of an external source ion trap tandem massspectrometer using dimethyl ether chemical ionization (Letter)Wu HF, Lin YP// Tamkang Univ, Dept Chem, Tamsui, Taipei, Hsien 25137,TaiwanJ Mass Spectrom 1999 34 (12) 1283

Internal calibrant for an exact mass measurement in electrospray ionizationmass spectrometryYamaguchi K, Sakamoto S, Imamoto T, Ishikawa T// Chiba Univ, Ctr ChemAnal, Yayoi, Chiba 263 8522, JapanAnal Sci 1999 15 (10) 1037

Beam capillary spectroscopyYamazaki Y// Univ Tokyo, Inst Phys, Meguro ku, 4-6-1 Komaba, Tokyo 1538902, JapanInt J Mass Spectrom 1999 192 437

3 GAS PHASE ION CHEMISTRY

Absolute cross sections for near-threshold electron-impact excitation of Be-like C2+, N3+, and O4+ ionsBannister ME, Djuric N, Woitke O, Dunn GH, Chung YS, Smith ACH, Wall-bank B, Berrington KA// Oak Ridge Natl Lab, Div Phys, Oak Ridge, Tn37831, USAInt J Mass Spectrom 1999 192 39

Long lived CH2+ and CD2+ dicationsBenitzhak I, Sidky EY, Gertner I, Levy Y, Rosner B// Kansas State Univ,Dept Phys, James R MacDonald Lab, Manhattan, Ks 66506, USAInt J Mass Spectrom 1999 192 157

Spontaneous and induced dissociation of singly and multiply charged fullereneionsBiasioli F, Fiegele T, Mair C, Senn G, Matt S, David R, Sonderegger M, Sta-matovic A, Scheier P, Mark TD*// *Comenius Univ, Dept Plasma Phys,Mlynska Dolina F2, SK-84215 Bratislava, SlovakiaInt J Mass Spectrom 1999 192 267

Reactivity and characterization of transition-metal carbonyl clusters using UVlaser desorption mass spectrometryCritchley G, Dyson PJ*, Johnson BFG, McIndoe JS, O’Reilly RK, Lang-ridge-Smith PRR// *Univ York, Dept Chem, York YO10 5DD, EnglandOrganometallics 1999 18 (20) 4090

Calculation of cross sections and rate coefficients for the electron impact mul-tiple ionization of beryllium, boron, carbon, and oxygen atomsDeutsch H, Becker K, Senn G, Matt S, Mark TD*// *Innsbruck Univ, InstIonenphys, AU-6020 Innsbruck, AustriaInt J Mass Spectrom 1999 192 1

Copyright © 2000 John Wiley & Sons, Ltd J. Mass Spectrom. 35, 279–287 (2000)

280 CURRENT LITERATURE IN MASS SPECTROMETRY

Metal clusters under strong laser field conditionsDoppner T, Teuber S, Schumacher M, Tiggesbaumker J*, Meiwes-Broer KH//*Univ Rostock, Fachbereich Phys, DE-18055 Rostock, GermanyInt J Mass Spectrom 1999 192 387

Multifragmentation after multi-ionization of hydrogen clusters in high energycluster-atom and cluster-cluster collisionsFarizon B, Farizon M*, Gaillard MJ// *Inst Phys Nucl, CNRS IN2P3, 43 Blvd11 Novembre 1918, FR-69622 Villeurbanne, FranceInt J Mass Spectrom 1999 192 259

Fragmentation dynamics of SO22+

Field TA, Eland JHD// Phys & Theoret Chem Lab, Sth Parks Rd, Oxford OX13QZ, EnglandInt J Mass Spectrom 1999 192 281

Femtosecond laser interactions with methyl iodide clusters. II. Coulomb ex-plosion at 397 nmFord JV, Poth L, Zhong Q, Castleman AW*// *Penn State Univ, Dept Chem,152 Davey Lab, University Park, Pa 16802, USAInt J Mass Spectrom 1999 192 327

Gas-phase ion-molecule reactions in organophosphorus estersGal JF, Herreros M, Maria PC, Operti L*, Pettigiani C, Rabezzana R, VaglioGA// *Univ Torino, Dipt Chim Gen & Organ Applicata, Corso Massimod’Azeglio 48, IT-10125 Turin, ItalyJ Mass Spectrom 1999 34 (12) 1296

An experimental and computational study of the double ionization of CH3Cl,CH2Cl2, and CHCl3 molecules to singlet and triplet electronic states on theirdicationsGrant RP, Harris FM*, Parry DE// *Univ Coll, Mass Spectrometry Res Unit,Singleton Pk, Swansea SA2 8PP, WalesInt J Mass Spectrom 1999 192 111

Gas phase reactions of dianions. II. The effect of a second change on SN2 po-tential energy surfaces: An an initio studyGronert S, Fong LM// San Francisco State Univ, Dept Chem & Biochem, SanFrancisco, Ca 94132, USAInt J Mass Spectrom 1999 192 185

Fragmentation reactions of alkylphenylammonium ionsHarrison AG// Unv Toronto, Dept Chem, Toronto, Ontario, Canada M5S 3H6J Mass Spectrom 1999 34 (12) 1253

Dynamics of chemical and change transfer reactions of molecular dications:Beam scattering and total cross section data on CF2D

+ (CF2H+), CF2

+, and CF+

formations in CF22+ + D2 (H2) collisions

Herman Z, Zabka J, Dolejsek Z, Farnik M// Acad Sci Czech Republ, J Hey-rovsky Inst Phys Chem, V Cermak Lab, Dolesjskova 3, CZ-18223 Prague 8,Czech RepublicInt J Mass Spectrom 1999 192 191

Heat of formation of the SiF2++ dication: A theoretical prediction

Hrusak J, Herman Z, Iwata S// Acad Sci Czech Republ, J Heyrovsky Inst PhysChem, Dolejskova 3, CZ-18223 Prague 8, Czech RepublicInt J Mass Spectrom 1999 192 165

Selected-ion flow tube studies of reactions of C60n+ (n = 1, 2, 3) with chlorin-

ated ethylenesLing Y, Koyanagi GK, Caraiman D, Hopkinson AC, Bohme DK*// *YorkUniv, Dept Chem, Nth York, Ontario, Canada M3J 1P3Int J Mass Spectrom 1999 192 215

D22+ dication as a probe of spatial alignment of D2 molecules in intense laser

lightMathur D, Bhardwaj VR, Safvan CP, Rajgara FA// Tata Inst FundamentalRes, Homi Bhabha Rd, DE-400005 Bombay, IndiaInt J Mass Spectrom 1999 192 367

Excited state formation in studies of electron capture by state prepared doublycharged atomic ionsMcCullough RW// Queen’s Univ Belfast, Dept Pure & Appl Phys, BelfastBT7 1NN, Northern IrelandInt J Mass Spectrom 1999 192 141

Photodissociation dynamics of CH2BrCl studied using resonance enhancedmultiphoton ionization (REMPI) with time-of-flight mass spectrometryMcGivern WS, Li RJ, Zou P, North SW*// *Texas A&M Univ, Dept Chem,POB 30012, College Station, Tx 77842, USAJ Chem Phys 1999 111 (13) 5771

Reactions of ionic species from acetonitrile with long-chain saturated and un-saturated alcoholsMoneti G, Pieraccini G, Favretto D*, Traldi P// *CNR, Area Ric, Corso StatiUniti 4, IT-35100 Padua, ItalyJ Mass Spectrom 1999 34 (12) 1354

Ion-molecule reactions of dimethyl ether cations with polycylic aromatic hy-drocarbons in a quadrupole ion trap mass spectrometerMosi AA, Skelton RH, Eigendorf GK*// *Univ British Columbia, Dept Chem,2036 Main Mall, Vancouver, Brit Columbia, Canada V6T 1Z1J Mass Spectrom 1999 34 (12) 1274

Plasma rate coefficients for highly charged ion-electron collisions: New ex-perimental access via iron storage ringsMuller A// Univ Giessen, Inst Kernphys, Strahlenzentrum, DE-35392 Giessen,GermanyInt J Mass Spectrom 1999 192 9

Magnesium- and calcium-containing molecular dications: A high-level theo-retical studyPetrie S, Radom L*// *Australian Natl Univ, Res Sch Chem, Canberra, ACT0200, AustraliaInt J Mass Spectrom 1999 192 173

A possible origin of [M - nH + mX](m-n)+ ions (X = alkali metal ions) in elec-trospray mass spectrometry of peptidesRodriguez CF, Fournier R, Chu IK, Hopkinson AC, Siu KWM*// *York Univ,Dept Chem, 4700 Keele St, Nth York, Ontario, Canada M3J 1P3Int J Mass Spectrom 1999 192 303

Electronic versus vibrational excitation in Heg+ collisions with fullerenesSchlatholter T, Hadjar O, Manske J, Hoekstra R, Morgenstern R// Univ Gron-ingen, KVI Atom Phys, Zernikelaan 25, NL-9747 AA Groningen, The Nether-landsInt J Mass Spectrom 1999 192 245

Redox properties of charged and neutral iron chlorides FeClmn (m = 1 - 3; n =

1-, 0, 1+, and 2+)Schroder D, Barsch S, Schwarz H// Tech Univ Berlin, Inst Organ Chem, Str17 Juni 135, DE-10623 Berlin, GermanyInt J Mass Spectrom 1999 192 125

Recombination of cooled highly charged ions with low-energy electronsSchuch R, Zong WY, Badnell NR// Stockholm Univ, Dept Atom Phys, SE-10405 Stockholm, SwedenInt J Mass Spectrom 1999 192 225

Low energy collisionally activated dissociation of Cu2+(glycine)(H2O),Cu2+(glycine)(H2O)2, Cu2+(glycine)2, and Cu2+(glycylglycine)2Seto C, Stone JA*// *Queen’s Univ, Dept Chem, Kingston, Ontario, CanadaK7L 3N6Int J Mass Spectrom 1999 192 289

Gas-phase hydrogen-deuterium exchange reactions of fulvic acids: An elec-trospray ionization Fourier transform ion cyclotron resonance mass spectralstudySolouki T, Freitas MA, Alomary A// Univ Maine, Dept Chem, Orono, Me04469, USAAnal Chem 1999 71 (20) 4719

Electron-impact ionization of Fe5+ ionsStenke M, Aichele K, Hathiramani D, Salzborn E*// *Univ Giessen, Strahlen-zentrum, Inst Kernphys, DE-35392 Giessen, GermanyInt J Mass Spectrom 1999 192 27

Electron-transfer and neutral-loss reactions in collisions of CF32+ with argon

Tafadar N, Kaltsoyannis N, Price SD*// *UCL, Dept Chem, 20 Gordon St,London WC1H 0AJ, EnglandInt J Mass Spectrom 1999 192 205

Direct observation by electrospray ionization mass spectrometry of[Cp*RhMo3O8(OMe)5]

-, a key intermediate in the formation of the double-bookshelf-type oxide cluster [(Cp*Rh)2Mo6O20(OMe)2]

2-

Takara S, Ogo S*, Watanabe Y, Nishikawa K, Kinoshita I, Isobe K// *OsakaCity Univ, Grad Sch Sci, Dept Mat Sci, Sumiyoshi ku, 3-3-138 Sugimoto,Osaka 558 8585, JapanAngew Chem Int Ed 1999 38 (20) 3051

4 BIOLOGY/BIOCHEMISTRY:

Amino acids, peptides & proteins

Chromogranin A from bovine adrenal medulla: Molecular characterization ofglycosylations, phosphorylations, and sequence heterogeneities by mass spec-trometryBauer SHJ, Zhang XY, Van Dongen W, Claeys M, Przybylski M*// *UnivKonstanz, Dept Chem, DE-78457 Constance, GermanyAnal Biochem 1999 274 (1) 69

Characterization of the noncovalent complex of human immunodeficiency vi-rus glycoprotein 120 with its cellular receptor CD4 by matrix-assisted laserdesorption/ionization mass spectrometryBorchers C, Tomer KB*// *NIH/NIEHS, Struct Biol Lab, POB 12233, ResTriangle Park, NC 27709, USABiochemistry 1999 38 (36) 11734

Gas chromatography-mass spectrometric analysis of stable isotopes of cysteineand glutathione in biological samplesCapitan P, Malmezat T, Breuille D, Obled C*// *INRA, Lab Etud MetabAzote, FR-63122 Ceyrat, FranceJ Chromatogr B 1999 732 (1) 127

Determination of 20 underivatized proteinic amino acids by ion-pairing chro-matography and pneumatically assisted electrospray mass spectrometryChaimbault P, Petritis K, Elfakir C*, Dreux M// *Univ Orleans, Inst Chim Or-gan & Analyt, CNRS, UPRES A 6005, BP 5759, Orleans 2, FranceJ Chromatogr A 1999 855 (1) 191

Protein cross-links: Universal isolation and characterization by isotopic deriva-tization and electrospray ionization mass spectrometryChen XH, Chen YH, Anderson VE*// *Case Western Reserve Univ, Sch Med,Dept Biochem, 10900 Euclid Ave, Cleveland, Oh 44106, USAAnal Biochem 1999 273 (2) 192

Copyright © 2000 John Wiley & Sons, Ltd J. Mass Spectrom. 35, 279–287 (2000)

CURRENT LITERATURE IN MASS SPECTROMETRY 281

Probing the nature of interactions in SH2 binding interfaces: Evidence fromelectrospray ionization mass spectrometryChung EW, Henriques DA, Renzoni D, Morton CJ, Mulhern TD, PitkeathlyMC, Ladbury JE, Robinson CV*// *Univ Oxford, Oxford Ctr Mol Sci, NewChem Lab, Sth Parks Rd, Oxford OX1 3QT, EnglandProtein Sci 1999 8 (10) 1962

An automated solid-phase microextraction-gas chromatography-mass selectivedetection approach for the determination of sugar-amino acid reaction mecha-nismsColeman WM, Lawson SN*// *RJ Reynolds Tobacco Co, POB 1487, WinstonSalem, NC 27102, USAJ Chromatogr Sci 1999 37 (10) 383

Cotter RJ, Fancher C, Cornish TJ// Johns Hopkins Univ Sch Med, Dept Phar-macol & Mol Sci, Baltimore, Md 21205, USAJ Mass Spectrom 1999 34 (12) 1368Minaturized time-of-flight mass spectrometer for peptide and oligonucleotideanalysis

Unfolding dynamics of a β-sheet protein studied by mass spectrometryEyles SJ, Dresch T, Gierasch LM, Kaltashov IA*// *Univ Massachusetts, DeptPolymer Sci & Engn, A528 Conte Center, Amherst, Ma 01003, USAJ Mass Spectrom 1999 34 (12) 1289

Matrix-assisted laser desorption/ionization mass spectrometry for monitoringbacterial protein digestion in yoghurt productionFedele L, Seraglia R, Battistotti B, Pinelli C, Traldi P*// *CNR, Area Ric,Corso Stati Uniti 4, IT-35100 Padua, ItalyJ Mass Spectrom 1999 34 (12) 1338

Identification of flow-dependent endothelial nitric oxide synthase phosphoryla-tion sites by mass spectrometry and regulation of phosphorylation and nitricoxide production by the phosphatidylinositol 3-kinase inhibitor LY294002Gallis B, Corthals GL, Goodlett DR, Ueba H, Kim F, Presnell SR, Figeys D,Harrison DG, Berk BC, Aebersold R, Corson MA// Univ Washington, DivCardiol, Dept Med, Box 359748, Seattle, Wa 98195, USAJ Biol Chem 1999 274 (42) 30101

Electrospray ionization mass spectrometric determination of the molecularmass of the ~200-kDa globin dodecamer subassemblies in hexagonal bilayerhemoglobinsGreen BN, Bordoli RS, Hanin LG, Lallier FH, Toulmond A, VinogradovSN*// *Wayne State Univ, Sch Med, Dept Biochem & Mol Biol, Detroit, Mi48201, USAJ Biol Chem 1999 274 (40) 28206

Analysis for TNF-α using solid-phase affinity capture with radiolabeled andMALDI-MS detectionHurst GB, Buchanan MV, Foote LJ, Kennel SJ// Oak Ridge Natl Lab, DivChem & Analyt Sci, Oak Ridge, Tn 37831, USAAnal Chem 1999 71 (20) 4727

Direct detection of proteins adsorbed on synthetic materials by matrix-assistedlaser desorption/ionization-mass spectrometryKingshott P, St John HAW, Griesser HJ*// *CSIRO Mol Sci, Private Bag 10,Clayton Sth MDC, Clayton, Vic 3169, AustraliaAnal Biochem 1999 273 (2) 156

The dominance of arginine-containing peptides in MALDI-derived trypticmass fingerprints of proteinsKrause E, Wenschuh W, Jungblut PR*// *Max Planck Inst Infect Biol, ProtAnal Unit, Monbijoustr 2, DE-10117 Berlin, GermanyAnal Chem 1999 71 (19) 4160

Reconstitution of acid-denatured holomyoglobin studied by time-resolvedelectrospray ionization mass spectrometryLee VWS, Chen YL, Konermann L*// *Univ Western Ontario, Dept Chem,London, Ontario, Canada N6A 5B7Anal Chem 1999 71 (19) 4154

Identification of intact proteins in mixtures by alternated capillary liquid chro-matography electrospray ionization and LC-ESI infrared multiphoton dissocia-tion Fourier transform ion cyclotron resonance mass spectrometryLi WQ, Hendrickson CL, Emmett MR, Marshall AG*// *Florida State Univ,Dept Chem, Tallahassee, Fl 32310, USAAnal Chem 1999 71 (19) 4397

Use of liquid chromatography-mass spectrometry coupling for monitoring theserralysin-catalyzed hydrolysis of a peptide libraryLouis D, Bernillon J, Paisse JO, Wallach JM*// *Univ Lyon 1, Lab BiochimAnalyt & Synthese Bioorgan, 43 Blvd 11 Novembre 1918, FR-69622 Villeur-banne, FranceJ Chromatogr B 1999 732 (2) 271

Millisecond radiolytic modification of peptides by synchrotron X-rays identi-fied by mass spectrometryMaleknia SD, Brenowitz M, Chance MR*// *Yeshiva Univ Albert EinsteinColl Med, Dept Physiol & Biophys, Bronx, NY 10461, USAAnal Chem 1999 71 (18) 3965

Localization of O-glycosylation sites in peptides by electron capture dissocia-tion in a Fourier transform mass spectrometerMirgorodskaya E, Roepstorff P, Zubarev RA// Odense Univ, Dept Chem,Campusvej 55, DK-5230 Odense M, DenmarkAnal Chem 1999 71 (20) 4431

Simultaneous analysis of hemoglobin adducts of acrylamide and glycidamide

by gas chromatography-mass spectrometryPerez HL, Cheong HK, Yang JS, Osterman-Golkar S// Stockholm Univ, DeptMol Genome Res, SE-10691 Stockholm, SwedenAnal Biochem 1999 274 (1) 59

Direct analysis of the products of sequential cleavages of peptides and proteinsaffinity-bound to immobilized metal ion beads by matrix-assisted laser desorp-tion/ionization mass spectrometryQian XH, Zhou W, Khaledi MG, Tomer KB*// *NIH/NIEHS, Struct Biol Lab,POB 12233, Res Triangle Park, NC 27709, USAAnal Biochem 1999 274 (2) 174

Effect of charge derivatization in the determination of phosphorylation sites inpeptides by electrospray ionization collision-activated dissociation tandemmass spectrometry (Letter)Sadagopan N, Malone M, Watson JT*// *Michigan State Univ, Dept Chem,East Lansing, Mi 48864, USAJ Mass Spectrom 1999 34 (12) 1279

Identification of fluorescein-5’-isothiocyanate-modification sites in proteins byelectrospray/ionization mass spectrometrySchnaible V, Przybylski M*// Univ Konstanz, Fak Chem, DE-78457 Con-stance, GermanyBioconjug Chem 1999 10 (5) 861

A simple assay for formate dehydrogenase activity by gas chromatography-mass spectrometryShiraishi T, Fukusaki E, Kajiyama S, Kobayashi A*// *Osaka Univ, Grad SchEngn, Dept Biotechnol, 2-1 Yamadaoka, Osaka 565 0871, JapanJ Chromatogr A 1999 855 (1) 337

Gas phase separations of electrosprayed peptide librariesSrebalus CA, Li JW, Marshall WS, Clemmer DE*// *Indiana Univ, DeptChem, Bloomington, In 47405, USAAnal Chem 1999 71 (18) 3918

Combined method for the determination of γ-aminobutyric and β-alanine incerebrospinal fluid by stable isotope dilution mass spectrometryStruys EA, Guerand WS, Ten Brink HJ, Jakobs C*// *Free Univ AmsterdamHosp, Dept Clin Chem & Pediat, De Boelelaan 1117, NL-1081 HV Amster-dam, The NetherlandsJ Chromatogr B 1999 732 (1) 245

Identification of factor C protein from Streptomyces griseus by microelectro-spray mass spectrometrySzabo PT, Kele Z, Birko Z, Szeszak F, Biro S, Janaky T// Albert Szent-Gyorgyi Med Univ, Dept Med Chem, Dom ter 8, HU-6720 Szeged, HungaryJ Mass Spectrom 1999 34 (12) 1312

Gas-phase memory of solution-phase protein conformation: H/D exchange andFourier transform ion cyclotron resonance mass spectrometry of the N-terminal domain of cardiac troponin CWang F, Freitas MA, Marshall AG*, Sykes BD// *Florida State Univ, NatlHigh Magnet Field Lab Ctr Interdisciplinary Magnet Resonance, Tallahassee,Fl 32310, USAInt J Mass Spectrom 1999 192 319

Toward the bilayer proteome, electrospray ionization-mass spectrometry oflarge, intact transmembrane proteinsWhitelegge JP, Le Coutre J, Lee JC, Engel CK, Prive GG, Faull KF, KabackHR// Calif State Univ, Dept Chem, 405 Hilgard Ave, Los Angeles, Ca 90095,USAProc Natl Acad Sci U S A 1999 96 (19) 10695

Chiral recognition of amino acids by electrospray ionisation mass spectrome-try/mass spectrometryYao ZP, Wan TSM*, Kwong KP, Che CT// *Hong Kong Univ Sci & Technol,Dept Chem, Clear Water Bay, Hong Kong, Peoples Rep ChinaChem Commun 1999 (20) 2119

Solid-phase extraction/MALDI-MS: Extended ion-pairing surfaces for the on-target cleanup of protein samplesZhang L, Orlando R*// *Univ Georgia, Complex Carbohydrate Res Ctr, DeptBiochem & Mol Biol, 220 Riverbend Rd, Athens, Ga 30602, USAAnal Chem 1999 71 (20) 4753

Carbohydrates

Analysis of 8-aminonaphthalene-1,3,6-trisulfonate-derivatized oligosaccharidesby capillary electrophoresis-electrospray ionization quadrupole ion trap massspectrometryChe FY, Song JF, Zeng R, Wang KY, Xia QC*// *Chinese Acad Sci, Shang-hai Inst Biochem, CN-200031 Shanghai, Peoples Rep ChinaJ Chromatogr A 1999 858 (2) 229

Multicomponent quantification of diastereomeric hexosamine monosaccharidesusing ion trap tandem mass spectrometryDesaire H, Leary JA*// *Univ Calif, Coll Chem, Berkeley, Ca 94720, USAAnal Chem 1999 71 (19) 4142

Quantitation of monosaccharide isotopic enrichment in physiologic fluids byelectron ionization or negative chemical ionization GC/MS using di-O-isopropylidene derivativesHachey DL, Parsons WR, McKay S, Haymond MW// Vanderbilt Univ, DeptPharmacol, Nashville, Tn 37232, USAAnal Chem 1999 71 (20) 4734

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282 CURRENT LITERATURE IN MASS SPECTROMETRY

Electron ionization mass spectra of acetals of β-D-glycopyranosylnitro-methanesKovacik V, Patoprsty V, Lattova E, Petrus L, Ovcharenko V, Pihlaja K// InstChem, Acad Sci, Dubravska cesta 9, SK-84238 Bratislava, Slovak RepublicJ Mass Spectrom 1999 34 (12) 1322

An automated interpretation of MALDI-TOF postsource decay spectra of oli-gosaccharides. I. Automated peak assignmentMizuno Y, Sasagawa T, Dohmae N, Takio K// Toray Res Ctr Ltd, Kamakura,Kanagawa 248 003, JapanAnal Chem 1999 71 (20) 4764

Structural characterization of chemically derivatized oligosaccharides by nano-flow electrospray ionization mass spectrometryMo WJ, Sakamoto H, Nishikawa A, Kagi N, Langridge JI, Shimonishi Y,Takao T*// *Osaka Univ, Inst Prot Res, Yamadaoka 3-2, Suita, Osaka 5650871, JapanAnal Chem 1999 71 (18) 4100

MALDI-MS characterization of maltooligo/polysaccharides from debranchedstarch amylopectin of corn and barleyWang J, Jiang GS, Vasanthan T, Sporns P*// *Univ Alberta, Dept Agr Food &Nutr Sci, Edmonton, Alberta, Canada T6G 2P5Starch 1999 51 (7) 243

Lipids

Phospholipid molecular species distribution of some medically important Can-dida species analysed by fast atom bombardment mass spectroscopyAbdi M, Drucker DB*, Boote V, Korachi M, Theaker ED// *Univ Manches-ter, Dept Dent Med & Surg, Oral Microbiol Lab, Higher Cambridge St, Man-chester M15 6FH, EnglandJ Appl Microbiol 1999 87 (3) 332

Mass spectrometric analysis of change in phospholipids in biological mem-brane by external environmental effectsKim BH, Chang YS*, Lee BD, Ryu SH, Shin DH// *Pohang Univ Sci &Technol, Sch Environm Engn, Pohang, South KoreaMicrochem J 1999 63 (1) 3

Quantitative determination of pregnenolone 3-sulfate in rat brains using liquidchromatography/electrospray ionization-mass spectrometryMitamura K, Yatera M, Shimada K*// *Kanazawa Univ, Fac Pharmaceut Sci,13-1 Takara machi, Kanazawa, Ishikawa 920 093, JapanAnal Sci 1999 15 (10) 951

A quantitative analysis of serum sulfatide by matrix-assisted laser desorption/ionization time-of-flight mass spectrometry with delayed ion extractionSugiyama E, Hara A, Uemura K// Nagano Prefectural Coll, Course Sci Living,Nagano 380 8525, JapanAnal Biochem 1999 274 (1) 90

Mass spectrometric identification of increased C16 ceramide levels duringapoptosisThomas RL, Matsko CM, Lotze MT, Amoscato AA*// *Univ Pittsburgh, CtrBiotechnol & Bioengn, Mass Spectrometry Facil, Pittsburgh, Pa 15219, USAJ Biol Chem 1999 274 (43) 30580

Quantitative and qualitative determination of estrogen sulfates in human urineby liquid chromatography/tandem mass spectrometry using 96-well technologyZhang HW, Henion J*// *Cornell Univ, New York State Coll Vet Med, 927Warren Dr, Ithaca, NY 14850, USAAnal Chem 1999 71 (18) 3955

Structural characterization of gangliosides isolated from mullet milt usingelectrospray ionization-tandem mass spectrometryZhu JH, Li YT, Li SC, Cole RB*// *Univ New Orleans, Dept Chem, New Or-leans, La 70148, USAGlycobiology 1999 9 (10) 985

Nucleic Acids

Analysis of DNA adducts using high-performance separation techniques cou-pled to electrospray ionization mass spectrometryAndrews CL, Vouros P, Harsch A*// *Northeastern Univ, Dept Chem, 341Mugar Bldg, 360 Huntington Ave, Boston, Ma 02115, USAJ Chromatogr A 1999 856 (1-2) 515

Comparison of 32P-postlabeling and high-resolution GC/MS in quantifyingN7-(2-hydroxyethyl) guanine adductsEide I, Zhao CY, Kumar R, Hemminki K, Wu KY, Swenberg JA// Statoil ResCtr, NO-7005 Trondheim, NorwayChem Res Toxicol 1999 12 (10) 979

Interaction between antitumor drugs and a double-stranded oligonucleotidestudied by electrospray ionization mass spectrometryGabelica V, De Pauw E, Rosu F// Univ Liege Sart-Tilman, Chem Inst, MassSpectrom Lab, Allee Chim, BE-4000 Liege, BelgiumJ Mass Spectrom 1999 34 (12) 1328

Determination of in vitro- and in vivo-formed DNA adducts of 2-amino-3-methylimidazo[4,5,f] quinoline by capillary liquid chromatography/microelec-trospray mass spectrometryGangl ET, Turesky RJ, Vouros P*// *Northwestern Univ, Dept Chem, 102

Hurtig Hall, 360 Huntington Ave, Boston, Ma 02115, USAChem Res Toxicol 1999 12 (10) 1019

Electrospray mass spectrometry of phosphoramidites, a group of acid-labilecompoundsKele Z, Kupihar Z, Kovacs L, Janaky T, Szabo PT*// Albert Szent-GyorgyiMed Univ, Dept Med Chem, Dom ter 8, HU-6720 Szeged, HungaryJ Mass Spectrom 1999 34 (12) 1317

5 PHARMACOLOGY/TOXICOLOGY

Identification and confirmation of 3-hydroxy metabolite of ketoprofen in cam-els by gas chromatography/mass spectrometry and nuclear magnetic resonancespectroscopyAlkatheeri NA, Wasfi IA*, Kvanagh P, Lambert M// *Forens Sci Lab, Camel-racing Forens Lab, POB 253, Abu Zaby, United Arab EmiratesJ Chromatogr B 1999 732 (2) 299

Liquid chromatographic-tandem mass spectrometric method for the determina-tion of the neuraminidase inhibitor zanamivir (GG167) in human serumAllen GD, Brookes ST, Barrow A*, Dunn JA, Grosse CM// *GlaxoWellcomeRes & Dev, Biomet Div, Park Road, Ware SG12 0DP, EnglandJ Chromatogr B 1999 732 (2) 383

Positive chemical ionization and tandem mass spectrometric fragmentation forthe gas chromatographic analysis of β-agonists using the ion trap techniquesBiancotto G, Angeletti R, Traldi P, Guidugli F// Ist Zooprofilattico Sperimen-tale Venezie, via Romea 14A, IT-35020 Legnaro, PD, ItalyJ Mass Spectrom 1999 34 (12) 1346

Monitoring of olanzapine in serum by liquid chromatography-atmosphericpressure chemical ionization mass spectrometryBogusz MJ, Kruger KD, Maier RD, Erkwoh R, Tuchtenhagen F// Rhein West-fal TH, Inst Forens Med, Klin RWTH, Paulwelsstr 30, DE-52057 Aachen,GermanyJ Chromatogr B 1999 732 (2) 257

Diacetylmorphine and its metabolites in plasma by HPLC with diode-arrayand atmospheric pressure ionization mass spectrometric detectionBourquin D, Bundeli P, Lehmann T, Brenneisen R*// *Univ Bern, Inst Pharm,Baltzerstr 5, CH-3012 Bern, SwitzerlandJ Liq Chromatogr Relat Technol 1999 22 (17) 2663

Determination of 11-nor-∆9-tetrahydrocannabinol-9-carboxylic acid in urineusing high-performance liquid chromatography and electrospray ionizationmass spectrometryBreindahl T, Andreasen K// Hjorring Bronderslev Hosp, Dept Clin Chem, Bis-pensgade 37, DK-9800 Hjorring, DenmarkJ Chromatogr B 1999 732 (1) 155

Prediction of substructure and toxicity of pesticides with temperature cons-trained-cascade correlation network from low-resolution mass spectraCai CS, Harrington PD*// *Ohio Univ, Ctr Intelligent Chem Instrumentat,Dept Chem & Biochem, Clippinger Labs, Athens, Oh 45701, USAAnal Chem 1999 71 (19) 4134

Comparison of the serum barbiturate fluorescence polarization immunoassayby the COBAS Integra to a GC/MS methodCannon RD, Wong SH*, Gock SB, Jentzen JJ// *Off Milwaukee County MedExaminer, 933 West Highland Ave, Milwaukee, Wi 53233, USATher Drug Monit 1999 21 (5) 553

Sensitive triple-quadrupole mass spectrometric assay for the determination ofBMS-181885, a 5-HT1 agonist, in human plasma following solid phase extrac-tionChang SY, Whigan D, Shyu WC, Srinivas NR*// *Bristol Myers Squibb Phar-maceut Res Inst, Dept Metab & Pharmacokinet, POB 4000, Princeton, NJ08543, USABiomed Chromatogr 1999 13 (6) 425

Determination of phenolic derivatives of antipyrine in plasma with solid-phaseextraction and high-performance liquid chromatography-atmospheric-pressurechemical ionization mass spectrometryCoolen SAJ, Ligor T, Van Lieshout M, Huf FA// Eindhoven Univ Technol,Instrumental Anal Lab, POB 513, NL-5600 MB Eindhoven, The NetherlandsJ Chromatogr B 1999 732 (1) 103

Determination of melatonin in pharmaceutical formulations and human plasmaby gas chromatography-electron impact mass spectrometryCovaci A, Doneanu C, Aboul-Enein HY*, Schepens P// *King Faisal Special-ist Hosp & Res Ctr, Dept Biol & Med Res, Bioanalyt & Drug Dev Lab, Ri-yadh 11211, Saudi ArabiaBiomed Chromatogr 1999 13 (6) 431

Quantitation of alprazolam and α-hydroxyalprazolam in human plasma usingliquid chromatography electrospray ionization MS-MSCrouch DJ, Rollins DE, Canfield DV, Andrenyak DM, Schulties JE// UnivUtah, Dept Pharmacol & Toxicol, Ctr Human Toxicol, 20 Sth 2030 East, 490Biomed Polymers Bldg, Salt Lake City, Ut 84112, USAJ Anal Toxicol 1999 23 (6) 479

Rapid determination of the anti-cancer drug chlorambucil (Leukeran ) and itsphenyl acetic acid mustard metabolite in human serum and plasma by auto-mated solid-phase extraction and liquid chromatography-tandem mass spec-trometry

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CURRENT LITERATURE IN MASS SPECTROMETRY 283

Davies ID, Allanson JP, Causon RC// Glaxo Wellcome Res & Dev Ltd, IntBioanal & Business Support, Biomet Park Rd, Ware SG12 0DP, EnglandJ Chromatogr B 1999 732 (1) 173

GC-MS determination of flunitrazepam and its major metabolite in wholeblood and plasmaElSohly MA, Feng S, Salamone SJ, Brenneisen R// ElSohly Labs Inc, 5 IndPk Dr, Oxford, Ms 38655, USAJ Anal Toxicol 1999 23 (6) 486

Immunoassay and GC-MS procedures for the analysis of drugs of abuse inmeconiumElSohly MA, Stanford DF, Murphy TP, Lester BM, Wright LL, SmeriglioVL, Verter J, Bauer CR, Shankaran S, Bada HS, Walls HC// Address asabove.J Anal Toxicol 1999 23 (6) 436

The detection and quantitation of 7-aminoflunitrazepam, the major urinary me-tabolite of flunitrazepam, by gas chromatography/mass spectrometryFeely J, Kavanagh PV, McNamara SM// Trinity Coll Dublin, Dept Pharmacol& Therapeut, Dublin 2, Rep IrelandIr J Med Sci 1999 168 (3) 189

Identification and quantification of cardiac glycosides in blood and urine sam-ples by HPLC/MS/MSGuan FY, Ishii A, Seno H, Watanabe-Suzuki K, Kumazawa T, Suzuki O*//*Hamamatsu Univ, Sch Med, Dept Legal Med, 3600 Handa cho, Hamamatsu,Shizuoka 431 319, JapanAnal Chem 1999 71 (18) 4034

Fast liquid chromatographic-mass spectrometric determination of pharmaceuti-cal compoundsHeinig K, Henion J*// *Cornell Univ, New York State Coll Vet Med, 927Warren Drive, Ithaca, NY 14850, USAJ Chromatogr B 1999 732 (2) 445

‘High throughput’ solid-phase extraction technology and turbo ionspray LC-MS-MS applied to the determination of haloperidol in human plasmaHempenius J, Steenvoorden RJJM, Lagerwerf FM, Wieling J, Jonkman JHG//Pharma Biores Int BV, POB 200, NL-9470 AE Zuidlaren, The NetherlandsJ Pharmaceut Biomed Anal 1999 20 (6) 889

Simultaneous determination of amphetamine, methamphetamine, methylenedi-oxyamphetamine (MDA), methylenedioxymethamphetamine (MDMA), andmethylenedioxyethylamphetamine (MDEA) enantiomers by GC-MSHensley D, Cody JT*// *Wilford Hall US Air Force Med Ctr, Clin Res Squad-ron, 1255 Wilford Hall Loop, Lackland AFB, Tx 78236, USAJ Anal Toxicol 1999 23 (6) 518

Liquid chromatography-tandem mass spectrometry of some anabolic steroidsJoos PE, Van Ryckeghem M// SGS Depauw & Stokoe, Dept IAC, Keetber-glaan 4, BE-9120 Melsele, BelgiumAnal Chem 1999 71 (20) 4701

Analysis of cyclophosphamide and five metabolites from human plasma usingliquid chromatography/mass spectrometry and gas chromatography-nitrogen-phosphorus detectionKalhorn TF, Ren S, Howald WN, Lawrence RF, Slattery JT*// *Fred Hutchin-son Canc Res Ctr, 1100 Fairview Ave Nth, POB 19024, Seattle, Wa 98104,USAJ Chromatogr B 1999 732 (2) 287

Automated in tube solid-phase microextraction coupled with liquid chromatog-raphy/electrospray ionization mass spectrometry for the determination ofβ-blockers and metabolites in urine and serum samplesKataoka H, Narimatsu S, Lord HL, Pawliszyn J*// *Univ Waterloo, DeptChem, Waterloo, Ontario, Canada N2L 3G1Anal Chem 1999 71 (19) 4237

Testing for α-chloralose by headspace-GC/MS (Case Reports)Kintz P, Doray S, Cirimele V, Ludes B// Inst Med Legale, 11 rue Humann,FR-67000 Strasbourg, FranceForensic Sci Int 1999 104 (1) 59

Amphetamines and their analysis by capillary gas chromatography and gaschromatography in combination with mass spectroscopy (Slovak, English Ab-stract)Korytar P, Matisova E, Cellar P// Slovak Tech Univ, Fac Chem Technol, Ra-dlinskeho 9, SK-81237 Bratislava, SlovakiaChem Listy 1999 93 (9) 554

Enantioselective gas chromatography-negative ion chemical ionization massspectrometry for methylphenidate in human plasmaLin SN, Andrenyak DM, Moody DE, Foltz RL// Univ Utah, Dept Pharmacol& Toxicol, Ctr Human Toxicol, 20 East 2030 Sth Rm 490, Salt Lake City, Ut84112, USAJ Anal Toxicol 1999 23 (6) 524

Determination of free and glucuronated hexane metabolites without prior hy-drolysis by liquid- and gas-chromatography coupled with mass spectrometryManini P, Andreoli R, Mutti A, Bergamaschi E, Franchini I// Univ Parma, SchMed, Dept Clin Med Nephrol & Hlth Sci, Lab Ind Toxicol, via Gramsci 14,IT-43100 Parma, ItalyToxicol Lett 1999 108 (2-3) 225

Fluoxetine bioequivalence study: Quantification of fluoxetine and norfluoxet-ine by liquid chromatography coupled to mass spectrometryMoraes MO, Lerner FE, Corso G, Bezzerra FAF, Moraes MEA, De Nucci

G*// *Jesvino Marcondes Machado 415, BR-13092-320 Campinas, SP, BrazilJ Clin Pharmacol 1999 39 (10) 1053

Identification and characterization of efavirenz metabolites by liquid chroma-tography/mass spectrometry and high field NMR: Species differences in themetabolism of efavirenzMutlib AE, Chen H, Nemeth GA, Markwalder JA, Seitz SP, Gan LS, ChristDD// DuPont Co Inc, Stine Haskell Res Ctr, Drug Metab & PharmacokinetSect, POB 30, 1094 Elkton Rd, Newark, De 19714, USADrug Metab Dispos 1999 27 (11) 1319

Simultaneous determination of residual tetracyclines in foods by high-performance liquid chromatography with atmospheric pressure chemical ioni-zation tandem mass spectrometryNakazawa H, Ino S, Kato K, Watanabe T, Ito Y, Oka H// Hoshi Univ, FacPharmaceut Sci, Dept Analyt Chem, Shinagawa ku, 2-4-41 Ebara, Tokyo 1428501, JapanJ Chromatogr B 1999 732 (1) 55

Simple analysis of arylamide herbicides in serum using headspace-solid phasemicroextraction and GC/MSNamera A, Watanabe T, Yashiki M, Iwasaki Y, Kojima T// Hiroshima Univ,Sch Med, Dept Legal Med, Minami ku, 1-2-3 Kasumi, Hiroshima 734 8551,JapanForensic Sci Int 1999 103 (3) 217

Highly sensitive micro-plate enzyme immunoassay screening and NCI-GC-MSconfirmation of flunitrazepam and its major metabolite 7-aminoflunitrazepamin hairNegrusz A, Moore C, Deitermann D, Lewis D, Kalceiak K, Kronstrand R,Feeley B, Niedbala RS// Univ Illinois, Coll Med, Dept Pharmaceut & Pharma-codynam, 833 Sth Wood St, Chicago, Il 60612, USAJ Anal Toxicol 1999 23 (6) 429

Analysis of 2-(3-methyl-4-aminophenyl)-benzothiazole (NSC 674495) inplasma by gas chromatography with mass-selective detectionPhillips LR, Bramhall C, Buckley J, Daw TW, Stinson SF// NCI, Lab DrugDiscovery Res & Dev, Dev Therapeut Program, Div Canc Treatment Diagno-sis & Ctr, Frederick, Md 21701, USAJ Chromatogr B 1999 732 (2) 315

Determination of lorazepam in plasma and urine as trimethylsilyl derivativeusing gas chromatography-tandem mass spectrometryPichini S, Pacifici R, Altieri I, Palmeri A, Pellegrini M, Zuccaro P*// *Ist Su-per Sanita, Dept Clin Biochem, Viale Regina Elena 299, IT-00161 Rome, ItalyJ Chromatogr B 1999 732 (2) 509

Solid-phase microextraction gas chromatographic-mass spectrometric methodfor the determination of inhalation anesthestics in urinePoli D, Bergamaschi E, Manini P*, Andreoli R, Mutti A// *Univ Parma, DiptClin Med Nefrol & Sci Prevenz, Lab Tossicol Ind, via Gramsci 14, IT-43100Parma, ItalyJ Chromatogr B 1999 732 (1) 115

Benzodiazepines in Miami-Dade County, Florida driving under the influence(DUI) cases (1995-1998) with emphasis on Rohypnol : GC-MS confirmation,patterns of use, psychomotor impairment, and results of Florida legislationRaymon LP, Steele BW, Walls HC// 12500 SW 152nd St, Bldg B, Miami, Fl33177, USAJ Anal Toxicol 1999 23 (6) 490

Detection of lysergic acid diethylamide (LSD) in urine by gas chromato-graphy-ion trap tandem mass spectrometrySklerov JH, Kalasinsky KS, Ehorn CA// Armed Forces Inst Pathol, Off ArmedForces Med Examiner, Div Forens Toxicol, 1413 Res Blvd, Bldg 102,Rockville, Md 20850, USAJ Anal Toxicol 1999 23 (6) 474

Determination of morphine, morphine-3-glucuronide, and morphine-6-gluc-uronide in plasma after intravenous and intrathecal morphine administrationusing HPLC with electrospray ionization and tandem mass spectrometrySlawson MH, Crouch DJ, Andrenyak DM, Rollins DE, Lu JK, Bailey PL//Univ Utah, Dept Pharmacol & Toxicol, Ctr Human Toxicol, 20 Sth 2030 East490, Salt Lake City, Ut 84112, USAJ Anal Toxicol 1999 23 (6) 468

Determination of the oral platelet aggregation inhibitor Sibrafiban in rat,dog, and human plasma utilising HPLC-column switching combined withturbo ion spray single quadrupole mass spectrometryTimm U, Birnbock H, Erdin R, Hopfgartner G, Zumbrunnen R// F HoffmannLa Roche Co Ltd, Div Pharmaceut, CH-4070 Basel, SwitzerlandJ Pharmaceut Biomed Anal 1999 21 (1) 151

Gas chromatographic-mass spectrometric method for quantitative determina-tion of ketotifen in human plasma after enzyme hydrolysis of conjugated keto-tifenTzvetanov S, Vatsova M, Drenska A, Gorantcheva J, Tyutyulkova N// Ni-farma 98 SA, Acad Bonchev Str, Sofia, BulgariaJ Chromatogr B 1999 732 (1) 251

Liquid chromatographic-mass spectrometric determination of the novel, re-cently identified thioTEPA metabolite, thioTEPA-mercapturate, in urineVan Maanen MJ, Beijnen JH// Univ Utrecht, Dept Pharmaceut Anal, Sorbon-nelaan 16, NL-3584 CA Utrecht, The NetherlandsJ Chromatogr B 1999 732 (1) 73

Glutathione conjugation of electrophilic metabolites of 1-nitronaphthalene in

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284 CURRENT LITERATURE IN MASS SPECTROMETRY

rat tracheobronchial airways and liver, identification by mass spectrometry andproton nuclear magnetic resonance spectroscopyWatt KC, Morin DM, Kurth MJ, Mercer RS, Plopper CG, Buckpitt AR// UnivCalif, Sch Vet Med, Dept Mol Biosci, 1311 Haring Hall, 1 Shields Ave,Davis, Ca 95616, USAChem Res Toxicol 1999 12 (9) 831

6 NATURAL PRODUCTS

Matrix-assisted laser desorption/ionization time-of-flight mass spectrometry ofVernonia galamensis oilAyorinde FO, Elhilo E, Hlongwane C, Saeed KA// Howard Univ, Dept Chem,525 Coll St NW, Washington, DC 20059, USAJ Am Oil Chem Soc 1999 76 (10) 1217

Characterization by mass spectrometry of poly(3-hydroxyalkanoates) producedby Rhodospirillum rubrum from 3-hydroxyacidsBallistreri A, Giuffrida M, Impallomeni G, Lenz RW, Fuller RC// Univ Cata-nia, Dipt Sci Chim, Viale A Doria 6, IT-95125 Catania, ItalyInt J Biol Macromol 1999 26 (2-3) 201

Mass spectrometric analyses in agriculture and natural products researchBarofsky DF// Oregon State Univ, Dept Chem, Gilbert Hall 153, Corvallis, Or97331, USABraz J Phys 1999 29 (3) 432

Quantitative determination and structure elucidation of type A- and B-tricho-thecenes by HPLC/ion trap multiple mass spectrometryBerger U, Oehme M*, Kuhn F// *Univ Basel, Neuhausstr 31, CH-4057 Basel,SwitzerlandJ Agric Food Chem 1999 47 (10) 4240

Neonatal diagnosis of long-chain 3-hydroxyacyl-CoA dehydrogenase defi-ciency and implications for newborn screening by tandem mass spectrometryCarpenter KH, Wilcken B// New Children’s Hosp, NSW Biochem Genet Serv,POB 3515, Sydney, NSW 2124, AustraliaJ Inherit Metab Dis 1999 22 (7) 840

An LC-MS method to determine concentrations of isoflavones and their sul-fate and glucuronide conjugates in urineCimino CO, Shelnutt SR, Ronis MJJ, Badger TM*// *Arkansas Children’sNutr Ctr, 1120 Sth Marshall St, Little Rock, Ar 72202, USAClin Chim Acta 1999 287 (1-2) 69

Liquid chromatography/mass spectrometry analysis of mixtures of rhamnolip-ids produced by Pseudomonas aeruginosa strain 57RP grown on mannitol ornaphthaleneDeziel E, Lepine F*, Dennie D, Boismenu D, Mamer OA, Villemur R// *UnivQuebec, Inst Armand Frappier, Ctr Microbiol & Biotechnol, INRS, Laval,Quebec, Canada H7V 1B7Biochem Biophys Acta 1999 1440 (2-3) 244

Electrospray ionization mass spectrometry as a tool for lignins molecularweight and structural characterisationEvtuguin DV, Domingues P, Amado FL, Neto CP, Correia AJF// Univ Aveiro,Dept Chem, PT-3810 Aveiro, PortugalHolzforschung 1999 53 (5) 525

Qualitative characterization of bacterial strains employed in the production ofyoghurt by matrix-assisted laser desorption/ionization mass spectrometry (Let-ter)Fedele L, Seraglia R, Battistotti B, Pinelli C, Traldi P*// *CNR, Area Ric,Corso Stati Uniti 4, IT-35100 Padova, ItalyJ Mass Spectrom 1999 34 (12) 1385

GC/MS analysis of lignin monomers, dimers and trimers in liquid smoke fla-vouringsGuillen MD, Ibargoitia ML// Univ Pais Vasco, Fac Farm, Paseo Univ 7, ES-01006 Vitoria, SpainJ Sci Food Agr 1999 79 (13) 1889

Identification of Bacillus spores by matrix-assisted laser desorption/ionization-mass spectrometryHathout Y, Demirev PA, Ho YP, Bundy JL, Ryzhov V, Sapp L, Stutler J,Jackman J, Fenselau C// Univ Maryland, Dept Chem & Biochem, CollegePark, Md 20742, USAAppl Environ Microbiol 1999 65 (10) 4313

Identification of isoflavone metabolites dihydrodiadzein, dihydrogenistein, 6’-OH-O-dma, and cis-4-OH-equol in human urine by gas chromatography/massspectroscopy using authentic reference compoundsHeinonen S, Wahala K, Adlercreutz H*// *Univ Helsinki, Dept Clin Chem,Inst Prevent Med Nutr, Mannerheimintie 97, FI-00014 Helsinki, FinlandAnal Biochem 1999 274 (2) 211

Reliable 14C AMS dates on bird and Pacific rat Rattus exulans bone gelatin,from a CaCO3-rich depositHoldaway RN, Beavan NR// POB 16 569, Christchurch, New ZealandJ R Soc N Z 1999 29 (3) 185

Identification and quantitation by GC-MS of zeatin and zeatin riboside in xy-lem sap from rootstock and scion of grafted apple treesKamboj JS, Blake PS*, Quinlan JD, Baker DA// *Hort Res Int, East MallingME19 6BJ, EnglandPlant Growth Regul 1999 28 (3) 199

Phaseolus (Fabaceae) in archaeology: AMS radiocarbon dates and their sig-nificance for pre-Colombian agricultureKaplan L, Lynch TF// Univ Massachusetts, Dept Biol, Boston, Ma 02125,USAEcon Bot 1999 53 (3) 261

Liquid chromatography/electrospray mass spectrometry of bioactive terpenoidsin Ginkgo biloba L.Mauri P, Migliazza B, Pietta P// ITBA/CNR, via Fratelli Cervi 93, IT-20090Segrate, Milan, ItalyJ Mass Spectrom 1999 34 (12) 1361

Mass spectrometry of 3,5- and 4,5-dicaffeoylquinic acids and selected deriva-tivesMiketova P, Schram KH*, Whitney J, Kearns EH, Timmermann BN//*University Arizona, Dept Pharmacol & Toxicol, Coll Pharm, Tucson, Az85721, USAJ Mass Spectrom 1999 34 (12) 1240

Analysis of tissues that reflect central nervous system disease by mass spec-trometryNilsson CL// Univ Gothenburg, Inst Med Biochem, Box 440, SE-40530 Goth-enburg, SwedenScand J Clin Lab Invest 1999 59 (5) 383

Separation of structurally related flavonoids by GC/MS technique and determi-nation of their polarographic parameters and potential carcinogenicityNovotny L, Vachalkova A, Al Nakib T, Mohanna N, Vesela D, Suchy V// Ku-wait University, Faculty Pharm, Dept Pharmaceut Chem, KU-13110 Safat,KuwaitNeoplasma 1999 46 (4) 231

Quantitation of oleuropein in virgin olive oil by ionspray mass spectrometry:Selected reaction monitoringPerri E, Raffaelli A, Sindona G*// *Ist Sperimentale Olivicoltura, IT-87036Arcavacata di Rende, CS, ItalyJ Agric Food Chem 1999 47 (10) 4156

Synthesis of deuterium labelled desulfoglucosinolates as internal standards forLC-MS analysisRobertson AAB, Botting NP*// *Univ St Andrews, Sch Chem, St AndrewsKY16 9ST, ScotlandTetrahedron 1999 55 (46) 13269

Determination of the Fusarium mycotoxins, fusaproliferin and beauvericin byhigh-performance liquid chromatography-electrospray ionization mass spectro-metrySewram V, Nieuwoudt TW, Marasas WFO, Shephard GS, Ritieni A// Sth Af-rican MRC, Programme Mycotoxins & Expt Carcinogenesis, POB 19070,ZA-7505 Tygerberg, Rep Sth AfricaJ Chromatogr A 1999 858 (2) 175

Determination of betaine in Lycium chinense fruits by liquid chromatography-electrospray ionization mass spectrometryShin YG, Cho KH, Kim JM, Park MK, Park JH*// *Seoul Natl Univ, CollPharm, Seoul 151742, South KoreaJ Chromatogr A 1999 857 (1-2) 331

Determination of betulinic acid in mouse blood, tumor and tissue homogenatesby liquid chromatography-electrospray mass spectrometryShin YG, Cho KH, Chung SM, Graham J, Das Gupta TK, Pezzuto JM*//*Univ Illinois, Coll Pharm, Program Collaborat Res Pharmaceut Sci, Chicago,Il 60612, USAJ Chromatogr B 1999 732 (2) 331

First accelerator mass spectrometry 14C dates documenting contemporaneity ofnonanalog species in late Pleistocene mammal communitiesStafford TW, Semken HA, Graham RW, Klippel WF, Markova A, SmirnovNG, Southon J// Stafford Res Labs Inc, 5401 Western Ave, Boulder, Co80301, USAGeology 1999 27 (10) 903

Solid phase microextraction of alkenylbenzenes and other flavor-related com-pounds from tobacco for analysis by selected ion monitoring gas chromatogra-phy/mass spectrometryStanfill SB, Ashley DL// Ctr Dis Control & Prevent, Dept Hlth & HumanServ, Natl Ctr Environm Hlth, Atlanta, Ga 30341, USAJ Chromatogr A 1999 858 (1) 79

Gender identification by matrix-assisted laser desorption/ionization time-of-flight mass spectrometryTaranenko NI, Potter NT, Allman SL, Golovlev VV, Chen CH*// *Oak RidgeNatl Lab, Div Life Sci, POB 2008, Oak Ridge, Tn 37831, USAAnal Chem 1999 71 (18) 3974

Degradation of desferrioxamines by Azospirillum irakense: Assignment of me-tabolites by HPLC/electrospray mass spectrometryWinkelmann G, Busch B, Hartmann A, Kirchhof G, Sussmuth R, Jung G//Univ Tubingen, Dept Microbiol & Biotechnol, Tubingen, GermanyBiometals 1999 12 (3) 255

Determination of zearalenone in grains by high-performance liquid chromato-graphy-tandem mass spectrometry after solid-phase extraction with RP-18 col-umns or immunoaffinity columnsZollner P, Jodlbauer J, Lindner W*// *Univ Vienna, Inst Analyt Chem,Wahringer Str 38, AU-1090 Vienna, AustriaJ Chromatogr A 1999 858 (2) 167

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CURRENT LITERATURE IN MASS SPECTROMETRY 285

7 ANALYSIS OF ORGANIC COMPOUNDS

Use of pyrolysis-GC-MS to assess the thermal degradation behaviour of poly-mers containing chlorine I. The limits of detection and measurement of HCl,deduced from a study of PVC pyrolysisDadvand N, Lehrle RS*, Parsons IW, Rollinson M// *Univ Birmingham, SchChem, POB 363, Birmingham B15 2TT, EnglandPolym Degrad Stabil 1999 66 (2) 247

Electrochemical polymerization of aniline investigated using on line electro-chemistry/electrospray mass spectrometryDeng HT, Van Berkel GJ*// Oak Ridge Natl Lab, Div Chem & Analyt Sci,Oak Ridge, Tn 37831, USAAnal Chem 1999 71 (19) 4284

Analysis of methyl tert-butyl ether and its degradation products by directaqueous injection onto gas chromatography with mass spectrometry or flameionization detection systemsHong S, Duttweiler CM, Lemley AT*// *Cornell Univ, Ithaca, NY 14853,USAJ Chromatogr A 1999 857 (1-2) 205

Secondary ion mass spectrometry of high-sulfur coal: Observation and inter-pretation of polysulfur ionsLiang HD// China Univ Min & Technol, Natl Branch Lab Characteristics CoalResources, CN-100083 Beijing, Peoples Rep ChinaChin Sci Bull 1999 44 (13) 1242

Mass spectrometric monitoring of fragments of organic compounds in adouble-flow glow discharge cellMoon HM, Kim K, Lee SC, Kim H*// *Seoul Natl Univ, Dept Chem, Seoul151742, South KoreaMicrochem J 1999 63 (1) 172

Ring structure of cyclic poly(2-vinylpyridine) proved by pyrolysis-GC/MSOhtani H, Kotsuji H, Momose H, Matsushita Y, Noda I, Tsuge S*// *NagoyaUniv, Grad Sch Engn, Dept Appl Chem, Nagoya, Aichi 464 8603, JapanMacromolecules 1999 32 (20) 6541

Aqueous dye diffusion in thin films of water-soluble poly(vinyl pyrrolidone)copolymers: A dynamic secondary ion mass spectrometry studyPinto JR, Novak SW, Nicholas M// Pinto Res & Consulting, 84 72nd St,Brooklyn, NY 11209, USAJ Phys Chem B 1999 103 (37) 8026

Synthesis and mass spectral characterization of diisopropylamino-ethanethiol,-sulfides and -disulfides and vinyl sulfidesRohrbaugh DK, Berg FJ, Szafraniec LJ, Rossman DI, Durst HD, MunavalliS*// *Geocenters Inc, Gunpowder Branch, POB 68, Aberdeen ProvingGround, Md 21010, USAPhosphorus Sulfur Silicon 1999 149 95

A new measurement technique of peroxyacetyl nitrate at parts per trillion byvolume levels: Gas chromatography/negative ion chemical ionization massspectrometryTanimoto H, Hirokawa J, Kajii Y, Akimoto H// Univ Tokyo, Adv Sci & Tech-nol Res Ctr, Meguro ku, 4-6-1 Komaba, Tokyo 153 8904, JapanJ Geophys Res-Atmos 1999 104 (D17) 21343

Analysis of polymer packaging products using pyrolysis-gas chromatography-mass spectrometryWampler TP, Zawodny CP// CDS Analyt Inc, Sci & Technol, 465 LimestoneRd, Oxford, Pa 19363, USAAm Lab 1999 31 (19) 30

Identification of 2,3-butanedione monoxime hydrogenation products by gaschromatography-mass spectrometry in an ion trap mass spectrometerWang XY, Hou ZY, Lu WM, Chen F, Zheng XM*// *Zhejiang Univ, Inst Ca-talysis, CN-310028 Hangzhou, Peoples Rep ChinaJ Chromatogr A 1999 855 (1) 341

8 ANALYSIS OF INORGANICS/ORGANOMETALLICS

Electrospray ionization in the study of polycondensation of Si(OEt)4 (Letter)Cristoni S, Armelao L, Tondello E, Traldi P*// *CNR, Ctr Studio Stabil & Re-attiv Compost Coord, via F Marzolo 1, IT-35100 Padova, ItalyJ Mass Spectrom 1999 34 (12) 1380

Triphenyl-phosphine and -arsine analogues which facilitate the electrospraymass spectrometric analysis of neutral metal complexesDecker C, Henderson W*, Nicholson BK// *Univ Waikato, Dept Chem, Pri-vate Bag 3105, Hamilton, New ZealandJ Chem Soc Dalton Trans 1999 (19) 3507

Low-temperature fast atom bombardment mass spectra of frozen nitric acid-water solutionKosevich MV, Boryak OA, Pashinskaya VA, Shelkovsky VS// Nat Acad SciUkraine, Verkin Inst Low Temperature Phys & Engn, 47 Lenin Ave, UA-310164 Kharkov, UkraineJ Mass Spectrom 1999 34 (12) 1303

Determination of nitrogen isotopomers of nitrous oxide on a modified isotoperatio mass spectrometerToyoda S, Yoshida N// JST, Japan Sci & Technol Corp, Crest, Kawaguchi,

Saitama, JapanAnal Chem 1999 71 (20) 4711

Preparation, characterization, and value assignment of carbon dioxide isotopicreference materials: RMs 8562, 8563, and 8564Verkouteren RM// NIST, Chem Sci & Technol Lab, Surface & Microanal SciDiv, Gaithersburg, Md 20899, USAAnal Chem 1999 71 (20) 4740

9 SURFACE ANALYSIS

New insights into carbon fluid chemistry and graphite precipitation: SIMSanalysis of granulite facies graphite from Ponmudi, South IndiaFarquhar J, Hauri E, Wang JH// Univ Calif San Diego, Dept Chem, Mail Code0356, 9500 Gilman Dr, La Jolla, Ca 92093, USAEarth Planet Sci Lett 1999 171 (4) 607

Calcium tracer diffusion in (La,Ca)CrO3 by SIMSHorita T, Ishikawa M, Yamaji K, Sakai N, Yokokawa H, Dokiya M// Natl InstMat & Chem Res, 1-1- Higashi, Tsukuba, Ibaraki 305 8565, JapanSolid State Ionics 1999 124 (3-4) 301

Formation and cascading decay of hollow Ar atoms at a Si surfaceStolterfoht N, Bremer JH, Muino RD// Hahn Meitner Inst Berlin GmbH,Bereich Festkorperphys, Glienicker Str 100, DE-14109 Berlin, GermanyInt J Mass Spectrom 1999 192 425

10 ENVIRONMENTAL ANALYSIS

Determination by solid-phase microextraction/gas chromatography/mass spec-trometry of polycyclic aromatic hydrocarbons in bitumen fumes during roadpaving (Letter)Agozzino P, Avellone G, Boscaino G, Miceli S// *Univ Palermo, Dipt Chim& Tecnol Farm, via Archirafi 32, IT-90123 Palermo, ItalyJ Mass Spectrom 1999 34 (12) 1383

Analysis of metsulfuron-methyl in soil by liquid chromatography/tandem massspectrometry. Application to a field dissipation studyBossi R, Seiden P, Andersen SM, Jacobsen CS, Streibig JC// Natl EnvironmRes Inst, Frederiksborgvej 399, DK-4000 Roskilde, DenmarkJ Agric Food Chem 1999 47 (10) 4462

Determination of short chain polychlorinated paraffins in fish samples by shortcolumn GC/ECNI-MSCoelhan M// Tech Univ Munich, Chair Chem Tech Anal, DE-85350 FreisingWeihenstephan, GermanyAnal Chem 1999 71 (20) 4498

Analysis of linear alkylbenzenesulfonates in water samples by large-volumeinjection-port derivatization and gas chromatography-mass spectrometryDing WH, Chen CT// Natl Cent Univ, Dept Chem, Chungli 32054, TaiwanJ Chromatogr A 1999 857 (1-2) 359

Detection of chlorinated and brominated byproducts of drinking water disin-fection using electrospray ionization-high-field asymmetric waveform ion mo-bility spectrometry-mass spectrometryElls B, Barnett DA, Froese K, Purves RW, Hrudey S, Guevremont R*// *NatlRes Council, Ottawa, Ontario, Canada K1A 0R6Anal Chem 1999 71 (20) 4747

Effects of cultural conditions on denitrification by Pseudomonas stutzeri meas-ured by membrane inlet mass spectrometryFirth JR, Edwards C// Univ Liverpool, Sch Biol Sci, Life Sci Bldg, Crown St,Liverpool L69 7ZB, EnglandJ Appl Microbiol 1999 87 (3) 353

Development of aromatic compounds of urban aerosols in the course of a 24-hour period: A study using two-step laser mass spectrometry (French, EnglishAbstract)Haefliger OP, Bucheli TD, Zenobi R// ETH Zurich, Chim Organ Lab, Univer-sitatsstr 16, CH-8092 Zurich, SwitzerlandAnalusis 1999 27 (4) 337

Direct REE determination in fresh waters using ultrasonic nebulization ICP-MSHalicz L, Segal I, Yoffe O// Geol Survey Israel, 30 Malkhe Israel St, IL-95501 Jerusalem, IsraelJ Anal Atom Spectrom 1999 14 (10) 1579

An investigation of micro-scale sealed vessel thermal extraction-gaschromatography-mass spectrometry (MSSV-GC-MS) and micro-scale sealedvessel pyrolysis-gas chromatography-mass spectrometry applied to a standardreference material of an urban dust/organicsHall PA, Watson AFR*, Garner GV, Hall K, Smith S, Waterman D, HorsfieldB// *Manchester Metropolitan Univ, Atmosphere Res & Informat Ctr, DeptGeog & Environm Sci, Chester St, Manchester M1 5GD, EnglandSci Total Environ 1999 235 (1-3) 269

Methylmercury monitoring in rainwater samples using in situ ethylation incombination with GC-AFS and GC-ICP-MS techniquesHolz J, Kreutzmann J, Wilken RD, Falter R// Nordum Inst Environm & AnalGmbH & Co KG, Weidenbruch, DE-18196 Kessin Rostock, GermanyAppl Organometal Chem 1999 13 (10) 789

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286 CURRENT LITERATURE IN MASS SPECTROMETRY

A GC-MS method for the determination of polar organic compounds in atmos-pheric samplesLimbeck A, Puxbaum H*// *Vienna Univ Technol, Inst Analyt Chem, Getrei-demarkt 9-1514, AU-1060 Vienna, AustriaInt J Environ Anal Chem 1999 73 (4) 329

Wide band ion isolation in an ion trap for the analysis of polychlorobiphenyls(Letter)Moret I, Piazza R, Gambaro A, Traldi P, Guidugli F*// *ThermoQuest Italia,Strada Rivoltana, IT-20090 Rodano, ItalyJ Mass Spectrom 1999 34 (12) 1389

An optimized sampling of GC-MS analysis method for benzene in exhaledbreath, as a biomarker for occupational exposurePlebani C, Tranfo G, Salerno A, Panebianco A, Marcelloni AM// Natl InstPrevent & Occupat Safety, Dept Occupat Hyg, IT-00040 Monte Porzio Ca-tone, RM, ItalyTalanta 1999 50 (2) 409

Determination of parts per trillion level of carboxylic degradation products oflinear alkylbenzenesulfonates in coastal water by solid-phase extraction fol-lowed by liquid chromatography/ionspray/mass spectrometry using negativeion detectionRiu J, Gonzalez-Mazo E, Gomez-Parra A, Barcelo D// CSIC, IIQAB, DeptEnvironm Chem, Jordi Girona 18-26, ES-08034 Barcelona, SpainChromatographia 1999 50 (5-6) 275

Determination of siloxanes and VOC in landfill gas and sewage gas by canis-ter sampling and GC-MS/AES analysisSchweigkofler M, Niessner R*// *Univ Munich, Inst Hydrochem, Marchionin-istr 17, DE-81377 Munich, GermanyEnviron Sci Technol 1999 33 (20) 3678

Ultra-trace-level determination of polar pesticides and their transformationproducts in surface and estuarine water samples using column liquid chromat-ography-electrospray tandem mass spectrometrySteen RJCA, Hogenboom AC, Leonards PEG, Peerboom RAL, Cofino WP,Brinkman UAT// Free Univ, Inst Environm Studies, De Boelelaan 1115, NL-1081 HV Amsterdam, The NetherlandsJ Chromatogr A 1999 857 (1-2) 157

Carbon isotope ratio monitoring-gas chromatography-mass spectrometricmeasurements in the marine environment: Biomarker sources and paleoclimateapplicationsTolosa I, Lopez JF, Bentaleb I, Fontugne M, Grimalt JO// Int Atom EnergyAgcy, Marine Environm Lab, 4 Quai Antoine 1, POB 800, MC-98012 MonteCarlo, MonacoSci Total Environ 1999 2389 473

Analysis of diquat and paraquat by solid phase extraction directly coupledwith matrix assisted laser desorption/ionization mass spectrometryVermillion-Salsbury RL, Hercules DM*// *Vanderbilt Univ, Dept Chem, Box1583, Nashville, Tn 37235, USAInt J Environ Anal Chem 1999 73 (4) 297

Doubly charged ions in the electron ionization mass spectra of 4,6-di(substi-tuted)amino s-triazinesVincze A, Yinon J, Peres T, Lifshitz C*// *Inst Biol Res, IL-74100 Ness Zi-ona, IsraelInt J Mass Spectrom 1999 192 99

Analytical method development for the determination of four biocides used inantifouling paints in estuarine waters and sediments by gas chromatography-mass spectrometryVoulvoulis N, Scrimshaw MD, Lester JN*// *Univ London, Imperial Coll SciTechnol & Med, Environm Proc & Water Technol Grp, TH Huxley Sch, Lon-don SW7 2BP, EnglandChromatographia 1999 50 (5-6) 353

In-line catalytic derivatization method for selective detection of chlorinatedaromatics with a hyphenated gas chromatography/laser mass spectrometrytechnique: A concept for comprehensive detection of isomeric ensemblesZimmermann R, Rohwer ER, Heger HJ// GSF Forschungszentrum Umwelt &Gesundheit, Inst Okol Chem, DE-85764 Oberschleissheim, Neuherberg, Ger-manyAnal Chem 1999 71 (19) 4148

11 ELEMENTAL ANALYSIS

Determination of Rh, Pd, and Pt in polar and alpine snow and ice by doublefocusing ICPMS with microconcentric nebulizationBarbante C, Cozzi G, Capodaglio G, Van de Velde K, Ferrari C, Veysseyre A,Boutron CF, Scarponi G, Cescon P// Univ Venice, Dipt Sci Ambientali, Dor-soduro 2137, IT-30123 Venice, ItalyAnal Chem 1999 71 (19) 4125

Quality assurance of arsenic, lead, tin and zinc in copper alloys using axial in-ductively coupled plasma time-of-flight mass spectrometry (ICP-TOF-MS)Emteborg H, Tian XD, Adams FC*// *Univ Instelling Antwerp, Dept Chem,Micro & Trace Anal Ctr, Universitetsplein 1, BE-2610 Wilrijk, BelgiumJ Anal Atom Spectrom 1999 14 (10) 1567

Accelerator mass spectrometry measurements and model calculations of iron-60 production rates in meteoritesKnie K, Merchel S, Korschinek G, Faestermann T, Herpers U, Gloris M, Mi-

chel R// Tech Univ Munich, Fak Phys, DE-85748 Garching, GermanyMeteorit Planetary Sci 1999 34 (5) 729

Urinary selenium speciation by high-performance liquid chromatography-inductively coupled plasma mass spectrometry: Advantages of detection with adouble-focusing mass analyser with a hydride generation interfaceLa Fuente JMG, Marchante-Gayon JM, Sanchez MLF, Sanz-Medel A*//*Univ Oviedo, Dept Phys & Analyt Chem, C/ Julian Claveria 8, ES-33006Oviedo, SpainTalanta 1999 50 (1) 207

EDTA as the modifier for the determination of Cd, Hg and Pb in fish byslurry sampling electrothermal vaporization inductively coupled plasma massspectrometryLiao HC, Jiang SJ*// *Natl Sun Yat Sen Univ, Dept Chem, Kaohsiung 804,TaiwanJ Anal Atom Spectrom 1999 14 (10) 1583

Measurement of total boron and 10B concentration and the detection and meas-urement of elevated 10B levels in biological samples by inductively coupledplasma mass spectrometry using the determination of 10B:11B ratiosMoreton JA, Delves HT// Milestones, Ampleforth YO62 4DA, EnglandJ Anal Atom Spectrom 1999 14 (10) 1545

Trace metals analysis in estuarine and seawater by ICP-MS using on line pre-concentration and matrix elimination with chelating resinNicolai M, Rosin C, Tousset N, Nicolai Y// INSERM U420, Lab Hyg & RechSante Publ, 11 bis rue Gabriel Peri, FR-54500 Vandoeuvre Les Nancy, FranceTalanta 1999 50 (2) 433

Alkylating vaporization of antimony using tungsten boat furnace-sample cu-vette technique for inductively coupled plasma mass spectrometryOkamoto Y// Hiroshima Univ, Grad Sch Sci, Dept Chem, Kagamiyama 1-3-1,Higashi-Hiroshima 739 8526, JapanJ Anal Atom Spectrom 1999 14 (10) 1631

Direct isotope ratio measurement of ultra-trace lead in waters by double focus-ing inductively coupled plasma mass spectrometry with an ultrasonic nebuliserand a desolvation unitPoitrasson F, Dundas SH// University Toulouse 3, CNRS, UMR MecanismesTransfert Geol, 5563 Lab Geochim, 38 rue 36 Ponts, FR-31400 Toulouse,FranceJ Anal Atom Spectrom 1999 14 (10) 1573

Determination of selenium species in human urine by high performance liquidchromatography and inductively coupled plasma mass spectrometryQuijano MA, Gutierrez AM*, Perez-Conde MC, Camara C// *Univ PolitecnMadrid, Dept Ciencias Basicas, ES-28014 Madrid, SpainTalanta 1999 50 (1) 165

Simultaneous determination of Cr(III) and Cr(VI) in ground and drinking wa-ters by IC-ICP-MSSacher F, Raue B, Klinger J, Brauch HJ// DVGW, Technol Zentrum Wasser,Karlsruher Str 84, DE-76139 Karlsruhe, GermanyInt J Environ Anal Chem 1999 74 (1-4) 191

Analysis of metal pollutants in the Houston Ship Channel by inductively cou-pled plasma/mass spectrometrySaleh MA, Wilson BL// Texas Sthn Univ, Dept Chem, Environm Chem &Toxicol Lab, Houston, Tx 77004, USAEcotoxicol Environ Saf 1999 44 (1) 113

Tin speciation in the femtogram range in open ocean seawater by gas chroma-tography/inductively coupled plasma mass spectrometry using a shield torch atnormal plasma conditionsTao H, Rajendran RB, Quetel CR, Nakazeto T, Tominaga M, Miyazaki A//Natl Inst Resources & Environm, 16-3 Onogawa, Tsukuba, Ibaraki 305 8569,JapanAnal Chem 1999 71 (19) 4208

Determination of arsenic speciation by capillary electrophoresis and ICP-MSusing a movable reduction bed hydride generation systemTian XD, Zhuang ZX, Chen B, Wang XR*// *Xiamen Univ, Dept Chem,SEDC Res Lab Analyt Sci Mat & Life Chem, CN-361005 Xiamen, PeoplesRep ChinaAtom Spectrosc 1999 20 (4) 127

Speciation of cadmium in plant tissues by size exclusion chromatography withICP-MS detectionVacchina V, Polec K, Szpunar J*// *CNRS EP132, 2 Ave Pr Angot, FR-64053 Pau, FranceJ Anal Atom Spectrom 1999 14 (10) 1557

Speciation of trace elements in proteins in human and bovine serum by sizeexclusion chromatography and inductively coupled plasma-mass spectrometrywith a magnetic sector mass spectrometerWang J, Houk RS*, Dreessen D, Wiederin DR// *Iowa State University Sci &Technol, Ames Lab, US Dept Energy, Department Chem, Ames, Ia 50011,USAJ Biol Inorg Chem 1999 4 (5) 546

Determination of copper, zinc, cadmium and lead in a fish otolith certified ref-erence material by isotope dilution inductively coupled plasma mass spec-trometry using off-line solvent extractionYoshinaga J, Morita M, Edmonds JS// Univ Tokyo, Inst Environm Studies,Bunkyo ku, Hongo 7-3-1, Tokyo 113 0033, JapanJ Anal Atom Spectrom 1999 14 (10) 1589

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