deutsche akkreditierungsstelle gmbh appendix to ...deutsche akkreditierungsstelle gmbh appendix to...

Deutsche Akkreditierungsstelle GmbH

Appendix to Accreditation Certificate D-PL-14082-01-00

in accordance with DIN EN ISO/IEC 17025:2005

Period of validity: 10 July 2013 to 9 July 2018 Date of issue: 10 July 2013

Holder of certificate:

LUFA-ITL GmbH

Dr.-Hell-Straße 6, 24107 Kiel

Tests in the areas:

Physical, physiochemical, chemical and microbiological analyses of water, waste water,

groundwater, surface water, water of swimming and bathing pools, water of bathing waters,

leachate, sludge, sediments and eluates; selected chemical and microbiological analyses of wastes

and waste eluates;

Chemical and microbiological analyses of drinking of drinking water according to the Drinking

Water Ordinance; analyses of mineral and medicinal water;

Analysis of water and sludge according to BEK 900 (Danish directive concerning quality

requirements in environmental measurements);

Microbiological, biomolecular, physical, physiochemical and chemical analysis of food, feeding

stuff and material of plants and animals;

Organoleptical analyses of food and feeding stuff; macroscopic, physical, chemical and biological

analyses of fertilisers;

Sampling of waste water, untreated and drinking water, water of swimming and bathing pools

and basins, mineral and medicinal water, water of standing waters, of aquifers and flowing

waters, and sewage sludge;

Specialist modules - water and waste

Abbreviations used: see last page

*) Within the * marked testing domains, the laboratory may apply standard or equivalent testing

methods not included in this certificate without prior notice to and approval of DakkS (Deutsche

Akkreditierungsstelle GmbH). The test methods cited are exemplary. The laboratory has a current

list of all test methods in the flexible accreditation domain.


Period of validity: 10 July 2013 to 9 July 2018 2/2

**) Within the ** marked testing domains, the laboratory may modify and develop testing

methods without prior notice to and approval of DAkkS (Deutsche Akkreditierungsstelle GmbH).

The testing methods listed are exemplary The test methods cited are exemplary. The laboratory

has a current list of all test methods in the flexible accreditation domain.

Within chapters 1-6 the laboratory is permitted to use the test methods cited here with different

revision levels of the standards, without requiring previous information and approval of the

DAkkS.

2 Analysis of water and sludge according to BEK 900 (Danish directive concerning

quality requirements in environmental measurements)

2.1 Microbiological parameters

ISO 17995

2005-06

Detection and Enumeration of thermotolerant Campylobacter

DIN EN ISO 6222

1999-07

Water quality - Enumeration of culturable micro-organisms -

Colony count by inoculation in a nutrient agar culture medium

DIN EN ISO 7899-2

2000-11

Water quality - Detection and enumeration of intestinal

enterococci - Part 2: Membrane filtration method

DIN EN ISO 16266

2008-05

Detection and Enumeration of Pseudomonas aeruginosa –

membrane filtration method

DS 266

1988-05

Vandundersoegelse. Kvalitativ og kvantitativ bestemmelse af

Salmonella i vand, slam, sediment og jord

Water quality - Qualitative and quantitative determination of

Salmonella in water, sludge, sediment and soil

DS 2255 200-01

Vandundersoegelse - Bestemmelse af coliforme bakterier og termotolerante coliforme bakterier - Fortyndingsmetoden

(MPN-metoden)

Water quality - Enumeration of coliform bacteria and

thermotolerant coliform bacteria - Multiple-tube fermentation

method (Most Probable Number-method)

DS 2256

1983-01

Vandundersoegelse. Bestemmelse af Clostridium perfringens

Water quality - Determination of Clostridium perfringens

DS 2401

1999-07

Miljoeundersoegelse. Bestemmelse af enterokokker.

Kolonitaelling paa fast substrat. Overfladeudsaed

Environmental quality - Enumeration of enterococci - Colony

count on solid medium - Spread plate method



DS 3029

2001-11

Enumeration of Legionella – modification of ISO 11731: 1998

SS 28192

1989

Detection and Enumeration of Yeasts and Moulds

Colilert 18/Quanti-Tray Method

from IDEXX

E. coli and coliform bacteria in drinking water and ground water

2.2 Chemical Parameters

M023, M043

DIN EN 25663

1993-11

Water quality; Determination of Kjeldahl nitrogen; Method after

mineralization with selenium

DIN ISO 15923-1

2012-01

Determination of ions by a discrete analysis system and

spectrophotometric detection – Part 1: Ammonium, chloride,

nitrate, nitrite, orthophosphate, silicate and sulfate

(here: Sulfate)

M016, M019, M027

DIN ISO 15705

2003-01

Water quality - Determination of the chemical oxygen demand

index (ST-COD) - Small-scale sealed tube method



M009, M011, M012

DIN EN ISO 6878

2004-09

Water quality - Determination of phosphorus - Ammonium

molybdate spectrometric method: digestion

M036

DIN EN ISO 7027

2000-04

Water quality - Determination of turbidity

M026

DIN EN ISO 7393-1

2000-04

Water quality - Determination of free chlorine and total chlorine -

Part 1: Titrimetric method using N,N-diethyl-1,4-phenylene-

diamine

DIN EN ISO 7393-2

2000-04 Berichtigung

2011

Water quality - Determination of free chlorine and total chlorine -

Part 2: Colorimetric method using N,N-diethyl-1,4-phenylene-diamine, for routine control purposes

M035: DS 289

1992-04

Bestemmelse af farvetal (sand farve): Determination of the Colour

index using the Pt-method

DIN EN ISO 7887

2012-04

Water quality - Examination and determination of colour

M037, M038, M039 DIN EN ISO 9963-1

1996-02

Water quality - Determination of alkalinity - Part 1: Determination of total and composite alkalinity

DIN EN ISO 10301

1997-08

Water quality - Determination of highly volatile halogenated

hydrocarbons - Gas-chromatographic methods

DIN EN ISO 10304-1

2009-07

Water quality - Determination of dissolved anions by liquid

chromatography of ions - Part 1: Determination of bromide,

chloride, fluoride, nitrate, nitrite, phosphate and sulfate

M013, M018, M024, M058

DIN EN ISO 11885

2009-09

Water quality - Determination of selected elements by inductively

coupled plasma optical emission spectrometry (ICP-OES)

M010

DIN EN ISO 11905-1

1998-08

Water quality - Determination of nitrogen - Part 1: Method using

oxidative digestion with peroxodisulfate

M008

DIN EN ISO 13395 1996-12

Water quality - Determination of nitrite nitrogen and nitrate

nitrogen and the sum of both by flow analysis (CFA and FIA) and spectrometric detection



M034

DIN EN ISO 14403-1

2012-10

Water quality - Determination of total cyanide and free cyanide

using continuous flow analytic

M020, M021 DIN EN ISO 15587-2

2002-07

Water quality - Digestion for the determination of elements in water - Part 2: Nitric acid digestion

DIN EN ISO 15923-1

2012-01

Determination of ions by a discrete analysis system and

spectrophotometric detection – Part 1: Ammonium, chloride,

nitrate, nitrite, orthophosphate, silicate and sulfate

(here: Chloride)

M014, M015, M049

DIN EN ISO 17294-2

2005-02

Water quality - Application of inductively coupled plasma mass

spectrometry (ICP-MS) - Part 2: Determination of 62 elements

DIN EN ISO 17993

2004-03

Water quality - Determination of 15 polycyclic aromatic

hydrocarbons (PAH) in water by HPLC with fluorescence detection

after liquid-liquid extraction

M040

DIN EN 872

2005-04

Water quality - Determination of suspended solids - Method by

filtration through glass fibre filters

DIN EN ISO 12846

2012-08

Water quality – Determination of mercury – method using atom

absorption spectrometry (AAS)

M032, M033

DIN EN 1484

1997-08

Water analysis - Guidelines for the determination of total organic

carbon (TOC) and dissolved organic carbon (DOC)

M017, M042

DIN EN 1899-1

1998-05

Water quality - Determination of biochemical oxygen demand

after n days (BODn) - Part 1: Dilution and seeding method with

allylthiourea acid addition

DIN EN ISO 12673

1999-05

Water quality - Gas chromatographic determination of some

selected chlorophenols in water

M022

DIN EN 25814

1992-11

Water quality; determination of dissolved oxygen by the

electrochemical probe method

M006

DIN EN 26777

1993-04

Water quality; determination of nitrite; molecular absorption

spectrometric method



DIN EN 27888

1993-11

Water quality; determination of electrical conductivity

DIN 38404-4 1976-12

German Standard Methods for Analysing of Water, Waste Water and Sludge; Physical and Physical-chemical Parameters (Group C);

Determination of Temperature (C 4)

DIN 38405-4

1985-07

German standard methods for the examination of water, waste

water and sludge; anions (group D); determination of fluoride

(D 4)

M004

DIN 38406-5

1983-10


water and sludge; cations (group E); determination of ammonia-

nitrogen (E 5)

DIN 38407-9

1991-05


water and sludge; substance group analysis (group F);

determination of benzene and some of its derivatives by gas

chromatography (F 9)

M029, M041

DS 204

1980-12

Vandundersoegelse. Toerstof og gloederest

Determination of total residue and total fixed residue in water,

sludge and sediment

DS/R 209

2006-09

Wasseruntersuchung - Fette und Öle - Extraktion mit Tetra-

chlorethen und Messungen mit Infrarot-Spektrophotometrie

DS 217

1991-08

Vandundersoegelse. COD (Oxygenforbrug med kaliumdichromat)

Water analysis - Determination of the chemical oxygen demand

(dicromate method)

M031

DS 236

1977-12

Vandundersoegelse. Aggressivitet over for calciumcarbonat

Water analysis - Stability with respect to calcium carbonate

M030

DS 278

1976-02

Vandundersoegelse. Bestemmelse af sulfid i recipient- og

drikkevand

Water analysis - Determination of sulphide in natural and pure

water

DS 280

1976

Bestimmung von Sulfid in Abwasser: Determination of sulfide in

waste water



M002

REFLAB methode 2

2002

Biokemisk oxygenforbrug over 5 doegn (BOD5) pa lavt niveau med

tilsaetning af N-allylthiourea

Biochemical oxygen demand over 5 days (BOD5) at low-level,

adding N-allylthiourea

QMP_504_KI_50_211

2009-12

Prüfung von Trinkwasser auf Geruch, Geschmack und

Geruchsschwellenwert; Determination of smell, taste and

threshold value of smell of drinking water

5 Analysis of feeding stuff, food, materials made from plants and animals

5.1 Preparation and pretreatment of samples*

ASU L 00.00-19/1

2003-12

Analysis of food - Determination of trace elements in food; Part

1: Treatment under pressure

ASU L 01.00-1

2011-06

Analysis of food - General guideline for the preparation of

analytical samples and the preparation of initial suspensions

and decimal dilutions for microbiological analysis - Part 5:

Specific rules for the preparation of milk and milk products

ASU L 02.07-1

1987-06

Analysis of food - Preparation of samples for microbiological

analysis; Method for powdered milk products

ASU L 03.00-1

2011-06




Specific rules for the preparation of cheese

ASU L 04.00-1

2011-06




Specific rules for the preparation of butter

ASU L 06.00-16

2004-12

Analysis of food - Microbiological analysis of meat and meat

products; Sample preparation

ASU L 42.00-1 2011-06

General guideline for the preparation of analytical samples and the preparation of initial suspensions and decimal dilutions for

microbiological analysis - Part 5: Specific rules for the

preparation of ice cream



ASU L 48.01-6

2011-06




Specific rules for the preparation of baby and infant formula on

the basis of milk

VDLUFA VII, 2.1.1

2011

Wet digestion under pressure

5.2 Organoleptical characteristic values

ASU L 00.90-6

1997-09

Analysis of food - Organoleptical testing methods; Simple

descriptive test

DLG-Testing stipulations and

test schemes 2011

Sampling and test technology for DLG organoleptic test


test schemes 2011

Organoleptic evaluation of bread, fine backed goods, cereal

food and confectionery in accordance with DLG test scheme


test schemes 2011

Organoleptic evaluation of convenience food in accordance

with DLG test scheme.


test schemes 2011

Organoleptic evaluation of meat products (ham and sausage) in

accordance with DLG test scheme


test schemes 2011

Organoleptic evaluation of milk and milk products including ice

cream in accordance with DLG test scheme


test schemes 2011

Organoleptic evaluation of fruit drinks in accordance with DLG

test scheme


test schemes 2011

Organoleptic evaluation of spirituous and alcoholic mixed

beverages in accordance with DLG test scheme


test schemes 2011

Organoleptic evaluation water in accordance with DLG test

scheme

5.3 Determination of characteristic values with physical and physiochemical methods

ASU 04.00-14

1996-02

Determination of the hardness of butter



ASU L 06.00-2

1980-09

Measurement of the pH value in meat and meat products

ASU L 06.00-8

2010-09

Determination of hydroxyproline content in meat and meat

products

ASU L 06.35-2 (EC)

1984-05

Standards for water content of frozen and deep frozen chicken

and hen; II: Drip method

VDLUFA. VI, C 8.2

2000

Acidity; pH value in milk and milk products

VDLUFA VI, C 25.2

1988

Physical testing methods of butter; Hardness

QMP_504_KI_51_142_x

1997-09

Grill juice loss

5.4 Determination of ingredients

5.4.1 Via gravimetry*

ISO 8262-1

2005-09

Milk products and milk-based foods - Determination of fat

content by the Weibull-Berntrop gravimetric method

(Reference method) - Part 1: Infant foods

ISO 8262-2

2005-09

Milk products and milk-based foods - Determination of fat

content by the Weibull-Berntrop gravimetric method

(Reference method) - Part 2: Edible ices and ice-mixes

ISO 8262-3 2005-09

Milk products and milk-based foods - Determination of fat content by the Weibull-Berntrop gravimetric method

(Reference method) - Part 3: Special cases

DIN EN ISO 1735

2005-05

Gravimetric methods for determination of fat content in milk

and milk products in accordance with SCHMID-BONDZYNSKI-

Ratzlaff

DIN EN ISO 2450

2009-03

Cream - determination of fat content - gravimetric method

(reference method)

DIN EN ISO 3727-1

2002-04

Butter. Determination of moisture, non-fat solids and fat

content - Part 1: Determination of moisture content

DIN EN ISO 3727-2

2002-04

Determination of moisture, non-fat solids and fat content of

butter - Part 2: Determination of non-fat solids



DIN EN ISO 8381

2009-03

Gravimetric methods for determination of fat content in milk

and milk products in accordance with RÖSE-GOTTLIEB

ASU L 00.00-18

1997-01 and

Corrigendum

2002-12

Determination of total dietary fibre in food

ASU L 02.06-E/2

1981-01

Dry matter (water contents); Water contents of powdered milk

products

ASU L 06.00-3

2004-07

Determination of dry matter in meat and meat products

ASU L 06.00-4

2007-04

Determination of ash in meet and meat products

ASU L 06.00-6

1980

Determination of total fat content in meat and meat products

VDLUFA III, 6.6.1

1999

Determination of enzyme-soluble organic substance

VDLUFA VI, C 35.3

1985

Dry matter (water content); Sea sand method

VO (EC) 152/2009, III, A

2009-02

Determination of moisture content in feed stuffs

VO(EC) 152/2009, III, H

2009-02

Determination of crude fat

VDLUFA III, 6.1.1

1993

VO(EC) 152/2009, III I

2009-02

Determination of crude fibre (Tecator)

VO(EC) 152/2009, III, M

2009-02

Determination of crude ash

VO(EC) 152/2009, III, N

2009-02

Determination of the ash fraction that is insoluble in

hydrochloric acid

5.4.2 Via Titrimetry*



DIN EN ISO 8968-1

2013-04

Milk and milk products - determination of the nitrogen content

and calculation of the crude protein content

ASU L 06.00-5

2010-09

Determination of the table salt content in meet and meat products

ASU L 06.00-7

2007-04

Determination of crude protein content in meat and meat

products

VO(EC) 152/2009, III, C

2009-02

Determination of crude protein content in feeding stuffs

VO(EC) 152/2009, III, Q

2009-02

Determination of chlorine from chlorides

VDLUFA VI, C 10.6.2

1988

Direct determination of inorganic components in milk and milk

products; Chloride in cheese in accordance with ERBACHER

5.4.3 Via photometric and polarimetric methods*

ASU L 02.00-9

2010-09

Determination of lactose and galactose content of milk and

milk products – enzymatic testing method

ASU L 02.00-12

2009-06

Determination of saccharose and glucose in milk products and

ice cream – enzymatic testing method

ASU L 01.00-26/1

2011-01

Determination of L- and D-lactic acid (L- and D- lactate) in milk

and milk products - enzymatic testing method (deviation: also

for feeding stuffs)

VDLUFA III, 12.1.1+2/12.3.1

1976

Determination of carotene and/or xanthophyll upon hot

saponification

VO(EC) 152/2009, III, J

2009-02

Determination of sugar

VO(EC) 152/2009, III, K

2009-02

Determination of lactose

VO(EC) 152/2009, III, L

2009-02

Determination of starch



5.4.4 Determination of elements via spectrometric methods*

DIN EN ISO 11885 (E 22)

2009-09

Water quality - Determination of selected elements through

inductively-coupled plasma atomic emission spectrometry (ICP-

OES)

(deviation: Matrix - foodstuffs and feeding stuffs)

DIN EN ISO 17294-2 (E 29)

2005-02

Water quality – Application of inductively coupled plasma mass


(deviation: Matrix - food stuffs and feeding stuffs, selected

elements)

DIN EN 15510

2007-10

Feeding stuffs - Determination of calcium, sodium, phosphor,

magnesium, potassium, iron, zinc, copper, manganese, cobalt,

molybdenum, arsenic, lead and cadmium by ICP-AES

DIN EN 15621

2012-04


magnesium, potassium, sulphur, iron, zinc, copper, manganese

and cobalt by ICP-AES

VDLUFA III, 10.8.2

2006

Determination of selected elements in plant material and

feeding stuffs with ICP-OES

(Determination in matrix-specific extraction solutions)

VDLUFA III, 17.9.1

2006

Determination of 14 elements in plants, as well as basic feeding

stuffs and complete feeding stuffs by ICP-MS (Determination in matrix-specific extraction solutions)

5.4.5 Determination of organic ingredients via liquid chromatography (LC) methods**

DIN EN 12821

2009-08

Foodstuffs - Determination of vitamin D with HPLC;

determination of cholecalciferol (D3) or ergocalciferol D2)

DIN EN 12822

2000-07

Foodstuffs - Determination of vitamin E with HPLC, α, β, γ and

δ-tocopherols

DIN EN 14122

2003-09

Corrigendum

2012-04

Foodstuffs - Determination of vitamin B1 with HPLC

DIN EN 14152

2003-10

Corrigendum

2012-04

Foodstuffs - Determination of vitamin B2 with HPLC



DIN EN 14663

2006-03

Foodstuffs - Determination of vitamin B6 (including glucosidic-

bound compounds) with HPLC

ASU L.00.00-9

1984-11

Examination of foodstuffs - Determination of preservatives in

low-fat foodstuffs

ASU L 40.00-7

1999-11

Corrigendum

2009-11

Determination of saccharide content

(deviation: Use of methods for foodstuffs and feeding stuffs in

general

ASU L 49.00-1

1991-06

Determination of vitamin D in dietetic food

ASU L 49.00-5

2006-12

Determination of tocopheroles and tocatrienoles in dietetic

food

VDLUFA II, 4.11.5; 4. suppl.

1997

Determination of methionine in feeding stuffs with high

chloride

VDLUFA III, 4.11.6

2004

Determination of lysine, methionine and threonine in

commercial amino acid products and premixes

VDLUFA III, 13.6.1

1983

Determination of Choline-Chloride

VDLUFA III, 13.8.1

2007

Determination of vitamin D3 in feeding stuffs; HPLC method

VDLUFA III, 13.9.1

2006

Feeding stuffs - Determination of B vitamins, including nicotinic

acid, HPLC method

VO (EC) 152/2009, IV, A

2009-02

Determination of vitamin A content

VO (EC) 152/2009, IV, B

2009-02

Determination of vitamin E content

VO(EC) 152/2009, III, F

2009-02

Determination of amino acids (except for tryptophane)

VO(EC) 152/2009, III, G

2009-02

Determination of tryptophane

QMP_504_KI_52_020_x

2010-08

Determination of vitamin C (ascorbic acid) in foodstuffs via

HPLC



QMP_504_KI_52_021_x

2009-09

Determination of vitamin K1 (phyllocquinone); HPLC method

after DC cleaning

QMP_504_KI_52_022_x

2009-05

Determination of menadione (vitamin K3); HPLC method

QMP_504_KI_52_023_x

2010-08

Determination of preservatives in foodstuffs via HPLC

QMP_504_KI_52_028_x

2009-04

Determination of vitamin K1 (phyllochinon); HPLC with post-

column derivatisation

QMP_504_KI_52_136_x

2011-08

Determination of selected sugars in foodstuffs and beverage

samples with HPLC-ELSD

5.4.6 Determination of organic ingredients via gas chromatography (GC) methods*

ASU L 05.00-16

2010-09

Determination of cholesterole in foodstuffs (gas

chromatography methods)

DGF VI 10a/11a

2000

Gas chromatography: Analysis of fatty acids and fatty acid

distribution

(deviations: Use also is milk fats, without C4 and C6 fatty acid

determination)

VDLUFA III, 5.6.2

1983

Presentation of fatty acid methyl ester for gas chromatographic

determination of the total acid range of feed fats

VDLUFA III, 5.6.2

1983 with DGF C IV 11 D

1998

Determination of eruca acid contents in rape samples

expressed in percent of the total fatty acids



5.5 Residues and trace elements

5.5.1 Via photometric methods*

DIN EN ISO 14673-3

2004-05

Determination of the nitrite and nitrate content in milk, Part 3

(deviation: Concentration and production of reagents)

ASU L 00.00-35

1998-09

UV photometric determination of dithiocarbamates and/or

thiuramdisulfides in food of vegetal origin (xanthogenate

method)

ASU L 07.00-12

1990-12

Determination of the nitrite and nitrate content in meat

products

(deviation: Concentration and production of reagents)

VDI 3795 Sheet 1

1976-06

Determination of fluorine contents in biological samples and in

IRMA solutions; Photometric determination

VO (EC) 152/2009, V, A

2009-02

Determination of the content of free and total gossypol

5.5.2 Via electrochemical methods*

DIN EN 16279

2012-09

Feeding stuffs - Determination of fluoride with an ion-selective

electrode (ISE)

5.5.3 Determination of elements via spectrometric methods*

DIN EN ISO 11885 (E 22)

2009-09


inductively-coupled plasma atomic emission spectrometry (ICP-

OES)

(deviation: Matrix - foodstuffs and feeding stuffs)

DIN EN ISO 17294-2 (E 29)

2005-02



(deviation: Matrix - food stuffs and feeding stuffs, selected

elements)

DIN EN 15510

2007-10


magnesium, potassium, iron, zinc, copper, manganese, cobalt,

molybdenum, arsenic, lead and cadmium by ICP-AES

DIN EN 15621

2012-04


magnesium, potassium, sulphur, iron, zinc, copper, manganese

and cobalt by ICP-AES



DIN EN 15763

2010-04

Foodstuffs - Determination of trace elements - Determination

of arsenic, cadmium, mercury, and lead in foodstuffs

inductively coupled plasma mass spectrometry (ICP-MS) in

accordance after wet digestion

(deviation: Without mercury)

DIN EN 16277

2012-09

Animal feeding stuffs - Determination of mercury by cold-

vapour atomic absorption spectrometry (CVAAS) after

microwave pressure digestion (extraction with 65% nitric acid

and 30% hydrogen peroxide);

ASU L 00.00-19/4

1993-08

Determination of trace elements in feeding stuffs; Part 4

Determination of mercury with the cold-vapour atomic

absorption spectrometry (CVAAS) technique

VDLUFA III, 10.8.2

2006

Determination of selected elements in plant material and

feeding stuffs with ICP-OES


VDLUFA III, 17.9.1

2006

Determination of 14 elements in plants, as well as basic feeding

stuffs and complete feeding stuffs by ICP-MS


5.5.4 Determination of inorganic residues and trace substances via ion chromatography

(IC) methods*

DIN EN ISO 10304-1

2009-07

Water quality - Determination of dissolved anions via liquid ion

chromatography - Part 1

ASU L 26.00-1

2001-07

Examination of foodstuffs - Determination of the nitrate

content in vegetable products - HPLC/IC methods

5.5.5 Determination of organic residues and trace substances via liquid chromatography

(LC) methods **

DIN EN 15662

2009-02

Foods of plant origin - Determination of pesticide residues via

HPLC-MSMS or GC (QuEChERS method)

ASU L 00.00-76

2002-12

Determination of chlormequat and mepiquat in foodstuffs and

feeding stuffs (HPLC-MS/MS method)

(deviation: Smaller weighted sample, automated sample

injection)



Official Journal of the

European Communities,

1864/90,

No. L 179/28

Determination of the glucosinal content in oilseeds by HPLC

IDF 171

1995

Determination of aflatoxin M1 in milk and milk powder via

HPLC cleanup with immuno-affinity column

VDLUFA III, 16.1.2

1993

Determination of aflatoxin B1; official method B: HPLC EC

method VDLUFA method

VDLUFA III, 16.1.4

1993

Determination of alphatoxin B1, extract cleaning with immuno-

affinity column VDLUFA method

VDLUFA III, 16.10.1

1993

Determination of ochratoxin A VDULFA method

VDLUFA III, 16.11.1

2004

Determination of ergosterol HPLC

QMP_504_KI_52_026_x

2011-03

Determination of ochratoxin A upon cleanup on immuno-

affinity column; HPLC method

QMP_504_KI_52_027_x

2011-10

Determination of ethoxyquin (HPLC method)

QMP_504_KI_52_113_x

2011-03

Determination of deoxynivalenol (DON) and zearalenon (ZEA)

in foodstuffs and feeding stuffs (HPLC-MS/MS methods)

QMP_504_KI_52_116_x

2011-03

Determination of Chloramphenicol in foodstuffs and feeding

stuffs (HPLC-MS/MS method)

QMP_504_KI_52_117_x

2011-03O

Determination of acrylamide in foodstuffs (HPLC-MS/MS

methods)

QMP_504_KI_52_123_x

2011-03

Determination of trichothecene (mycotoxins) via HPLC-MSMS

in foodstuffs and feeding stuffs

QMP_504_KI_52_129_x

2011-03

Determination of selected antibiotics in feeding stuffs samples

via HPLC-MSMS (screening multi-method)



QMP_504_KI_52_137_x

2012-12

Determination of coumarin in food samples via HPLC-UV

QMP_504_KI_52_145_x

2013-04

Determination of polar pesticides (e.g. ethephon, morpholine)

in fruit and vegetable samples (HPLC-MSMS method)

QMP_504_KI_52_146_x

2013-04

Determination of glyphosate and AMPA as FMOC derivatives

(HPLC-MSMS method)

QMP_504_KI_52_147_x

2013-04

Determination of selected ergo alkaloids in foodstuffs samples

and feeding stuff samples via LC-MSMS

QMP_504_KI_52_148_x

2013-04

Determination of ochratoxin A in foodstuffs samples and

feeding stuffs samples via LC-MSMS

QMP_504_KI_52_149_x

2013-04

Determination of aflatoxins in foodstuffs samples and feeding

stuffs samples via LC-MSMS

5.5.6 Determination of organic residues and trace substances via gas chromatography

methods **

DIN EN 15662

2009-02

Foods of plant origin - Determination of pesticide residues via

HPLC-MSMS or GC (QuEChERS method)

ASU L 00.00-34

2010-09

Modular multi-methods for determination of plant protectant

residues is foodstuffs (Extended new version of DFG

method S 19)

ASU L 00.00-36.2

2004-07

Determination of bromide residues in low-fat foodstuffs,

Part 1: Determination of total bromide

ASU L 00.00-49/2

1999-11 and

Corrigendum

2002-12

Determination of dithiocarbomate and thiram disulfide

residues (gas chromatography method)

deviation: smaller weighted sample, automated sample

injection)

VDLUFA. VII, 3.3.2.4

2011

Determination of polychlorinated dibenzo-p-dioxins (PSDD) and

polychlorinated dibenzofurans (PCDF), and additional selected

coplanar polychlorinated biphenyls (non-ortho PCB) in feeding

stuffs

VDLUFA VII, 3.3.3.2, 1. suppl.

2011

Determination of polynuclear aromatic hydrocarbons (PAH) in

plant material



QMP_504_KI_52_046_x

2007-06

KI_52_046_x Determination of selected polychlorinated

biphenyls (PCB) in feeding stuffs, foodstuffs and simultaneously

with the dioxin analysis via GC

QMP_504_KI_52_139_x

2011-09

Determination of chlorophenol residues in solid samples via CS-

MS (QuEChERS method)

5.6 Microbiological and molecular biological examinations of foodstuffs

5.6.1 Determination of the microbiological activity of vitamins with auxotrophic

microorganisms

DIN EN 14131

2003-09

Foodstuffs - microbiological determination of folate

USP 21, 3rd Supplement,

Method 88

1986

Determination of the microbiological activity of biotin (original

title: Biological Tests and Assays - Biotin Assay)

USP 34 Methode 91

2011

Determination of Calcium-D-Pantothenate (original title:

Biological Tests and Assays - Calcium Pantothenate Assay)

USP 34 Methode 171

2011

Determination of the microbiological activity of vitamin B12

(original title: Biological Test and Assays - Vitamin B12 Activity

Assay) (deviation: The concentration of sodium sulphite in the

extraction solution is not adjusted to the weighted sample)

USP 34 Methode 441

2011

Niacin or Niacinamide Assay (Determination of the

microbiological activity of niacin and niacinamide)

(deviation: Extraction with HCI instead of sulphuric acid)

QMP_504_KI_51_009

2013-02

Determination of inosite

QMP_504_KI_51_027

2013-02

Determination of the microbiological activity of choline

5.6.2 Analysis of antibiotics in feeding stuffs via microbiological sensitivity test

QMP_504_KI_51_022

2005-03

Qualitative detection of antibiotics in feeding stuffs -

microbiological diffusion in agar medium

QMP_504_KI_51_024

2005-03

Identification of antibiotics in feeding stuff – microbiological

method - 2005 method (bioautography)



5.6.3 Qualitative and quantitative detection of microorganisms via cultural methods*

(identifying bacterial count)

ISO 4831

2006-08

Microbiology - General guidance for the enumeration of

coliforms; Most probable number technique

ISO 4832

2006-02


coliforms; Colony count technique

ISO 4833

2003-06

Microbiology - General guidance for the enumeration of micro

organisms; Colony count technique at 30 °C

ISO 6579

2007-10

Microbiology of food and animal feeding stuffs - Horizontal

method for the detection of Salmonella spp.

ISO 7251

2005-02


presumptive Escherichia coli; Most probable number technique

ISO 13559

2002-11

Butter, fermented milks and fresh cheese - Enumeration of

contaminating microorganisms - Colony-count technique at

30 °C

ISO 15213

2003-05


method for the enumeration of sulphite-reducing bacteria

growing under anaerobic conditions

ISO 15214

1998-08

Microbiology of food and animal feeding stuffs - horizontal

method for the counting of mesophilic lactic acid bacteria -

colony count method at 30°C

ISO 21527-1

2008-07


method for the enumeration of yeasts and moulds - Part 1:

Colony count technique in products with water activity greater

than 0.95

ISO 21527-2

2008-07


method for the enumeration of yeasts and moulds - Part 2:

Colony count technique in products with water activity less

than or equal to 0.95

DIN ISO 21528-1

2009-12

Microbiology of food and feeding stuffs - horizontal method for

detection and enumeration of enterobacteriaceae - part 1:

Detection and enumeration via MPN technique with pre-

enrichment



DIN ISO 21528-2

2009-12


detection and enumeration of Enterobacteriaceae - part 2:

Colony counting technology

DIN EN ISO 6887-1

1999-04

Microbiology of food and animal feeding stuffs - General

guideline for the preparation of analytical samples and the

preparation of initial suspensions and decimal dilutions for

microbiological analysis - Part 1: General rules for the

preparation initial suspensions and decimal dilutions

DIN EN ISO 6887-5

2011-01

Microbiology of food and animal feeding stuffs - General

guideline for the preparation of analytical samples and the

preparation of initial suspensions and decimal dilutions for

microbiological analysis - Part 5: Specific rules for the

preparation of milk and milk products

DIN EN ISO 6888-1

2003-12


method for the enumeration of coagulase-positive

staphylococci (Staphylococcus aureus and other species) - Part

1: Methods with Baird-Parker agar

DIN EN ISO 6888-3

2005-07


method for the enumeration of coagulase-positive

staphylococci (Staphylococcus aureus and other species) - Part

3: Detection and MPN method for low bacterial counts

DIN EN ISO 7932

2005-03


method for the enumeration of Bacillus cereus - colony

enumeration method at 30°C

(deviation: Use of Bacara agar (AES. AFNOR validated))

DIN EN ISO 7937 2004-11

Microbiology of food and animal feeding stuffs - horizontal method for the enumeration of Clostridium perfringens -

colony enumeration method at 30 °C

DIN EN ISO 11290-1

2005-01


detection and enumeration of Listeria monocytogenes - Part 1:

Detection method

(deviation: Tasks in accordance with the ALOA one day method

(AFNOR validated) confirmation with rapid L-mono.)

DIN EN ISO 11290-2

2005-01


detection and enumeration of Listeria monocytogenes - Part 2:

Enumeration method

(deviation: Confirmation with rapid L-mono.)



DIN EN ISO 13720

2010-12

Meat and meat products - enumeration of presumptive

Pseudomonas spp.

DIN 10113-1

1997-07

Determination of surface colony count on fitment and utensils

in food areas - Part I: Quantitative swab method

DIN 10113-2

1997-07

Determination of surface colony count on fitment and utensils

in food areas - Part II: Semi-quantitative swab method

ASU L 06.00-18

1984-05

Examination of foodstuffs - Determination of the aerobic

enumeration at 30 °C in meat and meat products; spattle

method and poured plate method

ASU L 06.00-19

1984-05

Examination of foodstuffs - Determination of the aerobic

enumeration at 30 °C in meat and meat products; drop plate

method

ASU L 06.00-24

1987-11

Examination of foodstuffs - Determination of

Enterobacteriaceae in meat; spattle method (reference

method)

ASU L 06.00-25

1987-11

Examination of foodstuffs - Determination of

Enterobacteriaceae in meat; drop plate method

ASU L 06.00-40

1997-01

Examination of foodstuffs - Determination of the surface

colony count on meat; destructive method (removal method)

VDLUFA III, 28.1.1

2007

General documented procedure for determination of bacterial

counts via solid nutrient media

VDLUFA III, 28.1.2

2007

Procedure instruction for identification of bacteria, yeasts,

moulds and black fungi as product-typical spoilage indicating indicator germs in feeding stuffs

VDLUFA VI, 7.8.2

1996

Determination of enterococci, colony enumeration method

with kanamycin esculin azide agar



VDLUFA VI, 7.13

1996

Determination of the count of thermoduric (thermally-

resistant) microorganisms

Nordisk Metodikkommitté för

Livsmedel. NMKL No. 71, 5.

Ed., 1999

Detection of Salmonella spp. in foodstuffs

QMP_504_KI_51_133

2006-08

Determination of the count of bacillus spores from foodstuffs

Literature method: Literature method Baumgart, J.

Microbiological examination of foodstuffs

QMP_504_KI_51_166

2007-11

Determination of the count of thermophilic microorganisms -

literature method: Literature method Baumgart, J.

Microbiological examination of foodstuffs

5.7 Biochemical examinations of food and feeding stuffs

5.7.1 Analysis of nucleic acids via PCR* (Detection of genetically engineered changes,

microorganisms and other organisms groups)

DIN EN ISO 21570

2006-02

Corrigendum

2007-06

Method for detection of genetically modified organisms and

their products - quantitative based on nucleic acid based

methods, execution in the LightCycler 2

DIN EN ISO 21571

2005-05

Method for detection of genetically modified organisms and

their products - nucleic acid extraction

ASU L 00.00-98

2007-04

Analysis of food and feeding stuffs for the presence of

Salmonella spp., PCR method

ASU L 00.00-122

2008-06

Screening method for detection of genetically modified DNA

sequences in plants

(deviation: Use of the kit, “LightCycler GMO Screening Kit”

(biocetone))

ASU L 23.01-22-1

1998-03

Detection of genetically-modified soybeans.

(deviation: Use of the kit, “Lightcycler GMO Soya Quantification

Kit” (biocetone))

EURL-AP recommended

protocol: 2013-02

Detection of horse DNA using real time PCR

Government of Canada,

MFLP-25: 2006-03

MFLP-26: 2006-02

Analysis of food and feeding stuffs for the presence of shigella

spp., PCR method



QMP_504_KI_51_201

2005-01

Isolation of DNA from rapeseed, maize, soy, feeding stuffs and

foodstuffs with the Wizard Magnetic DNA Purification System

for Food (Promega)

QMP_504_KI_51_202

2005-04

Analysis of rapeseed DNA for genetically engineered

modifications via Real Time PCR

QMP_504_KI_51_203

2005-01

Analysis of maize DNA for genetically-engineered changes via

Real Time PRC

QMP_504_KI_51_206

2013-02

Analysis of food and feeding stuffs for the presence of

Salmonella spp., PCR method

QMP_504_KI_51_213

2013-02

PCR detection or PCR confirmation of various pathogenic

bacteria in accordance with literature methods

QMP_504_KI_51_216

2012-10

Analysis of food and feeding stuffs for the presence of Listeria

monocytogenes, PCR method in accordance with Guilbeaud M

et al., J. Appl. Micr. 2005

QMP_504_KI_51_217

2013-03

PCR detection or PCR confirmation of bacterial that are similar

to Clostridium estertheticum and Clostridium estertheticum in

accordance with DM et al., J. Appl. Micr. 2003

QMP_504_KI_51_207

2013-03

Analysis of animal material for the presence of specific DNA of

cattle, pig, sheep, chicken or turkey via Real Time PCR

5.7.2 Determination of toxins, allergens, antibodies, and viruses via immuno-chemical

examination methods*

QMP_504_KI_51_300

2007-01

Quantitative determination of mycotoxins (desoxynivalenol,

Zearalenone, Ochratoxine, aflatoxins) in food and feeding stuffs

due to enzyme immuno assay

QMP_504_KI_51_301

2006-10

Automated determination of anti-Salmonella antibodies in

meat juice or serum due to enzyme immuno assay

QMP_504_KI_51_304

2012-11

Allergen analysis: Quantitative determination of residues of

hazelnut, peanut, almond egg, ß-lactoglobulin, casein and

gluten in food through enzyme immuno assay



6 Examinations of fertilisers

6.1 Sample preparation

VO(EC) 2003/2003, IV, 3.1.1

2003-10

Extraction of the phosphorus soluble in mineral acids

VO(EC) 2003/2003, IV, 3.1.2

2003-10

Extraction of the phosphorus that can be dissolved in a

2% solution of antacid

VO(EC) 2003/2003, IV, 3.1.3

2003-10

Extraction of the phosphorus that can be dissolved in a

2% solution of citric acid

VO(EC) 2003/2003, IV, 3.1.4

2003-10

Extraction of the phosphorus that can be dissolved in neutral

ammonium citrate

VO(EC) 2003/2003, IV, 3.1.5.2

2003-10

Extraction of the phosphorus that can be dissolved at room

temperature in accordance with Permanent

VO(EC) 2003/2003, IV, 3.1.6

2003-10

Extraction of the water-soluble phosphorus

VO(EC) 2003/2003, IV, 8.1

2003-10

Extraction of total calcium, total magnesium and total sodium,

as well as the total sulphur in the form of sulphate

VO(EC) 2003/2003, IV, 8.3

2003-10

Extraction of water-soluble calcium, magnesium and sodium, as

well as the total sulphur in the form of sulphate

VO(EC) 2003/2003, IV, 9.1

2003-10

Extraction of total trace nutrient substances

VO(EC) 2003/2003, IV, 10.2 2003-10

Extraction of water-soluble trace nutrient substances

VDLUFA II, 4.1.2

2004

Determination the of antacid soluble phosphate, extraction

VDLUFA II, 4.1.3

1995

Determination of the citric acid soluble phosphate, extraction

VDLUFA II, 4.1.5

1995

Determination of the alkaline ammonium citrate soluble

phosphate in accordance with Petermann, extraction

VDLUFA II, 4.1.7

1995

Determination of the water soluble phosphate, extraction



VDLUFA II, 6.1.1

2004

Determination of mineral soluble calcium: Manufacturing of

the analysis solutions

VDLUFA II, 6.1.2

2004

Determination of total calcium in fertilisers with organic

fractions: Manufacturing of the analysis solutions

VDLUFA II, 6.1.3

1999

Determination of water-soluble calcium in mineral fertilisers:

Manufacturing of the analysis solutions

VDLUFA II, 7.1

2008

Magnesium: Manufacturing of the analysis solutions

VDLUFA II, 7.3.1.2

2008

Extraction of water-soluble sulphur that can be present in

different forms

VDLUFA II, 9.5.1

2004

Chemical digestion with aqua regia

6.2 Physiochemical characteristic values

DIN EN 12176 (S 5)

1998-06

Characterisation of sludge - determination of the pH value

DIN EN 12880 (S 2a)

2001-02

Characterisation of sludges - determination of the dry residue

and the water content

VDLUFA II, 6.3

1995

Determination of the alkaline effective components in calcium

fertilisers

VDLUFA II, 6.4

1995

Determination of the reactivity of carbonic acid calcium

fertilisers

VDLUFA II, 6.5.1

2008

Determination of sieve passage of fertilisers, dry method

VDLUFA II, 6.5.2

1995

Determination of sieve passage of moist or clumped fertilisers,

wet method

VDLUFA II, 10.1

1999

Determination of loss on ignition



6.3 Inorganic chemical parameters

DIN EN ISO 11885 (E 22)

2009-09


inductively-coupled plasma atomic emission spectrometry

(ICP-OES)


DIN EN ISO 17294-2 (E 29)

2005-02




VO(EC) 2003/2003, IV, 2.1

2003-10

Determination of ammonium nitrogen

VO(EC) 2003/2003, IV, 2.3.2

2003-10

Determination of total nitrogen in nitrate-containing calcium

cyanamide

VO(EC) 2003/2003, IV, 3.2

2003-10

Determination of phosphorus in the extracts (gravimetric as

Quinolinium Molybdophosphate)

VO(EC) 2003/2003, IV, 4.1

2003-10

Determination of water-soluble potassium

VDLUFA II, 3.2.1

1995

Determination of ammonium nitrogen

VDLUFA II, 3.4.1

1995

Determination of nitrate nitrogen

VDLUFA II, 3.5.2.3

2004

Determination of total nitrogen with the presence of nitrate,

reduction of the nitrate fraction with iron powder and

Tin-(II)-chloride

VDLUFA II, 3.5.2.4

1995

Determination of total nitrogen with the presence of nitrate,

reduction of the nitrate fraction with chrome powder

VDLUFA II, 4.2.2

1995

Determination of the phosphate in solutions and extracts

VDLUFA II, 4.2.4

2007

Determination of Ca, K, Mg, Na, P, S and Cl as main and

secondary fractions in fertilisers, ICP-OES method

VDLUFA II, 5.1.2

1995

Determination of mineral soluble potassium, production of the

analysis solution

VDLUFA II, 5.1.3

1995

Determination of total potassium, production of the analysis

solution



VDLUFA II, 5.2.1

2004

Determination of potassium (gavimetric method with sodium

tetraphenylboron)

VDLUFA II, 8.10

2007

Determination of micro nutrients in fertiliser extracts:

ICP-OES method

6.4 Organic-chemical parameters

VO(EG) 2003/2003, IV, 2.5

2003-10

Biuret in urea, photometric

VDLUFA II, 3.9.1

1999

Determination of biuret

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