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Dr. Gil Nonato C. Santos
Fabrication and Characterization of
Nanomaterials for
Nanotechnology Applications
DLSU Solid State
Physics Research Laboratory
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How to How to do do NanomaterialsNanomaterialscreatively?creatively?creatively?creatively?
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“INNERSPACE”- Dennis Quaid
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“Honey I Shrunk the Kids” – Rick Moranis
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Our Recipe: Semiconducting Oxide
PowderWe want to produce Semiconducting
Oxide Nanomaterials!Oxide Nanomaterials!
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Dr. Z.L. Wang (UAPT PI)
Material Science & Engineering
Georgia Institute of Technology
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Our Technique: HVPG
• Horizontal Vapor Phase Growth Technique
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MOTIVATION
• Grow high purity materials
• Source material is powder of any
form
• Greater quantity with less source
materialmaterial
• No gas molecules in between
• Versatility in composition of deposit
• Produces unusual microstructures
• Eliminate pollutants
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What will I do with the heater?
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Let’s Cook: Our Recipe and Ingredients
• A small amount of Semiconducting Oxide powder was loaded in a close-end quartz tube
• Was attached to the High Vacuum System for sealing at 10-6 Torr
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• Let’s Bake!• The sealed quartz tube
was placed in a tube furnace set with the desired growth temperature
900ºC 700ºC 400ºC
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• Temperature and
Deposition Time
Dependence of the
Geometrical Properties
of Tin Oxide
Nanostructures• Gil Nonato C. Santos, Arnel A.
Salvador, Reuben V. QuirogaSalvador, Reuben V. Quiroga
International Journal of Scientific &
Engineering Research Volume 2, Issue
10, October-2011
ISSN 2229-5518
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Synthesized SnO2 Nanomaterial via the HVPG
Bed of Nanowires Noodle Nanowires(Oishi)
Bon Jovi’s other version of Bed of Roses
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Nanobelts
• Nanobelts are have a well-defined geometrical shape and side surfaces. • Typical widths is in the range of 50 to 300 nm • Thicknesses are 10 to 30 nm.
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Physics Society of the Philippines
(Samahang Pisika ng Pilipinas)
• The Nanobelts were
featured in the first
Physics Journal in
the Philippinesthe Philippines
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Different growth temperature produced remarkable structures
Do you like vegetables?
Nanocauliflower
Nanobolo (Machete) (2nd Prize –photo micrograph contest
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SnO2 Nanomaterial on Si Substrate
• Silicon is an effective substrate for SnO2 nanomaterial. • Nanorods and nanobelts are grown without nanoparticles.
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Finalist – DOST MS Thesis - Physics
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Best Paper and Oral Presentation Award - MICROSPHIL
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Nanobelt for gas flow sensors
Dr. Z.L. Wang (UAPT PI)
Material Science & Engineering
Georgia Institute of Technology
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Two-probe measurements of electric conductance of
Nanobelts under ambient temperature
The electric conductance of the nanobelt depends on
the type and amount of molecules adsorbed on its
surface
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High Resolution SEM image of the SnO2 Nanomaterial
• The surface of the SnO2 nanomaterial is porose and composed of many uniform crystalline grains.
• It suggests that this nanomaterial is suitable for suitable for fabricating gas sensors because of the porosity over large surface.
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Photoluminescence of SnO2 Nanomaterials
• SnO2 Nanomaterial was excited
with a UV lamp
• The luminescence was a blue visible
light emission.
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2009 International Sustainable World Energy,
Engineering, and Environment Project
(I-SWEEEP) Olympiad in Houston, Texas
Simon Anthony Lorenzo and Hannah
Carize Sangalang won a silver medal for
the Philippines with their project
entitled “Development of Carbon
Nanomaterial as an Electrode Voltage Nanomaterial as an Electrode Voltage
Source” in the Senior Engineering
category
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Carissa May Enriquez and Kevin Bryan Jose
received an Honorable Mention award for their
project “Development of an Organic Battery
Using P-Toluene Polypyrrole as a Potential
Electrode Voltage Source and Coconut (Cocos
nucifera) Vinegar as Electrolyte
A – conducting polymer
B – SnO2 Nanomaterial on Si
C – Glass
E - PCB
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ZnO Nanomaterials – A. Ladines
Presented at ICMAT 2009 Singapore
3rd Place Photomicrography – Microsphil
Finalist- DOST MS Thesis – Materials Science
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CdO Nanomaterials – L. Tan
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Carbon nanowires, rods,
and tubes – J. Feraer
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Synthesis and Characterization of In2O3
NanomaterialsGwen B. Castillon, Gil Nonato C. Santos
3rd Best Paper and Oral Presentation -
Microsphil
International Journal of Scientific & Engineering
Research, Volume 3, Issue 2, February-2012
ISSN 2229-5518
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ZnS Nanowindmill and Nanorods –
K. Suycano
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Synthesis of α-Fe2O3
Nanomaterials on
Silicon Substrate
Using Horizontal Vapor
Phase Growth
Technique Technique
• Lim, T. de los Reyes, R., D.,
Castillon, G., Ladines, A.
Santos, G. N. C., Quiroga, R. V.
DLSU Solid State Physics
Research Laboratory
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Fabrication of Gallium
Nitride Nanomaterials
Grown by Horizontal
Unseeded Vapor
Phase
Growth TechniqueGrowth Technique
• Anciado, R. R., Alcantara, N., Castillon, G.,
Ladines, A., de los Reyes, R.
Santos, G. N. C., Quiroga, R. V.
DLSU Solid State Physics Department
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Synthesis and
Characterization
of TiO2
Nanomaterials
on
Silicon Substrate
by Modified
Silicon Substrate
by Modified
Horizontal
Vapor Phase
Growth
Technique• Abrasaldo, P. M. B., (BPI DOST AWARDEE)
Castillon, G., Ladines, A., de los Reyes, R.
Santos, G. N. C., Quiroga, R. V.
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Synthesis and
Photoluminescence of
Gold Nanostructures
Using Horizontal
Vapor Phase Growth Vapor Phase Growth
Technique
• Kahn, D., Ladines, A., Castillon, G., de
los Reyes, R.,
Santos, G. N. C., Quiroga, R. V.
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Preliminary THz-TDS
Measurements of
Polypyrrole with Varying
M of Na (p-TS) Composite
Nanomaterial
Mazano, C., Manzano, R., Mazano, C., Manzano, R.,
Santos, G. N. C., Quiroga, R.
DLSU Solid State Physics
Laboratory
Takage, Que, C., Furuya, T.,
Yamamoto, K., Tani, M.
Research Center for
Development
of Far-Infrared Region,
University of Fukui
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The Effect of Growth
Temperature, Dwell Time, and
Orientation of the Thermal
Gradient to the Gravitational
Field in the Synthesis of CdS
Nanomaterials using the Vapor
Phase Crystal Growth
Technique Eduardo B. Tibayan Jr., Gil Nonato C.
Finalist- DOST MS Thesis – Physics
Technique Eduardo B. Tibayan Jr., Gil Nonato C.
Santos, Reuben V. Quiroga
International Journal of Scientific & Engineering
ResearchVolume 2, Issue 10, October-2011
ISSN 2229-5518
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Synthesis and Characterization
of Superconducting
Magnesium Diboride MgB2
Nanomaterials through
Horizontal Vapor Phase Crystal
Growth Technique
Renante C. Embalzado, Gil Nonato C. Santos,
Reuben V. QuirogaReuben V. Quiroga
UP NIP CMPL Lab
International Journal of Scientific &
Engineering Research, Volume 3, Issue 2,
February-2012
ISSN 2229-5518
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Characterization of
Silver
Nanomaterials,
Synthesized by the
Horizontal Vapor
Phase Crystal
Growth Technique
for Antimicrobial for Antimicrobial
Purposes
Wilfred Espulgar, Gil Nonato C. Santos
International Journal of Scientific &
Engineering Research Volume 2, Issue 8,
August-2011 1 ISSN 2229-5518
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Synthesis and
Characterization of C-Ag
Composite Nanomaterial
for Battery Electrode
Application
Ruby Michelle N. Buot,
Gil Nonato C. Santos
International Journal of Scientific &
Engineering Research Volume 3, Issue Engineering Research Volume 3, Issue
2, February-2012
ISSN 2229-5518
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• Cadmium Selenide
Quantum Dots
Synthesized by
HVPC Growth
Technique for
Sensing Copper ion 2000
4000
6000
Counts
Se
Se
Au
Au
AuCd
Cd
Cd Au SeAuAu
SeAu
Au
Elmt Spect. Element
Atomic
Type % %
Se L ED 50.53 59.25
Cd L ED 49.47 40.75
Total 100.00
100.00
A B C
D E
PL Intensity (arb. Units)
Gold Medal – MS Thesis
Sensing Copper ion
Concentrations• Arra C. Quitaneg, Gil Nonato
C. Santos
0 5 10 15 20Energy (keV)
0
Cd Au Se Se Au
Wavelength (nm)
International Journal of Scientific & Engineering
Research Volume 2, Issue 12, December 2011
ISSN 2229-5518
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• Fabrication and
Characterization of Dye-
Sensitized Solar Cell
(DSSC) Using
Nanostructured TiO2 as
Photoelectrode• Abel F. Ole, GIL NONATO C.
SANTOSSANTOS
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• Fabrication and
Characterization of Tin
Oxide (SnO2)
Nanomaterials as
Carbon Dioxide (CO2)
Gas SensorGas Sensor• FAITH CELESTE C. BANCOLO, GIL
NONATO C. SANTOS
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• Bi2S3 Nanowires
Fabricated via
Horizontal Vapor Phase
Crystal (HVPC) Growth
Technique for
Photosensor
Application• BHEIM M. LLONA, GIL NONATO C. • BHEIM M. LLONA, GIL NONATO C.
SANTOS
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• Synthesis and
Characterization of Iron
Oxide Nanomaterials
using Horizontal Vapor
Phase Crystal (HVPC)
Growth Technique for Growth Technique for
Glucose Sensing
Application• DONNA MARIE B. DE MESA, GIL
NONATO C. SANTOS
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CATALYTIC
PERFORMANCE OF
AHYDROGEN FUEL CELL
WITH PLATINUM
NANOMATERIALS –
COATED GAS DIFFUSION
LAYER
RICHARD C. MONSERRAT,
Gil Nonato C. Santos
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What we are doing right now
• Characterize the other properties of Nanomaterials
• Understand the growth behavior and characteristics of
Nanomaterials
• Device Fabrication of Nanomaterials
• Environmental Nanomaterial Sensors (Challenge• Environmental Nanomaterial Sensors (Challenge
Grant Recipient)
• Solar Nanomaterials (AKI Project)
• Bio Nanomaterials (Interdisciplinary Research –for
funding)
• Nanocoatings (DOST PCIEERD)
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Fabrication and
Characterization of
SnO2 Nanomaterials
for AntiHeat and Anti
Microbial Applications
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Francisco V. Moreno Jr., Gil Nonato Santos
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Solid State Physics
SEM/EDX Facility
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Solid State Physics Thermal and
Electrical Characterization Facility
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Solid State Physics High Vacuum
System and LN2 Facility
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Solid State Physics
High Temperature Furnace
and XRD Facility
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Solid State Physics Fabrication Lab
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Solid State Physics
Optical Characterization Facility
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