effect of the aluminum source on the formation of yttrium aluminum garnet (yag) powder via solid...

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Effect of the aluminum source on the formation of yttrium aluminum garnet (YAG) powder via solid state reaction Reporter : Che-Wei Kuo Adviser : Ming-Shyong Tsai Date : 2011/010/26 1

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In this research, the author try to improve the diffusion of Al 3+ in Y 2 O 3 lattice. So the author uses different aluminum sources, such as α-Al 2 O 3 、 θ-Al 2 O 3 、 γ-Al 2 O 3 and boehmite to produce YAG powders by solid state reaction method. Other methods of synthesizing YAG powders, such as : Hydrothermal synthesis method Co-precipitation method Spray pyrolysis method Sol–gel method Methods of producing YAG powders 3

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Page 1: Effect of the aluminum source on the formation of yttrium aluminum garnet (YAG) powder via solid state reaction Reporter : Che-Wei Kuo Adviser : Ming-Shyong

Effect of the aluminum source on the formation of yttrium aluminum garnet (YAG) powder via solid state reaction

Reporter : Che-Wei KuoAdviser : Ming-Shyong Tsai

Date : 2011/010/261

Page 3: Effect of the aluminum source on the formation of yttrium aluminum garnet (YAG) powder via solid state reaction Reporter : Che-Wei Kuo Adviser : Ming-Shyong

In this research, the author try to improve the diffusion of Al3+ in Y2O3 lattice. So the author uses different aluminum sources, such as α-Al2O3 、 θ-Al2O3 、 γ-Al2O3

and boehmite to produce YAG powders by solid state reaction method.

Other methods of synthesizing YAG powders , such as :• Hydrothermal synthesis method• Co-precipitation method• Spray pyrolysis method• Sol–gel method

Methods of producing YAG powders

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Page 4: Effect of the aluminum source on the formation of yttrium aluminum garnet (YAG) powder via solid state reaction Reporter : Che-Wei Kuo Adviser : Ming-Shyong

Pure YAG powder can be formed successfully and easily by using boehmite as the aluminum source and calcining at 1500 ◦C for 5 h.

The composition diffusion occurs before the phase formation of YAG. The grain growth of Y2O3 and α-Al2O3 are effectively suppressed in this case.

The Y2O3 is decomposed by the diffusion of boehmite that can be observed from the TEM morphology.

Conclusions

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