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    ABSTRACT

    This paper describes the application of two relatively new diagnostic

    techniques for the determination of insulation condition in aged transformers. The

    techniques are (a) measurements of interfacial polarization spectra by a DC method

    and (b) measurements of molecular weight and its distribution by gel permeation

    chromatography. Several other electrical properties of the cellulose polymer were

    also investigated. Samples were obtained from a retired power transformer and

    they were analysed by the developed techniques. Six distribution transformers

    were also tested with the interfacial polarization spectra measurement technique,

    and the molecular weight of paper/pressboard samples from these transformers

    were also measured by the gel permeation chromatography. The variation of the

    results through different locations in a power transformer is discussed in this paper.

    The possible correlation between different measured properties was investigated

    and discussed in this paper.

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    1. INTRODUCTION

    The main function of a power system is to supply electrical energy to its

    customers with an acceptable degree of reliability and quality. Among many other

    things, the reliability of a power system depends on trouble free transformer

    operation. Now, in the electricity utilities around the world, a significant number of

    power transformers are operating beyond their design life. Most of these

    transformers are operating without evidence of distress. The same situation is

    evident in Australia. In PowaaerLink Queensland (PLQ), 25% of the power

    transformers were more than 25 years old in 1991. So priority attention should be

    directed to research into improved diagnostic techniques for determining the

    condition of the insulation in aged transformers.

    The insulation system in a power transformer consists of cellulosic

    materials (paper, pressboard and transformerboard) and processed mineral oil. The

    cellulosic materials and oil insulation used in transformer degrade with time. The

    degradation depends on thermal, oxidative, hydrolytic, electrical and mechanical

    conditions which the transformer experienced during its lifetime.

    The condition of the paper and pressboard insulation has been monitored by

    (a) bulk measurements (dissolved gas analysis (DGA) insulation resistance (IR),

    tan and furans and (b) measurements on samples removed from the transformer

    (degree of polymerization (DP) tensile strength). At the interface between the

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    paper and oil in the transformer, interfacial polarization may occur, resulting in an

    increase in the loss tangent and dielectric loss. A DC method was developed for

    measuring the interfacial polarization spectrum for the determination of insulation

    condition in aged transformers.

    This paper makes contributions to the determination of the insulation

    condition of transformers by bulk measurements and measurements on samples

    removed from the transformer. It is based on a University of Queensland research

    project conducted with cooperation from the PLQ and the GEC-Alsthom.

    Most of the currently used techniques have some drawbacks. Dissolved gas

    analysis requires a data bank based on experimental results from failed

    transformers for predicting the fault type. When transformer oil is rep or

    refurbished, the analysis of furans in the refurbished oil may not show any trace of

    degradation, although the cellulose may have degraded significantly. DP

    estimation is based on a single-point viscosity measurement. Molecular weight

    studies by single-point viscosity measurements are of limited value when dealing

    with a complex polymer blend, such as Kraft paper, particularly in cases where the

    molecular weight distribution of the paper changes significantly as the degradation

    proceeds. In these instances, a new technique, gel permeation chromatography

    (GPC), is likely to be more useful than the viscosity method, because it provides

    information about the change in molecular weight and molecular weight

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    distribution. Investigation of the GPO technique has been included in this research

    to assess its effectiveness in determining the condition of insulation.

    Conventional electrical properties (dissipation factor and breakdown

    strengths) of cellulosic materials are not significantly affected by ageing .so very

    little recent research has been directed to electrical diagnostic techniques, in this

    research project, thorough investigations were also undertaken of the conventional

    electrical properties, along with interfacial polarization parameters of the cellulosic

    insulation materials. The interfacial phenomena are strongly influenced by

    insulation degradation products, such as polar functionalities, water etc. The

    condition of the dielectric and its degradation due to ageing can be monitored by

    studying the rate and process of polarization and can be studied using a DC field.

    Furthermore, this is a non-destructive diagnostic test.

    A retired power transformer (25 MVA, l1/132 kV) and several distribution

    transformers were used for the experimental work. The results from these

    transformers will be presented and an attempt will be made to correlate the

    electrical and chemical test results. The variation of the results through the

    different locations in a power transformer will be discussed with reference to their

    thermal stress distribution. Accelerated ageing experiments were conducted to

    predict the long term insulation behaviour and the results are presented in the

    accompanying paper.

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    2. EXPERIMENTAL TECHNIQUES

    Experimental techniques used for the assessment of insulation condition in

    aged transformers are described in the following section.

    2.1 Conventional Electrical Tests

    The dissipation factor and capacitance were measured at 50 Hz using a

    Schering bridge. The partial discharge inception voltage was measured by a partial

    discharge detector using a circuit with an input unit in series with the test sample.

    Power frequency breakdown strength was measured by using the step by step

    method. The standard wave shape of l. was used for determining the negative

    lightning impulse breakdown strength. The electrical tests were carried out in

    accordance with relevant ASTM standards.

    2.2 Interfacial Polarization Spectra (IPS) Measurements

    When a direct voltage is applied to a dielectric for a long period of time,

    and it is then short circuited for a short period, after opening the short circuit, the

    charge bounded by the polarization will turn into free charges i.e, a voltage will

    build up between the electrodes on the dielectric. This phenomena is called the

    return voltage. After applying the field for a time t, the polarization is expressed by

    P(t) = P0 F(t), where P0 = E is the steady state value of the polarization, a is a

    proportionality factor between the polarization and the field strength (E), called the

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    polarizabiity, F(t) is the relaxation function of the polarization describing the

    development of polarization in time and P is the bound charge density.

    After opening the short circuit, the charge bound by the polarization will

    turn into free charge, and a voltage will build up. So an increase in the polarization

    due to bound charges will increase the voltage build up. Again, polarizabiity will

    increase when polarization increases. So the maximum return voltage can be

    correlated with the polarizability of the material.

    With the development of polarization, the charge bounded on the electrodes

    tends to grow. In the external circuit maintaining the field, this growth will cause

    an absorption current given by Ja(t) = P(t) = d/dt P (t). With polarization

    approaching a steady state value, the current decays in time to zero. As for

    polarization, the absorption current is proportional to the field strength. So the

    initial value can be written as Ja (0) = E, where is the proportionality factor

    between absorption cur rent and field strength, and is called polarization

    conductivity. It can be shown that the initial slope of the return voltage is

    proportional to the polarization conductivity [10]. When the return voltage

    approaches its maximum value quickly, the initial slope of the return voltage is

    larger. Another parameter termed as central time constant, i.e. the time at which

    the return voltage is maximum, is also dependent on the polarization conductivity.

    Hence the fundamental characteristics of the dielectric can be measured by return

    voltage measurements.

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    Figure 1: A typical return voltage wave shape of a specimen from the retired

    transformer

    An experimental set up with an IBM PC and a programmable electrometer

    (Keithley 617 model) was developed and implemented to measure the return

    voltage of a two terminal dielectric system. The charging voltage was 100 volt DC

    for the retired transformer insulation samples. The developed software was used to

    control the electrometer. Adsorbed moisture and temperature of the oil-paper

    insulation adversely affects the re turn voltage measurement. So the return voltage

    measurement was always conducted at a known and low oil-paper moisture content

    and at ambient environmental conditions (20 25 C).

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    A typical return voltage wave shape of a specimen from the retired

    transformer is shown in Fig. 1. The relevant parameters (maximum return voltage,

    initial slope and central time constant) are identified in Fig. 1. Initial slope is the

    slope of the return voltage graph (with linear approximation) for first few seconds.

    As interfacial polarization is predominant at longer time constants, the spectrum of

    the return voltage was investigated by changing the charging and discharging time

    over a range of times greater than 1 second until the peak value of the maximum

    return voltage was obtained The ratio of charging and discharging time was

    two.then the spectra of maximum return voltage and initial slope were plotted

    versus the central time constant (the time at which the return voltage is maximum).

    The peak value of the maximum return voltage (from the return voltage spectrum)

    and the corresponding initial slope (from the initial slope spectrum), along With

    central time constant (from either of the spectrum), are the parameters used to

    assess the insulation condition from the return voltage measurements.

    2.3 GPC Analysis

    Gel permeation chromatography provides a detailed molecular weight

    distribution of the polymer. GPC is a chromatographic technique which uses

    highly porous, non-ionic gel beads for the separation of polydispersed polymers in

    solution. GPC separates polymer molecules on the basis of their hydrodynamic

    volume. Detailed information of GPC technique is presented elsewhere [7].

    Cellulose is not soluble in any common GPC solvents. Hence, for GPC

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    measurements the cellulosic materials had to be derivatized to enhance their

    solubility in these solvents. For this purpose, a cellulose tricarbanilate derivative

    was prepared by the method of Evans et al. .

    The molecular weight distribution of the cellulose tricarbanilate was

    measured using a Waters Chromatograph equipped with a variable wavelength

    tunable absorbance detector. Four ultrastyragel columns were used in series in the

    Chromatograph, with tetrahydrofuran (THF) as the eluent. Detection was carried

    out using the absorbance at 236 nm and the elution profile was acquired by

    interfacing to an IBM computer. The elution profiles were converted to molecular

    weight distributions using a calibration based upon narrow molecular weight

    distribution polystyrene standards.

    3. RESULTS AND DISCUSSIONS

    Paper wrapped insulated conductor specimens 200 mm long and pressboard

    samples of dimension 80*80 mm were collected from an aged power transformer.

    Several distribution transformers were also tested.

    3.1 Case Study 1: Kareeya Transformer

    A 25 year old, 25 MVA, 132/11 kV transformer from Kareeya power

    station, North Queensland, had been gassing for some years. This transformer was

    dismantled and was used to investigate the quality of the insulation using electrical

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    and chemical testing techniques, Since the aged transformer had been exposed to

    air after dismantling, the samples had to be processed. The moisture content of

    processed samples varied in the range 0.5 to 1.3%.

    From our discussions with the experts from the GEC-Alsthom, it was

    revealed that the top coils are subjected to higher thermal stress than the bottom

    ones. To examine the differences that exist between the high stress and low stress

    insulation samples, the samples were collected from top, middle and bottom coils

    of low voltage and high voltage windings of the transformer. The schematic

    diagram of a low voltage winding is shown in Fig. 2.

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    Figure 2: Schematic diagram of one phase of LV winding of 25 MVA Kareeya

    transformer

    There were 90 coils/phase and 18 turns or layers of conductor/coil in the

    low voltage winding. There were 10 conductors in parallel in the low voltage

    winding. There were 60 coils/phase and 19 turns or layers of conductors/coil in the

    high voltage winding. The HV and LV conductors were of rectangular cross

    section 13.9 and 12 mm wide respectively and 2.6 mm thick with rounded corners.

    The test specimens for insulated conductor samples were made up by placing two

    samples side by side in a Perspex assembly, so that they overlapped each other for

    a length of 100 mm. With two insulated conductors placed side by side to form the

    specimen, the thickness of paper insulation between them was 1.0 mm and 0.8 mm

    for the HV and LV specimens respectively. Pressboard (of 0.2 mm thickness)

    samples were collected from the main bulk insulation between the high voltage and

    low voltage windings.

    Table 1: Results of conventional electrical tests on samples from LV A phase

    winding of Kareeya transformer

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    3.1.1 Conventional Electrical Test Results

    To obtain an understanding of the effects of varying stresses along complete

    windings, samples were taken from various locations of the LV A and HV B phase

    windings and were tested. Two sizes of new (unaged) paper wrapped conductors

    (New1 and New2) and new pressboard samples of similar composition and

    thickness were obtained from the transformer manufacturer GEC-Alsthom.

    Conventional electrical test results on paper wrapped insulated conductor

    specimens from the LV A phase and HV B phase windings are presented in Tables

    1 and 2 respectively.

    In LV A phase, coils 1,2/44,45/89,90 are from top/middle/ bottom locations

    respectively and layers 1,2/18 are from outer and inner locations. For each of the

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    samples at least two samples were tested and average was taken. The partial

    discharge inception stresses were usually very close to the power frequency

    dielectric strength, and hence these results are not presented. In HV B phase, coils

    1/29,30/59,60 are the top/middle /bottom locations and layers 1/12/19 are the

    outer/medium/ inner locations.

    The following comparison can be made between the results of the aged

    insulation samples and those of the new insulation.

    1. The average dissipation factor of LV A phase samples is 0.017 and that of

    the New1 (similar to LVA phase) sample is 0.008. The average dissipation

    factor of HV B phase samples is 0.015 and that of the New2 (similar to HV B

    phase) sample is 0.009. The dissipation factor of aged samples is significantly

    different from that of new insulation.

    2. The average power frequency dielectric strength of the LVA phase samples

    is 48.4 kVp/mm (with a SD= 3.16) and that of the New1 sample is 50.0

    kVp/mm. The average power frequency dielectric strength of the HV B phase

    samples is 41.6 kVp/mm (with a SD=3.5) and that of the New2 samples is 45.0

    kVp/mm. The difference between the average value of the power frequency

    breakdown strength of the LV A phase and the new samples is not significant,

    whereas the variation of the HV B phase samples is 7.5% lower than the

    corresponding new samples.

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    3. The average lightning impulse breakdown strength of the LV A phase

    samples is 77.0 kVp/mm (with a SD=7) and that of the New! samples is 81

    kVp/mm. The average lightning impulse strength of the HV B phase is 68.5

    kV/mm (with a SD=8.1) and that of the New2 samples is 84 kVp/mm. Again

    the variation is not very significant for the LV A phase samples. The LI

    strength of HV B phase sample is about 18% lower than the corresponding new

    sample strength.

    Table 2: Results of conventional electrical tests on samples from HV B phase of

    Kareeya transformer.

    3.1.2 Interfacial Polarization Spectra Results

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    The same aged insulation specimens from LV A and HV B phase and

    unaged insulation samples (New1and New2) were tested using interfacial

    polarization spectra (IPS) measurements. The results from the IPS measurements

    are presented in Tables 3 and 4.

    In Table 3 all the samples from the aged transformer show large peak

    maximum voltages, short central time constants and large initial slopes by

    comparison with the values for new samples. There are significant variations

    between the aged samples from different locations. For example, we see the

    maximum return voltage of top coil 1-1 (1st coil from top, 1st outside layer)

    reached its peak at 31 s, whereas 89-1 reached its peak value at 75 s, which is more

    than twice the time constant of 1-1. The dissipation factor for sample 1-1 is fifty

    percent larger than the 89-1 sample (Table 1). It is also observed that 45-1, 45-18,

    90-2 and 90-18 samples have maximum return voltages at very small (low) central

    time constants and large values of initial slope and dissipation factor. The variation

    of insulation status between top, middle and bottom coils of LV A phase, observed

    from the conventional tests is consistent with the data from IPS measurements. It

    suggests that degradation due to ageing is characterised by higher dissipation factor

    and consistent changes in IPS e.g. higher return voltage and initial slope, and low

    central time constant.

    Table 3: Results of IPS measurements on samples from LV A phase winding of

    Kareeya transformer

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    Table 4: Results of IPS measurements on samples from HV B phase winding of

    Kareeya transformer

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    In Table 4 for HV B phase, the peak maximum values of return voltage are

    somewhat lower than for the LV A phase. The variation of the peak maximum

    return voltage for the HV B phase is not as significant as LV A phase by

    comparison with the corresponding new samples. For example, the mean of the

    peak maximum return voltage of LV A phase is 3.2 volt and that for the

    New1sample is 1.6 volt, whereas, the mean of the peak maximum return voltage of

    HV B phase is 2.0 volt and that for the New2 sample is 1.8 volt. There are large

    variations in central time constant. Again, all but one (29-12) of the samples from

    the aged transformer show lower central time constant and larger initial slope by

    comparison with the new samples. The maximum return voltage of 1-12 reached

    its peak value at 43 s, where as 1-1 and 1-19 reached their peak values at 94 s. The

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    dissipation factor for sample 1-12 is at least fifty percent larger than that for the 1-1

    and 1-19 samples. This again illustrates consistency between dissipation factor and

    IPS characteristics. Also, for HV B phase samples, it was found that the condition

    of the insulation varies even between the layers. It is generally correct to say that

    whenever samples have peak values of maximum return voltage with a fast (low)

    central time constant, the associated values of the initial slope and dissipation

    factor are large. This is illustrated by the examples of samples 60-1, 60-12, 60-19

    and samples 29-1, 29-12, 29-19 (29-12 has already been mentioned as an

    exception, but even this sample demonstrates the link between better dissipation

    factor and better IPS characteristics). Although there are significant differences

    of insulation characteristics between top, middle and bottom coils, it is not possible

    to draw any conclusion about the trend of variation of insulation status between the

    coil locations.

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    3.1.3 GPC Test Results

    Figure 3: GPC chromatogram of insulating paper samples obtained from new stock

    and aged transformer

    The GPC chromatograms of typical new and aged (from Kareeya

    transformer insulation papers) cellulose are shown in Fig.3. The chromatogram of

    new paper shows the presence of two components. The major component at lower

    elution volume, high molecular weight, is due to cellulose, while the smaller, lower

    molecular weight component is due to hemi-cellulose. The peak molecular weight

    of the cellulose is 1.5 * 106 g/mol, while that of the hemi-cellulose is 5.8 * 104

    g/mol.

    The chromatogram of the cellulose paper taken from the aged transformer

    shows that the molecular weight of the cellulose component has decreased

    significantly, with the peak molecular weight falling to approximately 2 * 10

    5

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    g/mol. The molecular weight distribution of the cellulose has also broadened

    considerably, and the peak due to the hemi-cellulose has become barely

    discernible, suggesting that the hemi-cellulose component of the paper may have

    been largely degraded.

    In order to obtain an understanding of the nature of the reduction in the

    molecular weight of the paper, separate studies were made on the effects of

    accelerated ageing on paper and cotton linter (which only contains cellulose).the

    results enabled the chromatograms of the new and aged insulation samples to be

    simulated by combinations of components.

    The simulated chromatograms of the new paper are shown in Fig. 4. The x

    axis and y axis of Fig. 4 are in elution volume (ml) and in absorbance respectively

    (similar to fig.3). This profile can be simulated reasonably well by a combination

    of three components with three peaks, using the computer program peakfit and

    an exponential Gaussian function to simulate the peak shape. Of the three

    components used, two may be attributed to the cellulose component of the paper,

    and the third may be attributed to the hemi-cellulose component. The molecular

    weight at the peaks were calculated by employing the universal calibration

    procedure to correct the polystyrene calibration curve. Similar simulations were

    made for the transformer aged insulations, and the results of some selected samples

    have been summarised in Tables 5 and 6.

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    Table 5: Results from GPC analysis on samples from LV A phase of Kareeya

    transformer

    Figure 4: The simulation chromatogram of the new insulating paper

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    In Tables 5 and 6, the molecular weights of the peaks P1 and P2 of the

    insulating paper in the LV A phase and in the HV B phase of the transformer fall to

    about one half to one third of the molecular weights at the corresponding peaks for

    P1 and P2 of new insulating paper. A comparison between the LV A phase and the

    HV B phase papers indicates that the largest change in molecular weight occurs in

    the outermost layers (1-1,45-1,89-1) of the LV A phase conductors. The paper near

    the top of the transformer, where the temperature is greatest, shows the greatest

    decrease in molecular weight.

    3.1.4 Results From Pressboard Samples

    The conventional electrical test results of new pressboard and pressboard

    collected from Kareeya transformer are presented in Table 7. Unequal electrodes

    (ASTM D 149) were used for these tests.

    The results show that the dissipation factor of aged transformer pressboard

    is much higher than that for new pressboard samples. The power frequency

    breakdown strength for aged transformer pressboard is reduced by 29.7% from that

    of new unaged pressboard. The lightning impulse breakdown strength of aged

    pressboard is reduced by 14.3 %.

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    Table 6: Results from GPC analysis on samples from HV B phase of Kareeya

    transformer

    Table 7: Results obtained from aged and new press board: Unequal Electrodes

    (ASTM D 149)

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    The IPS results are shown in Table 8. The maximum return voltage of aged

    pressboard from the Kareeya transformer reached its peak value at 21 s, whereas

    the new pressboard sample reached its peak value after 360 s. The value of the

    peak maximum return voltage and initial slope of aged pressboard are also much

    larger than those of the new pressboard. Again, these findings are consistent with

    those presented earlier for pa per insulation. So, from both the conventional

    electrical tests and IPS measurements, it can be concluded that, the degradation of

    pressboard in the Kareeya transformer was much more severe than for the paper

    insulation.

    The GPC technique was applied to new pressboard samples and samples

    from the Kareeya transformer. The chromatograms were analysed in a similar way

    to that described previously. The results are summarised in Table 9. The reduction

    in the molecular weights of peak I and 2 for old pressboard relative to that of new

    pressboard shows the deterioration in the condition of the insulation. However, in

    contrast to what was observed for paper insulation, there was little change in the

    molecular weight of peak 3 (P3) for pressboard.

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    Table 8: Results of IPS measurements on new and aged pressboard samples

    Table 9: GPC Results obtained from aged and new pressboard Sample

    Figure 5: Peak molecular weight versus the central time constants for different

    samples of Kareeya transformer

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    3.1.6 Correlation Between Methods

    Attention has already been drawn to the consistency in changes to electrical

    (dissipation factor and IPS data) and chemical(peak molecular weight data)

    properties caused by ageing induced degradation. The results are now re-examined

    more closely to determine the level of consistency between the electrical and

    chemical test methods. Coil 1-1from LV A phase(Table 3 ) shows that the peak

    maximum return voltage is attained with a fast (short) central time constant, it has

    a large initial slope and its peak molecular weights P1 and P2 (Table 5) are both

    very low. So the same conclusion can be drawn from both the tests; that the

    insulation has been severely degraded by ageing, and sample 1-1 is one of the most

    degraded samples. Similar conclusions can be drawn for the samples 45-1 and 45-

    18. Sample 44-18 shows peak maximum return voltage at a larger central time

    constant, and as expected this is associated with a larger molecular weight. To

    examine the extent of correlation between the electrical and chemical properties,

    peak molecular weights P1 of the LV A phase and HV B phase specimens are

    plotted against central time constants and initial slopes of the return voltages.

    Although there were a few outlying points in both the graphs, Fig. 5 shows that the

    decrease in the peak molecular weight corresponds to a decrease (fast) in the

    central time constant and Fig. 6 shows that a decrease in the peak molecular weight

    corresponds to an increase in the initial slopes.

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    To test the statistical independence of the measured parameters, rank

    correlation coefficients [4] were calculated for both the cases (with all data points

    and with outlying omitted data points). These values are shown in Table 10.

    Critical values of the rank correlation coefficients for two sided test with

    significance level = 0.05 [4] are also shown in the Table 10. If the observed

    value of the rank correlation coefficient is greater than the critical rank correlation

    coefficient, then the statistical independence between the tested parameter is

    rejected. With omitted outlying data points both graphs show good linear

    correlations (with correlation coefficients greater than 0.9). At the same time their

    rank correlation coefficients are also greater than the corresponding critical

    correlation coefficients. When all the data points are considered, Fig. 6 show linear

    correlation with correlation coefficients greater than 0.5. With all the data points,

    the observed rank correlation coefficient is greater than the critical rank correlation

    coefficient for the data points in Fig. 6. Although the test programme was

    necessarily limited, a good trend has been emerged between the IPS parameters

    and the chemical test results.

    Table 10: Results of correlation coefficients from the correlation Figs. 5 and 6

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    Figure 6: Peak molecular weight versus the initial slopes for different samples of

    Kareeya transformer

    3.2 case study 2:distribution transformers

    3.2.1 Conventional E1ectrical Tests Results

    Six distribution transformers were provided by electricity distribution

    authorities. The dissipation factors of these transformers were measured by the

    Schering bridge. For a single phase transformer, the shorted low voltage winding

    was connected to the lower voltage arm of the Schering bridge, and shorted high

    voltage winding was connected to the high voltage supply. For a three phase

    transformer, three phases in the LV winding were short circuited and connected to

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    the lower voltage arm of the Schering bridge and three phases in the HV winding

    were short circuited and connected to the high voltage supply. Dissipation factors

    were measured at two different voltages and the average was determined. This

    arrangement measures the dissipation factor of the bulk insulation (insulation

    between HV and LV windings) of the transformers. Results from the Schering

    bridge measurements are shown in Table 11. Dissipation factors varied from 0.003

    to 0.067 for single phase transformers and 0.006 to 0.081 for three phase

    transformers. Transformers TI, T3 and T6 show high dissipation factors compared

    to the other transformers.

    3.2.2 Interfacial Polarization Test Results

    All the six distribution transformers were tested for IPS measurements. The

    charging voltage was 1000 volt DC and the procedure was similar to that followed

    for the specimens made

    Table 11: Results of Dissipation factors and capacitances of distribution

    transformers

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    Table 12: Results of IPS measurements of the single phase distribution

    transformers

    with two paper wrapped insulated conductors. The connection arrangements

    of the transformers (two terminal dielectric) were the same as those used for

    dissipation factor measurements. In this case, the bulk insulation between HV and

    LV was tested.

    From Tables 12 and 13, it is observed that the initial slopes and central time

    constants vary significantly between the trans formers. The variation of the peak

    maximum return voltage did not follow any specific trend. Some form of

    normalisation may be necessary to compare different peak maximum values, when

    the transformers are of different insulation resistances and capacitances. In general,

    higher initial slopes are associated with shorter central time constants, and this is

    consistent with previously presented results. Transformers with these

    characteristics also tend to have large dissipation factors. For example, transformer

    T1 and T3 show larger dissipation factors and higher initial slopes and lower

    central time constants than the transformer T2. The oldest transformer of the three

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    phase trans formers, T6 shows high dissipation factor, high initial slope and low

    central time constant compared to the corresponding values for the transformers T4

    and T5. Thus, a good correlation exists between initial slope, central time constant

    and dissipation factor.

    3.2.3 GPC Test Results

    Several paper and pressboard samples were taken from the distribution

    transformers (T1, T2, T3 and T5) for the GPC analysis. The results are shown in

    Table 14. From the Tables 11 and

    Table 13: Results of IPS measurements of the three phase distribution transformers

    Table 14: GPC Results of cellulose samples from distribution transformers

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    13, it is observed that the transformer T5 has a very low dissipation factor

    with a low peak maximum return voltage, initial slope and large central time

    constant. From Table 14, both paper and pressboard samples from T5 show high

    peak molecular weight P1, close to that of new paper. From both the electrical and

    chemical tests, it is evident that insulation of T5 is in very good condition. Both

    paper and pressboard samples from T1 and T3 show a large reduction in peak

    molecular weights compared to new ones. From Tables 11 and 12, it is observed

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    that the transformer T1 and T3 have high dissipation factors with large initial

    slopes and low central time constants compared to the transformer T2. A good

    correlation is observed between the IPS parameters, dissipation factor and the GPC

    results from the limited number of samples analysed from the distribution

    transformers. The important point is that this finding is consistent with similar

    findings for the aged power transformer, and as can be seen in the adjunct paper

    with the results for artificially aged paper [12].

    4 CONCLUSIONS

    Conventional electrical tests and IPS measurements were applied to

    insulated conductors and pressboard samples collected from a retired power

    transformer. The molecular weights of the samples were also studied by GPC

    analysis. Significant differences in the condition of the insulation have been ob

    served throughout different locations within the Kareeya transformer. The

    electrical test results (in particular dissipation factor and the IPS parameters) on the

    Kareeya transformer insulation specimens were found to be consistent with the

    GPC results. A good correlation has been observed between the electrical test

    results and GPC analysis for detecting changes in the properties of the insulation

    samples. The condition of aged pressboard from the Kareeya transformer has been

    found to be significantly deteriorated compared to new pressboard. This was also

    evident from both the electrical and chemical teat results.

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    Several distribution transformers were also studied, Dissipation factors and

    IPS measurements showed a good consistency in explaining the condition of

    insulation in distribution transformers. GPC results from the distribution

    transformers also correlated well with the dissipation factor and IPS parameters.

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