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Essential Oils GC-MS Test Results Conducted by the Aromatic Plant Research Center (APRC) May 2019 COMPANY CODES LAVENDER PEPPERMINT TEA TREE doTERRA 1A 1B 1C Young Living 2A 2B 2C Mountain Rose Herbs 3A 3B 3C Plant Therapy 4A 4B 4C Améo Zija 5A 5B 5C Aromatics International 6A 6B 6C Edens Garden 7A 7B 7C Aura Cacia 8A 8B 8C NOW 9A 9B 9C Rocky Mountain Oils 10A 10B 10C Artisan Aromatics 11A 11B 11C

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Essential Oils GC-MS Test Results Conducted by the Aromatic Plant Research Center (APRC)

May 2019 COMPANY CODES LAVENDER PEPPERMINT TEA TREE doTERRA 1A 1B 1C Young Living 2A 2B 2C Mountain Rose Herbs 3A 3B 3C Plant Therapy 4A 4B 4C Améo Zija 5A 5B 5C Aromatics International 6A 6B 6C Edens Garden 7A 7B 7C Aura Cacia 8A 8B 8C NOW 9A 9B 9C Rocky Mountain Oils 10A 10B 10C Artisan Aromatics 11A 11B 11C

LAVENDER 1A to 11A

Peak Report TIC R.Time Name Area%

8.451 Hexane, 1-methoxy- 0.12 10.165 Hexanol<n-> 0.06 13.130 Thujene <alpha-> 0.12 13.572 Pinene <alpha> 0.22 14.530 Camphene 0.15 15.831 Sabinene 0.04 16.151 1-Octen-3-ol 0.38 16.497 3-Octanone 0.98 16.771 Myrcene 0.67 17.127 Butyl butanoate 0.12 17.204 3-Octanol 0.21 17.900 Phellandrene <alpha-> 0.04 18.051 Carene<delta-3-> 0.25 18.156 Hexyl acetate 0.61 18.574 Terpienene <alpha> 0.05 18.729 Cymene<ortho-> 0.05 19.070 Cymene<para-> 0.20 19.376 Limonene 0.43 19.493 Phellandrene <beta> 0.31 19.587 1,8-cineole 1.08 19.780 Ocimene <Z-beta> 4.99 20.464 Ocimene <E-beta> 2.20 21.283 Terpinene <gamma> 0.16 22.108 Linalool oxide <cis-(furanoid)> 0.26 23.135 Terpinolene 0.11 23.200 Linalool oxide <trans> (furanoid) 0.13 24.329 Linalool 32.57 24.431 Propionate hexyl + Hotrienol 0.14 24.608 Octen-3-yl acetate<1> 1.22 25.422 Octanol acetate<3-> 0.10 26.053 Ocimene <allo> 0.18 27.375 Hexyl isobutanoate 0.05 27.465 Camphor 0.16 28.543 Lavandulol 1.22 29.204 Borneol 0.74 29.829 Terpinen-4-ol 4.25 30.193 Cryptone 0.22 30.474 Hexyl butanoate 0.52 30.795 Terpineol <alpha> 1.36 32.743 Nerol 0.19 33.528 Hexyl 2-methyl butanoate 0.03 34.035 Cuminal 0.05 34.653 Linalyl acetate 29.26 36.815 Lavandulyl acetate 4.95 36.903 Bornyl acetate 0.10 39.858 Hexyl tiglate 0.02 41.758 Neryl acetate 0.43 43.050 Geranyl acetate 0.78 43.565 Hexyl hexanoate 0.12 43.732 Sesquithujene<7-epi-> 0.06 45.869 Caryophyllene <trans> 3.44 46.643 Bergamotene <trans-alpha> 0.14 47.856 Farnesene<(E)-beta-> 2.72 48.097 Humulene <alpha> 0.10 49.688 Germacrene D 0.39 49.832 Farnesene <alpha-cis-cis-> 0.04 51.628 Amorphene <delta> 0.09 55.758 Caryophyllene oxide 0.35 59.162 Cadinol <epi-alpha> 0.07

100.00

min

5,487,321

10.0 20.0 30.0 40.0 50.0 60.0

TIC

8.4

51

10.1

65

13.1

30

13.5

72

14.5

30

15.8

31 16.1

51

16.4

97

16.7

71

17.1

27

17.2

04

17.9

00

18.0

51 1

8.1

56

18.5

74

18.7

29

19.0

70

19.3

76

19.4

93

19.5

87

19.7

80

20.4

64

21.2

83

22.1

08

23.1

35

23.2

00

24.3

29

24.4

31

24.6

08

25.4

22

26.0

53

27.3

75

27.4

65

28.5

43

29.2

04

29.8

29

30.1

93

30.4

74

30.7

95

32.7

43

33.5

28

34.0

35

34.6

53

36.8

15

36.9

03

39.8

58 41.7

58

43.0

50

43.5

65

43.7

32

45.8

69

46.6

43

47.8

56

48.0

97

49.6

88

49.8

32

51.6

28

55.7

58

59.1

62

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/24/2019 9:10:54 AM Sample Type : Essential Oil Sample Name : Lavender

Company Name : AD Practitioners, LLCLot# : 1A

Injection Volume : 0.30

Comments:

No adulteration or contamination was detected

in Lavender ADP 1A.

Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

Peak Report TIC R.Time Name Area%

8.446 Hexane, 1-methoxy- 0.11 10.156 Hexanol<n-> 0.08 13.124 Thujene <alpha-> 0.07 13.566 Pinene <alpha> 0.16 14.523 Camphene 0.18 15.824 Sabinene 0.03 16.145 1-Octen-3-ol 0.33 16.494 3-Octanone 1.18 16.762 Myrcene 0.48 17.120 Butyl butanoate 0.10 17.197 3-Octanol 0.28 18.044 Carene<delta-3-> 0.10 18.147 Hexyl acetate 0.55 18.717 Cymene <ortho> 0.06 19.054 Cymene<para-> 0.18 19.365 Limonene 0.31 19.484 Phellandrene <beta> 0.22 19.574 1,8-cineole 0.80 19.757 Ocimene <Z-beta> 2.89 20.461 Ocimene <E-beta> 2.25 21.278 Terpinene <gamma> 0.11 22.105 Linalool oxide <cis-(furanoid)> 0.33 23.125 Terpinolene 0.07 23.200 Linalool oxide <trans-(furanoid)> 0.19 24.316 Linalool 29.21 24.418 Propionate hexyl + Hotrienol 0.12 24.599 Octen-3-yl acetate<1> 0.96 25.415 Octanol acetate<3-> 0.13 26.045 Ocimene <allo> 0.09 27.369 Hexyl isobutanoate 0.04 27.464 Camphor 0.37 28.536 Lavandulol 0.88 29.208 Borneol 1.34 29.811 Terpinen-4-ol 3.02 30.187 Cryptone 0.20 30.469 Hexyl butanoate 0.51 30.785 Terpineol <alpha> 1.11 32.746 Nerol 0.13 33.099 Bornyl formate 0.05 33.527 Hexyl 2-methyl butanoate 0.04 34.033 Cuminal 0.03 34.230 Linalool oxide acetate <Z> 0.00 34.690 Linalyl acetate 37.10 35.287 Linalool acetate oxide <E> 0.01 36.796 Lavandulyl acetate 3.36 36.903 Bornyl acetate 0.13 39.852 Hexyl tiglate 0.08 41.753 Neryl acetate 0.36 43.046 Geranyl acetate 0.63 43.560 Hexyl hexanoate 0.15 43.727 Sesquithujene<7-epi-> 0.08 45.387 Bergamotene<alpha-cis-> 0.04 45.879 Caryophyllene <trans> 4.58 46.642 Bergamotene <trans-alpha> 0.20 47.854 Farnesene<(E)-beta-> 2.80 48.094 Humulene <alpha> 0.10 49.682 Germacrene D 0.41 49.828 Farnesene <alpha-cis-cis-> 0.06 49.982 Hydroxy linalyl acetate 0.00 51.621 Amorphene <delta> 0.11 51.898 Isobicyclogermacrene 0.04 55.753 Caryophyllene oxide 0.41 59.163 Cadinol <epi-alpha> 0.07

100.00

min

5,985,409

10.0 20.0 30.0 40.0 50.0 60.0

TIC

8.4

46

10.1

56

13.1

24

13.5

66

14.5

23

15.8

24

16.1

45

16.4

94

16.7

62

17.1

20

17.1

97

18.0

44 1

8.1

47

18.7

17

19.0

54

19.3

65

19.4

84

19.5

74

19.7

57

20.4

61

21.2

78

22.1

05

23.1

25

23.2

00

24.3

16

24.4

18

24.5

99

25.4

15

26.0

45

27.3

69

27.4

64 28.5

36 2

9.2

08

29.8

11

30.1

87

30.4

6930.7

85

32.7

46

33.0

99

33.5

27

34.0

33

34.2

30

34.6

90

35.2

87

36.7

96

36.9

03

39.8

52

41.7

53

43.0

46

43.5

60

43.7

27

45.3

87

45.8

79

46.6

42

47.8

54

48.0

94

49.6

82

49.8

28

49.9

82

51.6

21

51.8

98

55.7

53

59.1

63

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/24/2019 11:08:42 AM Sample Type : Essential Oil Sample Name : Lavender

Company Name : AD Practitioners, LLCLot# : 2A

Injection Volume : 0.30

Comments:

Synthetic markers of Linalyl acetate were detected

in the analysis of Lavender ADP 2A.

This indicated Linalyl acetate has been

added to Lavender ADP 2A.

Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

Peak Report TIC R.Time Name Area%

8.446 Hexane, 1-methoxy- 0.12 10.160 Hexanol<n-> 0.06 13.125 Thujene <alpha-> 0.11 13.566 Pinene <alpha> 0.21 14.525 Camphene 0.19 15.827 Sabinene 0.08 16.147 1-Octen-3-ol 0.35 16.498 3-Octanone 1.32 16.766 Myrcene 0.56 17.125 Butyl butanoate 0.13 17.200 3-Octanol 0.31 17.896 Phellandrene <alpha-> 0.04 18.047 Carene<delta-3-> 0.27 18.151 Hexyl acetate 0.70 18.572 Terpienene <alpha> 0.05 18.722 Cymene<ortho-> 0.08 19.057 Cymene<para-> 0.25 19.371 Limonene 0.46 19.491 Phellandrene <beta> 0.45 19.583 1,8-cineole 1.57 19.765 Ocimene <Z-beta> 3.18 20.464 Ocimene <E-beta> 2.40 21.282 Terpinene <gamma> 0.15 22.105 Linalool oxide <cis-(furanoid)> 0.21 23.131 Terpinolene 0.09 23.197 Linalool oxide <trans-(pyranoid)> 0.08 24.329 Linalool 30.12 24.430 Propionate hexyl + Hotrienol 0.12 24.607 Octen-3-yl acetate<1> 1.14 25.419 Octanol acetate<3-> 0.21 26.049 Ocimene <allo> 0.14 27.370 Hexyl isobutyrate 0.05 27.467 Camphor 0.26 28.535 Lavandulol 0.87 29.203 Borneol 0.89 29.824 Terpinen-4-ol 3.67 30.193 Cryptone 0.31 30.473 Hexyl butanoate 0.57 30.789 Terpineol <alpha> 1.15 32.741 Nerol 0.15 33.103 Bornyl formate 0.05 34.033 Cuminal 0.10 34.669 Linalyl acetate 31.10 36.800 Lavandulyl acetate 3.64 36.901 Bornyl acetate 0.15 41.753 Neryl acetate 0.38 43.047 Geranyl acetate 0.63 43.564 Hexyl hexanoate 0.17 43.732 Sesquithujene<7-epi-> 0.09 45.395 Bergamotene<alpha-cis-> 0.05 45.770 Santalene <alpha> 0.58 45.883 Caryophyllene <trans> 4.40 46.640 Bergamotene <trans-alpha> 0.20 47.866 Farnesene<(E)-beta-> 3.86 48.098 Humulene <alpha> 0.15 49.689 Germacrene D 0.70 49.834 Farnesene <alpha-cis-cis-> 0.07 51.625 Amorphene <delta> 0.18 55.758 Caryophyllene oxide 0.36 59.165 Muurolol <alpha> 0.09

100.00

min

5,543,254

10.0 20.0 30.0 40.0 50.0 60.0

TIC

8.4

46

10.1

60

13.1

25

13.5

66

14.5

25

15.8

27

16.1

47

16.4

98

16.7

66

17.1

25

17.2

00

17.8

96

18.0

47

18.1

51

18.5

72

18.7

22

19.0

57

19.3

71

19.4

91

19.5

83

19.7

65

20.4

64

21.2

82

22.1

05

23.1

31

23.1

97

24.3

29

24.4

30

24.6

07

25.4

19

26.0

49

27.3

70

27.4

67

28.5

35

29.2

03

29.8

24

30.1

93

30.4

7330.7

89

32.7

41

33.1

03

34.0

33

34.6

69

36.8

00

36.9

01

41.7

53

43.0

47

43.5

64

43.7

32

45.3

95

45.7

70

45.8

83

46.6

40

47.8

66

48.0

98 4

9.6

89

49.8

34

51.6

25

55.7

58

59.1

65

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/24/2019 1:06:32 PM Sample Type : Essential Oil Sample Name : Lavender

Company Name : AD Practitioners, LLCLot# : 3A

Injection Volume : 0.30

Comments:

No adulteration or contamination was detected

in Lavender ADP 3A.

Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

Peak Report TIC R.Time Name Area%

8.448 Hexane, 1-methoxy- 0.10 10.161 Hexanol<n-> 0.05 13.127 Thujene <alpha-> 0.10 13.567 Pinene <alpha> 0.18 14.527 Camphene 0.12 15.829 Sabinene 0.04 16.149 1-Octen-3-ol 0.31 16.496 3-Octanone 1.02 16.771 Myrcene 0.57 17.125 Butyl butanoate 0.12 17.202 3-Octanol 0.23 17.897 Phellandrene <alpha-> 0.03 18.048 Carene<delta-3-> 0.18 18.156 Hexyl acetate 0.59 18.576 Terpienene <alpha> 0.04 18.727 Cymene<ortho-> 0.04 19.067 Cymene<para-> 0.16 19.380 Limonene 0.40 19.495 Phellandrene <beta> 0.28 19.589 1,8-cineole 1.26 19.782 Ocimene <Z-beta> 4.19 20.465 Ocimene <E-beta> 2.23 21.283 Terpinene <gamma> 0.16 22.107 Linalool oxide <cis-(furanoid)> 0.22 23.130 Terpinolene 0.13 23.205 Linalool oxide <trans-(pyranoid)> 0.10 24.348 Linalool 31.59 24.443 Propionate hexyl + Hotrienol 0.12 24.611 Octen-3-yl acetate<1> 0.95 25.420 Octanol acetate<3-> 0.11 26.048 Ocimene <allo> 0.20 27.372 Hexyl isobutanoate 0.06 27.464 Camphor 0.20 28.538 Lavandulol 0.85 29.202 Borneol 0.77 29.829 Terpinen-4-ol 3.95 30.192 Cryptone 0.20 30.469 Hexyl butanoate 0.48 30.788 Terpineol <alpha> 1.11 32.745 Nerol 0.13 33.526 Hexyl 2-methyl butanoate 0.03 34.033 Cuminal 0.04 34.213 Linalool oxide acetate <Z> 0.01 34.688 Linalyl acetate 33.35 35.299 Linalool oxide acetate <E> 0.02 36.799 Lavandulyl acetate 3.22 36.903 Bornyl acetate 0.11 39.853 Hexyl tiglate 0.04 41.752 Neryl acetate 0.43 43.047 Geranyl acetate 0.73 43.566 Hexyl hexanoate 0.13 43.730 Sesquithujene<7-epi-> 0.06 45.880 Caryophyllene <trans> 4.24 46.644 Bergamotene <trans-alpha> 0.16 47.859 Farnesene<(E)-beta-> 2.89 48.097 Humulene <alpha> 0.08 49.687 Germacrene D 0.45 49.834 Farnesene <alpha-cis-cis-> 0.04 51.626 Amorphene <delta> 0.12 55.750 Caryophyllene oxide 0.22 59.160 Cadinol <epi-alpha> 0.06

100.00

min

5,929,218

10.0 20.0 30.0 40.0 50.0 60.0

TIC

8.4

48

10.1

61

13.1

27

13.5

67

14.5

27

15.8

29

16.1

49

16.4

96

16.7

71

17.1

25

17.2

02

17.8

97

18.0

48 1

8.1

56

18.5

76

18.7

27

19.0

67

19.3

80

19.4

95

19.5

89

19.7

82

20.4

65

21.2

83

22.1

07

23.1

30

23.2

05

24.3

48

24.4

43

24.6

11

25.4

20

26.0

48

27.3

72

27.4

64

28.5

38

29.2

02

29.8

29

30.1

92

30.4

69

30.7

88

32.7

45

33.5

26

34.0

33

34.2

13

34.6

88

35.2

99

36.7

99

36.9

03

39.8

53 41.7

52

43.0

47

43.5

66

43.7

30

45.8

80

46.6

44

47.8

59

48.0

97

49.6

87

49.8

34

51.6

26

55.7

50

59.1

60

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/24/2019 3:04:18 PM Sample Type : Essential Oil Sample Name : Lavender

Company Name : AD Practitioners, LLCLot# : 4A

Injection Volume : 0.30

Comments:

Synthetic markers of Linalyl acetate were detected

in the analysis of Lavender ADP 4A.

This indicated Linalyl acetate has been

added to Lavender ADP 4A.

Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

Peak Report TIC R.Time Name Area%

7.739 Hexane, 1-methoxy- 0.19 9.391 Hexanol<n-> 0.07

12.069 Thujene<alpha-> 0.11 12.482 Pinene<alpha-> 0.19 13.403 Camphene 0.12 14.672 Sabinene 0.04 14.979 Pinene<beta-> 0.04 15.059 Octen-3-ol<1-> 0.24 15.399 Octanone<3-> 1.66 15.591 Myrcene 0.58 16.001 Butyl butanoate 0.11 16.069 Octanol<3-> 0.41 16.682 Phellandrene<alpha-> 0.03 16.803 Carene<delta-3-> 0.11 17.004 Hexyl acetate 0.82 17.335 Terpinene<alpha-> 0.05 17.844 Cymene<para-> 0.15 18.116 Limonene 0.38 18.235 Phellandrene <beta> 0.33 18.314 Cineole<1,8-> 0.97 18.509 Ocimene<(Z)-beta-> 2.96 19.193 Ocimene<(E)-beta-> 2.20 20.000 Terpinene<gamma-> 0.16 20.824 Linalool oxide <cis-(furanoid)> 0.21 21.804 Terpinolene 0.09 21.907 Linalool oxide <trans-(furanoid)> 0.11 22.958 Linalool 33.36 23.105 Hotrienol 0.05 23.180 Hexyl propanoate 0.04 23.304 Octen-3-yl acetate<1> 1.07 24.106 Octanol acetate<3-> 0.19 24.725 Ocimene<allo-> 0.13 26.055 Hexyl isobutanoate 0.06 26.158 Camphor 0.19 27.204 Lavandulol 1.04 27.850 Borneol 0.60 28.008 Undecatriene <(3E,5Z)-1,3,5> 0.06 28.458 Terpinen-4-ol 3.97 28.951 Cryptone 0.23 29.142 Hexyl butanoate 0.61 29.471 Terpineol<alpha-> 1.10 31.413 Nerol 0.13 32.162 Hexyl 2-methyl butanoate 0.04 32.781 Cuminal 0.07 33.204 Linalyl acetate 30.43 35.422 Lavandulyl acetate 3.80 40.410 Neryl acetate 0.34 41.706 Geranyl acetate 0.62 42.026 Bourbonene <alpha> 0.04 42.216 Hexyl hexanoate 0.28 43.905 Bergamotene<alpha-cis-> 0.04 44.349 Caryophyllene <trans> 3.96 45.153 Bergamotene<alpha-trans-> 0.13 46.419 Farnesene<(E)-beta-> 4.02 46.606 Humulene <alpha> 0.12 48.211 Germacrene D 0.47 48.360 Farnesene <alpha-cis-cis-> 0.05 50.178 Amorphene <delta> 0.11 54.316 Caryophyllene oxide 0.28 57.782 Muurolol <alpha> 0.05

100.00

min

4,500,231

10.0 20.0 30.0 40.0 50.0 59.0

TIC

7.7

39

9.3

91

12.0

69

12.4

82

13.4

03

14.6

72

14.9

79

15.0

59

15.3

99

15.5

91

16.0

01

16.0

69

16.6

82

16.8

03

17.0

04

17.3

35

17.8

44

18.1

16

18.2

35 1

8.3

14

18.5

09

19.1

93

20.0

00

20.8

24

21.8

04

21.9

07

22.9

58

23.1

05

23.1

80

23.3

04

24.1

06

24.7

25

26.0

55

26.1

58

27.2

04

27.8

50

28.0

08

28.4

58

28.9

51

29.1

42

29.4

71

31.4

13

32.1

62

32.7

81

33.2

04

35.4

22

40.4

10

41.7

06

42.0

26

42.2

16

43.9

05

44.3

49

45.1

53

46.4

19

46.6

06

48.2

11

48.3

60

50.1

78

54.3

16

57.7

82

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/24/2019 12:08:14 PM Sample Type : Essential Oil Sample Name : Lavender

Company Name : AD Practitioners, LLCLot# : 5A

Injection Volume : 0.20

Comments:

No adulteration or contamination was detected in

Lavender ADP 5A.

Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

Peak Report TIC R.Time Name Area%

7.876 Hexane, 1-methoxy- 0.08 12.121 Tricyclene 0.02 12.269 Thujene<alpha-> 0.10 12.682 Pinene<alpha-> 0.23 13.597 Camphene 0.16 14.875 Sabinene 0.04 15.177 Pinene<beta-> 0.03 15.259 Octen-3-ol<1-> 0.06 15.561 Octanone<3-> 1.00 15.802 Myrcene 0.82 16.173 Butyl butanoate 0.10 16.285 Octanol <3> 0.03 16.884 Phellandrene<alpha-> 0.03 17.024 Carene<delta-3-> 0.12 17.180 Hexyl acetate 0.60 17.542 Terpinene<alpha-> 0.04 17.711 Cymene<ortho-> 0.04 18.036 Cymene<para-> 0.18 18.330 Limonene 0.42 18.440 Phellandrene <beta> 0.36 18.505 Cineole<1,8-> 0.82 18.743 Ocimene<(Z)-beta-> 5.09 19.418 Ocimene<(E)-beta-> 2.71 20.216 Terpinene<gamma-> 0.15 21.033 Linalool oxide <cis-(furanoid)> 0.13 22.031 Terpinolene 0.09 22.108 Linalool oxide <trans-(pyranoid)> 0.06 23.190 Linalool 29.12 23.355 Hexyl propanoate 0.09 23.513 Octen-3-yl acetate<1-> 1.08 24.322 Octanol acetate<3-> 0.13 24.945 Ocimene<allo-> 0.17 26.281 Camphor 0.24 27.425 Lavandulol 0.53 28.035 Borneol 0.09 28.650 Terpinen-4-ol 4.38 29.064 Cryptone 0.20 29.322 Hexyl butanoate 0.39 29.652 Terpineol<alpha-> 1.45 31.878 Bornyl formate 0.03 32.889 Cumin aldehyde 0.05 33.436 Linalyl acetate 30.83 35.303 Phellandral 0.02 35.623 Lavandulyl acetate 5.58 40.555 Neryl acetate 0.57 41.839 Geranyl acetate 0.99 42.351 Hexyl hexanoate 0.06 42.451 Sesquithujene<7-epi-> 0.09 44.098 Bergamotene<alpha-cis-> 0.05 44.550 Caryophyllene <trans-> 5.23 45.340 Bergamotene<alpha-trans-> 0.16 46.043 Farnesene <Z-beta-> 0.03 46.591 Farnesene<(E)-beta-> 3.82 46.767 Humulene <alpha> 0.14 46.895 Sesquisabinene 0.04 48.366 Germacrene D 0.44 48.521 Farnesene <alpha-cis-cis-> 0.06 50.322 Amorphene <delta> 0.12 54.418 Caryophyllene oxide 0.22 57.908 Cadinol <epi-alpha> 0.07

100.00

min

20,202,908

10.0 20.0 30.0 40.0 50.0 59.0

TIC

7.8

76

12.1

21

12.2

69

12.6

82

13.5

97

14.8

75

15.1

77

15.2

59

15.5

61

15.8

02

16.1

73

16.2

85

16.8

84

17.0

24 17.1

80

17.5

42

17.7

11

18.0

36

18.3

30

18.4

40

18.5

05

18.7

43

19.4

18

20.2

16

21.0

33

22.0

31

22.1

08

23.1

90

23.3

55

23.5

13

24.3

22

24.9

45

26.2

81

27.4

25

28.0

35

28.6

50

29.0

64

29.3

22

29.6

52

31.8

78

32.8

89

33.4

36

35.3

03

35.6

23

40.5

55

41.8

39

42.3

51

42.4

51

44.0

98

44.5

50

45.3

40

46.0

43

46.5

91

46.7

67

46.8

95

48.3

66

48.5

21

50.3

22

54.4

18

57.9

08

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/24/2019 12:31:07 AM Sample Type : Essential Oil Sample Name : Lavender

Company Name : AD Practitioners, LLCLot# : 6A

Injection Volume : 0.30

Comments:

No adulteration or contamination was detected in

Lavender ADP 6A.

Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

Peak Report TIC R.Time Name Area%

7.858 Hexane, 1-methoxy- 0.10 12.256 Thujene <alpha-> 0.07 12.669 Pinene<alpha-> 0.17 13.582 Camphene 0.12 14.862 Sabinene 0.03 15.165 Pinene<beta-> 0.06 15.244 Octen-3-ol<1-> 0.10 15.556 Octanone<3-> 1.67 15.791 Myrcene 0.66 16.158 Butyl butanoate 0.09 16.271 Octanol <3> 0.02 16.721 Pseudolimonene 0.04 16.869 Phellandrene<alpha-> 0.03 17.012 Carene<delta-3-> 0.18 17.166 Hexyl acetate 0.79 17.530 Terpinene<alpha-> 0.03 17.697 Cymene<ortho-> 0.04 18.024 Cymene<para-> 0.14 18.318 Limonene 0.50 18.430 Phellandrene <beta> 0.17 18.495 Cineole<1,8-> 0.77 18.731 Ocimene<(Z)-beta-> 3.98 19.416 Ocimene<(E)-beta-> 3.14 20.204 Terpinene<gamma-> 0.10 20.866 (6Z)-1-ethyl-6-ethylidene-cyclohexene 0.00 21.022 Linalool oxide <cis-> (furanoid) 0.14 22.021 Terpinolene 0.07 22.098 Linalool oxide <trans-(furanoid)> 0.08 23.223 Linalool 29.93 23.348 Propionate hexyl + Hotrienol 0.08 23.514 Octen-3-yl acetate<1-> 1.09 24.317 Octanol acetate<3-> 0.09 24.936 Ocimene<allo-> 0.22 26.236 Hexyl isobutanoate 0.68 27.423 Lavandulol 0.83 28.045 Borneol 0.07 28.216 Undecatriene <(3E,5Z)-1,3,5> 0.08 28.644 Terpinen-4-ol 3.56 29.056 Cryptone 0.16 29.313 Hexyl butanoate 0.39 29.643 Terpineol <alpha-> 0.98 31.870 Bornyl formate 0.03 32.882 Cuminal 0.05 32.995 Linalool oxide acetate <Z> 0.00 33.473 Linalyl acetate 33.80 34.095 Linalool oxide acetate <E> 0.03 34.817 Isopulegyl acetate<neo-> 0.03 35.624 Lavandulyl acetate 5.15 40.548 Neryl acetate 0.43 41.834 Geranyl acetate 0.75 42.337 Hexyl hexanoate 0.49 42.446 Sesquithujene<7-epi-> 0.04 44.094 Bergamotene<alpha-cis-> 0.03 44.549 Caryophyllene <trans> 4.52 45.333 Bergamotene<alpha-trans-> 0.10 46.578 Farnesene<(E)-beta-> 2.16 46.763 Humulene <alpha> 0.09 48.359 Germacrene D 0.36 48.512 Farnesene <alpha-cis-cis-> 0.04 50.317 Amorphene <delta> 0.09 54.413 Caryophyllene oxide 0.28 57.909 Cadinol <epi-alpha> 0.06

min

22,145,664

10.0 20.0 30.0 40.0 50.0 59.0

TIC

7.858

12.256

12.669

13.582

14.862

15.165

15.244

15.556

15.791

16.158

16.271

16.721

16.869

17.01217.166

17.530

17.697

18.024 18.318

18.430 18.495

18.731

19.416

20.204

20.866

21.022

22.021

22.098

23.223

23.348

23.514

24.317

24.936 26.236

27.423

28.045

28.216

28.644

29.056

29.313 29.643

31.870

32.882

32.995

33.473

34.095

34.817

35.624

40.548 41.834

42.337

42.446

44.094

44.549

45.333

46.578

46.763

48.359

48.512

50.317

54.413

57.909

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/23/2019 2:41:54 PM Sample Type : Essential Oil Sample Name : Lavender

Company Name : AD Practitioners, LLCLot# : 7A

Injection Volume : 0.30

Comments:Synthetic markers of Linalyl acetate were detectedin the analysis of Lavender ADP 7A.This indicated Linalyl acetate has beenadded to Lavender ADP 7A.

Copyright © 2018 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

R.Time Name Area% 100.00

Peak Report TIC R.Time Name Area%

7.869 Hexane, 1-methoxy- 0.03 12.254 Thujene<alpha-> 0.01 12.665 Pinene<alpha-> 0.06 13.578 Camphene 0.04 14.857 Sabinene 0.02 15.161 Pinene<beta-> 0.05 15.233 Octen-3-ol<1-> 0.21 15.543 Octanone<3-> 0.30 15.785 Myrcene 0.45 16.150 Butyl butanoate 0.11 17.007 Carene<delta-3-> 0.02 17.170 Hexyl acetate 0.14 18.018 Cymene<para-> 0.11 18.316 Limonene 0.67 18.497 Cineole<1,8-> 1.74 18.712 Ocimene<(Z)-beta-> 1.96 19.395 Ocimene<(E)-beta-> 1.26 20.196 Terpinene<gamma-> 0.20 21.017 Linalool oxide <cis-(furanoid)> 0.18 22.012 Terpinolene 0.19 22.093 Linalool oxide <trans-(pyranoid)> 0.11 23.243 Linalool 32.02 23.370 Hexyl propanoate 0.05 23.516 Octen-3-yl acetate<1-> 0.77 24.935 Ocimene<allo-> 0.12 26.278 Camphor 0.56 27.911 Terpineol <delta> 0.03 28.032 Borneol 0.43 28.651 Terpinen-4-ol 4.05 29.311 Hexyl butanoate 0.09 29.640 Terpineol <alpha-> 0.98 32.332 Hexyl 2-methyl butanoate 0.03 32.768 Hexyl isovalerate 0.27 33.014 Linalool oxide acetate <Z> 0.08 33.508 Linalyl acetate 40.52 34.098 Linalool oxide acetate <E> 0.12 34.985 Plinyl acetate 0.01 35.593 Lavandulyl acetate 2.13 38.655 Hexyl tiglate 0.10 39.610 Peroxylinalyl acetate A 0.03 39.798 Peroxylinalyl acetate B 0.04 40.550 Neryl acetate 1.15 41.839 Geranyl acetate 1.59 42.215 Bourbonene <alpha> 0.02 42.335 Hexyl hexanoate 0.03 42.442 Sesquithujene<7-epi-> 0.06 43.404 Sesquithujene 0.05 44.249 Lavandulyl isobutanoate 0.04 44.551 Caryophyllene <trans> 4.85 45.328 Bergamotene<alpha-trans-> 0.10 45.510 Coumarin 0.13 45.808 Farnesene<(Z)-beta-> 0.03 46.559 Farnesene<(E)-beta-> 0.72 46.756 Humulene <alpha-> 0.05 46.884 Neryl-propanoate 0.06 47.773 Dauca-5,8-diene 0.03 48.350 Germacrene D 0.26 49.590 Lavandulyl isovalerate <ent> 0.19 49.974 Bisabolene <beta-> 0.06 50.312 Amorphene <delta> 0.15 54.405 Caryophyllene oxide 0.12

100.00

min

24,615,028

10.0 20.0 30.0 40.0 50.0 56.0

TIC

7.869

12.254

12.665

13.578

14.857

15.161

15.233

15.543

15.785

16.150

17.007

17.170

18.01818.316

18.497 18.712

19.395

20.196

21.017

22.012

22.093

23.243

23.37023.516

24.935 26.278

27.911 28.032

28.651

29.31129.640

32.332

32.768

33.014

33.508

34.098

34.985

35.593

38.655

39.610

39.798

40.550 41.839

42.215

42.335

42.442

43.404

44.249

44.551

45.328

45.510

45.80846.559

46.756

46.884

47.773

48.350

49.590

49.974

50.312

54.405

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/23/2019 4:37:22 PM Sample Type : Essential Oil Sample Name : Lavender

Company Name : AD Practitioners, LLCLot# : 8A

Injection Volume : 0.30

Comments:TSynthetic markers of Linalyl acetate were detectedin the analysis of Lavender ADP 8A.This indicated Linalyl acetate has beenadded to Lavender ADP 8A.

Copyright © 2018 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

Peak Report TIC R.Time Name Area% 12.250 Thujene <alpha-> 0.03 12.666 Pinene<alpha-> 1.54 13.575 Camphene 0.11 14.852 Sabinene 0.04 15.156 Pinene<beta-> 0.12 15.241 Octen-3-ol<1-> 0.03 15.540 Octanone<3-> 0.32 15.780 Myrcene 0.43 16.163 Butyl butanoate 0.02 17.003 Carene<delta-3-> 0.03 17.170 Hexyl acetate 0.14 18.017 Cymene<para-> 0.06 18.310 Limonene 0.39 18.495 Cineole<1,8-> 2.93 18.698 Ocimene<(Z)-beta-> 1.22 19.387 Ocimene<(E)-beta-> 1.00 20.195 Terpinene<gamma-> 0.06 21.013 Linalool oxide <cis-(furanoid)> 0.17 22.009 Terpinolene 0.12 22.087 Linalool oxide <trans-(furanoid)> 0.19 23.203 Linalool 32.11 23.340 Hexyl propanoate 0.08 23.498 Octen-3-yl acetate<1-> 0.31 24.311 Octanol acetate<3-> 0.03 24.933 Ocimene<allo-> 0.05 26.289 Camphor 2.38 27.909 Terpineol <delta> 0.02 28.028 Borneol 1.58 28.611 Terpinen-4-ol 1.86 29.051 Cryptone 0.08 29.302 Hexyl butanoate 0.32 29.629 Terpineol <alpha-> 0.60 31.695 Linalool acetate<tetrahydro-> 0.01 31.865 Bornyl formate 0.10 32.327 Hexyl 2-methyl butanoate 0.05 32.762 Hexyl isovalerate 0.10 32.999 Linalool oxide acetate <Z> 0.06 33.459 Linalyl acetate 38.79 34.084 Linalool oxide acetate <E> 0.16 34.973 Plinyl acetate 3 0.01 35.576 Lavandulyl acetate 1.57 38.650 Hexyl tiglate 0.13 39.796 Hydroxylinalool B 0.03 40.539 Neryl acetate 0.31 41.682 Copaene <alpha> 0.06 41.826 Geranyl acetate 0.59 42.437 Sesquithujene<7-epi-> 0.05 43.401 Sesquithujene 0.04 44.553 Caryophyllene <trans-> 7.28 45.325 Bergamotene<alpha-trans-> 0.07 46.553 Farnesene<(E)-beta-> 0.70 46.750 Humulene <alpha> 0.51 46.878 Neryl-propanoate 0.03 47.767 Dauca-5,8-diene 0.03 48.343 Germacrene D 0.28 49.587 Lavandulyl isovalerate <ent> 0.14 49.746 Farnesene<(E,E)-alpha-> 0.04 49.965 Bisabolene <beta-> 0.04 50.304 Amorphene <delta> 0.11 54.399 Caryophyllene oxide 0.15 57.898 Cadinol <epi-alpha> 0.06 60.305 Bisabolol<epi-alpha-> 0.11

100.00

min

21,314,315

20.0 30.0 40.0 50.0 60.0 62.0

TIC

12.2

50

12.6

66

13.5

75

14.8

52

15.1

56

15.2

41

15.5

40

15.7

80

16.1

63

17.0

03

17.1

70

18.0

17

18.3

10

18.4

95

18.6

98

19.3

87

20.1

95

21.0

13

22.0

09

22.0

87

23.2

03

23.3

40

23.4

98

24.3

11

24.9

33

26.2

89

27.9

09

28.0

28 28.6

11

29.0

51

29.3

02

29.6

29

31.6

95

31.8

65

32.3

27

32.7

62

32.9

99

33.4

59

34.0

84

34.9

73

35.5

76

38.6

50

39.7

96

40.5

39

41.6

82

41.8

26

42.4

37

43.4

01

44.5

53

45.3

25 46.5

53

46.7

50

46.8

78

47.7

67

48.3

43

49.5

87

49.7

46

49.9

65

50.3

04

54.3

99

57.8

98

60.3

05

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/24/2019 6:17:58 AM Sample Type : Essential Oil Sample Name : Lavender

Company Name : AD Practitioners, LLCLot# : 9A

Injection Volume : 0.30

Comments:

Synthetic markers of Linalyl acetate were detected

in the analysis of Lavender ADP 9A. This indicated

Linalyl acetate has been added to Lavender ADP 9A.

Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

Peak Report TIC R.Time Name Area%

7.850 Hexane, 1-methoxy- 0.11 12.245 Thujene <alpha-> 0.13 12.658 Pinene<alpha-> 0.25 13.572 Camphene 0.11 14.850 Sabinene 0.03 15.153 Pinene<beta-> 0.02 15.232 Octen-3-ol<1-> 0.07 15.537 Octanone<3-> 1.03 15.777 Myrcene 0.51 16.145 Butyl butanoate 0.12 17.000 Carene<delta-3-> 0.07 17.154 Hexyl acetate 0.70 17.685 Cymene<ortho-> 0.03 18.012 Cymene<para-> 0.27 18.305 Limonene 0.28 18.483 Cineole<1,8-> 0.73 18.715 Ocimene<(Z)-beta-> 3.83 19.393 Ocimene<(E)-beta-> 2.04 20.190 Terpinene<gamma-> 0.10 21.009 Linalool oxide <cis-(furanoid)> 0.29 21.215 Pinene oxide <alpha> 0.03 22.005 Terpinolene 0.04 22.083 Linalool oxide <trans-(furanoid)> 0.15 22.428 Rosefuran 0.02 23.203 Linalool 31.07 23.340 Hexyl propanoate 0.10 23.501 Octen-3-yl acetate<1-> 1.34 24.301 Octanol acetate<3-> 0.12 24.923 Ocimene <allo> 0.13 25.693 Myroxide <trans> 0.03 26.259 Camphor 0.34 27.425 Lavandulol 0.08 28.651 Terpinen-4-ol 5.79 29.047 Cryptone 0.11 29.297 Hexyl butanoate 0.58 29.628 Terpineol <alpha-> 0.96 31.854 Bornyl formate 0.03 32.322 Hexyl 2-methyl butanoate 0.03 33.449 Linalyl acetate 34.72 35.602 Lavandulyl acetate 4.81 38.650 Hexyl tiglate 0.04 39.598 Peroxylinalyl acetate A 0.04 39.787 Peroxylinalyl acetate B 0.06 40.530 Neryl acetate 0.36 41.815 Geranyl acetate 0.62 42.203 Bourbonene <alpha> 0.03 42.322 Hexyl hexanoate 0.09 42.427 Sesquithujene<7-epi-> 0.07 44.073 Bergamotene<alpha-cis-> 0.04 44.521 Caryophyllene <trans-> 3.98 45.318 Bergamotene<alpha-trans-> 0.13 46.021 Isocaryophyllene 0.02 46.558 Farnesene<(E)-beta-> 2.30 46.745 Humulene <alpha> 0.11 48.341 Germacrene D 0.16 48.496 Farnesene <alpha-cis-cis-> 0.04 50.301 Amorphene <delta> 0.05 54.398 Caryophyllene oxide 0.61 80.637 Farnesyl acetate <isomer> 0.05

100.00

min

20,295,535

10.0 20.0 30.0 40.0 50.0 60.0 70.0 80.0

TIC

7.850

12.245

12.658

13.572

14.850

15.153

15.232

15.537

15.777

16.145

17.00017.154

17.68518.012

18.305 18.483

18.715

19.393

20.190

21.009

21.215

22.005

22.083

22.428

23.203

23.340

23.501

24.301

24.923

25.693

26.259

27.425

28.651

29.047 29.29729.628

31.854

32.322

33.449

35.602

38.650

39.598

39.787 40.530

41.815

42.203

42.322

42.427

44.073

44.521

45.318

46.021

46.558

46.745

48.341

48.496

50.301 54.398

80.637

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/23/2019 8:28:32 PM Sample Type : Essential Oil Sample Name : Lavender

Company Name : AD Practitioners, LLCLot# : 10A

Injection Volume : 0.30

Comments:No adulteration or contamination was detectedin Lavender ADP 10A.

Copyright © 2018 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika poudel

Peak Report TIC R.Time Name Area% 12.242 Thujene<alpha-> 0.02 12.655 Pinene<alpha-> 0.18 13.567 Camphene 0.09 14.845 Sabinene 0.04 15.150 Pinene<beta-> 0.18 15.237 Octen-3-ol<1-> 0.02 15.533 Octanone<3-> 0.25 15.774 Myrcene 0.29 16.997 Carene<delta-3-> 0.02 17.155 Hexyl acetate 0.22 18.009 Cymene<para-> 0.14 18.314 Limonene 1.90 18.501 1,8-cineole 3.83 18.691 Ocimene<(Z)-beta-> 0.96 19.379 Ocimene<(E)-beta-> 0.39 20.188 Terpinene<gamma-> 0.04 21.008 Sabinene hydrate <cis> 0.12 22.001 Terpinolene 0.05 22.084 Linalool oxide <trans-(furanoid)> 0.07 22.498 Plinol A 0.03 23.243 Linalool 36.42 23.503 Octen-3-yl acetate<1-> 0.20 24.934 Ocimene<allo-> 0.07 25.392 Linalool <dihydro> 0.16 26.317 Camphor 4.46 27.565 Lavandulol 0.34 27.899 Terpineol <delta> 0.04 28.021 Borneol 0.69 28.610 Terpinen-4-ol 1.95 29.295 Hexyl butanoate 0.19 29.624 Terpineol<alpha-> 0.54 31.873 Sabinene hydrate acetate 0.09 32.320 Hexyl 2-methyl butanoate 0.03 32.754 Hexyl isovalerate 0.08 33.473 Linalyl acetate 37.49 34.524 Linalyl acetae <dihydro> 0.23 35.331 Plinyl acetate 0.01 35.574 Lavandulyl acetate 1.90 38.640 Hexyl tiglate 0.11 39.590 Peroxylinalyl acetate A 0.01 39.781 Terpinyl acetate<alpha-> 0.04 40.530 Neryl acetate 0.25 41.674 Copaene<alpha-> 0.02 41.814 Geranyl acetate 0.63 42.426 Sesquithujene<7-epi-> 0.04 43.385 Sesquithujene 0.03 44.230 Lavandulyl isobutanoate 0.01 44.517 Caryophyllene <trans> 3.27 45.315 Bergamotene<alpha-trans-> 0.06 45.507 Coumarin 0.04 46.541 Farnesene<(E)-beta-> 0.51 46.741 Humulene <alpha> 0.22 46.873 Neryl-propanoate 0.04 48.335 Germacrene D 0.22 49.578 Lavandulyl isovalerate <ent> 0.15 49.960 Bisabolene <beta-> 0.05 50.297 Amorphene <delta> 0.11 50.926 Sesquiphellandrene<beta-> 0.04 52.797 Geranyl butanoate 0.05 54.392 Caryophyllene oxide 0.17 57.880 Cadinol <epi-alpha> 0.06 60.294 Bisabolol<epi-alpha-> 0.14

100.00

min

23,088,926

20.0 30.0 40.0 50.0 60.0 62.0

TIC

12.2

42

12.6

55

13.5

67

14.8

45

15.1

50

15.2

37

15.5

33

15.7

74

16.9

97

17.1

55

18.0

09

18.3

14

18.5

01

18.6

91

19.3

79

20.1

88

21.0

08

22.0

01

22.0

84

22.4

98

23.2

43

23.5

03

24.9

34

25.3

92

26.3

17

27.5

65

27.8

99 2

8.0

21

28.6

10

29.2

95

29.6

24

31.8

73

32.3

20

32.7

54

33.4

73

34.5

24

35.3

31

35.5

74

38.6

40

39.5

90

39.7

81

40.5

30

41.6

74 41.8

14

42.4

26

43.3

85

44.2

30

44.5

17

45.3

15

45.5

07

46.5

41

46.7

41

46.8

73

48.3

35

49.5

78

49.9

60

50.2

97

50.9

26

52.7

97

54.3

92

57.8

80

60.2

94

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/24/2019 10:09:11 AM Sample Type : Essential Oil Sample Name : Lavender

Company Name : AD Practitioners, LLCLot# : 11A

Injection Volume : 0.30

Comments:

Synthetic marker of Linalool and Linalyl acetate were

detected in the analysis of Lavender ADP 11A.

This indicated Linalool and Linalyl acetate has

been added to Lavender ADP 11A.

Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

PEPPERMINT 1B to 11B

Peak Report TIC R.Time Name Area%

5.808 Isopentyl alcohol 0.02 5.898 Butanol<2-methyl> 0.02

11.532 Furan, 2,5-diethyltetrahydro- 0.04 13.142 Thujene <alpha-> 0.05 13.588 Pinene <alpha> 0.81 14.289 Cyclohexanol <methyl> 0.00 15.850 Sabinene 0.52 16.183 Pinene <beta> 1.27 16.781 Myrcene 0.22 17.216 Octanol <3> 0.24 17.912 Phellandrene <alpha-> 0.02 18.591 Terpinene <alpha-> 0.30 19.080 Cymene<para-> 0.19 19.407 Limonene 2.16 19.633 1,8-cineole 5.85 19.754 Ocimene <Z-beta> 0.25 20.460 Ocimene <E-beta> 0.07 21.303 Terpinene <gamma> 0.49 22.116 Sabinene hydrate <cis> 0.61 23.149 Terpinolene 0.15 24.095 Linalool 0.25 24.228 Sabinene hydrate <trans> 0.06 24.298 Methyl butyl-2-methyl butyrate<2-> 0.07 24.677 Methyl butyl isovalerate<2-> 0.06 25.418 Octyl acetate <3-> 0.03 25.868 Menth-2-en-1-ol<cis-para-> 0.04 27.571 Isopulegol 0.11 28.255 Menthone 23.05 28.644 menthofuran 2.89 28.778 Isomenthone 4.11 29.098 Neomenthol 3.92 29.351 Dehydro menthone 0.01 29.434 Isopulegone <trans> 0.05 29.873 Menthol 34.97 29.905 Terpinen-4-ol 0.31 30.426 Menthol <iso> 0.61 30.605 Menthol <neoiso> 0.18 30.831 Terpineol <alpha> 0.36 32.209 Menthone oxy 0.03 33.529 Hexenyl 2-methyl butanoate <3Z> 0.03 33.783 Pulegone 1.25 34.142 Carvone 0.04 34.835 Piperitone 0.52 36.081 Menthyl acetate <neo> 0.38 36.200 Mentha-1(7),8(10)-dien-9-ol <para-> 0.03 37.318 Menthyl acetate 6.35 37.586 Dihydroedulan 0.05 38.325 Menthyl acetate <iso-> 0.27 40.995 Evodone+Mentho thiophene 0.00 41.096 Mint Furanone Isomer 0.01 41.187 Mint Furanone Isomer 0.01 43.020 Copaene <alpha> 0.04 43.556 Bourbonene <beta> 0.34 43.891 Elemene <beta> 0.12 45.886 Caryophyllene <trans> 2.89 46.494 Copaene <beta> 0.06 47.852 Farnesene<(E)-beta-> 0.35 48.115 Humulene <alpha> 0.13 49.299 Cadina-1(6),4-diene <trans-> 0.04 49.718 Germacrene D 1.87 50.589 Bicyclogermacrene 0.32 50.745 Muurolene <alpha> 0.06 51.930 Cadinene <delta> 0.11 55.769 Caryophyllene oxide 0.06 56.493 Viridiflorol 0.27

100.00

min

5,213,734

10.0 20.0 30.0 40.0 50.0 58.0

TIC

5.8

08

5.8

98

11.5

32

13.1

42

13.5

88

14.2

89

15.8

50

16.1

83

16.7

81

17.2

16

17.9

12

18.5

91

19.0

80

19.4

07

19.6

33

19.7

54

20.4

60 2

1.3

03

22.1

16

23.1

49

24.0

95

24.2

28

24.2

98

24.6

77

25.4

18

25.8

68

27.5

71

28.2

55

28.6

44

28.7

78

29.0

98

29.3

51

29.4

34

29.8

73

29.9

05

30.4

26

30.6

05

30.8

31

32.2

09

33.5

29

33.7

83

34.1

42 3

4.8

35

36.0

81

36.2

00

37.3

18

37.5

86

38.3

25

40.9

95

41.0

96

41.1

87

43.0

20

43.5

56

43.8

91

45.8

86

46.4

94

47.8

52

48.1

15

49.2

99

49.7

18

50.5

89

50.7

45

51.9

30

55.7

69

56.4

93

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/24/2019 1:27:38 AM Sample Type : Essential Oil Sample Name : Peppermint

Company Name : AD Practitioners, LLCLot# : 1B

Injection Volume : 0.30

Comments:

No adulteration or contamination was detected

in Peppermint ADP 1B.

Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

Peak Report TIC R.Time Name Area%

5.144 Ethyl furan <2> 0.01 5.820 Isopentyl alcohol 0.03 5.907 Butanol<2-methyl> 0.03

11.542 Furan, 2,5-diethyltetrahydro- 0.02 13.144 Thujene<alpha-> 0.04 13.585 Pinene <alpha> 0.64 15.847 Sabinene 0.44 16.180 Pinene <beta> 1.04 16.782 Myrcene 0.19 17.218 Octanol<3-> 0.29 17.919 Phellandrene<alpha-> 0.01 18.590 Terpinene<alpha-> 0.41 19.075 Cymene<para-> 0.14 19.389 Limonene 1.70 19.596 1,8-cineole 5.17 19.754 Ocimene<(Z)-beta-> 0.31 20.462 Ocimene<(E)-beta-> 0.07 21.302 Terpinene<gamma-> 0.63 22.110 Sabinene hydrate <cis> 0.80 23.151 Terpinolene 0.17 24.081 Linalool 0.22 24.221 Sabinene hydrate <trans-> 0.07 24.301 Methyl butyl-2-methyl butyrate<2-> 0.04 24.683 Methyl butyl isovalerate<2-> 0.08 25.420 Octyl acetate <3-> 0.03 25.856 Menth-2-en-1-ol <cis-p> 0.05 27.100 Menth-2-en-1-ol <trans-p> 0.03 27.541 Isopulegol 0.09 28.104 Menthone 24.40 28.588 Menthofuran 2.39 28.700 Menthone<iso-> 3.36 29.038 Neomenthol 4.00 29.410 Isopulegone <trans> 0.03 29.648 Menthol 40.19 29.817 Terpinen-4-ol 1.19 30.360 Menthol <iso> 0.71 30.554 Menthol <neoiso> 0.22 30.793 Terpineol <alpha-> 0.20 33.755 Pulegone 0.97 34.141 Carvone 0.16 34.819 Piperitone 0.52 36.078 Menthyl acetate <neo> 0.22 37.267 Menthyl acetate 4.78 37.579 Dihydroedulan IA 0.02 38.318 Menthyl acetate <iso-> 0.23 43.553 Bourbonene <alpha> 0.30 43.894 Elemene<beta-> 0.06 45.863 Caryophyllene <trans> 1.47 46.509 Copaene beta 0.03 47.852 Farnesene <(E)-, beta-> 0.17 48.112 Humulene <alpha> 0.04 49.705 Germacrene D 1.22 50.594 Bicyclogermacrene 0.20 51.938 Cadinene <delta> 0.06 56.491 Viridiflorol 0.12

100.00

min

1,741,560

10.0 20.0 30.0 40.0 50.0 58.0

TIC

5.1

44

5.8

20

5.9

07

11.5

42

13.1

44

13.5

85

15.8

47

16.1

80

16.7

82

17.2

18

17.9

19

18.5

90

19.0

75

19.3

89

19.5

96

19.7

54

20.4

62

21.3

02

22.1

10

23.1

51

24.0

81

24.2

21

24.3

01

24.6

83

25.4

20

25.8

56

27.1

00

27.5

41

28.1

04

28.5

88 28.7

00

29.0

38

29.4

10

29.6

48

29.8

17

30.3

60

30.5

54

30.7

93

33.7

55

34.1

41

34.8

19

36.0

78

37.2

67

37.5

79

38.3

18

43.5

53

43.8

94 4

5.8

63

46.5

09

47.8

52

48.1

12 49.7

05

50.5

94

51.9

38

56.4

91

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/23/2019 5:57:27 AM Sample Type : Essential Oil Sample Name : Peppermint

Company Name : AD Practitioners, LLCLot# : 2B

Injection Volume : 0.30

Comments:

No adulteration or contamination was detected in

Peppermint ADP 2B.

Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

Peak Report TIC R.Time Name Area% 11.543 Furan, 2,5-diethyltetrahydro- 0.02 13.143 Thujene <alpha-> 0.02 13.586 Pinene <alpha> 0.75 14.544 Camphene 0.05 14.648 Cyclohexanone <methyl> 0.02 15.848 Sabinene 0.36 16.182 Pinene <beta-> 1.12 16.783 Myrcene 0.12 17.217 Octanol <3> 0.16 18.592 Terpinene <alpha-> 0.18 19.083 Cymene<para-> 0.25 19.399 Limonene 2.55 19.607 1,8-cineole 5.32 19.758 Ocimene <Z-beta> 0.06 20.464 Ocimene <E-beta> 0.02 21.300 Terpinene<gamma-> 0.33 22.110 Sabinene hydrate <cis> 0.34 23.149 Terpinolene 0.13 23.918 Nonanol<3-> 0.01 24.082 Linalool 0.10 24.220 Sabinene hydrate <trans> 0.07 24.320 Methyl butyl-2-methyl butyrate<2-> 0.02 27.546 Isopulegol 0.08 28.156 Menthone 26.54 28.320 Menthan-4-ol <Z> 0.03 28.609 Menthofuran 4.67 28.721 Isomenthone 4.45 29.050 Neomenthol 3.99 29.220 Borneol 0.04 29.375 Dehydro menthone 0.01 29.426 Isopulegone <trans> 0.07 29.707 Menthol 35.02 29.837 Terpinen-4-ol 0.72 30.045 2,2-Dimethylcyclohexyl acetate 0.01 30.371 Menthol <iso> 0.62 30.567 Menthol <neoiso> 0.13 30.794 Terpineol <alpha-> 0.21 32.198 Menthone oxy 0.03 33.760 Pulegone 1.25 34.139 Carvone 0.14 34.823 Piperitone 0.27 36.075 Menthyl acetate <neo> 0.26 37.278 Menthyl acetate 5.84 38.320 Menthyl acetate <iso-> 0.14 40.120 Elemene <delta> 0.01 41.321 Eugenol 0.02 43.016 Copaene <alpha> 0.02 43.552 Bourbonene <beta> 0.08 43.883 Elemene <beta> 0.03 45.865 Caryophyllene <trans> 2.02 47.725 Muurola-3,5-dine <cis> 0.01 47.818 Isocaryophyllene 0.18 48.118 Humulene <alpha> 0.15 49.570 Himachalene <gamma> 0.06 49.697 Germacrene D 0.34 49.866 Ionone <trans-beta>+Himachala-1,4-diene <11aH> 0.02 50.593 Mint Lactone+Bicyclogermacrene 0.08 50.881 Himachalene <beta> 0.33 51.937 Cadinene <delta> 0.05 55.779 Caryophyllene oxide 0.01 56.494 Viridiflorol 0.02

100.00

min

2,758,766

20.0 30.0 40.0 50.0 60.0 70.0 80.0

TIC

11.543

13.14313.586

14.544

14.648 15.84816.182

16.783

17.217

18.592

19.083

19.399

19.607

19.758

20.46421.300

22.110

23.149

23.918

24.082

24.220

24.320

27.546

28.156

28.320

28.609

28.721

29.050

29.220

29.375

29.426

29.707

29.837

30.045 30.371

30.567

30.794

32.198

33.760

34.139

34.823

36.075

37.278

38.320

40.120

41.321

43.016

43.552

43.883

45.865

47.725

47.818

48.118

49.570

49.697

49.866

50.593

50.881

51.937

55.779

56.494

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/22/2019 8:10:12 PM Sample Type : Essential Oil Sample Name : Peppermint

Lot# : 3B Injection Volume : 0.30

Comments:The analysis of this peppermint sample has reduced biomarkers (viridiflorol, sabinene hydrate,geramcrene D) from authentic sample. So this peppermint oil has beenadulterated with menthol and menthyl acetate. Besidesaromachemical adulteration, this sample is tainted withHimalayan Cedarwood as well.

Copyright © 2018 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

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Peak Report TIC R.Time Name Area% 11.538 Furan, 2,5-diethyltetrahydro- 0.02 13.143 Thujene<alpha-> 0.03 13.586 Pinene <alpha> 0.83 14.548 Camphene 0.01 14.649 Cyclohexanone<3-methyl-> 0.01 15.849 Sabinene 0.47 16.182 Pinene <beta-> 1.23 16.782 Myrcene 0.14 17.217 Octanol <3> 0.13 17.761 Pseudolimonene 0.01 17.916 Phellandrene<alpha-> 0.03 18.590 Terpinene <alpha-> 0.22 19.085 Cymene<para-> 0.18 19.402 Limonene 2.52 19.615 1,8-cineole 5.80 19.757 Ocimene<(Z)-beta-> 0.12 20.459 Ocimene<(E)-beta-> 0.03 21.298 Terpinene<gamma-> 0.31 22.113 Sabinene hydrate <cis> 0.25 23.148 Terpinolene 0.09 24.084 Linalool 0.08 24.215 Sabinene hydrate <trans-> 0.02 24.301 Butyrate < 2-methyl-, 3-methylbutyl-> 0.03 24.679 Methyl butyl isovalerate<2-> 0.02 25.429 Octyl acetate <3-> 0.01 25.859 Menth-2-en-1-ol <cis-p> 0.02 27.550 Isopulegol 0.10 27.644 Terpineol<E-dihydro-alpha> 0.04 28.192 Menthone 26.38 28.330 Menthan-4-ol <Z> 0.02 28.614 Menthofuran 2.74 28.734 Isomenthone 4.12 29.066 Neomenthol 4.17 29.240 Borneol 0.02 29.365 Dehydro menthone 0.01 29.425 Isopulegone <trans> 0.15 29.764 Menthol 36.58 29.852 Terpinen-4-ol 0.61 30.065 2,2-Dimethylcyclohexyl acetate 0.03 30.387 Menthol <iso> 0.39 30.572 Menthol <neoiso> 0.11 30.803 Terpineol <alpha-> 0.18 32.202 Menthone oxy 0.03 33.517 Hexenyl 3-methyl butanoate<3Z-> 0.02 33.760 Pulegone 0.79 34.139 Carvone 0.09 34.820 Piperitone 0.35 35.970 Isopulegyl acetate <neo> 0.01 36.078 Menthyl acetate <neo> 0.40 37.294 Menthyl acetate 6.81 37.576 Dihydroedulan 0.03 38.318 Menthyl acetate <iso-> 0.22 43.553 Bourbonene <beta> 0.11 43.889 Elemene <beta> 0.06 45.865 Caryophyllene <trans> 1.87 47.850 Farnesene <(E)-, beta-> 0.11 48.114 Humulene <alpha> 0.04 49.698 Germacrene D 0.60 50.590 Bicyclogermacrene 0.09 51.922 Cadinene <delta> 0.02 56.487 Viridiflorol 0.04

100.00

min

3,704,224

20.0 30.0 40.0 50.0 60.0 70.0 80.0

TIC

11.538

13.143

13.586

14.548

14.649 15.84916.182

16.782

17.217

17.761

17.916

18.590

19.085

19.402

19.615

19.757

20.45921.298

22.113

23.148

24.084

24.215

24.301

24.679

25.429

25.859

27.550

27.644

28.192

28.330

28.614

28.734

29.066

29.240

29.365

29.425

29.764

29.852

30.065

30.387

30.572

30.803

32.202

33.51733.760

34.139

34.820

35.970 36.078

37.294

37.576

38.318

43.553

43.889

45.865

47.850

48.114 49.698

50.590

51.922

56.487

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/22/2019 10:08:10 PM Sample Type : Essential Oil Sample Name : Peppermint

Lot# : 4B Injection Volume : 0.30

Comments:The analysis of this peppermint sample has reducedbiomarkers (viridiflorol, sabinene hydrate,geramcrene D) from authentic sample.So this peppermint oil has beenadulterated with menthol and menthyl acetate.

Copyright © 2018 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

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Peak Report TIC R.Time Name Area%

5.143 Ethyl furan<2> 0.01 5.810 Isopentyl alcohol 0.02 5.898 Butanol<2-methyl> 0.02

11.535 Furan, 2,5-diethyltetrahydro- 0.02 13.142 Thujene <alpha-> 0.04 13.584 Pinene <alpha> 0.62 15.845 Sabinene 0.44 16.180 Pinene <beta> 1.01 16.780 Myrcene 0.17 17.212 Octanol <3> 0.30 18.582 Terpinene <alpha-> 0.24 19.076 Cymene<para-> 0.13 19.392 Limonene 1.26 19.505 Phellandrene <beta> 0.03 19.611 1,8-cineole 4.64 19.753 Ocimene <Z-beta> 0.30 20.462 Ocimene <E-beta> 0.08 21.302 Terpinene <gamma> 0.40 22.119 Sabinene hydrate <cis> 1.11 23.153 Terpinolene 0.12 24.089 Linalool 0.27 24.226 Sabinene hydrate <trans> 0.10 24.320 Methyl butyl-2-methyl butyrate<2-> 0.04 24.680 Methyl butyl isovalerate<2-> 0.08 25.424 3-Octyl acetate 0.04 25.860 Menth-2-en-1-ol <cis-p> 0.05 26.917 Sabinol <trans> 0.02 27.552 Isopulegol 0.09 28.183 Menthone 19.47 28.626 menthofuran 4.32 28.735 Isomenthone 2.84 29.070 neomenthol 3.62 29.370 Dehydro menthone 0.00 29.426 Isopulegone <trans> 0.03 29.809 Menthol 42.75 29.872 Terpinen-4-ol 0.61 30.402 Menthol <iso> 0.63 30.587 Menthol <neoiso> 0.18 30.813 Terpineol <alpha-> 0.18 32.209 Menthone oxy 0.02 33.528 Hexenyl 2-methyl butanoate <3Z> 0.03 33.773 Pulegone 1.32 34.829 Piperitone 0.49 35.965 Isopulegyl acetate <neo> 0.03 36.083 Menthyl acetate <neo> 0.22 36.189 Mentha-1(7),8(10)-dien-9-ol <para-> 0.03 37.297 Menthyl acetate 6.00 37.584 Dihydroedulan 0.04 38.322 Menthyl acetate <iso-> 0.26 40.995 Thiophene<mentho>+ Evodone 0.00 41.099 Mint Furanone Isomer 0.02 41.186 Mint Furanone Isomer 0.02 41.320 Eugenol 0.02 43.024 Copaene <alpha> 0.04 43.556 Bourbonene <beta> 0.36 43.894 Elemene <beta> 0.09 45.870 Caryophyllene <trans> 1.85 46.495 Copaene <beta> 0.05 47.404 Muurola-3,5-dine <cis> 0.02 47.852 Farnesene<(E)-beta-> 0.22 48.116 Humulene <alpha> 0.07 49.710 Germacrene D 1.97 50.592 Bicyclogermacrene 0.33 51.937 Cadinene <delta> 0.06 56.496 Viridiflorol 0.18

100.00

min

4,238,326

10.0 20.0 30.0 40.0 50.0 58.0

TIC

5.1

43

5.8

10

5.8

98

11.5

35

13.1

42

13.5

84

15.8

45 1

6.1

80

16.7

80

17.2

12

18.5

82

19.0

76

19.3

92

19.5

05

19.6

11

19.7

53

20.4

62

21.3

02

22.1

19

23.1

53

24.0

89

24.2

26

24.3

20

24.6

80

25.4

24

25.8

60

26.9

17

27.5

52

28.1

83

28.6

26

28.7

35

29.0

70

29.3

70

29.4

26

29.8

09

29.8

72

30.4

02

30.5

87

30.8

13

32.2

09

33.5

28

33.7

73

34.8

29

35.9

65

36.0

83

36.1

89

37.2

97

37.5

84

38.3

22

40.9

95

41.0

99

41.1

86

41.3

20

43.0

24

43.5

56

43.8

94

45.8

70

46.4

95

47.4

04

47.8

52

48.1

16

49.7

10

50.5

92

51.9

37

56.4

96

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/23/2019 11:50:50 AM Sample Type : Essential Oil Sample Name : Peppermint

Company Name : AD Practitioners, LLCLot# : 5B

Injection Volume : 0.30

Comments:

No adulteration or contamination was detected in

Peppermint ADP 5B.

Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

Peak Report TIC R.Time Name Area%

9.642 Hexenol <3Z> 0.01 11.547 Furan, 2,5-diethyltetrahydro- 0.02 13.152 Thujene <alpha-> 0.05 13.595 Pinene <alpha> 0.72 14.552 Camphene 0.01 15.858 Sabinene 0.54 16.192 Pinene <beta> 1.13 16.523 3-Octanone 0.02 16.790 Myrcene 0.21 17.228 Octanol <3> 0.26 18.600 Terpinene <alpha-> 0.24 19.092 Cymene<para-> 0.22 19.413 Limonene 2.20 19.632 1,8-cineole 5.92 19.764 Ocimene <Z-beta> 0.33 20.469 Ocimene <E-beta> 0.08 21.310 Terpinene <gamma> 0.42 22.126 Sabinene hydrate <cis> 1.05 23.158 Terpinolene 0.13 24.097 Linalool 0.36 24.234 Sabinene hydrate <trans> 0.08 25.431 Octanol acetate<3-> 0.05 25.872 Menth-2-en-1-ol<cis-para-> 0.05 26.926 Sabinol <trans> 0.02 27.122 Menth-2-en-1ol<trans-para-> 0.02 27.562 Isopulegol 0.09 28.182 Menthone 14.57 28.651 menthofuran 6.46 28.752 Isomenthone 2.78 29.086 Neomenthol 3.89 29.431 Isopulegone <trans> 0.10 29.833 Menthol 39.79 29.880 Terpinen-4-ol 0.53 30.418 Menthol <iso> 0.68 30.600 Menthol <neoiso> 0.19 30.822 Terpineol <alpha> 0.23 32.211 Menthone oxy 0.02 33.540 Hexenyl 2-methyl butanoate <3Z> 0.04 33.819 Pulegone 4.51 34.839 Piperitone 0.39 35.970 Isopulegyl acetate <neo> 0.03 36.087 Menthyl acetate <neo> 0.21 36.203 Mentha-1(7),8(10)-dien-9-ol <para-> 0.03 37.303 Menthyl acetate 4.94 37.594 Dihydroedulan 0.04 38.331 Menthyl acetate <iso-> 0.21 41.005 Thiophene<mentho>+Evodone 0.00 41.090 Mint Furanone Isomer 0.03 41.189 Mint Furanone Isomer 0.03 41.333 Eugenol 0.01 43.021 Copaene <alpha> 0.04 43.568 Bourbonene <beta> 0.33 43.899 Elemene <beta> 0.10 45.879 Caryophyllene <trans> 1.98 46.506 Copaene <beta> 0.04 47.414 Muurola-3,5-dine <cis> 0.02 47.860 Farnesene<(E)-beta-> 0.27 48.123 Humulene <alpha> 0.07 49.723 Germacrene D 2.27 50.606 Bicyclogermacrene 0.38 51.940 Cadinene <delta-> 0.06 55.443 Spathulenol 0.03 55.783 Caryophyllene oxide 0.05 56.507 Viridiflorol 0.43

100.00

min

4,950,699

10.0 20.0 30.0 40.0 50.0 58.0

TIC

9.6

42

11.5

47

13.1

52

13.5

95

14.5

52

15.8

58

16.1

92

16.5

23

16.7

90

17.2

28

18.6

00

19.0

92

19.4

13

19.6

32

19.7

64

20.4

69

21.3

10

22.1

26

23.1

58

24.0

97

24.2

34

25.4

31

25.8

72

26.9

26

27.1

22

27.5

62

28.1

82

28.6

51

28.7

52

29.0

86

29.4

31

29.8

33

29.8

80

30.4

18

30.6

00

30.8

22

32.2

11

33.5

40

33.8

19

34.8

39

35.9

70

36.0

87

36.2

03

37.3

03

37.5

94

38.3

31

41.0

05

41.0

90

41.1

89

41.3

33

43.0

21

43.5

68

43.8

99

45.8

79

46.5

06

47.4

14

47.8

60

48.1

23

49.7

23

50.6

06

51.9

40

55.4

43

55.7

83

56.5

07

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/23/2019 3:38:23 PM Sample Type : Essential Oil Sample Name : Peppermint

Company Name : AD Practitioners, LLCLot# : 6B

Injection Volume : 0.30

Comments:

No adulteration or contamination was detected in

Peppermint ADP 6B.

Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

Peak Report TIC R.Time Name Area%

5.147 Ethyl furan<2> 0.01 5.812 Isopentyl alcohol 0.02 5.902 Butanol<2-methyl> 0.01

11.540 Furan, 2,5-diethyltetrahydro- 0.02 13.147 Thujene <alpha-> 0.03 13.593 Pinene <alpha> 0.76 14.549 Camphene 0.01 15.854 Sabinene 0.52 16.191 Pinene <beta> 1.31 16.786 Myrcene 0.15 17.223 Octanol <3> 0.18 17.920 Phellandrene <alpha-> 0.02 18.595 Terpinene <alpha-> 0.24 19.087 Cymene<para-> 0.14 19.413 Limonene 1.93 19.638 1,8-cineole 5.69 19.760 Ocimene <Z-beta> 0.20 20.465 Ocimene <E-beta> 0.05 21.304 Terpinene <gamma> 0.40 22.123 Sabinene hydrate <cis> 0.60 23.155 Terpinolene 0.12 24.099 Linalool 0.18 24.235 Sabinene hydrate <trans> 0.05 24.303 Methyl butyl-2-methyl butyrate<2-> 0.05 24.683 Methyl butyl isovalerate<2-> 0.07 25.427 Octanol acetate<3-> 0.03 25.871 Menth-2-en-1-ol<cis-para-> 0.04 27.578 Isopulegol 0.10 28.253 Menthone 20.95 28.649 Menthofuran 2.91 28.781 Isomenthone 3.71 29.103 Neomenthol 3.67 29.363 Dehydro menthone 0.01 29.441 Isopulegone <trans> 0.02 29.914 Menthol 41.21 30.446 Menthol <iso> 0.58 30.621 Menthol <neoiso> 0.18 30.848 Terpineol <alpha> 0.36 32.223 Menthone oxy 0.03 33.535 Hexenyl 2-methyl butanoate <3Z> 0.03 33.784 Pulegone 0.71 34.155 Carvone 0.03 34.848 Piperitone 0.59 35.975 Isopulegyl acetate <neo> 0.02 36.089 Menthyl acetate <neo> 0.47 36.210 Mentha-1(7),8(10)-dien-9-ol <para-> 0.02 37.328 Menthyl acetate 6.18 37.597 Dihydroedulan 0.04 38.332 Menthyl acetate <iso-> 0.29 41.024 Evodone+Thiophene<mentho> 0.00 41.096 Mint Furanone Isomer 0.01 41.192 Mint Furanone Isomer 0.01 41.327 Eugenol 0.02 43.029 Copaene <alpha> 0.02 43.562 Bourbonene <beta> 0.26 43.898 Elemene <beta> 0.06 45.891 Caryophyllene <trans> 2.48 46.508 Copaene <beta> 0.03 47.861 Farnesene<(E)-beta-> 0.22 48.127 Humulene <alpha> 0.07 49.717 Germacrene D 1.41 50.599 Bicyclogermacrene 0.22 51.939 Cadinene <delta-> 0.05 55.773 Caryophyllene oxide 0.01 56.503 Viridiflorol 0.13

100.00

min

5,947,352

10.0 20.0 30.0 40.0 50.0 58.0

TIC

5.1

47

5.8

12

5.9

02

11.5

40

13.1

47

13.5

93

14.5

49

15.8

54

16.1

91

16.7

86

17.2

23

17.9

20

18.5

95

19.0

87

19.4

13

19.6

38

19.7

60

20.4

65 21.3

04

22.1

23

23.1

55

24.0

99

24.2

35

24.3

03

24.6

83

25.4

27

25.8

71

27.5

78

28.2

53

28.6

49

28.7

81

29.1

03

29.3

63

29.4

41

29.9

14

30.4

46

30.6

21

30.8

48

32.2

23

33.5

35

33.7

84

34.1

55 3

4.8

48

35.9

75 36.0

89

36.2

10

37.3

28

37.5

97

38.3

32

41.0

24

41.0

96

41.1

92

41.3

27

43.0

29

43.5

62

43.8

98

45.8

91

46.5

08

47.8

61

48.1

27

49.7

17

50.5

99

51.9

39

55.7

73

56.5

03

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/23/2019 5:36:15 PM Sample Type : Essential Oil Sample Name : Peppermint

Company Name : AD Practitioners, LLCLot# : 7B

Injection Volume : 0.30

Comments:

No adulteration or contamination was detected

in Peppermint ADP 7B.

Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

Peak Report TIC R.Time Name Area%

5.145 Ethyl furan <2> 0.02 5.810 Isopentyl alcohol 0.03 5.900 Butanol<2-methyl> 0.03

11.538 Furan, 2,5-diethyltetrahydro- 0.03 13.148 Thujene <alpha-> 0.05 13.591 Pinene <alpha> 0.64 15.854 Sabinene 0.44 16.187 Pinene <beta> 1.01 16.787 Myrcene 0.19 17.222 Octanol <3> 0.34 17.916 Phellandrene <alpha-> 0.02 18.597 Terpinene <alpha-> 0.37 19.086 Cymene<para-> 0.11 19.404 Limonene 1.61 19.627 1,8-cineole 4.85 19.761 Ocimene <Z-beta> 0.28 20.466 Ocimene <E-beta> 0.07 21.308 Terpinene <gamma> 0.58 22.123 Sabinene hydrate <cis> 0.85 23.156 Terpinolene 0.17 24.098 Linalool 0.28 24.234 Sabinene hydrate <trans> 0.09 24.308 Methyl butyl-2-methyl butyrate<2-> 0.06 24.683 Methyl butyl isovalerate<2-> 0.12 25.429 Octanol acetate<3-> 0.05 25.874 Menth-2-en-1-ol<cis-para-> 0.06 27.566 Isopulegol 0.10 28.220 Menthone 18.79 28.642 Menthofuran 3.38 28.757 Isomenthone 3.09 29.094 Neomenthol 4.36 29.385 Dehydro menthone 0.01 29.436 Isopulegone <trans> 0.03 29.873 Menthol 42.32 29.920 Terpinen-4-ol 0.18 30.433 Menthol <iso> 0.84 30.612 Menthol <neoiso> 0.23 30.833 Terpineol <alpha> 0.19 33.537 Hexenyl 3-methyl butanoate<3Z-> 0.04 33.787 Pulegone 1.29 34.840 Piperitone 0.52 35.975 Isopulegyl acetate <neo> 0.03 36.087 Menthyl acetate <neo> 0.29 36.201 Mentha-1(7),8(10)-dien-9-ol <para-> 0.03 37.317 Menthyl acetate 5.96 37.595 Dihydroedulan 0.05 38.329 Menthyl acetate <iso-> 0.28 38.521 Isopulegyl acetate <neoiso> 0.02 41.114 Mint Furanone Isomer 0.01 41.187 Mint Furanone Isomer 0.01 41.327 Eugenol 0.01 43.028 Copaene <alpha> 0.04 43.567 Bourbonene <beta> 0.41 43.760 Bourbonene <alpha> 0.03 43.900 Elemene <beta> 0.09 45.881 Caryophyllene <trans> 2.11 46.501 Copaene <beta> 0.05 47.417 Muurola-3,5-dine <cis> 0.02 47.862 Farnesene<(E)-beta-> 0.32 48.123 Humulene <alpha> 0.07 48.932 Caryophyllene<9-epi-trans> 0.02 49.722 Germacrene D 1.90 50.601 Bicyclogermacrene 0.31 51.939 Cadinene <delta> 0.08 56.501 Viridiflorol 0.18

100.00

min

5,357,698

10.0 20.0 30.0 40.0 50.0 58.0

TIC

5.1

45

5.8

10

5.9

00

11.5

38

13.1

48

13.5

91

15.8

54 1

6.1

87

16.7

87

17.2

22

17.9

16

18.5

97

19.0

86

19.4

04

19.6

27

19.7

61

20.4

66 2

1.3

08

22.1

23

23.1

56

24.0

98

24.2

34

24.3

08

24.6

83

25.4

29

25.8

74

27.5

66

28.2

20

28.6

42

28.7

57 2

9.0

94

29.3

85

29.4

36

29.8

73

29.9

20

30.4

33

30.6

12

30.8

33

33.5

37

33.7

87

34.8

40

35.9

75

36.0

87

36.2

01

37.3

17

37.5

95

38.3

29

38.5

21

41.1

14

41.1

87

41.3

27

43.0

28

43.5

67

43.7

60

43.9

00

45.8

81

46.5

01

47.4

17

47.8

62

48.1

23

48.9

32

49.7

22

50.6

01

51.9

39

56.5

01

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/23/2019 7:34:01 PM Sample Type : Essential Oil Sample Name : Peppermint

Company Name : AD Practitioners, LLCLot# : 8B

Injection Volume : 0.30

Comments:

No adulteration or contamination was detected in

Peppermint ADP 8B.

Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

Peak Report TIC R.Time Name Area% 11.538 Furan, 2,5-diethyltetrahydro- 0.07 13.147 Thujene <alpha-> 0.03 13.591 Pinene <alpha> 0.84 14.303 Cyclohexanol <methyl> 0.02 14.548 Camphene 0.03 14.647 Cyclohexanone<3-methyl-> 0.02 15.733 Menthane<trans-p-> 0.00 15.765 m-Menth-1-ene 0.00 15.852 Sabinene 0.26 16.187 Pinene <beta-> 1.03 16.455 Menthene<3-p-> 0.00 16.476 Pinane<cis-> 0.00 16.505 Pinane<E> 0.00 16.784 Myrcene 0.11 17.222 Octanol <3> 0.17 18.593 Terpinene <alpha-> 0.08 19.086 Cymene<para-> 0.14 19.416 Limonene 2.69 19.636 1,8-cineole 5.35 19.757 Ocimene <Z-beta> 0.04 20.466 Ocimene <E-beta> 0.02 21.305 Terpinene <gamma> 0.11 22.115 Sabinene hydrate <cis> 0.15 23.156 Terpinolene 0.05 23.931 Nonanol<3-> 0.02 24.099 Linalool 0.09 27.392 Verbenol<trans-> 0.02 27.577 Isopulegol 0.11 28.267 Menthone 24.04 28.363 Menthan-4-ol <Z> 0.05 28.472 Pinocamphone<trans-> 0.03 28.631 Menthofuran 1.42 28.776 Isomenthone 3.99 29.102 Neomenthol 3.70 29.281 Nonanol+Borneol 0.11 29.441 Isopulegone <trans> 0.04 29.908 Menthol 42.95 30.122 2,2-Dimethylcyclohexyl acetate 0.05 30.276 Cymen-8-ol<para-> 0.02 30.444 Menthol <iso> 0.55 30.622 Menthol <neoiso> 0.19 30.844 Terpineol <alpha> 0.29 32.227 Menthone oxy 0.04 33.776 Pulegone 0.41 34.153 Carvone 0.02 34.843 Piperitone 0.42 36.082 Menthyl acetate <neo> 0.25 37.327 Menthyl acetate 6.52 38.331 Menthyl acetate <iso-> 0.09 38.583 Nonyl acetate 0.03 40.126 Elemene <delta> 0.07 41.110 Cubebene<alpha-> 0.02 41.326 Eugenol 0.02 43.023 Copaene <alpha> 0.06 43.564 Bourbonene <beta> 0.14 43.895 Elemene <beta> 0.06 45.885 Caryophyllene <trans> 2.31 46.503 Copaene <beta> 0.05 47.409 Muurola-3,5-dine <cis> 0.02 47.837 Caryophyllene <epi> 0.12 48.119 Humulene <alpha> 0.15 49.707 Germacrene D 0.19

min

5,508,564

20.0 30.0 40.0 50.0 60.0 70.0 80.0

TIC

11.538

13.147

13.591

14.303

14.548

14.647

15.733

15.765 15.852

16.187

16.455

16.476

16.505

16.784

17.222

18.593

19.086

19.416

19.636

19.757

20.466

21.305

22.115

23.156

23.931

24.099

27.392

27.577

28.267

28.363

28.472

28.631

28.776

29.102

29.281

29.441

29.908

30.122

30.276 30.444

30.622

30.844

32.227 33.776

34.153 34.843

36.082

37.327

38.331

38.583

40.126

41.110

41.326

43.023

43.564

43.895

45.885

46.503

47.409

47.837

48.119

49.707

50.596

50.819

51.944

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/23/2019 9:46:52 AM Sample Type : Essential Oil Sample Name : Peppermint

Lot# : 9B Injection Volume : 0.30

Comments:The analysis of this peppermint sample has reducedor missing key biomarkers (viridiflorol, sabinene hydrate,geramcrene D) from authentic sample.So this peppermint oil has been adulterated with menthol and menthyl acetate.

Copyright © 2018 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

psatyal
Highlight
psatyal
Highlight

R.Time Name Area% 50.596 Bicyclogermacrene 0.05 50.819 Valencene 0.06 51.944 Cadinene <delta> 0.02

100.00

Peak Report TIC R.Time Name Area% 11.534 Furan, 2,5-diethyltetrahydro- 0.03 13.142 Thujene <alpha-> 0.03 13.589 Pinene <alpha> 0.82 14.296 Cyclohexanol <methyl> 0.01 14.543 Camphene 0.03 14.634 Cyclohexanone<3-methyl-> 0.06 15.849 Sabinene 0.42 16.188 Pinene <beta> 1.25 16.507 3-Octanone 0.02 16.550 Menthene<3-p> 0.01 16.782 Myrcene 0.20 17.051 Menthane<trans> 0.00 17.217 Octanol <3> 0.13 18.592 Terpinene <alpha-> 0.12 19.082 Cymene<para-> 0.26 19.177 Octyl methyl ether 0.00 19.245 Hexanol<2-ethyl> 0.01 19.418 Limonene 2.85 19.637 1,8-cineole 5.25 19.754 Ocimene <Z-beta> 0.08 20.461 Ocimene <E-beta> 0.03 21.301 Terpinene <gamma> 0.20 22.117 Sabinene hydrate <cis> 0.23 23.150 Terpinolene 0.09 24.096 Linalool 0.17 24.304 Methyl butyl-2-methyl butyrate<2-> 0.04 27.590 Isopulegol 0.11 28.283 Menthone 24.84 28.377 Menthan-4-ol <Z> 0.12 28.669 Menthofuran 4.05 28.801 Isomenthone 4.54 29.111 Neomenthol 4.05 29.272 Nonanol+Borneol 0.12 29.345 Dehydro menthone 0.00 29.447 Isopulegone <trans> 0.06 29.888 Menthol 33.34 29.930 Terpinen-4-ol 0.12 30.116 2,2-Dimethylcyclohexyl acetate 0.02 30.435 Menthol <iso> 0.65 30.618 Menthol <neoiso> 0.32 30.843 Terpineol <alpha> 0.54 31.011 Methyl chavicol 0.11 31.168 Piperitol <Z> 0.06 32.219 Menthone oxy 0.07 33.796 Pulegone 1.68 34.153 Carvone 0.23 34.847 Piperitone 0.71 36.077 Menthyl acetate <neo> 0.33 37.323 Menthyl acetate 6.45 38.326 Menthyl acetate <iso-> 0.14 39.072 Carvomenthyl acetate 0.04 40.121 Elemene <delta> 0.09 43.022 Copaene <alpha> 0.07 43.557 Bourbonene <beta> 0.23 43.891 Elemene <beta> 0.09 45.889 Caryophyllene <trans> 3.00 46.114 2,6-Diisopropylanisole 0.01 46.493 Copaene <beta> 0.06 47.406 Murrola-3,5-diene <trans> 0.03 47.842 Caryophyllene <epi> 0.18 48.118 Humulene <alpha> 0.22 49.297 Cadina-1(6),4-diene <trans-> 0.04

min

5,341,394

20.0 30.0 40.0 50.0 60.0 70.0 80.0

TIC

11.534

13.142

13.589

14.296

14.543

14.634 15.849

16.188

16.507

16.550 16.782

17.051

17.217

18.592

19.082

19.177

19.245

19.418

19.637

19.754

20.461

21.301

22.117

23.150

24.096

24.304

27.590

28.283

28.377

28.669

28.801

29.111

29.272

29.345

29.447

29.888

29.930

30.11630.435

30.61830.843

31.011

31.168

32.219

33.796

34.153 34.847

36.077

37.323

38.326

39.072

40.121

43.022

43.557

43.891

45.889

46.114

46.493

47.406

47.842

48.118

49.297 49.702

50.191

50.587

50.816

51.926

55.767

56.491

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/23/2019 3:40:22 PM Sample Type : Essential Oil Sample Name : Peppermint

Lot# : 10B Injection Volume : 0.30

Comments:The analysis of this peppermint sample has reducedor missing key biomarkers (viridiflorol, sabinene hydrate,geramcrene D) from authentic sample.So this peppermintoil has been adulterated with menthol and menthyl acetate.

Copyright © 2018 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

psatyal
Highlight

R.Time Name Area% 49.702 Germacrene D 0.44 50.191 Dehydromintlactone 0.02 50.587 Mint Lactone+Bicyclogermacrene 0.17 50.816 Valencene 0.11 51.926 Cadinene <delta-> 0.08 55.767 Caryophyllene oxide 0.09 56.491 Viridiflorol 0.06

100.00

psatyal
Highlight
psatyal
Highlight

Peak Report TIC R.Time Name Area%

5.807 Isopentyl alcohol 0.01 11.529 Furan, 2,5-diethyltetrahydro- 0.03 13.137 Thujene <alpha-> 0.04 13.581 Pinene <alpha> 0.62 14.538 Camphene 0.02 14.638 Cyclohexanone <methyl> 0.01 15.841 Sabinene 0.38 16.177 Pinene <beta> 0.95 16.775 Myrcene 0.16 17.212 Octanol <3> 0.14 17.906 Phellandrene <alpha-> 0.02 18.583 Terpinene <alpha-> 0.19 19.081 Cymene<para-> 0.23 19.401 Limonene 1.76 19.630 1,8-cineole 5.42 19.750 Ocimene <Z-beta> 0.14 20.454 Ocimene <E-beta> 0.03 21.293 Terpinene <gamma> 0.34 22.108 Sabinene hydrate <cis> 0.34 23.140 Terpinolene 0.11 24.085 Linalool 0.14 24.215 Sabinene hydrate <trans-> 0.04 24.294 Methyl butyl-2-methyl butyrate<2-> 0.05 24.670 Methyl butyl isovalerate<2-> 0.03 25.868 Menth-2-en-1-ol <cis-p> 0.03 27.566 Isopulegol 0.13 28.242 Menthone 20.17 28.631 Menthofuran 2.19 28.767 Isomenthone 3.79 29.094 Neomenthol 3.87 29.343 Dehydro menthone 0.01 29.427 Isopulegone <trans> 0.02 29.921 Menthol 43.22 29.955 Terpinen-4-ol 0.07 30.439 Menthol <iso> 0.52 30.615 Menthol <neoiso> 0.18 30.834 Terpineol <alpha> 0.24 32.210 Menthone oxy 0.03 33.522 Hexenyl 2-methyl butanoate <3Z> 0.03 33.771 Pulegone 0.78 34.140 Carvone 0.07 34.831 Piperitone 0.42 35.955 Isopulegyl acetate <neo> 0.02 36.081 Menthyl acetate <neo> 0.64 36.199 Mentha-1(7),8(10)-dien-9-ol <para-> 0.02 37.328 Menthyl acetate 7.63 37.583 Dihydroedulan 0.04 38.320 Menthyl acetate <iso-> 0.37 38.506 Isopulegyl acetate <neoiso> 0.02 41.319 Eugenol 0.02 43.550 Bourbonene <alpha> 0.19 43.882 Elemene <beta> 0.07 45.871 Caryophyllene <trans> 2.14 46.490 Copaene <beta> 0.02 47.845 Farnesene<(E)-beta> 0.26 48.110 Humulene <alpha> 0.09 49.289 Cadina-1(6),4-diene <trans-> 0.02 49.700 Germacrene D 1.07 50.584 Bicyclogermacrene 0.16 51.922 Cadinene <delta-> 0.06 55.761 Caryophyllene oxide 0.05 56.484 Viridiflorol 0.13

min

5,834,311

10.0 20.0 30.0 40.0 50.0 58.0

TIC

5.807

11.529

13.137

13.581

14.538

14.638 15

.84116.177

16.775

17.212

17.90618.583

19.081

19.401

19.630

19.750

20.454 21.293

22.108

23.140

24.085

24.215

24.294

24.670

25.868

27.566

28.242

28.631

28.767

29.094

29.343

29.427

29.921

29.95530.439

30.615

30.834

32.210

33.522

33.771

34.140 34.831

35.95536.081

36.199

37.328

37.583 38.320

38.506

41.319

43.550

43.882

45.871

46.490

47.845

48.110

49.289

49.700

50.584

51.922

55.761

56.484

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/23/2019 5:38:19 PM Sample Type : Essential Oil Sample Name : Peppermint

Lot# : 11B Injection Volume : 0.30

Comments:No adulteration or contamination was detected inPeppermint ADP 11B.

Copyright © 2018 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

R.Time Name Area% 100.00

TEA TREE 1C to 11C

Peak Report TIC R.Time Name Area% 13.130 Thujene <alpha-> 0.94 13.580 Pinene <alpha> 2.35 15.830 Sabinene 0.39 16.162 Pinene <beta-> 0.73 16.766 Myrcene 0.78 17.901 Phellandrene <alpha-> 0.56 18.640 Terpinene <alpha-> 9.33 19.090 Cymene <para-> 2.59 19.394 Limonene 0.87 19.506 Phellandrene <beta> 1.05 19.603 1,8-cineole 2.57 21.414 Terpinene<gamma-> 17.83 22.093 Sabinene hydrate <cis> 0.04 23.162 Terpinolene 3.42 23.451 Cymenene <para-> 0.05 24.062 Linalool 0.05 24.200 Sabinene hydrate <trans> 0.05 25.839 Menth-2-en-1-ol <cis-p> 0.30 27.100 Menth-2-en-1-ol <trans-p> 0.21 30.073 Terpinen-4-ol 41.21 30.854 Terpineol <alpha> 3.59 30.948 Piperitol<cis-> 0.07 31.729 Piperitol<trans-> 0.14 36.179 Ascaridol glycol <E> 0.06 39.332 4-isopropyl-6-methyl-3-cyclohexene-1,2-diol 0.06 40.093 Elemene <delta> 0.06 41.087 Cubebene <alpha> 0.08 42.668 Isoledene 0.07 42.998 Copaene <alpha> 0.20 45.043 Maaliene <beta-> 0.41 45.836 Caryophyllene <trans> 0.41 46.309 Caryophyllene <9-epi-cis-> 0.07 46.759 Maaliene <alpha-> 0.09 47.029 Aromadendrene 1.26 47.115 Bourb-11-ene 0.09 47.486 Myltayl-4(12)-ene 0.19 47.672 Muurola-3,5-diene<cis-> 0.19 47.863 Muurola-3,5-diene <trans> 0.05 48.092 Humulene <alpha> 0.07 48.375 Alloaromadendrene 0.65 49.097 Cadina-1(6),4-diene<trans-> 0.44 50.035 Selinene <delta> 0.18 50.168 Selinene <beta-> 0.22 50.299 Viridiflorene 1.24 50.586 Bicyclogermacrene 1.42 50.727 Muurolene <alpha> 0.18 51.929 Cadinene <delta-> 1.47 52.130 Calamenene <trans> 0.13 52.215 Zonarene 0.32 52.781 Cadine-1,4-diene <trans-> 0.23 54.563 Viridifloral <isomer> 0.07 55.413 Spathulenol 0.07 55.962 Globulol 0.27 56.473 Viridiflorol 0.14 56.599 Cubeban-11-ol 0.10 58.182 Eudesmol <isomer> 0.08 58.370 Cubenol<1-epi> 0.16 58.624 Spathulenol<iso-> 0.08 59.225 Cubenol 0.09

100.00

min

6,122,523

20.0 30.0 40.0 50.0 60.0

TIC

13.1

30

13.5

80

15.8

30 16.1

62

16.7

66

17.9

01

18.6

40

19.0

90

19.3

94

19.5

06

19.6

03

21.4

14

22.0

93

23.1

62

23.4

51

24.0

62

24.2

00

25.8

39

27.1

00

30.0

73

30.8

54

30.9

48

31.7

29

36.1

79

39.3

32

40.0

93

41.0

87

42.6

68

42.9

98

45.0

43

45.8

36

46.3

09

46.7

59

47.0

29

47.1

15

47.4

86

47.6

72

47.8

63

48.0

9248.3

75

49.0

97

50.0

35

50.1

68

50.2

99

50.5

86

50.7

27

51.9

29

52.1

30

52.2

15

52.7

81

54.5

63

55.4

13

55.9

62

56.4

73

56.5

99

58.1

82

58.3

70

58.6

24

59.2

25

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/25/2019 5:00:47 AM Sample Type : Essential Oil Sample Name : Tea Tree

Company Name : AD Practitioners, LLCLot# : 1C

Injection Volume : 0.30

Comments:

No adulteration or contamination was

detected in Tea tree ADP 1C.

Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

Peak Report TIC R.Time Name Area%

9.607 Hexenol <3Z> 0.04 13.131 Thujene <alpha-> 1.00 13.582 Pinene <alpha> 2.51 15.830 Sabinene 0.25 16.165 Pinene <beta-> 0.74 16.770 Myrcene 0.88 17.901 Phellandrene <alpha-> 0.53 18.646 Terpinene <alpha-> 9.94 19.093 Cymene <para-> 2.48 19.390 Limonene 0.97 19.509 Phellandrene <beta> 0.95 19.603 1,8-cineole 2.67 21.424 Terpinene<gamma-> 18.37 23.170 Terpinolene 3.55 23.453 Cymenene <para-> 0.06 24.063 Linalool 0.06 24.204 Sabinene hydrate <trans> 0.04 25.840 Menth-2-en-1-ol <cis-p> 0.25 27.102 Menth-2-en-1-ol <trans-p> 0.19 30.076 Terpinen-4-ol 39.72 30.212 Cymen-8-ol<para-> 0.07 30.856 Terpineol <alpha> 3.47 30.948 Piperitol<cis-> 0.07 31.728 Piperitol<trans-> 0.11 40.096 Elemene <delta> 0.03 41.087 Cubebene <alpha> 0.06 42.663 Isoledene 0.07 42.998 Copaene <alpha> 0.20 45.036 Maaliene <beta-> 0.40 45.837 Caryophyllene <trans> 0.40 46.308 Caryophyllene <9-epi-cis-> 0.07 46.762 Maaliene <alpha-> 0.08 47.031 Aromadendrene 1.45 47.230 Guaiene<alpha-> 0.06 47.480 Myltayl-4(12)-ene 0.21 47.672 Murrola-3,5-diene <trans-> 0.15 48.093 Humulene <alpha> 0.08 48.370 Alloaromadendrene 0.62 49.097 Cadina-1(6),4-diene<trans-> 0.44 50.038 Selinene <delta> 0.17 50.168 Selinene <beta-> 0.24 50.296 Viridiflorene 1.27 50.585 Bicyclogermacrene 0.94 50.728 Muurolene <alpha> 0.17 51.928 Cadinene <delta-> 1.41 52.125 Calamenene <trans> 0.14 52.209 Zonarene 0.32 52.780 Cadine-1,4-diene <trans-> 0.24 54.566 Viridifloral <isomer> 0.14 55.037 Palustrol 0.09 55.407 Spathulenol 0.10 55.965 Globulol 0.44 56.474 Viridiflorol 0.22 56.598 Cubeban-11-ol 0.18 57.067 Ledol 0.04 57.188 Rosifoliol 0.09 58.177 Eudesmol <isomer> 0.18 58.370 Cubenol<1-epi> 0.25 58.623 Spathulenol<iso-> 0.05 59.224 Cubenol 0.13

100.00

min

6,338,599

10.0 20.0 30.0 40.0 50.0 60.0

TIC

9.6

07

13.1

31

13.5

82

15.8

30

16.1

65

16.7

70

17.9

01

18.6

46

19.0

93

19.3

90

19.5

09

19.6

03

21.4

24

23.1

70

23.4

53

24.0

63

24.2

04

25.8

40

27.1

02

30.0

76

30.2

12

30.8

56

30.9

48

31.7

28

40.0

96

41.0

87

42.6

63

42.9

98

45.0

36

45.8

37

46.3

08

46.7

62

47.0

31

47.2

30

47.4

80

47.6

72

48.0

93 4

8.3

70

49.0

97

50.0

38

50.1

68

50.2

96

50.5

85

50.7

28

51.9

28

52.1

25

52.2

09

52.7

80

54.5

66

55.0

37

55.4

07

55.9

65

56.4

74

56.5

98

57.0

67

57.1

88

58.1

77

58.3

70

58.6

23

59.2

24

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/25/2019 3:03:06 AM Sample Type : Essential Oil Sample Name : Tea Tree

Company Name : AD Practitioners, LLCLot# : 2C

Injection Volume : 0.30

Comments:

No adulteration or contamination was

detected in Tea tree ADP 2C.

Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

Peak Report TIC R.Time Name Area% 13.123 Thujene <alpha-> 0.47 13.581 Pinene <alpha> 3.14 15.826 Sabinene 0.42 16.159 Pinene <beta-> 0.63 16.761 Myrcene 0.39 17.896 Phellandrene <alpha-> 0.35 18.439 1,4-Cineole 0.07 18.638 Terpinene <alpha-> 9.56 19.090 Cymene <para-> 3.07 19.382 Limonene 1.40 19.497 Phellandrene <beta> 0.58 19.584 1,8-cineole 1.03 20.445 Ocimene <E-beta> 0.17 21.416 Terpinene<gamma-> 18.16 22.104 Linalool oxide <cis-> (furanoid) 0.11 22.233 Pinol 0.05 23.160 Terpinolene 3.09 23.388 Fenchone 0.12 25.835 Menth-2-en-1-ol <cis-p> 0.14 27.000 Pinocarveol <trans-> 0.15 27.110 Menth-2-en-1-ol <trans-p> 0.11 27.579 Terpineol <cis-beta-> 0.08 30.067 Terpinen-4-ol 41.22 30.853 Terpineol <alpha> 3.68 31.724 Piperitol<trans-> 0.04 36.169 Ascaridol glycol <E> 0.04 39.323 4-isopropyl-6-methyl-3-cyclohexene-1,2-diol 0.04 42.993 Copaene <alpha> 0.17 45.032 Maaliene <beta-> 0.42 45.829 Caryophyllene <trans> 0.27 46.298 Caryophyllene <9-epi-cis-> 0.06 46.519 Gurjunene<beta-> 0.04 46.755 Maaliene <alpha-> 0.07 47.037 Aromadendrene 2.59 47.212 Guaiene<alpha-> 0.06 47.476 Selina5,11-diene 0.20 47.667 Muurola-3,5-diene<cis-> 0.11 47.855 Muurola-3,5-diene <trans> 0.06 48.088 Humulene <alpha> 0.06 48.361 Alloaromadendrene 0.59 49.093 Cadina-1(6),4-diene <cis-> 0.41 49.268 Cadina-1(6),4-diene <trans> 0.06 50.034 Selinene <delta> 0.15 50.162 Selinene <beta-> 0.55 50.297 Viridiflorene 1.57 50.572 Bicyclogermacrene 0.73 50.728 Muurolene <alpha> 0.17 51.914 Cadinene <delta-> 1.20 52.115 Calamenene <trans> 0.09 52.205 Zonarene 0.30 52.774 Cadine-1,4-diene <trans-> 0.19 54.553 Viridifloral <isomer> 0.10 55.404 Spathulenol 0.07 55.958 Globulol 0.57 56.467 Viridiflorol 0.22 56.592 Cubeban-11-ol 0.14 57.185 Rosifoliol 0.07 58.174 Eudesmol <isomer> 0.12 58.362 Cubenol<1-epi> 0.18 59.218 Cubenol 0.09

100.00

min

5,973,488

20.0 30.0 40.0 50.0 60.0

TIC

13.1

23

13.5

81

15.8

26

16.1

59

16.7

61

17.8

96

18.4

39

18.6

38

19.0

90

19.3

82

19.4

97

19.5

84

20.4

45

21.4

16

22.1

04

22.2

33

23.1

60

23.3

88

25.8

35

27.0

00

27.1

10

27.5

79

30.0

67

30.8

53

31.7

24

36.1

69

39.3

23

42.9

93

45.0

32

45.8

29

46.2

98

46.5

19

46.7

55

47.0

37

47.2

12

47.4

76

47.6

67

47.8

55

48.0

88 4

8.3

61

49.0

93

49.2

68

50.0

34

50.1

62

50.2

97

50.5

72

50.7

28

51.9

14

52.1

15

52.2

05

52.7

74

54.5

53

55.4

04 55.9

58

56.4

67

56.5

92

57.1

85

58.1

74

58.3

62

59.2

18

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/24/2019 9:17:38 PM Sample Type : Essential Oil Sample Name : Tea Tree

Company Name : AD Practitioners, LLCLot# : 3C

Injection Volume : 0.30

Comments:

No adulteration or contamination was

detected in Tea tree ADP 3C.

Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

Peak Report TIC R.Time Name Area%

9.600 Hexenol <3Z> 0.05 13.127 Thujene <alpha-> 0.90 13.577 Pinene <alpha> 2.19 15.825 Sabinene 0.29 16.160 Pinene <beta-> 0.68 16.764 Myrcene 0.80 17.896 Phellandrene <alpha-> 0.48 18.638 Terpinene <alpha-> 9.46 19.076 Cymene <para-> 2.17 19.378 Limonene 0.83 19.499 Phellandrene <beta> 0.92 19.592 1,8-cineole 2.07 21.413 Terpinene<gamma-> 17.61 23.166 Terpinolene 3.47 23.449 Cymenene <para-> 0.05 24.061 Linalool 0.05 24.197 Sabinene hydrate <trans> 0.05 25.838 Menth-2-en-1-ol <cis-p> 0.41 27.100 Menth-2-en-1-ol <trans-p> 0.30 30.078 Terpinen-4-ol 41.01 30.855 Terpineol <alpha> 3.68 30.947 Piperitol<cis-> 0.11 31.728 Piperitol<trans-> 0.19 40.093 Elemene <delta> 0.06 41.084 Cubebene <alpha> 0.06 42.655 Isoledene 0.07 42.994 Copaene <alpha> 0.19 45.033 Maaliene <beta-> 0.42 45.833 Caryophyllene <trans> 0.39 46.302 Caryophyllene <9-epi-cis-> 0.07 46.758 Maaliene <alpha-> 0.08 47.021 Aromadendrene 1.34 47.215 Guaiene<alpha-> 0.06 47.475 Myltayl-4(12)-ene 0.19 47.670 Murrola-3,5-diene <trans-> 0.17 48.089 Humulene <alpha> 0.08 48.370 Alloaromadendrene 0.64 49.094 Cadina-1(6),4-diene<trans-> 0.49 50.037 Selinene <delta> 0.16 50.165 Selinene <beta-> 0.23 50.296 Viridiflorene 1.32 50.581 Bicyclogermacrene 1.38 50.724 Muurolene <alpha> 0.19 51.927 Cadinene <delta-> 1.58 52.125 Calamenene <trans> 0.14 52.208 Zonarene 0.37 52.778 Cadine-1,4-diene <trans-> 0.26 54.559 Viridifloral <isomer> 0.14 55.049 Palustrol 0.12 55.408 Spathulenol 0.10 55.960 Globulol 0.48 56.468 Viridiflorol 0.26 56.593 Cubeban-11-ol 0.21 57.064 Ledol 0.06 57.186 Rosifoliol 0.10 58.175 Eudesmol <isomer> 0.20 58.367 Cubenol<1-epi> 0.31 58.624 Spathulenol<iso-> 0.08 59.222 Cubenol 0.16 59.415 Cadinol <delta> 0.05

100.00

min

5,907,133

10.0 20.0 30.0 40.0 50.0 60.0

TIC

9.6

00

13.1

27

13.5

77

15.8

25 1

6.1

60

16.7

64

17.8

96

18.6

38

19.0

76

19.3

78

19.4

99

19.5

92

21.4

13

23.1

66

23.4

49

24.0

61

24.1

97

25.8

38

27.1

00

30.0

78

30.8

55

30.9

47

31.7

28

40.0

93

41.0

84

42.6

55

42.9

94

45.0

33

45.8

33

46.3

02

46.7

58

47.0

21

47.2

15

47.4

75

47.6

70

48.0

89 4

8.3

70

49.0

94

50.0

37

50.1

65

50.2

96

50.5

81

50.7

24

51.9

27

52.1

25

52.2

08

52.7

78

54.5

59

55.0

49

55.4

08

55.9

60

56.4

68

56.5

93

57.0

64

57.1

86

58.1

75

58.3

67

58.6

24

59.2

22

59.4

15

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/24/2019 7:19:52 PM Sample Type : Essential Oil Sample Name : Tea Tree

Company Name : AD Practitioners, LLCLot# : 4C

Injection Volume : 0.30

Comments:

No adulteration or contamination was

detected in Tea tree ADP 4C.

Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

Peak Report TIC R.Time Name Area% 13.129 Thujene <alpha-> 0.94 13.580 Pinene <alpha> 2.40 15.827 Sabinene 0.12 16.163 Pinene <beta-> 0.70 16.767 Myrcene 0.79 17.901 Phellandrene <alpha-> 0.50 18.640 Terpinene <alpha-> 9.09 19.089 Cymene <para-> 2.63 19.386 Limonene 0.98 19.506 Phellandrene <beta> 0.89 19.604 1,8-cineole 3.07 21.417 Terpinene<gamma-> 17.63 23.168 Terpinolene 3.40 23.455 Cymenene <para-> 0.07 24.065 Linalool 0.05 25.839 Menth-2-en-1-ol <cis-p> 0.19 27.102 Menth-2-en-1-ol <trans-p> 0.15 30.065 Terpinen-4-ol 38.63 30.209 Cymen-8-ol<para-> 0.07 30.850 Terpineol <alpha> 3.29 30.946 Piperitol<cis-> 0.05 31.727 Piperitol<trans-> 0.10 36.179 Ascaridol glycol <E> 0.05 39.335 4-isopropyl-6-methyl-3-cyclohexene-1,2-diol 0.05 41.092 Cubebene <alpha> 0.06 42.667 Isoledene 0.09 43.005 Copaene <alpha> 0.27 45.045 Maaliene <beta-> 0.54 45.840 Caryophyllene <trans> 0.61 46.310 Caryophyllene <9-epi-cis-> 0.09 46.765 Maaliene <alpha-> 0.11 47.035 Aromadendrene 1.92 47.224 Guaiene<alpha-> 0.08 47.487 Myltayl-4(12)-ene 0.27 47.675 Murrola-3,5-diene <cis-> 0.18 47.862 Muurola-3,5-diene <trans> 0.06 48.092 Humulene <alpha> 0.11 48.376 Alloaromadendrene 0.79 49.104 Cadina-1(6),4-diene<trans-> 0.62 50.040 Selinene <delta> 0.23 50.171 Guaia-1(10),11-diene 0.32 50.305 Viridiflorene 1.60 50.580 Bicyclogermacrene 0.92 50.730 Muurolene <alpha> 0.24 51.937 Cadinene <delta-> 1.82 52.132 Calamenene <trans> 0.18 52.216 Zonarene 0.45 52.784 Cadine-1,4-diene <trans-> 0.32 54.567 Viridifloral <isomer> 0.17 55.026 Maaliol 0.12 55.410 Spathulenol 0.13 55.968 Globulol 0.53 56.474 Viridiflorol 0.24 56.597 Cubeban-11-ol 0.21 57.074 Ledol 0.05 57.195 Rosifoliol 0.12 58.180 Eudesmol <isomer> 0.21 58.372 Cubenol<1-epi> 0.30 58.626 Spathulenol<iso-> 0.07 59.226 Cubenol 0.15

100.00

min

5,697,866

20.0 30.0 40.0 50.0 60.0

TIC

13.1

29

13.5

80

15.8

27

16.1

63

16.7

67

17.9

01

18.6

40

19.0

89

19.3

86

19.5

06

19.6

04

21.4

17

23.1

68

23.4

55

24.0

65

25.8

39

27.1

02

30.0

65

30.2

09

30.8

50

30.9

46

31.7

27

36.1

79

39.3

35

41.0

92

42.6

67

43.0

05

45.0

45

45.8

40

46.3

10

46.7

65

47.0

35

47.2

24

47.4

87

47.6

75

47.8

62

48.0

92

48.3

76

49.1

04

50.0

40

50.1

71

50.3

05

50.5

80

50.7

30

51.9

37

52.1

32

52.2

16

52.7

84

54.5

67

55.0

26

55.4

10

55.9

68

56.4

74

56.5

97

57.0

74

57.1

95

58.1

80

58.3

72

58.6

26

59.2

26

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/24/2019 5:22:02 PM Sample Type : Essential Oil Sample Name : Tea Tree

Company Name : AD Practitioners, LLCLot# : 5C

Injection Volume : 0.30

Comments:

No adulteration or contamination was

detected in Tea tree ADP 5C.

Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

Peak Report TIC R.Time Name Area% 12.096 Thujene <alpha-> 0.89 12.514 Pinene <alpha> 2.23 14.702 Sabinene 1.83 15.009 Pinene <beta-> 0.68 15.619 Myrcene 0.72 16.712 Phellandrene <alpha-> 0.83 17.234 Cineole<1,4-> 0.03 17.397 Terpinene <alpha-> 10.69 17.879 Cymene<para-> 1.39 18.151 Limonene 0.87 18.275 Phellandrene <beta> 1.25 18.352 1,8-cineole 3.56 20.099 Terpinene <gamma> 18.43 20.857 Sabinene hydrate<cis-> 0.08 21.844 Terpinolene 3.37 22.240 Cymenene<para-> 0.03 22.825 Linalool 0.05 22.939 Sabinene hydrate <trans> 0.21 24.557 Menth-2-en-1-ol <cis-p> 0.30 25.810 Menth-2-en-1-ol <trans-p> 0.20 28.639 Terpinen-4-ol 38.31 29.524 Terpineol <alpha> 3.15 30.438 Piperitol<trans-> 0.09 36.150 Ascaridol glycol <E> 0.01 38.097 4-isopropyl-6-methyl-3-cyclohexene-1,2-diol 0.01 38.621 Bicylcoelemene 0.15 39.621 Cubebene <alpha> 0.09 41.176 Ylangene <alpha> 0.06 41.523 Copaene<alpha-> 0.20 42.424 Elemene <beta> 0.08 43.543 Gurjunene <alpha-> 0.34 43.808 Maaliene <beta-> 0.03 44.355 Caryophyllene <trans> 0.49 44.831 Caryophyllene <9-epi-cis-> 0.07 45.273 Maaliene <alpha-> 0.08 45.552 Aromadendrene 1.06 45.765 Guaiene<alpha-> 0.06 46.018 Myltayl-4(12)-ene 0.18 46.218 Murrola-3,5-diene <cis-> 0.27 46.409 Muurola-3,5-diene <trans> 0.05 46.631 Humulene <alpha-> 0.10 46.902 Aromadendrene allo 0.56 47.651 Cadina-1(6),4-diene<cis-> 0.48 47.840 Cadina-1(6),4-diene <trans-> 0.04 48.584 Selinene <delta> 0.11 48.714 Guaia-1(10),11-diene 0.14 48.839 Viridiflorene 1.13 49.129 Bicyclogermacrene 2.12 49.308 Muurolene <alpha> 0.20 50.495 Cadinene <delta-> 1.35 50.773 Zonarene 0.31 51.370 Cadine-1,4-diene <trans-> 0.23 53.148 Viridifloral <isomer> 0.06 53.635 Palustrol 0.04 54.035 Spathulenol 0.04 54.563 Globulol 0.21 55.072 Viridiflorol 0.10 55.206 Cubeban-11-ol 0.07 55.798 Rosifoliol 0.04 56.785 Eudesmol <isomer> 0.06 56.984 Cubenol<1-epi-> 0.13 57.842 Cubenol 0.06

100.00

min

5,039,090

20.0 30.0 40.0 50.0 59.0

TIC

12.0

96

12.5

14

14.7

02

15.0

09

15.6

19

16.7

12

17.2

34

17.3

97

17.8

79

18.1

51

18.2

75

18.3

52

20.0

99

20.8

57

21.8

44

22.2

40

22.8

25

22.9

39

24.5

57

25.8

10

28.6

39

29.5

24

30.4

38

36.1

50

38.0

97

38.6

21

39.6

21

41.1

76

41.5

23

42.4

24

43.5

43

43.8

08

44.3

55

44.8

31

45.2

73 4

5.5

52

45.7

65

46.0

18

46.2

18

46.4

09

46.6

31

46.9

02

47.6

51

47.8

40

48.5

84

48.7

14 4

8.8

39

49.1

29

49.3

08

50.4

95

50.7

73

51.3

70

53.1

48

53.6

35

54.0

35

54.5

63

55.0

72

55.2

06

55.7

98

56.7

85

56.9

84

57.8

42

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/24/2019 12:33:54 AM Sample Type : Essential Oil Sample Name : Tea tree

Company Name : AD Practitioners, LLCLot# : 6C

Injection Volume : 0.20

Comments: Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

No adulteration or contamination was detected in Tea tree ADP 6C.

Peak Report TIC R.Time Name Area% 12.085 Thujene <alpha-> 0.88 12.502 Pinene<alpha-> 2.51 14.689 Sabinene 0.04 14.997 Pinene <beta-> 0.65 15.370 Pinane<trans> 0.00 15.605 Myrcene 0.70 16.700 Phellandrene<alpha-> 0.36 17.224 1,4-Cineole 0.02 17.378 Terpinene <alpha-> 8.65 17.873 Cymene<para-> 3.92 18.139 Limonene 0.92 18.263 Phellandrene <beta> 0.56 18.339 1,8-cineole 2.85 20.090 Terpinene<gamma-> 20.18 21.832 Terpinolene 3.07 22.221 Cymenene<para-> 0.06 22.817 Linalool 0.05 24.550 Menth-2-en-1-ol <cis-p> 0.09 25.804 Menth-2-en-1-ol <trans-p> 0.08 28.637 Terpinen-4-ol 43.00 28.954 Cymen-8-ol<para-> 0.04 29.321 Cineole <1,4 hydroxy> 0.08 29.514 Terpineol <alpha> 3.19 30.435 Piperitol<trans-> 0.07 34.932 Ascaridol glycol<trans-> 0.07 36.129 Ascaridol glycol <cis-> 0.05 38.074 4-isopropyl-6-methyl-3-cyclohexene-1,2-diol 0.10 39.615 Cubebene<alpha-> 0.03 41.170 Ylangene <alpha-> 0.07 41.516 Copaene<alpha-> 0.17 43.538 Gurjunene <alpha-> 0.30 44.352 Caryophyllene <trans> 0.31 44.824 Caryophyllene <9-epi-cis-> 0.06 45.270 Maaliene <alpha-> 0.07 45.552 Aromadendrene 1.21 45.756 Guaiene<alpha-> 0.05 46.009 Myltayl-4(12)-ene 0.16 46.208 Muurola-3,5-diene<trans-> 0.06 46.627 Humulene<alpha-> 0.06 46.897 Aromadendrene allo 0.49 47.647 Cadina-1(6),4-diene<cis-> 0.27 48.577 Selinene <delta> 0.10 48.715 Guaia-1(10),11-diene 0.18 48.829 Viridiflorene 1.01 49.126 Bicyclogermacrene 0.28 49.304 Muurolene <alpha> 0.13 50.486 Cadinene <delta> 0.99 50.758 Zonarene 0.38 51.368 Cadine-1,4-diene <trans-> 0.17 53.152 Viridifloral <isomer> 0.07 53.639 Palustrol 0.06 54.023 Spathulenol 0.08 54.557 Globulol 0.30 55.065 Viridiflorol 0.16 55.199 Cubeban-11-ol 0.12 55.665 Ledol 0.02 55.796 Rosifoliol 0.05 56.779 Eudesmol <isomer> 0.13 56.982 Cubenol<1-epi-> 0.17 57.252 Spathulenol<iso-> 0.03 57.831 Cubenol 0.06

100.00

min

4,958,739

20.0 30.0 40.0 50.0 59.0

TIC

12.0

85

12.5

02

14.6

89 1

4.9

97

15.3

70 1

5.6

05

16.7

00

17.2

24

17.3

78

17.8

73

18.1

39

18.2

63

18.3

39

20.0

90

21.8

32

22.2

21

22.8

17

24.5

50

25.8

04

28.6

37

28.9

54

29.3

21

29.5

14

30.4

35

34.9

32

36.1

29

38.0

74

39.6

15

41.1

70

41.5

16

43.5

38

44.3

52

44.8

24

45.2

70

45.5

52

45.7

56

46.0

09

46.2

08

46.6

27

46.8

97

47.6

47

48.5

77

48.7

15 48.8

29

49.1

26

49.3

04 5

0.4

86

50.7

58

51.3

68

53.1

52

53.6

39

54.0

23

54.5

57

55.0

65

55.1

99

55.6

65

55.7

96

56.7

79

56.9

82

57.2

52

57.8

31

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/24/2019 2:29:40 AM Sample Type : Essential Oil Sample Name : Tea tree

Company Name : AD Practitioners, LLCLot# : 7C

Injection Volume : 0.20

Comments: Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

No adulteration or contamination was detected in Tea tree ADP 7C.

Peak Report TIC R.Time Name Area% 12.080 Thujene <alpha-> 0.91 12.496 Pinene<alpha-> 2.22 14.682 Sabinene 0.43 14.990 Pinene<beta-> 0.65 15.600 Myrcene 0.75 16.692 Phellandrene<alpha-> 0.53 17.218 1,4-Cineole 0.02 17.377 Terpinene <alpha-> 10.35 17.861 Cymene<para-> 1.83 18.132 Limonene 0.78 18.255 Phellandrene <beta> 0.91 18.331 1,8-cineole 2.34 20.085 Terpinene<gamma-> 19.82 20.841 Sabinene hydrate<cis-> 0.03 21.828 Terpinolene 3.33 22.218 Cymenene<para-> 0.04 22.809 Linalool 0.05 22.926 Sabinene hydrate <trans> 0.07 24.540 Menth-2-en-1-ol<cis-para-> 0.27 25.799 Menth-2-en-1ol<trans-para-> 0.20 28.639 Terpinen-4-ol 43.85 29.512 Terpineol <alpha> 3.31 30.424 Piperitol<trans-> 0.10 33.553 Piperitone 0.03 38.081 4-isopropyl-6-methyl-3-cyclohexene-1,2-diol 0.01 38.609 Bicylcoelemene 0.05 39.608 Cubebene<alpha-> 0.05 41.158 Ledene <iso> 0.04 41.511 Copaene<alpha-> 0.13 42.417 Elemene<beta-> 0.03 43.530 Gurjunene <alpha-> 0.26 44.344 Caryophyllene <trans> 0.28 44.819 Caryophyllene <9-epi-cis-> 0.04 45.261 Maaliene <alpha-> 0.05 45.540 Aromadendrene 0.88 45.754 Guaiene<alpha-> 0.04 46.003 Myltayl-4(12)-ene 0.13 46.204 Muurola-3,5-diene<cis-> 0.11 46.396 Muurola-3,5-diene <trans> 0.02 46.621 Humulene<alpha-> 0.06 46.890 Aromadendrene allo 0.41 47.642 Cadina-1(6),4-diene<cis-> 0.30 47.828 Cadina-1(6),4-diene <trans-> 0.02 48.571 Selinene <delta> 0.09 48.704 Selinene <beta-> 0.13 48.822 Viridiflorene 0.86 49.115 Bicyclogermacrene 0.95 49.296 Muurolene <alpha> 0.12 50.480 Cadinene <delta-> 0.94 50.761 Zonarene 0.28 51.361 Cadine-1,4-diene <trans-> 0.16 53.139 Viridifloral <isomer> 0.05 53.621 Palustrol 0.04 54.020 Spathulenol 0.04 54.551 Globulol 0.18 55.058 Viridiflorol 0.09 55.196 Cubeban-11-ol 0.07 55.794 Rosifoliol 0.03 56.772 Eudesmol <isomer> 0.07 56.974 Cubenol<1-epi-> 0.10 57.823 Cubenol 0.05

100.00

min

5,109,384

20.0 30.0 40.0 50.0 59.0

TIC

12.0

80

12.4

96

14.6

82

14.9

90

15.6

00

16.6

92

17.2

18

17.3

77

17.8

61

18.1

32

18.2

55

18.3

31

20.0

85

20.8

41

21.8

28

22.2

18

22.8

09

22.9

26

24.5

40

25.7

99

28.6

39

29.5

12

30.4

24

33.5

53

38.0

81

38.6

09

39.6

08

41.1

58

41.5

11

42.4

17

43.5

30

44.3

44

44.8

19

45.2

61 45.5

40

45.7

54

46.0

03

46.2

04

46.3

96

46.6

21

46.8

90

47.6

42

47.8

28

48.5

71

48.7

04

48.8

22

49.1

15

49.2

96 50.4

80

50.7

61

51.3

61

53.1

39

53.6

21

54.0

20

54.5

51

55.0

58

55.1

96

55.7

94

56.7

72

56.9

74

57.8

23

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/24/2019 4:25:16 AM Sample Type : Essential Oil Sample Name : Tea tree

Company Name : AD Practitioners, LLCLot# : 8C

Injection Volume : 0.20

Comments: Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

No adulteration or contamination was detected in Tea tree ADP 8C.

Peak Report TIC R.Time Name Area% 12.077 Thujene<alpha-> 0.94 12.494 Pinene<alpha-> 2.26 14.679 Sabinene 0.47 14.987 Pinene<beta-> 0.67 15.365 Menthene<3-p-> 0.00 15.598 Myrcene 0.74 16.690 Phellandrene<alpha-> 0.58 17.372 Terpinene <alpha-> 10.28 17.857 Cymene<para-> 1.89 18.128 Limonene 0.77 18.251 Phellandrene <beta> 1.00 18.328 1,8-cineole 2.29 20.079 Terpinene<gamma-> 19.64 20.837 Sabinene hydrate<cis-> 0.07 21.823 Terpinolene 3.36 22.215 Cymenene<para-> 0.04 22.807 Linalool 0.05 22.921 Sabinene hydrate<trans-> 0.13 24.535 Menth-2-en-1-ol<cis-para-> 0.25 25.791 Menth-2-en-1ol<trans-para-> 0.19 28.622 Terpinen-4-ol 42.52 29.504 Terpineol <alpha-> 3.45 30.421 Piperitol<trans-> 0.12 34.925 Ascaridol glycol <E> 0.05 38.069 4-isopropyl-6-methyl-3-cyclohexene-1,2-diol 0.05 38.604 Bicylcoelemene 0.07 39.604 Cubebene<alpha-> 0.05 41.156 Ylangene <alpha-> 0.06 41.505 Copaene<alpha-> 0.15 42.407 Elemene <beta> 0.03 43.523 Gurjunene <alpha-> 0.30 44.341 Caryophyllene <trans> 0.33 44.813 Caryophyllene <9-epi-cis-> 0.06 45.257 Maaliene <alpha-> 0.07 45.535 Aromadendrene 1.00 45.746 Guaiene<alpha-> 0.05 45.997 Myltayl-4(12)-ene 0.15 46.197 Muurola-3,5-diene<cis-> 0.15 46.392 Muurola-3,5-diene <trans> 0.04 46.615 Humulene<alpha-> 0.06 46.884 Aromadendrene allo 0.48 47.634 Cadina-1(6),4-diene<cis-> 0.34 48.570 Selinene <delta> 0.10 48.708 Selinene <beta-> 0.15 48.816 Viridiflorene 1.04 49.110 Bicyclogermacrene 1.07 49.289 Muurolene<alpha-> 0.13 50.476 Cadinene <delta-> 1.04 50.752 Zonarene 0.30 51.355 Cadine-1,4-diene <trans-> 0.17 53.142 Viridifloral <isomer> 0.06 53.623 Palustrol 0.04 54.012 Spathulenol 0.04 54.546 Globulol 0.18 55.053 Viridiflorol 0.10 55.189 Cubeban-11-ol 0.07 55.782 Rosifoliol 0.03 56.770 Eudesmol <isomer> 0.06 56.969 Cubenol<1-epi-> 0.11 57.247 Spathulenol<iso-> 0.06 57.817 Cubenol 0.05

100.00

min

4,758,266

20.0 30.0 40.0 50.0 59.0

TIC

12.0

77

12.4

94

14.6

79

14.9

87

15.3

65

15.5

98

16.6

90

17.3

72

17.8

57

18.1

28

18.2

51

18.3

28

20.0

79

20.8

37

21.8

23

22.2

15

22.8

07

22.9

21

24.5

35

25.7

91

28.6

22

29.5

04

30.4

21

34.9

25

38.0

69

38.6

04

39.6

04

41.1

56

41.5

05

42.4

07

43.5

23

44.3

41

44.8

13

45.2

57 45.5

35

45.7

46

45.9

97

46.1

97

46.3

92

46.6

15

46.8

84

47.6

34

48.5

70

48.7

08 48.8

16

49.1

10

49.2

89 5

0.4

76

50.7

52

51.3

55

53.1

42

53.6

23

54.0

12

54.5

46

55.0

53

55.1

89

55.7

82

56.7

70

56.9

69

57.2

47

57.8

17

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/24/2019 6:20:59 AM Sample Type : Essential Oil Sample Name : Tea tree

Company Name : AD Practitioners, LLCLot# : 9C

Injection Volume : 0.20

Comments: Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

No adulteration or contamination was detected in Tea tree ADP 9C.

Peak Report TIC R.Time Name Area% 12.074 Thujene<alpha-> 0.77 12.490 Pinene<alpha-> 2.33 14.674 Sabinene 0.28 14.984 Pinene<beta-> 0.61 15.594 Myrcene 0.62 16.685 Phellandrene<alpha-> 0.47 17.366 Terpinene <alpha-> 9.14 17.855 Cymene<para-> 2.06 18.126 Limonene 0.89 18.246 Phellandrene <beta> 0.75 18.323 1,8-cineole 2.53 19.206 Ocimene<(E)-beta-> 0.04 20.079 Terpinene<gamma-> 20.17 21.820 Terpinolene 3.51 22.209 Cymenene<para-> 0.05 22.801 Linalool 0.05 22.921 Sabinene hydrate <trans> 0.04 24.532 Menth-2-en-1-ol <cis-p> 0.17 25.788 Menth-2-en-1ol<trans-para-> 0.12 28.618 Terpinen-4-ol 41.19 29.498 Terpineol <alpha-> 3.05 30.416 Piperitol<trans-> 0.05 38.593 Elemene <delta> 0.06 39.599 Cubebene<alpha-> 0.06 41.151 Ylangene <alpha-> 0.08 41.500 Copaene<alpha-> 0.24 41.707 Isoledene 0.04 42.402 Elemene<beta-> 0.03 43.520 Gurjunene <alpha-> 0.45 43.933 Longifolene 0.04 44.336 Caryophyllene <trans-> 0.56 44.807 Caryophyllene <9-epi-cis-> 0.08 45.249 Maaliene <alpha-> 0.09 45.532 Aromadendrene 1.63 45.741 Guaiene<alpha-> 0.08 45.994 Selina5,11-diene 0.24 46.193 Murrola-3,5-diene <cis-> 0.17 46.390 Muurola-3,5-diene <trans> 0.04 46.609 Humulene<alpha-> 0.11 46.878 Aromadendrene allo 0.64 47.631 Cadina-1(6),4-diene<cis-> 0.52 47.818 Cadina-1(6),4-diene <trans-> 0.04 48.565 Selinene <delta> 0.15 48.699 Selinene <beta-> 0.20 48.812 Viridiflorene 1.27 49.104 Bicyclogermacrene 0.95 49.285 Muurolene <alpha> 0.18 50.472 Cadinene <delta-> 1.33 50.751 Zonarene 0.45 51.348 Cadine-1,4-diene <trans-> 0.23 53.132 Viridifloral <isomer> 0.10 53.619 Palustrol 0.06 54.008 Spathulenol 0.05 54.542 Globulol 0.29 55.048 Viridiflorol 0.13 55.183 Cubeban-11-ol 0.12 55.781 Rosifoliol 0.06 56.763 Eudesmol <isomer> 0.11 56.963 Cubenol<1-epi-> 0.16 57.814 Cubenol 0.07

100.00

min

4,788,720

20.0 30.0 40.0 50.0 59.0

TIC

12.0

74

12.4

90

14.6

74

14.9

84

15.5

94

16.6

85

17.3

66

17.8

55

18.1

26

18.2

46

18.3

23

19.2

06

20.0

79

21.8

20

22.2

09

22.8

01

22.9

21

24.5

32

25.7

88

28.6

18

29.4

98

30.4

16

38.5

93

39.5

99

41.1

51

41.5

00

41.7

07

42.4

02

43.5

20

43.9

33

44.3

36

44.8

07

45.2

49

45.5

32

45.7

41

45.9

94

46.1

93

46.3

90

46.6

09

46.8

78

47.6

31

47.8

18

48.5

65

48.6

9948.8

12

49.1

04

49.2

85

50.4

72

50.7

51

51.3

48

53.1

32

53.6

19

54.0

08

54.5

42

55.0

48

55.1

83

55.7

81

56.7

63

56.9

63

57.8

14

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/24/2019 8:16:45 AM Sample Type : Essential Oil Sample Name : Tea tree

Company Name : AD Practitioners, LLCLot# : 10C

Injection Volume : 0.20

Comments:

No adulteration or contamination was

detected in Tea tree ADP 10C.

Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel

Peak Report TIC R.Time Name Area% 12.071 Thujene<alpha-> 0.51 12.489 Pinene<alpha-> 2.43 14.672 Sabinene 0.62 14.982 Pinene<beta-> 0.67 15.591 Myrcene 0.37 16.684 Phellandrene<alpha-> 0.26 17.208 Cineole<1,4-> 0.02 17.366 Terpinene <alpha-> 9.49 17.855 Cymene<para-> 2.78 18.125 Limonene 1.19 18.245 Phellandrene <beta> 0.37 18.325 Cineole<1,8-> 3.21 20.074 Terpinene<gamma-> 18.68 20.825 Linalool oxide <cis-(furanoid)> 0.22 20.956 Pinol 0.06 21.817 Terpinolene 3.29 22.201 Cymenene<para-> 0.09 22.799 Linalool 0.05 22.913 Sabinene hydrate<trans-> 0.09 24.529 Menth-2-en-1-ol<cis-para-> 0.19 25.786 Menth-2-en-1-ol <trans-p> 0.15 26.291 Terpineol <cis-beta-> 0.06 28.630 Terpinen-4-ol 43.45 29.502 Terpineol<alpha-> 3.19 30.415 Piperitol<trans-> 0.06 34.911 Ascaridol glycol<trans-> 0.06 36.110 Ascaridol glycol <cis-> 0.03 38.057 4-isopropyl-6-methyl-3-cyclohexene-1,2-diol 0.08 41.150 Ylangene<alpha-> 0.04 41.496 Copaene<alpha-> 0.10 43.519 Gurjunene <alpha-> 0.33 44.331 Caryophyllene <trans-> 0.13 44.800 Caryophyllene <9-epi-cis-> 0.03 45.252 Maaliene <alpha-> 0.04 45.532 Aromadendrene 1.82 45.736 Guaiene<alpha-> 0.05 45.991 Selina5,11-diene 0.16 46.188 Muurola-3,5-diene<cis-> 0.06 46.879 Aromadendrene allo 0.32 47.630 Cadina-1(6),4-diene<cis-> 0.20 48.568 Selinene <delta> 0.08 48.696 Selinene <beta-> 0.31 48.816 Viridiflorene 1.34 49.103 Bicyclogermacrene 0.65 49.286 Muurolene <alpha> 0.11 50.465 Cadinene <delta> 0.62 50.746 Zonarene 0.18 51.343 Cadine-1,4-diene <trans-> 0.11 53.133 Viridifloral <isomer> 0.11 53.606 Palustrol 0.06 54.004 Spathulenol 0.13 54.538 Globulol 0.53 55.045 Viridiflorol 0.20 55.181 Cubeban-11-ol 0.16 55.775 Rosifoliol 0.08 56.758 Eudesmol <isomer> 0.14 56.960 Cubenol<1-epi-> 0.14 57.240 Spathulenol<iso-> 0.04 57.810 Cadin-4-en-7-ol <cis> 0.05

100.00

min

5,140,186

20.0 30.0 40.0 50.0 59.0

TIC

12.0

71

12.4

89

14.6

72

14.9

82

15.5

91

16.6

84

17.2

08

17.3

66

17.8

55

18.1

25

18.2

45

18.3

25

20.0

74

20.8

25

20.9

56

21.8

17

22.2

01

22.7

99

22.9

13

24.5

29

25.7

86

26.2

91

28.6

30

29.5

02

30.4

15

34.9

11

36.1

10

38.0

57

41.1

50

41.4

96

43.5

19

44.3

31

44.8

00

45.2

52

45.5

32

45.7

36

45.9

91

46.1

88

46.8

79

47.6

30

48.5

68

48.6

9648.8

16

49.1

03

49.2

86

50.4

65

50.7

46

51.3

43

53.1

33

53.6

06

54.0

04

54.5

38

55.0

45

55.1

81

55.7

75

56.7

58

56.9

60

57.2

40

57.8

10

Sample Information Analyzed by : Dr. Prabodh Satyal

Analyzed : 5/24/2019 10:12:31 AM Sample Type : Essential Oil Sample Name : Tea tree

Company Name : AD Practitioners, LLCLot# : 11C

Injection Volume : 0.20

Comments:

No adulteration or contamination was

detected in Tea tree ADP 11C.

Copyright © 2019 by Aromatic Plant Research Center (APRC). All rights reserved. The information contained in this document may not be used, published or redistributed, including online, without the prior written consent of APRC.

Reviewed by: Ambika Poudel