evaluation of the tensile and elastic properties of …
TRANSCRIPT
S. Tarancón1 | E. Tejado1 | M. Richou2 | J.Y. Pastor1
Presenting author: Elena Tejado, Ph.D.
1 Dpto. Ciencia de Materiales-CIME, Universidad Politécnica de Madrid, Spain
EVALUATION OF THE TENSILE AND ELASTIC PROPERTIES OF W/CU COATINGS FOR ITS APPLICATION TO THE FGM DEMO DIVERTOR CONCEPT
1. Cold-spray graded coatings demonstrated valid for the joint of W to Cu infuture DEMO divertor mockups
2. Tensile tests on single-coatings: revealed elastic behaviour up to fracture andhigh strength values; decohesion of W particles (intergranular fracture between Wgrains) with plastic deformation of the surrounding Cu matrix
3. New method has been followed to measure E through RFA on coating-substratesystems and these results are in agreement with both nE and Young modulusobtained from the σ-ε curves.
FindingsITER based conceptual design of EU-DEMO divertorenvisages W monoblocks as plasma-facing material joinedto a CuCrZr cooling tube with a thick Cu-OHFC interlayer.
Since divertor configuration will define the power exhaustcapabilities of the reactor, additional concepts have beendeveloped within the EUROfusion WPDIV project. TheFunctionally Graded Material (FGM) concept is one of theproposed alternatives.
Solution: replacement with a W to Cu compositionally graded thin film to reduce stresses at the interfaces
2 CEA, IRFM, F-13108 Saint-Paul-Lez-Durance, France
20-25 SEPTEMBER 2020 VIRTUAL EDITION31ST SYMPOSIUM ON FUSION TECHNOLOGY
Problem: armour-to-pipe W to Cu joint (non miscible, large CTE and E mismatch, need for a flexible technique to join tubes…)
40 µm
0 %W
40 µm
25 %W
40 µm
50 %W
40 µm
75 %W
ITER W armoured monoblock geometry at the inner and outer vertical targets
100 %W
100 %Cu
Particle size: 5-50 µm N2 atmosphere Pressure: 10-50 Bar T: 1000 °C
Φ < 4 %
Cold-Spray W/Cu coatings
Fractographic SE+EDX map of the tensile samples, W particles are in green, the Cu matrix in red
Real Strain obtained through DIC (Digital Image Correlation)
Loading rate 10 μm/minCoatings thickness: 260 μm
Linear elastic up to fracture ↑σs→ ↑vol%W except for:
Cu-75W: considerably lower vol%W than expected (≈ 48% lower)
Fracture surfaces: Strong adhesion Cu-W Ductile dimples of Cu matrix
while W particles remain intact
0 %W
20 µm 20 µm
25 %W
20 µm
50 %W
20 µm
75 %W
2 Tensile properties
Acknowledgements• This work has been carried out within the framework of the EUROfusion Consortium
and has received funding from the Euratom research and training programme 2014–2018 and 2019–2020 under grant agreement No 633053. The views and opinionsexpressed herein do not necessarily reflect those of the European Commission.
• The authors would also like to acknowledge the Ministerio de Economía yCompetitividad of Spain (MAT2015-70780-C4-4-P), the Comunidad de Madrid(S2018/NMT-4411 ADITIMAT-CM) and, especially, the Universidad Politécnica deMadrid in the line of action for encouraging research from young doctors (projectM190020074EMTG, COAT4FUSION) for funding this research.
L. Chandra and T. W. Clyne; Use of an ultrasonic resonance technique to measure
the in-plane Young’s Modulus of thin diamond films deposited by a DC plasma JET. J. Mat.
Letts. June 1992
ANEX: Measurement of ERFA of W/Cu coatings on the substrate:
1 Overview 3 Elastic properties
Real stress-strain curves of W/Cu coatings after tensile testing of the isolated coatings and DIC analysis (left) and the Ultimate tensile strength (right) as a function of W content. Tests performed at room temperature
Elastic modulus (otp left) and hardness (bottom right) as a function of W content of W/Cu coatings
Up to 50 %Cu: H with Cu Indentation size effect Lower standard error of
Vickers Hardness (as compared to Instrumented Indentation (75 mN and 0.5 N), where each phase is tested independently
3 different techniques to measure Young Modulus: Agreement among
obtained values, although nE>EIET>ETRAC
Macroscopic values of E can be obtained via RFA in coatings over substrate systems
Coatingsmanufacturingconditions
Functionally Graded Material (FGM) monoblock concept