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Page 1: February 3, 2018 - Virginia Tech...Data_18B0052 ARI ID Client ID Proj ID Matrix Sampled Rec Prep Analyzed Method CAS Compound Value Q Units 18B0052-01 WUFF-IN 13-05605-000 Water 02/03/2018

February 3, 2018

Page 2: February 3, 2018 - Virginia Tech...Data_18B0052 ARI ID Client ID Proj ID Matrix Sampled Rec Prep Analyzed Method CAS Compound Value Q Units 18B0052-01 WUFF-IN 13-05605-000 Water 02/03/2018
Page 3: February 3, 2018 - Virginia Tech...Data_18B0052 ARI ID Client ID Proj ID Matrix Sampled Rec Prep Analyzed Method CAS Compound Value Q Units 18B0052-01 WUFF-IN 13-05605-000 Water 02/03/2018

Data_18B0052ARI ID Client ID Proj ID Matrix Sampled Rec Prep Analyzed Method CAS Compound Value Q Units18B0052-01 WUFF-IN 13-05605-000 Water 02/03/2018 02/05/2018 02/06/2018 02/09/2018 SM 2340 B-97 Hardness 40.1 mg/L18B0052-03 WUFF-OUT 13-05605-000 Water 02/03/2018 02/05/2018 02/06/2018 02/09/2018 SM 2340 B-97 Hardness 39.2 mg/LBGB0091-BLK1 Blank 13-05605-000 Water 02/05/2018 02/05/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0040 U mg-P/LBGB0091-BS1 LCS 13-05605-000 Water 02/05/2018 02/05/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.148 mg-P/LBGB0091-DUP1 WUFF-IN 13-05605-000 Water 02/03/2018 02/05/2018 02/05/2018 02/05/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0130 L mg-P/LBGB0091-MS1 WUFF-IN 13-05605-000 Water 02/03/2018 02/05/2018 02/05/2018 02/05/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.114 mg-P/L18B0052-01 WUFF-IN 13-05605-000 Water 02/03/2018 02/05/2018 02/05/2018 02/05/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0100 mg-P/L18B0052-03 WUFF-OUT 13-05605-000 Water 02/03/2018 02/05/2018 02/05/2018 02/05/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0130 mg-P/LBGB0122-BLK1 Blank 13-05605-000 Water 02/06/2018 02/09/2018 EPA 6010C 7440-70-2 Calcium 0.0500 U mg/LBGB0122-BS1 LCS 13-05605-000 Water 02/06/2018 02/09/2018 EPA 6010C 7440-70-2 Calcium 9.98 mg/L18B0052-01 WUFF-IN 13-05605-000 Water 02/03/2018 02/05/2018 02/06/2018 02/09/2018 EPA 6010C 7440-70-2 Calcium 11.9 mg/L18B0052-03 WUFF-OUT 13-05605-000 Water 02/03/2018 02/05/2018 02/06/2018 02/09/2018 EPA 6010C 7440-70-2 Calcium 11.6 mg/LBGB0122-BLK1 Blank 13-05605-000 Water 02/06/2018 02/09/2018 EPA 6010C 7439-95-4 Magnesium 0.0500 U mg/LBGB0122-BS1 LCS 13-05605-000 Water 02/06/2018 02/09/2018 EPA 6010C 7439-95-4 Magnesium 10.1 mg/L18B0052-01 WUFF-IN 13-05605-000 Water 02/03/2018 02/05/2018 02/06/2018 02/09/2018 EPA 6010C 7439-95-4 Magnesium 2.55 mg/L18B0052-03 WUFF-OUT 13-05605-000 Water 02/03/2018 02/05/2018 02/06/2018 02/09/2018 EPA 6010C 7439-95-4 Magnesium 2.46 mg/LBGB0162-BLK1 Blank 13-05605-000 Water 02/08/2018 02/08/2018 EPA 200.8 7440-50-8 Copper 0.500 U ug/LBGB0162-BS1 LCS 13-05605-000 Water 02/08/2018 02/08/2018 EPA 200.8 7440-50-8 Copper 24.9 ug/L18B0052-01 WUFF-IN 13-05605-000 Water 02/03/2018 02/05/2018 02/08/2018 02/08/2018 EPA 200.8 7440-50-8 Copper 33.0 ug/L18B0052-03 WUFF-OUT 13-05605-000 Water 02/03/2018 02/05/2018 02/08/2018 02/08/2018 EPA 200.8 7440-50-8 Copper 22.7 ug/LBGB0162-BLK1 Blank 13-05605-000 Water 02/08/2018 02/08/2018 EPA 200.8 7440-50-8 Copper 0.500 U ug/LBGB0162-BS1 LCS 13-05605-000 Water 02/08/2018 02/08/2018 EPA 200.8 7440-50-8 Copper 26.2 ug/LBGB0162-BLK1 Blank 13-05605-000 Water 02/08/2018 02/08/2018 EPA 200.8 7440-66-6 Zinc 4.00 U ug/LBGB0162-BS1 LCS 13-05605-000 Water 02/08/2018 02/08/2018 EPA 200.8 7440-66-6 Zinc 79.9 ug/LBGB0162-BLK1 Blank 13-05605-000 Water 02/08/2018 02/08/2018 EPA 200.8 7440-66-6 Zinc 4.00 U ug/LBGB0162-BS1 LCS 13-05605-000 Water 02/08/2018 02/08/2018 EPA 200.8 7440-66-6 Zinc 75.3 ug/L18B0052-01 WUFF-IN 13-05605-000 Water 02/03/2018 02/05/2018 02/08/2018 02/08/2018 EPA 200.8 7440-66-6 Zinc 99.9 ug/L18B0052-03 WUFF-OUT 13-05605-000 Water 02/03/2018 02/05/2018 02/08/2018 02/08/2018 EPA 200.8 7440-66-6 Zinc 63.0 ug/LBGB0205-BLK1 Blank 13-05605-000 Water 02/09/2018 02/09/2018 EPA 200.8-Dissolved 7440-50-8 Copper 0.500 U ug/LBGB0205-BS1 LCS 13-05605-000 Water 02/09/2018 02/09/2018 EPA 200.8-Dissolved 7440-50-8 Copper 27.3 ug/L18B0052-02 WUFF-IN 13-05605-000 Water 02/03/2018 02/05/2018 02/09/2018 02/12/2018 EPA 200.8-Dissolved 7440-50-8 Copper 10.7 ug/L18B0052-04 WUFF-OUT 13-05605-000 Water 02/03/2018 02/05/2018 02/09/2018 02/12/2018 EPA 200.8-Dissolved 7440-50-8 Copper 10.6 ug/LBGB0205-BLK1 Blank 13-05605-000 Water 02/09/2018 02/09/2018 EPA 200.8-Dissolved 7440-50-8 Copper 0.500 U ug/LBGB0205-BS1 LCS 13-05605-000 Water 02/09/2018 02/09/2018 EPA 200.8-Dissolved 7440-50-8 Copper 27.4 ug/LBGB0205-BLK1 Blank 13-05605-000 Water 02/09/2018 02/09/2018 EPA 200.8-Dissolved 7440-66-6 Zinc 4.00 U ug/LBGB0205-BS1 LCS 13-05605-000 Water 02/09/2018 02/09/2018 EPA 200.8-Dissolved 7440-66-6 Zinc 86.6 ug/L18B0052-02 WUFF-IN 13-05605-000 Water 02/03/2018 02/05/2018 02/09/2018 02/12/2018 EPA 200.8-Dissolved 7440-66-6 Zinc 31.3 ug/L18B0052-04 WUFF-OUT 13-05605-000 Water 02/03/2018 02/05/2018 02/09/2018 02/12/2018 EPA 200.8-Dissolved 7440-66-6 Zinc 31.1 ug/LBGB0205-BLK1 Blank 13-05605-000 Water 02/09/2018 02/09/2018 EPA 200.8-Dissolved 7440-66-6 Zinc 4.00 U ug/LBGB0205-BS1 LCS 13-05605-000 Water 02/09/2018 02/09/2018 EPA 200.8-Dissolved 7440-66-6 Zinc 84.3 ug/LBGB0292-BLK1 Blank 13-05605-000 Water 02/13/2018 02/14/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0080 U mg-P/LBGB0292-BLK2 Blank 13-05605-000 Water 02/13/2018 02/14/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0080 U mg-P/LBGB0292-BS1 LCS 13-05605-000 Water 02/13/2018 02/14/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.144 mg-P/LBGB0292-BS2 LCS 13-05605-000 Water 02/13/2018 02/14/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.147 mg-P/LBGB0292-DUP1 WUFF-IN 13-05605-000 Water 02/03/2018 02/05/2018 02/13/2018 02/14/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.114 * mg-P/LBGB0292-MS1 WUFF-IN 13-05605-000 Water 02/03/2018 02/05/2018 02/13/2018 02/14/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 1.84 D mg-P/L18B0052-01 WUFF-IN 13-05605-000 Water 02/03/2018 02/05/2018 02/13/2018 02/14/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0840 mg-P/L18B0052-03 WUFF-OUT 13-05605-000 Water 02/03/2018 02/05/2018 02/13/2018 02/14/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0460 mg-P/L

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Page 1 of 28 18B0052 ARISample FINAL 20 Feb 2018 1605

Amanda Volgardsen

Digitally signed by Amanda Volgardsen DN: c=US, st=Washington, l=Tukwila, o=Analytical Resources, Inc., ou=Client Services, cn=Amanda Volgardsen, [email protected] Date: 2018.02.20 16:08:12 -08'00'

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Pag

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Page 4 of 28 18B0052 ARISample FINAL 20 Feb 2018 1605

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Page 5 of 28 18B0052 ARISample FINAL 20 Feb 2018 1605

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Page 23 of 28 18B0052 ARISample FINAL 20 Feb 2018 1605

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Page 24 of 28 18B0052 ARISample FINAL 20 Feb 2018 1605

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February 13, 2018

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Data_18B0197ARI ID Client ID Proj ID Matrix Sampled Rec Prep Analyzed Method CAS Compound Value Q UnitsBGB0371-BLK1 Blank 13-05605-000 Water 02/15/2018 02/15/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0040 U mg-P/LBGB0371-BS1 LCS 13-05605-000 Water 02/15/2018 02/15/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.155 mg-P/L18B0197-01 WUFF-IN 13-05605-000 Surface Water 02/14/2018 02/14/2018 02/15/2018 02/15/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0170 mg-P/L18B0197-02 WUFF-OUT 13-05605-000 Surface Water 02/14/2018 02/14/2018 02/15/2018 02/15/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0150 mg-P/LBGB0613-BLK1 Blank 13-05605-000 Water 02/26/2018 02/27/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0160 U mg-P/LBGB0613-BLK2 Blank 13-05605-000 Water 02/26/2018 02/27/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0160 U mg-P/LBGB0613-BS1 LCS 13-05605-000 Water 02/26/2018 02/27/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.150 mg-P/LBGB0613-BS2 LCS 13-05605-000 Water 02/26/2018 02/27/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.149 mg-P/L18B0197-01 WUFF-IN 13-05605-000 Surface Water 02/14/2018 02/14/2018 02/26/2018 02/27/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0960 mg-P/L18B0197-02 WUFF-OUT 13-05605-000 Surface Water 02/14/2018 02/14/2018 02/26/2018 02/27/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0860 mg-P/L

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Page 1 of 13 18B0197 ARISample FINAL 28 Feb 2018 1107

Amanda Volgardsen

Digitally signed by Amanda Volgardsen DN: c=US, st=Washington, l=Tukwila, o=Analytical Resources, Inc., ou=Project Manager, cn=Amanda Volgardsen, [email protected]: 2018.02.28 11:07:50 -08'00'

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February 28, 2018

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Data_18C0025ARI ID Client ID Proj ID Matrix Sampled Rec Prep Analyzed Method CAS Compound Value Q UnitsBGC0114-BLK1 Blank 13-05605-000 Water 03/06/2018 03/09/2018 NWTPH-Dx Diesel Range Organics (C12-C24) 0.100 U mg/LBGC0114-BS1 LCS 13-05605-000 Water 03/06/2018 03/09/2018 NWTPH-Dx Diesel Range Organics (C12-C24) 2.61 mg/LBGC0114-BSD1 LCS Dup 13-05605-000 Water 03/06/2018 03/09/2018 NWTPH-Dx Diesel Range Organics (C12-C24) 2.27 mg/L18C0025-01 WUFF-IN 13-05605-000 Surface Water 02/28/2018 03/01/2018 03/06/2018 03/09/2018 NWTPH-Dx Diesel Range Organics (C12-C24) 1.27 mg/L18C0025-02 WUFF-OUT13-05605-000 Surface Water 02/28/2018 03/01/2018 03/06/2018 03/09/2018 NWTPH-Dx Diesel Range Organics (C12-C24) 0.646 mg/LBGC0114-BLK1 Blank 13-05605-000 Water 03/06/2018 03/09/2018 NWTPH-Dx Motor Oil Range Organics (C24-C38) 0.200 U mg/LBGC0114-BS1 LCS 13-05605-000 Water 03/06/2018 03/09/2018 NWTPH-Dx Motor Oil Range Organics (C24-C38) 0.200 U mg/LBGC0114-BSD1 LCS Dup 13-05605-000 Water 03/06/2018 03/09/2018 NWTPH-Dx Motor Oil Range Organics (C24-C38) 0.200 U mg/L18C0025-01 WUFF-IN 13-05605-000 Surface Water 02/28/2018 03/01/2018 03/06/2018 03/09/2018 NWTPH-Dx Motor Oil Range Organics (C24-C38) 4.10 mg/L18C0025-02 WUFF-OUT13-05605-000 Surface Water 02/28/2018 03/01/2018 03/06/2018 03/09/2018 NWTPH-Dx Motor Oil Range Organics (C24-C38) 1.34 mg/LBGC0114-BLK1 Blank 13-05605-000 Water 03/06/2018 03/09/2018 NWTPH-Dx 84-15-1 o-Terphenyl 75.9 %BGC0114-BS1 LCS 13-05605-000 Water 03/06/2018 03/09/2018 NWTPH-Dx 84-15-1 o-Terphenyl 89.5 %BGC0114-BSD1 LCS Dup 13-05605-000 Water 03/06/2018 03/09/2018 NWTPH-Dx 84-15-1 o-Terphenyl 76.7 %18C0025-01 WUFF-IN 13-05605-000 Surface Water 02/28/2018 03/01/2018 03/06/2018 03/09/2018 NWTPH-Dx 84-15-1 o-Terphenyl 84.8 %18C0025-02 WUFF-OUT13-05605-000 Surface Water 02/28/2018 03/01/2018 03/06/2018 03/09/2018 NWTPH-Dx 84-15-1 o-Terphenyl 80.1 %

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Page 1 of 10 18C0025 ARISample FINAL 12 Mar 2018 1414

Amanda Volgardsen

Digitally signed by Amanda Volgardsen DN: c=US, st=Washington, l=Tukwila, o=Analytical Resources, Inc., ou=Project Manager, cn=Amanda Volgardsen, [email protected]: 2018.03.12 14:14:41 -07'00'

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Data_18C0031ARI ID Client ID Proj ID Matrix Sampled Rec Prep Analyzed Method CAS Compound Value Q UnitsBGC0062-BLK1 Blank 13-05605-000 Water 03/02/2018 03/02/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0040 U mg-P/LBGC0062-BS1 LCS 13-05605-000 Water 03/02/2018 03/02/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.145 mg-P/LBGC0062-DUP1 WUFF-IN 13-05605-000 Surface Water 02/28/2018 03/01/2018 03/02/2018 03/02/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0200 L mg-P/LBGC0062-MS1 WUFF-IN 13-05605-000 Surface Water 02/28/2018 03/01/2018 03/02/2018 03/02/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.115 mg-P/L18C0031-01 WUFF-IN 13-05605-000 Surface Water 02/28/2018 03/01/2018 03/02/2018 03/02/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0160 mg-P/L18C0031-02 WUFF-OUT 13-05605-000 Surface Water 02/28/2018 03/01/2018 03/02/2018 03/02/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0220 mg-P/LBGC0086-BLK1 Blank 13-05605-000 Water 03/05/2018 03/05/2018 EPA 200.8 7440-50-8 Copper 0.500 U ug/LBGC0086-BS1 LCS 13-05605-000 Water 03/05/2018 03/05/2018 EPA 200.8 7440-50-8 Copper 28.3 ug/L18C0031-01 WUFF-IN 13-05605-000 Surface Water 02/28/2018 03/01/2018 03/05/2018 03/05/2018 EPA 200.8 7440-50-8 Copper 41.1 ug/L18C0031-02 WUFF-OUT 13-05605-000 Surface Water 02/28/2018 03/01/2018 03/05/2018 03/05/2018 EPA 200.8 7440-50-8 Copper 20.3 ug/LBGC0086-BLK1 Blank 13-05605-000 Water 03/05/2018 03/05/2018 EPA 200.8 7440-50-8 Copper 0.500 U ug/LBGC0086-BS1 LCS 13-05605-000 Water 03/05/2018 03/05/2018 EPA 200.8 7440-50-8 Copper 28.4 ug/LBGC0086-BLK1 Blank 13-05605-000 Water 03/05/2018 03/05/2018 EPA 200.8 7440-66-6 Zinc 4.00 U ug/LBGC0086-BS1 LCS 13-05605-000 Water 03/05/2018 03/05/2018 EPA 200.8 7440-66-6 Zinc 88.6 ug/L18C0031-01 WUFF-IN 13-05605-000 Surface Water 02/28/2018 03/01/2018 03/05/2018 03/05/2018 EPA 200.8 7440-66-6 Zinc 138 ug/L18C0031-02 WUFF-OUT 13-05605-000 Surface Water 02/28/2018 03/01/2018 03/05/2018 03/05/2018 EPA 200.8 7440-66-6 Zinc 65.7 ug/LBGC0086-BLK1 Blank 13-05605-000 Water 03/05/2018 03/05/2018 EPA 200.8 7440-66-6 Zinc 4.00 U ug/LBGC0086-BS1 LCS 13-05605-000 Water 03/05/2018 03/05/2018 EPA 200.8 7440-66-6 Zinc 83.4 ug/LBGC0202-BLK1 Blank 13-05605-000 Water 03/08/2018 03/09/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0080 U mg-P/LBGC0202-BLK2 Blank 13-05605-000 Water 03/08/2018 03/09/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0080 U mg-P/LBGC0202-BS1 LCS 13-05605-000 Water 03/08/2018 03/09/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.151 mg-P/LBGC0202-BS2 LCS 13-05605-000 Water 03/08/2018 03/09/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.150 mg-P/L18C0031-02 WUFF-OUT 13-05605-000 Surface Water 02/28/2018 03/01/2018 03/08/2018 03/09/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0560 mg-P/LBGC0203-BLK1 Blank 13-05605-000 Water 03/08/2018 03/09/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0160 U mg-P/LBGC0203-BLK2 Blank 13-05605-000 Water 03/08/2018 03/09/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0160 U mg-P/LBGC0203-BS1 LCS 13-05605-000 Water 03/08/2018 03/09/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.145 mg-P/LBGC0203-BS2 LCS 13-05605-000 Water 03/08/2018 03/09/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.144 mg-P/L18C0031-01 WUFF-IN 13-05605-000 Surface Water 02/28/2018 03/01/2018 03/08/2018 03/09/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.112 mg-P/L

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Page 1 of 16 18C0031 ARISample FINAL 20 Mar 2018 1731

Amanda Volgardsen

Digitally signed by Amanda Volgardsen DN: c=US, st=Washington, l=Tukwila, o=Analytical Resources, Inc., ou=Project Manager, cn=Amanda Volgardsen, [email protected]: 2018.03.20 17:32:44 -07'00'

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March 8, 2018

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Data_18C0179ARI ID Client ID Proj ID Matrix Sampled Rec Prep Analyzed Method CAS Compound Value Q UnitsBGC0339-BLK1 Blank 13-05605-000 Water 03/14/2018 03/20/2018 NWTPH-Dx Diesel Range Organics (C12-C24) 0.100 U mg/LBGC0339-BS1 LCS 13-05605-000 Water 03/14/2018 03/20/2018 NWTPH-Dx Diesel Range Organics (C12-C24) 2.19 mg/LBGC0339-BSD1 LCS Dup 13-05605-000 Water 03/14/2018 03/20/2018 NWTPH-Dx Diesel Range Organics (C12-C24) 2.33 mg/L18C0179-01 WUFF-IN 13-05605-000 Water 03/08/2018 03/09/201803/14/2018 03/20/2018 NWTPH-Dx Diesel Range Organics (C12-C24) 0.499 mg/L18C0179-02 WUFF-OUT 13-05605-000 Water 03/08/2018 03/09/201803/14/2018 03/20/2018 NWTPH-Dx Diesel Range Organics (C12-C24) 0.325 mg/LBGC0339-BLK1 Blank 13-05605-000 Water 03/14/2018 03/20/2018 NWTPH-Dx Motor Oil Range Organics (C24-C38) 0.200 U mg/LBGC0339-BS1 LCS 13-05605-000 Water 03/14/2018 03/20/2018 NWTPH-Dx Motor Oil Range Organics (C24-C38) 0.200 U mg/LBGC0339-BSD1 LCS Dup 13-05605-000 Water 03/14/2018 03/20/2018 NWTPH-Dx Motor Oil Range Organics (C24-C38) 0.200 U mg/L18C0179-01 WUFF-IN 13-05605-000 Water 03/08/2018 03/09/201803/14/2018 03/20/2018 NWTPH-Dx Motor Oil Range Organics (C24-C38) 1.87 mg/L18C0179-02 WUFF-OUT 13-05605-000 Water 03/08/2018 03/09/201803/14/2018 03/20/2018 NWTPH-Dx Motor Oil Range Organics (C24-C38) 0.832 mg/LBGC0339-BLK1 Blank 13-05605-000 Water 03/14/2018 03/20/2018 NWTPH-Dx 84-15-1 o-Terphenyl 81.7 %BGC0339-BS1 LCS 13-05605-000 Water 03/14/2018 03/20/2018 NWTPH-Dx 84-15-1 o-Terphenyl 79.8 %BGC0339-BSD1 LCS Dup 13-05605-000 Water 03/14/2018 03/20/2018 NWTPH-Dx 84-15-1 o-Terphenyl 85.8 %18C0179-01 WUFF-IN 13-05605-000 Water 03/08/2018 03/09/201803/14/2018 03/20/2018 NWTPH-Dx 84-15-1 o-Terphenyl 75.7 %18C0179-02 WUFF-OUT 13-05605-000 Water 03/08/2018 03/09/201803/14/2018 03/20/2018 NWTPH-Dx 84-15-1 o-Terphenyl 79.2 %

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Page 1 of 10 18C0179 ARISample FINAL 21 Mar 2018 1451

Amanda Volgardsen

Digitally signed by Amanda Volgardsen DN: c=US, st=Washington, l=Tukwila, o=Analytical Resources, Inc., ou=Project Manager, cn=Amanda Volgardsen, [email protected] Date: 2018.03.21 14:52:10 -07'00'

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Data_18C0180ARI ID Client ID Proj ID Matrix Sampled Rec Prep Analyzed Method CAS Compound Value Q UnitsBGC0288-BLK1 Blank 13-05605-000 Water 03/10/2018 03/10/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0040 U mg-P/LBGC0288-BS1 LCS 13-05605-000 Water 03/10/2018 03/10/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.152 mg-P/LBGC0288-DUP2 WUFF-IN 13-05605-000 Water 03/08/2018 03/09/2018 03/10/2018 03/10/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0160 L mg-P/LBGC0288-MS1 WUFF-IN 13-05605-000 Water 03/08/2018 03/09/2018 03/10/2018 03/10/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.115 mg-P/L18C0180-01RE2 WUFF-IN 13-05605-000 Water 03/08/2018 03/09/2018 03/10/2018 03/10/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0120 mg-P/L18C0180-02RE1 WUFF-OUT 13-05605-000 Water 03/08/2018 03/09/2018 03/10/2018 03/10/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0140 mg-P/LBGC0291-BLK1 Blank 13-05605-000 Water 03/15/2018 03/16/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0140 mg-P/LBGC0291-BLK2 Blank 13-05605-000 Water 03/10/2018 03/16/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0160 U mg-P/LBGC0291-BS1 LCS 13-05605-000 Water 03/15/2018 03/16/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.316 mg-P/LBGC0291-BS2 LCS 13-05605-000 Water 03/15/2018 03/16/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.312 mg-P/L18C0180-01 WUFF-IN 13-05605-000 Water 03/08/2018 03/09/2018 03/15/2018 03/16/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.138 mg-P/L18C0180-02 WUFF-OUT 13-05605-000 Water 03/08/2018 03/09/2018 03/15/2018 03/16/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0580 mg-P/LBGC0293-BLK1 Blank 13-05605-000 Water 03/12/2018 03/12/2018 EPA 200.8 7440-50-8 Copper 0.500 U ug/LBGC0293-BS1 LCS 13-05605-000 Water 03/12/2018 03/12/2018 EPA 200.8 7440-50-8 Copper 29.2 ug/L18C0180-01 WUFF-IN 13-05605-000 Water 03/08/2018 03/09/2018 03/12/2018 03/13/2018 EPA 200.8 7440-50-8 Copper 45.9 ug/L18C0180-02 WUFF-OUT 13-05605-000 Water 03/08/2018 03/09/2018 03/12/2018 03/13/2018 EPA 200.8 7440-50-8 Copper 26.6 ug/LBGC0293-BLK1 Blank 13-05605-000 Water 03/12/2018 03/12/2018 EPA 200.8 7440-50-8 Copper 0.500 U ug/LBGC0293-BS1 LCS 13-05605-000 Water 03/12/2018 03/12/2018 EPA 200.8 7440-50-8 Copper 28.5 ug/LBGC0293-BLK1 Blank 13-05605-000 Water 03/12/2018 03/12/2018 EPA 200.8 7440-66-6 Zinc 4.00 U ug/LBGC0293-BS1 LCS 13-05605-000 Water 03/12/2018 03/12/2018 EPA 200.8 7440-66-6 Zinc 88.1 ug/L18C0180-01 WUFF-IN 13-05605-000 Water 03/08/2018 03/09/2018 03/12/2018 03/13/2018 EPA 200.8 7440-66-6 Zinc 142 ug/L18C0180-02 WUFF-OUT 13-05605-000 Water 03/08/2018 03/09/2018 03/12/2018 03/13/2018 EPA 200.8 7440-66-6 Zinc 77.4 ug/LBGC0293-BLK1 Blank 13-05605-000 Water 03/12/2018 03/12/2018 EPA 200.8 7440-66-6 Zinc 4.00 U ug/LBGC0293-BS1 LCS 13-05605-000 Water 03/12/2018 03/12/2018 EPA 200.8 7440-66-6 Zinc 86.9 ug/L

Page 1

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Page 1 of 18 18C0180 ARISample FINAL 28 Mar 2018 1048

Amanda Volgardsen

Digitally signed by Amanda Volgardsen DN: c=US, st=Washington, l=Tukwila, o=Analytical Resources, Inc., ou=Project Manager, cn=Amanda Volgardsen, [email protected] Date: 2018.03.28 10:50:08 -07'00'

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March 13, 2018

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Data_18C0251ARI ID Client ID Proj ID Matrix Sampled Rec Prep Analyzed Method CAS Compound Value Q Units18C0251-01 WUFF-IN 13-05605-000 Surface Water 03/13/2018 03/14/2018 03/29/2018 03/29/2018 ASTM D3977 SC_>500 >500 µm 1.20 mg/L18C0251-02 WUFF-OUT 13-05605-000 Surface Water 03/13/2018 03/14/2018 03/29/2018 03/29/2018 ASTM D3977 SC_>500 >500 µm 0.00 mg/L18C0251-01 WUFF-IN 13-05605-000 Surface Water 03/13/2018 03/14/2018 03/29/2018 03/29/2018 ASTM D3977 SC_500-125 500-125 µm 4.00 mg/L18C0251-02 WUFF-OUT 13-05605-000 Surface Water 03/13/2018 03/14/2018 03/29/2018 03/29/2018 ASTM D3977 SC_500-125 500-125 µm 1.00 mg/L18C0251-01 WUFF-IN 13-05605-000 Surface Water 03/13/2018 03/14/2018 03/29/2018 03/29/2018 ASTM D3977 SC_125-62.5 125-62.5 µm 2.50 mg/L18C0251-02 WUFF-OUT 13-05605-000 Surface Water 03/13/2018 03/14/2018 03/29/2018 03/29/2018 ASTM D3977 SC_125-62.5 125-62.5 µm 0.50 mg/L18C0251-01 WUFF-IN 13-05605-000 Surface Water 03/13/2018 03/14/2018 03/29/2018 03/29/2018 ASTM D3977 SC_62.5-4 62.5-4 µm 22.00 mg/L18C0251-02 WUFF-OUT 13-05605-000 Surface Water 03/13/2018 03/14/2018 03/29/2018 03/29/2018 ASTM D3977 SC_62.5-4 62.5-4 µm 7.00 mg/L18C0251-01 WUFF-IN 13-05605-000 Surface Water 03/13/2018 03/14/2018 03/29/2018 03/29/2018 ASTM D3977 SC_4-1 4-1 µm 24.30 mg/L18C0251-02 WUFF-OUT 13-05605-000 Surface Water 03/13/2018 03/14/2018 03/29/2018 03/29/2018 ASTM D3977 SC_4-1 4-1 µm 2.70 mg/L18C0251-01 WUFF-IN 13-05605-000 Surface Water 03/13/2018 03/14/2018 03/29/2018 03/29/2018 ASTM D3977 Suspended Sediment Concentration 58.00 mg/L18C0251-02 WUFF-OUT 13-05605-000 Surface Water 03/13/2018 03/14/2018 03/29/2018 03/29/2018 ASTM D3977 Suspended Sediment Concentration 11.50 mg/LBGC0291-BLK1 Blank 13-05605-000 Water 03/15/2018 03/16/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0140 mg-P/LBGC0291-BLK2 Blank 13-05605-000 Water 03/10/2018 03/16/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0160 U mg-P/LBGC0291-BS1 LCS 13-05605-000 Water 03/15/2018 03/16/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.316 mg-P/LBGC0291-BS2 LCS 13-05605-000 Water 03/15/2018 03/16/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.312 mg-P/L18C0251-01 WUFF-IN 13-05605-000 Surface Water 03/13/2018 03/14/2018 03/15/2018 03/16/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.140 mg-P/L18C0251-02 WUFF-OUT 13-05605-000 Surface Water 03/13/2018 03/14/2018 03/15/2018 03/16/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0640 mg-P/LBGC0416-BLK2 Blank 13-05605-000 Water 03/15/2018 03/15/2018 EPA 200.8 7440-50-8 Copper 0.500 U ug/LBGC0416-BS2 LCS 13-05605-000 Water 03/15/2018 03/15/2018 EPA 200.8 7440-50-8 Copper 25.6 ug/L18C0251-01 WUFF-IN 13-05605-000 Surface Water 03/13/2018 03/14/2018 03/15/2018 03/15/2018 EPA 200.8 7440-50-8 Copper 47.5 D ug/L18C0251-02 WUFF-OUT 13-05605-000 Surface Water 03/13/2018 03/14/2018 03/15/2018 03/16/2018 EPA 200.8 7440-50-8 Copper 23.8 ug/LBGC0416-BLK2 Blank 13-05605-000 Water 03/15/2018 03/15/2018 EPA 200.8 7440-50-8 Copper 0.500 U ug/LBGC0416-BS2 LCS 13-05605-000 Water 03/15/2018 03/15/2018 EPA 200.8 7440-50-8 Copper 25.9 ug/LBGC0416-BLK2 Blank 13-05605-000 Water 03/15/2018 03/15/2018 EPA 200.8 7440-66-6 Zinc 4.00 U ug/LBGC0416-BS2 LCS 13-05605-000 Water 03/15/2018 03/15/2018 EPA 200.8 7440-66-6 Zinc 87.0 ug/L18C0251-01 WUFF-IN 13-05605-000 Surface Water 03/13/2018 03/14/2018 03/15/2018 03/15/2018 EPA 200.8 7440-66-6 Zinc 182 D ug/L18C0251-02 WUFF-OUT 13-05605-000 Surface Water 03/13/2018 03/14/2018 03/15/2018 03/16/2018 EPA 200.8 7440-66-6 Zinc 77.8 ug/LBGC0416-BLK2 Blank 13-05605-000 Water 03/15/2018 03/15/2018 EPA 200.8 7440-66-6 Zinc 4.00 U ug/LBGC0416-BS2 LCS 13-05605-000 Water 03/15/2018 03/15/2018 EPA 200.8 7440-66-6 Zinc 79.3 ug/LBGC0438-BLK1 Blank 13-05605-000 Water 03/15/2018 03/15/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0040 U mg-P/LBGC0438-BS1 LCS 13-05605-000 Water 03/15/2018 03/15/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.148 mg-P/LBGC0438-DUP1 WUFF-IN 13-05605-000 Surface Water 03/13/2018 03/14/2018 03/15/2018 03/15/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0150 mg-P/LBGC0438-MS1 WUFF-IN 13-05605-000 Surface Water 03/13/2018 03/14/2018 03/15/2018 03/15/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.101 mg-P/L18C0251-01 WUFF-IN 13-05605-000 Surface Water 03/13/2018 03/14/2018 03/15/2018 03/15/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0130 mg-P/L18C0251-02 WUFF-OUT 13-05605-000 Surface Water 03/13/2018 03/14/2018 03/15/2018 03/15/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0110 mg-P/L

Page 1

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Amanda Volgardsen

Digitally signed by Amanda Volgardsen DN: c=US, st=Washington, l=Tukwila, o=Analytical Resources, Inc., ou=Project Manager, cn=Amanda Volgardsen, [email protected]: 2018.03.30 14:39:37 -07'00'

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March 22, 2018

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Data_18C0396ARI ID Client ID Proj ID Matrix Sampled Rec Prep Analyzed Method CAS Compound Value Q Units18C0396-01 WUFF-IN 13-05605-000 Water 03/22/2018 03/23/2018 04/06/2018 04/06/2018 ASTM D3977 SC_>500 >500 µm 5.00 mg/L18C0396-02 WUFF-OUT 13-05605-000 Water 03/22/2018 03/23/2018 04/06/2018 04/06/2018 ASTM D3977 SC_>500 >500 µm 1.00 mg/L18C0396-01 WUFF-IN 13-05605-000 Water 03/22/2018 03/23/2018 04/06/2018 04/06/2018 ASTM D3977 SC_500-125 500-125 µm 6.80 mg/L18C0396-02 WUFF-OUT 13-05605-000 Water 03/22/2018 03/23/2018 04/06/2018 04/06/2018 ASTM D3977 SC_500-125 500-125 µm 2.70 mg/L18C0396-01 WUFF-IN 13-05605-000 Water 03/22/2018 03/23/2018 04/06/2018 04/06/2018 ASTM D3977 SC_125-62.5 125-62.5 µm 5.70 mg/L18C0396-02 WUFF-OUT 13-05605-000 Water 03/22/2018 03/23/2018 04/06/2018 04/06/2018 ASTM D3977 SC_125-62.5 125-62.5 µm 4.80 mg/L18C0396-01 WUFF-IN 13-05605-000 Water 03/22/2018 03/23/2018 04/06/2018 04/06/2018 ASTM D3977 SC_62.5-4 62.5-4 µm 39.50 mg/L18C0396-02 WUFF-OUT 13-05605-000 Water 03/22/2018 03/23/2018 04/06/2018 04/06/2018 ASTM D3977 SC_62.5-4 62.5-4 µm 11.80 mg/L18C0396-01 WUFF-IN 13-05605-000 Water 03/22/2018 03/23/2018 04/06/2018 04/06/2018 ASTM D3977 SC_4-1 4-1 µm 11.70 mg/L18C0396-02 WUFF-OUT 13-05605-000 Water 03/22/2018 03/23/2018 04/06/2018 04/06/2018 ASTM D3977 SC_4-1 4-1 µm 6.80 mg/L18C0396-01 WUFF-IN 13-05605-000 Water 03/22/2018 03/23/2018 04/06/2018 04/06/2018 ASTM D3977 Suspended Sediment Concentration 74.50 mg/L18C0396-02 WUFF-OUT 13-05605-000 Water 03/22/2018 03/23/2018 04/06/2018 04/06/2018 ASTM D3977 Suspended Sediment Concentration 28.00 mg/LBGC0663-BLK1 Blank 13-05605-000 Water 03/24/2018 03/26/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0080 U mg-P/LBGC0663-BLK2 Blank 13-05605-000 Water 03/24/2018 03/26/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0080 U mg-P/LBGC0663-BLK3 Blank 13-05605-000 Water 03/24/2018 03/26/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0080 U mg-P/LBGC0663-BS1 LCS 13-05605-000 Water 03/24/2018 03/26/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.154 mg-P/LBGC0663-BS2 LCS 13-05605-000 Water 03/24/2018 03/26/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.155 mg-P/LBGC0663-BS3 LCS 13-05605-000 Water 03/24/2018 03/26/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.153 mg-P/L18C0396-01 WUFF-IN 13-05605-000 Water 03/22/2018 03/23/2018 03/24/2018 03/26/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.140 mg-P/L18C0396-02 WUFF-OUT 13-05605-000 Water 03/22/2018 03/23/2018 03/24/2018 03/26/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.100 mg-P/LBGC0664-BLK1 Blank 13-05605-000 Water 03/24/2018 03/24/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0040 U mg-P/LBGC0664-BS1 LCS 13-05605-000 Water 03/24/2018 03/24/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.145 mg-P/L18C0396-01 WUFF-IN 13-05605-000 Water 03/22/2018 03/23/2018 03/24/2018 03/24/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0120 mg-P/L18C0396-02 WUFF-OUT 13-05605-000 Water 03/22/2018 03/23/2018 03/24/2018 03/24/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0110 mg-P/LBGC0666-BLK1 Blank 13-05605-000 Water 03/26/2018 03/26/2018 EPA 200.8 7440-50-8 Copper 0.500 U ug/LBGC0666-BS1 LCS 13-05605-000 Water 03/26/2018 03/26/2018 EPA 200.8 7440-50-8 Copper 26.5 ug/L18C0396-02 WUFF-OUT 13-05605-000 Water 03/22/2018 03/23/2018 03/26/2018 03/27/2018 EPA 200.8 7440-50-8 Copper 36.3 ug/LBGC0666-BLK1 Blank 13-05605-000 Water 03/26/2018 03/26/2018 EPA 200.8 7440-50-8 Copper 0.500 U ug/LBGC0666-BS1 LCS 13-05605-000 Water 03/26/2018 03/26/2018 EPA 200.8 7440-50-8 Copper 26.7 ug/L18C0396-01 WUFF-IN 13-05605-000 Water 03/22/2018 03/23/2018 03/26/2018 03/27/2018 EPA 200.8 7440-50-8 Copper 51.4 ug/LBGC0666-BLK1 Blank 13-05605-000 Water 03/26/2018 03/26/2018 EPA 200.8 7440-66-6 Zinc 4.00 U ug/LBGC0666-BS1 LCS 13-05605-000 Water 03/26/2018 03/26/2018 EPA 200.8 7440-66-6 Zinc 86.2 ug/L18C0396-01 WUFF-IN 13-05605-000 Water 03/22/2018 03/23/2018 03/26/2018 03/27/2018 EPA 200.8 7440-66-6 Zinc 151 ug/L18C0396-02 WUFF-OUT 13-05605-000 Water 03/22/2018 03/23/2018 03/26/2018 03/27/2018 EPA 200.8 7440-66-6 Zinc 106 ug/LBGC0666-BLK1 Blank 13-05605-000 Water 03/26/2018 03/26/2018 EPA 200.8 7440-66-6 Zinc 4.00 U ug/LBGC0666-BS1 LCS 13-05605-000 Water 03/26/2018 03/26/2018 EPA 200.8 7440-66-6 Zinc 73.6 ug/L

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Amanda Volgardsen

Digitally signed by Amanda Volgardsen DN: c=US, st=Washington, l=Tukwila, o=Analytical Resources, Inc., ou=Project Manager, cn=Amanda Volgardsen, [email protected]: 2018.04.09 12:08:16 -07'00'

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Data_18C0399ARI ID Client ID Proj ID Matrix Sampled Rec Prep Analyzed Method CAS Compound Value Q UnitsBGC0680-BLK1 Blank 13-05605-000 Water 03/26/2018 03/28/2018 NWTPH-Dx Diesel Range Organics (C12-C24) 0.100 U mg/LBGC0680-BS1 LCS 13-05605-000 Water 03/26/2018 03/28/2018 NWTPH-Dx Diesel Range Organics (C12-C24) 2.33 mg/L18C0399-01 WUFF-IN 13-05605-000 Water 03/22/2018 03/23/2018 03/26/2018 03/28/2018 NWTPH-Dx Diesel Range Organics (C12-C24) 0.571 mg/L18C0399-02 WUFF-OUT 13-05605-000 Water 03/22/2018 03/23/2018 03/26/2018 03/28/2018 NWTPH-Dx Diesel Range Organics (C12-C24) 0.200 mg/LBGC0680-BLK1 Blank 13-05605-000 Water 03/26/2018 03/28/2018 NWTPH-Dx Motor Oil Range Organics (C24-C38) 0.200 U mg/LBGC0680-BS1 LCS 13-05605-000 Water 03/26/2018 03/28/2018 NWTPH-Dx Motor Oil Range Organics (C24-C38) 0.200 U mg/L18C0399-01 WUFF-IN 13-05605-000 Water 03/22/2018 03/23/2018 03/26/2018 03/28/2018 NWTPH-Dx Motor Oil Range Organics (C24-C38) 1.79 mg/L18C0399-02 WUFF-OUT 13-05605-000 Water 03/22/2018 03/23/2018 03/26/2018 03/28/2018 NWTPH-Dx Motor Oil Range Organics (C24-C38) 0.325 mg/LBGC0680-BLK1 Blank 13-05605-000 Water 03/26/2018 03/28/2018 NWTPH-Dx 84-15-1 o-Terphenyl 76.2 %BGC0680-BS1 LCS 13-05605-000 Water 03/26/2018 03/28/2018 NWTPH-Dx 84-15-1 o-Terphenyl 77.7 %18C0399-01 WUFF-IN 13-05605-000 Water 03/22/2018 03/23/2018 03/26/2018 03/28/2018 NWTPH-Dx 84-15-1 o-Terphenyl 78.5 %18C0399-02 WUFF-OUT 13-05605-000 Water 03/22/2018 03/23/2018 03/26/2018 03/28/2018 NWTPH-Dx 84-15-1 o-Terphenyl 82.9 %

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Amanda Volgardsen

Digitally signed by Amanda Volgardsen DN: c=US, st=Washington, l=Tukwila, o=Analytical Resources, Inc., ou=Project Manager, cn=Amanda Volgardsen, [email protected]: 2018.03.30 15:55:02 -07'00'

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December 12, 2018 – Rinsate Blank 3

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Data_18L0049ARI ID Client ID Proj ID Matrix Sampled Rec Prep Analyzed Method CAS Compound Value Q Units BatchBGL0098-BLK1 Blank 13-05605-000 Water 12/05/2018 12/05/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0040 U mg/L BGL0098BGL0098-BS1 LCS 13-05605-000 Water 12/05/2018 12/05/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.155 mg/L BGL0098BGL0098-DUP1 WUFF-IN-QA 13-05605-000 Water 12/04/2018 12/04/2018 12/05/2018 12/05/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0040 U mg/L BGL0098BGL0098-MS1 WUFF-IN-QA 13-05605-000 Water 12/04/2018 12/04/2018 12/05/2018 12/05/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.101 mg/L BGL009818L0049-01 WUFF-IN-QA 13-05605-000 Water 12/04/2018 12/04/2018 12/05/2018 12/05/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0040 U mg/L BGL009818L0049-03 WUFF-OUT-QA 13-05605-000 Water 12/04/2018 12/04/2018 12/05/2018 12/05/2018 SM 4500-P E-99 1426-54-42 Orthophosphorus 0.0040 U mg/L BGL0098BGL0137-BLK1 Blank 13-05605-000 Water 12/06/2018 12/06/2018 EPA 200.8 7440-50-8 Copper 0.500 U ug/L BGL0137BGL0137-BS1 LCS 13-05605-000 Water 12/06/2018 12/06/2018 EPA 200.8 7440-50-8 Copper 27.2 ug/L BGL013718L0049-01 WUFF-IN-QA 13-05605-000 Water 12/04/2018 12/04/2018 12/06/2018 12/06/2018 EPA 200.8 7440-50-8 Copper 0.500 U ug/L BGL013718L0049-03 WUFF-OUT-QA 13-05605-000 Water 12/04/2018 12/04/2018 12/06/2018 12/06/2018 EPA 200.8 7440-50-8 Copper 0.625 ug/L BGL0137BGL0137-BLK1 Blank 13-05605-000 Water 12/06/2018 12/06/2018 EPA 200.8 7440-50-8 Copper 0.500 U ug/L BGL0137BGL0137-BS1 LCS 13-05605-000 Water 12/06/2018 12/06/2018 EPA 200.8 7440-50-8 Copper 27.1 ug/L BGL0137BGL0137-BLK1 Blank 13-05605-000 Water 12/06/2018 12/06/2018 EPA 200.8 7440-66-6 Zinc 4.00 U ug/L BGL0137BGL0137-BS1 LCS 13-05605-000 Water 12/06/2018 12/06/2018 EPA 200.8 7440-66-6 Zinc 88.3 ug/L BGL013718L0049-01 WUFF-IN-QA 13-05605-000 Water 12/04/2018 12/04/2018 12/06/2018 12/06/2018 EPA 200.8 7440-66-6 Zinc 4.00 U ug/L BGL013718L0049-03 WUFF-OUT-QA 13-05605-000 Water 12/04/2018 12/04/2018 12/06/2018 12/06/2018 EPA 200.8 7440-66-6 Zinc 4.00 U ug/L BGL0137BGL0137-BLK1 Blank 13-05605-000 Water 12/06/2018 12/06/2018 EPA 200.8 7440-66-6 Zinc 4.00 U ug/L BGL0137BGL0137-BS1 LCS 13-05605-000 Water 12/06/2018 12/06/2018 EPA 200.8 7440-66-6 Zinc 83.1 ug/L BGL0137BGL0205-BLK1 Blank 13-05605-000 Water 12/10/2018 12/11/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0080 U mg-P/L BGL0205BGL0205-BLK2 Blank 13-05605-000 Water 12/10/2018 12/11/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0080 U mg-P/L BGL0205BGL0205-BS1 LCS 13-05605-000 Water 12/10/2018 12/11/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.300 mg-P/L BGL0205BGL0205-BS2 LCS 13-05605-000 Water 12/10/2018 12/11/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.296 mg-P/L BGL0205BGL0205-DUP1 WUFF-IN-QA 13-05605-000 Water 12/04/2018 12/04/2018 12/10/2018 12/11/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0080 U mg-P/L BGL0205BGL0205-MS1 WUFF-IN-QA 13-05605-000 Water 12/04/2018 12/04/2018 12/10/2018 12/11/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.202 mg-P/L BGL020518L0049-01 WUFF-IN-QA 13-05605-000 Water 12/04/2018 12/04/2018 12/10/2018 12/11/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0140 mg-P/L BGL020518L0049-03 WUFF-OUT-QA 13-05605-000 Water 12/04/2018 12/04/2018 12/10/2018 12/11/2018 SM 4500-P E-99 7723-14-0 Total Phosphorus 0.0080 U mg-P/L BGL0205BGL0206-BLK1 Blank 13-05605-000 Water 12/10/2018 12/11/2018 EPA 200.8-Dissolved 7440-50-8 Copper 0.500 U ug/L BGL0206BGL0206-BS1 LCS 13-05605-000 Water 12/10/2018 12/11/2018 EPA 200.8-Dissolved 7440-50-8 Copper 26.8 ug/L BGL020618L0049-02 WUFF-IN-QA 13-05605-000 Water 12/04/2018 12/04/2018 12/10/2018 12/11/2018 EPA 200.8-Dissolved 7440-50-8 Copper 0.500 U ug/L BGL020618L0049-04 WUFF-OUT-QA 13-05605-000 Water 12/04/2018 12/04/2018 12/10/2018 12/11/2018 EPA 200.8-Dissolved 7440-50-8 Copper 0.500 U ug/L BGL0206BGL0206-BLK1 Blank 13-05605-000 Water 12/10/2018 12/11/2018 EPA 200.8-Dissolved 7440-50-8 Copper 0.500 U ug/L BGL0206BGL0206-BS1 LCS 13-05605-000 Water 12/10/2018 12/11/2018 EPA 200.8-Dissolved 7440-50-8 Copper 26.8 ug/L BGL0206BGL0206-BLK1 Blank 13-05605-000 Water 12/10/2018 12/11/2018 EPA 200.8-Dissolved 7440-66-6 Zinc 4.00 U ug/L BGL0206BGL0206-BS1 LCS 13-05605-000 Water 12/10/2018 12/11/2018 EPA 200.8-Dissolved 7440-66-6 Zinc 81.5 ug/L BGL020618L0049-02 WUFF-IN-QA 13-05605-000 Water 12/04/2018 12/04/2018 12/10/2018 12/11/2018 EPA 200.8-Dissolved 7440-66-6 Zinc 4.00 U ug/L BGL020618L0049-04 WUFF-OUT-QA 13-05605-000 Water 12/04/2018 12/04/2018 12/10/2018 12/11/2018 EPA 200.8-Dissolved 7440-66-6 Zinc 4.00 U ug/L BGL0206BGL0206-BLK1 Blank 13-05605-000 Water 12/10/2018 12/11/2018 EPA 200.8-Dissolved 7440-66-6 Zinc 4.00 U ug/L BGL0206BGL0206-BS1 LCS 13-05605-000 Water 12/10/2018 12/11/2018 EPA 200.8-Dissolved 7440-66-6 Zinc 75.0 ug/L BGL0206

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Analytical Resources, Incorporated

Analytical Chemists and Consultants

Herrera Environmental Consultants

RE: Hydro International

Seattle, WA 98121

2200 6th Avenue, Suite 1100

Dylan Ahearn

Please find enclosed sample receipt documentation and analytical results for samples from the project referenced

above.

Sample analyses were performed according to ARI's Quality Assurance Plan and any provided project specific

Quality Assurance Plan. Each analytical section of this report has been approved and reviewed by an analytical

peer, the appropriate Laboratory Supervisor or qualified substitute, and a technical reviewer.

Should you have any questions or problems, please feel free to contact us at your convenience.

12 December 2018

Associated Work Order(s) Associated SDG ID(s)

18L0049 N/A

-----

I certify that this data package is in compliance with the terms and conditions of the contract, both technically

and for completeness, for other than the conditions detailed in the enclose Narrative. ARI, an accredited

laboratory, certifies that the report results for which ARI is accredited meets all the requirements of the

accrediting body. A list of certified analyses, accreditations, and expiration dates is included in this report.

Release of the data contained in this hardcopy data package has been authorized by the Laboratory Manager or

his/her designee, as verified by the following signature.

Analytical Resources, Inc. The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety.

Cert# 100006

PJLA TestingAccreditation # 66169

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ANALYTICAL REPORT FOR SAMPLES

Sample ID Laboratory ID Matrix Date Sampled Date Received

WUFF-IN-QA 18L0049-01 Water 04-Dec-2018 00:00 04-Dec-2018 16:00

WUFF-IN-QA 18L0049-02 Water 04-Dec-2018 00:00 04-Dec-2018 16:00

WUFF-OUT-QA 18L0049-03 Water 04-Dec-2018 00:00 04-Dec-2018 16:00

WUFF-OUT-QA 18L0049-04 Water 04-Dec-2018 00:00 04-Dec-2018 16:00

Analytical Resources, Inc. The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

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Sample receipt

Samples as listed on the preceding page were received December 4, 2018 under ARI work order 18L0049. For details

regarding sample receipt, please refer to the Cooler Receipt Form. The samples were split by sample receiving prior to

analysis.

Total and Dissolved Metals - EPA Method 200.8

The samples were digested and analyzed within the recommended holding times.

Initial and continuing calibrations were within method requirements.

The method blanks were clean at the reporting limits.

The LCS percent recoveries were within control limits.

Wet Chemistry (O-Phos, T-Phos)

The samples were prepared and analyzed within the recommended holding times.

Initial and continuing calibrations were within method requirements.

The method blanks were clean at the reporting limits.

The LCS percent recoveries were within control limits.

Matrix spikes and duplicates were prepared in conjunction with sample WUFF-IN-QA. The matrix spike percent recoveries

and duplicate RPD were within QC limits.

Work Order Case Narrative

Analytical Resources, Inc. The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety.

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WUFF-IN-QA

18L0049-01 (Water)

Sampled: 12/04/2018 00:00Method: EPA 200.8

Metals and Metallic Compounds

Instrument: ICPMS2 Analyst: MCB Analyzed: 12/06/2018 17:41

Preparation Batch: BGL0137

Prepared: 06-Dec-2018 Final Volume: 25 mL

Preparation Method: REN EPA 600/4-79-020 4.1.4 HNO3 matrixSample Preparation:

Sample Size: 25 mL

Analyte Limit

Reporting

Result Notes UnitsDilutionCAS Number

ND1 ug/L0.5007440-50-8 UCopper

ND1 ug/L4.007440-66-6 UZinc

Analytical Resources, Inc. The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety.

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WUFF-IN-QA

18L0049-01 (Water)

Sampled: 12/04/2018 00:00Method: SM 4500-P E-99

Wet Chemistry

Instrument: UV1800-2 Analyst: YK Analyzed: 12/05/2018 11:23

Preparation Batch: BGL0098

Prepared: 05-Dec-2018 Final Volume: 50 mL

Preparation Method: No Prep Wet ChemSample Preparation:

Sample Size: 50 mL

Limit

Reporting

Result Notes UnitsDilutionAnalyte

Detection

LimitCAS Number

ND1 mg/L0.00400.00401426-54-42 UOrthophosphorus

Preparation Batch: BGL0205

Prepared: 10-Dec-2018 Final Volume: 50 mL

Preparation Method: No Prep Wet ChemSample Preparation:

Sample Size: 25 mL

Limit

Reporting

Result Notes UnitsDilutionAnalyte

Detection

LimitCAS Number

0.01401 mg-P/L0.00800.00807723-14-0Total Phosphorus

Analytical Resources, Inc. The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety.

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WUFF-IN-QA

18L0049-02 (Water)

Sampled: 12/04/2018 00:00Method: EPA 200.8

Metals and Metallic Compounds (dissolved)

Instrument: ICPMS2 Analyst: MCB Analyzed: 12/11/2018 19:57

Preparation Batch: BGL0206

Prepared: 10-Dec-2018 Final Volume: 25 mL

Preparation Method: REN EPA 600/4-79-020 4.1.4 HNO3 matrixSample Preparation:

Sample Size: 25 mL

Analyte Limit

Reporting

Result Notes UnitsDilutionCAS Number

ND1 ug/L0.5007440-50-8 UCopper, Dissolved

ND1 ug/L4.007440-66-6 UZinc, Dissolved

Analytical Resources, Inc. The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety.

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WUFF-OUT-QA

18L0049-03 (Water)

Sampled: 12/04/2018 00:00Method: EPA 200.8

Metals and Metallic Compounds

Instrument: ICPMS2 Analyst: MCB Analyzed: 12/06/2018 17:45

Preparation Batch: BGL0137

Prepared: 06-Dec-2018 Final Volume: 25 mL

Preparation Method: REN EPA 600/4-79-020 4.1.4 HNO3 matrixSample Preparation:

Sample Size: 25 mL

Analyte Limit

Reporting

Result Notes UnitsDilutionCAS Number

0.6251 ug/L0.5007440-50-8Copper

ND1 ug/L4.007440-66-6 UZinc

Analytical Resources, Inc. The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety.

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Reported:

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WUFF-OUT-QA

18L0049-03 (Water)

Sampled: 12/04/2018 00:00Method: SM 4500-P E-99

Wet Chemistry

Instrument: UV1800-2 Analyst: YK Analyzed: 12/05/2018 11:24

Preparation Batch: BGL0098

Prepared: 05-Dec-2018 Final Volume: 50 mL

Preparation Method: No Prep Wet ChemSample Preparation:

Sample Size: 50 mL

Limit

Reporting

Result Notes UnitsDilutionAnalyte

Detection

LimitCAS Number

ND1 mg/L0.00400.00401426-54-42 UOrthophosphorus

Preparation Batch: BGL0205

Prepared: 10-Dec-2018 Final Volume: 50 mL

Preparation Method: No Prep Wet ChemSample Preparation:

Sample Size: 25 mL

Limit

Reporting

Result Notes UnitsDilutionAnalyte

Detection

LimitCAS Number

ND1 mg-P/L0.00800.00807723-14-0 UTotal Phosphorus

Analytical Resources, Inc. The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety.

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Reported:

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Dylan Ahearn

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WUFF-OUT-QA

18L0049-04 (Water)

Sampled: 12/04/2018 00:00Method: EPA 200.8

Metals and Metallic Compounds (dissolved)

Instrument: ICPMS2 Analyst: MCB Analyzed: 12/11/2018 20:02

Preparation Batch: BGL0206

Prepared: 10-Dec-2018 Final Volume: 25 mL

Preparation Method: REN EPA 600/4-79-020 4.1.4 HNO3 matrixSample Preparation:

Sample Size: 25 mL

Analyte Limit

Reporting

Result Notes UnitsDilutionCAS Number

ND1 ug/L0.5007440-50-8 UCopper, Dissolved

ND1 ug/L4.007440-66-6 UZinc, Dissolved

Analytical Resources, Inc. The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety.

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Batch BGL0137 - REN EPA 600/4-79-020 4.1.4 HNO3 matrix

Metals and Metallic Compounds - Quality Control

Instrument: ICPMS2 Analyst: MCB

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes QC Sample/Analyte Isotope

Prepared: 06-Dec-2018 Analyzed: 06-Dec-2018 14:59Blank (BGL0137-BLK1)

0.500ND ug/L UCopper 63

0.500ND ug/L UCopper 65

4.00ND ug/L UZinc 66

4.00ND ug/L UZinc 67

Prepared: 06-Dec-2018 Analyzed: 06-Dec-2018 15:03LCS (BGL0137-BS1)

0.50027.2 80-120109ug/L 25.0Copper 63

0.50027.1 80-120108ug/L 25.0Copper 65

4.0088.3 80-120110ug/L 80.0Zinc 66

4.0083.1 80-120104ug/L 80.0Zinc 67

Analytical Resources, Inc. The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety.

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Batch BGL0206 - REN EPA 600/4-79-020 4.1.4 HNO3 matrix

Metals and Metallic Compounds (dissolved) - Quality Control

Instrument: ICPMS2 Analyst: MCB

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes QC Sample/Analyte Isotope

Prepared: 10-Dec-2018 Analyzed: 11-Dec-2018 17:29Blank (BGL0206-BLK1)

0.500ND ug/L UCopper, Dissolved 63

0.500ND ug/L UCopper, Dissolved 65

4.00ND ug/L UZinc, Dissolved 66

4.00ND ug/L UZinc, Dissolved 67

Prepared: 10-Dec-2018 Analyzed: 11-Dec-2018 17:34LCS (BGL0206-BS1)

0.50026.8 80-120107ug/L 25.0Copper, Dissolved 63

0.50026.8 80-120107ug/L 25.0Copper, Dissolved 65

4.0081.5 80-120102ug/L 80.0Zinc, Dissolved 66

4.0075.0 80-12093.7ug/L 80.0Zinc, Dissolved 67

Analytical Resources, Inc. The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety.

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Reported:

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Batch BGL0098 - No Prep Wet Chem

Wet Chemistry - Quality Control

Instrument: UV1800-2 Analyst: YK

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes QC Sample/Analyte

Detection

Limit

Prepared: 05-Dec-2018 Analyzed: 05-Dec-2018 11:22Blank (BGL0098-BLK1)

0.0040ND mg/L U0.0040Orthophosphorus

Prepared: 05-Dec-2018 Analyzed: 05-Dec-2018 11:23LCS (BGL0098-BS1)

0.00400.155 90-110103mg/L 0.1500.0040Orthophosphorus

Prepared: 05-Dec-2018 Analyzed: 05-Dec-2018 11:24Source: 18L0049-01Duplicate (BGL0098-DUP1)

0.0040ND NDmg/L U0.0040Orthophosphorus

Prepared: 05-Dec-2018 Analyzed: 05-Dec-2018 11:24Source: 18L0049-01Matrix Spike (BGL0098-MS1)

0.00400.101 ND 75-125101mg/L 0.09990.0040Orthophosphorus

Recovery limits for target analytes in MS/MSD QC samples are advisory only.

Analytical Resources, Inc. The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety.

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Batch BGL0205 - No Prep Wet Chem

Wet Chemistry - Quality Control

Instrument: UV1800-2 Analyst: YK

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

Limit Notes QC Sample/Analyte

Detection

Limit

Prepared: 10-Dec-2018 Analyzed: 11-Dec-2018 15:42Blank (BGL0205-BLK1)

0.0080ND mg-P/L U0.0080Total Phosphorus

Prepared: 10-Dec-2018 Analyzed: 11-Dec-2018 15:45Blank (BGL0205-BLK2)

0.0080ND mg-P/L U0.0080Total Phosphorus

Prepared: 10-Dec-2018 Analyzed: 11-Dec-2018 15:43LCS (BGL0205-BS1)

0.00800.300 90-110100mg-P/L 0.3000.0080Total Phosphorus

Prepared: 10-Dec-2018 Analyzed: 11-Dec-2018 15:45LCS (BGL0205-BS2)

0.00800.296 90-11098.7mg-P/L 0.3000.0080Total Phosphorus

Prepared: 10-Dec-2018 Analyzed: 11-Dec-2018 15:44Source: 18L0049-01Duplicate (BGL0205-DUP1)

0.0080ND 0.0140mg-P/L U0.0080Total Phosphorus

Prepared: 10-Dec-2018 Analyzed: 11-Dec-2018 15:44Source: 18L0049-01Matrix Spike (BGL0205-MS1)

0.00800.202 0.0140 75-12594.1mg-P/L 0.2000.0080Total Phosphorus

Recovery limits for target analytes in MS/MSD QC samples are advisory only.

Analytical Resources, Inc. The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety.

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Certified Analyses included in this Report

CertificationsAnalyte

EPA 200.8 in Water

NELAP,WADOE,WA-DW,DoD-ELAPCopper-63

NELAP,WADOE,WA-DW,DoD-ELAPCopper-65

NELAP,WADOE,WA-DW,DoD-ELAPZinc-66

NELAP,WADOE,WA-DW,DoD-ELAPZinc-67

NELAP,WADOE,WA-DW,DoD-ELAPCopper-63

NELAP,WADOE,WA-DW,DoD-ELAPCopper-65

NELAP,WADOE,WA-DW,DoD-ELAPZinc-66

NELAP,WADOE,WA-DW,DoD-ELAPZinc-67

SM 4500-P E-99 in Water

WADOE,NELAPOrthophosphorus

WADOE,NELAPTotal Phosphorus

Code Description Number Expires

17-015Alaska Dept of Environmental Conservation 02/07/2019ADEC

2748California Department of Public Health CAELAP 06/30/2019CALAP

66169DoD-Environmental Laboratory Accreditation Program 02/07/2019DoD-ELAP

66169DoD-Environmental Laboratory Accreditation - Drinking Water 02/07/2019DoD-ELAP DW

WA100006-011ORELAP - Oregon Laboratory Accreditation Program 05/12/2019NELAP

C558WA Dept of Ecology 06/30/2019WADOE

C558Ecology - Drinking Water 06/30/2019WA-DW

Analytical Resources, Inc. The results in this report apply to the samples analyzed in accordance with the

chain of custody document. This analytical report must be reproduced in its

entirety.

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Notes and Definitions

The reported value is from a dilutionD

Estimated concentration value detected below the reporting limit.J

This analyte is not detected above the applicable reporting or detection limit.U

Sample results reported on a dry weight basis

Relative Percent DifferenceRPD

dry

Not ReportedNR

Analyte NOT DETECTED at or above the reporting limitND

Analyte DETECTEDDET

[2C] Indicates this result was quantified on the second column on a dual column analysis.

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