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Federal Aviation Administration COMPOSITE MATERIAL FIRE FIGHTING Presented to: The Sixth Triennial International Fire & Cabin Safety Research Conference Atlantic City, New Jersey Presented by: John C. Hode SRA International Date: October 25-28, 2010

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Page 1: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Federal AviationAdministration

COMPOSITE MATERIAL FIRE FIGHTING

Presented to: The Sixth Triennial International Fire & Cabin Safety Research Conference

Atlantic City, New Jersey

Presented by: John C. HodeSRA International

Date: October 25-28, 2010

Page 2: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch2Federal Aviation

AdministrationOctober 25-28, 2010

Creation of a Test MethodFirst objective:• Determine if self-sustained

combustion or smoldering will occur.

• Determine the time to naturally cool below 300°F (150°C)

Second objective:Determine how much fire agent is needed to extinguish visible fire and cool the material sufficiently to prevent re-ignition.

Exposure times of Initial tests:• 10, 5, 3, 2, & 1 minutes

– FAR Part 139 requires first due ARFF to arrive in 3 minutes.– Actual response times can be longer or shorter.

Page 3: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch3Federal Aviation

AdministrationOctober 25-28, 2010

Initial Test Set-up

Page 4: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch4Federal Aviation

AdministrationOctober 25-28, 2010

Initial Findings1. Post-exposure flaming

reduces quickly without heat source

2. Off-gassing causes pressurization inside the panel causing swelling

3. Internal off-gassing can suddenly and rapidly escape

4. Off-gas/smoke can be ignited

5. Longer exposures burn away more resin binder

6. Smoldering can occur7. Smoldering areas can cause

re-ignition8. Smoldering temperatures

can be near that of fuel fires9. Fibers can be oxidized by

high temperatures and sufficient oxygen

10. Insulated areas cooled much more slowly than uninsulated areas

Page 5: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch5Federal Aviation

AdministrationOctober 25-28, 2010

Small & Intermediate Scale Testing

Small-scale and Intermediate-scale testing being conducted by Hughes Associates Inc.

(HAI).

Page 6: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch6Federal Aviation

AdministrationOctober 25-28, 2010

Small & Intermediate Scale Testing• Baseline intermediate scale tests will be conducted to

see if results from Phase I are repeatable with Phase II test design.

• Small scale tests– ASTM E1354 Cone Calorimeter

• Data to support exterior fuselage flame propagation/spread modeling

– ASTM E1321 Lateral Flame Spread Testing (Lateral flame spread)

• Thermal Decomposition Modeling– Thermal Decomposition Apparatus (TDA)– Thermal Gravimetric Analysis (TGA)– Differential Scanning Calorimetry (DSC)– Pyrolysis Gas Chromatograph/Mass Spectroscopy (PY-

GC/MS)

Page 7: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch7Federal Aviation

AdministrationOctober 25-28, 2010

Small & Intermediate Scale Testing cont

• Intermediate scale tests (agent application to be tested at this scale)– Three different heat sources evaluated

• Propane fired area burner (2 sizes)• Propane torch• Radiant heater

– Sample panels are 4 feet wide by 6 feet tall• Protection added to test rig to avoid edge effects.

– A representative backside insulation was used in several tests.

Page 8: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch8Federal Aviation

AdministrationOctober 25-28, 2010

Small & Intermediate Scale Materials

• CFRP– Unidirectional T-800/350oF cure epoxy, 16 ply quasi-

isotropic [0,-45,45,90]S2, nominal thickness of 3.2 mm (0.126 inch) Finished 60/40 fiber-resin

• OSB– Georgia Pacific Blue Ribbon®, nominal thickness of

14.7 mm (0.578 inches)– Flame spread rating of 150-200

Page 9: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch9Federal Aviation

AdministrationOctober 25-28, 2010

Composite Skin Fire Characteristics and Suppression • Approach

– Small scale materials testing

– Results feed into fire model of combustion and propagation

– Intermediate scale tests• Reduce reliance on large

tests– Materials

• Composite ( CFRP -B787)• Aluminum/plastic (GLARE –

A380)• Surrogate – (wood board)

Page 10: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch10Federal Aviation

AdministrationOctober 25-28, 2010

ASTM E1321 Lateral Ignition & Flame Spread

• Wood was the only material in which lateral flame spread was observed

• CFRP and GLARE –some burning at seams

OSB

CFRP

GLARE

Page 11: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch11Federal Aviation

AdministrationOctober 25-28, 2010

Small Scale Tests - Combustibility

• Composite Skin Materials Have Similar or Lower Combustible Properties compared to “Ordinary”Combustibles

• Compared to wood, composites:– Require more imposed

energy to ignite– Ignite slower – Have a shorter duration of

burning( due to smaller thickness)

For 100 kW/m2 Exposure

Sample

Minimum Heat Flux

for Ignition (kW/m2)

Tim to Ignition

(sec)

Burning Duration

(sec)

Avg. HRR (kW/m2)

OSB 12 8 490 172

CFRP 16 29 113 153

GLARE 25 82.5 129 66.5

Page 12: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch12Federal Aviation

AdministrationOctober 25-28, 2010

Intermediate Test Series

12 total tests conducted• 9 with OSB

– 1 uninsulated– 8 insulated

• 3 with CFRP– 1 uninsulated– 2 insulated

Hood Calorimeter

Non-Combustible Mounting Wall

Propane Burner (Exposure Fire)

Water Suppression System

Test Panel

Hood Calorimeter

Non-Combustible Mounting Wall

Propane Burner (Exposure Fire)

Water Suppression System

Test Panel

Page 13: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch13Federal Aviation

AdministrationOctober 25-28, 2010

Intermediate-Scale Propane Area Burners

High Heat Flux Uniform Exposureq"e = 70 – 100 kW/m2

Low Heat Flux Uniform Exposureq"e = 35 – 70 kW/m2

Page 14: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch14Federal Aviation

AdministrationOctober 25-28, 2010

Small Area Exposure Large Area Exposure

Page 15: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch15Federal Aviation

AdministrationOctober 25-28, 2010

Intermediate-Scale Propane Torches

High Heat Flux Localized Exposureq"e = 120 – 200 kW/m2

Page 16: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch16Federal Aviation

AdministrationOctober 25-28, 2010

Torch (180kW/m2) Exposure Radiant Panel (100kW/m2) Exposure

Page 17: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch17Federal Aviation

AdministrationOctober 25-28, 2010

Large Area Burner On Burner Off – 0 seconds Burner Off – 30 seconds

Burner Off – 60 seconds Burner Off – 100 seconds

OSB Exposed to Large Area Burner with Insulation Backing

Page 18: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch18Federal Aviation

AdministrationOctober 25-28, 2010

Torch Ignition 1 minute after ignition 1.5 minutes after ignition

2.5 minutes after ignition 4 minutes after ignitionTorches Out

15 seconds after torches out

CFRP Exposed to Torch Burner with Insulation Backing

Page 19: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch19Federal Aviation

AdministrationOctober 25-28, 2010

Comparison of CFRP & OSB Heat Release

Page 20: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch20Federal Aviation

AdministrationOctober 25-28, 2010

Intermediate Scale Findings•Vertical/Lateral flame spread only occurred during exposure

•Post-exposure flaming reduced quickly without heat source

•Ignition occurred quickly into exposure

•Generally, time to ignition & HRR are consistent with cone calorimeter data

Page 21: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch21Federal Aviation

AdministrationOctober 25-28, 2010

CFRP Torch Test

• Exposure 180 kW/m2• Duration 250 seconds (4 min 10 sec)• Panel Ignition at 16 seconds• HRR increased after ignition to peak of 300

kW over 60 seconds• HRR decayed after 90 seconds to steady-

state value of 50 kW• Post-exposure burning for 37 seconds

Page 22: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch22Federal Aviation

AdministrationOctober 25-28, 2010

Intermediate Scale Test Conclusions

• OSB vs. CFRP

– Both materials burn and spread flame when exposed to large fire

– Heat release rates and ignition times similar

– The thicker OSB contributed to longer burning

• Large Scale Implications– OSB can be used as a

surrogate for CFRP– Flaming and combustion

does not appear to continue after exposure is removed

• Since there was no or very little post exposure combustion, no suppression tests performed as planned

• Minimal agent for suppression of intact aircraft?

Page 23: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch23Federal Aviation

AdministrationOctober 25-28, 2010

Qualifiers to Intermediate Scale Results

• Need to check GLARE– No significant surface burning

differences anticipated ( may be better than CFRP)

• Verify /check CFRP for thicker areas (longer potential burning duration)

• Evaluate edges/separations– Wing control surfaces– Engine nacelle– Stiffeners– Post –crash debris scenario

Can a well established fire develop in a post-crash environment?

EXAMPLE COMPLEX GEOMETRY FIRE TEST

SETUP FOR CFRP FLAMMABILITY EVALUATION.

Page 24: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch24Federal Aviation

AdministrationOctober 25-28, 2010

Flame Spread Modeling Analysis

• Analytical tool developed– Calculates flame spread on vertical

and horizontal surfaces– Multiple exposures

• External flux/flame radiation• Hot gas layer

– Predicts heat release rate and flame spread

– Input data developed from small scale tests

Page 25: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch25Federal Aviation

AdministrationOctober 25-28, 2010

Model Validation• Intermediate scale tests with ORP and CFRP

– Radiant panel/line burner/torch exposures

• Wood tests (literature) with accelerating and decelerating flame spread conditions

Time (minutes)0 5 10 15 20 25 30

Flam

e Sp

read

Dis

tanc

e (m

)

0.0

0.2

0.4

0.6

0.8

1.0

Flam

e Sp

read

Dis

tanc

e (ft

)

0.0

0.5

1.0

1.5

2.0

2.5

3.0 Predicted, Flame Spread Model (insulated panel back)Predicted, Flame Spread Model (back exposed to ambient)

Estimated spread distance in CFRP panel tests 

Heat release rate (CFRP radiant panel test)Flame spread distance (CFRP radiant panel test)

Time (minutes)0 10 20 30 40

Hea

t Rel

ease

Rat

e (k

W)

0

10

20

30

40

50

60

70

Hea

t Rel

ease

Rat

e (B

tu/s

)

0

10

20

30

40

50

60

Measured, uninsulated panel backMeasured, panel back insulated with gypsum wallboardPredicted, Uninsulated panel backPredicted, panel back insulated with gypsum wallboard

Page 26: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch26Federal Aviation

AdministrationOctober 25-28, 2010

Modeling Analysis of Aircraft Skin

• Twenty configurations evaluated (parameter variation)– Skin panel dimensions, exposure fires, exposure durations,

exposure fire suppression rate• Hydrocarbon pool fire exposures (JP-5) – skin

immersed, peak fluxes 135 – 180 kW/m²• Vertical panel (no curvature)• Flame spread not predicted beyond area initially

ignited by pool• Some vertical flame propagation after exposure fire suppressed• No significant lateral flame propagation after exposure fire

suppressed• Heat release rate decreases rapidly after suppression• Results not significantly affected by scenario parameters

Page 27: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch27Federal Aviation

AdministrationOctober 25-28, 2010

Flame Spread Model – Typical Result

• Heat Release Rate – 10 MW exposure fire/ 20 ft tall panel

• 2 minute exposure, rapid suppression

• Lateral propagation stops when fire suppressed

• Fire does not propagate to top of panels

• OSB and CFRP similar propagation behavior

• OSB has higher heat release rate after suppression

• OSB ignites faster and has a faster initial spread

Time (minutes)

0 1 2 3 4 5 6

Skin

Hea

t Rel

ease

Rat

e (k

W)

0

500

1000

1500

2000

2500

Skin

Hea

t Rel

ease

Rat

e (B

tu/s

)

0

500

1000

1500

2000

CFRPOSB

Page 28: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch28Federal Aviation

AdministrationOctober 25-28, 2010

Preliminary Modeling Conclusions• Fire propagation is not predicted for large scale fires

exposing vertical CFRP and OSB panels• OSB and CFRP have similar flame propagation and peak

heat release rates, but OSB has higher heat release rate after pool fire suppression and allows faster initial spread

• Modeling did not consider three-dimensional configurations (wing-fuselage connection)

• Fuselage treated as vertical flat surface – future flame spread model revisions could account for curvature

• Thermal penetration after ignition yet to be performed –decomposition model plus intermediate validation data will be used for this

Page 29: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch29Federal Aviation

AdministrationOctober 25-28, 2010

Overall Findings

• Flame propagation and self-sustained flaming does not significantly occur in the absence of external fire source.

• Epoxy off-gas is combustible.• CFRP can smolder.• Epoxy off-gas causes composite to swell

through internal pressurization.• OSB is potential surrogate for large scale tests

to assess extinguishment test methods to save composites for data collection.

Page 30: Federal Aviation COMPOSITE MATERIAL FIRE FIGHTING · Federal Aviation 27 October 25-28, 2010 Administration Flame Spread Model – Typical Result • Heat Release Rate – 10 MW exposure

Airport Technology Research & Development Branch30Federal Aviation

AdministrationOctober 25-28, 2010

Participation welcome• Soliciting comments and ideas on:

– Potential test configurations– Relevant previous testing results and data– Sources for aviation-type carbon fiber composites

and FML– Other helpful ideas