field/lab analytical procedures and equipment detail

1434
December 13, 2007 14:55:01 Field/Lab Analytical Procedures and Equipment Detail Page 1 of 1434 0800257 Procedure Source Procedure ID Procedure Name Citation Equipment Comparable National Procedure ID Clear Creek Superfund Status Unknown, 19--, No Cite - Method Not Cited, Unknown, Vol -- American Public Health Association, 1992, Standard Methods for the Examination of Water and Wastewater, 18th Edition., American Public Health Association, 18th Edition USEPA, 1994, Methods for the Determination of Metals in Environmental Samples, Supplement I, USEPA, EPA 600-R-94-111 USEPA, 1994, Methods for the Determination of Metals in Environmental Samples, Supplement I, USEPA, EPA 600-R-94-111 USEPA, 1994, Methods for the Determination of Metals in Environmental Samples, Supplement I, USEPA, EPA 600-R-94-111 USEPA, 1994, Methods for the Determination of Metals in Environmental Samples, Supplement I, USEPA, EPA 600-R-94-111 USEPA, 1994, Methods for the Determination of Metals in Environmental Samples, Supplement I, USEPA, EPA 600-R-94-111 USEPA, 1993, Methods for the Determination of Titration Apparatus Inductively Coupled Plasma Combined with Mass Spectrophotom e Inductively Coupled Plasma Combined with Mass Spectrophotom e Inductively Coupled Plasma Spectrophotom eter Temperature Stabilized Graphite Furnace AA Spectrophotom eter Cold Vapor Atomic Absorption Spectrophotom eter Ion 0800257 APHA USEPA USEPA USEPA USEPA USEPA USEPA UNKNOWN 2340 200.7(S) 200.7(W) 200.8(W) 200.9 245.1 300(A) Unknown Hardness in Water by EDTA Titration Metals in Soil by ICP-AES Metals in Water by ICP- AES Metals in Waters by ICP/MS Metals by Temperature Stabilized GFAA Mercury in Water by CVAA Inorganic Anions by Ion Active Active Active Active Active Active Active Active

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  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 1 of 1434

    0800257

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    Clear Creek Superfund

    Status

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1993, Methods for the Determination of

    TitrationApparatus

    InductivelyCoupledPlasmaCombined withMassSpectrophotome

    InductivelyCoupledPlasmaCombined withMassSpectrophotome

    InductivelyCoupledPlasmaSpectrophotometer

    TemperatureStabilizedGraphiteFurnace AASpectrophotometer

    Cold VaporAtomicAbsorptionSpectrophotometer

    Ion

    0800257

    APHA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    UNKNOWN

    2340

    200.7(S)

    200.7(W)

    200.8(W)

    200.9

    245.1

    300(A)

    Unknown

    Hardness in Water byEDTA Titration

    Metals in Soil by ICP-AES

    Metals in Water by ICP-AES

    Metals in Waters byICP/MS

    Metals by TemperatureStabilized GFAA

    Mercury in Water by CVAA

    Inorganic Anions by Ion

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 2 of 1434

    0800257

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    Clear Creek Superfund

    Status

    Inorganic Substances in EnvironmentalSamples, USEPA, EPA 600/R-93-100

    USEPA, 1993, EPA Contract LaboratoryProgram Water Quality Parameters in Multi-Concentration Water, USEPA, CLP_WQP

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    USEPA, 1986, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition., USEPA, EPA 530/SW-846

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    Chromatograph

    IonChromatograph

    TitrationApparatus

    InductivelyCoupledPlasmaSpectrophotometer

    GraphiteFurnace AtomicAbsorptionSpectrophotometer

    GraphiteFurnace AtomicAbsorptionSpectrophotometer

    Capillary GasChromatographwith MassSpectrophotometer

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    300_M

    310.1

    6020

    7060A

    7740

    8260A

    Chromatography

    Determination of Anions byIC

    Alkalinity by Titration

    Inductively CoupledPlasma - Mass Spec.

    Arsenic by GFAA

    Selenium in VariousMatrices by GFAA

    Volatile Organics in Wasteby CGC/MS

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 3 of 1434

    0800597

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    Ogden Railyard (US EPA Region 8)

    Status

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Society for Testing of Materials, 1994,ASTM Standards. Water and EnvironmentalTechnology (II), American Society for Testingand Materials, Vol 11.02

    Hach Chemical Company, 1992, Hach WaterAnalysis Handbook., HACH ChemicalCompany, 2nd Edition

    National Institute for Occupational Safety andHealth, 1994, NIOSH Manual of AnalyticalMethods, 4th Edition,, National Institute forOccupational Safety and Health, 4th Edition

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 19--, CLP SOW for InorganicsAnalysis-IHC01_3, USEPA, IHC01_3

    LaboratoryBalance

    Total OrganicCarbon -Coulometry

    Spectrophotometer

    GasChromatograph

    TitrationApparatus

    pH meter

    0800597

    0800597

    0800597

    0800597

    0800597

    0800597

    0800597

    APHA

    ASTM

    HACH

    NIOSH

    USEPA

    USEPA

    1668

    OLM04.2 -BNA SI

    OLM04.2 -PEST

    OLM04.2 -SVOA

    TO-14

    TO-14 SIM

    UNKNOWN

    2540-G

    D4129

    8021

    1005

    130.2

    150.2_M

    1668

    OLM04.2-BNA SIM

    OLM04.2-PEST/PCB

    OLM04.2-SVOA

    TO-14

    TO-14 SIM

    UNKNOWN

    Total, Fixed and VolatileSolids

    Total Carbon and OrganicCarbon in Water

    Free Chlorine in Water byDPD

    Methylene Chloride byGC/FID

    Total Hardness

    pH in Industrial WasteMaterials

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 4 of 1434

    0800597

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    Ogden Railyard (US EPA Region 8)

    Status

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1993, Methods for the Determination ofInorganic Substances in EnvironmentalSamples, USEPA, EPA 600/R-93-100

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1993, Methods for the Determination ofInorganic Substances in EnvironmentalSamples, USEPA, EPA 600/R-93-100

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1992, Methods for the Determination ofOrganic Compounds in Drinking Water,Supplement II, USEPA, EPA 600/R-92-129

    LaboratoryBalance

    LaboratoryBalance

    LaboratoryBalance

    InductivelyCoupledPlasmaCombined withMassSpectrophotome

    IonChromatograph

    TitrationApparatus

    Colorimeter

    Spectrophotometer

    Total OrganicCarbon - Infra-Red Detector

    Capillary GasChromatographwith MassSpectrophotometer

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    160.1

    160.2

    160.3

    200.7(W)

    300(A)

    310.1

    353.2

    354.1

    415.1

    524.2

    Filterable Residue - TDS

    Non-Filterable Residue -TSS

    Total Residue

    Metals in Water by ICP-AES

    Inorganic Anions by IonChromatography

    Alkalinity by Titration

    Nitrate-Nitrite Nitrogen byColorimetry

    Nitrite Nitrogen bySpectophotometry

    Total Organic Carbon byCombustion

    Purgeable Organics inWater by CGC/MS

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 5 of 1434

    0800597

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    Ogden Railyard (US EPA Region 8)

    Status

    USEPA, 1992, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update I., USEPA, SW-846_I

    USEPA, 1998, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, 3rdEdition, Final Update III., USEPA, SW-846_III

    USEPA, 19--, Guidelines Establishing TestProcedures for the Analysis of Pollutants.,USEPA, 40 CFR Part 136

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    USEPA, 1992, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update I., USEPA, SW-846_I

    USEPA, 1992, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update I., USEPA, SW-846_I

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    USEPA, 1994, Test Methods for Evaluating

    InductivelyCoupledPlasmaCombined withMassSpectrophotome

    InductivelyCoupledPlasmaCombined withMassSpectrophotome

    GC withPhotoionizationDetector

    InductivelyCoupledPlasmaSpectrophotometer

    Flame AtomicAbsorptionSpectrophotometer

    GraphiteFurnace AtomicAbsorptionSpectrophotometer

    Cold VaporAtomicAbsorptionSpectrophotometer

    Cold Vapor

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    6010A

    6010B

    602

    6020

    7000A(FLAA)

    7000A(GFAA)

    7470A

    7471A

    ICP Spectroscopy

    Inductively CoupledPlasma AES

    Purgeable Aromatics inWastewater by GC

    Inductively CoupledPlasma - Mass Spec.

    Atomic Absorption - FLAA

    Atomic Absorption - GFAA

    Mercury in Liquid Wastesby CVAA

    Mercury in Solid or

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 6 of 1434

    0800597

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    Ogden Railyard (US EPA Region 8)

    Status

    Solid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    USEPA, 1998, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, 3rdEdition, Final Update III., USEPA, SW-846_III

    USEPA, 1998, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, 3rdEdition, Final Update III., USEPA, SW-846_III

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    USEPA, 1998, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, 3rdEdition, Final Update III., USEPA, SW-846_III

    USEPA, 1998, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, 3rdEdition, Final Update III., USEPA, SW-846_III

    USEPA, 1998, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, 3rdEdition, Final Update III., USEPA, SW-846_III

    USEPA, 1998, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, 3rdEdition, Final Update III., USEPA, SW-846_III

    USEPA, 1998, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, 3rdEdition, Final Update III., USEPA, SW-846_III

    AtomicAbsorptionSpectrophotometer

    No equipment

    GC with FlameIonizationDetector

    GC withElectrolyticConductivityDetector

    Capillary GCElectronCaptureDetector

    Capillary GasChromatographwith MassSpectrophotometer

    Capillary GasChromatographwith MassSpectrophotometer

    Capillary GasChromatographwith MassSpectrophotometer

    No equipment

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    8000B

    8015B

    8080A

    8082(W)

    8260B

    8270C(S)

    8270C(W)

    9012A

    Semisolid Waste

    Organic Compounds byGas Chromatography

    Non-Halogenated OrganicsUsing GC/FID

    Pesticides and PCBs

    PCBs as Aroclors byCapillary Column GC

    Volatile Organics byCGC/MS

    Semivolatile OrganicCompounds by CGC/MS

    Semivolatile OrganicCompounds by CGC/MS

    Total and AmenableCyanide (Auto UV)

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 7 of 1434

    0800597

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    Ogden Railyard (US EPA Region 8)

    Status

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    USEPA, 1986, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition., USEPA, EPA 530/SW-846

    USEPA, 1986, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition., USEPA, EPA 530/SW-846

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    pH meter

    pH meter

    Total OrganicCarbon - Infra-Red Detector

    LaboratoryBalance

    LaboratoryBalance

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    9040A

    9045B

    9060

    9070

    9071A

    pH in Water byElectrometricMeasurement

    Soil and Waste pH

    Total Organic Carbon inWater and Waste

    Total Recoverable Oil andGrease

    Oil and Grease in Sludgeand Sediment

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 8 of 1434

    0800650

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    International Smelter (US EPA Region 8)

    Status

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1993, Methods for the Determination ofInorganic Substances in EnvironmentalSamples, USEPA, EPA 600/R-93-100

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1998, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, 3rdEdition, Final Update III., USEPA, SW-846_III

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-

    LaboratoryBalance

    LaboratoryBalance

    IonChromatograph

    pH meter

    TitrationApparatus

    InductivelyCoupledPlasmaCombined withMassSpectrophotome

    InductivelyCoupledPlasmaSpectrophotometer

    Cold VaporAtomicAbsorptionSpectrophotometer

    Cold VaporAtomic

    0800650

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    UNKNOWN

    160.1

    160.2

    300(A)

    305.1

    310.1

    6010B

    6020

    7470A

    7471A

    Unknown

    Filterable Residue - TDS

    Non-Filterable Residue -TSS

    Inorganic Anions by IonChromatography

    Acidity by Titration with apH Meter

    Alkalinity by Titration

    Inductively CoupledPlasma AES

    Inductively CoupledPlasma - Mass Spec.

    Mercury in Liquid Wastesby CVAA

    Mercury in Solid orSemisolid Waste

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 9 of 1434

    0800650

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    International Smelter (US EPA Region 8)

    Status

    846, 3rd Edition, Final Update II., USEPA, SW-846_II

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    AbsorptionSpectrophotometer

    pH meter

    pH meter

    USEPA

    USEPA

    9040A

    9045B

    pH in Water byElectrometricMeasurement

    Soil and Waste pH

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 10 of 1434

    0800852

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    Mystery Bridge Road - US Highway 20

    Status

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    USEPA, 1998, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, 3rdEdition, Final Update III., USEPA, SW-846_III

    Capillary GCwithPhotoionizationDetector

    Capillary GasChromatographwith MassSpectrophotometer

    0800852

    USEPA

    USEPA

    UNKNOWN

    8021A(PID)

    8260B

    Unknown

    Halo and AromaticVolatiles - CGC/PID

    Volatile Organics byCGC/MS

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 11 of 1434

    0801194

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    Summitville Superfund site (US EPA Region 8)

    Status

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    TitrationApparatus

    InductivelyCoupledPlasmaCombined withMassSpectrophotome

    InductivelyCoupledPlasmaSpectrophotometer

    TemperatureStabilizedGraphiteFurnace AASpectrophotometer

    0801194

    APHA

    USEPA

    USEPA

    USEPA

    UNKNOWN

    2340

    200.7(W)

    200.8(W)

    200.9

    Unknown

    Hardness in Water byEDTA Titration

    Metals in Water by ICP-AES

    Metals in Waters byICP/MS

    Metals by TemperatureStabilized GFAA

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 12 of 1434

    0801417

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    Red Mountain Pass Zinc (US EPA Region 8)

    Status

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    0801417 UNKNOWN

    UnknownActive

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 13 of 1434

    0801478

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    California Gulch (US EPA Region 8)

    Status

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,

    TitrationApparatus

    TitrationApparatus

    LaboratoryBalance

    Flame AtomicAbsorptionSpectrophotometer

    No equipment

    No equipment

    Flame Atomic

    0801478

    0801478

    0801478

    0801478

    0801478

    APHA

    APHA

    APHA

    APHA

    APHA

    APHA

    APHA

    200.2

    ILM05

    ILM05.3

    SOLIDCALC

    UNKNOWN

    2320

    2340

    2540-G

    3500-AG(B)

    3500-AL(B)

    3500-AS(B)

    3500-CA(B)

    Cal Gulch Procedure

    ILM05

    ILM05.3

    Cal Gulch Procedure

    Unknown

    Alkalinity in Water byTitration

    Hardness in Water byEDTA Titration

    Total, Fixed and VolatileSolids

    Silver in Water by FLAA orGFAA

    Aluminum in Water byFLAA or GFAA

    Arsenic in Water by GFAAor HYDAA

    Calcium in Water by FLAA

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 14 of 1434

    0801478

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    California Gulch (US EPA Region 8)

    Status

    Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,

    AbsorptionSpectrophotometer

    No equipment

    Flame AtomicAbsorptionSpectrophotometer

    No equipment

    Flame AtomicAbsorptionSpectrophotometer

    Flame AtomicAbsorptionSpectrophotometer

    Hydride AtomicAbsorptionSpectrophotometer

    Spectrophotometer

    TitrationApparatus

    No equipment

    APHA

    APHA

    APHA

    APHA

    APHA

    APHA

    APHA

    APHA

    APHA

    3500-CD(B)

    3500-CU(B)

    3500-FE(B)

    3500-MN(B)

    3500-PB(B)

    3500-SE(C)

    3500-ZN(D)

    4500-CL-(B)

    4500-CN(C)

    Cadmium in Water byFLAA/GFAA

    Copper in Water by FLAAor GFAA

    Iron in Water by FLAA orGFAA

    Manganese in Water byFLAA or GFAA

    Lead in Water by FLAA orGFAA

    Selenium in Water byHYDAA

    Zinc in Water bySpectrophotometry

    Chloride in Water byTitration- ArgentometricMethod

    Cyanide in Water after

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 15 of 1434

    0801478

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    California Gulch (US EPA Region 8)

    Status

    Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    USDOI, USGS, 19--, Methods for Determinationof Inorganic Substances in Water and FluvialSediments, Book 5, Chapter A1., USDOI,USGS, Book 5, Chapter A1

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    LaboratoryBalance

    AutoAnalyzer

    ConductivityBridge

    pH meter

    LaboratoryBalance

    LaboratoryBalance

    InductivelyCoupledPlasmaCombined withMassSpectrophotome

    InductivelyCoupledPlasmaCombined withMassSpectrophotome

    APHA

    USDOI/USGS

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    4500-SO4(D)

    I2700

    120.1

    150.1

    160.1

    160.2

    200.7(S)

    200.7(W)

    Distillation

    Sulfate in Water byGravimetric Analysis

    Silica in Water byColorimetry

    Conductance

    pH

    Filterable Residue - TDS

    Non-Filterable Residue -TSS

    Metals in Soil by ICP-AES

    Metals in Water by ICP-AES

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 16 of 1434

    0801478

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    California Gulch (US EPA Region 8)

    Status

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    InductivelyCoupledPlasmaSpectrophotometer

    InductivelyCoupledPlasmaSpectrophotometer

    TemperatureStabilizedGraphiteFurnace AASpectrophotometer

    Flame AtomicAbsorptionSpectrophotometer

    GraphiteFurnace AtomicAbsorptionSpectrophotometer

    Flame AtomicAbsorptionSpectrophotometer

    GraphiteFurnace AtomicAbsorptionSpectrophotometer

    Flame AtomicAbsorptionSpectrophotom

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    200.8(S)

    200.8(W)

    200.9

    202.1

    206.2

    213.1

    213.2

    220.1

    Metals in Wastes byICP/MS

    Metals in Waters byICP/MS

    Metals by TemperatureStabilized GFAA

    Aluminum by FLAA

    Arsenic by GFAA

    Cadmium by FLAA

    Cadmium by GFAA

    Copper by FLAA

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 17 of 1434

    0801478

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    California Gulch (US EPA Region 8)

    Status

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    eter

    GraphiteFurnace AtomicAbsorptionSpectrophotometer

    Flame AtomicAbsorptionSpectrophotometer

    Flame AtomicAbsorptionSpectrophotometer

    GraphiteFurnace AtomicAbsorptionSpectrophotometer

    Flame AtomicAbsorptionSpectrophotometer

    Cold VaporAtomicAbsorptionSpectrophotometer

    Flame AtomicAbsorptionSpectrophotometer

    GraphiteFurnace AtomicAbsorptionSpectrophotometer

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    220.2

    236.1

    239.1

    239.2

    242.1

    245.1

    272.1

    272.2

    Copper by GFAA

    Iron by FLAA

    Lead by FLAA

    Lead by GFAA

    Magnesium by FLAA

    Mercury in Water by CVAA

    Silver by FLAA

    Silver by GFAA

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 18 of 1434

    0801478

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    California Gulch (US EPA Region 8)

    Status

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1993, Methods for the Determination ofInorganic Substances in EnvironmentalSamples, USEPA, EPA 600/R-93-100

    USEPA, 1993, Methods for the Determination ofInorganic Substances in EnvironmentalSamples, USEPA, EPA 600/R-93-100

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1993, Methods for the Determination ofInorganic Substances in EnvironmentalSamples, USEPA, EPA 600/R-93-100

    USEPA, 1993, Methods for the Determination ofInorganic Substances in EnvironmentalSamples, USEPA, EPA 600/R-93-100

    USEPA, 1993, Methods for the Determination ofInorganic Substances in EnvironmentalSamples, USEPA, EPA 600/R-93-100

    USEPA, 1993, Methods for the Determination ofInorganic Substances in EnvironmentalSamples, USEPA, EPA 600/R-93-100

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    Flame AtomicAbsorptionSpectrophotometer

    GraphiteFurnace AtomicAbsorptionSpectrophotometer

    IonChromatograph

    IonChromatograph

    TitrationApparatus

    AutoAnalyzer

    Colorimeter

    Colorimeter

    Colorimeter

    Colorimeter

    LaboratoryBalance

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    273.1

    289.2

    300(A)

    300(B)

    310.1

    325.2

    335.4

    353.2

    365.1

    375.2

    375.3

    Sodium by FLAA

    Zinc by GFAA

    Inorganic Anions by IonChromatography

    Inorganic Anions by IonChromatography

    Alkalinity by Titration

    Chloride by ColorimetricAnalysis II

    Cyanide by Semi-Automated Colorimetry

    Nitrate-Nitrite Nitrogen byColorimetry

    Phosphorus by Colorimetry

    Sulfate in Water byColorimetry

    Sulfate by GravimetricDetermination

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 19 of 1434

    0801478

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    California Gulch (US EPA Region 8)

    Status

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1992, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update I., USEPA, SW-846_I

    USEPA, 1998, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, 3rdEdition, Final Update III., USEPA, SW-846_III

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    USEPA, 1992, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-

    Turbidimeter

    Total OrganicCarbon - Infra-Red Detector

    InductivelyCoupledPlasmaCombined withMassSpectrophotome

    InductivelyCoupledPlasmaCombined withMassSpectrophotome

    InductivelyCoupledPlasmaSpectrophotometer

    GraphiteFurnace AtomicAbsorptionSpectrophotometer

    GraphiteFurnace AtomicAbsorptionSpectrophotometer

    GraphiteFurnace Atomic

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    375.4

    415.1

    6010A

    6010B

    6020

    7060A

    7131A

    7211

    Sulfate by TurbidimetricDetermination

    Total Organic Carbon byCombustion

    ICP Spectroscopy

    Inductively CoupledPlasma AES

    Inductively CoupledPlasma - Mass Spec.

    Arsenic by GFAA

    Cadmium by GFAA

    Copper by GFAA

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 20 of 1434

    0801478

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    California Gulch (US EPA Region 8)

    Status

    846, 3rd Edition, Final Update I., USEPA, SW-846_I

    USEPA, 1986, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition., USEPA, EPA 530/SW-846

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    USEPA, 1992, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update I., USEPA, SW-846_I

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    USEPA, 1986, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition., USEPA, EPA 530/SW-846

    AbsorptionSpectrophotometer

    GraphiteFurnace AtomicAbsorptionSpectrophotometer

    Cold VaporAtomicAbsorptionSpectrophotometer

    GraphiteFurnace AtomicAbsorptionSpectrophotometer

    pH meter

    ConductivityBridge

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    7421

    7471A

    7761

    9040A

    9050

    Lead by GFAA

    Mercury in Solid orSemisolid Waste

    Silver by GFAA

    pH in Water byElectrometricMeasurement

    Specific Conductance

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 21 of 1434

    0801505

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    French Gulch Superfund site (US EPA Region 8)

    Status

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1983, Methods for Chemical Analysis

    TitrationApparatus

    TitrationApparatus

    Hydride AtomicAbsorptionSpectrophotometer

    ConductivityBridge

    pH meter

    LaboratoryBalance

    InductivelyCoupledPlasmaCombined withMassSpectrophotome

    InductivelyCoupledPlasmaSpectrophotometer

    Graphite

    0801505

    APHA

    APHA

    APHA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    UNKNOWN

    2320

    2340

    3500-SE(C)

    120.1

    150.1

    160.1

    200.7(W)

    200.8(W)

    204.2

    Unknown

    Alkalinity in Water byTitration

    Hardness in Water byEDTA Titration

    Selenium in Water byHYDAA

    Conductance

    pH

    Filterable Residue - TDS

    Metals in Water by ICP-AES

    Metals in Waters byICP/MS

    Antimony by GFAA

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 22 of 1434

    0801505

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    French Gulch Superfund site (US EPA Region 8)

    Status

    of Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1993, Methods for the Determination ofInorganic Substances in EnvironmentalSamples, USEPA, EPA 600/R-93-100

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1993, Methods for the Determination ofInorganic Substances in EnvironmentalSamples, USEPA, EPA 600/R-93-100

    USEPA, 1993, Methods for the Determination ofInorganic Substances in EnvironmentalSamples, USEPA, EPA 600/R-93-100

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    Furnace AtomicAbsorptionSpectrophotometer

    GraphiteFurnace AtomicAbsorptionSpectrophotometer

    GraphiteFurnace AtomicAbsorptionSpectrophotometer

    IonChromatograph

    TitrationApparatus

    AutoAnalyzer

    Colorimeter

    Colorimeter

    LaboratoryBalance

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    206.2

    279.2

    300(A)

    310.1

    325.2

    353.2

    365.1

    375.3

    Arsenic by GFAA

    Thallium by GFAA

    Inorganic Anions by IonChromatography

    Alkalinity by Titration

    Chloride by ColorimetricAnalysis II

    Nitrate-Nitrite Nitrogen byColorimetry

    Phosphorus by Colorimetry

    Sulfate by GravimetricDetermination

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 23 of 1434

    0801600

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    Captain Jack Mine (Colorado)

    Status

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1993, Methods for the Determination ofInorganic Substances in EnvironmentalSamples, USEPA, EPA 600/R-93-100

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    TitrationApparatus

    InductivelyCoupledPlasmaCombined withMassSpectrophotome

    InductivelyCoupledPlasmaSpectrophotometer

    Cold VaporAtomicAbsorptionSpectrophotometer

    IonChromatograph

    TitrationApparatus

    0801600

    APHA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    ILM05

    2340

    200.7(W)

    200.8(W)

    245.1

    300(A)

    310.1

    ILM05

    Hardness in Water byEDTA Titration

    Metals in Water by ICP-AES

    Metals in Waters byICP/MS

    Mercury in Water by CVAA

    Inorganic Anions by IonChromatography

    Alkalinity by Titration

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 24 of 1434

    0801695

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    Region 8 Superfund: Delta 400 West Plume

    Status

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    0801695 OLM04

    OLM04Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 25 of 1434

    0801698

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    Region 8 Superfund: 3700-3800 West 2100 South Solvent Plume

    Status

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    0801698

    0801698

    ILM05

    OLM04

    ILM05

    OLM04

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 26 of 1434

    0801800

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    Region 8 Superfund: Colorado and Evans PCE

    Status

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    0801800 OLC03

    OLC03Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 27 of 1434

    0801801

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    Region 8 Superfund: Fillmore and Cascade PCE Plume

    Status

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    0801801 OLC03

    OLC03Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 28 of 1434

    0801812

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    Region 8 Superfund: Murray Laundry 4200 S State Plume

    Status

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    0801812

    0801812

    ILM05

    OLM04

    ILM05

    OLM04

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 29 of 1434

    0801845

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    Region 8 Superfund: 5400 South 3600 West Plume

    Status

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    0801845

    0801845

    ILM05

    OLM04

    ILM05

    OLM04

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 30 of 1434

    0801966

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    Region 8 Superfund: Upper Uncompahgre River

    Status

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    0801966

    0801966

    ILM05

    ILM05.3

    ILM05

    ILM05.3

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 31 of 1434

    081575

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    Slide Mine Boulder County Colorado

    Status

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    TitrationApparatus

    LaboratoryBalance

    InductivelyCoupledPlasmaCombined withMassSpectrophotome

    InductivelyCoupledPlasmaCombined withMassSpectrophotome

    InductivelyCoupledPlasmaSpectrophotometer

    Cold VaporAtomicAbsorptionSpectrophotometer

    081575

    APHA

    APHA

    USEPA

    USEPA

    USEPA

    USEPA

    UNKNOWN

    2340

    2540-G

    200.7(S)

    200.7(W)

    200.8(W)

    7471A

    Unknown

    Hardness in Water byEDTA Titration

    Total, Fixed and VolatileSolids

    Metals in Soil by ICP-AES

    Metals in Water by ICP-AES

    Metals in Waters byICP/MS

    Mercury in Solid orSemisolid Waste

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 32 of 1434

    081577

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    Vasquez Blvd and I-70

    Status

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    TitrationApparatus

    InductivelyCoupledPlasmaCombined withMassSpectrophotome

    InductivelyCoupledPlasmaSpectrophotometer

    Cold VaporAtomicAbsorptionSpectrophotometer

    APHA

    USEPA

    USEPA

    USEPA

    2340

    200.7(W)

    200.8(W)

    7471A

    Hardness in Water byEDTA Titration

    Metals in Water by ICP-AES

    Metals in Waters byICP/MS

    Mercury in Solid orSemisolid Waste

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 33 of 1434

    081700

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    Gilt Edge Mine

    Status

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1993, Methods for the Determination ofInorganic Substances in EnvironmentalSamples, USEPA, EPA 600/R-93-100

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1993, Methods for the Determination ofInorganic Substances in EnvironmentalSamples, USEPA, EPA 600/R-93-100

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-

    TitrationApparatus

    LaboratoryBalance

    LaboratoryBalance

    LaboratoryBalance

    InductivelyCoupledPlasmaCombined withMassSpectrophotome

    IonChromatograph

    TitrationApparatus

    Colorimeter

    Spectrophotometer

    081700

    081700

    APHA

    APHA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    ILM05

    UNKNOWN

    2320

    2540-C

    160.1

    160.2

    200.7(W)

    300(B)

    310.1

    353.2

    353.3

    ILM05

    Unknown

    Alkalinity in Water byTitration

    Total Dissolved Solids inWater

    Filterable Residue - TDS

    Non-Filterable Residue -TSS

    Metals in Water by ICP-AES

    Inorganic Anions by IonChromatography

    Alkalinity by Titration

    Nitrate-Nitrite Nitrogen byColorimetry

    Nitrate-Nitrite Nitrogen byCd Reduction

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 34 of 1434

    081700

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    Gilt Edge Mine

    Status

    020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    USEPA, 1998, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, 3rdEdition, Final Update III., USEPA, SW-846_III

    USEPA, 1998, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, 3rdEdition, Final Update III., USEPA, SW-846_III

    USEPA, 1998, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, 3rdEdition, Final Update III., USEPA, SW-846_III

    USEPA, 19--, CLP SOW for InorganicsAnalysis-LC_INORGANICS, USEPA,LC_INORGANICS

    Total OrganicCarbon - Infra-Red Detector

    Cold VaporAtomicAbsorptionSpectrophotometer

    GC with FlameIonizationDetector

    Capillary GasChromatographwith MassSpectrophotometer

    Capillary GasChromatographwith MassSpectrophotometer

    InductivelyCoupledPlasmaCombined withMassSpectrophotome

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    415.1

    7470A

    8015B

    8260B

    8270C(W)

    ICP-AES

    Total Organic Carbon byCombustion

    Mercury in Liquid Wastesby CVAA

    Non-Halogenated OrganicsUsing GC/FID

    Volatile Organics byCGC/MS

    Semivolatile OrganicCompounds by CGC/MS

    Inductively CoupledPlasma

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 35 of 1434

    0834QB00

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    Cheyenne River

    Status

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    0834QB00 UNKNOWN

    UnknownActive

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 36 of 1434

    11113300

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    New Hampshire Dept. of Environmental Services

    Status

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    US EPA Research and Development,Cincinnati, Ohio, 1991, Test Methods forEscherichia Coli in Drinking Water, US EPA -Federal Register, Test Method 1104

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    American Public Health Association, 1995,Standard Methods for the Examination of Waterand Wastewater, APHA, 19th edition

    Dufour, Alfred P., Edley R. Strickland, andVictor Cabelli, 1981, Membrane Filter methodfor enumerating Escherechia coli, Applied andEnvironmental Microbiology, 41(5):1152-1158

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    Hach Chemical Company, 1992, Hach WaterAnalysis Handbook., HACH ChemicalCompany, 2nd Edition

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    Bovee, K.D., and R. Milhous, 1978, HydraulicSimulation in instream flow studies: Theory andTechniques, US Fish and Wildlife Service,Instream Flow Pap #5

    Olem, H. and G. Flock, 1990, Lake andReservoir Restoration Guidance Manual, EPA,2nd edition

    Chapman, Andrew and Chris Nash, 1992,Quality Assurance Project Plan for Shellfish

    11113300

    11113300

    11113300

    11113300

    11113300

    11113300

    11113300

    11113300

    11113300

    11113300

    11113300

    10-510-00-1-A

    1104

    353(VAR)

    APHA 3.0

    DUFOURMTEC

    HACH10029

    HACH 8025

    LIMNO QAMANUAL

    RIVERFLOW

    SECCHI

    SHELLFISHFLOW

    Potassium LACHATMETHOD

    Test Methods for E. Coli indrinking Water

    NITRATE/NITRITEVARIATION OF EPA 353

    Total Fecal Coliform

    Membrane filter method forenumerating Escherechiacoli

    m-ColiBlue24

    Apparent Color bySpectrophotometer at455nm

    Chlorophyll a (PROBE)

    VRAP and RASP methodfor determining river flow

    Determining watertransparency by SecchiDisk

    Shellfish Flow Methodology

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Description

    Description

    This Broth allows for the simultaneous detection of total coliform bacteria and E. coli within 24 hrs. An enzymatic indicator in the medium causes non-fecal total coliform colonies grown on the m-coliBlue24 medium to be red, while the E. coli (fecal coliform) colonies are blue.EPA Approved Method 10029

    SCUFA

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 37 of 1434

    11113300

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    New Hampshire Dept. of Environmental Services

    Status

    Sanitary Surveys, New Hampshire Departmentof Environmental Services Shellfish Program,55-56

    American Public Health Association, 1995,Standard Methods for the Examination of Waterand Wastewater, APHA, 19th edition

    American Public Health Association, 1998,Standard Methods for the Examination of Waterand Wastewater, 20th Edition., American PublicHealth Association, 20th Edition

    American Public Health Association, 1998,Standard Methods for the Examination of Waterand Wastewater, 20th Edition., American PublicHealth Association, 20th Edition

    American Public Health Association, 1998,Standard Methods for the Examination of Waterand Wastewater, 20th Edition., American PublicHealth Association, 20th Edition

    American Public Health Association, 1998,Standard Methods for the Examination of Waterand Wastewater, 20th Edition., American PublicHealth Association, 20th Edition

    American Public Health Association, 1998,Standard Methods for the Examination of Waterand Wastewater, 20th Edition., American PublicHealth Association, 20th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Water

    11113300

    11113300

    11113300

    11113300

    11113300

    11113300

    11113300

    SM 199213.D.3

    SM 2320 B

    SM 4110 A

    SM 4500-NH3-H

    SM 4500-P-F

    SM 5310 A

    SM9213.D.3

    E. Coli Counts

    Low Alkalinity Titration topH 4.5

    Metals

    NITROGEN, AMMONIUM(NH4) AS NH4

    PHOSPHORUS,ORTHOPHOSPHATE ASP

    Organic Carbon

    E. Coli Counts

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Description 1- The ecoregional character of NH lakes makes using a more dilute acid result in the higher sensitivity required to obtain adequate results. Thus, a titrantof .002N H2SO4 is used instead of the .02N acid of standard method.

    2- While lab analysis typically uses a pH meter, for the field we use a pH indicator solution for efficiency unless the water has high organic color. A mixedbromocresol green-methyl red indicator allows for a sharper equivalence point at the lower pH that the test requires. It is greenish-blue at pH 5.2, lightblue at pH 5.0, light gray at pH 4.8, and light pink at pH 4.5.Upon special request the protocol can be followed using the Hanna Model HI-9025 pH meter instead of indicator solution. Follow the protocols outlinedbelow but skip step C.2. and substitute pH 4.8 for gray endpoint and pH 4.5 for pink endpoint.

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 38 of 1434

    11113300

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    New Hampshire Dept. of Environmental Services

    Status

    and Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    Spectrophotometer

    Human Eye

    Spectrophotometer

    Nephelometer

    TitrationApparatus

    ConductivityBridge

    ConductivityBridge

    11113300

    11113300

    APHA

    APHA

    APHA

    APHA

    APHA

    APHA

    APHA

    SM9230.C.2

    UNKNOWN

    10200-H

    2120-B

    2120-C

    2130

    2320

    2510

    2520-B

    Enterococci

    Exact field or lab method isunknown

    Chlorophyll a-b-cDetermination

    Color in Water by VisualComparison

    Color in Water bySpectrophotometry

    Turbidity in Water

    Alkalinity in Water byTitration

    Conductivity in Water

    Salinity in Water- ElectricalConductivity Method

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 39 of 1434

    11113300

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    New Hampshire Dept. of Environmental Services

    Status

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1998,Standard Methods for the Examination of Waterand Wastewater, 20th Edition., American PublicHealth Association, 20th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    LaboratoryBalance

    LaboratoryBalance

    Thermometer

    GraphiteFurnace AtomicAbsorptionSpectrophotometer

    IonChromatograph

    pH meter

    Ion SelectiveElectrode

    Ion SelectiveElectrode

    APHA

    APHA

    APHA

    APHA

    APHA

    APHA

    APHA

    APHA

    APHA

    2540-B

    2540-D

    2550

    3113-B

    4110-B

    4500-H

    4500-NH3(H)

    4500-NO3(D)

    4500-O-G

    Total Solids Dried 103-105C in Water

    Total Suspended Solids inWater

    Temperature of Water byThermometer

    Metals in Water by GFAA

    Anions in Water by IonChromatography

    pH in Water

    Ammonia in Water - FlowInjection Analysis

    Nitrate in Water Using anISE

    Total Dissolved Oxygen byMembrane ElectrodeMethod

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 40 of 1434

    11113300

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    New Hampshire Dept. of Environmental Services

    Status

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1998,Standard Methods for the Examination of Waterand Wastewater, 20th Edition., American PublicHealth Association, 20th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American Public

    Colorimeter

    AutoAnalyzer

    Genericinspection-relatedequipment(egcolor charts)

    Genericinspection-relatedequipment(egcolor charts)

    Total OrganicCarbon - Infra-Red Detector

    Spectrophotometer

    Colorimeter

    Colorimeter

    APHA

    APHA

    APHA

    APHA

    APHA

    APHA

    APHA

    APHA

    APHA

    4500-P-E

    4500-P-F

    5210-B

    5210-C

    5310-B

    5910-B

    9213-D

    9221-B

    9221-E

    Phosphorus in Water byColorimetry- Ascorbic AcidMethod

    Phosphorus in Water byColorimetry- AutomatedAscorbic Acid Metho

    5-Day Biochemical OxygenDemand

    Ultimate BiochemicalOxygen Test

    Total Organic Carbon byCombustion-InfraredMethod

    UV - Absorbing OrganicCompounds

    E. coli method

    Standard Total ColiformFermentation Technique,Multi-tube FermentationTechnique

    Estimation of FecalColiform Group Density,Multi-tube Fermentation

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 41 of 1434

    11113300

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    New Hampshire Dept. of Environmental Services

    Status

    Health Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1998,Standard Methods for the Examination of Waterand Wastewater, 20th Edition., American PublicHealth Association, 20th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    American Public Health Association, 1992,Standard Methods for the Examination of Waterand Wastewater, 18th Edition., American PublicHealth Association, 18th Edition

    USEPA, 19--, Guidelines Establishing TestProcedures for the Analysis of Pollutants.,USEPA, 40 CFR Part 136

    USEPA, 19--, Guidelines Establishing TestProcedures for the Analysis of Pollutants.,USEPA, 40 CFR Part 136

    American Public Health Association, 1998,Standard Methods for the Examination of Waterand Wastewater, 20th Edition., American PublicHealth Association, 20th Edition

    USEPA, 1985, Test Method for E. Coli andEnterococci in Water by the Membr. FilterProcedure, Methods 1103.1 and 1106.1,USEPA, EPA 600/4-85-076

    USEPA, 1991, Test Methods for Escherichia

    OpticalMicroscope

    OpticalMicroscope

    Colorimeter

    FiltrationApparatus

    APHA

    APHA

    APHA

    APHA

    APHA

    HACH

    HACH

    IDEXX

    USEPA

    USEPA

    9222-B

    9222-D

    9223-B

    9230-B

    9230-C

    10029

    8025

    ENTEROLERT

    1103_1

    1104

    Technique

    Standard Total ColiformMembrane Filter Procedure

    Fecal Coliform MembraneFilter Procedure

    Enzyme Substrate Test, E.coli, Coliform Group

    Fecal Streptococcus andEnterococcus, Multi-tubeFermentation Technique

    Fecal Streptococcus andEnterococcus, MembraneFilter Technique

    m-ColiBlue24 Method ofthe Determination of TotalColiforms and E. coli

    Color, APHA Platinum-Cobalt

    Enterolert Quanti-Tray;Multi Tube, Multi Well, forEnterococcii

    E. coli in Water byMembrane Filtration

    E. coli in Drinking

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 42 of 1434

    11113300

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    New Hampshire Dept. of Environmental Services

    Status

    coli in Drinking Water., USEPA, EPA 600/4-91-016

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 2002, Method 1600: Enterococci inWater by Membrane Filtration Using membrane-Enterococcus Indoxyl-B-D-Glucoside Agar (mEl)(September 2002), USEPA, EPA 821-R-02-022

    USEPA, 1993, Methods for the Determination ofInorganic Substances in EnvironmentalSamples, USEPA, EPA 600/R-93-100

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1994, Methods for the Determination of

    ConductivityBridge

    TitrationApparatus

    pH meter

    LaboratoryBalance

    LaboratoryBalance

    Nephelometer

    No equipment

    InductivelyCoupledPlasmaCombined withMassSpectrophotome

    Inductively

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    120.1

    130.2

    150.1

    160.2

    160.3

    1600

    180.1

    200

    200.7(W)

    200.8(W)

    Water/EC Medium withMug Tub

    Conductance

    Total Hardness

    pH

    Non-Filterable Residue -TSS

    Total Residue

    Enterococci in Water byMembrane Filtration Usingmembrane-EnterococcusIndoxyl-B-D-GlucosideAgar (mEl)

    Turbidity by Nephelometry

    Metals by AtomicAbsorption

    Metals in Water by ICP-AES

    Metals in Waters by

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 43 of 1434

    11113300

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    New Hampshire Dept. of Environmental Services

    Status

    Metals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1994, Methods for the Determination ofMetals in Environmental Samples, SupplementI, USEPA, EPA 600-R-94-111

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    CoupledPlasmaSpectrophotometer

    TemperatureStabilizedGraphiteFurnace AASpectrophotometer

    GraphiteFurnace AtomicAbsorptionSpectrophotometer

    GraphiteFurnace AtomicAbsorptionSpectrophotometer

    GraphiteFurnace AtomicAbsorptionSpectrophotometer

    Flame AtomicAbsorptionSpectrophotometer

    Flame AtomicAbsorptionSpectrophotometer

    Flame AtomicAbsorptionSpectrophotometer

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    200.9

    202.2

    206.2

    213.2

    215.1

    218.1

    220.1

    ICP/MS

    Metals by TemperatureStabilized GFAA

    Aluminum by GFAA

    Arsenic by GFAA

    Cadmium by GFAA

    Calcium by FLAA

    Chromium by FLAA

    Copper by FLAA

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 44 of 1434

    11113300

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    New Hampshire Dept. of Environmental Services

    Status

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1993, Methods for the Determination ofInorganic Substances in EnvironmentalSamples, USEPA, EPA 600/R-93-100

    USEPA, 1993, Methods for the Determination ofInorganic Substances in EnvironmentalSamples, USEPA, EPA 600/R-93-100

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysis

    Flame AtomicAbsorptionSpectrophotometer

    GraphiteFurnace AtomicAbsorptionSpectrophotometer

    Flame AtomicAbsorptionSpectrophotometer

    Flame AtomicAbsorptionSpectrophotometer

    GraphiteFurnace AtomicAbsorptionSpectrophotometer

    Flame AtomicAbsorptionSpectrophotometer

    IonChromatograph

    IonChromatograph

    TitrationApparatus

    AutoAnalyzer

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    236.1

    239.2

    243.1

    249.1

    270.2

    289.1

    300(A)

    300(B)

    310.1

    325.2

    Iron by FLAA

    Lead by GFAA

    Manganese by FLAA

    Nickel by FLAA

    Selenium by GFAA

    Zinc by FLAA

    Inorganic Anions by IonChromatography

    Inorganic Anions by IonChromatography

    Alkalinity by Titration

    Chloride by Colorimetric

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 45 of 1434

    11113300

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    New Hampshire Dept. of Environmental Services

    Status

    of Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1993, Methods for the Determination ofInorganic Substances in EnvironmentalSamples, USEPA, EPA 600/R-93-100

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1993, Methods for the Determination ofInorganic Substances in EnvironmentalSamples, USEPA, EPA 600/R-93-100

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1993, Methods for the Determination ofInorganic Substances in EnvironmentalSamples, USEPA, EPA 600/R-93-100

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    USEPA, 1983, Methods for Chemical Analysisof Water and Wastes, USEPA, EPA 600/4-79-020

    Colorimeter

    TitrationApparatus

    Ion SelectiveElectrode

    Colorimeter

    TitrationApparatus

    Nessler Tube

    Potentiometer

    Colorimeter

    Spectrophotometer

    Spectrophotometer

    Genericinspection-related

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    USEPA

    350.1

    350.2(C)

    350.3

    351.2

    351.3(A)

    351.3(B)

    351.3(C)

    353.2

    365.2

    365.3

    405.1

    Analysis II

    Ammonia Nitrogen byColorimetry

    Ammonia Nitrogen byTitration

    Ammonia Nitrogen Usingan ISE

    Total Kjeldahl Nitrogen byColorimetry

    Total Kjeldahl Nitrogen byTitration

    Total Kjeldahl Nitrogen -Nesslerization

    Total Kjeldahl Nitrogen -Potentiometric

    Nitrate-Nitrite Nitrogen byColorimetry

    Phosphorus by SingleReagent Colorimetry

    Phosphorus by TwoReagent Colorimetry

    5 Day Biochemical OxygenDemand

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

    Active

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 46 of 1434

    11113300

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    New Hampshire Dept. of Environmental Services

    Status

    USEPA, 1993, Methods for the Determination ofInorganic Substances in EnvironmentalSamples, USEPA, EPA 600/R-93-100

    USEPA, 1992, Methods for the Determination ofOrganic Compounds in Drinking Water,Supplement II, USEPA, EPA 600/R-92-129

    USEPA, 1994, Test Methods for EvaluatingSolid Waste, Physical/Chemical Methods, SW-846, 3rd Edition, Final Update II., USEPA, SW-846_II

    US EPA, 2003, Guidelines Establishing TestProcedures for the Analysis of Pollutants;Analytical Methods for Biological Pollutants inAmbient Water; Final Rule, US EPA FederalRegistry, 40 CFR Part 136

    equipment(egcolor charts)

    Colorimeter

    Capillary GasChromatographwith MassSpectrophotometer

    IonChromatograph

    USEPA

    USEPA

    USEPA

    11113300

    410.4

    524.2

    9056

    ENTEROLERT

    Chemical Oxygen Demandby Colorimetry

    Purgeable Organics inWater by CGC/MS

    Anion ChromatographyMethod

    ENTEROLERT FORAMBIENT WATERTESTING

    Active

    Active

    Active

    Susp

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 47 of 1434

    1111REG1

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    USEPA, Region I

    Status

    Jack Paar, III, 1998, Fecal Coliform Analysis,U.S. EPA Office of Environmental Measurementand Evaluation, OEME SOP A102

    1111REG1 BIOLOGY001

    Fecal Coliform AnalysisActive

  • December 13, 2007 14:55:01Field/Lab Analytical Procedures and Equipment Detail

    Page 48 of 1434

    1117MBR

    ProcedureSource

    ProcedureID

    ProcedureName Citation Equipment

    ComparableNationalProcedure ID

    US EPA Region 7

    Status

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    Unknown, 19--, No Cite - Method Not Cited,Unknown, Vol --

    USEPA, REGION 7, ENVIRONMENTALSERVICES DIVISION, 2000, OPERATIONSAND QUALITY ASSURANCE MANUAL, EPA,R7, .

    R7 AMM - US EPA Region 7 Laboratory,Updated Annually, US EPA Region 7Laboratory Analytical Methods Manual, US EPARegion 7 Laboratory, .

    R7 AMM - US EPA Region 7 Laboratory,Updated Annually, US EPA Region 7Laboratory Analytical Methods Manual, US EPARegion 7 Laboratory, .

    R7 AMM - US EPA Region 7 Laboratory,Updated Annually, US EPA Region 7Laboratory Analytical Methods Manual, US EPARegion 7 Laboratory, .

    R7 AMM - US EPA Region 7 Laboratory,Updated Annually, US EPA Region 7Laboratory Analytical Methods Manual, US EPARegion 7 Laboratory, .

    Capillary GCwith HighResolutionMassSpectrophotometer

    1117MBR

    1117MBR

    1117MBR

    1117MBR

    1117MBR

    1117MBR

    1117MBR

    1117MBR

    1117MBR

    FM-PH

    M1613 REVB

    RAFT FISHPARAM

    REMAPFIELD PAR

    RLABM3230.2

    RLABM3121.14D