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US Environmental Protection A&enc.y Surveillance and Analyaia Division Raaton I 60 w..tview Strut Lexinaton, KA 02173

Attn : Mr. Steven R. Novick

Dear Hr. Novick :

). ' I. .:14

ll:ZI Kenmor. Avenue lluffalo.N-Vorll14207

!711117J-1300

Oc t ober 15, 1982

Re: Contract No, 68-<11-6598

Ple..a find enclosed the Final Documen tation Packaae aa required by Article Xtt-C of the above-referenced contract,

Abo encloaad aa

0 nporta, aanih1t1,

It v.. a pt...ure fraa to contact ••·

LVL/clm

Encloaurea

u

a part of thh packaae an analytical data , daily ..rvica the air 110nitortna loa, and aafety inforaation.

workin1 with you and if you have any qu..tione, pleau fed

Sincerely ,

CECOS INTERNATIONAL, INC,

~~p Special Environmental Services Division

) 1/ 470

I. Introductionr The following h the final documentat ion package for Contract Number 68-0 1-6598, as required by Articla XII-C of the contract.

II. Chronol oaical Su111111ation

Mobilization period wu from 6 July 1982 through 16 July 1982. Activitiu during thil tiae included aettins up of traileu, electric, plumbing, and telephone hookupa, and construction of parking .reas.

From 16 July 1982 through 5 August 1982, Emergency Technical Servicu Corporation and CECOS prepared a bunkered area fo r the unpac:ltin& of lab-packa and unpacked all drums in Building 2 auapected of being packaged laboratory chemicals (see Summary of Materials Dilpoaed for quantities), An averaae of ten druma per day were unpacked. The Caterpillar 215 Loader with drum arappler wu used throughout this period to move all dru•a out of Building 2 and i nto the bunkered area. All peraonnel in the bunkered area ware duaaed in a 110dif1ed Level A un1for11. Throughout the entire operation, the USEPA developed safety plan was adhered to.

For the period 6 Auguat 1982 through 9 August 1982. the dte vaa ahut down except for aecurity .

c Fro. 10 Auauat 1982 throua;h 24 September 1982 , work continued on other aateriala fr081 the aite. Our ina; thh period of t:lae • all efforta wen aade to bulk aateriab whenever posaible. Drums , tanka. and dut~paters were addruaed with the end nault that only one dumps ter re..ina on aite for uae aa a mixina box . Tanka , when poaaible . were pu~ed out to have only a heel .

At the cloae of buainus on 24 September 1982 , acUvitiea under this contract were concluded due to expenditure of contract funds.

Ill. Materials Diapoaed

A. Lnboratory Packa - Phase II

1. 21 detonation• with approximately five pounda per detonation for a total of 105 pounds.

360 pounds of material were tranaported and burned at the Emergency Technical S~rvicu facility in New Jersey. These materials conaiaud of:

Oxidizers 1.5 pounds Flamt11able Liquids 1.5 pounds Fla~~~~~&ble Solida 118.0 pounds Orsanic Peroxides 3.0 pounds Corroaive Liquids 145.0 pounds Corrosive Solids 18.0 pounds Watcr•Reactiv~ Solids 67 . 0 pounda

_) 3. 140 cylinders of va rious gases were also sen t to ETSC for

disposal. The cylinders were four cubic fee t lecture bottles.

4. 100 drums chnified aa laboratory packt were tent to CECOS ' Secure Chemical Management Facility in Niagara Falla, New York for diaposal. .. Bulk Container Removal - Phaae Ill

Product Coda Description ~

6920-B Mixed Organic Solids 92 drums 154.96 cubic yuda

6920-D Contaminated Water 9 drums 2,800 gallons

6920-E Con taminat ed Organic Sludse 8.3 cubic yarda 6920-G Inorganic Solids Contami nated

with Lead Ca rhona te 56.2 cubic yard1 6920-H Cru shed Drumt 35 cubic yards 6920-M Sodium Hypochlorite 8 drums 69 20-R PCB Solids under 500 ppm 67.81 cubic yards

2 drums 6920-T Lean Waters 9,841 gallons (TrieU) 6920-AE Contaminated Chlorinated

Solventa 45,000 pound s (Rollins) 6920-ZK PCB Liquid over 500 ppm 47 druaa (ENSCO)

0 All of the above aatuiala wen placed in CECOS' Secure Cheaical HanJit!Unt Facility in Niaaara Falla, New York, with the exception of codu 6920-T, 6920-AE, and 6920-ZK, which were diapoaed of at Tricil , Rollina , and ENSCO respectively ,

In addition to the above materiala, seven each 4-cubic feet lecture cylinders were disposed of on site, There were five chlorine cylinders which turned out to be empty and two phosgene cylinders which were full. The cylinders were elow\y bubbled through a sodium hydroxide scrub solution. Throuahout the bubbling procesa, the aolution was checked to ensure that the pH remained basic. Following complet i on of the cylinders, the drum was clond and left on aite for diapoaal, along with the othn cauatica.

An additional 19 cylinders, five pounda of DDT, and 27.33 pounds of reac tive materials were diapoaed of by Resource Conservation and Recovery Agency o( FanDin&ton, New Hampshire. The cylindera and reactive materiala were detonated at a State-approved site near Keene, New Hampshire. The DDT was brokered by RCRA to Signo Trading for reclamation.

) l/4 70

IV, Analytical Inforaation

All analytical data wu achieved uaina USEPA approved methode. Major equipunt ware a Hewhtt-Packard Hodel 5790-A Gas Chromatograph with Electron Catpure Detector and an Oceanographic International Hodel 525 Total Oraanic Carbon Analyzer with Infrared Detector. Analytical reaulu are enclo..d aa Enclosure A,

V. Index of Enclosuru ,.,"' ~

A. Analytical Data !i:"' 1. Laboratory Booka ~"'zz 2, GC Data ~<

"'~3. Outlide Lab Report& ~~ B. Daily Service Raporta l>Z C. Kanifeata -<:It

~"'D. Air Monhorina Loa <Z, ....E. Safety ,,..l> 1. a..pirator Fit Teat 2, Safety H..tina Report "' 01'1 ""'

o;s"'"' :;! "'