fm304

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FM 304: BATCH S ETTL I NG O F S O L I D S LURR I E S Objectiv es: 1. Vertical Cylinders: Obtain the batch settling data for the given calcium carbonate slurry (i.e. the settling rate versus concentration of slurry), and demarcate the different settling regimes. (‘free settling” and ‘hindered settling’) 2. Tilted Cylinders: Obtain the batch settling data in the free settling regime for different angles and check it’s agreement with PNK theory. Observe the flow patterns during the settling. Apparatu s: Vertical settling cylinder, inclined settling cylinder, glass rod, stop watch Reagent s: Water, Calcium Carbonate Theor y:

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Lab manual for FM 304 experiment CL333

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FM 304: BATCHS ETTL I NGOFS OL I DS LURR I ES Objectives:1!e"tic#$C%$i&'e"s:Obtainthebatchsettlingdataforthegivencalciumcarbonate slurry (i.e. the settling rateversusconcentration ofslurry),anddemarcatethe different settling regimes. (free settling and hindered settling)(Ti$te'C%$i&'e"s:Obtainthebatchsettlingdatainthefreesettlingregimefordifferentangles and check its agreement with P! theory.Observetheflow"atternsduring the settling.A))#"#t*s:#erticalsettlingcylinder,inclinedsettlingcylinder,glassrod,sto"watchRe#+e&ts:$ater, %alcium %arbonateT,e-"%:I&t"-'*cti-&:Sett$i&+isthe"rocessbywhich"articulatessettletothebottomofali&uidandformas e d i m e n t .Particlesthate'"erienceaforce,eitherduetogravityorduetoce n t rifu g a lm o ti o nwilltendtomoveinauniformmannerinthedirectione'ertedbythatforce.(orgravity settling,thismeansthatthe"articleswilltendtofalltothebottomofthevessel,forminga s l u rryat the vessel base.Fi+*"e1 F-"ces #cti&+ -& # )#"tic$e '*"i&+ sett$i&+(or settling "articles that are considered individually, i.e. dilute "article solutions, there are two main forcesenacting u"on any "article. )he"rimary force isana""liedforce, suchas gravity,andad ra g forcethatisduetothemotionofthe"articlethroughtheflu i d .)he a""liedforceisusuallynotaffectedbythe"article velocity."article*svelocity,whereasthedragforceisafunctionofthe(ora"articleatrestnodragforcewille'hibited,whichcausesthe"articletoaccelerate due to thea""lied force. $hen the"article accelerates, the drag force actsin thedirection o""ositetothe"article*s motion,retardingfurtheracceleration,intheabsenceofotherforces dragdirectly o""oses the a""lied force. +s the "article increases in velocity eventuallythedragforceandthea""liedforcewill a""ro'imately e&uate,causingno further change in the"article*svelocity.)hisvelocityisknownasthete".i$ve$-cit%,settlingvelocity orfallvelocity ofthe"article.)hisisreadily measurablebye'aminingtherateoffallofindividual"articles.)heterminalvelocity ofthe"articleisaffectedbymany"arameters,i.e.anythingthatwillalter the "article*s drag. ,ence the terminal velocity is most notably de"endent u"on grain si-e,the sha"e(roundnessands"hericity)anddensityofthegrains,aswellastotheviscosityand density of the fluid.)hebehaviourofsettling"articlesinslurrycanbeconvenientlystudiedinsmallbatche'"eriments.)hedataisthenusefulfordesigninglargescalesettlingtankswhichhavea number ofa""lications (e.g.clarification ofwaste water). )hemain information re&uired fordesign is the settling rate of the "articles as a function of the system "arameters such as "articlesi-e and sha"e, concentration, geometry of the system, etc.)heeffectofconcentrationonthesettlingslurrycontinuouslyincreaseswithtime.)heeffectofgeometryofthesystemonthesettlingratecanbesignificant.$henthecylinder istilted, .oycott(/012)foundthatthesettlingrateincreasesduetoshortersedimentation "ath.)his "henomenon is known as the B-%c-tt e//ect, and is used to enhance the rate of settling insome a""lications.(i)VerticalCylinders:3e"endingontheconcentrationoftheslurry,tworegimesofsettlingare"ossible,freesettling and hindered settling. +s the name im"lies, in free settling, each "articleisunaffected by the motion of the neighboring ones and its terminal velocity is givenby4+ll above e&uations are valid only for 5eynolds no. 5e 6 /. $here " and are the densities of the "article and the sus"ending medium res"ectively, 3" is the diameter of the "article, %3 is the drag coefficient+nd "article 5eynolds no. 7 7 7 7 7 7 (a)7 7 7 7 7 7 (b)7 7 7 7 7 7 (c)7 7 7 7 7 (d))he modelassumed for describing (ree 8ettling,has some limitations in "racticala""lication.8uchastheinteractionof"articlesinthefluid,ortheinteractionofthe"articleswiththecontainerwallscanmodifythesettlingbehavior.8ettlingthathasthese forces in a""reciable magnitude is known as hindered settling.9nthe,i&'e"e'sett$i&+regimedueto"article7"articleinteractionsandu"draftofli&uid,the velocity of individual "articlesisconsiderably smaller.)he settling velocity (US) may beestimated by an em"irical e&uation of the form.where,isthe volumefractionof the fluid and n is a constant.7 7 7 7 7 7 7 7 (e))he void fraction can be calculated as : ;/7 %