fracture toughness of filament wound bfr and gfr arc shaped specimens with charpy impact test method
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Accepted Manuscript
Fracture Toughness of Filament Wound BFR and GFR Arc Shaped Specimenswith Charpy Impact Test Method
Mehmet Turan Demirci, Necmettin Tarakç ıoğlu, Ahmet Avcı, mer FarukErkendirci
PII: S1359-8368(14)00171-1DOI: http://dx.doi.org/10.1016/j.compositesb.2014.04.015Reference: JCOMB 3000
To appear in: Composites: Part B
Received Date: 21 December 2013Revised Date: 17 April 2014Accepted Date: 22 April 2014
Please cite this article as: Demirci, M.T., Tarakç ıoğlu, N., Avcı, A., Erkendirci, .F., Fracture Toughness ofFilament Wound BFR and GFR Arc Shaped Specimens with Charpy Impact Test Method, Composites: Part B(2014), doi: http://dx.doi.org/10.1016/j.compositesb.2014.04.015
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Fracture Toughness of Filament Wound BFR and GFR Arc Shaped Specimens with Charpy Impact Test
Method
Mehmet Turan Demircia*, Necmettin Tarakçıoğlua, Ahmet Avcıb, Ömer Faruk Erkendircic
a *Selçuk University Metallurgy and Material Engineering Dep. Konya, Turkey
b Selçuk University Mechanical Engineering Dep. Konya, Turkey
c Zirve University, Marine Engineering Dep., Gaziantep, Turkey
*Corresponding author:
+90-332-223 2345 (phone)
+90-332-241 01 56 (fax)
[email protected] (email)
Abstract
The aim of this study is an examination of Charpy impact behaviors of ±6 layered basalt (BFR) and
glass fiber reinforced (GFR) epoxy composite pipe at the degree of ±55o filament winding angle with the arc-
shaped specimen technique of different notch depth ratios (a/W). As a result of Charpy impact experiments, BFR
composites were determined to have higher impact energy level and impact fracture toughness than GFR
composites. The occurred average delamination areas in between layers were detected by an image processing
method during the impact process. The delamination damage in GFR composites was observed to be more
dominant damage than in BFR composites. It is understood that damage modes change when the notch depth
ratio increases for composites. In BFR composites, the predominant damage mode was determined to be fiber
breakage as a consequence of experiments and SEM analyses.
Keywords: Basalt fiber, image processing, Charpy impact test, fracture toughness, arc shaped specimen,
filament winding.
Introduction
The Industrial revolution together with increased mechanization in Europe has brought forth many
problems. A new material, in other words composite material, was created to decrease costs, increase strength of
metallic materials and lighten these materials. Use of composite pipes and tanks which are produced by a
filament winding technique (one type of composite material producing method) is continuously increasing due to
advantages in aeronautics, transportation, logistics and space industry. The filament winding technique is
winding reinforced material fibers that have high strength and elasticity module by saturating it with a linking
resin then winding it on a cylinder in different angles and multiple layers until it reaches a certain thickness.
Main usage area of the materials that are produced by using this technique are pipes resistant to high pressure
and corrosion, compressed air, liquefied petroleum gas, vessel for compressed natural gas, space crafts, fuel
reservoir of war and airplane transportation, oxygen tube for submarines, muzzle of rocket launcher guns, body
of the submarine, structure of radar domes, and the body of a rocket [1-4].
Carbon fibers used as reinforced material in polymers have better mechanical characteristics that can be
utilized by specific sectors of the aerospace industry. However a redirection to use alternative fibers increased
due to the high cost of carbon fibers and difficult adhesion in between matrixes and carbon fibers [5-6]. For last
decades reinforced basalt fibers came to the forefront because they have better mechanical characteristics than
reinforced glass fibers as well as high impact resistance and lower cost than carbon fibers. Other superiorities of
basalt fibers than E-Glass and S-Glass fibers are recycling, natural long life, fire safety, chemical resistance,
thermal insulation, electrical insulation and working in high-low temperatures. These characteristics of basalt
fibers make them useful in thermal barrier insulation, underground cables, circuit boards and underground
evacuation channels [7-9]. In addition, the strength of the basalt fibers is five times higher and the density is
three times lower than low-carbon steels [4-5]. So use of basalt fibers in filament pipes and tanks had increased
nowadays and has become widespread in natural gas tanks, fire tubes, diver tubes, hydrogen tubes, medical
applications except military sectors all trade sectors. Companies of the countries which have great influence in
the natural gas sector have begun to use fiber-reinforced filament winding pipes (BTP) and tanks due to the
problems of weight and corrosion of metal tanks [10-11].
Many researchers have studied the impact behaviors of the different structures of composite materials.
Wang et al. manufactured hybrid long angle strut hangers by using basalt (BFR) and carbon (CFR) fiber
composites, studied their implementation on bridges and has compared them with other wire and fiber types [5].
They found that basalt or carbon hybrid composites have higher damage strain than the steel wire strain.
Colombo et al. confirmed in their study that BFR/epoxy composites have better adhesion force than CFR/epoxy
composites according to shear stress test in between layers and damage analyses [7]. Sfarra et al.applied low-
speed impact tests and they determined and compared the damage mechanisms that occurred. They found that
delamination mechanism areas exposed to impact in BFR composites are lower than CFR composites. They
established that damage mechanisms in BFR composites are principally in the form of fiber breakage [9].
Manikandan et al. applied shear, tensile and Izod impact tests to BFR/polyester and GFR/polyester composites,
and determined that BFR composites have good shear, tensile and impact resistance or impact absorption
characteristics. They linked reasons why BFR composites have high energy absorption to there being high shear
stress in between layers and that basalt fibers have better adhesion force than glass fibers [6]. Dehkordi et al.
specified that fiber breakage occurs in impact damage of basalt fibers when the low-speed impact test on
basalt/nylon hybrid composites is applied, but pull-out and delamination damage occurs in nylon fibers when the
same test is applied [12].
The charpy test is commonly used on metals, but is also applied to composites, ceramics and polymers.
With charpy test one most commonly evaluates the relative toughness of materials as such, it is used as a quick
and economical quality control device. Erkendirci examined plain weave S-2 glass fiber reinforced high density
polyethylene (HDPE) thermoplastic composites of different fiber volume ratios and thicknesses by using the
Charpy impact test with impact toughness and impact energy. He observed that increasing the fiber volume ratio
increases the impact toughness and impact energy. He has identified that fiber composites exhibited brittle
fracture behavior with the increase of the fiber volume fraction [13]. Ghasemnejad et al. established delamination
in the CFR and GFR reinforced composite samples by applying the Charpy impact test. They observed
interaction of delamination and absorbed impact energy [14]. Bansal et al. added weight ratio of 2.5% alumina
fly ash to GFR/epoxy composites and applied the Charpy impact test to samples in different notch depth ratios.
They obtained the high impact energy in the alumina added GFR/epoxy composites. They identified that alumina
particles increase interlaminar adhesion strength. They found that fiber breakage is the predominant damage
mode and delamination damage decreased with increased notch depth ratios [15]. Shokrieh et al. examined the
damage mechanism of GFR/epoxy composites by applying the Charpy impact test at a different temperature.
They determined that the damage mechanism at low-temperature occurs in the form of delamination and fiber
breakage, but matrix cracking occurs at high-temperature. They expressed that interlaminar shear stress increases
when the temperature increases [16]. Molnar et al. examined fracture toughness and impact resistance of
seventeen different samples formed PP/BaSO4 elastomer composites by using the Charpy impact test. They
mentioned the importance of the effect of temperature to impact resistance [17]. Khalli et al. identified impact
behaviors of three different notch depth ratios opened aluminum plates by patching with CFR/epoxy and
GFR/epoxy and detected that more impact energy was absorbed by the CFR / epoxy patch [18]. Lee and Chean
tested interlaminar shear stress, impact energy and fracture toughness of GFR/epoxy and GFR/polyester
composites with the Charpy impact test according to changing fiber volume fraction. They found that GFR /
epoxy composites absorbed the high impact energy around 60% in fiber volume fraction and absorbed impact
energy decreased after this value. They identified that delamination damage is predominant in the composites
which have interlaminar shear stress as low fiber volume fractions, but fiber breakage and pull out damage types
are predominant in the composites which have interlaminar shear stress as high fiber volume fractions [19].
Cheon et al. contacted relation between total area of delaminated area for laminated GFR/epoxy composites and
impact energy and reported that it is effective to increase interlaminar delamination and energy absorption
capacity [20]. Niglia et al. calculated fracture toughness of arc-shaped specimens cut from polyethylene pipes to
ASTM 399 standard by carrying out Charpy impact tests. In order to calculate the shaped factor because of the
arc-shape of specimens, derived formulas for each notch depth ratios (a/W) were used in their study [21]. Özbek
et al. studied fracture toughness (Gıc) and PE 100 arc-shaped specimens by using the Charpy impact test like to
similar to Niglia et al’s work and to find the shape factors of specimens with respect to changing notch depth
ratios, they derived the formulas [22].
The objectives of this study of basalt and E-glass fiber reinforced composite filament wound pipes are to
research the possibility of alternate basalt fibers, to contribute to the literature, and to increase the usability of the
Charpy impact tests on pipes for wide application. The Charpy impact test was applied on the arc-shaped
specimens taken from ±6-layered filament wound BFR and GFR reinforced pipes with a layup [±55o]6 and were
opened to different notch depth ratios (a/W). To minimize spring effect that stem from arc shape of specimen
according to the different depth ratios, the equations derived from the literature were used for the calculation of
the shape factors of the arc-shaped specimens. The fracture toughness (energy release rate) and impact energy of
basalt and E- glass reinforced filament wound specimens were compared. After the Charpy impact test, occurred
damage types were investigated and interlaminar delamination areas of BFR and GFR specimens were observed
and determined by the image processing method and compared with the impact energy.
Preparation of specimens
In this study, Kammany Vek 400 tex and 600 tex Vetrotex E-Glass fiber reinforcement were used in
filament wound pipes. The diameters of used fibers measured were measured by using ZEISS LS-10 Scanning
Electron Microscope. The measured average diameter is about 13 µm for E -glass fiber and 11,14µm for basalt
fiber given in Fig. 1. Modified Bisphenol A epoxy resin used as matrix material. Some important mechanical,
physical, and thermal properties of basalt are compared with E- glass fibers in Table 1, which clearly illustrate
the advantages of properties provided by the basalt. The filament wound pipes manufactured by IZOREEL
Composites Company via using CNC filament winding machines according to 10N fiber tension, average 11 mm
bandwidth and 60oC resin bath as filament winding parameters. The fibers passed through a resin bath in 60oC
and were manufactured to be ±6-layer, 72 mm internal diameter, average 2.62 mm thickness for BFR and
average 2,75 mm thickness for GFR ±55o winding angle in the same temperature over mandrel. After winding
processes, pre-curing and curing operations were applied at 135oC and at 150oC respectively.
Table 1 Comparison of mechanical properties of basalt and E-glass [7].
Fig. 1. Diameter values of basalt fiber.
To determine the fiber volume fraction, a burn-off test was applied to specimens according to ASTM-
D2584.The fiber fractions of [±55o]6 filament wound BFR and GFR specimens were found to be about 0,61.
Specimens cut from pipes, under a coolant that is manufactured in accordance with studies of Niglia et
al., Özbek et al. and ASTM 399-90 side cross-sectional areas, were grinded with 1200 grid abrasive papers to
minimize edge effects of the arc shaped specimens. The preparation scheme of specimens is given in Fig. 2.
Fig. 2. Specimens obtained from BFR and GFR filament wound pipes[21].
Four different notch depths for arc shaped specimens were determined and prepared by cutting them with a 1
mm thick diamond disk and bistoury according to four different a/W ratios (0.25, 0.38, 0.5, and 0.63). In totally,
24 specimens were prepared. To get fine results, tests for each type specimen were repeated three times and their
average results were evaluated.
Experimental procedure
BFR and GFR specimens were prepared as four different notch depth ratios tested by using the
Zwick/Roel Charpy impact test device at room temperature with respect to ISO 179/92 standard (Fig 3a). Impact
energy and energy release rates (Gc) were ascertained. Fig. 3c shows the fundamental principle of the Charpy
impact test and Fig. 4 shows the experimental setup of specimen.
a) b)
Fig. 3. a) Charpy test device b) Fundamental Principle of the Charpy impact test.
Fig. 4 Experimental set up of specimen
Energy release rate (impact toughness), which is one of fracture toughness methods, were benefited from the
studies of Niglia et al. and Özbek et al. These formulas given below, Eq.1 & Eq. 2, were used to calculate
fracture toughness [21-22].
U Ua Ub= − (1)
UG =c
BWφ(a/W) (2)
In here, c
G is the energy release rate (fracture toughness), U is absorbed impact energy, B is material width, W
is the height of the material specimen, and ( / )a Wφ is a shape factor of the specimen to minimize the spring
effect of arc shape according to the changing depth ratio. Derived equations (Eq. 3,4,5,6) from Niglia et al [21].
and Özbek et al. by finite element method for calculating shape factors are shown below. In here x , 0C and r
represents /a W , fixed number, and 1 2/r r respectively [22].
'C + C0φ = 'dC /dx
(3)
'dC 2 2
= -52.488 + 10, 080r + 1.031r + (5 .645 - 21.312r)x + 18.023rx +dx
2(64.224 - 26.064r + 0.202r ) (19.44 - 5 .059r) 31.683
(59.328 - 47.52r)x + - +2 3(1 - x) (1 - x) (1 - x)
(4)
(2.655-4.425r) 2C (r) = 10.879 + 3.136e - 2.165r - 2.51r0 (5)
' 2 2 3C = (-52.488 +10.08r +1.031r )x + (2.822 -10.656r)x + 6.008rx +
4 2(-14.832 +11.88)x + (-64.224 + 26.064r - 0.202r )ln(1- x)
(19.44 - 5.059r) (15.84)- + 2(1- x) (1- x)
(6)
The white colorant which has low viscosity was injected with needle tip among layers of specimens in
order to determine interaction between interlaminar delamination and impact energy at the end of impact tests.
Then layers were separated and photographed to depict the colored delamination surface under the light source
with a high density CCD camera. The approximate percentage of dissemination areas of these photos were
examined by imaging with a MATLAB image processing toolbox. Schematic picture of the image processing
system and steps of the image processing are shown Fig. 5 and Fig. 6 c) : raw picture (1), making gray operation
(2), and noise suppression filtering (3). Diaz et al. determined damages by the same method of recording with a
high density camera to see fatigue damage that plastic deformation caused on the crack tip [23].
Fig. 5. Schematic picture of the Image Processing System.
a) b)
c)
Fig. 6. Injected white color layer a) Separated layer b) Identification of % delamination areas by Image processing method for BFR specimen c).
Experimental results and discussion
BFR and GFR composite specimens were tested three times for determining impact energy and fracture
toughness in four different a/W ratios (0.25, 0.38, 0.5, and 0.63). Impact energies and fracture toughness, which
are obtained according to notch depth of BFR and GFR composite specimens, were analyzed and compared. The
standard deviations of impact energies of composites are given on Fig. 7 as vertical bars. Comparing impact
energies of BFR and GFR specimens according to notch depth ratio revealed a decrease in impact energy of each
composite specimen with increasing notch depth ratio (Fig. 7). While BFR composite specimens have an average
value of 10.8 J by 0.25 a/W ratio, GFR composite specimens have an average value of 8.8 J. BFR composite
specimens have an average value of 5.2 J by 0.63 a/W ratio, but GFR composite specimens have an average
value of 4.4 J. All of average impact energies of BFR and GFR composites are presented on Fig.7.
Fig. 7. Impact energies of the BFR and GFR composite specimens.
Being at a high level of absorbed impact energy for both of the composites in low notch depth ratios
(a/W), it is thought that the predominant type of damage that occurred in the Charpy impact test originates from
delamination damage for GFR and BFR composites as give in Fig. 8. It can be interpreted that the reasons of
decrease in absorbed impact energy are fast crack propagation and passing from predominant delamination
damage through predominant fiber breakage. In short, impact energy was absorbed with predominant fiber
breakage damage for specimens which had high notch depth ratios, while impact energy was absorbed with
predominant delamination damage for specimens which had low notch depth ratios (Fig. 8, 9). In Fig. 7, it is
noticable in the two composites compared to each other, impact energies of BFR composite specimens are higher
than GFR composite specimens in all notch depth. Bansal et al. expressed in their study that predominant
damage by decreasing notch depth ratio is delamination damage and they found similar evidences in this study
[15]. When compared the diameters of basalt and E-glass fibers each other, the tested E-glass fiber has larger
average diameter (13µm) then basalt fiber (11.14). However, basalt fiber has higher tensile strength, elastic
module (Table 1.) and impact energy then E-glass fiber [7]. According to literature data, the mechanical
properties of basalt and E-glass fiber are strongly dependent on their Al2O3 content. This identification gives us
that the strengths of these fibers increase by adding Al2O3 [24-25]. Therefore, for understanding higher
mechanical behaviors of basalt fiber than E-glass, the chemical compositions of fibers play an important role.
The main composition of glass fiber contains Al2O3, SiO2, CaO and B2O3 while basalt fiber contains higher
Al2O3 and SiO2, CaO, TiO2, K2O, MgO, Na2O and Fe2O3 except boron oxide [26]. Deak and Czigany studied the
effect of diameters and chemical composition of basalt and E-glass fibers. They found that basalt and E-glass
fiber did not depended on the mechanical properties on diameter after diameters of fibers exceed 9µm. In
addition, they reported that SiO2 and Al2O3 higher contents and ceramic materials of basalt fiber exhibited
correlation with the mechanical properties [26]. In this paper, the effect of the diameter of fibers was not
considered for impact properties and delamination.
a) b)
c) d)
Fig. 8. Damage types of GFR a) 0.25 a/W b) 0,38 a/W) and BFR c) 0.25 a/W d) 0,38 a/W
a) b)
c) d)
Fig. 9. Damage types of GFR a) 0.5 a/W b) 0,63 a/W) and BFR c) 0.5 a/W d) 0,63 a/W
Image processing method is used to compare the delamination damages which occur in BFR and
GFR/epoxy composites and to opine both of the composite damages. Also average the delamination damage
areas which occurred in the layers were identified for a/W depth ratios. The average delamination areas of each
a/W depth ratios and their standard deviations are given in Fig. 10.
Fig. 10. Delamination areas of BFR and GFR composites.
GFR composites have higher values than BFR composites for the delamination damage areas in each of a/W
ratios measured from the impact tests, as given in Fig. 10. Here, for BFR composites it can be mentioned that
basalt fibers have strong adhesion force with matrix and so they provide better interface than glass fibers [6, 9].
In this case, fiber breakage is the predominant damage mode for BFR composites (Fig. 8, 9). While increasing
the notch depth ratio, impact energy decreased and so the delamination damaged areas of both composites were
decreased. The differences between the the delamination areas, in particular 0.5 and 0.63 a/W nothes decreased.
From here, it can be commented that while the a/W ratio increased, fiber breakage and pull out damages highly
occurred as seen Fig. 9 and SEM micrographs. In Fig. 10 the differences of delamination areas between BFR
and GFR composites can be explained by two cases. First are the differences of impact energies of BFR and
GFR composites (see Fig.7) due to their different module which may cause debonding and delamination between
fibers and polymer matrix at the interface and other is the surface roughness of fibers (see Fig.1) Mility et al.
reported that the smooth surface roughness of E-glass fibers greatly affected the bonding between fibers and
matrix. Wu et al. mentioned that the surface characteristics of fibers contributed to the delamination damage of
composites and the smooth surface of glass fibers resulted in delamination damage, whereas the rough surface of
basalt fibers assured a fine bonding anf providing the enhancement of mechanical properties [27]. Sfarra et al.
reported that the delamination and whitening (debonding) damages of GFR were observed higher than BFR
composites. It was mentioned that the interface ability of fiber and epoxy is significant and basalt fibers have
good interface with epoxy [9]. Manikandan et al.found that the impact energy of BFR polyester composites take
higher values than GFR polyester composites owing to fact that basalt fibers have higher adhesion force with
polyester than glass fibers [6]. At the same time they stated that low shear strength triggers the interlaminar
delamination in their study. Colombo et al. found evidence in parallel with the findings that basalt fibers create a
strong adhesion force with epoxy [7]. For representation of general crack propagation, assumed crack
propagation of 0.25 a/W notched BFR specimen are given in Fig. 11.
Fig. 11. Assumed crack propagation of 0.25 a/W notched BFR composite.
Fig. 12. Fracture toughness of GFR and BFR composites.
The fracture toughness values (energy release rate) of BFR and GFR composite were calculated
according to Equation 1 and are given in Fig. 12. When the values in the chart were examined, fracture
toughness of BFR specimens for each a/W ratio was found to be higher than GFR specimens. The fracture
toughness of GFR and BFR specimens for notch depth ratios get slightly different values. While the notch depth
ratio is increasing, a very small decrease in the fracture toughness values is observed.
When the fracture toughness was analyzed, high values were attained due to the high fiber volume
fraction. In many studies it was examined that impact energies increase when fiber volume fraction increased.
Lee and Cheon observed that maximum impact energies increased when the fiber volume fraction of filament
wound GFR / epoxy composites was around 60% and they reported that above this fiber volume fraction, impact
energies decreased [19]. While in their study the fracture toughness was about 600 kJ/m2 at 60-65% fiber volume
fractions, the fracture toughness values of GFR composites at the fiber volume fraction of 61% in our study were
similar to the work of Lee and Cheon.
Fig. 13. SEM image of the fracture surface of BFR (a) and GFR (b) composites.
According to experimental results and SEM images of BFR composites as given in Fig. 13 (a), it was
observed that the fiber breakage was more dominant than delamination and pullout damages, especially in low
notch depth ratios for BFR composites due to their good adhesion strength with epoxy. Surface roughness of
basalt fiber (see Fig.1) may be decreased pull out and debonding damage by providing good bonding [27].
However, in GFR composites, as given in Fig. 13(b), both pull-out and fiber breakage damage modes were seen
as damage modes. All of the damage modes are clearly visible in Fig. 13 (a) and (b). Dehkordi et al. indicated
that impact energy was transferred to the matrix during low-speed impact tests applied to BFR composites and
when impact strength exceeded basalt fiber strength, depending on the fiber matrix adhesion strength, the fiber
breakage occurred on fracture surface. And so they found that fiber breakage was the effective fracture
mechanism on fracture surfaces of BFR composites [12].
Conclusions
At the end of the Charpy impact test and image processing of arc shaped [±55o]6 BFR and GFR/epoxy
composites, the main findings are given below.
• The Charpy impact test to determine the fracture toughness and damage types of BFR and GFR/epoxy
composites was applied as practically.
• BFR/epoxy composites showed higher impact energies and fracture toughness than GFR/epoxy
composites for each of the notch depth ratios (a/W).
• The absorbed impact energy decreased when the notch depth ratio of BFR and GFR composites
increased. The delamination damage is most effective to absorb high impact energy for low-notch
depth ratio (a/W).
• The delamination areas of BFR and GFR/epoxy composites were calculated by using the image
processing method. The highest delamination areas for each a/W ratio were founded on GFR/epoxy
composites. As the notch depth ratio (a/W) increased, the differences in the delamination areas between
BFR and GFR/epoxy composites decreased. It was considered that this was caused by the increasing
a/w ratio activating fiber breakage damage.
• According to the test results and literatures, the effect of surface roughness of fiber for providing good
bonding with matrix particularly in polymer resins, was observed on BFR/epoxy composites and lower
delamination area of BFR/epoxy composites were clarified by this identification. The fine interface
adhesion of BFR affected the delamination damage.
• The delamination and pull-out damage modes occurred at low a/W ratios (0.25 and 0.38), while fiber
breakage damage mode were observed at high a/W ratios (0.5 and 0.63).
• When SEM images of the fracture surface of the composites were analyzed, the fiber breakage and pull-
out were found out to be the more effective damage modes on GFR composites. However, the fiber
breakage was observed intensively on BFR composites due to the fine interaction between the basalt
fiber and epoxy.
Acknowledgements
Some basalt fiber data was benefited from a Ph.D. thesis studies of Mehmet Turan Demirci supported by the
Selcuk University Scientific Research Projects (B.A.P) under grant number 11101030. In addition, Thanks to
Asist. Prof. Dr. Rahmi Akın at Nişantaşı University for his helping us.
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Figure Captions and Figures
Fig. 1. Diameter values of basalt fiber.
Fig. 2. Specimens obtained from BFR and GFR filament wound pipes[21].
Fig. 3. a) Charpy test device b) Fundamental Principle of the Charpy impact test.
Fig. 4 Experimental set up of specimen.
Fig. 5. Schematic picture of the Image Processing System�
Fig. 6. Injected white color layer a) Separated layer b) Identification of % delamination areas by Image
processing method for BFR specimen c).
Fig. 7. Impact energies of the BFR and GFR composite specimens.
Fig. 8. Damage types of GFR a) 0.25 a/W b) 0,38 a/W) and BFR c) 0.25 a/W d) 0,38 a/W
Fig. 9. Damage types of GFR a) 0.5 a/W b) 0,63 a/W) and BFR c) 0.5 a/W d) 0,63 a/W
Fig. 10. Delamination areas of BFR and GFR composites.
Fig. 11. Assumed crack propagation of 0.25 a/W notched BFR composite.
Fig. 12. Fracture toughness of GFR and BFR composites.
Fig. 13. SEM image of the fracture surface of BFR (a) and GFR (b) composites.
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Fig. 1. Diameter values of basalt fiber.
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Fig. 2. Specimens obtained from BFR and GFR filament wound pipes[21].
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Fig. 3. a) Charpy test device b) Fundamental Principle of the Charpy impact test.
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Fig. 4 Experimental set up of specimen.
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Fig. 5. Schematic picture of the Image Processing System�
a) b)
c)
Fig. 6. Injected white color layer a) Separated layer b) Identification of % delamination areas by Image processing method for BFR specimen c).
c) d)
Fig. 9. Damage types of GFR a) 0.5 a/W b) 0,63 a/W) and BFR c) 0.5 a/W d) 0,63 a/W
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Fig. 10. Delamination areas of BFR and GFR composites.
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Fig. 11. Assumed crack propagation of 0.25 a/W notched BFR composite.
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Fig. 12. Fracture toughness of GFR and BFR composites.
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Fig. 13. SEM image of the fracture surface of BFR (a) and GFR (b) composites.
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List of Tables
Table 1 Comparison of mechanical properties of basalt and E-glass [7].
Table 1 Comparison of mechanical properties of basalt and E-glass [7]. �
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Tensile strength
(MPa)
Elastic modulus
(GPa)
Density
(g/cm3)
Elongation
at break(%)
Max operating
temp. (oC)
Basalt 4840 89 2.8 3.1 650
E-Glass 3450 72.4 2.6 4.7 380