future synthesis and annealing program in cmpmsd · pdf filemotivations for hot isostatic...
TRANSCRIPT
![Page 1: Future Synthesis and Annealing Program in CMPMSD · PDF fileMotivations for Hot Isostatic Press " Oxygen Annealing for High Temperature Superconductors and for High Pressure Single](https://reader031.vdocuments.net/reader031/viewer/2022030504/5ab13f437f8b9a1d168c54e2/html5/thumbnails/1.jpg)
Future Synthesis and Annealing Program in CMPMSD
Ø Manufacturer: American Isostatic Presses, Inc
Ø Gas pressure to 100,000 psi, up to 20% Oxygen
Ø Installation: Chemistry, Site specifically
configured for HIP
Ø Acceptance testing at BNL ongoing
![Page 2: Future Synthesis and Annealing Program in CMPMSD · PDF fileMotivations for Hot Isostatic Press " Oxygen Annealing for High Temperature Superconductors and for High Pressure Single](https://reader031.vdocuments.net/reader031/viewer/2022030504/5ab13f437f8b9a1d168c54e2/html5/thumbnails/2.jpg)
Motivations for Hot Isostatic Press
§ Oxygen Annealing for High Temperature Superconductors and for High Pressure Single Crystal Growth.
§ Is High Tc primarily a 2D Phenomena occurring in CuO Planes?
§ Can Tc be increased by Oxygen Annealing? § Stored Energy Required ASME, Boiler and Pressure
Vessel Code, Section VIII, Division 3
![Page 3: Future Synthesis and Annealing Program in CMPMSD · PDF fileMotivations for Hot Isostatic Press " Oxygen Annealing for High Temperature Superconductors and for High Pressure Single](https://reader031.vdocuments.net/reader031/viewer/2022030504/5ab13f437f8b9a1d168c54e2/html5/thumbnails/3.jpg)
3
Overview of AIP Hot Isostatic Press
§ Design Pressure 110,000 psi at 400o F § Operating Pressure 100,000 psi at 400o F § Hydrotest Pressure 137,500-144,375 psi § Furnace 1200o C § Oxygen Annealing to 20% Oxygen § Vessel Temp Range 40 - 400o F § Inside Diameter 4.998”/5.000” § Inside Length 16” Nominal § Internal Volume 0.18 cubic feet § Vessel Weight 3000 lbs § Yoke Weight 6,000 lbs § Stored Energy 2.5 Mega Joules ~ 1
stick of dynamite
![Page 4: Future Synthesis and Annealing Program in CMPMSD · PDF fileMotivations for Hot Isostatic Press " Oxygen Annealing for High Temperature Superconductors and for High Pressure Single](https://reader031.vdocuments.net/reader031/viewer/2022030504/5ab13f437f8b9a1d168c54e2/html5/thumbnails/4.jpg)
![Page 5: Future Synthesis and Annealing Program in CMPMSD · PDF fileMotivations for Hot Isostatic Press " Oxygen Annealing for High Temperature Superconductors and for High Pressure Single](https://reader031.vdocuments.net/reader031/viewer/2022030504/5ab13f437f8b9a1d168c54e2/html5/thumbnails/5.jpg)
5
![Page 6: Future Synthesis and Annealing Program in CMPMSD · PDF fileMotivations for Hot Isostatic Press " Oxygen Annealing for High Temperature Superconductors and for High Pressure Single](https://reader031.vdocuments.net/reader031/viewer/2022030504/5ab13f437f8b9a1d168c54e2/html5/thumbnails/6.jpg)
![Page 7: Future Synthesis and Annealing Program in CMPMSD · PDF fileMotivations for Hot Isostatic Press " Oxygen Annealing for High Temperature Superconductors and for High Pressure Single](https://reader031.vdocuments.net/reader031/viewer/2022030504/5ab13f437f8b9a1d168c54e2/html5/thumbnails/7.jpg)
![Page 8: Future Synthesis and Annealing Program in CMPMSD · PDF fileMotivations for Hot Isostatic Press " Oxygen Annealing for High Temperature Superconductors and for High Pressure Single](https://reader031.vdocuments.net/reader031/viewer/2022030504/5ab13f437f8b9a1d168c54e2/html5/thumbnails/8.jpg)
![Page 9: Future Synthesis and Annealing Program in CMPMSD · PDF fileMotivations for Hot Isostatic Press " Oxygen Annealing for High Temperature Superconductors and for High Pressure Single](https://reader031.vdocuments.net/reader031/viewer/2022030504/5ab13f437f8b9a1d168c54e2/html5/thumbnails/9.jpg)
Top Platen
![Page 10: Future Synthesis and Annealing Program in CMPMSD · PDF fileMotivations for Hot Isostatic Press " Oxygen Annealing for High Temperature Superconductors and for High Pressure Single](https://reader031.vdocuments.net/reader031/viewer/2022030504/5ab13f437f8b9a1d168c54e2/html5/thumbnails/10.jpg)
Furnace
![Page 11: Future Synthesis and Annealing Program in CMPMSD · PDF fileMotivations for Hot Isostatic Press " Oxygen Annealing for High Temperature Superconductors and for High Pressure Single](https://reader031.vdocuments.net/reader031/viewer/2022030504/5ab13f437f8b9a1d168c54e2/html5/thumbnails/11.jpg)
Bottom Platen, Electrodes, TC’s