g_o'brien phd dissertation

272
Design and Fabrication of MEMS Angular Rate and Angular Acceleration Sensors with CMOS Switched Capacitor Signal Conditioning by Gary J. O’Brien A dissertation submitted in partial fulfillment of the requirements for the degree of Doctor of Philosophy (Electrical Engineering) in The University of Michigan 2004 Doctoral Committee: Professor Khalil Najafi, Chair Professor Richard B. Brown Professor Noel C. Perkins Professor Kensall D. Wise Dr. David J. Monk, Sensor Development Engineering Manager, Sensor Products Division, Motorola Inc.

Upload: gary-obrien

Post on 16-Jul-2015

151 views

Category:

Documents


10 download

TRANSCRIPT

Page 1: G_O'Brien PhD Dissertation

Design and Fabrication of MEMS Angular Rate and Angular Acceleration Sensors with CMOS Switched

Capacitor Signal Conditioning

by

Gary J. O’Brien

A dissertation submitted in partial fulfillment of the requirements for the degree of

Doctor of Philosophy (Electrical Engineering)

in The University of Michigan 2004

Doctoral Committee:

Professor Khalil Najafi, Chair Professor Richard B. Brown Professor Noel C. Perkins Professor Kensall D. Wise Dr. David J. Monk, Sensor Development Engineering Manager, Sensor Products Division, Motorola Inc.

Page 2: G_O'Brien PhD Dissertation

© Reserved Rights All

BrienO' J.Gary 2004

Page 3: G_O'Brien PhD Dissertation

ii

DEDICATION

This dissertation is dedicated to my wife Pamela and son Connor whose

unyielding love, support, and encouragement have enriched my soul and inspired me to

pursue and complete this research.

Page 4: G_O'Brien PhD Dissertation

iii

ACKNOWLEDGMENTS

I would like to express my gratitude and appreciation for the guidance and support

given by my research advisor Professor Khalil Najafi. I also would like to thank

Professors Wise, Brown, and Perkins for their interest in my research. Many thanks to

Professor Perkins for discussions on rotating body dynamics.

I would also like to express my sincere gratitude to Dr. David Monk, Sensor

Development Engineering Manager, Motorola Sensor Products Division. Dave was able

to provide me with technical guidance, vision, and focus while functioning as both my

manager at Motorola and as my PhD industrial research advisor. Demetre Kondylis

supported this research through direct funding in his former role as Operations Manager,

Motorola Sensor Products Division. I will be forever grateful to Demetre for his

passionate and loyal support without whom none of this research would have been

possible. Brett Richmond continued to support my research efforts after taking the

leadership helm as General Manager, Motorola Sensor Products Division. I would like to

take this opportunity to thank Brett for his continued support and leadership in addition to

being a fellow Georgia Tech alumni (“GO Jackets”).

I want to thank my inertial sensor research group members, past and present, Arvind

Salian, Jun Chae, Hsiao Chen, Fatih Kocer, Haluk Kulah, and Jason Weigold for all their

help and friendship. I would especially like to thank both Arvind and Ark Wong for the

many interesting discussions regarding design and operation of MEMS devices while

working many late hours in the Solid State Electronics Lab.

Page 5: G_O'Brien PhD Dissertation

iv

Mike McCorquodale, Ruba Borno, T. J. Harpster, Stefan Nikles, and Joseph Potkay,

all welcomed and allowed me to virtually live at their Ann Arbor apartment on multiple

occasions during my last year and a half of research for which I will be forever grateful.

Near honorable mention is in order for Brian Stark who was the source and sink of much

humor during my years in Ann Arbor; I wish him the best of luck in his future virtual

engineering endeavors.

I also wish the best of luck to the spring/2004 wave of Michigan PhD graduates who I

was fortunate enough to take classes with in addition to spending many hours in the

SSEL clean room including Andy DeHennis, T-Roy Olsson, Brian Stark, Mike

McCorquodale, Keith Kraver, and T.J. Harpster (who was kind enough to bring

donuts/drinks to my final defense for PhD committee and audience members).

I would also like to thank my sister Kathy and parents Jane and Donald O’Brien for

their love, support and encouragement. Both my grandmothers passed away during the

course of this research and I would like to sincerely thank both Lillian Brennen-O’Brien

and Alberta Nelson-Smith for all their love, support, and fond memories which I will

forever cherish.

This dissertation is dedicated to my wife Pamela Okamoto-O’Brien and son Connor

whose unyielding love, support, and encouragement have enriched my soul and inspired

me to both pursue and complete this research.

Finally, I would like to thank all my past Michigan MEMS research professors,

friends, and alumni with a loud and clear cheer; “GO BLUE”.

Page 6: G_O'Brien PhD Dissertation

v

TABLE OF CONTENTS

DEDICATION................................................................................................................... ii

ACKNOWLEDGEMENTS ............................................................................................ iii

LIST OF FIGURES ......................................................................................................... ix

LIST OF TABLES ...........................................................................................................xv

LIST OF APPENDICES ............................................................................................... xvi CHAPTER

1. INTRODUCTION.........................................................................................1

1.1 Automotive Accelerometer Evolution .............................................2

1.2 MEMS Linear Axis Accelerometers................................................4

1.2.1 Piezoelectric Inertial Sensor Transduction ...................................7

1.2.2 Piezoresistive Inertial Sensor Transduction..................................8

1.2.3 Tunneling Inertial Sensor Transduction......................................11

1.2.4 Thermal Inertial Sensor Transduction ........................................13

1.2.5 Capacitive Inertial Sensor Transduction.....................................15

1.3 MEMS Angular Acceleration and Rate Sensors............................17

1.4 Thesis Outline ................................................................................19

2. VIBRATORY RATE GYROSCOPE PRINCIPLES ..............................21

2.1 Foucault Pendulum History ...........................................................22

2.2 Foucault Pendulum Properties .......................................................24

2.3 Pendulum Physical Properties........................................................27

Page 7: G_O'Brien PhD Dissertation

vi

2.4 Pendulum Normal Mode Model ....................................................29

2.5 Open Loop Normal Mode Model ..................................................32

2.6 Closed Loop Normal Mode Model ................................................33

2.7 Summary of Angular Rate Sensor Principles ................................34

3. VIBRATORY RATE GYROSCOPE TYPES..........................................35

3.1 Prismatic Beam Vibratory Gyroscopes..........................................35

3.2 Tuning Fork Vibratory Gyroscopes ...............................................37

3.3 Linear Axis Accelerometer Vibratory Gyroscopes........................39

3.4 Torsion Mode Vibratory Gyroscopes ............................................42

3.5 Vibrating Shell Gyroscopes ...........................................................45

3.6 Automotive Gyroscope Classification and Performance...............49

3.7 Vibratory Gyroscope Performance Summary................................51

4. SURFACE MICROMACHINED DUAL ANCHOR GYROSCOPE .............................................................................................53

4.1 Dual Anchor Gyroscope Basic Design and Performance Goals ..............................................................................................53

4.2 Angular Rate Sensor Operation .....................................................54

4.3 Basic Angular Rate Sensor Configuration.....................................57

4.4 Angular rate Sensor Design Enhancements...................................59

4.4.1 Anti-Stiction Beam Tip Anchors ................................................60

4.4.2 Dual Anchor Attach ....................................................................63

4.4.3 Z-Axis Overtravel Stop...............................................................69

4.4.4 Dual Beam Torsion Spring .........................................................73

4.4.5 Differential Dual Electrode Sense Ring Capacitance .................75

4.5 Angular Rate Sensor Resonant Frequency Models .......................80

4.6 Angular Rate Sensor Empirical Results.........................................82

Page 8: G_O'Brien PhD Dissertation

vii

4.7 Angular Rate Sensor FEA Simulation Results ..............................83

4.8 Brownian Noise .............................................................................85

4.9 Angular Rate Sensor Summary......................................................85

5. DUAL ANCHOR ANGULAR ACCELERATION SENSOR ................88

5.1 Angular Acceleration Sensor Fundamentals..................................88

5.2 Angular Acceleration Sensor Applications....................................91

5.3 Angular Rate Sensor and Angular Acceleration Sensor Design Comparison........................................................................92

5.4 Surface Micromachined Angular Accelerometer Basic Operation........................................................................................94

5.4.1 Surface Micromachined Angular Accelerometer Resonant Frequencies ...............................................................................105

5.5 Angular Accelerometer Surface Micromachined to SOI Design Conversion.......................................................................112

5.5.1 SOI Angular Accelerometer Basic Operation...........................119

5.5.2 SOI Angular Accelerometer Basic Signal Conditioning C-V Conversion ........................................................................127

5.5.3 SOI Angular Accelerometer Finite Element Analysis Simulation Results ....................................................................130

5.6 Angular Acceleration Sensor Summary.......................................133

6. CMOS SWITCHED CAPACITOR SIGNAL CONDITIONING ........137

6.1 Front End Architecture ................................................................137

6.2 Front End Capacitive Sensor Charge Redistribution ...................140

6.3 Theoretical Calculation and SPICE Simulation Comparison ......143

6.4 CMOS Control Chip Top Level Overview..................................145

6.5 CMOS Signal Conditioned Angular Accelerometer Electrical Output ..........................................................................................147

6.6 CMOS Signal Conditioned Angular Acceleration Sensor Summary ......................................................................................149

Page 9: G_O'Brien PhD Dissertation

viii

7. SENSOR FABRICATION PROCESS FLOWS ....................................152

7.1 SOI Sensor Mechanical Anchor Fabrication Fundamentals........153

7.2 Short SOI Process Flow...............................................................154

7.2.1 Clear Field Sensor Perimeter Fabrication .................................156

7.2.2 Dark Field Sensor Perimeter Fabrication..................................157

7.3 Integrated SOI Process Flow .......................................................159

7.3.1 Substrate Anchor Trench Refill Etch Stop Process Example ...160

7.4 SOI Process Flow Summary ........................................................166

8. SUMMARY AND FUTURE WORK ......................................................168

APPENDICES ................................................................................................................173

BIBLIOGRAPHY ..........................................................................................................241

Page 10: G_O'Brien PhD Dissertation

ix

LIST OF FIGURES

Figure 1.1 Electromechanical event accelerometer used 1990’s automobiles.................2

Figure 1.2 Simple mass-spring accelerometer with acceleration along z-axis.................5

Figure 1.3 Piezoresistive strain-gage based silicon accelerometer. ...............................10

Figure 1.4. Tunneling tip accelerometer with electrostatic force feedback loop ............12

Figure 1.5 Thermal accelerometer isometric view.........................................................13

Figure 1.6 Thermal accelerometer cross section ............................................................14

Figure 1.7 Thermal accelerometer differential temperature profile versus x-axis .........14

Figure 1.8 Capacitive sensor configuration cases ..........................................................16

Figure 1.9 Capacitive accelerometer sandwiched between two glass wafers ................17

Figure 2.1 Foucault pendulum located at north pole......................................................24

Figure 2.2 Foucault pendulum path as interpreted by earth bound observer .................25

Figure 2.3 Rotation of Foucault pendulum as a function of latitude..............................26

Figure 2.4. Foucault pendulum rotation coupling at different locations on earth ...........26

Figure 2.5 Simple pendulum and mass-spring system oscillators..................................27

Figure 2.6 Foucault pendulum normal mode model ......................................................30

Figure 2.7 Open loop angular rate sense operation ........................................................32

Figure 3.1 Rectangular beam vibrating rate gyroscope..................................................35

Figure 3.2 Murata Gyrostar triangular beam gyroscope ................................................36

Figure 3.3 Tuning fork y-axis drive and x-axis Coriolis coupling about z-axis ............38

Figure 3.4 Dual accelerometer isometric view and cross section ..................................40

Figure 3.5 Dual accelerometer linear acceleration signal rejection ...............................41

Figure 3.6 Prismatic beam torsion decoupled mode vibratory gyroscope .....................42

Figure 3.7 Two axis vibrating disc gyroscope ...............................................................43

Page 11: G_O'Brien PhD Dissertation

x

Figure 3.8 Polysilicon vibrating disc gyroscope Coriolis induced rotation ...................44

Figure 3.9 Top and side view of decoupled torsion mode vibratory gyroscope ............44

Figure 3.10 Wine glass shaped hemispherical resonator gyroscope ................................46

Figure 3.11 Node precession of the HTG with externally applied angular rate...............47

Figure 3.12 Micromachined vibrating ring gyroscope drive and sense modes................48

Figure 4.1 Angular rate sensor Coriolis force diagram..................................................55

Figure 4.2 Basic angular rate sensor cross section.........................................................57

Figure 4.3 Basic polysilicon angular rate sensor configuration .....................................58

Figure 4.4 Centrally anchored polysilicon beam springs ...............................................58

Figure 4.5 Simple torsion beam spring outer mass coupling suspension.......................59

Figure 4.6 Enhanced anchor parallel plate electrostatic sense-actuation arrays ............60

Figure 4.7 Centrally anchored electrostatic array vertical stiction.................................61

Figure 4.8 Standard and split central drive disc designs ................................................61

Figure 4.9 Electrostatic beam array cross section with tip anchors ...............................62

Figure 4.10 Tip anchor electrical isolation on nitride passivated substrate .....................62

Figure 4.11 Fixed electrode parallel plate array substrate electrode interconnect ...........63

Figure 4.12 Dual anchor angular rate sensor suspension .................................................64

Figure 4.13 Folded beam and torsion post equivalent spring constant model .................64

Figure 4.14 Folded beam equivalent spring constant model............................................65

Figure 4.15 Z-axis mechanical over-travel stop...............................................................69

Figure 4.16 Mechanical over-travel stop tilted view........................................................70

Figure 4.17 Sub-micron mechanical over-travel stop-gap ...............................................71

Figure 4.18 Enhanced angular rate sensor decoupled mode suspension..........................74

Figure 4.19 Dual torsion beam coupling spring ...............................................................74

Figure 4.20 Dual torsion beam coupling spring stress concentration simulation ...........75

Page 12: G_O'Brien PhD Dissertation

xi

Figure 4.21 Angular rate sense ring capacitance electrode configuration ......................76

Figure 4.22 Tilted view of differential electrode capacitor..............................................76

Figure 4.23 Differential capacitor support post detail......................................................77

Figure 4.24 Drive disc displacement and velocity at sense ring inner radius (rin) ...........78

Figure 4.25 Angular rate coupled Coriolis force sense ring displace simulation.............78

Figure 4.26 Sense ring z-axis displacement electrode capacitance and schematic ..........79

Figure 4.27 Sense mode resonant frequency measurement test configuration ................82

Figure 4.28 Sense mode resonant peak @44.96kHz, Q=225...........................................83

Figure 4.29 Angular rate sensor measurement data .........................................................83

Figure 5.1 Description of rigid body rotation using a fixed particle point reference.....89

Figure 5.2 Example of rate table excited with 15 deg. displacement 2Hz sinusoid.......89

Figure 5.3 Angular rate sensor and angular acceleration sensor comparison ................92

Figure 5.4 Angular acceleration sensor capacitive parallel plate beam arrays ..............93

Figure 5.5 Capacitive angular acceleration sensor bond pad electrical schematic ........93

Figure 5.6 Angular accelerometer disc configuration ....................................................94

Figure 5.7 Capacitive array radial dimensions referenced from center of rotation........95

Figure 5.8 Angular accelerometer dual beam spring suspension attach points..............97

Figure 5.9 Outer connected spring constant directed along x-y plane ...........................98

Figure 5.10 Inner connected spring constant directed along x-y plane............................98

Figure 5.11 Interleaved folded beam spring design .........................................................99

Figure 5.12 Lateral spring constant theoretical model and FEA simulation results ......100

Figure 5.13 %ΔC/C0 Vs beam spring length (L) and outer disc radius (R2). .................101

Figure 5.14 Outer connected spring constant directed along z-axis...............................102

Figure 5.15 Inner connected spring constant directed along z-axis ...............................102

Figure 5.16 Model of z-axis surface tension sensor displacement Vs thickness ...........104

Page 13: G_O'Brien PhD Dissertation

xii

Figure 5.17 Torsion mode frequency Vs spring length and outer disc radius................107

Figure 5.18 Modal z-axis frequency for 2μm thick proof mass disc .............................108

Figure 5.19 Modal z-axis frequency for 20μm thick proof mass disc ...........................108

Figure 5.20 Modal z-axis frequency ratio for 2μm thick proof mass disc .....................109

Figure 5.21 Modal z-axis frequency ratio for 20μm thick proof mass disc ...................110

Figure 5.22 Angular acceleration sensor design conversion from polysilicon to SOI...112

Figure 5.23 Centrally anchored folded beam spring array with solid central hub .........113

Figure 5.24 Beam spring substrate anchor and central hub detail..................................114

Figure 5.25 DRIE trench defined SOI suspension BOX anchor cross section ..............115

Figure 5.26 Angular acceleration sensor interleaved inner and outer radial anchors ....116

Figure 5.27 Angular acceleration sensor identical spring dual radius interleave...........117

Figure 5.28 SOI 20μm thick angular accelerometer ΔC/C0 sensitivity @α=100r/s2 ....118

Figure 5.29 Angular acceleration sensor and bond pad schematic ................................119

Figure 5.30 SOI angular accelerometer capacitive array radial dimensions..................120

Figure 5.31 Sensor capacitance Vs applied angular acceleration (α) ............................121

Figure 5.32 Linearized sensor capacitance Vs applied angular acceleration (α)...........122

Figure 5.33 Capacitive sensor C-V plot test equipment configuration ..........................124

Figure 5.34 Capacitance-Voltage plot theoretical comparison to empirical data ..........125

Figure 5.35 Self-Test capacitance array (N=10 electrodes) ...........................................125

Figure 5.36 Self-Test capacitance array applied voltage Vs angular acceleration(α) ...126

Figure 5.37 Simplified switched capacitor front end .....................................................128

Figure 5.38 Control chip voltage output Vs applied angular acceleration (α)...............129

Figure 5.39 Angular accelerometer two-chip interconnection top view........................130

Figure 5.40 ANSYS angular acceleration sensor meshed solid model..........................131

Figure 5.41 Displacement simulation of proof mass using z-axis linear acceleration ...132

Page 14: G_O'Brien PhD Dissertation

xiii

Figure 5.42 Beam spring displacement due to angular acceleration about z-axis .........133

Figure 6.1 Switched capacitor front end top level schematic.......................................138

Figure 6.2 Phases 0-2 front end charge distribution.....................................................141

Figure 6.3 Transmission gate charge re-distribution clock phase detail ......................142

Figure 6.4 Basic transmission gate schematic sub-circuit (T-gate7)............................143

Figure 6.5 First stage capacitance to voltage (C to V) transconduction slope .............144

Figure 6.6 Front end sample-and-hold voltage output for a 1%ΔC/C0 ........................144

Figure 6.7 CMOS control chip functional block diagram............................................145

Figure 6.8 CMOS control chip analog signal path top level schematic .......................146

Figure 6.9 CMOS control chip interfaced to capacitive angular accelerometer ..........147

Figure 6.10 CMOS control chip output voltage reference (Noise=4.3VRMS) ................148

Figure 6.11 Output voltage measurement for a sinusoidal 40r/s2 input .........................148

Figure 6.12 Angular rate table test equipment configuration.........................................149

Figure 6.13 Eccentric cam sinusoidal arm linkage with motor driven transmission .....149

Figure 7.1 Typical SOI MEMS mechanical BOX attached anchor .............................153

Figure 7.2 Short SOI process flow DRIE trench defined Box anchor cross section....155

Figure 7.3 Short SOI process flow released device and bond pad cross section .........155

Figure 7.4 Clear field perimeter SOI short process flow angular accelerometers .......156

Figure 7.5 Bond pad interconnect beam anchor electrical isolation from substrate ....157

Figure 7.6 Bond pad metal and interconnect beam detail ............................................157

Figure 7.7 Dark field perimeter SOI short process flow angular accelerometer..........158

Figure 7.8 Dark field SOI electrical short to bond pad with substrate contact plate....159

Figure 7.9 SOI anchor perimeter etch-stop process flow.............................................160

Figure 7.10 SOI anchor trench refill perimeter etch-stop example ...............................161

Figure 7.11 Polysilicon trench refill substrate electrical contact process flow..............162

Page 15: G_O'Brien PhD Dissertation

xiv

Figure 7.12 Polysilicon trench refill substrate electrical contact cleaved sample..........162

Figure 7.13 Substrate polysilicon electrical contact bond pad interconnection .............163

Figure 7.14 Substrate electrical contact cross section and electrical schematic ............164

Figure 7.15 Silicon dopant density (cm-3) Vs resistivity (Ω-cm)...................................165

Figure 8.1 Fully inner hub connected folded beam spring suspension ........................170

Figure 8.2 Fully inner hub connected folded beam spring suspension detail ..............170

Figure 8.3 1200μm angular accelerometer with extra beam spring folds....................171

Figure 8.4 1200μm angular accelerometer beam spring fold detail.............................172

Page 16: G_O'Brien PhD Dissertation

xv

LIST OF TABLES

TABLE

1.1 Inertial Sensor Transduction Types and Mechanisms ....................................7

1.2 Common MEMS transducer piezoelectric materials and properties ..............8

1.3 Typical piezoresistance coefficients for n- and p-type silicon.....................10

3.1 Multiple classes of gyroscope performance..................................................49

3.2 Commercial automotive gyroscope performance comparison ....................51

4.1 Angular rate sensor model comparison results ............................................84

4.2 ANSYS sense ring moment of inertia simulation results ............................84

5.1 Angular accelerometer specification data....................................................92

5.2 Angular accelerometer SOI model verification results..............................130

5.3 ANSYS modal frequency simulation results .............................................132

5.4 Commercial/research prototype angular accelerometer performance ........135

6.1 Simulated Vs theoretical sample and hold stage output voltage................143

Page 17: G_O'Brien PhD Dissertation

xvi

LIST OF APPENDICES APPENDIX

A. Electrostatic Latch and Release of MEMS Cantilever Beams....................173

B. Super Critical CO2 Chamber Design and Operation...................................193

C. Deep Reactive Ion Etch Tool Characterization ..........................................206

D. Switched Capacitor Low Pass Filter/Amplifier ..........................................225

E. Stiction Assisted Substrate Contact Design and Operation ........................230

F. Integrated SOI Process Flow ......................................................................236

Page 18: G_O'Brien PhD Dissertation

1

CHAPTER 1

INTRODUCTION

Inertial sensing is typically categorized into three distinct sensor system types

represented by linear axis acceleration, angular rate (gyroscopes), and angular

acceleration. The development and commercialization of high volume low cost silicon

surface micromachined linear axis accelerometers [1-3] has been the predominant micro-

electromechanical system (MEMS) based sensor application realized by the automotive

market over the past decade. However, due to rapid advances in MEMS fabrication

technology made over the past several years, design efforts have been recently re-focused

in the development of low cost automotive micromachined gyroscopes. Currently, the

primary automotive gyroscope applications are active vehicle traction control, roll over

detection, and stabilization systems [4-7]. The target resolution for automotive angular

rate sensors used to detect vehicle roll-over is typically less than 2deg/s in a 40Hz

bandwidth with a (+/-)300deg/s full scale span. Active vehicle control applications [6]

typically require a target resolution of less than 1deg/s in a 50Hz bandwidth with a (+/-)

100deg/s full scale span. The target cost is between $10 and $20 per sensor, with single

customer orders typically ranging in millions of units per year [8]. Angular acceleration

sensors are currently used as feedback elements for computer hard drive read/write head

positioning algorithm applications [9, 10] in commercial volumes [11] with target costs

typically ranging from $5 to $9 per sensor. Although automotive angular acceleration

crash detection applications have been proposed [12] they have not yet been realized in

the commercial domain due to the poor sensitivity and resolution of low cost MEMS

sensors currently commercially available. Applications such as hand held camera

stabilization and active vehicle control [6] may also benefit from the use of low cost

Page 19: G_O'Brien PhD Dissertation

2

lightweight angular accelerometers as closed loop feedback elements, provided sensors

with higher sensitivity and resolution can be provided in commercial volumes.

1.1 Automotive Accelerometer Evolution

The Intermodal Surface Transportation Efficiency Act (ISTEA), signed into law

during 1991, ensured that 100% of production automobiles sold in the United States were

to be equipped with occupant safety airbags by 1998. Electromechanical accelerometers

used for automotive crash detection and subsequent air bag deployment in the early

1990’s consisted of a roller anchored via a flat spring band [13] as shown in the top view

of Figure 1.1.

A B

A B

ConstantVelocity(0 acceleration)

Motion

Large deceleration (>6g) upon impact

R1

RAB = ∞ Ω

RAB ≅ R1Ω

Metal Cover

Baseplate

Backstop Roller ElectricalContact

Spring Band

ElectricalResistor

R1

Proof mass roller completes electrical contact circuit for >6g acceleration

A B

A B

ConstantVelocity(0 acceleration)

Motion

Large deceleration (>6g) upon impact

R1

RAB = ∞ Ω

RAB ≅ R1Ω

Metal Cover

Baseplate

Backstop Roller ElectricalContact

Spring Band

ElectricalResistor

R1

Proof mass roller completes electrical contact circuit for >6g acceleration

Figure 1.1 Electromechanical event accelerometer used in early 1990’s automobiles.

Page 20: G_O'Brien PhD Dissertation

3

Sufficient deceleration experienced during a crash event, typically in excess of 6g’s

(where 1g = 9.81m/s2), caused the roller to displace from its zero-acceleration position

until the electrical contact was closed as shown in the bottom view of Figure 1.1.

Electrical resistance measured at the accelerometer’s connections A and B provided the

airbag control system with discrete event detection where an open/short circuit

represented less/greater than 6g’s respectively. Three of the electromechanical discrete

event accelerometers were used in the early airbag control system loops to evaluate the

severity of a crash regarding discrimination of intentional activation/deployment. Two of

the accelerometers were placed in the vehicle’s front crush zone typically located on the

frame behind the front bumper or on the lower portion of the radiator supports [14]. The

remaining accelerometer was placed in the occupant zone either in or near the passenger

compartment often referred to as a “safing sensor”. Deceleration values experienced in

the crush and occupant zones are separated by both magnitude and phase (time).

Although the crush zone accelerometers provided both earlier crash warning and larger

deceleration magnitudes they were not able to discriminate actual acceleration values

occurring along the vehicle’s major axis. The “safing sensor” was added as a redundant

crash event verification accelerometer to prevent inadvertent airbag deployment should

both crush zone accelerometers either malfunction or experience a shock not correlated to

an actual crash event.

Micromachined electromechanical capacitive accelerometers [1-3] were a logical

replacement since these analog sensors provided sufficient bandwidth, sensitivity, and

resolution to facilitate adequate single point testing when located in the vehicle’s

occupant zone. MEMS capacitive accelerometers were initially available for less than $8

per device in production quantities. This represented a significant cost reduction over the

electromechanical event detection accelerometers supplied by Breed and TRW at a target

cost of $15 per device [14] where three devices were required per automobile. In

Page 21: G_O'Brien PhD Dissertation

4

addition, wiring harness costs were reduced using the single point MEMS accelerometer

approach. The MEMS accelerometers were less expensive, more reliable, provided a

continuous analog signal output, and were smaller than their electromechanical switch

counterparts.

A typical MEMS accelerometer currently used in the automotive airbag market is the

MMA3201D manufactured by Motorola. The MMA3201D accelerometer exhibits a

bandwidth of 0-400Hz, sensitivity of 50mV/g, span of (+/-) 40g, and resolution of 0.06g.

The continuous analog output of this type of MEMS accelerometer significantly

enhanced automotive inertial sensing control applications. Modern airbag deployment

control loops were quickly adapted in the mid 1990’s to recognize and discriminate front,

side, and rear vehicle crash signatures using rule based and/or fast Fourier transform

algorithms evaluated via electronic modules. The electronic modules consisted of

application specific integrated circuits coupled with embedded microprocessors.

Typically, the accelerometer was incorporated directly onto the electronic module’s

printed circuit board providing both electrical interconnection and mechanical support.

The front, side, and rear acceleration crash signatures of an automobile are model specific

requiring automotive manufacturers to tailor and qualify airbag crash detection

algorithms based on deceleration data acquired from intentionally crashed vehicles

whenever a new product line is introduced.

1.2 MEMS Linear Axis Accelerometers

Virtually all inertial MEMS sensors exhibit electromechanical transduction

components which can be modeled as simple linear or rotational acceleration. As a

result, inertial MEMS models contained in this thesis expand and exploit this relationship

wherever applicable.

Page 22: G_O'Brien PhD Dissertation

5

Linear accelerometers measure acceleration directed along a specific axis of desired

sensitivity. Typically the accelerometer consists of a mechanically suspended proof

mass-spring system as shown in Figure 1.2.

SpringAnchor

Fixed Electrode

Movable Proof-mass z0

z0 - Δz

KZ

MKf Z

π21

0 =

M = massKZ = spring constantaZ = accelerationFZ = acceleration force

Resonant Frequency

QMfTfKa Z

BrownianΔ

= 08π

Brownian Noise Equivalent Acceleration

KZ

x

yz

Zero Acceleration Proof Mass PositionNon-Zero Acceleration Proof Mass Displacement

T = temperatureΔf = bandwidthQ = quality factor

SpringAnchor

Fixed Electrode

Movable Proof-mass z0

z0 - Δz

KZ

MKf Z

π21

0 =

M = massKZ = spring constantaZ = accelerationFZ = acceleration force

Resonant Frequency

QMfTfKa Z

BrownianΔ

= 08π

Brownian Noise Equivalent Acceleration

KZ

x

yz

x

yz

Zero Acceleration Proof Mass PositionNon-Zero Acceleration Proof Mass Displacement

T = temperatureΔf = bandwidthQ = quality factor

T = temperatureΔf = bandwidthQ = quality factor

Figure 1.2 Simple mass-spring accelerometer with acceleration along z-axis.

An externally applied z-axis acceleration causes the movable proof-mass to translate

location as referenced to the initial gap (z0) between the proof-mass and fixed reference

electrode. The movable proof-mass experiences a mechanical force proportional to the

block’s mass (M) multiplied by the externally applied acceleration (aZ) as given by

Newton’s second law of motion in Eq. 1.1. The relationship between the mechanical

Page 23: G_O'Brien PhD Dissertation

6

spring constant (KZ) and proof-mass translation distance (ΔZ) due to an externally applied

force results in spring elongation described by Hooke’s law as given in Eq. 1.2.

ZZ MaF = (1.1)

ZZZ KF Δ= (1.2)

The relationship between applied acceleration and proof-mass displacement is

described by combining equations 1.1 and 1.2 as given in Eq. 1.3.

ZZ

Z aKM

=Δ (1.3)

Therefore, the proof-mass displacement (Δz) is directly proportional to the applied

external acceleration (aZ) and scaled by the ratio of mass (M) to the system’s mechanical

spring constant (KZ) for small linear deflections.

The proof-mass displacement as a function of applied external acceleration from the

zero-acceleration position is converted into an electrical signal using electronics

interfaced to the sensor. The electronic circuit configuration is dictated by the type of

acceleration sensor used. Inertial MEMS sensor interface circuits have been previously

demonstrated as compatible with capacitive [1-3], piezoelectric [15, 16], piezoresistive

[17-19], tunneling [20-25], and thermal [26] sensor transduction types as listed in Table

1.1.

Page 24: G_O'Brien PhD Dissertation

7

Table 1.1 Inertial Sensor Transduction Types and Mechanisms Sensor Type DC/Low Freq AC/High Freq Limit Transduction MechanismPiezoelectric >5 Hz >100kHz (4-40kHz typical) compression of spring redistrubutes chargePiezoresistive 0 Hz <10kHz (0.4-5kHz typical) stress in spring changes resistanceTunneling 0 Hz <1kHz (4-400Hz typical) tunneling currrent due to tip/electrode proximityThermal 0 Hz <100Hz (30-40Hz typical) thermal transport delay of heat pulse in N2 gasCapacitive 0 Hz >100kHz (1-20kHz typical) capacitive sense gap between mass/electrode

1.2.1 Piezoelectric Inertial Sensor Transduction

Crystalline materials in which an applied mechanical stress produces an electric

polarization, and reciprocally, an applied electric field generates a mechanical strain are

referred to as piezoelectric. Piezoelectric sensors are classified as “self generating” since

the electric field resulting from an applied mechanical stress generates a differential

voltage signal. However, a key potential limitation of this transduction mechanism is that

while the piezoelectric effect produces a DC charge polarization it will not sustain a DC

current [27, 28]. Therefore, piezoelectric transducers are inherently incapable of

providing a DC response. The limited low frequency response of piezoelectric

transducers is primarily due to parasitic charge leakage paths in the non-centrosymmetric

crystal materials under constant mechanical strain.

The piezoelectric differential voltage signal is easily signal conditioned using typical

low noise voltage amplification circuits [15]. Although silicon is not a piezoelectric

material, thin piezoelectric films such as PZT (lead zirconate titanate) or BaTiO3 (barium

titanate) can be deposited onto silicon substrates to form MEMS based sensors and

actuators. Several common piezoelectric materials and properties are listed in Table 1.2

[29].

Page 25: G_O'Brien PhD Dissertation

8

Table 1.2 Common MEMS transducer piezoelectric materials and properties. Material ZnO Quartz AlN BaTiO3 PZT Units

Piezoelectric coefficient (d33) 246 2.3 3.9 190 130 [pC/N]Relative dielectric constant (εr) 1400 4.5 8.5 4100 1000 εr ε0 [F/m]

Piezoelectric materials exhibit charge leakage under constant strain and eventually the

electric field providing the sensor differential voltage will decrease towards zero [30].

As a result, low frequency sensor operation at values less than 10Hz have been difficult

to demonstrate using piezoelectric transducer materials [14]. An example of a constant

mechanical strain would be to orient the accelerometer’s sense axis in line with the

earth’s gravitational field.

Piezoelectricity, pyroelectricity, and ferroelectricity share properties inherent to the

electrical polarization vector associated with the non-centrosymmetric crystals which

comprises the sensor bulk material. If a material is piezoelectric, in most cases it will

also be pyroelectric and ferroelectric with very few exceptions of exotic materials [29]

outside the scope of typical MEMS processing/research. The pyroelectric behavior limits

the use of these materials in automotive applications since most suitable piezoelectric

sensor materials exhibit considerable temperature sensitivity requiring some form of an

integrated sensor [15] or signal conditioned analog/digital compensation technique. The

increase in sensor interface complexity to compensate for pyroelectric effects coupled

with the lack of DC operation make piezoelectric sensing a less attractive technology

regarding automotive applications where large temperature spans and static operation are

key system requirements. While quartz has proven to be an excellent material regarding

negligible aging effects, this attribute does not describe thin film PZT deposited by

sputter or SOLGEL lanthanum doping techniques [31]. Creep and depoling of the

ferroelectric PZT material domains have been identified as possible material degradation

effects responsible for an observed 5% drop in displacement amplitude of a piezoelectric

Page 26: G_O'Brien PhD Dissertation

9

micromechanical resonator tested over a 100 hour period [32]. Delaminations have been

observed at the PZT-Pt interface [33], suggesting that these films may be susceptible to

interfacial failure with repeated bending which raises significant concern as to the long

term reliability of piezoelectric thin film deposition based sensors and actuators. The Pt

electrode may be replaced by other materials such as doped polysilicon with respect to

PZT film deposition and annealing which desirably developed a random polycrystalline

perovskite phase, but were also subject to tensile cracking [34]. Film integrity at the PZT

electrode film interface may require significant process innovation before this technology

can guarantee the high degree of reliability required for automotive safety applications

where a 10year operational device lifetime is a typical requirement.

1.2.2 Piezoresistive Inertial Sensor Transduction

Crystalline materials in which an applied mechanical strain produces a change in the

electrical resistance are piezoresistive. Many crystalline materials exhibit a change in the

mobility or the number of charge carriers as a function of volume deformation due to

applied mechanical stress [35]. The deformed volume affects the energy gap between the

valence and conduction bands resulting in a change in the number of available carriers

responsible for bulk electrical resistivity in semiconductor materials with additional

effects modeled by Herring [36]. Monocrystalline silicon exhibits a large piezoresistivity

[37] combined with excellent mechanical properties making this material a good

candidate for potential sensor applications regarding mechanical strain measurement [38-

40]. The use of dopant diffusion techniques in the fabrication of piezoresistive sensors

for stress, strain, and pressure was initially proposed by Pfann and Thurston [41] in 1961.

Thin single crystal silicon dopant diffused membranes were used to form a pressure

sensor fabricated by Tufte et al [42] in 1962 . The first micromachined piezoresistive

strain gage accelerometer was demonstrated by Roylance and Angell [17] in 1979 for use

in biomedical implants to measure heart wall accelerations. The accelerometer was

Page 27: G_O'Brien PhD Dissertation

10

fabricated from a silicon wafer sandwiched between two anodically bonded 7740 Pyrex

glass wafers to provide hermetic operation as shown in Figure 1.3.

Pyrex Glass

Pyrex Glass

Silicon MovableProof Mass

Cantilever Beam Diffused Piezoresistor

Device Cross-section

Cavity

AnodicBonds

Figure 1.3 Piezoresistive strain-gage based silicon accelerometer.

Strain gage accelerometers are fabricated by placing either deposited polycrystalline

silicon or diffused single crystal silicon resistors onto the proof mass suspension at areas

of peak stress [43]. The sensitivity of single crystal silicon is highly orientation

dependent based on πXX coefficients [37, 44] as shown in Table 1.3.

Table 1.3 Typical piezoresistance coefficients for n- and p-type silicon. Dopant Resistivity Concentration π11 π12 π44

n-type 11.7 3*1014 -102.2 53.4 -13.6p-type 7.8 2*1015 6.6 -1.1 138.1Units Ω-cm cm-3 10-11 Pa-1 10-11 Pa-1 10-11 Pa-1

Therefore, mask misalignment rotation errors during photolithography steps with the

wafer flat can result in some reduction in piezoresistive sensitivity. Polycrystalline

silicon is more tolerant of mask alignment rotation errors regarding piezoresistance, but is

less sensitive than single crystal material. Also, polycrystalline silicon piezoresistance is

strongly influenced by grain size. Large grain polycrystalline silicon can approach 60-

Page 28: G_O'Brien PhD Dissertation

11

70% the piezoresistance of single crystal silicon [45]. However, the piezoresistance of

small grain polysilicon is approximately seven times less than single crystal silicon [46].

Piezoresistance coefficients depend strongly on dopant type, n-type or p-type, and are

weak functions of doping levels for values less than 1019 cm-3, but then decrease

significantly as doping is increased. The piezoresistive coefficients also decrease with

increasing temperature, falling to 70% at 150C as compared to room temperature

operation. The piezoresistive temperature dependence is nonlinear which is compounded

with the need to compensate for the large temperature coefficient of resistivity due to

typically low dopant concentrations used [37, 44]. A Wheatstone bridge configuration

can be used to optimize the output sensitivity over temperature without the typical large

nonlinearity error due to temperature coefficients of resistance associated with other

compensation techniques such as increased voltage gain [47-49]. Doping can also be

increased at the cost of decreased piezoreistance sensitivity to compensate for undesirable

temperature coefficient of resistance effects.

1.2.3 Tunneling Inertial Sensor Transduction

Electron tunneling is used between a sharp conductive tip and electrode in near

contact suspended via a mechanical spring to form an accelerometer [21]. The tunneling

current (IT) is a function of the applied bias voltage (VB) and tip to proof-mass separation

(dT) where constants are used for the quantum mechanical barrier height (Φ = 0.2eV) and

αI = 1.025 Å-1eV-0.5. A feedback control loop is used to maintain a relatively constant

tunneling current (IT) by controlling the feedback voltage (VF) providing the electrostatic

force to maintain the movable proof-mass and tunneling tip separation (dT) as shown in

Figure 1.4.

Page 29: G_O'Brien PhD Dissertation

12

Anchor

Movable Proof Mass

Tunneling Tip

+

-

Silicon Substrate

IT VF

Suspension Spring

Dielectric (SiXNY)

dT

TI dBT eVI Φ−∝ α

VB

+

-

Anchor

Movable Proof Mass

Tunneling Tip

+

-

Silicon Substrate

IT VF

Suspension Spring

Dielectric (SiXNY)

dT

TI dBT eVI Φ−∝ α

VB

+

-

Figure 1.4 Tunneling tip accelerometer with electrostatic force feedback loop.

The tunneling tip bias voltage is typically less than 1 volt for separations on the order

of 10 angstroms between the tip and proof-mass. The separation distance is typically

fabricated much larger than the 10 angstrom operating gap where the electrostatic force

provided by the feedback loop is used to reduce and maintain the gap during operation.

The feedback loop voltage is typically on the order of 20 volts [50]. Mechanical shocks

experienced during normal device operation will inevitably result in undesirable tip to

proof-mass contact referred to as tip-crashing due to the small operating separation

distance. The accelerometer control electronics must also include current limiting during

tip-crashing to preclude destruction of the conductive tip [51]. The tunneling current

exhibits a 1/f noise spectrum with a noise floor on the order of 20nano-g/√Hz reported in

a 5Hz-1.5kHz bandwidth [52].

While tunneling accelerometers have proven to be extremely sensitive they have been

difficult to manufacture due to large device to device variation. Tunneling

accelerometers are not yet as repeatable as capacitive sensors regarding both their basic

sensitivity and noise characteristics [53].

Page 30: G_O'Brien PhD Dissertation

13

1.2.4 Thermal Inertial Sensor Transduction

The operating principle of a thermal accelerometer is based on the effect of

acceleration with respect to the free convection heat transfer of a hot gas bubble inside a

sealed cavity. A single-axis thermal accelerometer consisting of a central heater located

between two temperature coefficient of resistance (TCR) based polysilicon temperature

sensors suspended over an etched cavity, to provide thermal isolation to the silicon

substrate, has been previously demonstrated [26] as shown in Figure 1.5.

Silicon Substrate

Etched Cavity BottomOxide

HeaterTemp Sensor2Temp Sensor1

X

YZ

X

YZ

Figure 1.5 Thermal accelerometer isometric view.

The two suspended temperature sensors, temperature sensor1 (TS1) and temperature

sensor2 (TS2), are located at equal distances symmetric about the central heater as shown

in Figure 1.6. The temperature profile in the proximity of the central heater is symmetric

when no external acceleration is applied. However, the symmetry is disturbed when a

non-zero acceleration is applied as shown by dotted lines in Figure 1.7.

Page 31: G_O'Brien PhD Dissertation

14

BottomOxide

SidewallOxide Polysilicon

Nickel

Silicon Substrate

Heater

TempSensor1

TempSensor2

Etched Cavity

X

Z

Figure 1.6 Thermal accelerometer cross section.

Temperature

X AxisLocation

Zero X Axis Acceleration-X Axis Acceleration

X

T

+X Axis Acceleration

X

T

ΔT ΔT

HTRTS1 TS2HTRTS1 TS2 HTRTS1 TS2

Figure 1.7 Thermal accelerometer differential temperature profile versus x-axis.

The temperature coefficient of resistance of the lightly-doped polysilicon is used to

measure the differential temperature as a function of acceleration. The thermal time

constant of the temperature sensors, with their polysilicon coefficient of thermal

resistance controlled via doping concentration to approximately 2000ppm/C, are coupled

with the thermal properties of the sealed cavity gas as a multi-pole control system with

the first pole located at approximately 20 Hz [26]. A sensor bandwidth extension

technique has been described to extend the thermal accelerometer to 160Hz [54] by

increasing the analog system gain as a function of frequency matched with the initial

mechanical pole at 20dB/decade. This electrical-zero/mechanical-pole matching

Page 32: G_O'Brien PhD Dissertation

15

technique increases the apparent system bandwidth at the cost of significantly degraded

signal to noise ratio beyond the initial mechanical pole frequency. As a result, it may

prove difficult for this technology to achieve the 400Hz bandwidth typically required for

automotive accelerometer applications. In addition, the central heater consumes power

on the order of 20mW which must also be regulated, to maintain a constant heater

temperature versus an automotive ambient temperature swing of -40C to 85C, using

closed loop electronics which consume additional power. As a result, this method

consumes a significant amount of power and may prove difficult to implement in either

automotive or battery powered commercial applications where capacitive linear axis

accelerometers are currently available with lower power drain and wider signal

bandwidth.

1.2.5 Capacitive Inertial Sensor Transduction

An important advantage of capacitive accelerometers is that, as opposed to the

piezoresistive accelerometers, there is a very small degree of inherent temperature

sensitivity [55]. Changes in capacitance over temperature, for devices operated at

constant low pressures, are primarily attributed to the thermal expansion/contraction of

sensor electrodes causing a change in the effective dielectric gap. However, the

temperature coefficient for the dielectric constant of air, maintained at a constant pressure

of 1-atmosphere and normalized to 20°C, has been identified as 2ppm/°C for dry air and

7ppm/C for moist air [56]. Although non-zero, this capacitive temperature dependence is

typically orders of magnitude less than piezoresistive devices.

Capacitive sensors are typically integrated using a combination of fixed and movable

electrodes which sense mechanical displacement. The inherent nonlinearity associated

with several types of capacitive sensor operation is often overshadowed by their

Page 33: G_O'Brien PhD Dissertation

16

simplicity and very small temperature coefficients. Several potential capacitive sensor

configurations [57, 58] are illustrated in Figure 1.8.

a

b

c

a

c

ΔzΔz

ParallelPlate

Differential

C1

C2

z0 z0C1

a

c

Δx

z0C1

aΔx

z0C1 C2

a

c

z0

Δx

εrDielectric

b c

zzACΔ−

=0

01

εzz

ACΔ−

=0

01

ε

zzACΔ+

=0

02

ε0

101 z

yWC ε=

OverlapArea

xyA =

xxW Δ−=1

0

101 z

yWC ε=

0

202 z

yWC ε=

xxW Δ+=2

DifferentialOverlap Area

MovableDielectric

0

101 z

yWC ε=

0

202 z

yWC rεε=

21 CCCtotal +=

Case 1 Case 2 Case 3 Case 4 Case 5

a

b

c

a

c

ΔzΔz

ParallelPlate

Differential

C1

C2

z0 z0C1

a

c

Δx

z0C1

aΔx

z0C1 C2

a

c

z0

Δx

εrDielectric

b c

zzACΔ−

=0

01

εzz

ACΔ−

=0

01

ε

zzACΔ+

=0

02

ε0

101 z

yWC ε=

OverlapArea

xyA =

xxW Δ−=1

0

101 z

yWC ε=

0

202 z

yWC ε=

xxW Δ+=2

DifferentialOverlap Area

MovableDielectric

0

101 z

yWC ε=

0

202 z

yWC rεε=

21 CCCtotal +=

Case 1 Case 2 Case 3 Case 4 Case 5

Figure 1.8 Capacitive sensor configuration cases.

The parallel plate capacitor has been used to measure a spring suspended proof mass

displacement as a function of the separation between the proof mass and a fixed reference

electrode [59]. Interface circuits to convert the parallel plate sensor capacitance to an

output voltage signal have been previously demonstrated [60].

Differential capacitance accelerometers with a vertical out of plane displacement have

been demonstrated in bulk silicon [61], as shown in Figure 1.9, and surface

micromachined polysilicon [1, 3]. Lateral displacement in the wafer plane has also been

demonstrated using a differential capacitance interdigitated finger scheme [2]. The

maximum displacement of these devices is typically limited to 10% the initial gap due to

the non-linear capacitance relationship.

Page 34: G_O'Brien PhD Dissertation

17

Glass

Glass

Silicon MovableElectrode (b)

Fixed Metal Electrode (c)

Fixed Metal Electrode (a) a

b

c

Cantilever BeamSchematicDevice Cross-section

Figure 1.9 Capacitive accelerometer sandwiched between two glass wafers.

Interdigitated comb drives, which utilize electrode area overlap, can be used to sense

lateral [62] and vertical [63] proof mass displacement via linear capacitance changes.

However, this technique is typically used only for large travel electrostatic displacement

actuation due to its lower inherent sensitivity to the proof mass displacement .

Capacitive sensing is currently the default transduction mechanism for MEMS based

mass/spring accelerometers used in the automotive market [1-3] primarily due to its

relatively low temperature sensitivity.

1.3 MEMS Angular Acceleration and Rate Sensors

Angular accelerometers [10-12, 64] typically employ a capacitive inertial sensor

interface similar to the linear accelerometer described in the previous section. These

angular accelerometers complete the desired mapping of 6 degrees of freedom with

respect to accelerations directed along (linear x,y,z) and about (angular x,y,z) the x,y,z

axes. The major difference between a linear and angular accelerometer is in the proof

mass suspension mode coupling with all other aspects remaining virtually identical. As a

result, significant reuse of technology can be incorporated to fabricate angular

acceleration devices as described in Chapters 4 and 5 of this thesis.

Page 35: G_O'Brien PhD Dissertation

18

Gyroscopes measure angular rate optically or mechanically using either the Sagnac or

Coriolis effects [65], respectively. Currently, the performance of both ring laser and fiber

optic gyroscopes is far superior to that of their mechanical counterparts, but their high

manufacturing cost and size prohibits their use in low cost automotive applications even

in high volume production quantities [66]. As a result, mechanical Coriolis effect

gyroscopes currently dominate 100% of the automotive angular rate sensor market

During the past decade a great deal of research has been performed on MEMS based

vibratory rate gyroscopes (VRG) for intended use in automotive applications. Angular

rate sensors (gyroscopes) have been implemented using vibrating rings [67-69], prismatic

beams [70-74], tuning forks [75-77], and torsion [78, 79] oscillation.

Micromachined processing technologies capable of producing gyroscopes can be

categorized as piezoelectric quartz [6, 7], electroplated nickel [4, 68, 75], bulk silicon

[73, 80], surface micromachined polysilicon [1-3, 5, 8, 76-79], polysilicon trench refill

[63, 69], and silicon on insulator (SOI) [81-83]. Our research is focused on aspects of

both surface and SOI micromachining as these technologies represent the current trend to

fabricate the sensor and CMOS interface integrated circuitry in the same facility. Also,

single chip fusion comprised of sensor and integrated circuitry can be eventually realized

using this methodology.

1.4 Thesis Outline

Chapter 2 introduces the Foucault pendulum as a model for vibratory rate

gyroscopes. The normal mode model is described and several modes of gyroscope

operation are identified. Open and closed loop (force feedback) operation address the

trade-off between angular rate resolution and sensor bandwidth respectively.

Page 36: G_O'Brien PhD Dissertation

19

Chapter 3 describes the various classes and types of vibratory gyroscopes. Examples

from each class are presented with advantages and disadvantages compared from each

configuration. A list of desirable characteristics is presented as a set of design rules for

an enhanced surface micromachined gyroscope.

Chapter 4 introduces the surface micromachined dual anchor gyroscope as a means

to solve many of the challenges listed in Chapter 2. The desire for low cost surface

micromachined gyroscopes required several design and process innovations to increase

both device performance and yield. Device cross sections, process flow, and

characterization results are included. Device models specific to the dual anchor

gyroscope are presented with verification results simulated using ANSYS finite element

analysis (FEA) software.

Chapter 5 describes basic operation of angular accelerometers and provides a model

and characterization results of a surface micromachined dual anchor angular

accelerometer. Model results suggest thicker substrates are required to achieve angular

acceleration sensitivities to satisfy the computer hard disk and automotive markets. This

argument is used as a rationale to develop high aspect ratio angular acceleration sensors

in thick silicon on insulator (SOI) substrates. Characterization results are compared to

theoretical models and finite element analysis (FEA) simulation where applicable.

Chapter 6 describes the capacitive MEMS angular accelerometer and gyroscope

switched capacitor CMOS front end electronic signal conditioning architecture. Noise

rejection at the sensor interface is addressed at the initial capacitance to voltage (C-V)

stage by sampling the differential sensor capacitance values in parallel using a sample

Page 37: G_O'Brien PhD Dissertation

20

and hold technique. Switched capacitor transient simulations are compared to theoretical

transfer functions summarized in this thesis.

Chapter 7 describes the angular accelerometer fabricated in an SOI process flow.

Design enhancements made possible using SOI with a polysilcion/nitride trench refill

process are demonstrated.

Chapter 8 briefly summarizes the body of research included in this thesis and

suggests potential improvements to the demonstrated angular rate and acceleration sensor

designs.

Page 38: G_O'Brien PhD Dissertation

21

CHAPTER 2

VIBRATORY RATE GYROSCOPE PRINCIPLES

Vibrating elastic bodies, like the Foucault pendulum [84], can be used to measure

rotation. The vast majority of micromachined gyroscopes use vibrating mechanical

elements to sense rotation. These vibrating rate gyroscopes (VRG) are angular rate

sensing devices which have no unidirectional rotating parts that would require bearings

and as a result can be easily miniaturized and batch fabricated using micromachining

techniques [85]. Vibratory gyroscopes are based on the transfer of energy between two

normal operating modes of a structure described by Coriolis acceleration. Coriolis

acceleration, named after the French scientist and engineer G. G. de Coriolis (1792-

1843), is an apparent acceleration that arises in a rotating reference frame which is

proportional to the frame’s rate of rotation. MEMS vibratory gyroscopes which utilize

Coriolis acceleration to measure angular rate are typically categorized into one of several

basic classes; vibrating rings [67-69], prismatic beams [71-74], tuning forks [75-77],

and torsion [78, 79] oscillation.

This chapter describes the principles of vibratory gyroscope rotation measurement

using the Foucault pendulum as a reference model. The Foucault pendulum model is

referenced throughout this dissertation providing a consistent explanation as to how

vibratory gyroscopes work and as a comparison between the multiple classes listed

above. The normal mode model provides the theoretical basis to understand and predict

the performance of typical MEMS vibratory gyroscopes. As a result, the normal mode

model will be applied to multiple vibratory gyroscope classes, throughout the remainder

of this thesis, in order to predict angular rate sensitivity and compare different design

implementations.

Page 39: G_O'Brien PhD Dissertation

22

2.1 Foucault Pendulum History

Jean Bernard Leon Foucault (1819-1868), the inventor of the gyroscope in 1852,

demonstrated during the 1851 World's Fair that a pendulum could track the rotation of

the Earth. This work began in 1848 while Leon Foucault was setting up a long and

slender metal rod in his shop lathe. Foucault “twanged" the free end of the singly

clamped rod with an impulse, similar to a strike of a tuning fork, causing it to vibrate at

its natural frequency in a vertical direction. Foucault then slowly rotated the lathe chuck

by 90 degrees and observed no change in the vibration pattern vertical alignment.

Serendipity allowed Leon Foucault to analyze the physical implications of the

vibrating rod oscillation plane, observed to be independent of the lathe chuck base

rotation, and construct a second experiment to test his hypothesis. Subsequently, he set

up a small pendulum in his drill press, started the pendulum into oscillation by hand, and

then rotated the drill press about the earth’s gravity acceleration vector direction. Once

again, the pendulum kept swinging in its original oscillation plane independent of the fact

that its mounting point reference was rotating.

Foucault then spent the next several months constructing a 2 meter long wire

suspended pendulum with a 5 kilogram ball in his cellar workshop. Before the amplitude

of the swing was fully damped he observed that the weight on the end of the pendulum

appeared to rotate clockwise, as noted in Foucault’s journal at exactly two o'clock in the

morning on January 6, 1851 [86]. Foucault hypothesized that the rotation of the earth

must be responsible for the clockwise rotation of the pendulum pattern by analogy to the

rotating drill press in his previous experiment. Now convinced of the rotating reference

frame principle, Foucault constructed a second pendulum with an 11 meter wire in the

Paris Observatory and it also rotated clockwise as predicted due to the earth’s rotation.

Page 40: G_O'Brien PhD Dissertation

23

Foucault publicly demonstrated a 67-meter tall pendulum at the 1851 Paris Exhibition

in the Pantheon - a Parisian church. A stylus was placed under the 28 kg cannon ball

proof mass with sand scattered in a circular pattern to record the pendulum trace over

multiple oscillations. The cannon ball was pulled to one side and held fixed in place with

a string. With much ceremony, the string was ignited and the ball began to describe a

straight (non-elliptical) path in the sand. Within a few minutes, the pendulum had begun

to swing slightly clockwise and the previous narrow straight-line in the sand had widened

to look like a twin-bladed propeller. Foucault described to the crowd of invited guests

and formally trained scientists that the earth rotated "under" his pendulum. As a result,

he provided the empirical evidence for rotation of the earth that had been unsuccessfully

attempted by Copernicus, Kepler, Descartes, Galileo, and Newton during the preceding

three centuries.

In the following year, during 1852, Foucault repeated his pendulum experiment with

a massive spinning weight which he called the gyroscope [87]. He showed that the

gyroscope, just like the pendulum, ignored the local effect of earth rotation.

Foucault’s gyroscope used the relatively constant inertia of a large unidirectional

spinning mass, analogous to the sinusoidal inertia of the pendulum, to maintain the initial

proof mass oscillation plane independent of the earth’s rotating reference frame.

An object will remain either at rest or in uniform motion along a straight line unless

compelled to change its state by the action of an external force. This is normally taken as

the definition of inertia as described by Newton’s first law of motion. Inertia is the

physical property responsible for maintaining the oscillation plane of both the Foucault

pendulum and gyroscope fixed in space while the earth rotates beneath them.

Page 41: G_O'Brien PhD Dissertation

24

2.2 Foucault Pendulum Properties

MEMS vibratory rate gyroscopes do not exhibit the gyroscope property of constant

inertia due to a proof mass spinning with a constant rotation rate. It is therefore

unfortunate that MEMS angular rate sensors are referred to as vibratory rate gyroscopes.

Instead, MEMS vibratory rate gyroscopes operate very similar to the Foucault pendulum

based on their shared properties of bi-directional proof mass oscillation coupled with

displacement angles much smaller than 2π radians.

The Foucault pendulum can be most easily understood by considering a pendulum

that is set into motion at the earth’s north pole. To an observer, who is fixed in space

above the north pole, it appears that the plane of the pendulum swing remains stationary

while the earth rotates [88]. However, an observer standing on the earth at the north pole

would perceive that pendulum precession is occurring at the rotation rate of the earth (Ω

= 360°/day). The apparent force causing the pendulum to precess in a clockwise

direction, as viewed by the observer standing at the north pole, is described by the

Coriolis acceleration vector as shown in Figure 2.1.

North Pole

North Pole

South Pole Fixed Space View Above North Pole

Earth Rotation

Pendulum

Pendulum

aCoriolis

North Pole

North Pole

South Pole Fixed Space View Above North Pole

Earth Rotation

Pendulum

Pendulum

aCoriolis

Figure 2.1 Foucault pendulum located at north pole.

Page 42: G_O'Brien PhD Dissertation

25

The periodic path of the pendulum can be used to calculate the earth’s rotation rate

(Ω) via the measured period (τ) and the angular separation between complete precession

cycles (θ) as shown in Figure 2.2. In this mode of operation, called whole angle mode

[89], the pendulum operates as a rate integrating gyroscope.

North Pole

View Above North Pole at t=0

Earth Rotation

Pendulumbob

1

23

45

67

θ

8

View observed standing at north pole as earth rotates from t = 0-2τ, where τ = tB-tA

Pendulum path

Pendulumbob

A

B

Ω

Ω×= vaCoriolis 2

τθ

North Pole

View Above North Pole at t=0

Earth Rotation

Pendulumbob

1

23

45

67

θ

8

View observed standing at north pole as earth rotates from t = 0-2τ, where τ = tB-tA

Pendulum path

Pendulumbob

A

B

Ω

Ω×= vaCoriolis 2

τθ

Observer

Figure 2.2 Foucault pendulum path as interpreted by earth bound observer.

The coupling of the earth’s rotation with the Foucault pendulum, a strong function of

latitude, is based on the magnitude of the Coriolis acceleration. The Coriolis acceleration

vector magnitude and direction are defined by the cross products of the proof mass

velocity vector (v) and rotation rate vector (Ω) of the earth. The 0° latitude at the equator

orients the maximum velocity vector of the pendulum proof mass and the rotation vector

of the earth along a parallel direction resulting in a zero magnitude Coriolis acceleration

vector cross product. The maximum velocity vector of the pendulum proof mass is

tangent to the earth’s surface assuming an idealized uniform gravitational field at sea

level for all latitudes. The coupling of the Foucault pendulum, neglecting surface altitude

and gravitational deviations [90], as a function of latitude is described by the function

plotted in Figure 2.3.

Page 43: G_O'Brien PhD Dissertation

26

Equator

Pendulum

North Pole

South Pole

0 10 20 30 40 50 60 70 80 900

90

180

270

360

Pend

ulum

rota

tion

[°/d

ay]

Latitude location of pendulum

Lat 90° N

Lat 0°

Lat 90° S

)sin(360 latitudeday

=θEquato

r

Pendulum

North Pole

South Pole

0 10 20 30 40 50 60 70 80 900

90

180

270

360

Pend

ulum

rota

tion

[°/d

ay]

Latitude location of pendulum

Lat 90° N

Lat 0°

Lat 90° S

Equator

Pendulum

North Pole

Equator

Pendulum

North Pole

South Pole

0 10 20 30 40 50 60 70 80 900

90

180

270

360

Pend

ulum

rota

tion

[°/d

ay]

Latitude location of pendulum

Lat 90° N

Lat 0°

Lat 90° S

)sin(360 latitudeday

Figure 2.3 Rotation of Foucault pendulum as a function of latitude.

The coupling of earth’s rotation and the Foucault pendulum produces a clockwise

(CW) and counterclockwise (CCW) rotation as witnessed by a local observer in the

northern and southern hemispheres respectively, as shown in Figure 2.4.

San Francisco~225°/day CW

Mexico City~120°/day CW

Ann Arbor~242°/day CW

Chandler, AZ~196°/day CW Equator

0°/day

North Pole360°/day CW

Cape Canaveral~175°/day CW

South Pole360°/day CCW

Rio de Janeiro~120°/day CCW

CW = ClockwiseCCW = Counterclockwise

San Francisco~225°/day CW

Mexico City~120°/day CW

Ann Arbor~242°/day CW

Chandler, AZ~196°/day CW Equator

0°/day

North Pole360°/day CW

Cape Canaveral~175°/day CW

South Pole360°/day CCW

Rio de Janeiro~120°/day CCW

CW = ClockwiseCCW = Counterclockwise

Figure 2.4 Foucault pendulum rotation coupling at different locations on earth.

Page 44: G_O'Brien PhD Dissertation

27

2.3 Pendulum Physical Properties

The simple pendulum is described by an idealized model consisting of a proof mass

suspended by a mass-less string of fixed length in a uniform gravitational field. When

the proof mass is pulled to one side of its straight down equilibrium position and

subsequently released it will oscillate along a semicircular path isochronously.

Although the pendulum is not truly a simple harmonic oscillator, enhanced insight

and overall model simplification is afforded by direct comparison to the operation of a

simple mass-spring system. The initial step requires defining the mechanical restoring

forces of the pendulum (FT) and mass-spring (Fx) systems, as shown in Figure 2.5, and

given by Eq. 2.1 and Eq. 2.2 respectively.

mm

TF

mg

Tθ L

2xK

2xKx

xKF xx −=

x

y

1 Degree of freedom pendulum 1 Degree of freedom mass-spring

)sin(θmgFT −=

mK x

x =ϖ

Spring

CartesianSystem

PolarSystem

Equilibriumposition

mm

TF

mg

Tθ L

2xK

2xKx

xKF xx −=

x

y

1 Degree of freedom pendulum 1 Degree of freedom mass-spring

)sin(θmgFT −=

mK x

x =ϖ

Spring

CartesianSystem

PolarSystem

mm

TF

mg

Tθ L

2xK

2xKx

xKF xx −=

x

y

1 Degree of freedom pendulum 1 Degree of freedom mass-spring

)sin(θmgFT −=

mK x

x =ϖ

Spring

CartesianSystem

PolarSystem

Equilibriumposition

Figure 2.5 Simple pendulum and mass-spring system oscillators.

)sin()( θθ mgFT −= (2.1)

xKxF xx −=)( (2.2)

Page 45: G_O'Brien PhD Dissertation

28

The pendulum mechanical restoring force is non-linear in nature. However, if the

maximum angle (θ) is small, the small angle approximation can be used to linearize the

pendulum model mechanical restoring force as given by Eq. 2.3.

θθ mgFT −≅)( (2.3)

The pendulum mechanical restoring force can then be converted to linear terms in x

using the relationship θ = x/L as given by Eq. 2.4.

xL

mgxFT −≅)( (2.4)

The linearized mechanical restoring force of the pendulum is defined by equating Eq.

2.2 and Eq. 2.4 while solving for Kx as given by Eq. 2.5.

LmgK x ≅ (2.5)

The resonant frequency of a simple mass-spring system is given by Eq. 2.6.

mK x=ϖ (2.6)

As a final step, we substitute Eq. 2.5 into Eq. 2.6 to represent the resonant frequency

of the pendulum in terms of a linearized simple mass-spring system as given by Eq. 2.7.

Lg

≅ϖ (2.7)

Page 46: G_O'Brien PhD Dissertation

29

The period of the linearized pendulum model is then dependent upon the length (L)

and gravity (g) defined by Eq. 2.8.

gLπτ 2≅ (2.8)

This results in the familiar relationship that a pendulum’s period (τ) is independent of

mass. This relationship approximates the pendulum motion as simple harmonic and is

valid only for small angle displacements. The linearized simple harmonic model error,

as compared to the accurate non-linear model regarding prediction of τ, is less than 0.5%

for an angular displacement of +/-15 degrees as measured from the pendulum equilibrium

position [91]. Therefore, the approximation is useful where small angle displacements

are prescribed.

All vibratory gyroscopes are based on the transfer of energy between two resonant

modes as a function of Coriolis acceleration. Although the Foucault pendulum is one of

the simplest vibratory gyroscopes, its basic operating principles can be applied to all

Coriolis acceleration based devices. As a result, the following section will address the 2-

D simple harmonic oscillation model of the Foucault pendulum.

2.4 Pendulum Normal Mode Model

Mathematically, the precession of the Foucault pendulum can be modeled as a

function of its normal mode model. The normal mode model consists of a central proof

mass suspended with linear mechanical springs oriented about the x and y axes as shown

in Figure 2.6.

Page 47: G_O'Brien PhD Dissertation

30

m

2xK

2xK

2 Degree of freedom pendulum 2 Degree of freedom mass-spring

Spring

2yK

2yK

x

y

z

Ωz

x

y

m

Ω×= vaCoriolis 2mm

2xK

2xK

2 Degree of freedom pendulum 2 Degree of freedom mass-spring

Spring

2yK

2yK

x

y

z

Ωz

x

y

m

Ω×= vaCoriolis 2

Figure 2.6 Foucault pendulum normal mode model.

Vibration theory provides a methodology from which any arbitrary vibration mode of

an elastic body can be modeled in terms of its normal modes [92]. These normal modes

of vibration are uncoupled in the absence of a rotating reference frame. The normal

mode model orients the drive and sense normal modes along the x and y axes

respectively which significantly simplifies the pendulum analysis. The coupled equations

of motion for the Foucault pendulum in the x-y plane [93] are given by Eq. 2.9 and 2.10,

where x(t) and y(t) represent the displacement amplitudes directed along the principal x

and y axes of vibration respectively.

0)()(2)( 22

2

=+Ω− txdt

tdydt

txdz ϖ (2.9)

0)()(2)( 22

2

=+Ω+ tydt

tdxdt

tydz ϖ (2.10)

The solution to this system of equations is given by Eq. 2.11 and Eq. 2.12.

Page 48: G_O'Brien PhD Dissertation

31

)sin()cos()( ttAtx z ϖΩ= (2.11)

)sin()sin()( ttAty z ϖΩ−= (2.12)

These normal mode solutions predict that the Foucault pendulum will transfer energy

between modes at a precession rate equal to the applied rotation rate about the z-axis.

This analysis assumes that the spring constant for both the x and y axes are equal forcing

the normal mode frequency (ω) to equivalent values for all possible solutions in the x-y

plane. Asymmetries due to variation in spring constant (Kx, Ky), distributed among

individual springs, are neglected in the normal mode model analysis.

Energy transfer in the normal mode model assumes no damping present in the system.

The damping coefficient (b) will be introduced in Chapter 3 as a parametric measurement

of energy loss in the system extracted from the quality factor (Q) which describes the

ratio of the normal mode energy storage/dissipation while excited at resonance (ω).

In a practical system, where the damping coefficient (b) is non-zero, energy must be

continually introduced into the system to maintain a constant drive mode amplitude at, or

near, resonance to compensate for energy dissipation. Damping can be attributed to

multiple factors including viscous damping of the ambient gas surrounding the resonating

proof mass [94], acoustic radiation of energy through the anchor supports [67], and

intrinsic energy dissipation in the resonator structural materials [95] where polysilicon,

single crystal silicon, and quartz represent several typical examples.

Page 49: G_O'Brien PhD Dissertation

32

2.5 Open Loop Normal Mode Model

Applying an excitation signal to maintain drive mode displacement amplitude while

simultaneously monitoring the sense mode displacement amplitude to measure the

angular rate signal is described as the open loop mode [89, 96] as shown in Figure 2.7.

2xK

2xKSpring

2yK

2yK

x

y

m

x-axis drive signal applied to maintain fixed amplitude at resonance

y-axis displacement signal used as parametric measurement of angular rate

ωzQ

xy Ω

= 2

2xK

2xKSpring

2yK

2yK

x

y

m

x-axis drive signal applied to maintain fixed amplitude at resonance

y-axis displacement signal used as parametric measurement of angular rate

ωzQ

xy Ω

= 2

Figure 2.7 Open loop angular rate sense operation.

The quality factor (Q) is a function of the proof mass (m), the resonant frequency (ω),

and the damping coefficient (b) as given by Eq. 2.13.

bmQ ω= (2.13)

The ratio of x to y axis displacement amplitudes has been modeled as a function of

angular rate for a normal mode gyroscope with damping [96] and is given by Eq. 2.14.

ωzQ

xy Ω

= 2 (2.14)

Page 50: G_O'Brien PhD Dissertation

33

This relationship implies that the secondary mode is amplified by the quality factor

(Q) and inversely proportional to the resonant drive frequency (w). However, when the

pendulum based vibratory gyroscope is operated in open loop mode there is a lag time

associated between the application of an external angular rate and the corresponding y-

axis secondary mode to reach its steady state amplitude [96], as given by Eq. 2.15.

ωτ Q2

= (2.15)

The lag time between the externally applied angular rate signal and amplitude build-

up in the y-axis sense direction is the significant bandwidth limiting factor of the open

loop mode. However, the bandwidth can be significantly extended by using forced

feedback to null displacement of the sense mode [89, 96] similar to closed loop

accelerometer operation [2, 97].

2.6 Closed Loop Normal Mode Model

This mode of operation is similar to open loop operation with the additional

constraint that the y-axis amplitude is maintained at zero displacement. As a result, the

long time period (t) required to increase the sense axis amplitude over multiple drive

cycles at resonance (ω) is not required. This method potentially extends the sensor

bandwidth to the resonant drive frequency (ω) where an appropriate force feedback

signal is applied as given by Eq. 2.16.

ωz

xy QFF Ω= 2 (2.16)

Page 51: G_O'Brien PhD Dissertation

34

However, the application of the force feedback signal to null sense mode

displacement causes a control loop oscillation which introduces more system noise than

is observed for the open loop mode. This design trade-off results in an increased sensor

bandwidth with decreased angular rate resolution.

2.7 Summary of Angular Rate Sensor Principles

MEMS based vibratory rate gyroscopes utilize some aspect of the Foucault pendulum

normal mode model with very few potentially noteworthy exceptions [98]. This normal

mode model applies across the macro to micro domains where economy of scale can be

exploited in the latter [94]. Most vibratory rate gyroscope designs use quality factor

amplification to boost the coupled mode angular rate signal. Design trade-offs must be

evaluated dependent upon which method of angular rate measurement is employed. The

methods of angular rate measurement include whole angle, open loop, or closed loop

forced feedback. Typically, MEMS vibratory rate gyroscopes are operated in the open or

closed loop modes. Open loop mode sensing provides a simple and high resolution

measurement technique at the cost of significantly reduced bandwidth. As the quality

factor (Q) increases, angular rate sensitivity increases while bandwidth is decreased. The

closed loop forced feedback mode addresses the bandwidth problem by extending the

usable sensor bandwidth theoretically to near resonant operation frequencies. However,

this technique causes the proof mass to oscillate about the zero displacement position

which introduces intrinsic noise into the detection scheme. As a result, the closed loop

forced feedback technique provides a larger bandwidth, at the expense of reduced angular

rate resolution, when compared to an open loop implementation with identical sensor

configurations. Chapter 3 will describe previously introduced angular rate sensor

designs. Development of design trade-offs with respect to the vibratory rate gyroscope

designed, fabricated, and characterized as a function of this thesis work will be

documented in chapter 4.

Page 52: G_O'Brien PhD Dissertation

35

CHAPTER 3

VIBRATORY RATE GYROSCOPE CLASSES

Vibrating elastic bodies, similar to the Foucault pendulum [84], can be used to

measure rotation. Vibratory rate gyroscopes are based on the transfer of energy between

two normal operating modes of a structure described by Coriolis acceleration. MEMS

vibratory gyroscopes which utilize Coriolis acceleration to measure angular rate are

typically categorized into one of several basic classes; vibrating rings [67-69], prismatic

beams [70-74], tuning forks [75-77], and torsion [78, 79] oscillation.

3.1 Prismatic Beam Vibratory Gyroscopes

A basic MEMS gyroscope can be described by a vibrating rectangular cantilever

beam with identical drive and sense vibratory modes [71, 99] as shown in Figure 3.1.

Drive modepiezoelectric transducer

Sense modepiezoelectric transducer

ΩzRotation Rate

Sense mode(Coriolisresponse)vibration

Drive mode vibration

Cantilever beamsubstrate anchor

Drive modepiezoelectric transducer

Sense modepiezoelectric transducer

ΩzRotation Rate

Sense mode(Coriolisresponse)vibration

Drive mode vibration

Cantilever beamsubstrate anchor

Figure 3.1 Rectangular beam vibrating rate gyroscope.

Page 53: G_O'Brien PhD Dissertation

36

The beam dimensions for the drive and sense modes are closely matched to define a

system almost identical to the Foucault pendulum normal mode model. As a result, the

analysis and description of this system is straight forward using an input signal to drive a

fixed amplitude while measuring the secondary mode.

A variation of the rectangular beam gyroscope has been demonstrated using

triangular vibrating beams [74]. Excitation voltage is used to drive the beam into

resonance via a piezoelectric electrode located on one of the three triangular beam faces.

Energy radiated in the form of mechanical displacement to two non-normal modes is

sensed by the remaining two piezoelectric electrodes as a differential voltage signal with

unequal displacement amplitudes representing a non-zero angular rate input, as shown in

Figure 3.2.

Isometric view of beam

Top view in a zero rotation rate field

Drive C

Sense A Sense B ΩzSense A Sense B

Rotation rate(t)=B(t)-A(t)

Top view in a non-zero rotation rate field

Energy transfer from drive to sense modes of triangular beam used to measure angular rate input signal

Piezoelectric electrodes

DisplacementDrive CDisplacement

B(t)-A(t)=0

Isometric view of beam

Top view in a zero rotation rate field

Drive C

Sense A Sense B ΩzSense A Sense B

Rotation rate(t)=B(t)-A(t)

Top view in a non-zero rotation rate field

Energy transfer from drive to sense modes of triangular beam used to measure angular rate input signal

Piezoelectric electrodes

DisplacementDrive CDisplacement

B(t)-A(t)=0

Figure 3.2 Murata Gyrostar triangular beam gyroscope.

Page 54: G_O'Brien PhD Dissertation

37

Characterization results of this device, commercially available from Murata,

produced a relatively large change in angular rate sensitivity versus ambient temperature

[100], primarily due to the pyroelectric behavior of piezoelectric materials.

Prismatic beam vibratory rate gyroscopes typically exhibit several additional

problems inherent to the design which significantly limit device performance [65]. These

problems include acoustic energy loss at the beam/substrate anchor interface [67] and the

inability to discriminate between linear axis acceleration, oscillating at or near the sense

mode frequency, and an actual rotation rate signal. Automotive applications typically

experience environmental vibrations in the form of spurious linear axis accelerations up

to 5kHz in frequency. Undesirable linear axis acceleration sensitivity can be reduced by

increasing the vibratory gyroscope’s resonant frequency well beyond the intended sensor

application environment noise frequency range [65].

3.2 Tuning Fork Vibratory Gyroscopes

A design technique to reduce linear acceleration sensitivity of prismatic vibratory

gyroscopes is described by integrating two vibrating prismatic beams driven with anti-

phase displacement amplitude to form a differential Coriolis based angular rate sensor. A

further enhancement is achieved by mounting the vibrating beams to a common base to

form a tuning fork. Tuning forks form a balanced oscillator where no net torque is

transferred to the common base, referred to as the stem, under a zero rotation rate input

[101]. A non-zero angular rate causes Coriolis force induced sinusoidal anti-phase

displacement of the sense tines orthogonal to the drive mode vibration. The angular rate

signal can be measured as a function of differential tine displacement [102], or as a

torsion vibration of the tuning fork stem [103], as shown in Figure 3.3.

Page 55: G_O'Brien PhD Dissertation

38

Ωz Ωz

DriveMode

Coriolis Force

DriveMode

Coriolis Force

Tuning Fork Stem Torque CW Tuning Fork Stem Torque CCW

xy

z

Ωz Ωz

DriveMode

Coriolis Force

DriveMode

Coriolis Force

Tuning Fork Stem Torque CW Tuning Fork Stem Torque CCW

xy

z

Figure 3.3 Tuning fork with y-axis drive and x-axis Coriolis coupling about z-axis.

The balanced tuning fork gyroscope is theoretically less sensitive to undesired linear

axis accelerations than the prismatic beam designs, at least to a first order analysis.

However, this design is more susceptible to angular accelerations directed about the input

axis. As a result, tuning fork gyroscope designs are typically operated at a resonant drive

frequency an order of magnitude higher than the application environmental noise to

reduce angular rate sensing errors [104].

When the drive and sense modes of a tuning fork are matched, the normal mode

model describes an increase in the angular rate sensitivity multiplied directly by the

quality factor (Q). However, variation due to wafer processing photolithography and etch

steps typically result in slightly mismatched mass centers with respect to the individual

tines. This mass center variation can manifest itself as a resonant frequency mismatch

between the individual tines [65, 94]. Since unmatched tines exhibit different resonant

frequencies they will require either mass addition/removal near the mass center [105,

106] or electromechanical compensation to ensure anti-phase displacement at a given

drive frequency near resonance. This mode mismatch problem may also be further

Page 56: G_O'Brien PhD Dissertation

39

exacerbated by dependence of resonant frequency upon ambient temperature, typically

ranging from –40C to 125C for automotive applications. As a result, many tuning fork

designs are not based upon matched drive and sense resonant vibration modes.

3.3 Linear Axis Accelerometer Vibratory Gyroscopes

A single linear axis accelerometer can be configured to operate as a vibratory

gyroscope similar in operation to the prismatic beam devices described in section 3.1.

The accelerometer is driven at, or near, resonance along a primary drive axis while an

orthogonal secondary sense mode is used to measure the Coriolis based angular rate

signal.

Single linear accelerometer vibratory gyroscopes have been previously described with

orthogonal drive and sense modes [76, 107] using polysilicon as the resonator structural

material. However, these sensors are unable to discriminate between angular rate and

linear acceleration input signals. Dual accelerometer vibratory gyroscope designs,

similar to the dual tine tuning fork, are able to reject linear acceleration inputs at the

sensor making them better suited for automotive applications.

A dual linear accelerometer vibratory gyroscope design was fabricated by Draper

Labs with nickel as the structural resonator material with metal electrodes formed on a

glass substrate used to drive and measure displacement capacitively [75]. A second

generation of the Draper Labs dual accelerometer tuning fork gyroscope was fabricated

using single crystal silicon as the structural resonator material [108] bonded to the

underlying glass substrate and subsequently released using ethylene diamine

pyrocatechol (EDP) based on the dissolved wafer process [109].

Page 57: G_O'Brien PhD Dissertation

40

Multiple electrostatic comb drives [62] were used to both excite and measure the

primary drive mode frequency of each individual proof mass displaced parallel to the

wafer substrate. Closed loop electrostatic feedback was used to maintain a constant drive

mode displacement amplitude (a0). An external rotation rate (Ω) applied normal to the

drive mode plane causes a Coriolis force based displacement (aCoriolis) of each proof mass

in opposite directions [104] as given by Eq. 3.1.

)sin(2 0 taaCoriolis ωΩ= (3.1)

The Coriolis force based displacement is measured via the parallel plate capacitance

as a function of separation between the proof mass and metal electrodes deposited on the

quartz substrate, as shown in Figure 3.4.

Quartz Substrate

Electrode 1 Electrode 2

ProofMass 1

ProofMass 1

Z0 Z0

Silicon Silicon

A

A

View A-A: Sensor Cross SectionNickel Sensor Isometric View

AnchorSuspensionSpring

ProofMass 1

ProofMass 2

CombDrive

0

00 Z

AC ε=

ZZACΔ−

=0

0εΩ

Ω=0

Drive

Quartz Substrate

Electrode 1 Electrode 2

ProofMass 1

ProofMass 1

Z0 Z0

Silicon Silicon

A

A

View A-A: Sensor Cross SectionNickel Sensor Isometric View

AnchorSuspensionSpring

ProofMass 1

ProofMass 2

CombDrive

0

00 Z

AC ε=

ZZACΔ−

=0

0εΩ

Ω=0

Drive

Figure 3.4 Dual accelerometer isometric view with capacitive sensor cross section.

First order rejection of linear acceleration is realized by configuring the dual proof

mass capacitance measurement as differential. This differential capacitance

configuration can also be signal conditioned to simultaneously measure both linear

Page 58: G_O'Brien PhD Dissertation

41

acceleration and angular rate signals which may be desirable in many inertial navigation

and automotive applications. A comparison of differential capacitance values

experienced by the dual accelerometer vibratory gyroscope for both angular rate and

linear acceleration inputs is shown in Figure 3.5.

Angular Rate Signal Response

Electrode 1 Electrode 2

Ω

Electrode 1 Electrode 2

Ω=0Z1 Z2a

Z0

Quartz Substrate Quartz Substrate

Linear Acceleration Signal Rejection

2121 CCZZ <⇒>

12 CCC −=Δ2121 CCZZ =⇒=

0=ΔCn

n ZAC 0ε

=CenterPosition

Mass 1 Mass 2 Mass 1 Mass 2

12 CCC −=Δ0≠ΔC

Z2Z1

Angular Rate Signal Response

Electrode 1 Electrode 2

ΩΩ

Electrode 1 Electrode 2

Ω=0Z1 Z2a

Z0

Quartz Substrate Quartz Substrate

Linear Acceleration Signal Rejection

2121 CCZZ <⇒>

12 CCC −=Δ2121 CCZZ =⇒=

0=ΔCn

n ZAC 0ε

=CenterPosition

Mass 1 Mass 2 Mass 1 Mass 2

12 CCC −=Δ0≠ΔC

Z2Z1

Figure 3.5 Dual accelerometer linear acceleration signal rejection.

Drive mode closed loop electrostatic feedback is typically required to compensate for

signal error due to geometric differences in either the proof mass magnitudes or

suspension spring constants. Mechanical spring coupling can also be used to better

match the dual proof mass displacements. Bosch has demonstrated a dual accelerometer

tuning fork vibratory gyroscope with a mechanical coupling spring between each mass

and its suspension springs [77]. This device was driven into oscillation using Lorentz

forces resulting from an electric current loop located within the magnetic field of a

permanent magnet suspended above the proof masses.

A silicon bulk micromachined gyroscope has been demonstrated by JPL using four

proof masses suspended above a glass wafer substrate by a single support post [110].

Page 59: G_O'Brien PhD Dissertation

42

The major components of this device include the silicon clover leaf shaped vibrating

structure, a quartz baseplate with metal electrodes used to excite and measure proof mass

displacement, and a metal post which is manually epoxy bonded to both the proof mass

and underlying glass substrate [111]. An improvement over this manually epoxy

assembled bulk micromachined gyroscope utilized a two sided anisotropic etch to release

the clover leaf set of four proof masses while simultaneously forming a single crystal

silicon support post [112].

3.4 Torsion Mode Vibratory Gyroscopes

Torsion mode vibratory gyroscopes operate similar to the normal mode model where

energy is transferred from a primary drive mode to a secondary sense mode as a function

of applied angular rate excitation. An early micromachined example was demonstrated

by Draper Labs using a gimbal structure [73]. The gyroscope was driven into torsion at a

frequency of 3 kHz with constant amplitude along a single axis as shown in Figure 3.6.

Ω

DrivenVibratoryAxis

Sense Vibratory AxisFixed Electrodes

Rotation Signal Input AxisGyro Element

Ω

DrivenVibratoryAxis

Sense Vibratory AxisFixed Electrodes

Rotation Signal Input AxisGyro Element

Figure 3.6 Prismatic beam torsion decoupled mode vibratory rate gyroscope.

Page 60: G_O'Brien PhD Dissertation

43

A two axis surface micromachined gyroscope has been demonstrated using a disc

resonator driven about the z-axis [78]. The disc resonator is suspended above two pairs

of electrodes by four beam springs anchored to the wafer substrate as shown in Figure

3.7.

A A

X-Axis Electrode

X-Axis Electrode

y

y

Y-Axis Electrodes

Ωx

Z-AxisResonantDrive

zSubstrateAnchors

Z-Axis Torsion Disc Resonator

DiscResonator

Top View of Torsion Disc Resonator View A-A

x

A A

X-Axis Electrode

X-Axis Electrode

y

y

Y-Axis Electrodes

Ωx

Z-AxisResonantDrive

zSubstrateAnchors

Z-Axis Torsion Disc Resonator

DiscResonator

Top View of Torsion Disc Resonator View A-A

x

Figure 3.7 Two-axis vibrating disc gyroscope.

Capacitive electrodes are used to measure the disc z-axis separation. The electrodes

are oriented in differential pairs along both the x and y axes. An input rotation rate signal

about the x-axis induces a Coriolis acceleration causing the disc to oscillate about the y-

axis as shown in Figure 3.8. Similarly, an input rotation rate signal about the y-axis

induces a Coriolis acceleration causing the disc to oscillate about the x-axis. Different

sense modulation frequencies were used for each of the two sense axes. However, small

micromachined wafer process variations [113] produced devices with well-matched sense

modes with low noise but degraded cross-axis rejection while poorly-matched modes

produced an increase in noise with improved cross-axis rejection. A proposed method to

avoid the trade-off nature of noise versus cross-axis sensitivity was to employ a closed

loop electrostatic feedback loop in future designs.

Page 61: G_O'Brien PhD Dissertation

44

z

x

y

Ωx

z

x

y

ΩxCoriolis Force Couple CW

Coriolis Force Couple CCW

Z-Axis Drive CW Vibration Phase

Z-Axis Drive CCW Vibration Phase

y

y

z

x

y

Ωxz

x

y

Ωx

z

x

y

ΩxCoriolis Force Couple CW

Coriolis Force Couple CCW

Z-Axis Drive CW Vibration Phase

Z-Axis Drive CCW Vibration Phase

y

y

Figure 3.8 Polysilicon vibrating disc gyroscope Coriolis induced tilt oscillation.

A mechanically decoupled mode torsion vibratory gyroscope has been demonstrated

with improved cross axis rejection. The mechanical sensor consists of an inner drive

wheel, anchored to the substrate with beam springs radiating from a central post,

connected to an outer proof mass by two torsion springs [79] as shown in Figure 3.9.

Substrate

Torsion Primary Drive Mode Torsion Secondary Sense Mode

Dielectric

Sense Electrodes

AnchorPost

Comb Drives

BeamSprings

Coriolis Force Couple for CCW Drive Phase

Gap

Ωxx

yx

z

Torsion Beam

ProofMass

Substrate

Torsion Primary Drive Mode Torsion Secondary Sense Mode

Dielectric

Sense Electrodes

AnchorPost

Comb Drives

BeamSprings

Coriolis Force Couple for CCW Drive Phase

Gap

Ωxx

yx

z

Torsion Beam Substrate

Torsion Primary Drive Mode Torsion Secondary Sense Mode

Dielectric

Sense Electrodes

AnchorPost

Comb Drives

BeamSprings

Coriolis Force Couple for CCW Drive Phase

Gap

Ωxx

yx

yx

zx

z

Torsion Beam

ProofMass

Figure 3.9 Top and side view of decoupled torsion mode vibratory gyroscope.

Page 62: G_O'Brien PhD Dissertation

45

Electrostatic comb drives [62] are used to excite the torsion drive mode about the z-

axis inner disc. Coriolis forces produce a torque in the torsion beam suspended outer

proof mass. The torque displacement is sensed capacitively as a function of separation

between the surface micromachined thick polysilicon proof mass [114] and fixed

substrate electrodes.

3.5 Vibrating Shell Gyroscopes

Tuning fork vibratory gyroscopes utilize the transfer of energy between two normal

modes of operation. These normal modes, although frequency matched, are typically not

identical such as tuning fork tine bending versus stem torsion. Dual accelerometer

designs also exhibit different mode properties in the primary and secondary modes

independent of the matched resonant frequency values. The primary and secondary mode

resonant frequencies may be matched at room temperature while large excursions from

these values may occur, which typically do not track with each other, as temperature is

swept over a –40C to 90C temperature range. In contrast, vibrating shell gyroscopes

transfer energy between two identical primary and secondary vibration modes avoiding

temperature stability problems experienced by tuning fork designs.

Vibrating shell gyroscopes typically have a bell-like structure and may be shaped

either like a wine glass [96, 115], cylinder [116], or ring [68]. The Delco wine glass

shaped hemispherical resonator gyroscope (HRG) was fabricated in fused quartz

suspended by a fixed stem with the vibrating shell rim encapsulated by concentric drive

and sense electrodes as shown in Figure 3.10.

Page 63: G_O'Brien PhD Dissertation

46

Drive Electrodes

Sense Electrodes

Node

Anti-nodeRim

SupportStem

HemisphericalResonator

HemisphericalResonator Rim

FixedOuter HermeticEnclosure

Side View of HRG Resonator Top View of HRG Rim and Fixed Electrodes

Drive Electrodes

Sense Electrodes

Node

Anti-nodeRim

SupportStem

HemisphericalResonator

HemisphericalResonator Rim

FixedOuter HermeticEnclosure

Side View of HRG Resonator Top View of HRG Rim and Fixed Electrodes

Figure 3.10 Wine glass shaped quartz hemispherical resonator gyroscope.

The metal plated HRG shell is excited electrostatically at the resonator natural

frequency by a sinusoidal signal applied to the outer case fixed electrodes. A closed loop

servo is used to maintain the resonator rim amplitude during operation. The cavity

pressure is maintained at near vacuum to avoid both damping and mechanical coupling

between the resonator with respect to the inner and outer case surfaces. The reported

quality factor (Q) for the HRG was greater than 6x106, with time constants on the order

of 17 minutes in duration. As a result, it is possible to excite the HRG with intermittent

drive signals applied to the shell with 10-15 minute intervals between bursts.

The nodes of a wine glass resonator do not remain stationary in space as compared to

the Foucault pendulum. Instead, the nodal pattern of a vibrating shell will rotate in the

direction of fixed case rotation with a displacement angle coupling of 0.3 times the case

rotation angle [117], as shown in Figure 3.11. As a result, precession of the nodal pattern

relative to the fixed case electrodes can be used to measure the externally applied angular

rate signal.

Page 64: G_O'Brien PhD Dissertation

47

Static Operation of HRG Node Precession of CW Rotated HRG Body

Case Index Point Case RotationVibration

Pattern NodalRotation θ

θ3.0

Static Operation of HRG Node Precession of CW Rotated HRG Body

Case Index Point Case RotationVibration

Pattern NodalRotation θ

θ3.0

Figure 3.11 Node precession of the HRG with externally applied angular rate signal.

Researchers at General Motors and the University of Michigan have developed a

nickel vibrating ring gyroscope suspended by semicircular beam springs anchored to the

silicon substrate wafer at a common central point [68]. Symmetry considerations require

that at least eight replicated springs are included to balance the device with two identical

drive and sense flexural modes that exhibit near equal natural frequencies [89].

Electrodes were located along the outer perimeter of the resonating ring to provide drive,

sense, and mode tuning capability of the natural frequencies. The ring is electrostatically

excited into an elliptical shaped drive mode vibration pattern with a fixed amplitude.

When subjected to an external rotation rate about its normal axis, Coriolis acceleration

causes energy to be transferred from the primary drive to secondary sense mode as shown

in Figure 3.12. The capacitively monitored sense mode amplitude is proportional to the

applied external angular rate signal. This normal mode gyroscope sensitivity is

proportional to the resonating ring quality factor with values reported greater than 2000.

A polysilicon version of the ring gyroscope demonstrated significant increases in quality

factor and angular rate sensitivity [69].

Page 65: G_O'Brien PhD Dissertation

48

Drive Mode Sense Mode

Support Springs Outer Fixed Electrodes Resonator Ring

Drive Mode Sense Mode

Support Springs Outer Fixed Electrodes Resonator Ring

Figure 3.12 Micromachined vibrating ring gyrsocope drive and sense modes.

A wide range of stiffness asymmetries in the structure, arising from fabrication based

geometric imperfections, can be balanced using electronic tuning of the remaining non-

drive mode fixed electrodes.

British Aerospace Systems, in collaboration with Sumitomo Precision Products, have

also developed a vibratory silicon ring gyroscope [118]. This device differs from

previously demonstrated vibratory ring gyroscopes [68, 69] by use of Lorentz force drive

mode electric current loops located on each of the eight suspension springs. Pairs of two

suspension springs are used to form two sets of four complete current loops. A

samarium-cobalt permanent magnet was mounted inside the package to provide a

constant magnetic field. Electromagnetic interaction between the current loops and

permanent magnetic field induce the Lorentz force used to excite the vibratory drive

mode. The voltage induced around the current loops as they are displaced with respect to

the permanent magnetic field, in accordance with Faraday’s law, was used to sense

Coriolis acceleration. Any two suspension spring current loops which are on opposite

sides of the vibrating ring constitute a differential voltage which can be used to measure

Page 66: G_O'Brien PhD Dissertation

49

normal mode primary to secondary energy transfer due to externally applied angular rate

signal. Closed loop feedback was used to simultaneously increase bandwidth and

decrease sensitivity to cross axis linear and angular acceleration. Supply voltage and

current were 12V and 100mA respectively making this device acceptable for automotive

applications. However, supply current and power consumption was 5-10x larger than

typical automotive vibratory gyroscopes [68, 102]. In addition, the sense ring measured

6mm in diameter with a square sensor die size of 1cm per side. Large power

consumption and sensor die size may preclude this sensor from use in both automotive

and battery powered consumer applications.

3.6 Automotive Gyroscope Classification and Performance

In general, gyroscopes can be classified into three different categories based on their

performance [85] as summarized in Table 3.1. The rate grade is typically addressed

using Coriolis based vibratory gyroscopes while tactical and inertial grade devices are

almost exclusively fiber optic and ring laser Sagnac based devices respectively.

Table 3.1 Multiple classes of gyroscope performance.

Parameter Rate Grade Tactical Grade Inertial Grade

Random Angle Walk [deg/√h] > 0.5 0.5-0.05 < 0.001

Bias Drift [deg/h] 10-1000 0.1-10 <0.01

Scale Factor Accuracy 0.1-1 0.01-0.1 <0.001

Full Scale Range [deg/s] 50-1000 >500 >400

Max Shock, 1ms Half-sine [g] 103 103-104 103

Bandwidth [Hz] >20 ~100 ~100

Page 67: G_O'Brien PhD Dissertation

50

Currently, the automotive market utilizes only rate grade Coriolis based vibratory

gyroscopes. Although the Coriolis based HRG has been demonstrated with inertial grade

performance [96, 115], its large size and high cost preclude it from use in automotive

applications.

All normal mode vibratory gyroscopes exhibit some form of zero rate output (ZRO)

in the absence of a rotation input signal due to geometric imperfections [113] and

misalignment [104]. This misalignment of the drive and/or sense mode coupling will

produce a vibrating torque in phase quadrature with the rotation rate induced Coriolis

acceleration signal. This error, often referred to as quadrature error, can be larger than

the Coriolis signal and may saturate the sensor interface electronic amplifier [76].

Random angle walk describes the combination of noise rate output which causes a

long term growth in angle error referred to as random angle walk [119]. If the rate noise

has a white spectrum with a non-zero root mean square value (σ) it gives rise to random

walk (Rθ) in the measured angle which propagates as the square root of sample time as

given by Eq. 3.2.

tR σθ = (3.2)

Scale factor is defined as the amount of change in the output signal per unit change of

rotation rate [120] typically expressed in units of V/(deg/s). Output resolution of the

angular rate input signal is defined as the ratio of sensor noise voltage divided by the

scale factor typically expressed in units of deg/s. Angular rate sensor resolution of

commercially available rate grade gyroscopes is summarized in Table 3.2

Page 68: G_O'Brien PhD Dissertation

51

Table 3.2 Commercial automotive gyroscope performance comparison.

Gyroscope

Type

Resonator

Material

Drive

Method

Sense

Method

Resolution

[deg/s]

Bandwidth

[Hz]

Ref:

Tri-Beam Quartz Piezoelectric Piezoelectric 14 50 [74]

Tuning Fork Quartz Piezoelectric Piezoelectric 0.25 50 [102]

Dual Accel. Silicon Capacitive Capacitive 0.13 60 [108]

Dual Accel. Silicon Electromag. Capacitive 0.3 100 [77]

Dual Accel. Silicon Capacitive Capacitive 0.6 40 [121]

Torsion Silicon Capacitive Capacitive 4 1 [73]

Ring Nickel Capacitive Capacitive 0.5 25 [89]

Ring Silicon Electromag. Electromag. 0.15 30 [118]

Typically, rate grade gyroscopes used for automotive dynamic vehicle control [6]

exhibit a minimum resolution of 0.5 deg/s, bandwidth greater than 20 Hz, and a full scale

span on the order of +/- 100 deg/s .

3.7 Vibratory Gyroscope Performance Summary

Prismatic beams excited and sensed using piezoelectric electrodes are among the

most straight forward vibratory angular rate sensors. However, these devices suffer from

poor temperature performance. In addition, prismatic beam vibratory gyroscopes cannot

discriminate between a constant angular rate or linear acceleration signal synchronous

with the primary mode excitation frequency. Due to the inherently noisy environment of

automotive applications, typically exhibiting a frequency spectrum up to 5 kHz, prismatic

beam vibratory gyroscopes are not implemented due to their poor performance regarding

elevated temperature and low rejection of linear cross axis acceleration.

Page 69: G_O'Brien PhD Dissertation

52

Piezoelectric tuning forks provide high rejection of linear cross axis acceleration but

suffer from elevated temperature output signal degradation. Dual accelerometer tuning

forks, using capacitive drive and sense electrodes, can provide both temperature stability

and increased rejection of undesirable linear cross axis accelerations. However, an

additional problem associated with dual accelerometer vibratory gyroscopes is that slight

phase mismatching due to normal process variation [113] of the individual mass/spring

accelerometers results in an angular rate output signal error in phase quadrature with the

resonant drive mode input signal [122]. This quadrature error signal effects all normal

mode gyroscopes where the primary drive and secondary sense modes are slightly

mismatched [104].

Vibrating shell gyroscopes exhibit less quadrature error than other designs due to the

theoretically identical drive and sense mode resonant frequencies. In practice, vibrating

shell gyroscope performance tracks well over temperature due to the closely matched

drive and sense modes [120]. However, mode tuning is often required to provide desired

angular rate sensitivity due to small mode frequency mismatch attributed to wafer process

variation. Several vibrating shell mode tuning techniques have been demonstrated

including electrostatic [89], mass addition, and laser ablation mass removal [106].

Decoupled mode torsion vibratory gyroscopes significantly reduce quadrature error

[73], but a previously demonstrated design which utilized a single centrally located

anchor post [79] exhibits low rejection of cross axis linear and angular accelerations. A

decoupled mode vibratory gyroscope design presented in Chapter 4 describes a

significantly improved cross axis acceleration rejection device.

Page 70: G_O'Brien PhD Dissertation

53

CHAPTER 4

SURFACE MICROMACHINED DUAL ANCHOR GYRSOSCOPE

MEMS based vibratory gyroscopes typically provide poor cross axis rejection to both

linear and angular accelerations. In addition, actuation voltage amplitudes in excess of

20V are typically required to drive the primary mode displacement at or near resonance.

Automotive application supply voltage is limited to 12VDC with 3-5VDC being the desired

sensor operation range. While electronic circuit techniques exist to increase the supply

voltage via charge pumps [123], they consume significant die space and are difficult to

operate reliably with low power consumption regarding electronic noise injected at

typical resonant primary mode drive frequencies. Also, mechanical shock in excess of

2000g must not damage or degrade sensor operation. This chapter describes a low cost

surface micromachined vibratory gyroscope design which addresses improved cross axis

rejection, low voltage primary mode actuation, and 2000g multi-axis mechanical shock

survivability for intended use in an automotive environment.

4.1 Dual Anchor Gyroscope Basic Design and Performance Goals

A single resonant accelerometer used as an angular rate sensor is unable to

discriminate between linear and Coriolis based acceleration [76, 107]. Discrimination of

linear and Coriolis acceleration is possible using a dual resonant accelerometer approach

[75, 108]. However, the dual accelerometer approach typically requires frequency/phase

matching of each anti-phase excited proof mass to reduce quadrature error [120], due

primarily to process variations in the etched proof mass and suspension springs [113],

and significantly increases the control circuitry complexity, power consumption, and die

area.

Page 71: G_O'Brien PhD Dissertation

54

A centrally anchored mechanically decoupled drive and sense proof mass scheme has

been described previously [73, 79] that matches the dual sense mass frequency and phase

using an outer rotating structural frame to reduce quadrature error. However, the central

anchor is mechanically compliant with respect to rotations directed about the x and y

axes. As a result, the single central support anchor provides poor cross axis rejection

regarding angular acceleration.

The main angular rate sensor design goal was to minimize the out of plane deflection

of the primary mode central disc to increase cross axis rejection without simultaneously

degrading the secondary mode Coriolis acceleration sensitivity. This chapter describes

the operation of the dual anchor angular rate sensor and the basic design enhancements to

increase device performance and process yield characteristics.

4.2 Angular Rate Sensor Operation

Vibratory gyroscopes sense angular rate based on the Coriolis acceleration

measurement defined by the cross product of the mass velocity v, and the applied angular

rate Ω, as given by Eq. 4.1.

Ω×= vaC 2 (4.1)

Coriolis force is defined by the product of the effective sense ring proof mass m and

Coriolis acceleration as given by Eq. 4.2.

Ω×= vmFC 2 (4.2)

The angular rate sensor is comprised of a centrally anchored drive disc and a

mechanically decoupled outer proof mass sense ring using a torsion spring. The drive

Page 72: G_O'Brien PhD Dissertation

55

disc is electrostatically actuated about the z-axis with an angular rate applied parallel to

the x-y plane. The resulting Coriolis force couple causes a torsion (deflection out of

plane) of the outer sense ring for a counter clockwise rotation as shown in Figure 4.1.

v

v

v

Ω

+FC

-FC

FC=0

FC=0

Ω

Top View Side View

x

y

x

z

FC=0

v

rmax

Drive

Sense

v

v

v

Ω

+FC

-FC

FC=0

FC=0

Ω

Top View Side View

x

y

x

z

FC=0

v

rmax

Drive

Sense

Figure 4.1 Angular rate sensor Coriolis force diagram.

The outer sense ring velocity is a sinusoidally varying function of the applied driving

displacement versus time, as given by Eq. 4.3, where θmax represents the maximum proof

mass angular displacement, ω is the drive voltage frequency, and t is time.

)sin()( max tt ϖθθ = (4.3)

The angular displacement is converted to a linear displacement, as given by Eq. 4.4,

where rmax represents the distance measured from the proof mass center point to the mid

point on the outer sense proof mass ring.

maxmaxmax ry θ= (4.4)

Page 73: G_O'Brien PhD Dissertation

56

The angular displacement is converted to linear displacement along the y-axis, as

given by Eq. 4.5, where the ymax represents the maximum displacement.

)sin()( max tyty ϖ= (4.5)

The velocity of the outer ring is defined by the time derivative of the position vector

given by Eq. 4.6.

)cos()(max ty

dttdy ϖϖ= (4.6)

The Coriolis force can be approximated using the y-axis component of the sense ring

multiplied by one half the total sense ring mass and the cross product of the applied

angular rate vector as given by Eq. 4.7.

Ω×≅dt

tdymFCoriolis)(

(4.7)

The Coriolis force causes a displacement of the outer ring which is capacitively

sensed using two underlying polysilicon electrodes labeled a and c as shown in Figure

4.2.

The drive ring capacitance of a single parallel plate beam is defined by the

displacement angle θ, as given by Eq. 4.8, where Z0 represents the initial dielectric gap,

and T represents the structural polysilicon film thickness .

⎟⎟⎠

⎞⎜⎜⎝

⎛−−

=θθ

θεθ

out

in

rZrZTC

0

00 ln)( (4.8)

Page 74: G_O'Brien PhD Dissertation

57

Poly2Poly1

bc

a

b

aCccw

c

CcwA

A

View A-A

Substrate

θ

Nitride

CapacitiveElectrodes

Displacement Angle

rinrout

Poly2Poly1

bc

a

b

aCccw

c

CcwA

A

View A-A

Substrate

θ

Nitride

CapacitiveElectrodes

Displacement Angle

Poly2Poly1

bc

a

b

aCccw

c

CcwA

A

View A-A

Substrate

θ

Nitride

CapacitiveElectrodes

Displacement Angle

rinrout

Figure 4.2 Basic angular rate sensor cross section.

The maximum static angular displacement possible prior to electrostatic latching

[124] of the sense ring is given by Eq. 4.9, as derived in Appendix A.

outrZ0

max45.0

=θ (4.9)

4.3 Basic Angular Rate Sensor Configuration

The basic surface micromachined angular rate sensor was fabricated using a 2μm

thick structural polyslicon film as shown in Figure 4.3. The structure is suspended above

the substrate using polysilicon beam springs centrally anchored to the underlying

electrode as shown in Figure 4.4.

Page 75: G_O'Brien PhD Dissertation

58

DriveDisc

SenseRingDrive

Disc

SenseRing

Figure 4.3 Basic polysilicon angular rate sensor configuration.

DriveDisc

Anchors

SupportSprings

DriveDisc

Anchors

SupportSprings

Figure 4.4 Centrally anchored polysilicon beam springs.

The simple torsion spring coupling the drive disc and sense ring is shown in Figure

4.5. The torsional drive and sense modes were intentionally mismatched by as much as

10% to reduce resonant frequency variation over temperature at the cost of reduced

overall angular rate sensitivity.

Page 76: G_O'Brien PhD Dissertation

59

SimpleTorsionBeamSpring

Sense Ring

Drive Disc

SimpleTorsionBeamSpring

Sense Ring

Drive Disc

Figure 4.5 Simple torsion beam spring outer mass coupling suspension.

Parallel plate electrostatic arrays were used to actuate the drive disc at the resonant

frequency of the outer sense ring/torsion spring system. The initial parallel plate actuator

design was anchored near the beam center at the underlying electrical polysilicon

interconnection resulting in an 8X overall increase in the vertical spring constant as

compared to cantilever beams of equal length. However, vertical stiction [125] was

observed in arrays with beam lengths greater than 160μm during the sacrificial oxide etch

process sequence. Centrally anchored beams shorter than 160μm were observed to resist

vertical stiction during processing and comprise the drive disc’s outer electrostatic

actuator array. Parallel plate actuator beams longer than 160μm in length were modified

with a tip anchor, as described in the following section, resulting in an increased vertical

spring constant larger than the stiction threshold limit.

4.4 Angular Rate Sensor Design Enhancements

Multiple design enhancements were made to the basic angular rate sensor resulting in

either increased post process device yield or desired parameter improvement. The

significant design enhancements are described individually in the following sections.

Page 77: G_O'Brien PhD Dissertation

60

4.4.1 Anti-Stiction Beam Tip Anchors

The parallel plate electrostatic actuator arrays are comprised of beams in which the

anchor also provides electrical interconnection. Electrostatic arrays have traditionally

been fabricated as singly clamped cantilever beams [2, 75, 76, 79, 121], with the vertical

spring constant given by Eq. 4.10, where E is the Young’s modulus and the beam’s

length, width, and thickness are described by L, W, and T respectively.

3

3

_ 4LEWTK beamZ = (4.10)

Initial design improvement was accomplished by anchoring the beams near the center

as shown for the outer parallel plate array in Figure 4.6.

Parallel PlateArrays

InnerArray

OuterArray Parallel Plate

Arrays Parallel PlateArrays

InnerArray

OuterArray

Figure 4.6 Enhanced anchor parallel plate electrostatic sense-actuation arrays.

The effective beam length is halved which increases the z-axis spring constant by 8X,

using Eq. 4.10, in an attempt to prevent vertical stiction [125]. However, vertical stiction

was observed for beam lengths in excess of 160μm on earlier centrally anchored designs,

as shown in Figure 4.7, for devices released in HF acid/H20-IPA rinse/air dry.

Page 78: G_O'Brien PhD Dissertation

61

StictionReleased

StictionReleased

Figure 4.7 Centrally anchored electrostatic array vertical stiction.

Tip anchors were added to electrostatic beam arrays in excess of 160μm of length,

converting from a singly to doubly clamped beam as shown in Figures 4.8 and 4.9.

Standard Drive Disc

Split Drive Disc

Standard and Split Drive Disc Tilted View

Reference following figure for beam electrode cross section

Standard Drive Disc

Split Drive Disc

Standard and Split Drive Disc Tilted View

Reference following figure for beam electrode cross section

Figure 4.8 Standard and split central drive disc designs.

Page 79: G_O'Brien PhD Dissertation

62

Electrical Interconnection

TipAnchor

Drive Disc

Electrical Interconnection

TipAnchor

Electrical Interconnection

TipAnchor

Drive Disc

Figure 4.9 Electrostatic beam array cross section with tip anchors.

The split drive disc design is shown only to clearly illustrate a typical electrostatic

array cross section. The tip anchor doubly clamped beam configuration, used on both the

standard and split drive disc designs, cause an increase in the vertical spring constant of

128X, as compared to a singly clamped cantilever beam of the same length, width, and

thickness dimensions. The tip anchors are electrically isolated from the adjacent

polysilicon electrode using an island as shown in Figure 4.10.

Polysilicon Isolation IslandFixed Electrode Tip Anchor

Polysilicon Isolation IslandFixed Electrode Tip Anchor

Figure 4.10 Tip anchor electrical isolation on nitride passivated substrate.

The parallel plate fixed beam electrode is electrically interconnected and

mechanically anchored to the underlying polysilicon runner as shown in Figure 4.11.

Page 80: G_O'Brien PhD Dissertation

63

CCW ArrayPolysiliconInterconnection

Drive Disc

Fixed Beam

CCW ArrayPolysiliconInterconnection

Drive Disc

Fixed Beam

Figure 4.11 Fixed electrode parallel plate array substrate electrical interconnect.

Vertical stiction [125] was completely eliminated from the fixed parallel plate

actuator arrays using the dual tip post anchor implementation [83] processed with

standard wet hydrofluoric (HF) acid sacrificial oxide release with a subsequent de-

ionized (DI) water and isopropyl alcohol (IPA) rinse prior to drying in a warm nitrogen

ambient.

4.4.2 Dual Anchor Attach

Typically, angular rate sensors incorporate a single type of replicated suspension

spring with a central support scheme [68, 69, 73, 79]. Precession of the excited vibration

pattern occurs when the Coriolis acceleration causes energy to be transferred between

identical normal mode. However, precession is undesirable regarding a mechanically

decoupled drive and sense mode gyroscope [79]. Our goal was to reduce the drive disc

out of X-Y plane displacement during sinusoidal excitation about the Z-Axis without

significantly increasing the rotational spring constant. A dual anchor scheme using a

support post and folded beams [83] was incorporated to reduce undesirable drive mode

precession as shown in Figure 4.12.

Page 81: G_O'Brien PhD Dissertation

64

SupportPost

Proof Mass

Folded BeamSprings

SupportPost

Proof Mass Disc

Folded BeamSprings

R1SupportPost

Proof Mass

Folded BeamSprings

SupportPost

Proof Mass Disc

Folded BeamSprings

R1

Figure 4.12 Dual anchor angular rate sensor suspension.

The parallel combination of the folded beam springs and central support post result in

the total drive disc rotational spring constant as shown in Figure 4.13.

R0

R1

R2

xz

R0

R1

R2r

R1

R2Kx_post

Kx_beam

Kx_total

PostPost hr

Substrate Anchor

Proof Mass Disc Top View Proof Mass Disc Side View

Proof Mass DiscR0

R1

R2

xz

xz

R0

R1

R2r

R1

R2Kx_post

Kx_beam

Kx_total

PostPost hr

Substrate Anchor

Proof Mass Disc Top View Proof Mass Disc Side View

Proof Mass Disc

Figure 4.13 Folded beam and torsion post equivalent spring constant model.

The folded beam springs are segmented into equal sections and solved for the

equivalent spring constant Keq as shown in Figure 4.14. The lateral spring constant of the

Page 82: G_O'Brien PhD Dissertation

65

folded beam array, as given by Eq. 4.11, where E is the Young’s modulus of polysilicon,

folded beam spring width W, thickness T, and section length L.

3

3

22

21

_ 43

LTEW

RRK beamx = (4.11)

The central support post torsion spring constant [126] with a radius of r is given by

Eq. 4.12.

4

21 rK πθ = (4.12)

))()((2()( 3||2||1 kkkkeq =⎟⎟⎠

⎞⎜⎜⎝

⎛+

+

⎟⎟⎠

⎞⎜⎜⎝

⎛+

=

32

321

32

321

_

2

2

kkkkk

kkkkk

k outeq

Let k = k1 and k1 ≅ k2 ≅ k3;2_kk outeq =

m

k1

k2 k3k3 k2

keq

m

Folded Beam Spring

))()((2()( 3||2||1 kkkkeq =⎟⎟⎠

⎞⎜⎜⎝

⎛+

+

⎟⎟⎠

⎞⎜⎜⎝

⎛+

=

32

321

32

321

_

2

2

kkkkk

kkkkk

k outeq

Let k = k1 and k1 ≅ k2 ≅ k3;2_kk outeq =

m

k1

k2 k3k3 k2

keq

m

Folded Beam Spring

))()((2()( 3||2||1 kkkkeq =⎟⎟⎠

⎞⎜⎜⎝

⎛+

+

⎟⎟⎠

⎞⎜⎜⎝

⎛+

=

32

321

32

321

_

2

2

kkkkk

kkkkk

k outeq

Let k = k1 and k1 ≅ k2 ≅ k3;2_kk outeq =

m

k1

k2 k3k3 k2

keq

m

keq

m

Folded Beam Spring

Figure 4.14 Folded beam equivalent spring constant model.

Page 83: G_O'Brien PhD Dissertation

66

The units of Eq. 4.11 and 4.12 are not identical. As a result, linearization of the

torsion spring constant is required in order to combine effects with the beam spring

constant to describe the total system suspension. Multiple equations are necessary to

support the linear transformation of the torsion spring constant. Torsion deflection angle

θ is described by an applied torque Γ, where h is the post height, and G is the shear

modulus as given by Eq. 4.13.

GKh

θ

θ Γ= (4.13)

The shear modulus is described by the Young’s modulus and Poisson ratio, as given

by Eq. 4.14, where E = 160GPa and ν = 0.27 respectively for polysilicon.

( )ν+=

12EG (4.14)

The applied torque Γ can be represented by a force F2 applied tangentially at the outer

disc radius R2 as given by Eq. 4.15.

22RF=Γ (4.15)

Combining Eq. 4.13 into Eq. 4.15 and solving for the force F2 is described by Eq.

4.16.

hRGKF

22

θθ= (4.16)

Page 84: G_O'Brien PhD Dissertation

67

The linear spring constant Kx will experience a displacement Δx due to an applied

force F1 as given by Eq. 4.17.

22 xKF x Δ= (4.17)

The relationship used to relate angular displacement θ to linear displacement Δx is

given by Eq. 4.18.

θ22 Rx =Δ (4.18)

The linearized spring constant Kx which describes the torsion post deflection is

defined by substituting Eq. 4.18 into Eq. 4.17 and equating the result with Eq. 4.16 as

given by Eq. 4.19.

22

_ hRGKK postx

θ= (4.19)

Finally, the torsion post linearized spring constant is described by substituting Eq.

4.12 into Eq. 4.19 as given by Eq. 4.20.

22

4

_ 2hRGrK postx

π= (4.20)

The linearized system spring constant is defined by the sum of Eq. 4.11 and Eq. 4.20

as given by Eq. 4.21.

Page 85: G_O'Brien PhD Dissertation

68

22

4

3

3

22

21

_ 243

hRGr

LTEW

RR

K totalxπ

+= (4.21)

The vertical z-axis folded beam spring constant is given by Eq. 4.22.

3

3

_ 43

LEWTK beamz = (4.22)

The vertical z-axis spring constant of the supported drive disc is dominated by the

central support post treated as a column in compression as given by Eq. 4.23.

hrEK postz

2

= (4.23)

The total z-axis spring constant is represented by summing Eq. 4.22 and 4.23 as given

by Eq. 4.24.

hrE

LEWTK totalz

2

3

3

_ 43 π

+= (4.24)

The vertical spring constant of the drive disc suspension is increased from 11.25 N/m

using only the folded beam springs to over 240 kN/m with the torsion post loaded into

compression; greater than 4 orders of magnitude improvement in the z-axis spring

constant was achieved using this technique. Post fabrication process vertical stiction was

not observed on angular rate sensor designs using the dual folded beam and support post

anchoring scheme.

Page 86: G_O'Brien PhD Dissertation

69

4.4.3 Z-Axis Overtravel Stop

Automotive accelerometers and angular rate sensors are typically required to survive

X-Y-Z-Axes shock loads in excess of 2000g. Typically, device sensitivity is proportional

to the proof mass magnitude and inversely proportional to the system spring constant. In

contrast, the maximum shock load is inversely proportional to the device sensitivity. The

maximum device shock load has also previously been observed to significantly decrease

as a function of decreased pressure [8] from ambient to 50mtorr. This performance

tradeoff is an added requirement for the system designer to consider where a hermetic

low pressure ambient is desired to promote high Q resonant sensor operation [127, 128].

An over-travel limit structure has previously been described [129, 130] which

effectively de-convolves the maximum shock load and device sensitivity design

parameters. This work is provided as an improvement on the original over-travel

mechanical stop design using conformal oxide and polysilicon deposition, as shown in

Figure 4.15.

Z-AxisOver-travel Stop

DriveDisc Z-Axis

Over-travel Stop

DriveDisc

Figure 4.15 Z-axis mechanical over-travel stop.

Page 87: G_O'Brien PhD Dissertation

70

The process flow contains two structural polysilicon films each 2μm thick. The

structural polysilicon films are separated by 2μm (Zbot) and 0.75μm (Ztop) thick films of

phosphosilicate glass (PSG) provided as a sacrificial oxide material. The over-travel

mechanical stop is anchored to the underlying 0.5μm thick electrical interconnection

polysilicon film via both structural polysilicon layers. The drive disc is comprised of the

Poly2 film only, while the Z-Axis over-travel mechanical stop is comprised of both Poly2

and Poly3 films. The sacrificial oxide deposition thickness determines the drive disc Z-

Axis maximum travel displacement. The over-travel stop is electrically interconnected to

the drive disc node to preclude undesirable non-zero differential voltage before and after

mechanical contact. Profile of the mechanical over-travel stop is shown in Figure 4.16.

Over-travel Stop

DriveDisc

Poly3

Poly2Poly2

Over-travel Stop

DriveDisc

Poly3

Poly2Poly2

Figure 4.16 Mechanical over-travel stop tilted view.

Sub-micron lateral and vertical gaps can be formed between the two structural

polysilicon films, as shown in Figure 4.17. This process technique can also be used to

form lateral sub-micron electrostatic actuators without the need for either sub-micron

photolithography or post process polysilicon deposition [131].

Page 88: G_O'Brien PhD Dissertation

71

DriveDisc

Over-travel Stop0.75μm

DriveDisc

Over-travel Stop0.75μm

Figure 4.17 Sub-micron mechanical over-travel stop gap.

Functional sensors were exposed to 2000g half-sine shock 4ms in duration directed

along the x, y, and z-linear axes. Capacitance measurements were performed before and

after shock loading with no observed shift in capacitance for the 5 angular rate sensors

tested. SEM inspection was performed post shock load at several over-travel stop sites

with no apparent degradation or silicon particles observed. Similarly, failure

mechanisms in polysilicon MEMS components operated in direct mechanical contact do

not exhibit particulate generating mechanisms [132] for values significantly less then the

yield strength 7GPa [133], although lower fracture values been reported as a strong

function of silicon etchant used (KOH, EDP, TMAH, and XeF2) in the range from 0.6-

1.2GPa [134]. Brittle materials such as silicon exhibit ultimate stresses that are

essentially the same as their yield strength. Ductile materials such as most metals exhibit

an ultimate stress much greater than their yield stress. As a result, ductile materials

undergo plastic deformation prior to fracture. While fatigue is a potential problem with

ductile materials, brittle silicon does not typically suffer from this mechanical

degradation mechanism in a moisture free ambient. However, deliberate stress

concentration on resonators and actuators in the presence of water vapor during

Page 89: G_O'Brien PhD Dissertation

72

mechanical cycling has been shown to accelerate crack growth and material failure [135-

138]. The angular rate sensor operation and storage ambient was in dry nitrogen which

effectively eliminated moisture contamination of polysilicon surfaces.

The peak mechanical stress of the over-travel stop can be modeled by applying a

2000g acceleration to the inertial proof mass magnitude and transfer the resulting force to

the stop beam tip. The over-travel stop is approximated as a singly clamped cantilever

beam with the largest stress occurring at the base for a load applied at the tip as given by

Eq. 4.25, where m = 4.1*10-9kg is the proof mass magnitude, a = 2000g is the z-axis

directed linear acceleration, L = 10μm is the beam length, W = 4μm is the beam width,

and T = 2μm is the beam thickness.

2max 6WTmaL

=σ (4.25)

The resulting maximum stress for one singly clamped beam base is max = 0.8GPa;

approximately an order of magnitude less than the 7GPa silicon yield strength. The

spring constant of a single stop is 640N/m, as defined by Eq. 4.26.

3

3

_ 4LEWTK stopz = (4.26)

The displacement of a single over-travel stop cantilever beam restraining the entire

proof mass under a 2000g acceleration load is Δz = 0.13μm, as described by Eq. 4.27,

well within the linear beam theory maximum deflection limit.

stopzstop K

maz_

=Δ (4.27)

Page 90: G_O'Brien PhD Dissertation

73

Each over-travel stop consists of four singly clamped beams and there are a

minimum of 48 complete over-travel stops on all fabricated angular rate sensor designs.

The distributed stress load of 4.2MPa for a 2000g shock load directed along the z-axis

has a maximum stress value several orders smaller than the silicon fracture limit [134].

4.4.4 Dual Beam Torsion Spring

Mechanical decoupling of the drive and sense modes using a simple torsion beam

spring has been previously demonstrated [79] using a novel 10.3μm thick polysilicon

process [139]. Traditionally, CMOS compatible polysilicon deposition has been limited

to a thickness of 5μm in order to minimize the film’s residual stress properties [140].

Although a low stress 12 μm thick low pressure chemical vapor deposition (LPCVD)

polysilicon film has been previously demonstrated [141], the surface micromachined

polysilicon film was limited to a thickness of 2μm in this work.

It should be noted that stiffer single and dual beam torsion springs were observed to

consistently produce higher quality factors. The normal mode model, as described in

section 2.5, states that higher quality factors provide higher resolution Coriolis based

angular rate sensors. As a result, focus on the higher quality factor devices was

emphasized in this section.

The ratio of minimum photolithography defined feature size to structural polysilicon

thickness was 1:1. A simple torsion beam could not reliably produce the desired spring

constant resulting in outer sense ring resonant frequency values greater than 8kHz using

the current design parameter thickness (T). Dual torsion beams were simulated using

finite element analysis (FEA) to determine an optimized designs for multiple resonant

frequencies ranging from 8kHz to 45kHz. The result was a slotted dual torsion beam

spring design, as shown in Figures 4.18 and 4.19.

Page 91: G_O'Brien PhD Dissertation

74

DriveDisc

SenseRing

x

y

TorsionSprings

DriveDisc

SenseRing

x

y

TorsionSprings

Figure 4.18 Enhanced angular rate sensor decoupled mode suspension.

Drive Disc

Sense Ring

Torsion

Spring

Drive Disc

Sense Ring

Torsion

Spring

Figure 4.19 Dual torsion beam coupling spring.

The peak stress location of the slotted dual torsion springs is shown in Figure 4.20

with a torsion resonant frequency of 45kHz and applied z-axis angular rate of 100deg/s.

Stress concentration was intentionally diverted away from the sense ring and drive disc

interface to the mid torsion spring in order to increase the overall torsion spring constant.

Page 92: G_O'Brien PhD Dissertation

75

Figure 4.20 Dual torsion beam coupling spring stress concentration simulation.

4.4.5 Differential Dual Electrode Sense Ring Capacitance

This differential configuration allows for an approximate 2X increase in the sensor

initial capacitance [142]. Electrostatic coupling attributed to fringing electric field lines

terminating on the top surface of the capacitive sensor [143] were eliminated using the

differential capacitance electrode configuration as shown in Figure 4.21.

Linear z-axis acceleration is rejected at the sensor as a function of both differential

and actual capacitance values. The initial and differential sensor capacitance is

theoretically unaffected by a z-axis linear displacement of the proof mass disc using the

electrode configuration as shown in Figure 4.21. This electrode configuration represents

a significant cross axis rejection improvement over the single sided differential

capacitance angular rate sensor where only the differential capacitance remains fixed

under the influence of z-axis linear acceleration [75, 79].

Page 93: G_O'Brien PhD Dissertation

76

Poly3Poly2

Poly1

bc

a

b

aCccw

c

CcwA

A

View A-A

Substrate

Poly3Poly2

Poly1

bc

a

b

aCccw

c

CcwA

A

View A-A

Substrate

Figure 4.21 Differential angular rate sense ring capacitive electrode configuration.

Each differential electrode covers one quarter of the outer proof mass ring area as

shown in Figure 4.22.

DriveDisc

Differential¼ RingCapacitor

Sense Ring

DriveDisc

Differential¼ RingCapacitor

Sense Ring

Figure 4.22 Tilted view of differential electrode capacitive electrodes.

Polysilicon support posts suspend the fixed plate electrode above the movable sense

ring proof mass, as shown in Figure 4.23.

Page 94: G_O'Brien PhD Dissertation

77

FixedTop Electrode

ProofMass

Posts

FixedTop Electrode

ProofMass

Posts

Figure 4.23 Differential capacitor support post detail.

The four individual parallel plate capacitors are interconnected to form a single

differential array. The initial theoretical capacitance of one side of the differential array

is 1.724pF, calculated using Eq. 4.28, where Zbot=2μm, Ztop=0.75μm, rin=536μm, and

rout=650μm.

bottop

bottopinout

ZZZZrr

C4

))(( 220

0

+−=

πε (4.28)

Initial sensor capacitance was measured using an HP 4824A LCR meter as 1.68pF

which is in close agreement with theoretical calculation.

Capacitive detection of sense ring coupled Coriolis force is used to measure the

applied angular rate signal. The Coriolis force is coupled to the angular rate signal by the

velocity of the sense disc driven about the z-axis, as previously described by Eq. 4.2.

Displacement of the sense disc, driven about the z-axis at a sinusoidal frequency of

45kHz, is limited to an amplitude of 0.9μm (Δymax) measured at the inner radius (Rin).

Page 95: G_O'Brien PhD Dissertation

78

The drive disc inner radius (Rin) maximum sinusoidal velocity (vmax) is 0.254m/s as

shown in Figure 4.24.

0 1 .10 5 2 .10 5 3 .10 5 4 .10 50.4

0.2

0

0.2

0.4

t [s]

y(t), Drive Disc Displacement @Rin [10-5m]

v(t), Drive Disc Velocity @Rin [m/s] kHzf 45=θ

θπϖ f2=

)sin()( max tyty ϖΔ=

)cos()( max tytv ϖϖΔ=

y(t),v(t)

dttdytv )()( =

my μ9.0max =Δ

0 1 .10 5 2 .10 5 3 .10 5 4 .10 50.4

0.2

0

0.2

0.4

t [s]

y(t), Drive Disc Displacement @Rin [10-5m]

v(t), Drive Disc Velocity @Rin [m/s] kHzf 45=θ

θπϖ f2=

)sin()( max tyty ϖΔ=

)cos()( max tytv ϖϖΔ=

y(t),v(t)

dttdytv )()( =

my μ9.0max =Δ

Figure 4.24 Drive disc displacement and velocity at the sense ring inner radius (rin).

Sense ring z-axis peak displacement (Δzin=6.19nm) was simulated for an applied

100deg/s angular rate signal directed along the x-axis as shown in Figure 4.25.

Figure 4.25 Angular rate coupled Coriolis force sense ring displacement simulation.

Page 96: G_O'Brien PhD Dissertation

79

The differential electrode capacitance is modeled as a function of Coriolis force

induced sense ring z-axis displacement (Δzin) as shown in Figure 4.26

Poly3Poly2

Poly1

bc

a

c

Substrate

Poly3Poly2

Poly1

bc

a

b

Substrate

a

Δzin

Sense Ring

))((4)2)(( 22

0

inbotintop

inbottopinoutab zZzZ

zZZrrC

Δ+Δ+

Δ++−=

πε

))((4)2)(( 22

0

inbotintop

inbottopinoutbc zZzZ

zZZrrC

Δ−Δ−

Δ−+−=

πε

z

x

CCCW = Cab

CCW = Cbc

Poly3Poly2

Poly1

bc

a

c

Substrate

Poly3Poly2

Poly1

bc

a

b

Substrate

a

Δzin

Sense Ring

))((4)2)(( 22

0

inbotintop

inbottopinoutab zZzZ

zZZrrC

Δ+Δ+

Δ++−=

πε

))((4)2)(( 22

0

inbotintop

inbottopinoutbc zZzZ

zZZrrC

Δ−Δ−

Δ−+−=

πε

z

x

z

x

CCCW = Cab

CCW = Cbc

Figure 4.26 Sense ring z-axis displacement electrode capacitance and schematic.

The simulated peak z-axis displacement for a 100deg/s angular rate (Δzin=6.19nm)

yields a minimum theoretical capacitance of Cab=1.714pF as given by Eq.4.29.

))((4)2)(( 22

0

inbotintop

inbottopinoutab zZzZ

zZZrrC

Δ+Δ+

Δ++−=

πε (4.29)

The simulated peak z-axis displacement for a 100deg/s angular rate (Δzin=6.19nm)

yields a maximum theoretical capacitance of Cbc=1.733pF as given by Eq.4.30.

))((4)2)(( 22

0

inbotintop

inbottopinoutbc zZzZ

zZZrrC

Δ−Δ−

Δ−+−=

πε (4.30)

Page 97: G_O'Brien PhD Dissertation

80

The theoretical differential capacitance is 19fF as given by Eq. 4.31

bcab CCC −=Δ (4.31)

. The theoretical sense ring capacitance sensitivity was calculated as ΔC/C0 =1.1%

for a simulated 100deg/s applied angular rate signal directed along the x-axis. Typically,

a target full scale signal ΔC/C0 =1.0% is used to utilize the linear portion of the

differential sensor capacitance. Implementing a maximum ΔC/C0 =1.0% would limit the

angular rate sensor design to a full scale span of +/-91deg/s using dimensions presented

in this section.

4.5 Angular Rate Sensor Resonant Frequency Models

The proof mass disc drive mode resonant frequency about the z-axis is defined by

Eq. 4.32, where k’ is the torque constant and Izz is the proof mass disc moment of inertia

regarding angular simple harmonic motion.

zzIk '

=θϖ (4.32)

The torque constant k’ is defined by Eq. 4.33.

θΓ

='k (4.33)

The torque constant is described in linear terms by substituting Eq. 4.15, 4.17, and

4.18 into Eq. 4.33 as given by Eq. 4.34.

Page 98: G_O'Brien PhD Dissertation

81

22_

' RKk totalx= (4.34)

The moment of inertia about the z-axis where m is the mass of the proof mass disc is

given by Eq. 4.35.

)(21 2

221 RRmI zz += (4.35)

The mass m of the of the proof mass disc is defined by Eq. 4.36 with the 0.85

multiplier used to approximate the presence of sacrificial etch port holes present in the

poly2 proof mass where the density of silicon (ρsi) used was 2.33*103 kg/m3..

siRRTm ρπ )(85.0 21

22 −= (4.36)

The proof mass disc drive mode resonant frequency about the z-axis is described in

linear terms by substituting Eq. 4.34-4.36 into Eq. 4.28 as given by Eq. 4.37.

( )( )21

22

21

22

_2 22 RRRRT

KRf

si

totalx

+−=

ρππθ (4.37)

Similarly, the resonant frequency directed along the z-axis is defined by simple

harmonic motion as defined by Eq. 4.38.

mK

f totalzz

_

21π

= (4.38)

Page 99: G_O'Brien PhD Dissertation

82

4.6 Angular Rate Sensor Empirical Results

The decoupled sense mode angular rate frequency was measured using an HP-8751

network analyzer to supply the input drive signal. The silicon sensor die was attached to

a test board using conductive epoxy and wire bonded to adjacent input/output

connections as shown in Figure 4.27.

-+-+

NetworkAnalyzerDriveSignal

550kΩVDCBias(1.4VDC) Network

AnalyzerInputSignal

TransimpedanceAmplifier

Sensor

DifferentialAmplifier

Figure 4.27 Sense mode resonant frequency measurement test configuration.

The resonant frequency of the sense mode proof mass ring was measured at 44.96kHz

in a 3mtorr pressure ambient using an HP-8751 Network Analyzer as shown in Figure

4.28. The quality factor Q=225 was extracted from the sense mass resonant frequency

measurement, as given by Eq. 4.39, where the high and low –3dB frequency

measurements were 45.02 kHz and 44.82 kHz respectively.

LOdBHIdB FFF

Q_3_3

0

−− −= (4.39)

Page 100: G_O'Brien PhD Dissertation

83

-25.0

-20.0

-15.0

-10.0

-5.0

0.0

42.0 43.0 44.0 45.0 46.0 47.0 48.0

Frequency [kHz]

Tran

smis

sion

[dB]

Frequency [kHz]

Tran

smis

sion

[dB

]

-25.0

-20.0

-15.0

-10.0

-5.0

0.0

42.0 43.0 44.0 45.0 46.0 47.0 48.0

Frequency [kHz]

Tran

smis

sion

[dB]

Frequency [kHz]

Tran

smis

sion

[dB

]

Figure 4.28 Sense mode resonant peak @44.96 kHz, Q=225.

Angular rate resolution was measured as 3.8 deg/sec in a 20 Hz bandwidth, as shown

in Figure 4.29, representing an 8.1 mV/deg/sec sensitivity.

y = 0.0081xR2 = 0.9957

0

0.1

0.2

0.3

0.40.5

0.6

0.7

0.8

0.9

0 20 40 60 80 100 120Angular Rate [deg/s]

Vout

(fftp

eak

V)

3.8 [deg/s] resolution,31 [mV] Noise Floor

y = 0.0081xR2 = 0.9957

0

0.1

0.2

0.3

0.40.5

0.6

0.7

0.8

0.9

0 20 40 60 80 100 120Angular Rate [deg/s]

Vout

(fftp

eak

V)

3.8 [deg/s] resolution,31 [mV] Noise Floor

Figure 4.29 Angular rate sensor measurement data.

4.7 Angular Rate Sensor Finite Element Analysis Simulation Results

Finite element analysis (FEA) was used to compare theoretical prediction and

empirical results of key angular rate sensor output variables as shown in Table 4.1.

Page 101: G_O'Brien PhD Dissertation

84

Table 4.1 Angular rate sensor model comparison results. Parameter Empirical Theoretical FEA (ANSYS) % Diff 1 % Diff 2 % Diff 3K x_total [N/m] 9.2 8.71 8.93 -5.6 -3.0 -2.5

Kz [kN/m] N/A 251 249 N/A N/A 0.8I yy [m4] N/A 3.51E-16 3.60E-16 N/A N/A -2.6

m ring [kg] N/A 1.98E-09 2.05E-09 N/A N/A -3.6Δ z in [nm] 5.79 6.06 6.19 4.5 6.5 -2.1

F Coriolis [pN] 1.68 1.758 1.795 4.4 6.4 -2.1W [μm] 6L [μm] 80 Description EquationT [μm] 2

Z top [μm] 2 % Diff 1 = 100*( Theo.-Emp.)/Theo.Z bot [μm] 0.75R 1 [μm] 150 % Diff 2 = 100*(FEA - Emp.)/FEAR 2 [μm] 516R in [μm] 536 % Diff 3 = 100*(Theo. - FEA)/Theo.R out [μm] 650

The sense ring moment of inertia (Iyy) and mass (mring) are defined by Eq. 4.40 and

4.41 respectively with theoretical and simulation results listed in Tables 4.1 and 4.2.

)(41 22

inoutringzz RRmI += (4.40)

)( 22

inoutsiring RRTm += πρ (4.41)

Table 4.2 ANSYS sense ring moment of inertia simulation results.

Page 102: G_O'Brien PhD Dissertation

85

4.8 Brownian Noise

Brownian noise was calculated [76, 144] as 2.98*10-3 rad/s where Kb is Boltzman’s

constant, T is the ambient temperature in Kelvin, Δf is 20 Hz, mr is the mass of the outer

sense ring, Q is the quality factor, ωo is the resonant drive frequency, and Δx is the linear

displacement of the outer sense ring, as given by Eq. 4.42.

2xQmfTK

or

bn Δ

Δ=Ω

ω (4.42)

The resolution of the angular rate sensor was 3.8 deg/s while the theoretical Brownian

noise floor is 0.17 deg/s, representing a 22x difference. The noise above the Brownian

noise floor is attributed primarily to the large parasitic capacitance associated with off-

chip signal conditioning. This parasitic capacitance was primarily due to the bond pads

and inter-chip wire bonds required to interface the sensor and CMOS signal conditioning

chip. Single chip integration of sensor and CMOS signal conditioning circuits has

potential to reduce the noise floor above the Brownian limit by 8x as compared to the two

chip implementation as described in Chapter 6.

4.9 Angular Rate Sensor Summary

A surface micromachined gyroscope is demonstrated with a decoupled drive and

sense proof mass. A dual anchor approach is described using folded beam springs and a

torsion post to significantly reduce undesired drive proof mass out of plane deflection

while maintaining a comparatively low rotational mechanical restoring force. The Z-axis

(vertical) proof mass suspension spring constant was increased from 11N/m to over 240

kN/m with the addition of the central torsion post. Interleaved springs attached at least

two different radii can be used to suppress precession of the central proof mass in lieu of

the central torsion post. The interleaved support spring design scheme typically increases

Page 103: G_O'Brien PhD Dissertation

86

Z-axis spring constant by 2X while increasing the rotational spring constant by only 5-

10%. Vertical stiction was eliminated from the design using the dual anchor scheme for

the proof mass and a triply clamped beam approach for the fixed electrostatic drive/sense

beams. The increase in the Z-axis spring constant of the fixed triply clamped beams is

greater than 128X as compared to singly clamped cantilever beams of equal length. The

parasitic capacitance of the fixed beam electrostatic arrays referenced to the silicon

substrate is increased less than 16% due to the tip anchor inclusion. In addition, a

differential capacitance measurement scheme is presented which rejects undesired proof

mass linear acceleration error at the sensor. The differential capacitance electrode

configuration also shields the sensor from fringing electrostatic fields allowing for

increased angular rate sensitivity. The sense mode resonant frequency was measured at

44.96kHz with a quality factor Q of 225 in a 3mtorr ambient. Angular rate resolution

was measured at 3.8deg/s in a 20Hz bandwidth with an 8.1mV/deg/s sensitivity. Signal

resolution was significantly reduced by parasitic capacitance between the sensor

polysilicon interconnection and bond pad layer to silicon substrate. The elimination of

bond pad parasitic capacitance could potentially increase signal resolution by 8x where

single chip sensor and CMOS signal conditioning circuit integration is possible. Another

method to increase signal resolution is to switch from 2μm thick surface micromachined

polysilicon to 20μm thick silicon on insulator (SOI) material. Assuming the parasitic

capacitance for runners and bond pads is identical for both surface micromachined and

SOI substrates, the potential for a 10x increase in signal capacitance would allow for sub

1deg/s angular rate sensor resolution using a 2 chip sensor integration scheme.

The basic and enhanced angular rate sensor design was implemented using surface

micromachining techniques. The central drive disc of the enhanced angular rate sensor

can also function independently as an angular accelerometer. Therefore, we propose

extending the presented design enhancements demonstrated on the surface

Page 104: G_O'Brien PhD Dissertation

87

micromachined dual anchor angular rate sensor to include SOI micromachining applied

to an angular accelerometer design as described in the following chapter.

Page 105: G_O'Brien PhD Dissertation

88

CHAPTER 5

DUAL ANCHOR ANGULAR ACCELERATION SENSOR

MEMS based vibratory gyroscopes typically provide poor cross axis rejection to

linear axis and angular acceleration. The angular rate sensor described in Chapter 4 is

comprised of a central drive disc coupled to an outer sense ring via torsion beam

coupling. The central drive disc is essentially an angular accelerometer which was

designed with a large torsion spring constant to reject external angular acceleration and

provide drive mode resonant frequencies in the range from 4-40kHz. Angular

acceleration sensitivity is inversely proportional to the torsion spring constant and

corresponding modal frequencies. As a result, this chapter will provide electro-

mechanical and process based design strategies aimed at maximizing angular acceleration

sensor coupling via the spring suspended proof mass with resonant frequency targets in

the 400-2kHz range. Design and fabrication of surface micromachined and SOI based

devices is presented with emphasis on the trade off between angular acceleration

sensitivity and the fundamental torsion mode resonant frequency.

5.1 Angular Acceleration Sensor Fundamentals

A rotating rigid body can be described in terms of its angular displacement (θ),

angular rate (Ω), and angular acceleration (α) components as described in Figure 5.1.

Rate tables are typically used to apply external rotation to sensors mounted on their

surface. Rate tables can be excited using either constant or sinusoidal angular rate. An

example of a rate table driven with a sinusoidal angular displacement (θ) of 15 degrees at

a frequency of 2Hz is shown in Figure 5.2 with corresponding angular rate(Ω) and

angular acceleration (α) signals defined for a particle located anywhere on the table top.

Page 106: G_O'Brien PhD Dissertation

89

Center of Rotation

θRP

Particle location at t = 0

Particle location at t > 0, t = t

θPP RL =

dtdθ

dtd

dtd Ω

== 2

2θα

Rotation

Rigid Body Disc

Ω= PRv

θ = displacement angle of particleRP = radial distance to particle from center of rotationLP = distance of particle travel along outer discΩ = angular rate of particleα = angular acceleration of particlev = tangential velocity of particleaT = tangential acceleration of particlea⊥ = centripetal acceleration of particle

αPT Rdtdva ==

22

Ω==⊥ PP

RRva

Angular Rate and Acceleration

Linear Rate and Acceleration

Center of Rotation

θRP

Particle location at t = 0

Particle location at t > 0, t = t

θPP RL =

dtdθ

dtd

dtd Ω

== 2

2θα

Rotation

Rigid Body Disc

Ω= PRv

θ = displacement angle of particleRP = radial distance to particle from center of rotationLP = distance of particle travel along outer discΩ = angular rate of particleα = angular acceleration of particlev = tangential velocity of particleaT = tangential acceleration of particlea⊥ = centripetal acceleration of particle

θ = displacement angle of particleRP = radial distance to particle from center of rotationLP = distance of particle travel along outer discΩ = angular rate of particleα = angular acceleration of particlev = tangential velocity of particleaT = tangential acceleration of particlea⊥ = centripetal acceleration of particle

αPT Rdtdva ==

22

Ω==⊥ PP

RRva

Angular Rate and Acceleration

Linear Rate and Acceleration

Figure 5.1 Description of rigid body rotation using a fixed particle reference point.

Center of Rotation

θRP Particle location atθ = 0

Particle location at +θMax dtdθ

dtd

dtd Ω

== 2

2θα

Rotation

Rigid Body Disc

Angular Rate and Acceleration

15=Maxθ

)sin( tMax ωθθ =

s2=τ τ1=f fπω 2=

)cos( tMax ωωθ=Ω

)sin(2 tMax ωωθα −=

[deg]

[deg]

[deg/s]

[deg/s2]0 1 2 3 4 5 6

160

120

80

40

0

40

80

120

160

Time [s]

Particle location at -θMax

θ

αΩ

Center of Rotation

θRP Particle location atθ = 0

Particle location at +θMax dtdθ

dtd

dtd Ω

== 2

2θα

Rotation

Rigid Body Disc

Angular Rate and Acceleration

15=Maxθ

)sin( tMax ωθθ =

s2=τ τ1=f fπω 2=

)cos( tMax ωωθ=Ω

)sin(2 tMax ωωθα −=

[deg]

[deg]

[deg/s]

[deg/s2]0 1 2 3 4 5 6

160

120

80

40

0

40

80

120

160

Time [s]

Particle location at -θMax

θ

αΩ

Figure 5.2 Example of rate table excited with 15 degree displacement 2Hz sinusoid.

Page 107: G_O'Brien PhD Dissertation

90

Angular acceleration sensors measure the change of an externally applied angular

rate signal with respect to time. Angular rate sensors based on normal mode coupling via

Coriolis acceleration require some form of forced seismic mass oscillation to transfer

energy from the primary drive mode to the secondary sense mode proportional to an

externally applied angular rate signal, as described in Chapter 4. In contrast, angular

acceleration sensor operation is not based on Coriolis acceleration.

A linear accelerometer can be used to measure the tangential component (aT) of

angular acceleration. However, the linear acceleration sensor seismic mass radial

distance to the system center of rotation (RP) is required to calculate the actual angular

acceleration as a function of the measured tangential acceleration as shown in Figure 5.1.

Similarly, a linear accelerometer can also be used to measure angular rate using the

centripetal acceleration component (a⊥) dependent upon the seismic mass radial distance

to the system center of rotation (RP), as described in Figure 5.1.

Rotating rigid body applications where the center of rotation is invariant, such as a

flywheel, can use the radial separation (RP) as an amplification property of centripetal

acceleration and tangential acceleration when implementing linear accelerometers to

measure angular rate and angular acceleration respectively. However, in applications

where the center of rotation is either variable or unknown can result in large error terms

regarding angular rate and angular acceleration measurement using linear accelerometers.

As a result, sensors which couple directly with angular rate (Ω) and angular

acceleration (α) are desirable for use in applications where the center of rotation is

variable or unknown with respect to sensor location. The angular acceleration sensor

seismic mass displacement is directly proportional to an externally applied angular

Page 108: G_O'Brien PhD Dissertation

91

acceleration signal independent of radial separation to the system center of rotation (RP).

This chapter describes an angular acceleration sensor with its sensitivity independent of

radial distance between sensor location and the center of rotation (RP).

5.2 Angular Acceleration Sensor Applications

Applications such as computer hard drive read/write head compensation [9] require

an angular acceleration signal to provide control loop feedback. While an angular rate

sensor output could provide angular acceleration signal data, this is typically not advised

since high frequency noise and random angle walk can provide large error signals when

differentiated. Sensor signal integration is typically preferred to differentiation where

low signal bandwidth and reduced high frequency noise are desired due to the inherent

time averaged signal conditioning. As a result, non-zero angular accelerometer signal

output can be integrated to provide angular rate information.

Angular accelerometers can be used in applications such as automotive rollover

detection, computer hard drive read/write head compensation, washing machines, and

video camera stabilization provided proper sensor resolution and bandwidth can be

realized.

An angular accelerometer has been previously reported [10] with a noise floor on the

order of 75rad/s2/(rt-Hz) and sensitivity of 0.24μVrms/rad/s2. Automotive angular

accelerometer ranges have been described [12] in the range of (+/-) 5000°/s2, although

sensitivity and noise floor results were omitted. Production angular accelerometers from

Delphi and ST Microelectronics are currently available with a full scale span reported in

the range of 200-2000rad/s2, with reported sensitivity as low as 2.5rad/s2, as shown in

Table 5.1.

Page 109: G_O'Brien PhD Dissertation

92

Table 5.1 Angular accelerometer specification data. Sensitivity Resolution Span Bandwidth Current

Company [mV/r/s2] [r/s2] +/- [r/s2] [Hz] [mA]Delphi 4 5 500, 2000 250,500 5ST Micro. 10 2.5 200 800 26

The device electronics required to signal condition a capacitive angular acceleration

sensor are virtually identical to those required for linear capacitive accelerometer

applications [1]. Technology re-use can be employed to significantly shorten the product

design/fabrication cycle time to market due to direct application of existing linear

accelerometer CMOS signal conditioning circuitry with only minor modification.

5.3 Angular Rate Sensor and Angular Acceleration Sensor Design Comparison

The angular rate sensor utilizes a polysilicon central disc equipped with capacitive

array based electrostatic actuation to drive the structure near its primary mode torsional

resonance. The outer Coriolis sense ring deflects as a function of Coriolis acceleration

coupled external angular rate which is sensed using capacitive differential electrodes.

The angular acceleration sensor is a subset of the angular rate sensor with the Coriolis

ring and its capacitive differential electrodes removed as shown in Figure 5.3.

Angular Rate Sensor Angular

Acceleration Sensor

Coriolis Sense Ring

Torsion Beam Coupling Springs

Capacitive Arrays

SeismicMassDrive

SenseSense

Sense

Angular Rate Sensor Angular Acceleration Sensor

Coriolis Sense Ring

Torsion Beam Coupling Springs

Capacitive Arrays

SeismicMassDrive

SenseSense

Sense

Figure 5.3 Angular rate sensor and angular acceleration sensor comparison.

Page 110: G_O'Brien PhD Dissertation

93

The remaining capacitive arrays are used to both sense angular acceleration and

actuate an electrostatic self test based central disc seismic mass displacement. Beam

sidewall area forms the 2μm thick polysilicon parallel plate capacitive arrays with an

initial gap of 2μm, as shown in Figure 5.4.

2μmView Tilt:75° aboutx-axis

SeismicMassElectrode

FixedSubstrateElectrodesCapacitive

Arrays

2μmView Tilt:75° aboutx-axis

SeismicMassElectrode

FixedSubstrateElectrodesCapacitive

Arrays

Figure 5.4 Angular acceleration sensor capacitive parallel plate beam arrays.

Electrical interconnection from the capacitive electrode arrays to bond pads is

facilitated using a conductive 0.5μm thick photolithography defined polysilicon film

deposited over a 0.4μm thick low stress silicon nitride film as shown in Figure 5.5.

B Sub C ST2

CCCW CCW

CST_CW

CST_CCW

CCW

CST_CW

CST_CCW

Self TestArray

Proof Mass Electrode (B)

CCW

CST_CW

CST_CCW

A ST1

B Sub C ST2A ST1

CapacitiveSelf Test Array

CapacitiveSense Array

SenseArray

SenseArray

Self TestArray

B Sub C ST2

CCCW CCW

CST_CW

CST_CCW

CCW

CST_CW

CST_CCW

Self TestArray

Proof Mass Electrode (B)

CCW

CST_CW

CST_CCW

A ST1

B Sub C ST2A ST1

CapacitiveSelf Test Array

CapacitiveSense Array

SenseArray

SenseArray

SenseArray

SenseArray

Self TestArray

Figure 5.5 Capacitive angular acceleration sensor bond pad electrical schematic.

Page 111: G_O'Brien PhD Dissertation

94

5.4 Surface Micromachined Angular Accelerometer Basic Operation

Angular acceleration is sensed as a torque causing an angular displacement of a

centrally anchored proof mass disc, as given by Eq. 5.1, where I is the moment of inertia

and α is the applied angular acceleration.

αI=Γ (5.1)

The moment of inertia for a simple disc is given by Eq. 5.2, where m is the mass, R1

is the inner disc radius, and R2 is outer disc radius. The disc is assumed to be symmetric

about the system center of rotation with the angular displacement independent of the

offset Lc, as shown in Figure 5.6.

222

1 mRI = (5.2)

xyy

Lc

R1

R2

Center of System Rotation

Center of Disc Rotation

Kx

α

AngularAcceleration

Proof Mass Disc

xyy

Lc

R1

R2

Center of System Rotation

Center of Disc Rotation

Kx

α

AngularAcceleration

Proof Mass Disc

Figure 5.6 Angular Accelerometer Disc Configuration.

The mass of the disc is given by Eq.5.3 where T is the thickness and ρsi = 2.33 kg/m3

is the density of silicon.

22RTm siπρ= (5.3)

Page 112: G_O'Brien PhD Dissertation

95

Externally applied angular acceleration results in a non-zero angular displacement of

the centrally supported seismic mass measured using the capacitive sense array. Radial

dimensions defining the initial and final length of the sense array capacitive electrodes

referenced from the seismic mass center of rotation are shown in Figure 5.7.

g0 = 2μmt = 2μm

ProofMass

FixedBeamArray

r1

r0

LB = r1-r0

g0 = 2μmt = 2μm

ProofMass

FixedBeamArray

r1

r0

LB = r1-r0

Figure 5.7 Capacitive array radial dimensions referenced from center of rotation.

The single sided capacitance of the array is defined by Eq. 5.4, and given by Eq. 5.5

where θ represents the proof mass disc displacement angle.

∫ −= 1

0

rr )( dr

rgT

Co

o

θε

θ (5.4)

⎟⎟⎠

⎞⎜⎜⎝

⎛−−

=10

000 ln)(rgrgT

Cθθ

θε

θ (5.5)

Electrostatic latching [124] occurs for a beam tip displacement at radius r1 greater

than 0.45*g0, where g0 represents the initial non-displaced dielectric gap as described in

Appendix A. The angular accelerometer disc capacitance can be closely approximated

using a parallel plate model for small proof mass displacements representing less than

Page 113: G_O'Brien PhD Dissertation

96

10% the original dielectric gap. The design target of the sensor is based on a (+/-) 1%

ΔC/C0 full scale span to be signal conditioned by a CMOS control chip. As a result, the

parallel plate capacitor approximation is adequate and significantly simplifies the

theoretical analysis. The initial and final parallel plate capacitances are given by Eq. 5.6

and Eq. 5.7 respectively, where g0 is the initial dielectric gap and Δx ≅ R2θ.

0

0100

)(g

TrrC

−=

ε (5.6)

20

0101

)(xg

TrrCΔ−

−=

ε (5.7)

The change in capacitance versus initial capacitance is defined by Eq. (5.8).

0

01

0 CCC

CC −

=Δ (5.8)

Combining Eq. 5.6 and 5.7 into Eq. 5.8 is described by Eq. 5.9.

20

2

0 xgx

CC

Δ−Δ

=Δ (5.9)

Solving for Δx in terms of the torque induced as a function of angular acceleration α

is the next step. The torque can be represented by a force vector F2 applied at the outer

disc radius R2 as given by Eq. 5.10.

22 RF=Γ (5.10)

Page 114: G_O'Brien PhD Dissertation

97

The force magnitude F2 can be described in terms of linear displacement Δx measured

at the outer disc radius R2 by the linear system spring constant K2 as given by Eq. 5.11.

The angular accelerometer can be linearly approximated by substituting Eq. 5.1, 5.10

and 5.11, into Eq. 5.9 as given by Eq. 5.12.

222 xKF Δ= (5.11)

αα

IKRgI

CC

−=

Δ

2200

(5.12)

The linear spring constant of the beam suspension is defined as the displacement Δx

observed for a force vector F2 applied tangential to the disc at the radial distance R2.

Two basic spring configurations were available with proof mass disc attach point located

at radii R0 and R1 as shown in Figure 5.8. The centrally located substrate anchors are

located near the center of rotation at a distance less than R0 to minimize temperature

effects of differential expansion and contraction associated between the substrate films

and suspended proof mass.

OuterConnected

InnerConnected

OuterConnected

InnerConnected

R1

R1 RIN

R0

OuterConnected

InnerConnected

OuterConnected

InnerConnected

R1

R1 RIN

R0

Figure 5.8 Angular accelerometer dual beam spring suspension attach points.

Page 115: G_O'Brien PhD Dissertation

98

The lateral spring constants for the outer (KOUT) and inner (KIN) connected springs,

defined at attach point radius R1, are listed in Figures 5.9 and 5.10 respectively.

L

W

Anchor

Proof Mass

KB2

3

3

4LTEWKBn =

42

423

42

423

BB

BBB

BB

BBB

OUT

KKKKK

KKKKK

K

++

⎟⎟⎠

⎞⎜⎜⎝

⎛+

=Cantilever Beam

KB1

KB3

KB4

KB5

3

3

6LTEWKOUT ≅

bnBB KKK ...21 ≅≅Let

Linear spring constant at R1

RIN

Centerof

RotationL

W

Anchor

Proof Mass

KB2

3

3

4LTEWKBn =

42

423

42

423

BB

BBB

BB

BBB

OUT

KKKKK

KKKKK

K

++

⎟⎟⎠

⎞⎜⎜⎝

⎛+

=Cantilever Beam

KB1

KB3

KB4

KB5

3

3

6LTEWKOUT ≅

bnBB KKK ...21 ≅≅Let

Linear spring constant at R1

RIN

Centerof

Rotation

Figure 5.9 Outer connected spring constant directed along x-y plane.

L

W

KB3

KB1

KB2Anchor

ProofMass

2KK IN = 3

3

4LTEWKBn = Cantilever

Beam

3

3

21

2

4LTEW

RRK IN

IN ≅bnBB KKK ...21 ≅≅Let

Linear spring constant at R1

ProofMass

R1RIN

L

W

KB3

KB1

KB2Anchor

ProofMass

2KK IN = 3

3

4LTEWKBn = Cantilever

Beam

3

3

21

2

4LTEW

RRK IN

IN ≅bnBB KKK ...21 ≅≅Let

Linear spring constant at R1

ProofMass

R1RIN

Figure 5.10 Inner connected spring constant directed along x-y plane.

Page 116: G_O'Brien PhD Dissertation

99

The spring suspension initially utilized for the angular rate sensor, as described in

Chapter 4, was modified with a small radius torsion post to allow for lower torsion spring

constants while retaining a configuration which maintains the disc in the x-y plane with a

stiffened z-axis spring constant. The torsion post was omitted from the angular

accelerometer suspension which significantly lowered both spring constants about and

along the z-axis. As a result of the torsion post omission, the proof mass was more

susceptible to undesirable precession modes while excited with off axis angular

acceleration using the standard inner and outer connected spring suspensions.

Undesirable disc precession was alleviated by using an interleaved combination of the

inner and outer connected springs as shown in Figure 5.11.

InterleavedSprings

AnchorsCentralHub

SeismicMass

InterleavedSprings

AnchorsCentralHub

SeismicMass

Figure 5.11 Interleaved folded beam spring design.

The angular displacement sensitivity of the seismic mass is determined by the lateral

spring constant of the interleaved spring suspension. The lateral spring constant of the

interleaved spring suspension is a linear combination of the outer and inner springs. The

lateral spring constant theoretical model prediction referenced to radial location R1 was

compared to finite element analysis (FEA) simulation results with a -1.1% difference

observed as shown in Figure 5.12.

Page 117: G_O'Brien PhD Dissertation

100

3

3

6LTEWKOUT ≅

E = 160GPa, R1 = 160μm, RIN = 144μm

xFK Ansys Δ

= 1

L = 120μm, T = 2μN, W = 2μm, F1 = 1μN

Constants :

Theoretical Model:

73.11 ≅K [N/m]

FEA Simulation:Input: Γ1 = F1R1

Output: Δx = 0.57μm

75.1=AnsysK [N/m]

Comparison:

( )OUTIN KKK +≅ 31

3

3

21

2

4LTEW

RRK IN

IN ≅

100%2

1

KKK

Diff Ansys−≅1.1% −=Diff

Γ1

Δx=0.57μm

Γ1 =F1 R1

F1=1μN

@ R1

Outer Spring

InnerSpring

3

3

6LTEWKOUT ≅

E = 160GPa, R1 = 160μm, RIN = 144μm

xFK Ansys Δ

= 1

L = 120μm, T = 2μN, W = 2μm, F1 = 1μN

Constants :

Theoretical Model:

73.11 ≅K [N/m]

FEA Simulation:Input: Γ1 = F1R1

Output: Δx = 0.57μm

75.1=AnsysK [N/m]

Comparison:

( )OUTIN KKK +≅ 31

3

3

21

2

4LTEW

RRK IN

IN ≅

100%2

1

KKK

Diff Ansys−≅1.1% −=Diff

Γ1

Δx=0.57μm

Γ1 =F1 R1

F1=1μN

@ R1

Outer Spring

InnerSpring

Figure 5.12 Lateral spring constant theoretical model and FEA simulation results.

It should be noted that both the inner and outer spring designs use similar values for

beam length L and width W. The linearized lateral spring constant of the outer and inner

connected beam suspensions referenced to radial location R1 are given by Eq. 5.13 and

5.14 respectively where n1 is the number of individual springs.

3

3

1 6LTEWnKOUT = (5.13)

3

3

21

2

1 4LTEW

RRnK IN

IN = (5.14)

The effective lateral spring constant present at the seismic mass outer perimeter radial

location R2 is defined by Eq. 5.15 and described by Eq. 5.16 with n1 = 3 springs for each

inner and outer configurations where R0 << R1.

)(22

21

2 OUTIN KKRRK += (5.15)

Page 118: G_O'Brien PhD Dissertation

101

( )21

232

2

3

2 234

RRLRTEWK IN += (5.16)

The change in capacitance as a function of applied angular acceleration a is described

by combining Eq. 5.2, 5.3 and 5.16 into Eq. 5.12 as given by Eq. 5.17

( ) 52

321

230

52

3

0 2232

RLRREWgRL

CC

siIN

si

απραπρ

−+=

Δ (5.17)

The change in capacitance for a 100 rad/s2 angular acceleration is shown in Figure

5.13 for a constant beam width W = 2μm.

Outer Disc Radius (R2) [m]

BeamSpring Length (L) [m]

%ΔC/C0

Outer Disc Radius (R2) [m]

BeamSpring Length (L) [m]

%ΔC/C0

Figure 5.13 %ΔC/C0 Vs beam spring length (L) and outer disc radius (R2).

The linear spring constants directed along the z-axis for the outer and inner connected

beam springs are described in Figures 5.14 and 5.15 respectively.

Page 119: G_O'Brien PhD Dissertation

102

L

W

Anchor

Proof Mass

KB2

3

3

4LEWTK Bn =

54

54

21

213

54

54

21

213

_

BB

BB

BB

BBB

BB

BB

BB

BBB

ZOUT

KKKK

KKKKK

KKKK

KKKKK

K

++

++

⎟⎟⎠

⎞⎜⎜⎝

⎛+

++

=Cantilever Beam

KB1

KB3

KB4

KB5

3

3

_ 8LEWTK ZOUT ≅

bnBB KKK ...21 ≅≅Let

Linear spring constant at R1

L

W

Anchor

Proof Mass

KB2

3

3

4LEWTK Bn =

54

54

21

213

54

54

21

213

_

BB

BB

BB

BBB

BB

BB

BB

BBB

ZOUT

KKKK

KKKKK

KKKK

KKKKK

K

++

++

⎟⎟⎠

⎞⎜⎜⎝

⎛+

++

=Cantilever Beam

KB1

KB3

KB4

KB5

3

3

_ 8LEWTK ZOUT ≅

bnBB KKK ...21 ≅≅Let

Linear spring constant at R1

Figure 5.14 Outer connected spring constant directed along z-axis.

L

W

KB3

KB1

KB2Anchor

ProofMass

31

312

31

312

_

BB

BBB

BB

BBB

ZIN

KKKKK

KKKKK

K

++

⎟⎟⎠

⎞⎜⎜⎝

⎛+

=3

3

4LEWTKBn = Cantilever

Beam

3

3

_ 6LEWTK ZIN ≅bnBB KKK ...21 ≅≅Let

Linear spring constant at R1

ProofMass

L

W

KB3

KB1

KB2Anchor

ProofMass

31

312

31

312

_

BB

BBB

BB

BBB

ZIN

KKKKK

KKKKK

K

++

⎟⎟⎠

⎞⎜⎜⎝

⎛+

=3

3

4LEWTKBn = Cantilever

Beam

3

3

_ 6LEWTK ZIN ≅bnBB KKK ...21 ≅≅Let

Linear spring constant at R1

ProofMass

Figure 5.15 Inner connected spring constant directed along z-axis.

The linear spring constant directed along the z-axis for the outer and inner connected

beam springs are described by Eq. 5.18 and 5.19 respectively.

Page 120: G_O'Brien PhD Dissertation

103

3

3

1_ 8LEWTnK ZOUT = (5.18)

3

3

1_ 6LEWTnK ZIN = (5.19)

The linearized z-axis spring constant is defined by Eq. 5.20 and described by Eq. 5.21

with n1 = 3 springs for each inner and outer configuration.

ZINZUTZ KKK __0_2 += (5.20)

3

3

_2 87

LEWTK Z = (5.21)

The difference between theoretical z-axis spring constant prediction (K2_Z = 1.29N/m)

and FEA simulation results (K2_Z_ANSYS = 1.32N/m) is 2.3% using beam spring dimensions

listed in Figure 5.12. The analytical z-axis deflection of the proof mass (m = 5.03*10-

9kg) due to gravity (a = 9.802m/s2) was calculated as 0.038μm using the z-axis spring

constant (K2_Z) stiffness.

The z-axis spring constant (K2_Z) also provides mechanical restoring force opposing

surface tension forces [145] present after wet HF sacrificial oxide etch due to subsequent

rinse and gradual evaporation of de-ionized water from the silicon wafer surfaces. An

unacceptably small z-axis spring constant (K2_Z) allows surface tension forces to displace

the seismic proof mass until eventual physical contact with a substrate electrode is

observed. MEMS structures fabricated in silicon are prone to exhibit undesirable stiction

[125] when placed in physical contact with an adjacent silicon surface. As a result,

physical contact of the movable proof mass and adjacent silicon fixed electrodes should

Page 121: G_O'Brien PhD Dissertation

104

be avoided by appropriate design with respect to adequate suspension z-axis spring

stiffness. The surface micromachined z-axis spring constant (K2_Z) would allow a 2μm

thick polysilicon sensor proof mass to travel over 200μm before the mechanical restoring

force is large enough to balance surface tension forces, as graphically represented by

point A in Figure 5.16.

Center of Rotation (Z-Axis)

R2γ = surface tension of liquid (H2O)

g0 = z-axis gap between seismic mass and substrate electrodeφ = contact angle between liquid and polysilicon surfaceFsurf = force due to surface tension

)cos(φγPFSurf =

Sensor Proof MassP = seismic mass outer perimeter at R2

zKF ZZ Δ= _2

FZ = z-axis spring mechanical restoring force

1)

2)

3

3

_2 87

LEWTK Z =

3)

22 RP π= 0=φ

SurfZ FF =

Z

Surf

KF

z_2

3

32

716

EWTLRz πγ

FZ

FSurf

1 10 1000.01

0.1

1

10

100

103

6

Sensor Thickness (T) [μm]

Subs

trate

Gap

(ΔZ)

[μm

] Z-Axis Displacement of Proof Mass due to Surface Tension of H2O Post Wet HF Based Oxide Sac-Etch

Constants:L = 120μm, W = 2μm, E = 160GPa, R2 = 586μm, γ = 0.071N/m

TSensor Thickness

A

B

Center of Rotation (Z-Axis)

R2γ = surface tension of liquid (H2O)

g0 = z-axis gap between seismic mass and substrate electrodeφ = contact angle between liquid and polysilicon surfaceFsurf = force due to surface tension

)cos(φγPFSurf =

Sensor Proof MassP = seismic mass outer perimeter at R2

zKF ZZ Δ= _2

FZ = z-axis spring mechanical restoring force

1)

2)

3

3

_2 87

LEWTK Z =

3)

22 RP π= 0=φ

SurfZ FF =

Z

Surf

KF

z_2

3

32

716

EWTLRz πγ

FZ

FSurf

1 10 1000.01

0.1

1

10

100

103

6

Sensor Thickness (T) [μm]

Subs

trate

Gap

(ΔZ)

[μm

] Z-Axis Displacement of Proof Mass due to Surface Tension of H2O Post Wet HF Based Oxide Sac-Etch

1 10 1000.01

0.1

1

10

100

103

6

Sensor Thickness (T) [μm]

Subs

trate

Gap

(ΔZ)

[μm

] Z-Axis Displacement of Proof Mass due to Surface Tension of H2O Post Wet HF Based Oxide Sac-Etch

Constants:L = 120μm, W = 2μm, E = 160GPa, R2 = 586μm, γ = 0.071N/m

TSensor Thickness

A

B

Figure 5.16 Model of z-axis surface tension sensor displacement Vs sensor thickness.

However, the present gap between sensor and substrate electrode is only 2μm which

implies that silicon to silicon contact is highly probable due to wet process (de-ionized

water) surface tension effects. The z-axis spring constant (K2_Z) can be increased by a 3rd

order function of thickness while keeping all other design dimension parameters fixed.

This relationship is described by point B, in Figure 5.16, that a 2μm sensor to substrate

Page 122: G_O'Brien PhD Dissertation

105

gap between the original proof mass cross sectional area would require a 9.5μm thick

sensor to balance the surface tension force upon contact. A sensor thickness greater than

9.5μm will preclude silicon sensor to silicon substrate electrode contact and should be

utilized where wet wafer processing is desired. As a result, increasing the sensor

thickness from 2μm to 20μm will be evaluated in the following sections.

Surface micromachined devices evaluated in this chapter were released using a wet

hydrofluoric (HF) acid sacrificial oxide etch followed by super critical CO2 processing

[146] to minimize z-axis oriented surface tension forces on the proof mass disc, as

described in Appendix B. While super critical CO2 is an effective tool to eliminate

stiction regarding MEMS sensor research on a single wafer basis, there is not yet a

commercially available multi-wafer tool which is fully clean room compatible intended

for use in an industrial CMOS wafer fabrication facility. Therefore, sensor designs

intended for eventual transfer from a research lab environment to a high volume

fabrication/production facility should provide an adequate z-axis spring constant to

minimize proof mass displacements due to surface tension based wet processing steps.

5.4.1 Surface Micromachined Angular Accelerometer Resonant Frequencies

The surface micromachined angular accelerometer fundamental mode resonant

frequency is rotational about the z-axis. The rotational resonant frequency is defined by

Eq. 5.22 where k’ is the torque constant [145] defined by Eq. 5.23.

Ik '

=θϖ (5.22)

θΓ

='k (5.23)

Page 123: G_O'Brien PhD Dissertation

106

The displacement angle θ is described in linearized terms by Eq. 5.24.

2

2

RxΔ

=θ (5.24)

The rotational resonant frequency can be described by substituting Eq. 5.10, 5.11,

5.23, and 5.24 into Eq. 5.22 as given by Eq. 5.25, where k’ = K2R22.

IRK 2

22=θϖ (5.25)

Further simplification is made by substitution of Eq. 5.16 into Eq. 5.25 as given by Eq.

5.26 where dependence on device thickness is not observed.

LRREW

LRWf

si

IN

πρπθ 2)23(

2

21

2

22

+= (5.26)

The theoretical resonant torsion frequency Vs spring length (L) and outer disc radius

(R2) is plotted in Figure 5.17.

It should be noted that the torsion mode resonant frequency is independent of proof

mass thickness (T). The resonant frequency directed along the z-axis is defined by Eq.

5.27.

mK Z

Z_2=ϖ (5.27)

Page 124: G_O'Brien PhD Dissertation

107

Outer Disc Radius (R2) [m]

BeamSpring Length (L) [m]

TorsionModeFreq [Hz]

Figure 5.17 Torsion mode frequency Vs spring length (L) and outer disc radius (R2).

Further simplification is made by substitution of Eq. 5.21 into Eq. 5.27 as given by Eq.

5.28 where dependence on device thickness is observed.

siZ L

EWLR

Tfπρπ 2

74 2

= (5.28)

The z-axis resonant frequency is a strong function of proof mass thickness in addition

to beam length (L) and outer disc radius (R2) for T = 2μm and T = 20μm thick proof mass

discs as shown in Figures 5.18 and 5.19 respectively. It should be noted that the z-axis

resonant frequency increases linearly with increasing thickness as previously described

by Eq. 5.28.

Page 125: G_O'Brien PhD Dissertation

108

Outer Disc Radius (R2) [m]

BeamSpring Length (L) [m]

Z-AxisModeFreq [Hz]

Outer Disc Radius (R2) [m]

BeamSpring Length (L) [m]

Z-AxisModeFreq [Hz]

Figure 5.18 Modal z-axis frequency for 2μm thick proof mass disc.

Outer Disc Radius (R2) [m]

BeamSpring Length (L) [m]

Z-AxisModeFreq [Hz]

Outer Disc Radius (R2) [m]

BeamSpring Length (L) [m]

Z-AxisModeFreq [Hz]

Figure 5.19 Modal z-axis frequency for 20μm thick proof mass disc.

Page 126: G_O'Brien PhD Dissertation

109

When the suspension beam width (W) and thickness (T) are identical, the modal

frequencies directed along and about the z-axis are similar with the ratio plotted in Figure

5.20. This ratio varies as a function of outer disc radius (R2) it is independent of beam

spring length (L).

Outer Disc Radius (R2) [m]

BeamSpring Length (L) [m]

Ratio of modal frequency directed about and along the z-axis

Outer Disc Radius (R2) [m]

BeamSpring Length (L) [m]

Ratio of modal frequency directed about and along the z-axis

Figure 5.20 Modal z-axis frequency ratio for 2μm thick proof mass disc.

While matching the modal frequencies along and about the z-axis is desirable for

coupled mode gyroscope designs [78] it is undesirable for an angular accelerometer

implementation.

In addition, the relatively small z-axis spring constants of the 2μm thick polysilicon

designs typically require super critical CO2 processing [146], as described in Appendix B,

in order to avoid vertical stiction [125] after sacrificial oxide wet hydrofluoric-acid/H20

rinse wafer processing. However, similarly designed devices fabricated in 20μm thick

Page 127: G_O'Brien PhD Dissertation

110

SOI substrates did not exhibit vertical stiction when processed using a wet HF acid

sacrificial oxide etch followed by a wet H20-IPA rinse. The 20μm thick vertical spring

constant is 1000 times larger than a spring 2μm thick with an identical cross section and

is responsible for the observed increased resistance to wet process related vertical

stiction. Increasing mechanical film thickness of the proof mass disc and support beam

springs does not effect the angular acceleration based sensor capacitance sensitivity

(ΔC/C0) or the torsion mode resonant frequency (ωz). However, increasing the

mechanical film thickness significantly stiffens the z-axis spring constant allowing for

standard wet hydrofluoric (HF) acid etching of wafers without the need for post de-

ionized H20 rinse supercritical CO2 processing. In addition, the increase in mechanical

film thickness further separates the modal frequencies directed about and along the z-axis

as shown in Figure 5.21 for a 20μm thick film.

Outer Disc Radius (R2) [m]

BeamSpring Length (L) [m]

Ratio of modal frequency directed about and along the z-axis

Outer Disc Radius (R2) [m]

BeamSpring Length (L) [m]

Ratio of modal frequency directed about and along the z-axis

Figure 5.21 Modal z-axis frequency ratio for 20μm thick proof mass disc.

Page 128: G_O'Brien PhD Dissertation

111

Polysilicon films have been described up to 12μm thick to fabricate inertial sensors

[141] and are typically limited by significantly increased film stress as a function of

deposition thickness. However, silicon on insulator (SOI) substrates typically range from

microns to hundreds of microns yielding a virtually stress free single crystal silicon film

[147].

While polysilicon is a homogenous polycrystalline material described by a single

valued Young’s modulus, <100> surface orientation single crystal silicon exhibits a

different Young’s moduli depending upon the crystal orientation [148]. This result

typically precludes <100> type single crystal silicon wafers for use with vibrating shell

normal mode MEMS gyroscopes due poor orthogonal mode matching. A <111> surface

orientation single crystal silicon vibrating ring normal mode gyroscope fabricated on an

SOI substrate [149] has been previously demonstrated. Although the <111> surface

orientation yields a single valued Young’s modulus and is commonly used in bipolar

integrated circuit transistor fabrication, this wafer orientation is not currently fabricated in

large production volumes using SOI substrates due to degraded performance of CMOS

integrated circuit transistor operation [150].

Suspension spring location symmetry can be used to describe mechanical MEMS

structures in <100> single crystal silicon assuming an average Young’s modulus of

160GPa [151]. The homogenous Young’s modulus assumption of <100> single crystal

silicon yields a reasonably good approximation in MEMS devices which operate at

frequencies well below mechanical resonance such as open loop seismic mass angular

accelerometers with radial distribution of suspension spring geometries. As a result,

single crystal SOI wafers were used for further angular acceleration sensor development

in 20μm thick structural films to provide an adequate z-axis spring constant stiffness post

HF-acid sacrificial oxide etch during subsequent wet processing steps.

Page 129: G_O'Brien PhD Dissertation

112

5.5 Angular Accelerometer Surface Micromachined to SOI Design Conversion

A simplified SOI process flow was developed for use in rapid development of the

capacitive sensor prototypes described in this chapter. The angular acceleration sensor

SOI based designs presented in this chapter can also be fabricated using a novel

integrated SOI process flow intended for use in a high volume manufacturing

environment, as described in Chapter 7, which addresses handle wafer substrate electrical

contact and isolation using conformal film trench refill techniques.

In order to utilize the thick mechanical films available in SOI it was necessary to

modify the original surface micromachined polysilicon design. The initial design

conversion required modification of the suspension spring substrate anchors and bond

pad to capacitive electrode electrical interconnect runners as shown in Figure 5.22.

Bond Pads

Fixed Electrode CCW

Fixed Electrode CW

Electrical InterconnectRunner

ProofMassDiscCentral

Hub

FoldedBeam Springs

Bond Pads

Fixed Electrode CCW

Fixed Electrode CW

Electrical InterconnectRunner

ProofMassDiscCentral

Hub

FoldedBeam Springs

Figure 5.22 Angular acceleration sensor design conversion from polysilicon to SOI.

Page 130: G_O'Brien PhD Dissertation

113

The surface micromachined inner and outer connected folded beam springs were

replicated in a 20μm thick SOI based process flow as shown in Figure 5.23.

R1

R0

Inner Connected Folded Beam Spring

Outer Connected Folded Beam Spring

ProofMassDisc

R1

R0

Inner Connected Folded Beam Spring

Outer Connected Folded Beam Spring

ProofMassDisc

Figure 5.23 Centrally anchored folded beam spring array with solid central hub.

The simplified SOI process flow substrate anchor is mechanically connected to the

handle wafer via the buried oxide (BOX) which remains post sacrificial oxide etch.

Design rules were formulated to differentiate between mechanically anchored and

released structures using a timed wet HF sacrificial BOX etch. The SOI sensor outline

was trenched by a photolithography defined deep reactive ion etch (DRIE) utilizing a

time division multiplexed passivation and etch algorithm with input/output parameters

defined in Appendix C. The inner and outer connected beam spring anchors are

distributed symmetrically around the central hub as shown in Figure 5.24.

Page 131: G_O'Brien PhD Dissertation

114

Anchor

CentralHub

Anchor

Anchor

Anchor Anchor

Anchor

Inner Beam Spring Proof Mass Attach Radius (R0)

Anchor

CentralHub

Anchor

Anchor

Anchor Anchor

Anchor

Inner Beam Spring Proof Mass Attach Radius (R0)

Figure 5.24 Beam spring substrate anchor and central hub detail.

The conservative design rule for a mechanically released beam requires a maximum

cross section of 8μm while the anchor design rule requires a minimum cross section of

32μm to ensure that a robust amount of residual BOX exists post sacrificial buried oxide

etch as shown in Figure 5.25.

Identical springs can be interleaved to form the SOI angular accelerometer design

yielding identical lateral and vertical spring constant sets independent of crystal

orientation as rotated normal to the <100> silicon wafer surface plane. The handle wafer

and SOI mechanical film are both comprised of single crystal silicon with a rotation

misalignment typically less than 1 degree with respect to the wafer flat [148].

Page 132: G_O'Brien PhD Dissertation

115

Handle Wafer (525μm Thick)

SOI (20μm Thick)

BOX (2μm Thick)

Pre Sacrificial Oxide Etch

Handle Wafer (525μm Thick)

SOI (20μm Thick)

BOX

32μm

Post Sacrificial Oxide Etch

8μm

Lateral Undercut (> 4μm)

AnchorReleasedBeam

Handle Wafer (525μm Thick)

SOI (20μm Thick)

BOX (2μm Thick)

Pre Sacrificial Oxide Etch

Handle Wafer (525μm Thick)

SOI (20μm Thick)

BOX

32μm

Post Sacrificial Oxide Etch

8μm

Lateral Undercut (> 4μm)

Handle Wafer (525μm Thick)

SOI (20μm Thick)

BOX (2μm Thick)

Pre Sacrificial Oxide Etch

Handle Wafer (525μm Thick)

SOI (20μm Thick)

BOX

32μm

Post Sacrificial Oxide Etch

8μm

Lateral Undercut (> 4μm)

AnchorReleasedBeam

Figure 5.25 DRIE trench defined SOI suspension BOX anchor cross section.

The single crystal orientation dependence of silicon thermal expansion coefficients are

closely matched between the handle wafer and adjacent SOI. The matched thermal

expansion coefficient relationship between the SOI and silicon handle wafer allows for

distributed anchor placement farther away from the center of device rotation without

significant degradation of the angular acceleration sensor’s temperature coefficient of

offset (TCO) or sensitivity (TCS). The interleaved anchor distribution placement

produces no change on beam suspension spring constants directed along or about the z-

axis when compared to the original centrally located anchor design as shown in Figure

5.23. However, the anchor distribution located farther away from the center of rotation,

as shown in Figure 5.26, significantly stiffens the proof mass to undesirable out of plane

tilt directed about the x or y axes.

Page 133: G_O'Brien PhD Dissertation

116

Anchor

HubAnchors

Anchor Anchor

R0

Anchor

HubAnchors

Anchor Anchor

R0

Figure 5.26 Angular acceleration sensor interleaved inner and outer radial anchors.

Identical folded beam springs were interleaved in order to further compensate for any

photolithography induced rotation misalignment with respect to the SOI wafer flat. This

results in a self-aligned suspension spring design which is tolerant of silicon crystal plane

rotation misalignment due to symmetry about the sensor center of rotation as shown in

Figure 5.27.

The torsion spring constant is defined for two sets of N=3 springs for a beam spring

with a force moment applied to the tip resulting equivalent system described by Eq. 5.29.

3

3

22

21

2

_2 2LTEW

RRRK IN

SOI ⎟⎟⎠

⎞⎜⎜⎝

⎛ += (5.29)

The z-axis linear spring constant is defined for N=6 identical SOI springs independent

of substrate anchor attach point location with the resulting equivalent system described

by Eq. 5.30.

3

3

_ 43

LEWTK SOIZ = (5.30)

Page 134: G_O'Brien PhD Dissertation

117

Electrical Interconnect from Anchor to Bond Pad

R1

RIN

Electrical Interconnect from Anchor to Bond Pad

Electrical Interconnect from Anchor to Bond Pad

R1

RIN

Figure 5.27 Angular acceleration sensor identical spring dual radius interleave.

The SOI angular accelerometer capacitance change (ΔC/C0) as a function of linear

displacement (Δx) measured at the annulus outer disc radius (R2) is defined by Eq. 5.31.

320

3

0 xRRgxR

CC

Δ−Δ

=Δ (5.31)

The sensor capacitance sensitivity (ΔC/C0) as a function of angular acceleration (α) is

described for the SOI interleaved spring design by combining Eq. 5.1-5.3, Eq. 5.10-5.11,

and Eq. 5.29 into Eq. 5.31 as given by Eq. 5.32.

423

322

230

423

3

0 )( RRLRREWgRRL

CC

siIN

si

απραπρ

−+=

Δ (5.32)

Page 135: G_O'Brien PhD Dissertation

118

Capacitive sensitivity is plotted as a function of outer disc radius (R2) and suspension

beam spring length (L) in Figure 5.28. Comparison of Figures 5.13 and 5.28 illustrate the

small difference (less than 5% using typical sensor dimensions) existing between the

surface micromachined polysilicon and SOI angular accelerometer designs regarding

capacitance sensitivity. Similarly, the torsion modal frequencies for the micromachined

polysilicon and SOI angular accelerometer designs exhibit small model differences when

similar thickness (T) values are compared. The modal frequency directed about the z-

axis in torsion is defined by Eq. 5.22 and given by Eq. 5.33, where k’=K2R22.

Outer Disc Radius (R2) [m]

BeamSpring Length (L) [m]

%ΔC/C0

Outer Disc Radius (R2) [m]

BeamSpring Length (L) [m]

%ΔC/C0

Figure 5.28 SOI 20μm thick angular accelerometer ΔC/C0 sensitivity @ α=100r/s2.

si

in

LRREW

LRWf

πρπθ)(

2

21

2

22

+= (5.33)

The modal frequency directed linearly along the z-axis is given by Eq. 5.34.

Page 136: G_O'Brien PhD Dissertation

119

siz L

EWLRTf

πρπ3

4 2

= (5.34)

5.5.1 SOI Angular Accelerometer Basic Operation

The SOI angular acceleration sensor consists of four arrays of fixed beam electrodes

located around the disc perimeter. The fixed beam electrode arrays are configured in sets

of two to form the sensor clockwise and counter clockwise differential capacitance

(CCW,CCCW) and electrostatic self test (CST_CW) arrays as shown in Figure 5.29.

B Sub C ST2

CCCW CCW

CST_CW

CST_CCW

CCW

CST_CW

CST_CCW

CCCWArrayN=80

Self TestArrayN=10 Self Test

Array

SOI Electrical Interconnect Runners w/Anchors

Proof Mass Electrode (B)

CCW

CST_CW

CST_CCW

CCWArrayN=80

A ST1 B Sub C ST2

CCCW CCW

CST_CW

CST_CCW

CCW

CST_CW

CST_CCW

CCCWArrayN=80

Self TestArrayN=10 Self Test

Array

SOI Electrical Interconnect Runners w/Anchors

Proof Mass Electrode (B)

CCW

CST_CW

CST_CCW

CCWArrayN=80

CCWArrayN=80

A ST1

Figure 5.29 Angular acceleration sensor and bond pad schematic.

The sensor differential capacitance arrays have an initial electrostatic gap (g0) of 2μm

with two sets of N=80 beams symmetric about the clockwise and counterclockwise

semicircles. The capacitive electrodes extend beyond the proof mass disk radius (R2) to

the outer electrode radius (R3) as shown in Figure 5.30. The single sided capacitance of

the array is defined by Eq. 5.35, and given by Eq. 5.36 where θ represents the proof mass

disc displacement angle.

Page 137: G_O'Brien PhD Dissertation

120

Figure 5.30 SOI angular accelerometer capacitive array radial dimensions.

∫ −= 3

R

2R

)( drrg

TNC

o

o

θε

θ (5.35)

⎟⎟⎠

⎞⎜⎜⎝

⎛−−

=30

200 ln)(RgRgT

NCθθ

θε

θ (5.36)

The angular displacement (θ) can be linearly approximated at radial location R2 by Eq.

5.37.

2

2

RxΔ

=θ (5.37)

Capacitance can then be defined as a function of linear displacement by substituting

Eq. 5.37 into Eq.5.36 as given by Eq.5.38.

⎟⎟⎠

⎞⎜⎜⎝

⎛Δ−Δ−

Δ=Δ

3220

2220

2

202 ln)(

RxRgRxRg

xTR

NxCsε (5.38)

The linear displacement can be described in terms of angular acceleration (α) by

combining Eq. 5.1, 5.10, and 5.11 as given by Eq. 5.39.

Page 138: G_O'Brien PhD Dissertation

121

⎟⎟⎟⎟

⎜⎜⎜⎜

−=

2

3220

2202220 ln)(

RR

IRKg

IRKgI

RTKNCs

α

αα

εα (5.39)

The parallel plate capacitance approximation in terms of Δx2 and α are given by Eq.

5.40 and 5.41 respectively.

( )

3220

23202 )(

RxRgTRRR

NxC p Δ−−

=Δε (5.40)

( )

32220

232220)(

RIRKgTRRRK

NC p αε

α−

−= (5.41)

Capacitance for the angular and parallel plate models described by Eq. 5.39 and 5.41

respectively are plotted in Figure 5.31 versus angular acceleration (α) for a specific

design example with R3=1010μm, R2=850μm, L=200μm, T=20μm, W=2μm, and

g0=2μm.

1.5 .104 1 .104 5000 0 5000 1 .104 1.5 .104500

1000

1500

2000

2500

6

Electrostatic latch limit point (Δx≅0.45 g0)

CS

CP

InitialValue

Eq. 5.41

Eq. 5.39

Angular Acceleration α [r/s2]

Cap

acita

nce

[fF]

1.5 .104 1 .104 5000 0 5000 1 .104 1.5 .104500

1000

1500

2000

2500

6

1.5 .104 1 .104 5000 0 5000 1 .104 1.5 .104500

1000

1500

2000

2500

6

Electrostatic latch limit point (Δx≅0.45 g0)

CS

CP

InitialValue

Eq. 5.41

Eq. 5.39

Angular Acceleration α [r/s2]

Cap

acita

nce

[fF]

Figure 5.31 Sensor capacitance Vs applied angular acceleration (α).

Page 139: G_O'Brien PhD Dissertation

122

The capacitance can be considered linear over a small subset of the range limited to

+/- 2000r/s2 as shown in Figure 5.32 for this design example. The sensor capacitance

operation range is typically limited to the linear capacitance region to avoid non-linear

electronic signal conditioning.

CS

CP

InitialValue

Eq. 5.41

Eq. 5.39

Angular Acceleration α [r/s2]

Cap

acita

nce

[fF]

Linear CapacitanceAngular AccelerationRange (+/- 2000 [r/s2])

2000 1000 0 1000 20001000

1075

1150

1225

13000

0

CS

CP

InitialValue

Eq. 5.41

Eq. 5.39

Angular Acceleration α [r/s2]

Cap

acita

nce

[fF]

Linear CapacitanceAngular AccelerationRange (+/- 2000 [r/s2])

CS

CP

InitialValue

Eq. 5.41

Eq. 5.39

Angular Acceleration α [r/s2]

Cap

acita

nce

[fF]

Linear CapacitanceAngular AccelerationRange (+/- 2000 [r/s2])

2000 1000 0 1000 20001000

1075

1150

1225

13000

0

Figure 5.32 Linearized sensor capacitance Vs applied angular acceleration (α).

The potential energy (P.E.) for a parallel plate capacitor is defined by Eq. 5.42 where

V is the differential voltage maintained between parallel plates.

2

2 )(21.. VxCEP p Δ= (5.42)

Electrostatic force is generated by applying a differential voltage between a fixed and

proof mass electrode pair. The electrostatic force (FES) is described as a function of the

derivative of potential energy with respect to displacement Δx2 as defined by Eq. 5.43.

Page 140: G_O'Brien PhD Dissertation

123

2

22 )(

2 xdxdCVFES Δ

Δ= (5.43)

The electrostatic force for the angular capacitor model in terms of linear displacement

(Δx2) is described by combining Eq. 5.38 and 5.43 as given by Eq. 5.44.

2

2302

2202

223022202

0223

2

20_ ln1

))(())((

2V

xRgRxRgR

xxRgRxRgRgRRR

xTRNF SES ⎟

⎟⎠

⎞⎜⎜⎝

⎛⎟⎟⎠

⎞⎜⎜⎝

⎛Δ−Δ−

Δ−

Δ−Δ−−

Δ=

ε (5.44)

Similarly, the electrostatic force extracted from the parallel plate capacitor model in

terms of linear displacement (Δx2) is described by combining Eq. 5.40 and 5.43 as given

by Eq. 5.45.

2

23220

23320_ )(

)(2

VRxRg

RRRTRNF PES Δ−−

=ε (5.45)

The electrostatic force (FES) described by Eq. 5.43 can be equated to the folded beam

spring mechanical restoring force described by Eq. 5.11 and Eq. 5.29 as given by Eq.

5.46

2

22

2_2)(

2 xdxdCVxK SOI Δ

Δ=Δ (5.46)

Voltage can isolated from the equated mechanical restoring force and electrostatic

force as described by Eq. 5.47.

⎟⎟⎠

⎞⎜⎜⎝

⎛ΔΔ

Δ=

2

2

2_2

)(2

xdxdC

xKV SOI (5.47)

Page 141: G_O'Brien PhD Dissertation

124

Sensor capacitance was measured as a function of differential voltage applied to the

clockwise (CCW) array using an HP-4824A LCR meter connected to device bond pads via

wafer probe station micro-manipulator needles as shown in Figure 5.33.

PC

LCR Meter

ProbeStation

DUT

PC

LCR Meter

ProbeStation

DUT

Figure 5.33 Capacitive sensor C-V plot test equipment configuration.

A program generated in LabView was used to control the HP-4824A meter and

record measurements in computer spreadsheet format via the Hewlett Packard interface

bus (HPIB). The measured initial sensor capacitance value was 5% larger than the

theoretically predicted value. The 5% difference regarding empirical and theoretical

capacitance is attributed to process variation [113] in forming the initial dielectric gap

(g0) and electrostatic fringing [143] on the non-parallel surfaces between adjacent array

electrodes.

The predicted capacitance values described by Eq. 5.39 and 5.41 are plotted versus

voltage [152] using the relationship defined by Eq. 5.46 and compared to empirical data

as shown in Figure 5.34.

Page 142: G_O'Brien PhD Dissertation

125

0 0.2 0.4 0.6 0.81000

1200

1400

1600

18000 Electrostatic latch limit

point

CS

CP

C0

Eq. 5.41

Eq. 5.39

CCW Array Differential Voltage [V]

Cap

acita

nce

[fF]

Empirical

Theoretical0 0.2 0.4 0.6 0.8

1000

1200

1400

1600

18000 Electrostatic latch limit

point

CS

CP

C0

Eq. 5.41

Eq. 5.39

CCW Array Differential Voltage [V]

Cap

acita

nce

[fF]

Empirical

Theoretical0 0.2 0.4 0.6 0.8

1000

1200

1400

1600

18000 Electrostatic latch limit

point

CS

CP

C0

Eq. 5.41

Eq. 5.39

CCW Array Differential Voltage [V]

Cap

acita

nce

[fF]

Empirical

Theoretical

Figure 5.34 Capacitance-Voltage plot theoretical model comparison to empirical data.

Voltage applied to the Self-Test capacitive array causes electrostatic force to displace

the proof mass and is used to simulate an angular acceleration during normal sensor

operation. The excitation electrodes for both the Self-Test and CCW capacitance arrays

are electrically isolated as listed by nodes ST and C respectively in Figure 5.29. The

Self-test array consists 10 electrodes as shown in Figure 5.35.

Figure 5.35 Self-Test capacitance array (N=10 electrodes).

The voltage applied to the Self-Test capacitance array (N=10 electrodes) can be used

to cause an electrostatic angular displacement of the proof mass as a function of

Page 143: G_O'Brien PhD Dissertation

126

equivalent angular acceleration (α) by combining Eq. 5.41 and 5.47 as described by Eq.

5.48 and plotted in Figure 5.36.

( ) ( )233220

32220

2RRRTRN

IRIRKgV−

−=ε

αα (5.48)

0 2000 4000 6000 80000

0.5

1

1.5

2

Lat

Unstableregion

Stableregion

Electrostatic Latch Voltage

Angular Acceleration (α) [r/s2]

Self-

Test

Arr

ay V

olta

ge [V

]

0 2000 4000 6000 80000

0.5

1

1.5

2

Lat

Unstableregion

Stableregion

Electrostatic Latch Voltage

Angular Acceleration (α) [r/s2]

Self-

Test

Arr

ay V

olta

ge [V

]

Figure 5.36 Self-Test capacitance array applied voltage Vs angular acceleration (α).

Self-Test is enabled by applying a non-zero differential voltage, referenced to the

potential of the movable proof mass, to cause a rotational displacement in a

counterclockwise direction. The control chip contains a logic input pin to control the

voltage applied to the sensor self test array. Self-Test external input logic high is within

(2.6V-5.5V) and controls a buffered voltage source applied to the Self-Test array in the

range from (0.1-1.6V) in increments of 100mV using a 4 bit digital code written to the

control chip electrically-erasable-programmable-read-only-memory (EEPROM) cells

used for device trim and calibration. Self-Test external input logic low is within (0V-

2.2V) and controls a buffered voltage source equivalent to the proof mass node voltage

Page 144: G_O'Brien PhD Dissertation

127

resulting in a zero differential voltage between proof mass and fixed Self-Test array

electrodes.

5.5.2 SOI Angular Accelerometer Basic Signal Conditioning C-V Conversion

The capacitive sensor output is signal conditioned using a switched capacitor

complimentary metal oxide semiconductor (CMOS) control chip as described in Chapter

6. The control chip uses a 4 phase clock, as described in Chapter 6, to perform a singly

sampled sensor capacitance to voltage (C-V) conversion with 3 cascaded amplifiers in

series with the front end to provide signal gain and temperature compensation.

A simplified version of the switched capacitor front end is shown in Figure 5.37 using

a two phase clock to illustrate sensor C-V conversion. Gain greater than unity is present

in the front end is described by the ratio of the sensor capacitance difference to the

matched feedback capacitors (CF1=CF2=CF ). The transfer function for the simplified C-

V front end is given by Eq. 5.49.

F

CWCCWINAC C

CCVV −= (5.49)

Noting that the change in differential sensor capacitance is ΔC=(CCCW-CCW)/2 we can

further simplify the transfer function by substituting this relationship into Eq. 5.49 as

defined by Eq. 5.50.

FINAC C

CoCCVV0

2 Δ= (5.50)

The electromechanical transfer function for the first stage C-V conversion can now be

defined in terms of capacitive coupling using the mechanical input design parameters by

substituting Eq. 5.32 into Eq. 5.50 as given by Eq. 5.51.

Page 145: G_O'Brien PhD Dissertation

128

CCCW

CCW

VIN

A

B

C

VOS2

VOS1

Sensor

φ1

φ1

φ2

φ2

-

+

-

+

a

c

Vac

CF1

CF2

CCCW

CCW

VIN

A

B

C

VOS2

VOS1

Sensor

φ1

φ1

φ2

φ2

-

+

-

+

a

c

Vac

CF1

CF2

Figure 5.37 Simplified switched capacitor C-V front end.

⎟⎟⎠

⎞⎜⎜⎝

⎛−+

= 423

321

230

423

3

)(2)(

RRLRREWgRRL

CCoVV

siin

si

FINAC απρ

απρα (5.51)

The initial capacitance of the sensor (C0) is modeled by substituting Eq. 5.41 into Eq.

5.51 with the initial condition α=0 as given by Eq. 5.52.

⎟⎟⎠

⎞⎜⎜⎝

⎛−+⎟⎟

⎞⎜⎜⎝

⎛ −= 4

2332

123

0

423

3

0

230

)()(2)(

RRLRREWgRRL

gRRTN

CVV

siin

si

F

INAC απρ

απρεα (5.52)

The control chip nominal analog gain (AGAIN) was set to 75 with an offset of 2.5Volts.

Theoretical and empirical angular acceleration sensitivities were 11.8mV/r/s2 and

9.9mV/r/s2 respectively. This represents a 16% difference between the theoretical model

Page 146: G_O'Brien PhD Dissertation

129

and empirical sensor data. The final output of the control chip is described by Eq. 5.53

and plotted with empirical data versus applied angular acceleration in Figure 5.38.

5.2)()( += αα ACGAINOUT VAV (5.53)

200 150 100 50 0 50 100 150 2000

0.5

1

1.5

2

2.5

3

3.5

4

4.5

5

Angular Acceleration (α) [r/s2]

Vou

t[V]

Theoretical Sensitivity 11.8mV/r/s2

Empirical Sensitivity 9.9mV/r/s2

Eq. 5.52

200 150 100 50 0 50 100 150 2000

0.5

1

1.5

2

2.5

3

3.5

4

4.5

5

Angular Acceleration (α) [r/s2]

Vou

t[V]

Theoretical Sensitivity 11.8mV/r/s2

Empirical Sensitivity 9.9mV/r/s2

Eq. 5.52

Figure 5.38 Control chip voltage output Vs applied angular acceleration (α).

The control chip output root mean squared (RMS) noise was measured as 4.1mV

using an HP-34401 digital multi-meter. This noise measurement yields an empirical

resolution of 0.81r/s2 with a span of +/- 228r/s2 at operational amplifier upper and lower

rails set at 0.2-4.8VDC respectively with applied angular acceleration limited to a 100Hz

bandwidth. Brownian noise was calculated as 0.069 r/s2/rt-Hz [144] for a critically

damped part at standard room temperature and pressure, which is approximately four

times less than the measured angular acceleration sensor resolution in a 100Hz

bandwidth. The majority of the angular accelerometer system output noise is attributed

to the switched capacitor CMOS control chip. Additional noise is present due to the

parasitic capacitance due to the pad to pad wire bonds used to electrically interconnect

Page 147: G_O'Brien PhD Dissertation

130

the sensor and CMOS control chip. A picture of the dual sensor and control chip

interconnection in a 16 pin ceramic dual inline package (DIP) is shown in Figure 5.39.

Ceramic DIP

2mil Wire bonds

SOISensor

CMOS ControlChip

Ceramic DIP

2mil Wire bonds

SOISensor

CMOS ControlChip

Figure 5.39 Angular accelerometer two-chip interconnection top view.

5.5.3 Angular Accelerometer Finite Element Analysis Simulation Results

Finite element analysis (FEA) was used to compare theoretical model prediction and

empirical results of key angular accelerometer output variables as shown in Table 5.2.

Table 5.2 Angular accelerometer SOI model verification results. Parameter Empirical Theoretical FEA (ANSYS) % Diff 1 % Diff 2 % Diff 3K 2_SOI [N/m] 0.34 0.338 0.347 -0.6 2.0 -2.7

Kx [N/m] N/A N/A 1371 N/A N/A N/AKy [N/m] N/A N/A 997 N/A N/A N/AKz [N/m] N/A 240 243 N/A N/A -1.3F θ [Hz] 431 402 412 -7.2 -4.6 -2.5Fz [kHz] 10.8 8.8 10.2 -22.7 -5.9 -15.9

V Latch [VDC] 0.65-0.70 0.72 N/A 2.8 N/A N/AI [m4] N/A 3.82E-14 3.76E-14 N/A N/A 1.6m [kg] N/A 1.06E-07 9.43E-08 N/A N/A 11.0W [μm] 2L [μm] 200 Description EquationT [μm] 20g 0 [μm] 2 % Diff 1 = 100*( Theo.-Emp.)/Theo.R 0 [μm] 50R 1 [μm] 300 % Diff 2 = 100*(FEA - Emp.)/FEAR 2 [μm] 850R 3 [μm] 1010 % Diff 3 = 100*(Theo. - FEA)/Theo.

Page 148: G_O'Brien PhD Dissertation

131

The major output parameter defining angular acceleration sensor performance is

defined by torsion spring constant parameter K2_SOI as given by Eq. 5.29. The FEA

simulation results for system outputs K2_SOI, KX, KY, KZ, Fθ, and FZ are compared to both

empirical and theoretical data as shown in Table 5.2.

FEA modeling was performed by converting the angular accelerometer mask layout

geometry directly into ANSYS format, extruded 20 microns along the z-axis, and meshed

using SOLID92 elements as shown in Figure 5.40.

MeshedSensor LayoutMeshedSensor Layout

Figure 5.40 ANSYS angular acceleration sensor meshed solid model.

Modal analysis was used to identify the natural frequencies associated with motion

directed about (FθZ) and along (FZ) the z-axis as shown in Table 5.3.

The largest output parameter difference (-15.9%) observed between theoretical model

and FEA simulation results is referenced to the modal frequency directed along the z-

axis. The theoretical model is based on linear beam theory accounts only for

displacement directed along the z-axis. Slightly off-axis displacement was observed in

the folded beam springs for proof mass displacement due to linear acceleration directed

along the z-axis.

Page 149: G_O'Brien PhD Dissertation

132

Table 5.3 ANSYS modal frequency simulation results.

1) FθZ

4) FZ

1) FθZ

4) FZ

This complex out-of-plane spring torsion is illustrated using a simplified ANSYS

simulation with the anchors and inner ring structural lattice beams removed to allow

viewing of folded beam spring deflection as shown in Figure 5.41.

Figure 5.41 Displacement simulation of proof mass using z-axis linear acceleration.

Seismic mass displacement about the z-axis due to an applied angular acceleration

results in beam spring deflection confined to the x-y plane, as shown in Figure 5.42.

Page 150: G_O'Brien PhD Dissertation

133

Figure 5.42 Beam spring deflection due to angular acceleration directed about z-axis.

The x-y plane confined beam spring displacement is well described by the linear

beam theoretical model regarding the parameter K2_SOI as reflected in the 2.7% difference

when compared to ANSYS simulation results as listed in Table 5.2.

5.6 Angular Acceleration Sensor Summary

Building blocks of the angular rate sensor research described in Chapter 4 were used

to form a surface micromachined polysilicon angular accelerometer. Process stiction

observed during the wet HF based sacrificial oxide etch proved to be a significant yield

problem. Stiction was avoided on the angular acceleration sensors, fabricated in 2μm

thick polysilicon structural film, by performing critical point drying using CO2 [146] as

described in Appendix B. Although critical point drying is very effective at eliminating

stiction on a single wafer basis geared primarily towards research efforts, this process is

not currently provided by semiconductor equipment vendors for high volume MEMS

silicon wafer production. As a result, an angular acceleration sensor design change was

necessary to harden the device against stiction using standard wet HF sacrificial oxide

etch processes.

Page 151: G_O'Brien PhD Dissertation

134

Increased mechanical film thickness is a significant design input parameter which

reduces process stiction in MEMS devices by increasing the seismic mass mechanical

spring constant directed along the z-axis normal to the wafer plane. Theoretical models

indicate that capacitive sensitivity and torsion mode natural frequency are both

independent of the sensor structural film thickness. Design scaling with existing

theoretical models was used to identify 20μm as a robust mechanical film thickness.

Polysilicon films are typically limited to less than 5μm due to intrinsic film stress.

However, SOI structural films are typically available in thickness ranging from sub-

micron to several hundreds of microns. As a result, SOI substrates were used to fabricate

the second generation angular acceleration sensors.

Design conversion from polysilcon to SOI single crystal structural film included an

interleaved spring design. The interleaved spring design compensates for the crystal

orientation dependence of the Young’s moduli via radial placement symmetry of the

suspension beams. In addition, the interleaved spring design is tolerant of both

photolithography and silicon wafer flat rotational misalignment with respect to the actual

crystal plane orientations.

Theoretical models describing capacitive sensitivity as a function of applied angular

acceleration were provided using polar and Cartesian coordinates. The two models are

compared and observed to yield quite similar results over the region of angular

acceleration interest as shown in Figure 5.32. While the polar coordinate based capacitor

model is more accurate the Cartesian coordinate based capacitor model, its derivatives

are significantly more cumbersome regarding manual design performance prediction.

The Cartesian coordinate based parallel plate capacitor model is more compact and

allows the designer clearer insight into key design performance input parameters. Both

capacitor models are compared to empirical results of an angular acceleration sensor as

Page 152: G_O'Brien PhD Dissertation

135

shown in Figure 5.34. The empirical capacitance was swept as a function of applied

voltage [152] with observed overall trends well described by both theoretical models.

Initial sensor capacitance was 6.9% larger than predicted by the theoretical capacitor

model and is attributed to fringing electric fields [143] in the sensor vicinity. A

derivative of the parallel plate capacitance model was used to calculate the electrostatic

latch voltage of 1.7VDC regarding Self-Test capacitive array (N=10) as plotted in Figure

5.36. Similarly, the electrostatic latch voltage of the CCW and CCCW sensor capacitance

arrays (N=80) were observed to latch in between the range of 0.65-0.70VDC with a

theoretical model prediction of 0.72VDC as listed in Table 5.2.

A simplified switched capacitor signal conditioning circuit was presented to illustrate

sensor capacitance to CMOS control chip voltage conversion. A theoretical

electromechanical model describing the control chip output voltage as a function of

applied angular acceleration is compared to empirical results with a 16% difference

observed as shown in Figure 5.38. The control chip output root mean squared (RMS)

noise was measured as 4.1mV yielding an empirical resolution of 0.81r/s2 with a span of

+/- 228r/s2 at operational amplifier upper and lower rails set at 0.2-4.8VDC respectively

with applied angular acceleration limited to a 100Hz bandwidth as shown in Table 5.4.

Table 5.4 Commercial and research prototype angular accelerometer performance. Sensitivity Resolution Span Bandwidth Current

Company [mV/r/s2] [r/s2] +/- [r/s2] [Hz] [mA]Delphi 4 5 500, 2000 250,500 5ST Micro. 10 2.5 200 800 26*Motorola 10 0.8 228 100 4.3*Research Prototypes Only

Brownian noise was calculated as 0.069 r/s2/rt-Hz [144] for a critically damped part

at standard room temperature and pressure, which is approximately four times less than

Page 153: G_O'Brien PhD Dissertation

136

the measured angular acceleration sensor resolution in a 100Hz bandwidth. The majority

of the angular accelerometer system output noise is attributed to the switched capacitor

CMOS control chip described in Chapter 6.

Finite element analysis performed using ANSYS software was used to verify

theoretical model prediction of key angular accelerometer output variables K2_SOI, KX, KY,

KZ, Fθ, and FZ. The key output variable used throughout theoretical model prediction was

K2_SOI. Theoretical model and FEA simulation prediction of the key output variable

K2_SOI was compared to empirical results with a –0.6 and 2.0 %Difference listed in table

5.2. The small difference observed between empirical, theoretical, and FEA simulation

results increase confidence regarding angular acceleration sensor theoretical model

prediction. Future angular acceleration design iterations, beyond the scope of this thesis,

will be required to further characterize and improve the presented theoretical models.

Page 154: G_O'Brien PhD Dissertation

137

CHAPTER 6

CMOS SWITCHED CAPACITOR SIGNAL CONDITIONING

An analog front end design is presented using switched capacitor design techniques to

provide electronic signal conditioning of variable capacitance MEMS angular

acceleration and rate sensors. The presented front end design rejects both high and low

frequency noise injected at the excitation voltage node via a novel common mode

differential charge redistribution sensing scheme. The main clock is designed to operate

at a frequency of 480kHz and consists of four phases per charge-to-voltage conversion

cycle regarding front end signal conditioning. Charge redistribution is used prior to

analog signal amplification allowing for a reduced number of operational amplifiers

required in the front end.

6.1 Front End Architecture

A switched capacitor architecture [123] is used to sample charge injected onto a

MEMS based differential capacitance acceleration sensor. The sensor is interfaced with a

CMOS charge summing front end prior to first stage amplification. The charge

difference between the top and bottom capacitive acceleration sensor nodes is summed

and added to the DC offset voltage induced charge at the input to the first stage amplifier

as shown in Figure 6.1. The transfer function describing the voltage measured at the

sample and hold output node is given by Eq. 6.1.

( ) ⎟⎟⎠

⎞⎜⎜⎝

⎛+⎟

⎟⎠

⎞⎜⎜⎝

+++

−++

+−=

1

5

1

4

41

3

3 FFPBB

PBB

FPTtop

PTtop

CC

VoffsetCC

CCCCC

CC

CCCCC

VinVosVout (6.1)

Page 155: G_O'Brien PhD Dissertation

138

C3

C4

C5

CF1

CPT

CPB

Vin

VoffsetVos

Vout

Cbot

Ctop

V-

V+

C3

C4

C5

CF1

CPT

CPB

Vin

VoffsetVos

Vout

Cbot

Ctop

V-

V+

Figure 6.1 Switched capacitor front end top level schematic.

The capacitors CPB and CPT represent the parasitic capacitance present at the top and

bottom sensor nodes due to bond pads and electrical interconnect traces. The transfer

function can be simplified by matching the gain capacitors CPB and CPT to each other

given by Eq. 6.2.

PPTPB CCC == (6.2)

Similarly, the transfer function can be further simplified by matching the gain

capacitors C3 and C4 to each other given by Eq. 6.3.

SCCC == 43 (6.3)

Page 156: G_O'Brien PhD Dissertation

139

The sampling gain capacitor value (CS) is set to the parallel combination of the initial

sensor and parasitic capacitances as given by Eq. 6.4 where the initial capacitance (C0) is

approximated using Eq. 6.5.

0CCC PS += (6.4)

200

0bt CC

C+

= (6.5)

Finally, we combine Eq. 6.1 through Eq. 6.5 as given by Eq. 6.6.

( ) ⎟⎟⎠

⎞⎜⎜⎝

⎛+⎟⎟

⎞⎜⎜⎝

++

−−≅

1

5

12

0 )()(

FF

S

SP

bottops

CC

VoffsetCC

CCCCCC

VinVosVout (6.6)

The sensor capacitance change with increasing top capacitance and decreasing

bottom capacitance is given by Eq. (6.7) and Eq. (6.8) respectively.

CCC ttop Δ+= 0 (6.7)

CCC bbot Δ−= 0 (6.8)

The simplified function is given by Eq. 6.9.

( ) ⎟⎟⎠

⎞⎜⎜⎝

⎛+⎟⎟

⎞⎜⎜⎝

++Δ

−≅1

5

1

2

20 )(

)(2

FF

S

SP CC

VoffsetCC

CCCCVinVosVout (6.9)

Page 157: G_O'Brien PhD Dissertation

140

Further simplification is possible by substituting Eq. 6.4 into Eq. 6.9 and setting the

integration feedback capacitor CF1 equal to the initial sensor capacitance C0 described by

Eq. 6.10.

( ) ⎟⎟⎠

⎞⎜⎜⎝

⎛+⎟⎟

⎞⎜⎜⎝

⎛ Δ−≅

1

5

02 FCC

VoffsetCCVinVosVout (6.10)

Final simplification is achieved by setting Vin to analog ground and C5 equal to CF1 is

described by Eq. 6.11.

VoffsetCCVosVout +⎟⎟

⎞⎜⎜⎝

⎛ Δ≅

02 (6.11)

6.2 Front End Capacitive Sensor Charge Redistribution

The sensor is comprised of two variable capacitors with near identical initial

condition values. Inertial excitation causes the sensor spring suspended seismic mass to

displace from its initial at-rest state. This seismic mass displacement causes one

capacitor to increase while the other decreases at a similar rate. This change in

capacitance can also be described by charge redistribution.

The switched capacitor front end utilizes charge redistribution to convert the sensor

output from differential to single ended during the first three clock phases as shown in

Figure 6.2.

Page 158: G_O'Brien PhD Dissertation

141

+VosC3 C4

Ctop Cpt Cbot CpbCtop Cpt Cbot Cpb

+VosC3 C4

Qbot-Qtop

Phase 0 Phase 1 Phase 2

+ + + ++VosC3 C4

Ctop Cpt Cbot CpbCtop Cpt Cbot Cpb

+VosC3 C4

Qbot-Qtop

Phase 0 Phase 1 Phase 2

+ + + +

Figure 6.2 Phases 0-2 front end charge distribution.

Clock Phase 0

The variable sensor and parasitic capacitors are shorted to voltage Vin (where Vin=

analog ground) during phase 0 which represents sensor charge reset.

Clock Phase 1

The top portion of the sensor is charged to the opamp offset voltage (Vos) based on

the parallel combination of Ctop and Cpt added in series with C3, (C3= Ctb). Similarly, the

bottom portion of the sensor is charged to the opamp offset voltage (Vos) based on the

parallel combination of Cbot and Cpb added in series with C4, (C4= Csb)

Clock Phase 2

The charge on the top sense capacitor (C3=Cst) is connected with opposite polarity to

the bottom sense capacitor (C4=Csb). If the capacitors are matched (C3=C4) the output

voltage is a function of the difference between the Phase 1 charges.

Clock Phase 3

This phase is used to charge the sample-and-hold capacitor (Ch) to the operational

amplifier output voltage.

Page 159: G_O'Brien PhD Dissertation

142

The offset charge redistribution block adds a net charge to the summed sensor charge

to maintain a single valued polarity for all possible capacitive sensor values. Detail of the

clocked signals applied to transmission gates controlling the charge re-distribution

portion of the switched capacitor front end is shown in Figure 6.3. A transmission gate

sub-circuit [123] is shown in Figure 6.4.

C3

C4

C5

Sensor

CF1

Ctop

Cbot

Cpb

Cpt

Voffset

V-

V+

Q TOP

Vos

Vin

Vin

Q BOTTOM

Q OFFSET

C3

C4

C5

Sensor

CF1

Ctop

Cbot

Cpb

Cpt

Voffset

V-

V+

Q TOP

Vos

Vin

Vin

Q BOTTOM

Q OFFSET

Figure 6.3. Transmission gate charge re-distribution clock phase detail.

Page 160: G_O'Brien PhD Dissertation

143

ClockInput(Ctrl)

InputNode

OuputNode

ClockInput(Ctrl)

InputNode

OuputNode

Figure 6.4 Basic transmission gate schematic sub-circuit (T-gate7).

6.3 Theoretical Calculation and SPICE Simulation Result Comparison

The circuit was simulated using PSpice software with a four phase clock extracted

from the 480kHz main clock frequency. The transient simulation results are compared to

theoretical calculations using Eq. 6.1 as listed in Table 6.1 with a 2.5V offset reference.

Table 6.1 Simulated Vs theoretical sample and hold stage output voltage. Vos Vin Voffset Ct Cb Vout(sim) Vout(theo) ΔC ΔV (sim) ΔV (theo) % Diff

2 0 2.5 0.35 0.45 2.3619 2.3583 0.050 -0.1390 -0.1417 1.9%2 0 2.5 0.4 0.4 2.5009 2.5000 0.000 0.0000 0.0000 0.0%2 0 2.5 0.41 0.39 2.5287 2.5283 -0.010 0.0278 0.0283 1.9%2 0 2.5 0.42 0.38 2.5564 0.0567 -0.020 0.0555 0.0567 2.1%2 0 2.5 0.43 0.37 2.584 2.5850 -0.030 0.0831 0.0850 2.3%2 0 2.5 0.45 0.35 2.6398 2.6389 -0.050 0.1389 0.1417 2.0%

The difference between the theoretical model defined by Eq. 6.1 and simulated output

node voltage was on the order of 2%. The simulated and theoretical sample-and-hold

stage was observed to be relatively linear over the maximum sensor operation range

represented by a ΔC/C0 of (+/-) 0-12% referenced to an initial capacitance of 400fF. The

first stage voltage output simulated at the sample and hold node is shown in Figure 6.5.

Page 161: G_O'Brien PhD Dissertation

144

Vout [V] Vs ΔC [pF]

-0.2

-0.15

-0.1

-0.05

0

0.05

0.1

0.15

0.2

-0.06 -0.04 -0.02 0 0.02 0.04 0.06

ΔC Sensor [pF]

ΔV

Out

put [

V]

Vos=2V

Vos=1V

Vout [V] Vs ΔC [pF]

-0.2

-0.15

-0.1

-0.05

0

0.05

0.1

0.15

0.2

-0.06 -0.04 -0.02 0 0.02 0.04 0.06

ΔC Sensor [pF]

ΔV

Out

put [

V]

Vos=2V

Vos=1V

Figure 6.5 First stage capacitance to voltage (C to V) transconduction slope.

The switched capacitor front end bandwidth [153] was calculated as 60kHz for an

8.3μs clocked sample cycle time using the Nyquist limit [154] for the four phase 480kHz

main clock frequency. Simulation of the front end was performed using a sinusoidal 1%

ΔC/C0 to represent transient sensor operation from 100Hz - 2kHz as shown in Figure 6.6.

Ti me

0 s 0 . 2 ms 0 . 4 ms 0 . 6 ms 0 . 8 ms 1 . 0 ms 1 . 2 ms 1 . 4 ms 1 . 6 ms 1 . 8 ms 2 . 0 msV( o u t _ f i n a l )

2 . 4 V

2 . 5 V

2 . 6 V

2 . 7 V

100 [Hz]

500 [Hz]2000 [Hz] 1000 [Hz]

Ti me

0 s 0 . 2 ms 0 . 4 ms 0 . 6 ms 0 . 8 ms 1 . 0 ms 1 . 2 ms 1 . 4 ms 1 . 6 ms 1 . 8 ms 2 . 0 msV( o u t _ f i n a l )

2 . 4 V

2 . 5 V

2 . 6 V

2 . 7 V

100 [Hz]

500 [Hz]2000 [Hz] 1000 [Hz]

Ti me

0 s 0 . 2 ms 0 . 4 ms 0 . 6 ms 0 . 8 ms 1 . 0 ms 1 . 2 ms 1 . 4 ms 1 . 6 ms 1 . 8 ms 2 . 0 msV( o u t _ f i n a l )

2 . 4 V

2 . 5 V

2 . 6 V

2 . 7 V

100 [Hz]

500 [Hz]2000 [Hz] 1000 [Hz]

Figure 6.6. Front end sample-and-hold voltage output for a sinusoidal 1% ΔC/C0.

Page 162: G_O'Brien PhD Dissertation

145

6.4 CMOS Control Chip Top Level Overview

A CMOS control chip functional block diagram has been previously demonstrated

[48] for use with automotive capacitive acceleration sensors. The charge redistribution

portion of the CMOS control chip functional block diagram providing capacitance to

voltage (C to V) conversion and trimmed offset voltage is shown in Figure 6.7. This

portion of the original design was modified to include a similar charge redistribution

scheme as described in section 6.2. A top level schematic of the analog signal path is

shown in Figure 6.8 with the 4 pole Bessel filter omitted. A switched capacitor low pass

filter with analog gain which could be used to replace the Bessel filter in future designs as

described in Appendix D. The analog signal path output voltage is described by Eq. 6.12.

( ) ( )⎟⎟⎠

⎞⎜⎜⎝

⎛ +⎟⎟

⎜⎜

⎛+⎟

⎟⎠

⎞⎜⎜⎝

+++

−++

+−=

32

332

1

5

1

4

41

3

3

3_RC

RRCCC

VoffsetCC

CCCCC

CC

CCCCC

VinVosVoutF

BAS

FFPBB

PBB

FPTtop

PTtop (6.12)

CapacitiveSensor

Charge RedistributionFront End

InertiaCtop

Cbot

CapacitiveSensor

Charge RedistributionFront End

InertiaCtop

Cbot

Figure 6.7. CMOS control chip functional block diagram.

Page 163: G_O'Brien PhD Dissertation

146

C3

C4

C5

CF1

Cpt

Cbt

Vin

Ctop

Cbot

Vout_1

Vout_3CS2

CF2 R3A R3BR3

CH2 CH3

C3

C4

C5

CF1

Cpt

Cbt

Vin

Ctop

Cbot

Vout_1

Vout_3CS2

CF2 R3A R3BR3

CH2 CH3

Figure 6.8. CMOS control chip analog signal path top level schematic.

Surface micromachined capacitive angular acceleration sensors, as described in

Chapter 5, were electrically interfaced to the CMOS control chips using 2mil wire bonds.

Electrical interconnection between the CMOS control chip and ceramic dip (cerdip) pins

were made using 1mil wire bonds. Both the sensor and CMOS control chip were

adhesively attached to the ceramic dip as shown in Figure 6.9.

Page 164: G_O'Brien PhD Dissertation

147

Figure 6.9. CMOS control chip interfaced to capacitive angular acceleration sensor

6.5 CMOS Signal Conditioned Angular Accelerometer Electrical Output

The CMOS control chip was connected to a 5V power supply with a measured chip

current draw of 4.3mA. Control chip offset voltage was manually trimmed to provide a

2.52V output reference. The electrical output voltage of the CMOS control chip was

measured using a Tektronix digital oscilloscope with a zero acceleration input (rest state)

over a 1 second interval at a sampling rate of 1kHz as plotted in Figure 6.10.

Angular acceleration was applied to the sensor with a peak amplitude of 40r/s2 using

a sinusoidal 2Hz oscillation frequency. Output voltage measurements with angular

acceleration excitation applied over a 1 second period are plotted in Figure 6.11. The

CMOS control chip output angular acceleration sensitivity was measured as 1.9mV/r/s2.

Full scale span was calculated as (+/-) 1260r/s2 using output amplifier high and low rails

conservatively estimated at 4.9V and 0.1V respectively. Angular acceleration resolution

was calculated as 2.3r/s2 using the measured noise and sensitivity.

Page 165: G_O'Brien PhD Dissertation

148

Figure 6.10 CMOS control chip output voltage reference (Noise = 4.3mVRMS).

Figure 6.11 Output voltage measurement for sinusoidal 40r/s2 input.

The angular acceleration test configuration consists of an oscillating aluminum arm

which pivots up to 15 degrees about an automotive wheel bearing mounted to a stationary

table as shown in Figure 6.12. An eccentric cam is used to convert the unidirectional

motor input into a sinusoidal motion via an arm linkage equipped with end attached

Page 166: G_O'Brien PhD Dissertation

149

bearings. The variable drive speed motor is rated up to 5000rpm requiring a step down

transmission be included to decrease arm oscillation speed while increasing available

drive torque. An angular rate signal reference is available from an automotive grade

quartz gyroscope attached to the arm end point as shown in Figure 6.13.

DigitalOscilloscope

RateTable

BearingSensor TestBoard

RateTable

Sensor

DigitalOscilloscope

RateTable

BearingSensor TestBoard

RateTable

Sensor

Figure 6.12 Angular rate table test equipment configuration.

Motor

Rear View

ReferenceGyroscope

ArmMotion

ArmLinkage

Top View

Motor

Rear View

ReferenceGyroscope

ArmMotion

ArmLinkage

Top View

Figure 6.13 Eccentric cam sinusoidal arm linkage with motor driven transmission.

6.6 CMOS Signal Conditioned Angular Acceleration Sensor Summary

Switched capacitor based charge redistribution was used to convert the sensor

differential output into a single ended output prior to front end integration. The top and

Page 167: G_O'Brien PhD Dissertation

150

bottom sensor capacitive plates are charged, sampled, and discharged in parallel.

Additionally, the sensor charge and discharge cycles are provided by single node voltage

sources allowing for common mode noise cancellation at the sensor [153]. Offset charge

was added to guarantee the combination of charge from the top and bottom sensor

capacitive plates would maintain a constant polarity over the angular acceleration sensor

full scale span range. The offset charge also facilitates trimming of the output voltage to

half the full scale output as an offset reference. Offset voltage was measured on a CMOS

control chip output, interfaced to a surface micromachined angular accelerometer via

wire bonds, as 2.52V with 4.3mVRMS of noise. The sensor was excited using a 40r/s2

peak amplitude yielding a measured sensitivity of 1.9mV/r/s2. Angular acceleration

sensor resolution was calculated as 2.3r/s2 using the measured noise and sensitivity

measurements.

Parasitic capacitance due to sensor and CMOS chip integration is estimated at 3pF as

referenced from the sensor bond pad nodes to analog ground. The primary parasitic

capacitance mechanisms are attributed to the large areas consumed by conductive wire

bond pads and polysilicon interconnection traces required to electrically interconnect the

sensor. Presently, the CMOS control chip output signal voltage amplitude is reduced by

a multiplication factor of 2.4 when compared to a null parasitic capacitance condition as

modeled by Eq. 6.12. While complete nulling of parasitic capacitance is not practical, a

reduction from 3pF to 0.3pF would yield an increase in voltage signal output by a

multiplication factor of 2.2. Smaller bond pad areas and thicker dielectrics between

sensor electrical interconnections and the underlying conductive substrate are effective

design methods to reduce parasitic capacitance. Two additional design methods which

can reduce signal conditioned voltage output sensitivity to parasitic capacitance are to

increase the sensor capacitance by using thicker structural films and to integrate the

CMOS signal conditioning circuitry on the same chip. Sensor structural films in excess

Page 168: G_O'Brien PhD Dissertation

151

of 20μm have been realized using SOI substrates effectively increasing sensor

capacitance as thickness is increased while parasitic capacitance remains fixed. Single

chip integration of sensor and signal conditioning electronics [2, 3] eliminates long

polysilicon electrical interconnections, bond pads, and wire bonds between sensor output

nodes and CMOS signal conditioning electronics. The SOI process flow described in

Chapter 7 could be modified to satisfy CMOS integrated circuit compatibility regarding

single chip sensor realization.

Page 169: G_O'Brien PhD Dissertation

152

CHAPTER 7

SOI SENSOR FABRICATION PROCESS FLOWS

Surface micromachining using polysilicon as a structural material [155-157] has

traditionally been limited to a deposition thickness of less than 5μm in order to minimize

film stress [140]. Excessive thin film stress can result in either bowing or buckling of

structures such as beam spring suspensions mechanically anchored to the substrate [158,

159]. In-situ doped single crystal silicon provides a virtually stress free mechanical film

for use in MEMS device applications [148, 160]. However, single crystal silicon wafers

heavily doped with boron at a surface concentration of 1020cm-3 have been previously

observed to induce a non-zero tip deflection regarding 3μm thick cantilevered beams

[161] released using ethylene diamine pyrocatechol (EDP). Although an accelerometer

has been fabricated using a boron etch stop process without any observed stress related

problems [162], a stress free structural film with mechanical properties superior to

polysilicon is desired.

This chapter describes two process flows used to fabricate MEMS capacitive

acceleration sensors on SOI substrates. The short SOI flow describes a minimized

number of process steps to realize a sensor with electrically isolated mechanical anchors.

The integrated SOI flow includes deep reactive ion etch (DRIE) with subsequent

trench refill using low pressure chemical vapor deposition (LPCVD) of conformal films

[63] typically used in the fabrication of CMOS integrated circuits. Multiple trench refill

steps deposit conductive and non-conductive conformal films to provide selective handle

wafer substrate electrical contact and mechanical anchor electrical insulation

respectively.

Page 170: G_O'Brien PhD Dissertation

153

7.1 SOI Sensor Mechanical Anchor Fabrication Fundamentals

SOI provides mechanical film properties superior to polysilicon with the addition of a

buried oxide (BOX) layer. The BOX can be used as a built in release layer for MEMS

devices fabricated in SOI using a single mask process to define the sensor structural

outline. Sacrificial etching of the BOX is performed using hydrofluoric (HF) acid [163,

164]. A timed HF etch is typically used to release the device using large laterally etched

areas to form electrically insulated mechanical substrate anchors due to incomplete BOX

removal, as shown in Figure 7.1.

B B

View B-B

SOI

Si Substrate

Oxide Anchor

Top View TimeDependentIsotropic Oxide EtchUndercut (HF)

SOI

Si Substrate

Side View

MEMSCantileverBeam

B B

View B-B

SOI

Si Substrate

Oxide Anchor

Top View TimeDependentIsotropic Oxide EtchUndercut (HF)

SOI

Si Substrate

Side View

MEMSCantileverBeam

Figure 7.1 Typical SOI MEMS mechanical BOX attached anchor.

The BOX defined anchor cross sectional area is a function of the layout defined

anchor perimeter, sacrificial oxide lateral undercut etch rate, and etch duration. The

timed etch process step requires the HF concentration and temperature be tightly

controlled in order to minimize the BOX etch rate variation distributed over multiple

Page 171: G_O'Brien PhD Dissertation

154

wafer lots. Agitation of HF during sacrificial BOX etch is typically used to reduce

localized oxide etch variation as a function of wafer location.

7.2 Short SOI Process Flow

The short SOI process flow substrate anchor is mechanically connected to the handle

wafer via the buried oxide (BOX) which remains post sacrificial oxide HF etch as

previously shown in Figure 7.1. Design rules were formulated to differentiate between

mechanically anchored and released structures using a timed wet HF sacrificial BOX

etch. The SOI sensor outline was trenched by a photolithography defined deep reactive

ion etch (DRIE) with input/output parameters defined in Appendix C. The conservative

design rule for a mechanically released beam requires a maximum cross section of 8μm

while the anchor design rule requires a minimum cross section of 32μm to ensure that a

robust amount of residual BOX exists post HF etch as shown in Figure 7.2.

The short SOI process consists of two masks. The first mask and photoresist step is

used to define the bond pad metal area using a lift-off technique [165]. The second mask

and photoresist step is used to define the sensor outline regarding deep reactive ion

etching. The final step involves sacrificial oxide etch in aqueous HF to release the device

as shown in Figure 7.3.

Page 172: G_O'Brien PhD Dissertation

155

Handle Wafer (525μm Thick)

SOI (20μm Thick)

BOX (2μm Thick)

Pre Sacrificial Oxide Etch

Handle Wafer (525μm Thick)

SOI (20μm Thick)

BOX

32μm

Post Sacrificial Oxide Etch

8μm

Lateral Undercut (> 4μm)

AnchorReleasedBeam

Handle Wafer (525μm Thick)

SOI (20μm Thick)

BOX (2μm Thick)

Pre Sacrificial Oxide Etch

Handle Wafer (525μm Thick)

SOI (20μm Thick)

BOX

32μm

Post Sacrificial Oxide Etch

8μm

Lateral Undercut (> 4μm)

Handle Wafer (525μm Thick)

SOI (20μm Thick)

BOX (2μm Thick)

Pre Sacrificial Oxide Etch

Handle Wafer (525μm Thick)

SOI (20μm Thick)

BOX

32μm

Post Sacrificial Oxide Etch

8μm

Lateral Undercut (> 4μm)

AnchorReleasedBeam

Figure 7.2 Short SOI process flow DRIE trench defined BOX anchor cross section.

SOI

Si Substrate

Cr-Au Metal

SOI

Si Substrate

BondPad

Si Substrate

ReleasedDevice

1) Metal deposition and Lift-Off

2) Sensor outline DRIE

3) Aqueous HF BOX etch

Mask 1

Mask 2

SOI

Si Substrate

Cr-Au Metal

SOI

Si Substrate

BondPad

Si Substrate

ReleasedDevice

1) Metal deposition and Lift-Off

2) Sensor outline DRIE

3) Aqueous HF BOX etch

Mask 1

Mask 2

SOI

Si Substrate

Cr-Au Metal

SOI

Si Substrate

BondPad

Si Substrate

ReleasedDevice

1) Metal deposition and Lift-Off

2) Sensor outline DRIE

3) Aqueous HF BOX etch

Mask 1

Mask 2

SOI

Si Substrate

Cr-Au Metal

SOI

Si Substrate

BondPad

Si Substrate

ReleasedDevice

1) Metal deposition and Lift-Off

2) Sensor outline DRIE

3) Aqueous HF BOX etch

Mask 1

Mask 2

Figure 7.3 Short SOI process flow released device and bond pad cross section.

Page 173: G_O'Brien PhD Dissertation

156

7.2.1 Clear Field Sensor Perimeter Fabrication

Clear field refers to the perimeter of silicon surrounding the sensor. Clear field

perimeter angular accelerometers fabricated using the short SOI process flow are shown

in Figure 7.4. The large gap between the sensor fixed electrodes and rectangular SOI

perimeter reduces the parasitic sidewall capacitance by more than an order of magnitude.

ClearFieldPerimeter

SOI

SOI Etched

SOI

ClearFieldPerimeter

SOI

SOI Etched

SOI

Figure 7.4. Clear field perimeter SOI short process flow angular acceleration sensors

Long electrical interconnect beams are used to electrically interconnect the sensor

capacitive electrodes to the corresponding bond pads. The electrical interconnect beams

are 4μm wide and 20μm thick with multiple anchors placed on long runs and corner

transitions. The anchors support the interconnect beams above the silicon substrate post

sacrificial oxide etch as shown in Figure 7.5.

Page 174: G_O'Brien PhD Dissertation

157

Anchor

FixedElectrode

Bond Pad Interconnect

Anchor

FixedElectrode

Bond Pad Interconnect

Figure 7.5 Bond pad interconnect beam anchor electrical isolation from substrate.

Termination of the electrical interconnect beams occurring at sensor bond pads

patterned with Cr-Au metal is shown in Figure 7.6.

Metal(CrAu)

Bond Pads

Metal(CrAu)

Bond Pads

Figure 7.6 Bond pad metal and interconnect beam detail.

7.2.2 Dark Field Sensor Perimeter Fabrication

Dark field perimeter is described by a single continuous frame of SOI within

proximity of the sensor. Trench width located between the sensor fixed electrodes and

dark field perimeter are typically on the order of 2μm. Both clear and dark field designs

can be fabricated side by side on the same wafer as shown in Figure 7.7.

Page 175: G_O'Brien PhD Dissertation

158

ClearField Perimeter

DarkField Perimeter

ClearField Perimeter

DarkField Perimeter

Figure 7.7. Dark field perimeter SOI short process flow angular acceleration sensor

Dark field designs are better suited to hermetic encapsulation techniques [166]

intended to protect the sensor from particulates and moisture during operation. However,

parasitic capacitance between the fixed sensor electrodes and the dark field perimeter is

typically an order of magnitude larger than observed for clear field designs. Parasitic

capacitance modeling treats the dark field trench width dimension as the dielectric gap

(g0) of a parallel plate capacitor sidewall as described by Eq. 7.1.

0

30_ g

TRC DarkP

πε= (7.1)

Parasitic capacitance (CP_Dark) was calculated as 281fF using data values listed in

Table 5.2. The dark field SOI is connected to the substrate contact bond pad (Sub) using

a silicon interconnect beam as shown in Figure 7.8.

Page 176: G_O'Brien PhD Dissertation

159

ST1 B Sub C

Stiction assisted substrate contact plate

Folded beam spring

Dark field shorted to bond pad “Sub”

View tilt 15 degrees about y-axis

ST1 B Sub C

Stiction assisted substrate contact plate

Folded beam spring

Dark field shorted to bond pad “Sub”

View tilt 15 degrees about y-axis

Figure 7.8 Dark field SOI electrical short to bond pad with substrate contact plate.

Substrate electrical contact was realized using a silicon plate attached by folded beam

spring to the substrate bond pad (Sub) which is manually deflected until contact with the

silicon substrate is achieved. Silicon to silicon contact was maintained after initial

contact between the spring suspended plate and substrate by in-use stiction [125].

Substrate contact designs intended for release stiction initiation were optimized to

produce high surface tension, large silicon to silicon contact area, and low mechanical

restoring force folded beam springs as described in Appendix E.

7.3 Integrated SOI Process Flow

Mechanical anchors can be formed in SOI using a trench refill conformal film [63]

defined perimeter. Polysilicon and silicon nitride low pressure chemical vapor deposition

(LPCVD) conformal films were chosen based on their lower etch rates in HF as

compared to thermal oxide. The ratios of thermal oxide etch as compared to both

Page 177: G_O'Brien PhD Dissertation

160

LPCVD polysilicon and stoichiometric silicon nitride (Si3N4) are 1000:1 and 83:1

respectively [147]. The large etch selectivity ratios of polysilicon and silicon nitride

allows their use as effective etch-stop films in aqueous HF.

7.3.1 Substrate Anchor Trench Refill Etch Stop Process Example

The process example begins with a 1.5kA thick oxide deposition onto a 10μm thick

SOI film with a 0.5μm thick BOX and 525μm thick silicon substrate handle wafer. An

example of mechanical anchor etch stops is described for a 10μm thick SOI film with

0.5μm BOX using the trench refill process flow as shown in Figure 7.9.

Step 1Mask1, Anchora) Plasma-Therm (1.5kA Oxide Etch)b) STS Deep RIE (10μm Si Etch)c) Plasma-Therm (0.5μm Oxide Etch)

Step 2Deposition:LPCVD Nitride (1.5kA)

Step 4Deposition:LPCVD Polysilicon (2um)

Step 6HF Sacrificial Oxide Etch

Step 3Mask2, Windowa) Plasma-Therm (1.5kA nitride etch)b) Plasma-Therm (1.5kA oxide etch)

SOI

Step 5Mask 3, OutlineSTS Deep RIE (12μm Si Etch)

(BOX=0.5μm)Si Substrate

PR

1.5kA Oxide

Photoresist (PR)

PR

PR

Nitride/poly protected oxide anchor

Step 1Mask1, Anchora) Plasma-Therm (1.5kA Oxide Etch)b) STS Deep RIE (10μm Si Etch)c) Plasma-Therm (0.5μm Oxide Etch)

Step 2Deposition:LPCVD Nitride (1.5kA)

Step 4Deposition:LPCVD Polysilicon (2um)

Step 6HF Sacrificial Oxide Etch

Step 3Mask2, Windowa) Plasma-Therm (1.5kA nitride etch)b) Plasma-Therm (1.5kA oxide etch)

SOI

Step 5Mask 3, OutlineSTS Deep RIE (12μm Si Etch)

(BOX=0.5μm)Si Substrate

PR

1.5kA Oxide

Photoresist (PR)

PR

PR

Nitride/poly protected oxide anchor

Figure 7.9 SOI anchor perimeter etch-stop process flow.

The nitride/polysilicon trench refill films form an etch-stop perimeter which protects

the encapsulated oxide anchor from HF exposure during the sacrificial oxide etch.

Variation in BOX anchor cross section due to timed etch in aqueous HF are virtually

eliminated using trench refill etch stop perimeter.

Page 178: G_O'Brien PhD Dissertation

161

The nitride coated trench surfaces act as an electrical insulator providing isolation

between the SOI and silicon handle wafer substrate and as a diffusion barrier during

LPCVD polysilicon deposition and subsequent annealing steps. An example of an

angular accelerometer with anchors fabricated using this process is shown in Figure 7.10.

polysilicon anchor cap

10μm SOI w/0.5 μm BOX

Silicon handle wafer substrate

Anchors

Trench Refill Perimeter

Trench sidewall nitride/

FixedElectrode

polysilicon anchor cap

10μm SOI w/0.5 μm BOX

Silicon handle wafer substrate

Anchors

Trench Refill Perimeter

Trench sidewall nitride/

FixedElectrode

Figure 7.10 SOI anchor trench refill perimeter etch-stop example.

The polysilicon film needs to cover a slightly larger area than the trench window defined

by mask 2 as described in Figure 7.11. Modification of mask 2 and addition of a poly

trench window mask could be used to remove polysilicon over all sensor areas less the

trenched anchor perimeters using the underlying oxide as an effective silicon etch stop.

7.3.2 Substrate Contact Trench Refill Process Example

A substrate contact is formed using the polysilicon trench refill film. Subsequent

thermal annealing is used to form an electrical contact to the substrate via diffusion from

Page 179: G_O'Brien PhD Dissertation

162

the highly doped SOI to intrinsic trench refilled polysilicon. The process flow for auto-

doped LPCVD polysilicon film is shown in Figure 7.9

Step 1Mask1, Contacta) Plasma-Therm (1.5kA Oxide Etch)b) STS Deep RIE (10μm Si Etch)c) Plasma-Therm (0.5μm Oxide Etch)

Step 2Deposition:LPCVD Polysilicon (2μm)

Step 4Mask 2: MetalBond pad metal deposition and lift-off

Step 6HF Sacrificial Oxide Etch

Step 3Blanket Etcha) Plasma-Therm (2μm poly etch)b) Plasma-Therm (1.5kA oxide etch)c) Anneal > 950C for 30minutes to auto-dope intrinsic polysilicon

Step 5Mask 3, OutlineSTS Deep RIE (12μm Si Etch)

(BOX=0.5μm)

Polysiliconelectrical short to substrate

SOI

Photoresist (PR)Bond Pad Metal

HeavilyDoped

Si Substrate

PR

Step 1Mask1, Contacta) Plasma-Therm (1.5kA Oxide Etch)b) STS Deep RIE (10μm Si Etch)c) Plasma-Therm (0.5μm Oxide Etch)

Step 2Deposition:LPCVD Polysilicon (2μm)

Step 4Mask 2: MetalBond pad metal deposition and lift-off

Step 6HF Sacrificial Oxide Etch

Step 3Blanket Etcha) Plasma-Therm (2μm poly etch)b) Plasma-Therm (1.5kA oxide etch)c) Anneal > 950C for 30minutes to auto-dope intrinsic polysilicon

Step 5Mask 3, OutlineSTS Deep RIE (12μm Si Etch)

(BOX=0.5μm)

Polysiliconelectrical short to substrate

SOI

Photoresist (PR)Bond Pad Metal

HeavilyDoped

Si Substrate

PR

Figure 7.11 Polysilicon trench refill substrate electrical contact process flow.

A cross section of a cleaved polysilicon trench refill substrate contact is shown in

Figure 7.12.

Polysilicon

SOI SOI

Silicon Substrate Silicon Substrate

PolysiliconTrench Refill

KeyholeTrenchRefill

Post HF BOX Etch

Polysilicon

SOI SOI

Silicon Substrate Silicon Substrate

PolysiliconTrench Refill

KeyholeTrenchRefill

Post HF BOX Etch

Figure 7.12 Polysilicon trench refill substrate electrical contact cleaved cross section.

Page 180: G_O'Brien PhD Dissertation

163

The polysilicon trench refill substrate contact was evaluated by measuring electrical

resistance between two contacts separated by approximately 330μm on the substrate

surface. Bond pads were interconnected to the substrate contacts using SOI interconnect

beams as shown in Figure 7.13.

Sub2Sub1 contactcontactSub2Sub1 contactcontact

Figure 7.13 Substrate contact polysilicon trench refill bond pad interconnection.

Electrical resistance was measured using an HP 34401 digital multimeter with probe

needles connected to the subtsrate contact bond pads as 1.343kΩ. The electrical

resistances of SOI, polysilicon contacts, and silicon substrate were modeled using Eq. 7.2

through Eq. 7.4 respectively where ρ is the material resistivity as described in Figure

7.14. The measured electrical resistance RTotal represents the sum of SOI, polysilicon

contacts, and silicon substrate resistances as described by Eq. 7.5.

BB

BSOISOI TW

LR ρ= (7.2)

PP

PPolyPoly TW

LR ρ= (7.3)

Page 181: G_O'Brien PhD Dissertation

164

SS

SSubSub TW

LR ρ= (7.4)

PolySOISubTotal RRRR 22 ++= (7.5)

330μm

SOILB = 210μm, WB = 6μm, TB = 20μm

BondPad Sub1

BondPad Sub2

Silicon SubstrateTS = 525μm

TopView

SideView Polysilicon

contacts to substrate

TP = 2μm

RSOI

RPoly RSub

RSOI

RPoly

RTotal=RSub+ 2RSOI+ 2RPoly

SubstrateLS = 330μm, WS = 8μm, TS = 525μm

PolysiliconLP = 2μm, WP = 8μm, TP = 2μm

ρSOI =0.008Ω-cm

ρSub=0.01Ω-cm

WP = 8μm

WB = 6μm

TB = 20μm

XX

XXX TW

LR ρ=

330μm

SOILB = 210μm, WB = 6μm, TB = 20μm

BondPad Sub1

BondPad Sub2

Silicon SubstrateTS = 525μm

TopView

SideView Polysilicon

contacts to substrate

TP = 2μm

RSOI

RPoly RSub

RSOI

RPoly

RTotal=RSub+ 2RSOI+ 2RPoly

SubstrateLS = 330μm, WS = 8μm, TS = 525μm

PolysiliconLP = 2μm, WP = 8μm, TP = 2μm

ρSOI =0.008Ω-cm

ρSub=0.01Ω-cm

WP = 8μm

WB = 6μm

TB = 20μm

XX

XXX TW

LR ρ=

Figure 7.14 Substrate contact cross section and electrical schematic.

The post anneal polysilicon resistivity ρPoly was calculated as 0.42Ω-cm by combining

Eq. 7.2-7.4 into Eq. 7.5 as given by Eq. 7.6. The polysilicon contact resistance was

calculated as 528Ω per contact using Eq. 5.3. The post anneal polysilicon contact

Page 182: G_O'Brien PhD Dissertation

165

phosphorous dopant density was graphically estimated [167] at 1.2*1016cm-3 as shown in

Figure 7.15.

( )SOISubTotalP

PPPoly RRR

LTW 2

2+−=ρ (7.6)

Figure 7.15 Silicon dopant density (cm-3) Vs resistivity (Ω-cm).

The integrated process flow steps used to combine the trench refill etch stop and

polysilicon substrate contact features is described in Appendix F.

Page 183: G_O'Brien PhD Dissertation

166

7.4 SOI Process Flow Summary

A short SOI sensor fabrication process flow was demonstrated in SOI using only 2

photolithography mask steps to develop rapid prototypes. An integrated SOI sensor

fabrication flow providing a trench refill etch stop and electrical substrate contact was

demonstrated using only 4 photolithography mask steps.

The trench refill etch-stop significantly reduces anchor cross section variation and

reduces the sacrificial etch dependence on both time and aqueous HF concentration. In

addition, the etch-stop trench refill encapsulated BOX island provides a robust

mechanical anchor structure. Although not demonstrated, the nitride/polysilicon trench

refill process can be used to form a robust composite beam attaching the silicon substrate

to the SOI layer independent of BOX encapsulation. While the maximum trench width

is typically on the order of 2-3μm, multiple nitride/polysilicon composite beams can be

placed in proximity to form aggregate anchor arrays.

Parasitic capacitance existing between the sensor seismic mass and substrate nodes

degrades the CMOS control chip output voltage sensitivity as previously described in

Chapter 6. The polysilicon electrical substrate contact allows for the substrate voltage to

be externally controlled. Control of the substrate voltage is critical to reducing parasitic

capacitance present between the conductive sensor seismic mass and substrate nodes.

Maintaining the substrate and sensor seismic mass nodes at a near zero differential

voltage significantly reduced the parasitic capacitance observed across these critical

nodes.

The polysilicon electrical substrate contact was autodoped by surrounding SOI

material with an initial dopant concentration of 6*1018cm-3 using an anneal temperature

of 950C maintained for 30 minutes. Post anneal resistance measurements of the

polysilicon substrate contacts yielded an estimated autodoped phosphorous concentration

Page 184: G_O'Brien PhD Dissertation

167

of 1.2*1016cm-3. Electrical resistance measurements were used to calculate a polysilicon

substrate contact resistance of 528Ω. Methods which could lower the post anneal

polysilicon contact resistance include higher initial SOI dopant concentrations, higher

anneal temperature, and longer anneal duration.

Page 185: G_O'Brien PhD Dissertation

168

CHAPTER 8

SUMMARY AND FUTURE WORK

The main objective of this research work was the design, fabrication, and

characterization of angular rate and angular acceleration sensors combined with front end

signal conditioning electronics.

In summary, the main contributions of this research are:

1) Designed, fabricated, and characterized a decoupled mode surface micromachined

angular rate sensor utilizing a fully differential capacitance array which rejects

cross axis linear acceleration.

2) Designed a radial proof mass central hub structural framework which significantly

increased angular rate and acceleration sensor inner ring rigidity. In addition, the

central hub is the seismic mass center of rotation where multiple folded beam

springs are attached. Previously demonstrated designs require springs be attached

directly to the inner or outer radius of the seismic mass. The central hub design

utilizes mechanical lever action to increase sensor angular sensitivity by affording

spring to proof mass spring attach points well within 50μm of the center of

rotation.

3) Developed theoretical models for radial folded beam spring distributions and

compared prediction values to finite element analysis simulation and empirical

results.

4) Designed, fabricated, and tested radial angular acceleration sensors which utilized

the developed theoretical models to minimize the mechanical spring constant

directed about the z-axis while maximizing the spring constant directed along the

z-axis.

Page 186: G_O'Brien PhD Dissertation

169

5) Developed multiple surface micromachined process and device enhancements

including seismic mass over travel stops and anti-stiction beam tip support posts.

6) Designed, fabricated, and characterized a CMOS switched capacitor front end

used to signal condition angular rate and acceleration sensor differential

capacitance outputs. Charge redistribution was used to represent the sensor

differential capacitance output nodes sampled at discrete time intervals in parallel.

7) Developed an SOI substrate electrical contact and demonstrated its successful use

in SOI MEMS fabrication. The substrate contact was comprised of a deep

reactive ion etched trench subsequenly filled with LPCVD intrinsic polysilicon.

The polysilison was auto-doped using the adjacent low resistivity SOI as a dopant

source via a thermal anneal step.

8) Developed an SOI anchor etch-stop perimeter using a nitride/polysilicon

composite and demonstrated its successful use in SOI MEMS fabrication. This

significantly reduced BOX anchor sacrificial etch dependence on both time and

aqueous HF concentration.

Although the work outlined in this thesis has provided solutions to several of the

technical problems and challenges pertaining to angular rate and angular acceleration

sensing systems, there are a number of areas and topics which require further research.

These areas and topics include:

1) Fully inner connected hub attached springs, as shown in Figures 8.1 and 8.2, can

be used to realize even more sensitive angular acceleration sensors regarding

spring constant about the z-axis without a reduction in the spring constant directed

along the z-axis. Although this design is more susceptible to out of x-y plane

sensor seismic mass tilt, how much this will adversely affect device performance

should be predicted, simulated and characterized..

Page 187: G_O'Brien PhD Dissertation

170

Figure 8.1 Fully inner hub connected folded beam spring suspension.

Figure 8.2 Fully inner hub connected folded beam spring suspension detail.

Page 188: G_O'Brien PhD Dissertation

171

2) Larger proof mass radii can be used to increase the angular acceleration sensor

moment of inertia. Defining the upper end limits of radial seismic mass size in an

SOI based process technology should be addressed and incorporated into set of

basic angular acceleration sensor design rules. In addition, more folds per beam

spring can be explored to determine the practical scaling limits inherent to this

design. A single design example with a 1200μm radius and two extra folds per

beam spring fabricated in 20mm thick SOI is shown in figures 8.3 and 8.4

respectively.

Figure 8.3 1200μm radius angular accelerometer with extra beam spring folds.

Page 189: G_O'Brien PhD Dissertation

172

Figure 8.3 1200μm radius angular accelerometer extra beam spring fold detail.

3) Future angular rate sensor development will almost certainly realize the large

mass and high quality factor values possible in SOI based sensor process flows.

4) Hermetic packaging of angular rate sensors with emphasis on robust low pressure

sealing projected to survive in an automotive environment for a minimum 10yrs is

required. This result should verified via an Arrhenius relationship based

accelerated test methodology.

Page 190: G_O'Brien PhD Dissertation

173

APPENDIX A

ELECTROSTATIC LATCH and RELEASE of MEMS CANTILEVER BEAMS

Two closed form algebraic models describing electrostatic latch and release of micro

cantilever beams are presented. The 1st model is based on beam theory with a fixed

moment at the boundary to represent the electrostatic force and it predicts that

electrostatic pull-in occurs at a beam tip displacement of 46% the initial actuator gap.

The 2nd model uses a rigid beam pinned at the anchor with a spring equivalent to the

beam’s mechanical restoring force attached to the tip and describes electrostatic pull-in

occurring at a beam tip deflection of 44% the initial actuator gap. Pull-in voltage

measurements of polysilicon cantilever beam arrays (6μm wide, 2μm thick, 160 μm long)

correlate to both the 1st and 2nd presented models with errors of 8.2% (σ=1.3%), and

4.9% (σ=1.4%), respectively. The 1st and 2nd models were observed to improve pull-in

voltage prediction by at least 10.3% and 13.7% respectively when compared to

previously presented models without the use of empirical correction factors.

A.1 MEMS Cantilever Beam Background Material

Numerous MEMS applications incorporate both cantilever and doubly clamped

beams as an integral part of their design. A brief application list includes resonators

[128, 157, 168, 169], vapor/pressure sensors [155, 170, 171], accelerometers [1, 2], high-

Q electronic filters [172, 173], and micro relay switches [174-176]. Surface

micromachined polysilicon cantilever beams suspended above an isolated electrode are

common throughout the majority of applications listed above and are addressed in this

paper specifically, as shown in Figure A.1.

Page 191: G_O'Brien PhD Dissertation

174

(Latched)+ -

Vpull-in

Electrode

Cantilever BeamL

Z0z

xy

T

(Released) (Latched)+ -

Vpull-in

Electrode

Cantilever BeamL

Z0z

xy

z

xy

T

(Released)

Figure A.1 Cantilever beam model using electrostatic displacement in ANSYS.

The maximum static differential voltage sustainable between the beam and

underlying electrode, prior to beam tip/electrode contact, is defined as the pull-in voltage.

Applied voltages greater than the pull-in magnitude cause instability between the

electrostatic actuation and mechanical restoring forces resulting in beam tip/electrode

latching [168, 169, 171, 174-176]. The static deflection of a cantilever beam excited

dynamically at resonance is magnified by the quality factor [94] (Q) magnitude. In either

case, the system designer is required to accurately predict the static pull-in voltage

magnitude prior to device fabrication.

The pull-in voltage for a cantilever beam previously modeled as a parallel plate

actuator [168] is represented by the peak value of Eq. A.1 swept over the range 0<z<Z0.

The peak value occurs at z=2Z0/3 corresponding to a beam tip displacement of 33% the

initial dielectric gap (Z0). The discrete pull-in voltage VPI [1] was calculated using Eq.

A.1 with z=2Z0/3 as given by Eq. A.2.

LWzZzKzV Z

AB0

02 )(2)(

ε−

= (A.1)

LWZK

V ZPI

0

30

278

ε= (A.2)

Page 192: G_O'Brien PhD Dissertation

175

Cantilever beam capacitance has been previously described using beam theory [169]

with the electrostatic force directed at the beam tip along the z axis by a third order

function of x, as given by Eq. (3), where ε0 is the permittivity of free space.

dx

EIxLxzZKZ

WzCZ

BE ∫ −−−

=L

0 320

0

0

6)3)((

)( ε (A.3)

The voltage satisfying static equilibrium was calculated by equilibrating mechanical

restoring force and applied electrostatic force using Eq. A.4. The pull-in voltage

represents the peak value of Eq. A.4 swept over the range {0<z<Z0}. The peak value of

Eq. A.4 occurs at z≅0.55Z0 corresponding to a beam tip displacement of 45% the initial

dielectric gap Z0. The previously reported pull-in voltage Vth [169] was approximated

using Eq. A.5.

dzzdCzZKzV

BE

ZBE )(

)(2)( 0

−= (A.4)

WLEIZ

Vth 40

30

518ε

= (A.5)

Empirical pull-in voltage results were significantly smaller than modeled by Eq. A.5

resulting in calculated %Error in excess of 20%. Empirical pull-in voltage results were

significantly larger than modeled by Eq. A.2 resulting in a calculated %Error in excess of

28%. Based on the significant %Error observed for both the parallel plate [168] and

beam theory [169] models (reference Table 1), a more accurate theoretical model is

desired which does not incorporate empirical correction factors [175]. Computer based

electromechanical simulation tools have previously demonstrated more accurate pull-in

Page 193: G_O'Brien PhD Dissertation

176

voltage prediction values, as compared to theoretical models, by skewing the appropriate

stiffness and residual stress model coefficients by empirical correction factors [176].

However, this requires the electromechanical simulator to reside in the design feedback

loop requiring multiple simulation and layout change iterations to converge at the initial

design target pull-in voltage magnitude. The work described in this appendix potentially

reduces the number of design iterations required to optimize MEMS cantilever beam

based devices by providing a more accurate initial pull-in voltage prediction magnitude

prior to verification via computer simulation. Also, the designer is afforded valuable

insight regarding system operation via the presented closed form models.

A.2 Beam Theory Model with Bending Moment Applied at Tip

The 1st model proposes use of a bending moment applied at the cantilever tip to

represent the electrostatic force distributed across the beam as shown in Figure A.2.

L

r0

z0Electrode

Cantilever BeamM1

Figure A.2 Cantilever beam w/moment applied at free end.

Unlike the previous model that used a vertical force applied at the tip to approximate

the distributed electrostatic force [169], the bending moment assumption is proposed to

provide a better emulation of electrostatic force.

Assuming constant flexural rigidity given by the product of the Young’s modulus (E)

and the moment of inertia (I), the equation defining the beam moment [177] is given by

Eq. A.6. The boundary conditions regarding beam deflection are ν = 0, and θ = 0, at the

Page 194: G_O'Brien PhD Dissertation

177

cantilever beam anchor base where x = 0. The displacement of the beam was solved via

successive integration of Eq. A.6 as given by Eq. A.7 where both constants of integration

were observed to be zero based on the boundary conditions listed above.

2

2

1dx

vdEIM −= (A.6)

EIxM

xv2

)(2

1= (A.7)

The moment applied at the beam tip is given by Eq. A.8, with the force applied at the

beam tip is given by Eq. A.9.

LzFM M )(1 = (A.8)

)()( 0 zZKzF MM −−= (A.9)

The capacitance between the beam and electrode was calculated using Eq. A.7

through Eq. A.9, as given by Eq. A.10. The capacitance as a function of beam tip

deflection and its derivative with respect to beam tip deflection are given by Eq. A.11,

and Eq. A.12 respectively.

∫ −−

=Lr

2)(

)(0

20

dx

EILxzZKZ

WzCM

o

oCE

ε (A.10)

⎥⎥⎦

⎢⎢⎣

−−

−= −

)()(tan

)()(

00

01

00

0

ZzZZz

ZzZLWzCCE

ε (A.11)

Page 195: G_O'Brien PhD Dissertation

178

))(2)()(tan

))((2

)(

0

0

00

01

23

00

00

ZzzLW

ZzZZz

ZzZ

LWZdZ

zdCCE

−+

⎥⎥⎦

⎢⎢⎣

−= − εε (A.12)

Equating the electrostatic and mechanical restoring force while solving for voltage is

given by Eq. A.13.

dZzdC

zZKzV

CE

MCE )(

)(2)( 0

−= (A.13)

The spring constant is defined by Eq. A.14, calculated using Eq. A.7 through Eq.

A.9, as given Eq. A.15.

)()(Lxv

zFK MM =

= (A.14)

3

3

6LEWTKM = (A.15)

The pull-in voltage (VCPI) represents the peak value of Eq. A.13 swept over the range

{0<z<Z0.} The pull-in voltage (VCPI) was approximated using z=Z0(1-0.46) substituted

into Eq. A.13 and Eq. A.15, normalized via Eq. A.2, as given by Eq. A.16.

WLEIZ

VCPI 40

30

518

5043

ε= (A.16)

A.3 Pinned Rigid Beam with Spring Applied at Tip

The 2nd model describes the electrostatic deflection of a polysilicon cantilever beam

using the derivative of the system capacitance function. The proposed model is

comprised of a hinge pin located at the cantilever beam anchor with the free end

Page 196: G_O'Brien PhD Dissertation

179

suspended via a mechanical spring equivalent to the beam’s mechanical restoring force as

shown in Figure A.3.

KZ

θr1r1

r0r0

Simple HingeCtr of Rotation

Figure A.3 Cantilever beam deflection model parameters.

The cantilever beam capacitance is defined by Eq. A.17 and given by Eq. A.18 where

L’Hopitals rule is used as the beam tip displacement angle (θ) approaches zero [178].

∫ −=

1

0

rr

)( drrZ

WC

o

o

θε

θ (A.17)

⎟⎟⎠

⎞⎜⎜⎝

⎛−−

=10

000 ln)(rZrZW

Cθθ

θε

θ (A.18)

The potential energy of the capacitor and spring as a function of angular displacement

are given by Eq. A.19 and Eq. A.20 respectively.

2)(

21)( θθθ VCU cap = (A.19)

2

1)(21)( rKU Zspring θθ = (A.20)

The electrostatic and mechanical restoring torques are given by Eq. A.21 and Eq.

A.22 respectively.

Page 197: G_O'Brien PhD Dissertation

180

2)(

21)(

θθθ

θθ

Vd

dCd

dUcap = (A.21)

)()( 2

1rKd

dUZ

spring θθ

θ= (A.22)

The rate of capacitance change with respect to angular displacement is given by Eq.

A.23. The beam spring constant applied at the rigid beam tip is given by Eq. A.24.

⎥⎥⎦

⎢⎢⎣

⎡⎟⎟⎠

⎞⎜⎜⎝

⎛−−

−−−

−−−=

)()(

ln1))((

)()()(

10

00

1000

1000010

rZrZ

rZrZrZrrZrW

ddC

θθ

θθθθθ

θε

θθ (A.23)

3

3

4LEWTK z = (A.24)

Finally, Vθ is modeled using Eq. A.21 and Eq. A.22 as a sum moments satisfying

static equilibrium as given by Eq, A.25. The beam voltage as a function of rotation angle

combines Eq. A.23 through Eq. A.25 as given by Eq. A.26.

θθ

θθθ

ddC

rKV Z)(

2)(2

1= (A.25)

⎥⎥⎦

⎢⎢⎣

⎡⎟⎟⎠

⎞⎜⎜⎝

⎛−−

−−−

−−−=

)()(ln1

))(()()(2

)(

10

00

1000

10000110

32

rZrZ

rZrZrZrrZrr

TEV

θθ

θθθθθε

θθθ (A.26)

The cantilever beam tip to electrode theoretical contact angle upon pull-in is given by

Eq. A.27. The voltage described by Eq. A.26 can be converted from beam deflection

angle to beam tip displacement as a function of z as given by Eq. A.28.

Page 198: G_O'Brien PhD Dissertation

181

1

0max r

Z=θ (A.27)

1

0

rzZ −

=θ (A.28)

Applied voltage versus normalized cantilever beam tip displacement for the 1st and

2nd models are compared to the previous parallel plate [168] and beam theory models

[169] as shown in Figure A.4.

0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 10

5

10

15

20

25

0

0

ZzZ −

V PIV

CPIV

thV

BPIV

Parallel Plate Model

Beam Theory

Model

Proposed 1st and 2nd

Models

Figure A.4 Applied voltage Vs normalized beam tip displacement.

The peak shown in Figure A.4 represents the maximum voltage possible for a steady

state electrostatic solution. Solving Eq. A.26 with θ=(11Z0)/(25r1) yields the pull-in

voltage (VBPI) given by Eq. A.29.

⎥⎥⎥⎥

⎢⎢⎢⎢

⎟⎟⎠

⎞⎜⎜⎝

⎛ −−

=

1

01

01

010

30

3

21

141125

ln14

2511

)(1125

7725

11

rrr

rr

rr

ZETr

VBPI

ε

(A.29)

Page 199: G_O'Brien PhD Dissertation

182

A.4 Hybrid Cantilever Beam Model

A combination of the 1st and 2nd models was performed to reduce the capacitance

function from second order to first order in x while maintaining the ability to model

capacitance due to curvature under beam deflection. The hybrid model splits the beam

into n discrete line segments and is solved for capacitance over n discrete line segment

intervals

An example of the hybrid model with three segments (n=3) is provided via line

equations, given by Eq. A.30 through Eq. A.32, where z represents the dielectric gap

between the beam tip and electrode and x represents the beam length from the anchor to

beam tip.

( ) ⎟⎟⎠

⎞⎜⎜⎝

⎛−−=

10 3

532),(

rxzZzxYtip ; { 1

1

32

rxr

≤< } (A.30)

( ) ⎟⎟⎠

⎞⎜⎜⎝

⎛−−=

10 9

2),(rxzZzxYmid ; {

32

311 r

xr

≤< } (A.31)

( ) ⎟⎟⎠

⎞⎜⎜⎝

⎛ −−=

10 3

),(rxzZzxYanc ; {

30 1rx ≤< } (A.32)

The 1st, 2nd, and hybrid models’ beam curvature versus beam length are plotted in

Figure A.5 for a normalized Z-axis beam tip displacement of Z0 corresponding to the post

pull-in (z=0) latched beam condition.

Page 200: G_O'Brien PhD Dissertation

183

0 0.33 0.67 11

0.90.80.70.60.50.40.30.20.1

00

10 0.33 0.67 1

10.90.80.70.60.50.40.30.20.1

00

1

AnchorSegment

MiddleSegment

Beam TipSegment

HybridModel

1st Model

2nd Model

1rx

0

0

ZzZ −

2nd

1st

0 0.33 0.67 11

0.90.80.70.60.50.40.30.20.1

00

10 0.33 0.67 1

10.90.80.70.60.50.40.30.20.1

00

1

AnchorSegment

MiddleSegment

Beam TipSegment

HybridModel

1st Model

2nd Model

1rx

0

0

ZzZ −

2nd

1st

Figure A.5 Normalized beam deflection Vs beam length.

The capacitance of each region is defined by the summation of electric field lines

between the line segment and underlying electrode as given by Eq. A.33 through Eq.

A.35.

( )dx

rxzZZ

WzC

rrtip ∫

⎟⎟⎠

⎞⎜⎜⎝

⎛−−+

=1

1

32

100

0

35

32

)(ε (A.33)

( )dx

rxzZZ

WzC

r

rmid ∫⎟⎟⎠

⎞⎜⎜⎝

⎛−−+

= 32

3

100

01

1

92

)(ε (A.34)

( )dx

rxzZZ

WzC

r

ranc ∫

⎟⎟⎠

⎞⎜⎜⎝

⎛ −−+

= 3

100

01

0

3

)(ε (A.35)

The integrations shown above were performed as given by Eq. A.36 through Eq.

A.38. The total system capacitance is represented by the summation of beam segment

capacitances as given by Eq. A.39.

Page 201: G_O'Brien PhD Dissertation

184

⎟⎟⎠

⎞⎜⎜⎝

⎛++−

=zZ

zzZ

WrzCtip 45

9ln)(5

3)(

00

10ε (A.36)

⎟⎟⎠

⎞⎜⎜⎝

⎛+

++−

=zZzZ

zZWr

zCmid0

0

0

10

845

ln)(

)(ε (A.37)

⎟⎟⎠

⎞⎜⎜⎝

⎛+

+−+−

−=

)8()(3

ln)(

3)(

01

00010

0

10

zZrzrrZrZ

zZWr

zCancε (A.38)

)()()()( zCzCzCzC ancmidtiphybrid ++= (A.39)

The hybrid model approach accounts for beam curvature with a first order system

capacitance function. The 1st, 2nd, and hybrid models’ capacitance values are plotted

versus Z-axis beam tip displacement swept over the range {0 ≤ z ≤Z0}, as shown in

Figure A.6. The case where n=1 represents the 2nd model capacitance function while as

n increases the hybrid model converges to the 1st model capacitance function for a Z-axis

beam tip displacement swept over the range {0 ≤ z ≤Z0}. The hybrid model example

(n=3) demonstrates that a good approximation of the 2nd model capacitance

encompassing beam curvature can be obtained using a relatively small number of discrete

line segments as shown in Figure A.6. The hybrid model also describes the regional

capacitance distribution along the beam as a function of beam deflection along the x-axis.

The capacitance was calculated for the tip, middle, and anchor regions, at the point of

theoretical electrostatic pull-in, with increases of 51.6%, 15.0%, and 1.0% respectively

when referenced to their initial magnitudes of C0/3. The hybrid model distributes the

total electrostatic force along the beam with 76.3% over the tip region, 22.2% over the

middle region, and 1.5% over the anchor region upon pull-in.

Page 202: G_O'Brien PhD Dissertation

185

0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 10

0.2

0.4

0.6

0.8

1

1.2

1.4

1.6

1.8

2

0

)(C

zC

0

0

ZzZ −

HybridModel

1st Model

2nd Model

)(zCtip

)(zCmid

)(zCancElectrostaticPull-in Point

2nd

1st

0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 10

0.2

0.4

0.6

0.8

1

1.2

1.4

1.6

1.8

2

0

)(C

zC

0

0

ZzZ −

HybridModel

1st Model

2nd Model

)(zCtip

)(zCmid

)(zCancElectrostaticPull-in Point

2nd

1st1st

Figure A.6 Normalized capacitance Vs beam tip displacement

A.5 Capacitance-Voltage (C-V) Plot Beam Measurement Description

Capacitance-Voltage measurements [152] were performed using an HP-4284A LCR

Meter controlled via LabView software as shown in Figure A.7. Electrostatic actuation

was accomplished by independently stepping the bias voltage between the cantilever

beam and underlying electrode via discrete 50mV increments. A time delay loop was

incorporated into the C-V plot measurements such that beam motion dampened to steady

state between successive capacitance measurements.

Page 203: G_O'Brien PhD Dissertation

186

Figure A.7 Cantilever beam array electrostatic latch and release C-V plot.

A typical surface micromachined polysilicon cantilever beam array with an

underlying polysilicon electrode is shown in Figure A.8.

Figure A.8 Polysilicon cantilever beam array with underlying polysilicon electrode.

A.6 Comparison of Theoretical Models and Empirical Data

The beam arrays observed per this experiment were 160 microns long and 2 microns

thick. Beam widths were varied at 2, 4, and 6 microns. The initial dielectric gap was

fixed at 2 microns for all beam arrays. The beam displacement predicted by the voltage

Page 204: G_O'Brien PhD Dissertation

187

models are valid from (0,0) to the parabolic maxima represented by pull-in voltage as

shown in Figure A.4. Voltage values greater than pull-in do not satisfy static

equilibrium. Cantilever beam electrostatic pull-in models are compared to empirical

results in Table A.1.

Table A.1 Cantilever beam model prediction comparison to empirical data. Beam L = 160u Empirical Eq(13) Eq(11) Eq(24) Eq(40) Eq(13) Eq(11) Eq(24) Eq(40)Array T = 2u Pull-in Vpi Vth Vcpi Vbpi Vpi Vth Vcpi VbpiID # Width [u] [V] [V] [V] [V] [V] % Error % Error % Error % Error

1 2 14.20 11.07 22.28 19.18 18.50 -28.3 36.3 26.0 23.22 2 14.35 11.07 22.28 19.18 18.50 -29.6 35.6 25.2 22.43 2 14.15 11.07 22.28 19.18 18.50 -27.8 36.5 26.2 23.54 4 15.80 11.07 22.28 19.18 18.50 -42.7 29.1 17.6 14.65 4 16.30 11.07 22.28 19.18 18.50 -47.2 26.8 15.0 11.96 4 15.90 11.07 22.28 19.18 18.50 -43.6 28.6 17.1 14.17 6 17.85 11.07 22.28 19.18 18.50 -61.2 19.9 6.9 3.58 6 17.35 11.07 22.28 19.18 18.50 -56.7 22.1 9.5 6.29 6 17.60 11.07 22.28 19.18 18.50 -59.0 21.0 8.2 4.9

The empirical result referenced %Error metric, as shown in Table A.1, was used to

gage model performance versus cantilever beam width as shown in Figure A.9.

-80.0

-60.0

-40.0

-20.0

0.0

20.0

40.0

60.0

0 2 4 6 8

VBPI [Eq. (29)]

Beam Width [μm]

Pull-inModel%Error

VCPI [Eq. (16)]

Vth [Eq. (5)]

VPI [Eq. (2)]

Figure A.9 Pull-in voltage model prediction %Error Vs beam width

Page 205: G_O'Brien PhD Dissertation

188

The observed non-zero slope in pull-in voltage versus beam width is not accounted

for by any of the pull-in voltage models described in this paper. Fringing electric fields

may result in electrostatic levitation [143] of the suspended cantilever beams accounting

for the poor fit over beam width as fringing was neglected in the pull-in voltage models.

The theoretical cantilever beam capacitance area is given by width W times length L. The

ratio of fringing electric field to theoretical cantilever beam capacitance area decreases as

the beam width is increased for a fixed beam thickness and length. Therefore, the

empirical pull-in voltage is expected to converge as beam width is increased. Based on

the %Error metric, both proposed electromechanical models (reference Eq. A.16 and Eq.

A.29) yielded more accurate results than either the previously described parallel plate or

beam theory models.

A final comparison of relative pull-in voltage magnitude is presented by reducing

model input variables to common terms. Our 1st pull-in model as a function of the

Young’s modulus and beam dimensions by substituting Eq. A.40 into Eq. A.16 as given

by Eq. A.41.

12

3WTI = (A.40)

40

30

3

103

5043

LZET

VCPIε

= (A.41)

Similarly, substituting Eq. A.24 into Eq. A.2, and Eq. A.40 into Eq. A.5, yields the

previously presented parallel plate [168] and beam theory [169] models as given by Eq.

A.42 and Eq. A.43 respectively.

Page 206: G_O'Brien PhD Dissertation

189

40

30

3

103

952

LZET

VPIε

= (A.42)

40

30

3

103

LZET

Vthε

= (A.43)

The maximum stable beam tip deflection prior to electrostatic pull-in was measured

optically on two devices as 0.45Z0 and 0.46Z0 using a Zygo confocal microscope. The

2micron wide beam arrays did not self-release upon removal of differential voltage post

electrostatic pull-in. The beams permanently latched to the substrate are attributed to

stiction [125] as shown in Figure A.10.

Figure A.10 Post electrostatic actuation permanent beam latching (stiction).

A.7 Finite Element Analysis (FEA) Computer Simulation

Computer simulation was performed via ANSYS software, version 5.6, using a

sequential electrostatic-structural coupled field approach. The beam length and thickness

were scaled to 160microns and 2microns respectively, with a Young’s Modulus of

150GPa as used in the previous theoretical calculations. The beam displacement ANSYS

Page 207: G_O'Brien PhD Dissertation

190

simulation [179] yielded a pull-in voltage of 22.3V, as shown normalized in Figure A.11,

using a 2D plane strain electrostatic element.

0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 0.4 0.45 0.50

0.2

0.4

0.6

0.8

1

0

0

ZzZ −

PIV

CPIV

thV

Parallel Plate Model

Proposed 1st

Model

ANSYSV

ANSYS SimulatedModel

thVV

Figure A.11 Electrostatic latch model prediction compared to 2D ANSYS FEA.

Subsequent ANSYS 2D plane stress and 3D element simulations predicted the

average empirical pull-in voltages for the 6micron wide beams with %Errors of 5.1% and

0.6% respectively, as shown in Table A.2.

Table A.2 ANSYS ANSYS Simulated Empirical Eq(13) Eq(11) Eq(24) Eq(40)Element Element Pull-in Pull-in Vpi Vth Vcpi Vbpi

Dimension Type [V] [Avg. V] [V] [V] [V] [V]2D PLANE82 with Plane Strain 22.3 17.6 11.07 22.28 19.18 18.502D PLANE82 with Plane Stress 18.5 17.6 11.07 22.28 19.18 18.503D SOLID122, w=6um 17.5 17.6 11.07 22.28 19.18 18.50

Note that the ANSYS 2D plane stress and strain simulations yield similar pull-in

results as predicted by Eq. A.41 and Eq. A.43 respectively. However, the ANSYS 3D

Page 208: G_O'Brien PhD Dissertation

191

simulations exhibit less error when compared to both empirical data and the models

derived in this Appendix described by Eq. A.16 (VCPI) and A.29 (VBPI) as shown in Table

A.2.

Both empirical and FEA simulation results support the conclusion that the derived

theoretical models (VCPI and VBPI) are more accurate regarding cantilever pull-in

prediction than those previously presented [168, 169] without the use of empirical

correction factors [175, 176].

A.8 Cantilever Beam Electrostatic Latch Model Summary/Conclusion

Two new closed form algebraic models describing MEMS cantilever beam

electrostatic actuation and pull-in have been independently derived and presented. The

1st model employed beam theory to describe the system electrical capacitance. Pull-in

displacement of the beam tip was calculated at 46% of the original dielectric gap using

the 1st model’s capacitance function. This model accounts for beam deflection

applicable to cantilever beam and micro-relay electromechanical systems where the

underlying electrode fully extends to the cantilever beam tip. The proposed beam theory

model %Error was compared to empirical pull-in voltage measurements for the 2, 4, and

6 micron wide beams as 25.8% (σ=0.5%), 16.6% (σ=1.4%), and 8.2% (σ=1.3%),

respectively. The 2nd model employs a more accurate capacitance function near the

beam tip accounting for orthogonal electric field termination on both the deflected beam

and underlying electrode conductive surfaces. The proposed 2nd model %Error was

compared to empirical pull-in voltage measurements for the 2, 4, and 6 micron wide

beams as 23.1% (σ=0.6%), 13.5% (σ=1.4%), and 4.9% (σ=1.4%), respectively. Both

proposed models consistently predicted electrostatic pull-in voltage results with less

%Error than previously reported theoretical models without the use of empirical

correction factors. Fringing electric fields may account for the discrepancy in pull-in

Page 209: G_O'Brien PhD Dissertation

192

voltage regarding varied beam width. The empirical pull-in voltage is expected to

converge as beam width is increased beyond the 6 micron upper limit explored per this

experiment. A hybrid model was presented as a method to account for beam curvature

during electrostatic deflection while reducing the model from second to first order

functions in terms of x directed along the beam length axis.

Page 210: G_O'Brien PhD Dissertation

193

APPENDIX B

SUPER CRITICAL POINT CO2 CHAMBER DESIGN and OPERATION

Beam spring suspended MEMS structures fabricated in silicon which are externally

deflected until physical contact with adjacent silicon surfaces occur are subject to remain

in contact after external deflection force application is referred to as stiction [125].

Release stiction is common in MEMS devices which utilize a wet sacrificial oxide etch in

hydrofluoric acid followed by de-ionized water rinse and evaporation. The de-ionized

water evaporation phase is associated with a surface tension force between the suspended

MEMS structure and substrate silicon electrodes. In MEMS devices with relatively small

suspension beam spring constants or large suspended structure perimeters typically result

in a release stiction condition. Release stiction in MEMS devices represents catastrophic

yield loss and should be avoided wherever possible. An effective method to reduce yield

loss due to stiction is to substitute the post rinse evaporation phase de-ionized water with

a lower surface tension liquid such as isopropyl alcohol or methanol. Another method

eliminates liquid evaporation phase surface tension by using sublimation technique

described by super critical point CO2 process [146]. This appendix describes the

fabrication and operation of a super critical point CO2 chamber.

B.1 Super Critical Point CO2 Background

Yield loss due to release stiction [125] is a multi-step process which begins with

deflection of a deformable MEMS structure due to the surface tension force associated

with a liquid evaporated from the wafer surface. Surface tension force based deflection

due to the liquid evaporation process is described for low and high z-axis spring constant

MEMS polysilicon cantilever beams in Figure B.1.

Page 211: G_O'Brien PhD Dissertation

194

1

2

3

4

Meniscus Propagation Direction

Short Beam (rigid)

Long Beam (compliant)

Stiction occurs during Step 3; where the Long Polysilicon Beam contacts the Polysilicon substrate.

1

2

3

4

Meniscus Propagation Direction

Short Beam (rigid)

Long Beam (compliant)

Stiction occurs during Step 3; where the Long Polysilicon Beam contacts the Polysilicon substrate.

1

2

3

4

Meniscus Propagation Direction

Short Beam (rigid)

Long Beam (compliant)

Stiction occurs during Step 3; where the Long Polysilicon Beam contacts the Polysilicon substrate.

Figure B.1 Cross section of short (high spring constant KZ) and long (low spring

constant KZ) MEMS cantilever beam release stiction due to de-ionized

water evaporating from wafer surface.

The surface tension of a gas or super critical fluid is essentially zero. As a result, dry

etching, as described in Appendix C, does not cause surface tension. Similarly, super

critical CO2 processing allows the device to transition from a liquid to supercritical fluid

ambient without surface tension effects. Super critical temperature and pressure for

several common materials [145] is shown in Table B.1.

Table B.1 Super critical temperature, pressure, and density of common materials. Critical Critical Critical Critical Critical

Material Temp(K ) Temp(C ) Press(MPa) Press(PSI) Density(kg/m3)H2O 647.4 374.3 22.12 3207 320CO2 304.2 31.1 7.39 1072 468NH3 405.5 132.4 11.28 1636 235O2 154.8 -118.4 5.08 737 410N2 126.2 -147.0 3.39 492 311

Page 212: G_O'Brien PhD Dissertation

195

While water could be processed in the super critical region, the large critical point

temperature and pressure make design and safe operation of such a system cost

prohibitive. In contrast, the critical point temperature and pressure of CO2 is relatively

low and allows for near room temperature operation. As a result, super critical CO2

chambers have been previously designed and fabricated for use in MEMS research [146].

B.2 Super Critical Point CO2 Process

Wet hydrofluoric acid used to etch the MEMS device sacrificial oxide. The wet HF

acid is then diluted and replaced with de-ionized water. Since de-ionized water is not

miscible in liquid CO2, methanol is introduced as an intermediate transition fluid.

Supercritical CO2 processing is initiated after the de-ionized water has been diluted and

completely replaced with methanol. The released MEMS device submerged in methanol

is then placed into a pressure vessel and subsequently filled with liquid CO2. A liquid

CO2 flow rate of 20scfh at a regulated pressure of 1050psi is used to purge and

completely replace the methanol in the sealed chamber. The chamber is then sealed and

heated to 40°C using a hotplate which results in an increase in the chamber pressure in

excess of the critical point pressure of 1071°C. The transition from liquid to super

critical fluid occurs at a minimum temperature of 31°C, and pressure of 1072psi as shown

in Figure B.2. The chamber is maintained at 40°C and vented to atmosphere at a flow

rate of 20scfh after 10minutes of super critical CO2 exposure. The chamber is opened

after atmospheric pressure is achieved and devices are removed completing the super

critical CO2 process.

Page 213: G_O'Brien PhD Dissertation

196

SolidLiquid

Gas

Super CriticalFluid

Triple Point(-57°C, 75 psi)

1

14.7 psi

-78°C

3

2

31°C

1072 psi

Pressure

Temperature

1) Dilute Methanol in liquid CO2.

1 → 2) Close Chamber, add heat using hotplate. Chamber pressure increases due to temperature increase.

2 → 3) Slowly bleed off pressure ensuring that chamber temperature does not fall below 31°C during venting.

SolidLiquid

Gas

Super CriticalFluid

Triple Point(-57°C, 75 psi)

1

14.7 psi

-78°C

3

2

31°C

1072 psi

Pressure

Temperature

1) Dilute Methanol in liquid CO2.

1 → 2) Close Chamber, add heat using hotplate. Chamber pressure increases due to temperature increase.

2 → 3) Slowly bleed off pressure ensuring that chamber temperature does not fall below 31°C during venting.

Figure B.2 Super critical point CO2 transition from liquid to gas phase.

B.3 Super Critical Point CO2 Equipment Configuration

A schematic of the super critical chamber is shown in Figure B.3.

CO2

HeDipTube

CO2 Vent line

G1 G2 G3

H1

H2

M1

M2

H3

H4

M3

M4

HotplateCPD Chamber

Methanol Liquid Filter/Trap

ControlValves

ControlValves

LiquidCO2Bottle

CO2

HeDipTube

CO2 Vent line

G1 G2 G3

H1

H2

M1

M2

H3

H4

M3

M4

HotplateCPD Chamber

Methanol Liquid Filter/Trap

ControlValves

ControlValves

LiquidCO2Bottle

Figure B.3 Super critical CO2 chamber system schematic.

Page 214: G_O'Brien PhD Dissertation

197

The super critical CO2 chamber system is shown with the cap installed and removed

as shown in Figures B.4 and B.5 respectively.

Base

Cap

Thermocouple

RegulatedSupply Pressure

Control Valves

Slow Fill

Fast Fill

Chamber Purge

ChamberVent

SupplyPressure

ChamberPressure

Overpressure Burst Disc

HeaterSwitch

H1

H2

H3

H4

Base

Cap

Thermocouple

RegulatedSupply Pressure

Control Valves

Slow Fill

Fast Fill

Chamber Purge

ChamberVent

SupplyPressure

ChamberPressure

Overpressure Burst Disc

HeaterSwitch

H1

H2

H3

H4

Figure B.4 Super Critical CO2 Chamber with cap installed.

Base

Slow Fill

Fast Fill

Chamber Purge

ChamberVent

SupplyPressure

ChamberPressureHeaterSwitch

4” Wafer

Cap Bolt HolesBase

Slow Fill

Fast Fill

Chamber Purge

ChamberVent

SupplyPressure

ChamberPressureHeaterSwitch

4” Wafer

Cap Bolt Holes

Figure B.5 Super critical CO2 chamber cap removed exposing 100mm wafer sample.

Page 215: G_O'Brien PhD Dissertation

198

The stainless steel chamber base is shown in Figure B.6. The chamber is machined

from stainless steel with specifications shown in Figure B.7.

CO2 Drain Holes

Wafer Support Pins

CO2 Drain Line

Wafer Retaining Pins

100mm Silicon WaferCO2 Drain Holes

Wafer Support Pins

CO2 Drain Line

Wafer Retaining Pins

100mm Silicon Wafer

Figure B.6 Super critical CO2 chamber stainless steel chamber base.

Figure B.7 Super critical CO2 chamber base mechanical specifications.

Page 216: G_O'Brien PhD Dissertation

199

The chamber base and cap are shown in Figures B.8 and B.9.

100mm Wafer O-Ring DiffuserSealing Surface

Cap (internal chamber side shown)Base w/100mm Silicon Wafer

100mm Wafer O-Ring DiffuserSealing Surface

Cap (internal chamber side shown)Base w/100mm Silicon Wafer

Figure B.8 Super critical chamber base with cap.

Cap

Base

Cap with Diffuser

Cap

Base

Cap with Diffuser

Figure B.9 Super critical chamber cap mechanical specifications.

Page 217: G_O'Brien PhD Dissertation

200

The MEMS wafer sample is immersed in liquid methanol at room temperature and

pressure upon process initiation. Liquid CO2 is introduced through the cap diffuser using

on-off valve H1 set to on, as shown in Figure B.4, at a slow fill rate of 10psi/s which is

preset using metered valve M1 located internal to the chamber base pedestal. Upon

pressure equalization of the regulated CO2 supply line and internal chamber pressure

(~1050psi) the fast fill on-off valve H2 is set to on, as shown in Figure B.4. The liquid

CO2 filled chamber is then purged/vented to an organic solvent hood exhaust for a

minimum of 10minutes to dilute and replace the initial methanol charge with liquid CO2

using on-off valve H3 set to on, and metered valve M3 set to a flow rate of 20scfh. The

diffuser shape and hole locations, as shown in Figure B.10, were designed to agitate the

liquid CO2 by introducing a clockwise rotation flow during purge/vent operations. The

cap diffuser hole placement mechanical specifications are listed in Figure B.11.

CO2 Diffuser HolesCO2 Diffuser Holes

Figure B.10 Cap diffuser used dispense liquid CO2 with a clockwise flow.

Page 218: G_O'Brien PhD Dissertation

201

Figure B.11 Diffuser tubing and hole placement mechanical specifications.

An extension sleeve can be installed between the cap and base to process twenty four

100mm MEMS wafer samples per process run as shown in Figures B.12 and B.13.

24 Wafer100mm Boatfits insideChamberExtension

Cap

SleeveSleeve

Cap

24 Wafer100mm Boatfits insideChamberExtension

Cap

SleeveSleeve

Cap

Figure B.12 Super critical CO2 chamber extension sleeve.

Page 219: G_O'Brien PhD Dissertation

202

7.000

10.000

A

7.640

7.5000.385

Cap

Base

ChamberExtensionSleeve

7.000

ChamberExtensionSleeve

Cap

Base

TopView

SideView

7.000

10.000

A

7.640

7.5000.385

Cap

Base

ChamberExtensionSleeve

7.000

ChamberExtensionSleeve

Cap

Base

TopView

SideView

Figure B.13 Chamber extension sleeve mechanical specifications.

The chamber valves (H1-H4) are all turned to the off position after methanol chamber

purging with liquid CO2 is complete.

A hot plate located under the aluminum chamber pedestal housing, as shown in

Figure B.14, is used to elevate the internal chamber temperature beyond the 31°C super

critical CO2 point.

Page 220: G_O'Brien PhD Dissertation

203

Chamber Pedestal

HotPlate

1)

2)

3)

4)

Chamber Pedestal

HotPlate

1)

2)

3)

4)

Figure B.13 Chamber pedestal hot plate location.

A thermocouple feed-thru probe is used to measure the chamber internal cavity gas

temperature as previously shown in Figure B.4. Temperature is maintained at 40°C for a

minimum of 5minutes with chamber pressure verified as greater than 1072psi (typically

1250-1350psi). The vent line valve H3 is then opened and purged to an organic solvent

hood exhaust at a maximum flow rate of 20scfh using pre-set metered valve M3 as shown

in Figure B.14. Temperature is maintained at 40°C during chamber vent operation.

The MEMS sample can be removed from the chamber after internal pressure reaches

ambient (~14.7psi).

Page 221: G_O'Brien PhD Dissertation

204

Valves M1, M2

HotPlate Removed

Valves M1, M2

HotPlate Removed

Figure B.14 Super critical CO2 internal chamber pedestal metered valve locations.

B.4 Super Critical Point CO2 Equipment Process Sequence

1) Release MEMS device using hydrofluoric (HF) acid etch with de-ionized water

(H2O) rinse followed by methanol (CH3OH) rinse with 30minute minimum soak

time.

2) Place methanol (CH3OH) immersed sample into super critical CO2 chamber.

3) Install eight cap with bolts using a star pattern until snug using 15ft-lb applied

via torque wrench.

4) Install ¼ inch stainless steel CO2 supply line using crescent wrench until snug.

5) Verify liquid CO2 bottle pressure regulator set to 1050psi.

6) Open valve H1. Wait until chamber pressure reaches ~1050psi before

proceeding.

7) Open valve H2.

8) Open valve H3 for a minimum of 10minutes.

9) Close valves H1, H2, and H3.

10) Turn on hotplate electrical power heater switch on front right panel of chamber

assembly as shown in Figure B.4.

Page 222: G_O'Brien PhD Dissertation

205

11) Verify and maintain chamber temperature above 40°C using thermocouple

temperature measurement probe as shown in Figure B.4.

12) Verify chamber pressure is greater than 1072psi (typically 1250-1350psi) using

chamber pressure gage as shown in Figure B.5 for a minimum of 5minutes.

13) Open valve H3 and verify/maintain chamber temperature above 40°C using

hotplate control with thermocouple probe measurement data as shown in Figure

B.4.

14) Turn off hot plate electrical heater switch as shown in Figure B.4.

15) Remove ¼ inch stainless steel CO2 supply line using crescent wrench.

16) Remove eight cap bolts and cap.

17) Remove MEMS sample/process complete.

B.5 Super Critical CO2 Chamber Summary/Conclusion

A super critical CO2 chamber has been designed, fabricated, and characterized for

use with MEMS devices where release stiction [125] is an identified problem. The

chamber accommodates 100mm and 150mm silicon wafer samples. In addition, a

chamber extension sleeve has been fabricated with 24 100mm wafers processed in a

single run to demonstrate batch capability of the super critical CO2 process.

Page 223: G_O'Brien PhD Dissertation

206

APPENDIX C

DEEP REACTIVE ION ETCH (DRIE) TOOL CHARACTERIZATION

High aspect ratio beam/trench arrays were etched into single crystal silicon substrates

(100 orientation) using a Surface Technology Systems (STS) deep reactive ion etch

(DRIE) tool. Process input parameters are varied using high/low values for etch cycle

time, passivation cycle time, RF coil power, and SF6 flow rate. The silicon etch process

is characterized using photo-resist masked trench arrays varied from 1.5μm through 6μm

in both width and spacing. A design of experiments (DOE) approach is used to model

the following measured outputs: 1) trench depth (R2=0.985), 2) lateral trench etch

(R2=0.852), 3) trench sidewall angle (R2=0.815), and 4) aspect ratio dependent etch

(R2=0.942), where R2 represents the correlation between actual and model predicted

values. The presented characterization models are employed to form beams as small as

300nm wide etched to a depth greater than 15μm with near vertical sidewalls using

standard photolithography equipment. In addition, the provided models are exploited to

produce a dual re-entrant/tapered beam etch release process. Released silicon beams are

demonstrated over 1200μm long and 30μm thick with a base width of 300nm.

C.1 MEMS Based Deep Reactive Ion Etch Background

High aspect ratio silicon structures are desired in MEMS devices such as

accelerometers [139] and gyroscopes [69, 89]. Fluorine based chemistry is the common

choice for deep silicon etching because of its high etch rate and selectivity. Fluorine etch

anisotropy can be improved by using a time multiplexed plasma etch and passivation

process previously developed by Bosch [180]. Etching of silicon microstructures with

feature sizes typically ranging from two to hundreds of microns have been thoroughly

studied with etch parameters extensively characterized [181-183]. Fluorine based

Page 224: G_O'Brien PhD Dissertation

207

chemistries have been previously shown to significantly increase both selectivity and etch

rate in excess 100:1 and 10μm/minute [183] respectively. Deep reactive ion etching of

silicon trenches based on Cl2 chemistry [184] exhibits slow silicon etch rates and lower

selectivity toward the desired SiO2 masking film [185], typically 20-30:1. Photo-resist

etch selectivity in Cl2 chemistry is on the order of 1:1 when compared to silicon,

practically excluding its use as an etch mask in deep trench etching. In contrast to

chlorine, fluorine radicals etch silicon without the need for ion impact assistance resulting

in an isotropic etch. Anisotropy has previously been improved for SF6 based chemistries

by ion impact assistance coupled with sidewall passivation using polymer deposition

[180] and/or O2 plasma oxidation and re-deposition at the silicon sidewall surface [186,

187]. The introduction of O2 during the etch cycle has also been previously suggested to

improve anisotropy by acting as a getting agent for carbon [188]. In any case, the trench

width is generally increased as compared to the original mask opening due to the

presence of mixed silicon etching of the sidewall typically on the order of hundreds of

nanometers.

The passivation cycle, ranging from 4 to 8 seconds, deposits a fluorocarbon polymer

on the wafer surface using C4F8 as a plasma source gas. The fluorocarbon polymer is

comprised of a chain of CF2 molecules similar in composition to Teflon with a film

thickness of approximately 10-50nm. The following etch cycle, ranging from 4 to 12

seconds, uses SF6 as a plasma source gas to etch silicon. The ion assisted SF6 etch

removes the polymer passivation on exposed horizontal surfaces prior to etching the

underlying silicon. Scalloping occurs when chemically reactive fluorine is adsorbed at a

non-passivated silicon trench sidewall surface resulting in a localized isotropic silicon

etch. Trench sidewall scalloping is typically more pronounced at the top, lessening in

severity from top to bottom. The STS inductively coupled plasma etch tool cross section

with first five steps for the etch sequence are shown in Figures C.1 and C.2 respectively.

Page 225: G_O'Brien PhD Dissertation

208

RFMatchingUnit

Plasma

Si Wafer

RFMatchingUnit

WaferChuck

Si Wafer

Helium ClampCoolingInlet/Outlet

SealedBellowsPumping Port

CeramicProcessChamberWalls

IsolationValve

InspectionWindow

WeightedMechanicalClamp

Figure C.1 Surface Technology Systems deep reactive ion etch tool cross section.

Mask

SiliconSubstrate

Pre-Etch Step 3: Passivate

Step1: Passivate Step 4: Etch

Step 2: Etch Step 5: Passivate

Polymer (CF2)

+ SF+n

F

SF+n

F

+

CF2

CF2

Scalloping

Mask

SiliconSubstrate

Pre-Etch Step 3: Passivate

Step1: Passivate Step 4: Etch

Step 2: Etch Step 5: Passivate

Polymer (CF2)

++ SF+nSF+n

F

SF+nSF+n

F

++

CF2

CF2

Scalloping

Figure C.2 STS etch/passivation algorithm trench sidewall scalloping example.

Smaller feature size with larger aspect ratio is typically preferred in MEMS

accelerometer and gyroscope proof mass suspension tethers. This appendix presents a

DOE based characterization of silicon deep trench etching using typical input parameters

for the STS DRIE tool. Characterization results are used to form sub-micron MEMS

Page 226: G_O'Brien PhD Dissertation

209

suspension tethers as beams released from the substrate using typical photolithography

minimum feature sizes of 1μm-6μm.

C.2 Micrometer Width Trench Arrays

A Surface Technology Systems (STS) DRIE tool was used with 1.3μm thick positive

photo-resist (AZ-1813) to pattern trench arrays etched in this experiment. Fixed trench

width was maintained on an individual array basis while inter trench spacing (beam

width) was varied from 1μm to 6μm. Three fixed trench width arrays of 2μm, 4μm, and

6mm are evaluated in this paper. An array with fixed layout defined trench width of 2μm

is shown in Figure C.3.

Bottom Width

Top Width

Depth

Figure C.3 Silicon trench array measurements used to characterize STS DRIE tool.

A design of experiments (DOE) approach provides a viable method to evaluate the

maximum number of simultaneous input variables producing a statistically significant

change in a specific output variable over a minimum number of evaluated samples [189].

DOE also provides rank order of statistical significance regarding input variable versus

modeled output variable responses. Interactions of 1st and higher orders can also be

evaluated simultaneously among the input variables versus output responses. Proper

choice of input variable levels was required to preclude artificial correlation of input

variables. Typical STS process parameters (etch cycle time, passivation cycle time, RF

Page 227: G_O'Brien PhD Dissertation

210

coil power, and SF6 flow rate) were varied in this 2 level (high/low) screening experiment

as shown in Table C.1.

Table C.1 STS etch tool screening experiment input parameters. Level Pattern Etch (sec) Passivate (sec) Power (Watts) SF6 Flow (sccm)

1 ---- 4 4 600 1302 ---+ 4 4 800 1303 --+- 4 4 600 1604 --++ 4 4 800 1605 -+-- 4 8 600 1306 -+-+ 4 8 800 1307 -++- 4 8 600 1608 -+++ 4 8 800 1609 +--- 12 4 600 13010 +--+ 12 4 800 13011 +-+- 12 4 600 16012 +-++ 12 4 800 16013 ++-- 12 8 600 13014 ++-+ 12 8 800 13015 +++- 12 8 600 16016 ++++ 12 8 800 160

The sample size used in this experiment consisted of sixteen silicon wafers with nine

scanning electron microscope (SEM) based measurement sites per wafer. Layout defined

trench width and spacing were also included as model geometric variable inputs over all

levels shown in Table C.1. The modeled output variables were trench etch depth, lateral

trench etch width, trench sidewall angle, and aspect ratio dependent etch (ARDE). The

output models were evaluated using JMP statistical software. Input variables observed to

produce weak influence (less than 5% increase in model R2) on model prediction were

excluded. The total etch duration was fixed at 8 minutes for all sample measurements

incorporated into the presented models. A constant O2 flow rate of 12sccm was

introduced during the etch cycle to improve anisotropy.

C.3 Trench Depth Model

Trench etch depth was modeled (R2=0.985) with the following input variables listed

in order of decreasing statistical significance: 1) etch cycle time, 2) passivation cycle

Page 228: G_O'Brien PhD Dissertation

211

time, 3) RF coil power, as shown in Figure C.4. Etch rate can be extracted from the

contour plot shown in Figure 3 by dividing the etch depth by the 8 minute etch period.

An example of calculated etch rate for the following input parameters (etch=10s,

passivate=5s, RF coil power=800W) is modeled as 19μm deep over the 8min duration, or

2.4μm/min.

Power (Watts)=600

4

5

6

7

800

22

44

66

88

1010

1212 1414 1616 1818 2020 2222 2424

3 4 5 6 7 8 9 10 11 12 13Etch (sec)

Power (Watts)=700

4

5

6

7

800

22

44

66

88

10101212 1414 1616 1818 2020 2222 2424

3 4 5 6 7 8 9 10 11 12 13Etch (sec)

Power (Watts)=800

4

5

6

7

8

00

22

44

66

88

1010 1212 1414 1616 1818 2020 22222424

3 4 5 6 7 8 9 10 11 12 13Etch (sec)

Figure C.4 Trench depth model as a function of passivation and etch cycle time for

individual RF coil power inputs of 600, 700, and 800W.

C.4 Lateral Trench Etch Model

The lateral trench etch model was referenced to the trench top width measurement.

As a result, the lateral trench etch model defines the lateral mask undercut/erosion at the

photo-resist/silicon interface.

Lateral trench etch was modeled (R2 = 0.852) with the following input variables listed

in order of decreasing significance: 1) etch cycle time, 2) passivation cycle time, and 3)

RF etch power, as shown in Figure C.5.

Page 229: G_O'Brien PhD Dissertation

212

Power (Watts)=600

4

5

6

7

8

00

0.10.1

0.20.2

0.30.3

0.40.4

0.50.5

0.60.6

0.70.7

3 4 5 6 7 8 9 10 11 12 13Etch (sec)

Power (Watts)=700

4

5

6

7

8

000.10.1

0.20.2

0.30.3

0.40.4

0.50.5 0.60.60.70.7

0.80.8

3 4 5 6 7 8 9 10 11 12 13Etch (sec)

Power (Watts)=800

4

5

6

7

8

00

0.10.1

0.20.2

0.30.3

0.40.40.50.5

0.60.60.70.7

0.80.8

0.90.9

3 4 5 6 7 8 9 10 11 12 13Etch (sec)

Figure C.5 Lateral trench etch model as a function of passivation and etch cycle time

for individual RF coil power inputs of 600, 700, and 800W.

The lateral trench etch model was re-evaluated with the following input variables

listed in order of decreasing significance: 1) etch cycle time, 2) passivation cycle time, 3)

RF etch power, and 4) layout defined trench width. The second lateral trench etch model

(R2 = 0.901) exhibited an increase of only 4.9% in prediction as compared to the initial

model. Although the second model accurately predicts the trend of higher etch rate for

larger width trenches, the small increase in prediction as compared to added complexity

should be noted. Second model dependence upon trench width using cases of 2μm, 4μm,

and 6μm wide trenches is shown in Figure C.6.

Power (Watts)=800 Tr Width (u)=2

4

5

6

7

800

0.10.1

0.20.2

0.30.3

0.40.4

0.50.5

0.60.6

0.70.7 0.80.8

3 4 5 6 7 8 9 10 11 12 13Etch (sec)

Power (Watts)=800 Tr Width (u)=4

4

5

6

7

8

00

0.10.1

0.20.2

0.30.3

0.40.4

0.50.5

0.60.6

0.70.7

0.80.8 0.90.9

3 4 5 6 7 8 9 10 11 12 13Etch (sec)

Power (Watts)=800 Tr Width (u)=6

4

5

6

7

8 00

0.10.1

0.20.2

0.30.3

0.40.4

0.50.5

0.60.6

0.70.7

0.80.80.90.9 11

3 4 5 6 7 8 9 10 11 12 13Etch (sec)

Figure C.6 Lateral etch model as a function of passivation and etch cycle time for an RF

coil power of 800W with 2μm, 4μm, and 6μm trench widths.

Page 230: G_O'Brien PhD Dissertation

213

Statistical model dependence on inter-trench spacing (beam width) was not observed.

C.5 Sidewall Angle Model

Trench sidewall angle [190] was measured as the straight angle between the top and

bottom trench width measurements as shown in Figure C.7.

180º-θθ

Photoresist

SiliconSubstrate

Trench180º-θθθθ

Photoresist

SiliconSubstrate

Trench

Figure C.7 Trench sidewall angle measurement.

Trench sidewall angle was initially modeled with the following input variables listed

in order of decreasing statistical significance: 1) etch cycle time, 2) passivation cycle

time, and 3) RF coil power. The trench sidewall angle model (R2 = 0.815) is a weak, but

statistically significant function of layout defined trench width. Additional modeling

included layout defined trench width with an increase in prediction of only 2.4% (R2 =

0.839). Although the prediction increase is small, the etch trend is captured and results

for the layout defined 2μm and 6μm wide trenches are shown in Figures C.8 and C.9

respectively.

Page 231: G_O'Brien PhD Dissertation

214

Tr Width (u)=2 Power (Watts)=600

4

5

6

7

887.587.5

888888.588.5

8989

89.589.5

909090.590.5

9191

3 4 5 6 7 8 9 10 11 12 13Etch (sec)

Tr Width (u)=2 Power (Watts)=700

4

5

6

7

8 8888

88.588.5 8989 89.589.5

9090 90.590.5

9191

3 4 5 6 7 8 9 10 11 12 13Etch (sec)

Tr Width (u)=2 Power (Watts)=800

4

5

6

7

888.588.5

8989

89.589.5

9090

90.590.5

9191

3 4 5 6 7 8 9 10 11 12 13Etch (sec)

T

Figure C.8 Trench sidewall angle model as a function of passivation and etch cycle time

for a fixed 2μm trench width and RF coil power of 600, 700, and 800W.

Tr Width (u)=6 Power (Watts)=600

4

5

6

7

886.586.5

8787

87.587.5

8888

88.588.58989

89.589.5

909090.590.5

9191

3 4 5 6 7 8 9 10 11 12 13Etch (sec)

Tr Width (u)=6 Power (Watts)=700

4

5

6

7

88787

87.587.5

8888

88.588.58989

89.589.5 9090

90.590.5

9191

91.591.5

3 4 5 6 7 8 9 10 11 12 13Etch (sec)

Tr Width (u)=6 Power (Watts)=800

4

5

6

7

8 87.587.5

8888

88.588.5 8989

89.589.5

9090

90.590.5

9191 91.591.5

3 4 5 6 7 8 9 10 11 12 13Etch (sec)

Figure C.9 Trench sidewall angle model as a function of passivation and etch cycle time

for a fixed 6μm trench width and RF coil power of 600, 700, and 800W.

To produce a near vertical sidewall we note that the slope of the 90° sidewall angle

model line, shown in both Figures C.8 and C.9, is approximately 1. Our model predicts

that for etch cycle times greater than 8 seconds, the corresponding passivation cycle time

producing a 90º sidewall is four seconds shorter overall. Although the SF6 flow rate and

mask defined trench spacing were both statistically significant they had less than a 5%

affect on model R2 when factored either together or separately. As a result, both the SF6

and trench width input parameters were excluded from the model.

Page 232: G_O'Brien PhD Dissertation

215

C.6 Aspect Ratio Dependent Etch

Aspect ratio dependent etch [182] trench depth was modeled with the following input

variables listed in order of decreasing statistical significance: 1) etch cycle time, 2)

passivation cycle time, 3) mask defined trench width, and 4) RF coil power. The ARDE

model (R2 = 0.942) describes the relationship between layout defined trench width and

etch depth; as the trench width is decreased the etch depth also decreases for a fixed etch

and passivation cycle time. The ARDE trench depth model is shown in Figure C.10 with

a constant etch cycle time of 12s.

Etch (sec)=12 Power (Watts)=600

4

5

6

7

81616

1818

2020

2222

2424

2626

2 3 4 5 6Tr Width (u)

Etch (sec)=12 Power (Watts)=700

4

5

6

7

81818

2020

2222

2424

2626

2 3 4 5 6Tr Width (u)

Etch (sec)=12 Power (Watts)=800

4

5

6

7

82020

2222

2424

2626

2 3 4 5 6Tr Width (u)

Figure C.10 Trench depth model ARDE effects with a fixed 12s etch cycle and RF

power of 600, 700, and 800W.

The ARDE can be minimized by adjusting the ratio of etch to passivation cycle time

[182]. As the ratio of etch to passivation cycle time approaches unity, the etch rate

distributed across the 2μm through 6μm layout defined trench widths is relatively

uniform for a fixed 8s etch cycle time as shown in Figure C.11.

Page 233: G_O'Brien PhD Dissertation

216

Etch (sec)=8 Power (Watts)=600

4

5

6

7

888

1010

1212

1414

1616

1818

2020

2 3 4 5 6Tr Width (u)

Etch (sec)=8 Power (Watts)=700

4

5

6

7

888

1010

1212

1414

1616

1818

2 3 4 5 6Tr Width (u)

Etch (sec)=8 Power (Watts)=800

4

5

6

7

8 1010

1212

1414

1616

1818

2 3 4 5 6Tr Width (u)

Figure C.11 Trench depth model ARDE effects with a fixed 8s etch cycle and RF power

of 600, 700, and 800W.

However, a 1:1 etch to passivation cycle significantly reduces the overall etch rate

and the resulting sidewall angle is less than vertical. The sidewall profile observed for

levels 1 through 4 were tapered (ϑ<90°) and all trenches formed using these etch input

parameters exhibited grass [186] formation as shown in Figure C.12.

Figure C.12 Tapered etch with silicon grass formation in large width trenches.

The re-entrant (ϑ>90°) and vertical (ϑ≅90°) sidewall trenches were not observed to

form grass. The re-entrant etch trench sidewall is represented by levels 9 through 12

while the vertical trench etch profiles are represented by levels 13 through 16, as shown

in Table C.1. Grass was observed when the ratio of etch to passivation cycle time was

Page 234: G_O'Brien PhD Dissertation

217

less than 3:2. Also, the surface density of grass was observed to significantly increase as

the ratio of etch to passivation cycle time was decreased below 1:1 respectively.

C.7 Trench Interspaced Sub-micron Beam Formation

Beam arrays with a photo defined 1.5μm trench spacing were etched for 8min using

level 15 etch parameters, as shown in Table C.1. The lateral trench etch model predicted

a post etch 0.5μm beam width. The actual post etch beam width was approximately

0.3μm, as shown in Figure C.13.

0.3μm0.3μm

Figure C.13 Sub-micron (300nm) beam width with near vertical sidewalls.

Scalloping of the trench sidewall near the top of the trench was observed as large as

95nm. Sidewall asperities near the trench midsection were limited to <50nm. Beam

sidewall angle was estimated as nearly vertical.

C.8 Submicron Beam Re-entrant Etch Release

A 10 minute re-entrant etch (level 9 from Table C.1) was immediately followed with

a 20 minute tapered etch (level 1 from Table C.1) to release beams from the substrate.

Page 235: G_O'Brien PhD Dissertation

218

The released silicon beam tip is approximately 1250μm long, 30μm thick, with a

maximum width of 300nm at the etch mask/Si interface as shown in Figure C.14.

SideView

FrontView

~30μm

~300nmwide atmaskinterface

Re-entrant etch released beam tip

Beam TipDetail

1500μm

SideView

FrontView

~30μm

~300nmwide atmaskinterface

Re-entrant etch released beam tip

Beam TipDetail

1500μm

Figure C.14 Midpoint re-entrant etch released beam.

This represents an aspect ratio of approximately 100 (0.3μm/30μm). The rough

bottom etch is attributed to abrupt switching between re-entrant and tapered recipes. The

abrupt switching rationale is supported by the rough etch band located at the trench

midpoint corresponding to the STS etch recipe transition region on large width silicon as

shown in Figure C.15.

Re-entrant Etch Beam

TaperedEtch Beam

STS Etch RecipeTransition

Re-entrant Etch Beam

TaperedEtch Beam

STS Etch RecipeTransition

Figure C.15 Midpoint re-entrant etch released beam detail.

Page 236: G_O'Brien PhD Dissertation

219

Future release etch efforts will include a chamber gas stabilization period between the

re-entrant and tapered STS etch recipe transition.

The ratio of etch to passivation cycle time was changed from 3:1 to 1:1, with all other

input parameters held constant, resulting in a swing from re-entrant to tapered sidewall

etching at the beam midpoint respectively. The silicon wafers (100 orientation) were

insitu doped with phosphorous during Czochralski growth [148] to a uniform bulk

resistivity of 7.5-12.5W-cm. The absence of a buried dielectric layer coupled with a

photo-resist etch mask suggests that the angle of ion assisted incidence is not

significantly affected by trapped dielectric charge [147, 190] in the case presented in this

appendix.

C.9 Submicron Beams and Trenches

Lateral and vertical trench etching was evaluated at the submicron level using a nano-

imprint defined [191] oxide hardmask. Trenches 350nm wide with a 700nm period were

formed using a 120nm thick oxide etch mask. Etch parameters were fixed to 4s

passivation cycle, RF coil power of 800W, and SF6 flow rate of 130sccm, for a total

duration of 20 minutes. The etch cycle time was varied over three evaluated etch

samples. The first sample etch cycle time was set to 4.5s. The 4.5s etch sample

exhibited an average trench depth was measured as 10.3μm (σ=0.7μm) where

σ represents the standard deviation. Lateral trench etching was observed on the order of

95nm per side with scalloping sidewall asperities as large as 75nm were observed using

the 4.5 second etch cycle time as shown in Figure C.16.

Page 237: G_O'Brien PhD Dissertation

220

Figure C.16 Sub-micron lateral trench etching using 4.5s etch cycle.

A 1:1 etch to passivation cycle time ratio was chosen to minimize lateral trench

etching. Lateral trench etching on the order of 30nm per side with scalloping sidewall

asperities as large as 75nm were observed using a 4.0 second etch cycle time described

by level 2 etch parameters as described in Table C.1. Surface roughness due to

scalloping can be reduced post etch by thermal oxidation of the sidewall followed by

removal of the oxide [192]. The average trench depth was measured as 9.7μm

(σ=0.4μm) as shown in Figure C.17.

Figure C.17 Minimized sub-micron lateral trench etching using 4.0s etch cycle.

Negative lateral trench etching on the order of 95nm per side with scalloping sidewall

asperities as large as 45nm were observed using a 3.5 second etch cycle time described

Page 238: G_O'Brien PhD Dissertation

221

by level 3 etch parameters as described in Table C.1. The average trench depth was

3.9μm (σ=0.3μm) as shown in Figure C.18.

Figure C.18 Negative sub-micron lateral trench etching using 3.5s etch cycle.

The average etched trench depth for the 4.0s and 3.5s etch cycle samples were

10.3μm and 3.9μm respectively representing a decrease in etch rate on the order of 2.6X.

The post etch trench for the 3.5s etch cycle was approximately 150nm wide as compared

to the SiO2 masked 350nm wide opening. This negative lateral etch represents an

approximate reduction of 0.2μm in the SiO2 masked trench width.

Silicon etching was not observed for an etch cycle of 3.2s due to excessive CF2

deposition at the oxide hard mask and exposed silicon surface. A combination of CF2

pile-up and silicon surface oxidation may be responsible for the smaller than mask

defined trenches observed. Oxygen has been previously proposed to passivate the silicon

surface [186, 187] by forming an oxide film and may also protect the sidewall at the

SiO2/Si interface resulting in a smaller than mask defined etched trench width.

Sub-micron layout defined beam and trench spacing, with or without an SiO2 hard-

mask, requires lateral silicon etching to be minimized by setting the etch to passivation

Page 239: G_O'Brien PhD Dissertation

222

ratio with approximately 1:1 values. As a result, very little sidewall etch angle control is

afforded sub-micron layout defined beam spacing since all etch profiles in this regime are

slightly tapered. In addition, trench widths larger than 500nm were observed to form

grass [186] using a near 1:1 etch to passivation cycle ratios. Trench widths in excess of

500nm require an etch to passivation ratio larger than 3:2 respectively where silicon grass

formation is undesired.

Scalloping has previously been eliminated using electroplated Ni masks [184]. A

dual trench etch process has also been previously shown to significantly reduce both

sidewall scalloping and inter trench depth variation in sub-micron trench arrays by using

HBr/Cl chemistry to etch the initial 500nm of trench depth followed by a 10μm etch in a

SF6/C4F8 based time multiplexed process [193] sequence. This diffusion rate limited

deep etch process is very sensitive to sub-micron inter trench sidewall scallop variation

across an array as the silicon etch byproduct is transported away from the trench bottom

in gas phase causing an increase the etched trench depth variability. This microscopic

loading effect manifests itself as an etch rate dependence on feature size and array density

[194]. Scalloping asperities were observed to decrease where the etch to passivation ratio

was fixed and both etch and passivation cycle times were decreased resulting in a lower

overall etch rate and higher sidewall scallop frequency versus normalized depth.

C.11 Initial LAM 9400-TCP HBR/Cl etch with subsequent STS DRIE

It is notable that the scalloping sidewall asperity is much smaller in the middle and

bottom part of the trench than in the top part of the trench. The scalloping near the top of

the trench was further reduced by performing a two step etch process. The initial trench

depth of 500nm was etched using HBr/Cl chemistry in a LAM 9400-TCP etch tool while

the trench remainder was etched to a depth of 10.3μm (σ=0.1μm) using the STS tool with

Page 240: G_O'Brien PhD Dissertation

223

parameters set as etch cycle=4s, passivation cycle=4s, RF power=800W and SF6 flow

rate=130sccm, as shown in Figure C.19.

Figure C.19 Dual etch sidewall scallop reduction process.

A large sidewall asperity of approximately 65nm due to scalloping exists at the

Lam/STS etch interface near the top of the trench, while the remaining sidewall asperities

are less than 25nm.

The etch rates in these processes are on the order of 0.5-1.5μm/min, much higher than

that of high-aspect ratio sub-micron Si trench etch based on Cl2 with an ECR source,

which is on the order of 0.1μm/min [184]. Also the etch selectivity over oxide is more

than 10 times of that for ECR etch with Cl2. These attributes make these recipes very

attractive for fabricating sub-micron high-aspect ratio structures for optical gratings and

Page 241: G_O'Brien PhD Dissertation

224

MEMS applications such as accelerometer [162] proof mass support tethers utilizing an

etch release process as described by Shaw et. al [195].

In addition, the dual etch process reduced the trench array depth variation from a

measured standard deviation of 0.7μm to 0.1μm representing significant improvement of

etch repeatability across the wafer sample as shown in Figures C.17 and C.19

respectively. Trench depth non-uniformity across the wafer can be significantly reduced

using a two step etch process where scalloping is minimized near the trench opening as

demonstrated in Figure C.19.

C.10 DRIE Tool Characterization DOE Model Summary/Conclusion

Sub-micron high aspect ratio beams etched into silicon wafers have been

demonstrated using standard photolithography equipment in conjunction with STS deep

reactive ion etch equipment. Models were presented for 1) trench depth (R2=0.985), 2)

trench sidewall angle (R2=0.815), 3) trench lateral etch (R2=0.852), and 4) aspect ratio

dependent etch (R2=0.942). The most significant parameters common throughout all four

presented models were etch cycle time, passivation cycle time, and RF coil power.

Proper mask bias can be estimated using the models presented in this paper with to form

sub-micron beam/trench designs on silicon wafer substrates with nearly vertical

sidewalls. Re-entrant etch released beams with an aspect ratio of approximately 100 are

demonstrated. Future work will address fabrication of accelerometer sub-micron width

high aspect ratio tethers using the re-entrant etch release process. Modeled lateral etch

trends were observed on sub-micron width trench arrays with an oxide hard mask using a

1:1 etch to passivation cycle time ratio. Sidewall scalloping was observed to decrease as

the etch to passivation ratio is decreased below a 1:1 ratio respectively.

Page 242: G_O'Brien PhD Dissertation

225

APPENDIX D

SWITCHED CAPACITOR LOW PASS FILTER/AMPLIFIER

A switched capacitor circuit is provided which reduces the input signal bandwidth by

the number of discrete time averaged samples (N) per sample and hold cycle. The input

voltage signal (Vin) is time multiplexed onto N cascoded sample and hold stage

capacitors (C1-CN) as shown in Figure D.1

Figure D.1 Switched capacitor low pass filter with time averaged analog gain.

Page 243: G_O'Brien PhD Dissertation

226

The transmission gate sub-circuit is shown in Figure D.2

Vdd Vss

CNTL

outin

T-Gate4Sub-circuitSymbol

Vdd Vss

CNTL

outin

T-Gate4Sub-circuitSymbol

Figure D.2 Transmission gate sub-circuit T-Gate4.

D.1 Switched Capacitor Low Pass Filter Amplification Operation

A multi-phase (N+1) clock is used to sample and hold the input voltage signal (Vin)

using cascaded time multiplexed scheme. The example shown in Figure D.1 uses 5 clock

phases (0-4), with phase 0 used for reset while phase 4 is used to pass the discrete time

averaged and amplified signal (Vout1) to the output stage sample and hold node (Vout2).

Clock phases 1-3 discretely control sampling of the input voltage signal (Vin) and sum

the corresponding charge onto the amplified output voltage node (Vout1). Discrete time

distributed output voltage amplification (Vout1, Vout2) is demonstrated using a

Page 244: G_O'Brien PhD Dissertation

227

sinusoidal input voltage signal (Vin) with a 100mV amplitude, 800Hz frequency, and a

2.5V offset as shown in Figure D.3.

Ti me

0 . 8 0 0 ms 1 . 0 0 0 ms 1 . 2 0 0 ms 1 . 4 0 0 ms 1 . 6 0 0 ms 1 . 8 0 0 ms0 . 6 0 3 msV( o u t _ 1 ) V( i n ) V( o u t _ 2 )

2 . 2 5 V

2 . 5 0 V

2 . 7 5 V

2 . 1 4 V

2 . 8 7 V

Ref. next slide for detail

Input (100mV, 800Hz, 2.5V offset)

Output (3X Gain with 2.5V offset)

Ti me

0 . 8 0 0 ms 1 . 0 0 0 ms 1 . 2 0 0 ms 1 . 4 0 0 ms 1 . 6 0 0 ms 1 . 8 0 0 ms0 . 6 0 3 msV( o u t _ 1 ) V( i n ) V( o u t _ 2 )

2 . 2 5 V

2 . 5 0 V

2 . 7 5 V

2 . 1 4 V

2 . 8 7 V

Ref. next slide for detail

Input (100mV, 800Hz, 2.5V offset)

Output (3X Gain with 2.5V offset)

Ti me

0 . 8 0 0 ms 1 . 0 0 0 ms 1 . 2 0 0 ms 1 . 4 0 0 ms 1 . 6 0 0 ms 1 . 8 0 0 ms0 . 6 0 3 msV( o u t _ 1 ) V( i n ) V( o u t _ 2 )

2 . 2 5 V

2 . 5 0 V

2 . 7 5 V

2 . 1 4 V

2 . 8 7 V

Ref. next slide for detail

Input (100mV, 800Hz, 2.5V offset)

Output (3X Gain with 2.5V offset)

Ref. next slide for detail

Input (100mV, 800Hz, 2.5V offset)

Output (3X Gain with 2.5V offset)

Figure D.3 SPICE simulation of switched capacitor amplifier circuit.

An overlay of the control clock phases is shown in Figure D.4 which describes the

input voltage (Vin) in terms of N discrete time averaged sum steps as the output voltage

amplitude.

Ti me

9 0 0 u s 9 1 0 u s 9 2 0 u s 9 3 0 u s 9 4 0 u s 9 5 0 u s 9 6 0 u s 9 7 0 u s 9 8 0 u s 9 9 0 u s 1 0 0 0 u sV( o u t _ 1 ) V( i n ) V( o u t _ 2 )

2 . 5 0 V

2 . 7 5 V

2 . 3 4 VSEL>>

V( CLK_ 0 ) V( CLK_ 1 ) V( CLK_ 2 ) V( CLK_ 3 ) V( CLK_ 4 )0 V

2 . 5 V

5 . 0 V

0 1 2 3 40 1 2 3 4

0 1 2 3 40 1 2 3 40 1 2 3 4

Input

OutputTimeAveraging

N+2 Clocked Cycle Period

Ti me

9 0 0 u s 9 1 0 u s 9 2 0 u s 9 3 0 u s 9 4 0 u s 9 5 0 u s 9 6 0 u s 9 7 0 u s 9 8 0 u s 9 9 0 u s 1 0 0 0 u sV( o u t _ 1 ) V( i n ) V( o u t _ 2 )

2 . 5 0 V

2 . 7 5 V

2 . 3 4 VSEL>>

V( CLK_ 0 ) V( CLK_ 1 ) V( CLK_ 2 ) V( CLK_ 3 ) V( CLK_ 4 )0 V

2 . 5 V

5 . 0 V

0 1 2 3 40 1 2 3 4

0 1 2 3 40 1 2 3 40 1 2 3 4

Input

OutputTimeAveraging

N+2 Clocked Cycle Period

0 1 2 3 40 1 2 3 40 1 2 3 40 1 2 3 4

0 1 2 3 40 1 2 3 40 1 2 3 40 1 2 3 40 1 2 3 40 1 2 3 4

Input

OutputTimeAveraging

N+2 Clocked Cycle Period

Figure D.4 SPICE simulation of switched capacitor amplifier with clock phases.

Page 245: G_O'Brien PhD Dissertation

228

The output voltage amplitude (Vout) is a function of the offset voltage (Vos) and the

ratio of input voltage (Vin) charge sampling capacitors (C1-CN) to the switched capacitor

amplifier feedback capacitor (CF) as described by Eq. D.1.

VosC

CCCVinVosVoutF

N +⎟⎟⎠

⎞⎜⎜⎝

⎛ ++−≅

…21)( (D.1)

Although the example listed above set the value of the charge sampling capacitors

(C1-CN) equal to the integration feedback capacitor (CF), analog gain greater than unity is

desirable in practical applications. The output signal bandwidth is reduced by discrete

values of N only, which is independent of capacitor ratio based analog gain. An example

of a practical application would set the ratio of input voltage (Vin) charge sampling

capacitors (C1-CN) to integration feedback capacitor (CF) as 2. Using N=3 cascaded

charge sampling capacitors (C1-C3) would yield a single stage gain of 6 where CF=C1/2,

and C1=C2=C3. Assuming a switched capacitor front end 60kHz bandwidth, as described

in Chapter 6, the reduced bandwidth realized after a complete cycle is reduced by N=3 as

20kHz. Cascading two additional stages would result in a theoretical system gain of 63

yielding a system bandwidth reduced by 33 to 2.2kHz as shown in Figure D.5.

Clock Phase Generation Digital Control Logic

Clock Phase Generation Digital Control Logic

Clock Phase Generation Digital Control Logic

Cascaded Switched Capacitor Low Pass Filter/AmplifierN=3, CF=C1/2

Cascaded Switched Capacitor Low Pass Filter/AmplifierN=3, CF=C1/2

Cascaded Switched Capacitor Low Pass Filter/AmplifierN=3, CF=C1/2

0 1 2 3 4 0 1 2 3 4 0 1 2 3 4ClockPhases

MasterClock Frequency

CLK CLK/N CLK/N2

Vin+

Vout_stage1-

BWin=60kHz BW1=20kHzA=6

BW2=6.6kHzA=36

Vout_stage2

BW3=2.2kHzA=216

Vout_stage3+

-

ClockFrequencyReduction

ClockFrequencyReduction

Clock Phase Generation Digital Control Logic

Clock Phase Generation Digital Control Logic

Clock Phase Generation Digital Control Logic

Cascaded Switched Capacitor Low Pass Filter/AmplifierN=3, CF=C1/2

Cascaded Switched Capacitor Low Pass Filter/AmplifierN=3, CF=C1/2

Cascaded Switched Capacitor Low Pass Filter/AmplifierN=3, CF=C1/2

0 1 2 3 40 1 2 3 4 0 1 2 3 40 1 2 3 4 0 1 2 3 40 1 2 3 4ClockPhases

MasterClock Frequency

CLK CLK/N CLK/N2

Vin+

Vout_stage1-

BWin=60kHz BW1=20kHzA=6

BW2=6.6kHzA=36

Vout_stage2

BW3=2.2kHzA=216

Vout_stage3+

-

ClockFrequencyReduction

ClockFrequencyReduction

Figure D.5 Cascaded switched capacitor low pass filter/amplifier.

Page 246: G_O'Brien PhD Dissertation

229

D.2 Switched Capacitor Low Pass Filter/Amplifier Summary/Conclusion

MEMS capacitive acceleration sensors intended for use in automotive applications

are typically limited to relatively small output voltage signal bandwidths typically

ranging from 400-800Hz. Switched capacitor techniques to reduce MEMS acceleration

sensor output signal bandwidth, such as Bessel filters [48], are typically implemented.

However, Bessel filters typically provide a gain of unity in the pass band. As a result,

additional gain stage circuits are required with this architecture implementation.

A cascoded switched capacitor amplifier design has been presented to allow for input

signal voltage low pass filtering and amplification in a single gain stage. Cascading

multiple stages of the design allows for large increases in signal amplification in addition

to significantly reduced signal bandwidth. As a result, the switched capacitor low pass

filter/amplifier design presented in this appendix could be used to replace the Bessel filter

and adjacent gain stages as previously described in Chapter 6. Future research will

address this topic.

Page 247: G_O'Brien PhD Dissertation

230

APPENDIX E

STICTION ASSISTED SOI SUBSTRATE ELECTRICAL CONTACT

Large surface area silicon substrate contacts with multiple sacrificial etch hole arrays

were connected to bond pads via electrically conductive folded beam springs in a 20μm

thick SOI structural film. The beam springs are designed to deflect the proof mass to the

substrate using surface tension experienced during de-ionized H2O rinse/evaporation.

Upon contact with the substrate, stiction is used to maintain mechanical and electrical

contact between SOI and substrate silicon layers as shown in 3D microscope Figure E.1.

Single and dual folded beam spring substrate contacts are shown in Figures E.2 and E.3.

BondPad

BondPad

Proof Masses

SpringsBondPad

BondPad

Proof Masses

Springs

Figure E.1 Stiction assisted substrate contact bond pad structures.

Page 248: G_O'Brien PhD Dissertation

231

BondPad

FoldedBeamSpring

ProofMass

BondPad

FoldedBeamSpring

ProofMass

Figure E.2 Dual folded beam spring (left side) stiction assisted substrate contact.

Bond Pad

ProofMass

FoldedBeamSpring

Bond Pad

ProofMass

FoldedBeamSpring

Figure E.3 Single folded beam spring (right side) stiction assisted substrate contact.

Page 249: G_O'Brien PhD Dissertation

232

E.1 Substrate Contact Folded Beam Mechanical Spring Constants

The dual and single folded beam spring displacements in a 1g field directed along the

z-axis were simulated using ANSYS finite element analysis software. The single folded

beam suspension mechanical spring constant (KZ_Single) was calculated using the

maximum proof mass displacement (Δz), and the mass of the substrate contact plate

(msub) as shown in Figure E.4.

Figure E.4 Single folded beam suspension mechanical spring constant simulation.

Similarly, the dual folded beam suspension mechanical spring constant (KZ_Dual) was

calculated using the maximum proof mass displacement (Δz), and the mass of the

substrate contact plate (msub) as shown in Figure E.5.

Page 250: G_O'Brien PhD Dissertation

233

Figure E.5 Dual folded beam suspension mechanical spring constant simulation.

E.2 Substrate Contact Surface Tension Based Displacement Calculation

Evaporation of de-ionized H2O from the wafer surface, after sacrificial oxide etch in

hydrofluoric acid, causes a z-axis directed force upon the underside of the substrate

contact proof mass plate. This z-axis force is a function of the substrate contact plate

perimeter (P) and surface tension (γ=0.071N/m) of H2O assuming a zero contact angle

(φ=0) as described by Eq. E.1.

)cos(φγPFSurf = (E.1)

The perimeter (P=3.1*10-3m) of the contact plate includes the outside perimeter

(LSub=100*10-6m) plus the summation of a 13x13 x-y grid array of sacrificial oxide etch

holes (LSac=4*10-6m) as described by Eq. E.2.

Page 251: G_O'Brien PhD Dissertation

234

)4(13)(4 2SacSub LLP += (E.2)

The surface tension force due to H2O evaporation after sacrificial oxide etch is

calculated as FSurf=220μN by substituting Eq. E.2 into E.1.

The surface tension based displacement of the single folded beam spring substrate

contact (ΔzSingle=40.3μm) is defined by Eq. E.3.

SingleZ

SurfSingle K

Fz

_

=Δ (E.3)

The surface tension based displacement of the dual folded beam spring substrate

contact (ΔzSingle=3.7μm) is defined by Eq. E.4.

DualZ

SurfDual K

Fz

_

=Δ (E.4)

The initial gap defined by the SOI buried oxide (BOX) thickness is 2μm. Therefore,

the surface tension displacements listed above guarantee silicon to silicon contact

between the proof mass plate and substrate by design.

E.3 Stiction Assisted Substrate Contact Electrical Measurements

Electrical measurements of the stiction assisted substrate contacts was performed on

several identical devices using probe needles connected directly to bond pad and silicon

substrate with an HP-34401 digital multi-meter. Electrical resistance measurements,

localized to the contact site, varied from as low as 396Ω to as high as 1242Ω. The large

Page 252: G_O'Brien PhD Dissertation

235

variation in electrical resistance measurements is attributed to a non-planar post stiction

surface contact angle [125] between the electrode and substrate. Future research will

focus on identifying the actual mechanism causing the large electrical resistance variation

observed.

E.4 Stiction Assisted SOI Substrate Contact Summary/Conclusion

A stiction assisted SOI substrate contact has been demonstrated for use in MEMS

device fabrication. Surface tension of H2O during a wet rinse/evaporation process step

was used to deflect the substrate contact plate to the silicon substrate. Stiction is

responsible for maintaining the physical contact of the proof mass plate and substrate

silicon surfaces after all H20 has been evaporated form the surface. Z-axis proof mass

displacement referenced to the silicon substrate was measured on actual devices using a

Zygo 3-D confocal microscope. Released device electrical resistance measurements were

performed using an HP-34401 digital muti-meter. Future work will focus on identifying

the actual mechanism causing the large electrical resistance variation observed.

Additionally, future research will evaluate the use of large amplitude voltage and current

pulses post substrate contact stiction initiation to evaluate the potential of decreasing

electrical resistance using this technique.

Page 253: G_O'Brien PhD Dissertation

236

APPENDIX F

INTEGRATED SILICON ON INUSLATOR (SOI) PROCESS FLOW

The integrated SOI process includes deep reactive ion etch (DRIE) with subsequent

trench refill using low pressure chemical vapor deposition (LPCVD) of conformal films

[63] typically used in the fabrication of CMOS integrated circuits. Multiple trench refill

steps deposit conductive and non-conductive conformal films to provide selective handle

wafer substrate electrical contact and mechanical anchor electrical insulation

respectively.

F.1 Integrated SOI Process Steps

The initial SOI is 20μm thick with a 2μm buried oxide (BOX) and 525μm thick

handle wafer as shown in Figure F.1.

SOI

BOX

Si Substrate 525μm

20μm

2μm

SOI

BOX

Si Substrate 525μm

20μm

2μm

Figure F.1 Standard SOI wafer cross section.

Page 254: G_O'Brien PhD Dissertation

237

1) Deposit Oxide (1.5kA)

Figure F.2 Deposit 1.5kA oxide.

1) Mask 1: Trench1

1) Etch Oxide (Plasma-therm)2) Etch Silicon (STS)3) Etch Oxide (Plasma-therm)

Photo-resist

1) Mask 1: Trench1

1) Etch Oxide (Plasma-therm)2) Etch Silicon (STS)3) Etch Oxide (Plasma-therm)

1) Mask 1: Trench1

1) Etch Oxide (Plasma-therm)2) Etch Silicon (STS)3) Etch Oxide (Plasma-therm)

Photo-resist

Figure F.3 Photolithography and etch of anchor trench.

1) Deposit 1.5kA LPCVD Nitride1) Deposit 1.5kA LPCVD Nitride

Figure F.4 Low pressure chemical vapor deposition (LPCVD) nitride.

Page 255: G_O'Brien PhD Dissertation

238

1) Etch nitride (Plasma-therm)2) Etch Oxide (Plasma-therm)3) Etch Silicon (STS)4) Etch Oxide (Plasma-therm)

Photo-resist

Mask 2: Substrate_Contact1) Etch nitride (Plasma-therm)2) Etch Oxide (Plasma-therm)3) Etch Silicon (STS)4) Etch Oxide (Plasma-therm)

Photo-resist

Mask 2: Substrate_Contact

Figure F.5 Photolithography and etch substrate contact trench.

1) Deposit LPCVD Polysilicon (2μm)1) Deposit LPCVD Polysilicon (2μm)

Figure F.6 Low pressure chemical vapor deposition (LPCVD) polysilicon.

1) Etch-Back Polysilicon (STS or Plasma-therm)1) Etch-Back Polysilicon (STS or Plasma-therm)

Figure F.7 Polysilicon etch-back.

Page 256: G_O'Brien PhD Dissertation

239

1) Etch Nitride (Plasma-therm)2) Etch Oxide (Plasma-therm)1) Etch Nitride (Plasma-therm)2) Etch Oxide (Plasma-therm)

Figure F.8 Nitride and oxide etch-back.

1) Mask 3: Metal (lift-off)

Photo-resist Metal

1) Mask 3: Metal (lift-off)

Photo-resist Metal

Figure F.9 Metal evaporation and lift-off.

Strip Photo-resist (lift-off)

Bond Pad Metal

Strip Photo-resist (lift-off)

Bond Pad Metal

Figure F.10 Metal lift-off photo-resist strip.

Page 257: G_O'Brien PhD Dissertation

240

1) Mask 4: Outline (STS etch)

Photo-resist

1) Mask 4: Outline (STS etch)

Photo-resist

Figure F.11 Sensor outline DRIE etch mask.

1) BOX Sac-Etch (Wet HF Acid) MEMS Device Release

Substrate ElectricalContact(Polysilicon)

BondPad

Electrically IsolatedMechanical Anchor

1) BOX Sac-Etch (Wet HF Acid) MEMS Device Release1) BOX Sac-Etch (Wet HF Acid) MEMS Device Release

Substrate ElectricalContact(Polysilicon)

BondPad

Electrically IsolatedMechanical Anchor

Figure F.12 Sacrificial buried oxide (BOX) etch.

F.2 Integrated SOI Process Summary

The integrated SOI process flow enabled the fabrication of MEMS devices with

mechanical buried oxide anchors protected by silicon nitride and polysilicon films during

sacrificial oxide etch. An electrical substrate contact is realized using auto-doped

polysilicon to allow the potential of the conductive silicon handle wafer to be

manipulated during sensor operation. MEMS devices fabricated using this process are

described/shown in chapter 5 and chapter 7 respectively.

Page 258: G_O'Brien PhD Dissertation

241

BIBLIOGRAPHY

[1] L. J. Ristic, R. Gutteridge, B. Dunn, D. Mietus, and P. Bennet, "Surface Micromachined Polysilicon Accelerometer," presented at IEEE Solid State Sensors and Actuators Workshop, Hilton Head, pp. 118-121, 1992.

[2] S. J. Sherman, W. K. Tsang, T. A. Core, R. S. Payne, D. E. Quinn, K. H. Chau, J. Farash, and S. Baum, "A Low Cost Monolithic Accelerometer; Product Technology Update," IEEE Electron Devices, pp. 501-504, 1992.

[3] L. Spangler and C. J. Kemp, "ISAAC - Integrated Silicon Automotive Accelerometer," presented at IEEE Transducers, pp. 585-588, 1995.

[4] D. R. Sparks, S. R. Zarabaldi, J. D. Johnson, Q. Jiang, M. Chia, O. Larsen, W. Higdon, and P. Borelley-Castillo, "A CMOS Integrated Surface Micromachined Angular Rate Sensor: It's Automotive Applications," presented at IEEE Transducers, pp. 851-854, 1997.

[5] M. Lutz, W. Golderer, J. Gerstenmeir, J. Marek, B. Malhofer, and D. Schubert, "A Precision Yaw Rate Sensor in Silicon Micromachining," Society of Automotove Engineers (SAE), vol. # 980267, 1998.

[6] D. D. Hoffman and M. D. Rizzo, "Chevrolet C5 Corvette Vehicle Dynamic Control System," Society of Automotive Engineers, vol. #980233, 1998.

[7] J. Yukawa, T. Nozoe, H. Ohgoshi, M. Murakami, T. Uemura, T. Nagaki, and Y. Ishai, "Angular Rate Sensor for Dynamic Chassis Control," Society of Automotive Engineers (SAE), vol. # 980269, 1998.

[8] J. Geen, "A Path to Low Cost Gyroscopy," presented at IEEE Solid State Sensors and Actuators Workshop, Hilton Head, pp. 51-54, 1998.

[9] D. B. Davies, "Analysis of Active Compensation for Shock, Vibration, and Wind-up of Disk Drives," in Masters Thesis, Massachusetts Institute of Technology, 1991.

[10] T. J. Brosnihan, A. P. Pisano, and R. T. Howe, "Micromachined Angular Accelerometer with Force Feedback," presented at ASME Conference and Expo, pp. 941-947, 1995.

[11] A. Gola, N. Bagnalasta, P. Bendiscioli, S. D. E. Chiesa, E. Lasalandra, F. Pasolini, M. Tronconi, T. Ungaretti, and A.Baschirotto, "A MEMS-based Rotational Accelerometer for HDD Applications with 2.5rad/sec2 Resolution and Digital Output," presented at European Solid State Circuits Conference (ESSCIRC2001), pp. 336-339, 2001.

Page 259: G_O'Brien PhD Dissertation

242

[12] J. Mizuno, K. Nottmeyer, Y. Kanai, O. Berberig, T. Kobayashi, and M. Esashi, "A Silicon Bulk Micromachined Crash Detection Sensor with Simultaneous Angular and Linear Sensitivity," presented at IEEE Transducers, pp. 1302-1305, 1999.

[13] L. J. Ristic, "Sensor Technology and Devices." Norwood, MA: Artech House Inc., 1994, pp. 402.

[14] M. Madou, "Fundamentals of Microfabrication," in CRC Press, vol. 1st Edition, 1997, pp. 464-465.

[15] P. L. Chen, R. S. Mueller, and A. P. Andrews, "Integrated Silicon Pi-FET Accelerometers with Proof Mass," Sensors and Actuators, vol. 5. no. 2, pp. 119-126, 1984.

[16] D. L. DeVoe and A. P. Pisano, "A Fully Surface Micromachined Piezoelectric Accelerometer," Solid State Sensors and Actuators, vol. 2, pp. 1205-1208, 1997.

[17] L. M. Roylance and J. B. Angell, "A Batch-Fabricated Silcon Accelerometer," IEEE Electron Devices, vol. ED-26, no. 12, pp. 1911-1917, 1979.

[18] W. Riethmuller, W. Benecke, U. Schnakneberg, and B. Wagner, "Development of Commercial CMOS Process-Based Technologies fro the Fabrication of Smart Accelerometers," presented at Solid State Sensors and Actuators, pp. 416-419, 1991.

[19] H. Seidel, U. Freitsch, R. Gottinger, J. Schalk, J. Walter, and K. Ambaum, "A Piezoresistive Silicon Accelerometer with Monolithically Integrated CMOS-Circuitry," Solid State Sensors and Actuators, vol. 1, pp. 597-600, 1995.

[20] H. Rockstad, T. W. Kenny, J. K. Reynolds, W. J. Kaiser, and T. B. Gabrielson, "A Miniature High Sensitivity Broad Band Accelerometer Based on Electron Tunneling Transducers," presented at IEEE Transducers, pp. 836-839, 1993.

[21] T. W. Kenny, W. J. Kaiser, H. K. Rockstad, J. K. Reynolds, J. A. Podosek, and E. C. Vote, "Wide Bandwidth Electromechanical Actuators for Tunneling Displacement Transducers," Journal of MicroElectromechanical Systems, vol. 3, pp. 97-104, 1994.

[22] J. Wang, B. McClelland, P. M. Zavracky, F. Hartley, and B. Dolgin, "Design, Fabrication and Measurement of a Tunneling Tip Accelerometer," presented at IEEE Solid State Sensors and Actuators Workshop, Hilton Head, pp. 68-71, 1996.

[23] J. Grade, A. Barzilai, J. K. Reynolds, C. H. Liu, A. Partridge, T. W. Kenny, T. R. VanZandt, L. M. Miller, and J. A. Podesek, "Progress in Tunnel Sensors," presented at Solid State Sensors and Actuators, Hilton Head, pp. 72-75, 1996.

Page 260: G_O'Brien PhD Dissertation

243

[24] P. R. Scheeper, J. K. Reynolds, and T. W. Kenny, "Development of a Modal Analysis Accelerometer Based on a Tunneling Displacement Transducer," presented at IEEE Transducers, pp. 867-870, 1997.

[25] C. Yeh and K. Najafi, "Micromachined Tunneling Accelerometer with a Low-Voltage CMOS Interface Circuit," presented at IEEE Transducers, pp. 1213-1216, 1997.

[26] A. M. Leung, J. Jones, E. Czyzewska, J. Chen, and B. Woods, "Micromachined Accelerometer Based on Convection Heat Transfer," presented at IEEE MEMS98, pp. 627-630, 1998.

[27] W. P. Mason, Piezoelectric Crystals and Their Applications to Ultrasonics. New York, NY: Van Nostrand, 1950.

[28] T. Ikeda, "Fundamentals of Piezoelectricity." New York, NY: Oxford Univeristy Press, 1990.

[29] G. T. A. Kovacs, "Micromachined Transducers Sourcebook." New York, NY: McGraw-Hill, 1998, pp. 216-217.

[30] W. G. Cady, Piezoelectricity, 2nd ed. New York, NY: McGraw-Hill, 1964.

[31] C. Ye, P. Baude, and D. L. Polla, "Critical Phenomena and Phase Transition in SOL-GEL Derived Ferroelectric PLZT Thin Films," presented at Proceedings of the 8th International Meeting on Ferroelectricity, pp. 347-352, 1993.

[32] P. Muralt, A. Kholkin, M. Kohli, T. Meader, K. G. Brooks, and R. Luthier, "Fabrication and Characterization of PZT Thin Films for Micromotors," presented at Seventh International Symposium on Integrated Ferroelectrics, pp. 213-220, 1995.

[33] D. F. Bahr, J. C. Merlino, P. Banerjee, C. M. Yip, and A. Bandyopadhyay, "Reliability and Properties of PZT Thin Films for MEMS Applications," Materials Research Society Symposium - Proceedings, vol. 546, pp. 153-158, 1999.

[34] C. F. Knowllenberg, T. D. Sands, A. S. Nikles, and R. M. White, "Issues in the Flexible Integration of Sputter-Deposited PZT Thin Films with Polysilicon and Ti/Pt Electrode Layers for use as Sensors and Actuators in Microelectromechanical Systems (MEMS)," presented at Materials Science of MEMS Devices Symposium, pp. 351-356, 2001.

[35] P. W. Bridgman, "The Effect of Homogenous Mechanical Stress on the Electrical Resistance of Materials," Phys. Rev., vol. 42, pp. 858-863, 1932.

[36] C. Herring, "Transport Properties of a Many Valley Semiconductor," J. Bell System Tech., vol. 34, pp. 237-290, 1955.

Page 261: G_O'Brien PhD Dissertation

244

[37] C. S. Smith, "Piezoresistance Effect in Germanium and Silicon," Phys. Rev., vol. 94, pp. 22-29, 1954.

[38] R. W. Keyes, "The Effects of Elastic Deformation on the Electrical Conductivity of Semiconductors," Solid State Phys., vol. 11, pp. 149-221, 1960.

[39] F. T. Geyling and J. J. Frost, "Semiconductor Strain Transducers," Bell Systems Tech., vol. 39, pp. 705-731, 1960.

[40] W. P. Mason and R. N. Thurston, "Use of Piezoresistive Materials in the Measurement and Displacement of Force and Torque," Phys. Rev., vol. 105, pp. 525-539, 1957.

[41] W. G. Pfann and R. N. Thurston, "Semiconducting Stress Trabsducers Utilizing the Transverse and Shear Piezoresistance Effects," Appl. Phys., vol. 32, pp. 2008-2019, 1961.

[42] O. N. Tufte, P. W. Chapman, and D. Long, "Silicon Diffused-element Piezoresistive Diaphragms," Appl. Phys., vol. 33, pp. 3322-3327, 1962.

[43] H. Sandmaier, K. Kuhl, and E. Obermeier, "A Silicon Based Micromechanical Accelerometer with Cross Acceleration Sensitivity Compensation," presented at IEEE Transducers, 399-402, 1987.

[44] O. N. Tufte and D. Long, "Recent Developments in Semiconductor Piezoresistive Devices," Solid State Electronics, vol. 6, pp. 323-338, 1963.

[45] V. A. Gridchin, V. M. Lubinsky, and M. P. Sarina, "Piezoresistive Properties of Polysilicon Films," Sensors and Actuators, vol. A49, pp. 67-72, 1995.

[46] D. W. Burns, "Micromechanics of Integrated Sensors and the Planar Processed Pressure Transducer." Madison: University of Wisconsin, PhD Thesis, 1988.

[47] S. K. Clark and K. D. Wise, "Pressure Sensitivity in Anisotropically Etched Thin-Diaphragm Pressure Sensors," IEEE Electron Devices, vol. ED-26, pp. 1887-1896, 1979.

[48] Motorola, Sensor Device Data/Handbook, 4th ed. Phoenix, AZ: Motorola Inc., 1998.

[49] G. Bitko, A. McNeil, and R. Frank, "Improving the MEMS Pressure Sensor," in Sensors Magazine, 2000, pp. 62-67.

[50] C. H. Liu, A. M. Barzilai, J. K. Reynolds, A. Partridge, T. W. Kenny, J. D. Grade, and H. K. Rockstad, "Characterization of a High Sensitivity Micromachined Tunneling Accelerometer," Journal of MicroElectromechanical Systems, vol. 7, pp. 235-244, 1998.

Page 262: G_O'Brien PhD Dissertation

245

[51] C. H. Liu, H. K. Rockstad, and T. W. Kenny, "Robust Controller Design via μ-Synthesis for High Performance Micromachined Tunneling Accelerometers," presented at American Control Conference, pp. 247-252, 1999.

[52] C. H. Liu and T. W. Kenny, "A High Precision Wide Bandwidth Micromachined Tunneling Accelerometer," Journal of MicroElectromechanical Systems, vol. 10, pp. 425-433, 2001.

[53] S. D. Senturia, "Microsystem Design." Norwell, MA: Kluwer Academic Publishers, 2000, pp. 529-530.

[54] R. Dao, "Thermal Accelerometers Frequency Compensation," vol. AN-00MX-003. North Andover, MA: MEMSIC Inc., 2002, pp. 1.

[55] S. M. Sze, "Semiconductor Sensors." New York, NY: John Wiley and Sons, 1994, pp. 191-193.

[56] L. K. Baxter, "Capacitive Sensors: Desings and Applications." Piscataway, NJ: IEEE Press, 1997, pp. 37-47.

[57] R. S. Cobbold, "Transducers for Biomedical Applications." New York, NY: John Wiley and Sons, 1974, pp. 23-36.

[58] G. T. A. Kovacs, "Micromachined Transducers Sourcebook." New York, NY: McGraw-Hill, 1998, pp. 219-221.

[59] F. R. Rudolf, "A Micromechanical Capacitive Accelerometer with a Two Point Inertial-mass Suspension," Sensors and Actuators, vol. 4, pp. 191-198, 1982.

[60] K. E. Petersen, A. Shartel, and N. F. Raley, "Micromechanical Accelerometer Integrated with MOS Detection Circuitry," IEEE Electron Devices, vol. ED-29, pp. 23-26, 1982.

[61] H. Seidel, "Capacitive Silicon Accelerometer with Highly Symmetric Design," Sensors and Actuators, vol. A21, pp. 312-315, 1990.

[62] W. C. Tang, C. T. Nguyen, M. W. Judy, and R. T. Howe, "Electrostatic Comb Drive of Lateral Polysilicon Resonators," Sensors and Actuators, vol. A21, pp. 328-331, 1990.

[63] A. Selvakumar and K. Najafi, "High Density Vertical Comb Array Microactuators Fabricated Using a Novel Bulk/Polysilicon Trench Refill Technology," presented at Solid State Sensors and Actuators, Hilton Head, pp. 138-141, 1994.

[64] G. J. O'Brien, D. J. Monk, and K. Najafi, "Angular Accelerometer with Dual Ancor Support," presented at Solid State Sensors and Actuators, Transducers03, pp. 1371-1374, 2003.

Page 263: G_O'Brien PhD Dissertation

246

[65] A. Lawrence, "Modern Inertial Technology Guidance and Control." New York, NY: Springer-Verlag, 1993, pp. 84-181.

[66] T. Kumagai, "Development of Optical Fiber Gyroscopes for Industrial Use," Hitiachi Cable Review, vol. 9, pp. 43-48, 1990.

[67] J. S. Burdess and T. Wren, "The Theory of a Piezoelectric gyroscope," IEEE Transactions on Aerospace and Electronic Systems, vol. AES-23, pp. 410-418, 1986.

[68] M. W. Putty and K. Najafi, "A Micromachined Vibrating Ring Gyroscope," presented at Solid State Sensors and Actuators, Hilton Head, pp. 213-217, 1994.

[69] A. Ayazi and K. Najafi, "Design and Fabrication of a High Performance Polysilicon Ring Gyroscope," presented at IEEE MEMS98, pp. 621-626, 1998.

[70] W. D. Gates, "Vibrating Angular Rate Sensor May Threaten the Gyroscope," Electronics, vol. 10, pp. 130-134, 1968.

[71] H. Sato, T. Fukada, F. Arai, and K. Itogawa, "Parallel Beam Gyroscope," presented at Sensors and Actuators, Transducers99, pp. 1586-1589, 1999.

[72] K. Maenaka and T. Shiozawa, "A Study of Silicon Angular Rate Sensors using Anisotropic Etching Technology," Sensors and Actuators A (Physical), vol. A43, pp. 72-77, 1994.

[73] P. Greiff, B. Boxenhorn, T. King, and L. Niles, "Silicon Monolithic Gyroscope," presented at Solid State Sensors and Actuators, Transducers91, pp. 966-968, 1991.

[74] S. Fujishima, T. Nakamura, and K. Fujimoto, "Piezoelectric Vibratory Gyroscope using Flexural Vibration of a Triangular Bar," presented at 45th Annual Symposium on Frequency Control, pp. 261-265, 1991.

[75] J. Bernstein, S. Cho, A. T. King, A. Kourepenis, P. Maciel, and W. Weinberg, "A Micromachined Comb-Drive Tuning Fork Rate Gyroscope," presented at IEEE MEMS93, pp. 143-148, 1993.

[76] W. A. Clark and R. T. Howe, "Surface Micromachined Z-axis Vibratory Rate Gyroscope," presented at Solid State Sensors and Actuators, Hilton Head, pp. 283-287, 1996.

[77] M. Lutz, W. Golderer, J. Gerstenmeir, J. Marek, B. Malhofer, and D. Shubert, "A Precision Yaw Rate Sensor in Silicon Micromachining," presented at Solid State Sensors and Actuators, Transducers97, pp. 847-850, 1997.

Page 264: G_O'Brien PhD Dissertation

247

[78] T. Juneau, A. Pisano, and J. H. Smith, "Dual Axis Operation of a Micromachined Rate Gyroscope," presented at Solid State Sensors and Actuators,Transducers97, pp. 883-886, 1997.

[79] W. Geiger, B. Folkmer, J. Merz, H. Sandmeir, and W. Lang, "A New Silicon Rate Gyroscope," presented at IEEE MEMS98, pp. 615-620, 1998.

[80] T. K. Tang, R. C. Guiterrez, J. Z. Wilcox, C. Stell, V. Vorperian, R. Calvet, W. J. Li, I. Charkaborty, R. Bartman, and W. J. Kaiser, "Silicon Bulk Micromachined Vibratory Gyroscope," Solid State Sensors and Actuators, Hilton Head, pp. 288-293, 1996.

[81] T. Brosnihan, J. Bustillo, and A. Pisano, "Embedded Interconnectand Electrical Isolation for High Aspect Ratio SOI Inertial Measurements," presented at Solid State Sensors and Actuators, Transducers97, pp. 637-640, 1997.

[82] G. J. O'Brien and D. J. Monk, "SOI Selective Electrical Isolation and Contact Method and Process," in US Patent, Pat. Pending, 2001.

[83] G. J. O'Brien, D. J. Monk, and K. Najafi, "Dual Anchor Angular Rate Sensor (Gyroscope)," presented at IEEE Solid State Sensors and Actuators, Hilton Head, pp. 285-288, 2002.

[84] L. Foucault, "Sur Une Nouvelle Demonstration Experimentalle Mouvement de la Terre Fondee sur la Fixete du Plan de Rotation," C. R. Acad. Sci, vol. 35, 1852.

[85] N. Yazdi, F. Ayazi, and K. Najafi, "Micromachined Inertial Sensors," Proceedings of the IEEE, vol. 86, no. 8, pp. 1640-1659, 1998.

[86] A. D. Aczel, "Pendulum: Leon Foucault and the Triumph of Science." New York, NY: Simon and Schuster, 2003, pp. 5-11.

[87] J. P. Hartog, Mechanics. New York City, NY: Dover Publications, 1948.

[88] J. C. Maxwell and J. Larmor, "Matter and Motion." Mineola, NY: Dover Inc., 1920 (reprint 1991), pp. 97-104.

[89] M. W. Putty, "A Micromachined Vibrating Ring Gyroscope," in Dept. of Electrical Engineering and Computer Science. Ann Arbor, MI: University of Michigan, 1995.

[90] G. S. Division, "WGS 84 EGM96 Earth Gravity Model," National Imagery and Mapping Agency, NASA/Goddard Space Flight Center 1997.

[91] F. W. Sears, M. W. Zemansky, and H. D. Young, "University Physics, 7th Ed.," Addison-Wesley, Reading, MA, 1987, pp. 276-277.

Page 265: G_O'Brien PhD Dissertation

248

[92] S. Timoshenko, D. H. Young, and W. Weaver, "Vibration Problems in Engineering." New York, NY: John Wiley and Sons, 1974, pp. 279-362.

[93] R. A. Becker, "Introduction to Theoretical Mechanics." New York, NY: McGraw-Hill, 1954, pp. 256-258.

[94] W. E. Newell, "Miniaturization of Tuning Forks," Science, vol. 161, pp. 1320-1326, 1968.

[95] G. T. A. Kovacs, "Micromachined Transducers Sourcebook." New York, NY: McGraw-Hill, 1998, pp. 311-312.

[96] E. J. Loper and D. D. Lynch, "Hemispherical Resonator Gyro: Status Report and Test Results," presented at National Techical Meeting of the Institute of Navigation, pp. 103-107, 1984.

[97] F. Rudolf, A. Jornod, and P. Bencze, "Silicon Microaccelerometer," presented at IEEE Solid State Sensors and Actuators, Transducers87, pp. 395-398, 1987.

[98] C. Shearwood, K. Y. Ho, and H. Q. Gong, "Testing of a Micro-Rotating Gyroscope," presented at IEEE Transducers99, pp. 984-987, 1999.

[99] K. Maenaka, T. Fujita, K. Y, and M. Maeda, "Analysis of a Highly Sensitive Silicon Gyroscope with Cantilever Beam as Vibrating Mass," Sensors and Actuators A (Physical), vol. 54, pp. 568-573, 1996.

[100] I. Pappas, T. Keller, and M. Popovic, "Experimental Evaluation of the Gyroscope Sensor Used in a New Gait Phase Detection System," presented at 4th Annual Conference of the International Functional Electrical Stimulation Society, IFESS99, pp. 96-101, 1999.

[101] G. C. Newton, "Theory and Practice in Vibratory Rate Gyroscopes," Control Engineering, pp. 95-99, 1963.

[102] S. D. Orlosky and H. D. Morris, "Quartz Rotation Rate Sensor," presented at Sensors Expo, Cleveland, OH, pp. 171-177, 1994.

[103] J. Soderkvist, "Design of a Solid State Gyroscopic Sensor Made of Quartz," Sensors and Actuators, vol. A21, pp. 293-296, 1990.

[104] A. Lawrence, "Modern Inertial Technology Navigation Guidance and Control, 2nd Edition." New York, NY: Springer-Verlag, 1998, pp. 153-155.

[105] R. Voss, K. Bauer, W. Ficker, T. Gleissner, W. Kupke, M. Rose, S. Sassen, J. Schalk, H. Seidel, and E. Stenzel, "Silicon Angular Rate Sensor for Automotive Applications with Piezoelectric Drive and Piezoresistive Read-Out," presented at Solid State Sensors and Actuators, Transducers97, pp. 879-882, 1997.

Page 266: G_O'Brien PhD Dissertation

249

[106] C. P. Fell, "Method For Matching Vibrating Frequencies on a Vibrating Mode Structure," in U.S. Patent Number 5,739,410: British Aerospace PLC, 1998.

[107] S. Bhave, J. I. Seeger, X. Jiang, B. E. Boser, R. T. Howe, and J. Yasaitis, "An Integrated, Vertical Drive, In-Plane-Sense Microgyroscope," presented at Solid State Sensors and Actuators, Transducers03, pp. 171-174, 2003.

[108] M. Weinberg, J. Bernstein, J. Borenstein, J. Campbell, J. Cousens, B. Cunningham, R. Fields, P. Greiff, B. Hugh, L. Niles, and J. Sohn, "Micromachining Intertial Instruments," Proceedings of the SPIE, vol. 2879, pp. 26-26, 1996.

[109] Y. Gianchandani and K. Najafi, "A Bulk Silicon Dissolved Wafer Process for Microelectromechanical Devices," Journal of MicroElectromechanical Systems, vol. 1, pp. 77-85, 1992.

[110] T. K. Tang, R. C. Gutierrez, J. Z. Wilcox, C. Stell, V. Vorporian, R. Calvet, W. J. Li, I. Charkaborty, R. Bartman, and W. J. Kaiser, "Silicon Bulk Micromachined Gyroscope," presented at Solid State Sensors and Actuators Workshop, Hilton Head96, pp. 288-293, 1996.

[111] T. K. Tang, R. C. Gutierrez, C. B. Stell, V. Vorporian, G. A. Arakaki, J. T. Rice, W. J. li, I. Chakraborty, K. Scheglov, J. Z. Wilcox, and W. J. Kaiser, "A Packaged Silicon MEMS Vibratory Gyroscope for Microspacecraft," presented at IEEE Microelectromechanical Workshop, MEMS97, pp. 500-505, 1997.

[112] G. I. Andersson, N. Hedenstierna, P. Svenson, and H. Pettersson, "A Novel Silicon Bulk Gyroscope," presented at Solid State Sensors and Actuators, Transducers99, pp. 902-905, 1999.

[113] C. H. Mastrangelo and W. C. Tang, "Semiconductor Sensors," S. M. Sze, Ed. New York, NY: John Wiley and Sons, Inc., 1994, pp. 38-42.

[114] M. Illing, "Micromachining Foundry Design Rules, Version 1.0," Bosch Mikroelektronik 1997.

[115] D. D. Lynch, "Hemispherical Resonator Gyro," IEEE Transactions on Aerospace and Electronics Systems, vol. AES-20, pp. 414-444, 1984.

[116] J. S. Burdess, "The Dynamics of a Thin Piezoelectric Cylinder Gyroscope," Institute of Mechanical Engineers, vol. 200, no. C4, pp. 271-280, 1986.

[117] G. H. Bryan, "On the Beats in the Vibrations of a Revolving Cylinder or Bell," Proc. Camb. Phil. Soc., vol. VII, no. 24, pp. 101-111, 1890.

[118] N. Maluf, "An Introduction to Microelectromechanical Systems Engineering." Norwood, MA: Artech-House, 2000, pp. 126-128.

Page 267: G_O'Brien PhD Dissertation

250

[119] A. Lawrence, "Modern Inertial Technology Navigation Guidance and Control, 2nd Edition." New York, NY: Springer-Verlag, 1998, pp. 31-32.

[120] A. Lawrence, "Modern Inertial Technology Navigation Guidance and Control, 2nd Ed.." New York, NY: Springer-Verlag, 1998, pp. 148-162.

[121] J. Geen and D. Krakauer, "New iMEMS Angular Rate Sensing Gyroscope," Analog Devices Inc., Analog Dialogue 37-03, 2003.

[122] W. C. Albert, "Vibrating Beam Accelerometer," IEEE Transactions on Aerospace and Electronics Systems, vol. AES-20, pp. 414-444, 1984.

[123] P. E. Allen and D. R. Holberg, "CMOS Analog Circuit Design." Orlando, FL: Harcourt Brace Jovanovich Inc., 1987, pp. 208-211.

[124] G. J. O'Brien, D. J. Monk, and L. Lin, "MEMS Cantilever Beam Electrostatic Pull-in Model," presented at SPIE MEMS, pp. 31-41, 2001.

[125] C. H. Mastrangelo and C. H. Hsu, "Mechanical Stability and Adhesion of Microstructures Under Capillary Forces -Part 1: Basic Theory," Journal of MicroElectromechanical Systems, vol. 2, pp. 121-129, 1993.

[126] R. J. Roark and W. C. Young, "Roark's Formulas for Stress and Strain, 6th Ed.," McGraw-Hill, 1989, pp. 345-349.

[127] Y. H. Cho, A. P. Pisano, and R. T. Howe, "Viscous Damping Model for Laterally Oscillating Microstructures," Journal of MicroElectromechanical Systems, vol. 3, pp. 81-86, 1994.

[128] W. Tang, C. T. Nguyen, and R. T. Howe, "Laterally Driven Polysilicon Resonant Microstructures," presented at IEEE Microelectromechanical Systems, pp. 53-59, 1989.

[129] D. J. Koch, J. H. Hammond, D. N. Koury, and J. F. Gorrell, "Method of Manufacturing a Sensor," in U. S. Patent 6,228,275, 2001.

[130] R. Gutteridge and L. J. Ristic, "Micromachined Capacitor Structure and Method for Making," in U. S. Patent 5,181,156, 1993.

[131] J. M. Noworolski and M. Judy, "VHARM: Sub-micrometer Electrostatic MEMS," presented at Solid State Sensors and Actuators, Transducers99, pp. 1482-1485, 1999.

[132] S. L. Miller, G. LaVigne, M. S. Rodgers, J. J. Sniegowski, J. P. Walters, and P. J. McWhorter, "Routes to Failure in Rotating MEMS Devices Experiencing Sliding Friction," presented at SPIE Micromachined Devices and Components, pp. 24-30, 1997.

Page 268: G_O'Brien PhD Dissertation

251

[133] G. T. A. Kovacs, "Micromachined Transducers Sourcebook." New York, NY, 1998, pp. 193-194.

[134] T. Yi and C. J. Kim, "Microscale Material Testing:Etchant Effect on the Tensile Strength," presented at Solid State Sensors and Actuators, Transducers99, pp. 518-521, 1999.

[135] J. A. Connally and S. B. Brown, "Slow Crack Growth in Single Crystal SiIicon," Science, vol. 256, no. 5063, pp. 1537-1539, 1992.

[136] J. A. Connally and S. B. Brown, "Micromechanical Fatigue Testing," presented at Solid State Sensors and Actuators, Transducers91, pp. 953-956, 1991.

[137] S. B. Brown, G. Povrik, and J. Connally, "Measurement of Slow Crack Growth in Silicon and Nickel Micromechanical Devices," presented at IEEE Micro Electro Mehanical Workshop, MEMS93, pp. 99-104, 1993.

[138] S. B. Brown, W. V. Arsdell, and L. Muhlstein, "Materials Reliabilty in MEMS Devices," presented at Solid State Sensors and Actuators, Transducers97, pp. 591-593, 1997.

[139] M. Offenberg, F. Larmer, B. Elsner, H. Munzel, and W. Riethmuller, "Novel Process for an Integrated Acelerometer," presented at Solid State Sensors and Actuators, Transducers95, pp. 24-29, 1995.

[140] T. W. Kim, B. Gogoi, K. G. Goldman, A. C. McNeil, N. J. Rivette, S. E. Garling, and D. J. Koch, "Substrate and Annealing Influence on the Residual Stress of Polysilicon," presented at Solid State Sensors and Actuators, Hilton Head, pp. 237-240, 1998.

[141] Y. H. Chen, T. D. Kudrle, and N. C. Tien, "Characteristics of 12micron Thick Polysilicon of an Optically Sensed Accelerometer," presented at ASME Microelectromechanical Systems, pp. 325-331, 1999.

[142] H. Funabashi, T. Tsuchiya, Y. Kageyama, and J. Sakata, "Fabrication Technology of Three Layer Polysilicon Microstructures without CMP for Gyroscope," presented at Solid State Sensors and Actuators, Transducers99, pp. 336-339, 1999.

[143] W. Tang, M. G. Lim, and R. T. Howe, "Electrostatic Comb Drive Levitation and Control Method," Journal of MicroElectromechanical Systems, vol. 1, No. 4, pp. 221-226, 1992.

[144] T. B. Gabrielson, "Mechanical Thermal Noise in Micro- machined Acoustic and Vibration Sensors," IEEE Transactions on Electron Devices, vol. 40, pp. 903-909, 1993.

Page 269: G_O'Brien PhD Dissertation

252

[145] F. W. Sears, M. W. Zemansky, and H. D. Young, University Physics, 7th Ed. Reading, MA: Addison-Wesley, 1987.

[146] G. T. Mulhern, D. S. Soane, and R. T. Howe, "Supercritical Carbon Dioxide Drying of Microstructures," presented at Sensors and Actuators, Transducers93, pp. 296-299, 1993.

[147] S. A. Campbell and H. J. Lewerenz, Semiconductor Micromachining, vol. 2. New York, NY: John Wiley & Sons, 1998.

[148] S. Wolf and R. N. Tauber, Silicon Processing for the VLSI Era, vol. 1, 2 ed. Sunset Beach, CA: Lattice Press, 2000.

[149] G. He and K. Najafi, "A Single-Crystal Silicon Vibrating Ring Gyroscope," presented at IEEE MEMS02, pp. 651-655, 2002.

[150] S. Wolf, Silicon Processing for the VLSI Era, The Submicron Mosfet, vol. 3. Sunset Beach, CA: Lattice Press, 1995.

[151] N. Maluf, An Introduction to Microelectromechanical Systems Engineering. Norwood, MA: Artech House, Inc., 2000.

[152] G. J. O'Brien, D. J. Monk, and L. Lin, "A Stiction Study via Capacitance-Voltage Plot Electrostatic Actuation/Latching," presented at ASME MEMS, pp.275-280, 1999.

[153] P. R. Gray and R. G. Meyer, "Analysis and Design of Analog Integrated Circuits," 3rd ed. New York, NY: J. Wiley and Sons, Inc., 1993, pp. 417-420.

[154] F. G. Stremler, Introduction to Communication Systems, 3rd ed. Reading, MA: Addison-Wesley, 1990.

[155] R. T. Howe and R. S. Mueller, "Integrated Resonant-Microbridge Vapor Sensor," IEEE Electron Devices, vol. 84CH2099-0, pp. 213-216, 1984.

[156] T. A. Lober and R. T. Howe, "Surface Micromachining for Electrostatic Microactuator Fabrication," presented at Solid State Sensors and Actuators Workshop, Hilton Head, pp. 59-62, 1988.

[157] M. W. Putty, S. Chang, R. T. Howe, A. L. Robinson, and K. D. Wise, "Process Integration for Active Polysilicon Resonant Structures," Sensors and Actuators, vol. 20, pp. 143-147, 1989.

[158] L. S. Fan and R. S. Mueller, "As Deposited Low Strain LPCVD Polysilicon," presented at Sensors and Actuators Workshop, Hilton Head, pp. 55-58, 1988.

Page 270: G_O'Brien PhD Dissertation

253

[159] H. Guckel, T. Randazzo, and D. W. Burns, "A Simple Technique for the Determination of Mechanical Strain in Thin Films With Applications to Polysilicon," J. of Applied Physics, vol. 57, pp. 1671-1675, 1985.

[160] K. Petersen, "Silicon as a Mechanical Material," Proceedings of the IEEE, vol. 70, pp. 420-457, 1982.

[161] J. W. Weigold, W. H. Juan, S. W. Pang, and J. T. Borenstein, "Characterization of Bending in Single Crystal Silicon Beams and Resonators," J. Vacuum Science Technology, vol. 17, pp. 1336-1340, 1999.

[162] J. W. Weigold, K. Najafi, and S. W. Pang, "Design and Fabrication of Submicrometer Single Crystal Accelerometer," Journal of MicroElectromechanical Systems, vol. 10, pp. 518-524, 2000.

[163] D. J. Monk, D. S. Soane, and R. T. Howe, "Hydrofluoric Acid Etching of Silicon Dioxide Sacrificial Layers. Part I. Experimental Observations," J. Electrochemical Society, vol. 141, pp. 264-269, 1994.

[164] D. J. Monk, D. S. Soane, and R. T. Howe, "Hydrofluoric Acid Etching of Silicon Dioxide Sacrificial Layers. Part II. Experimental Observations," J. Electrochemical Society, vol. 141, pp. 270-274, 1994.

[165] M. J. Madou, "Fubdamentals of Microfabricatrion," 2nd ed. New York, NY: CRC Press, 2001, pp. 18-19.

[166] L. J. Risic, "Sensor Technology and Devices." Norwood, MA: Artech House, Inc., 1994, pp. 208-215.

[167] R. S. Muller and T. I. Kamins, in Device Electronics for Integrated Circuits. New York, NY: J. Wiley and Sons, 1986, pp. 31.

[168] H. C. Nathanson, W. E. Newell, R. A. Wickstrom, and J. R. Davis, "The Resonant Gate Transistor," IEEE Electron Devices, vol. ED-14, no. 3, pp. 117-133, 1967.

[169] K. E. Petersen, "Dynamic Micromechanics on Silicon: Techniques and Devices," IEEE Transactions on Electron Devices, vol. ED-25, pp. 1241-1250, 1978.

[170] C. H. Mastrangelo and R. S. Muller, "Fabrication and Performance of a Fully Integrated μ-Pirani Pressure Gauge with Digital Readout," presented at IEEE Transducers91, pp. 245-248, 1991.

[171] R. K. Gupta and S. Senturia, "Pull-In Dynamics as a Measure of Absolute Pressure," presented at IEEE MEMS97, pp. 290-294, 1997.

[172] K. Wang and C. T. Nguyen, "High Order Micromechanical Filters," presented at IEEE MEMS97, pp. 25-30, 1997.

Page 271: G_O'Brien PhD Dissertation

254

[173] C. T. Nguyen, "High-Q Micromechanical Oscillators and Filters for Communications," presented at IEEE International Symposium on Circuits and Systems, pp. 2825-2828, 1997.

[174] K. E. Petersen, "Micromechanical Membrane Switches on Silicon," IBM Journal of Research and Development, vol. 23, no. 4, pp. 376-385, 1978.

[175] P. M. Zavracky, S. Majumder, and N. E. McGruer, "Micromechanical Switches Fabricated Using Nickel Surface Micromachining," Journal of MicroElectromechanical Systems, vol. 6, pp. 3-9, 1997.

[176] M. A. Gretillat, Y. J. Yang, E. S. Hung, V. Rabinovich, G. K. Ananthasuresh, and S. Senturia, "Nonlinear Electromechanical Behavior of an Electrostatic Microrelay," presented at IEEE MEMS97, pp. 1141-1144, 1997.

[177] E. P. Popov, Mechanics of Materials. Englewood Cliffs, NJ: Prentice-Hall, 1976.

[178] G. J. O'Brien, D. J. Monk, and L. Lin, "Electrostatic Latch and Release; a Theoretical and Empirical Study," presented at ASME MEMS, pp. 275-280, 2000.

[179] ANSYS, "Silicon Beam Suspended Above a Grounded Gate," in Coupled Field Analysis Guide, version 5.6, Example 2.11.1, vol. 5.6. Cannonsburg, PA, 2001.

[180] F. Laermer and A. Schlip, "Method of Anisotropically Etching Silicon," in U. S. Patent Nos. 4,855,017 and 4,784,720: R. Bosch GMBH, 1991.

[181] J. W. Weigold, "Dry Etching of High Aspect Ratio Si Microstructures in High Density Plasma for use in MEMS." Ann Arbor, MI: PhD Thesis, University of Michigan, 2000.

[182] A. A. Ayon, R. Braff, C. C. Lin, H.H.Sawin, and M. A. Schmidt, "Characterization of a Time Multiplexed Inductively Coupled Plasma Etcher," J. Electrochemical Society, vol. 146, pp. 339-349, 1999.

[183] F. Laermer, A. Schlip, K. Funk, and M. Offenberg, "Bosch Deep Silicon Etching: Improving Uniformity and Etch Rate for Advanced MEMS Applications," presented at IEEE MEMS99, pp. 211-216, 1999.

[184] W. C. Tian, J. W. Weigold, and S. W. Pang, "Comparison of Cl2 and F-based Dry Etching for High Aspect Ratio Si Microstructures Etched with an Inductively Coupled Plasma," J. Vacuum Science Technology, vol. B18, pp. 1890-1896, 2000.

[185] K. T. Sung and S. W. Pang, "Etching of Si with Cl2 Using an Electron Cyclotron Resonance Source," J. Vacuum Science Technology, vol. A11, 1993.

[186] H. Jansen, M. d. Boer, and M. Elwenspoek, "The Black Silicon Method," Journal of MicroElectromechanical Systems, vol. 5, pp. 115-120, 1995.

Page 272: G_O'Brien PhD Dissertation

255

[187] C. P. D'Emic, K. K. Chan, and J. Blum, "Deep Trench Plasma Etching of Single Crystal Silicon using SF6/O2 Gas Mixtures," J. Vacuum Science Technology, vol. B10, pp. 1105-1109, 1992.

[188] J. Bhardwaj, H. Ashraf, and A. McQuarrie, "Dry Silicon Etching for MEMS," presented at Symposium on Microstructures and Microfabricated Systems, Electrochemical Society, pp. 126-131, 1997.

[189] D. C. Montgomery, Design and Analysis of Experiments. New York, NY: J. Wiley and Sons, 1991.

[190] A. A. Ayon, S. Nagle, L. Frechette, A. Epstein, and M. A. Schmidt, "Tailoring Etch Directionality in a Deep Reactive Ion Etching Tool," J. Vacuum Science Technology, vol. B18, pp. 1412-1416, 2000.

[191] S. Y. Chou, P. R. Krauss, W. Zhang, L. J. Guo, and L. Zhuang, "Nanoscale Silicon Field Effect Transistors Fabricated using Imprint Lithography," J. Vacuum Science Technology, vol. B15, pp. 1881-1883, 1997.

[192] W. H. Juan and S. W. Pang, "Batch-Micromachined, High Aspect Ratio Si Mirror Arrays for Optical Switching Applications," presented at ", International Conference on Solid-State Sensors and Actuators, pp. 93-97, 1997.

[193] G. J. O'Brien, D. J. Monk, and K. Najafi, "Deep Reactive Ion Etched Submicron Beam/Trench Characterization," presented at ASME MEMS, pp. 586-591, 2001.

[194] R. A. Gottscho, C. W. Jurgenson, and D. J. Kitkavage, "Microscopic Uniformity in Plasma Etching," J. Vacuum Science Technology, vol. B10, pp. 2133-2138, 1992.

[195] K. A. Shaw, Z. L. Zhang, and N. C. MacDonald, "SCREAM: A Single Mask, Single Crystal Silicon Process for MEMS Structures," presented at IEEE MEMS93, pp. 155-160, 1993.