icp test report certification packet - littelfuse/media/files/... · nov^ test report no....

96
1 ICP Test Report Certification Packet Company name : Littelfuse, Inc. Product Series: 3AB Axial Leads Product #: 325xxxP Series Issue Date: February 28, 2013 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC, 2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components. Issued by: <Global EHS Engineer> (1) Parts, sub-materials and unit parts This document covers the 3AB Axial Leads RoHS-Compliant series products manufactured by Littelfuse, Inc. Raw Materials Used Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1 RemarksForm 585-047 Rev. A 2/21/06

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Page 1: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

1

ICP Test Report Certification Packet

Company name : Littelfuse, Inc. Product Series: 3AB Axial Leads Product #: 325xxxP Series Issue Date: February 28, 2013 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC, 2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components.

Issued by:

<Global EHS Engineer>

(1) Parts, sub-materials and unit parts

This document covers the 3AB Axial Leads RoHS-Compliant series products manufactured by Littelfuse, Inc. < Raw Materials Used

Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1

Remarks:

Form 585-047 Rev. A 2/21/06

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2

Table 1: List of Raw Materials covered by this report

Total Parts Raw Material Part Number Raw Material Description Page(s) 1 910-005 Cap 3-6

2 C610

(909-532, 909-162, 909-165) Ceramic Body 7-35 3 11-0595 (082xxx-001) Element- CU99.9MSn 36-39 4 917-44xxxx Element - Cu(CA102) Cu110 Strip 40-43 5 RD series (899-401X-1) Resistor - RoHS 44-49 6 899-401X-1 Resistor - Halogens 50-53 7 912-228 Spring – Copper Berrylium rod 54-57 8 (YTW108) 692535-003 Solder 58-62 9 YTW102 (648102) Yarn 63-70 10 090187 Filler 71-77 11 090184 Filler 78-85 12 (3M 3779-PG) 087244 HMA - RoHS 86-89 13 (3M 3779-PG) 087244 HMA - RoHS 90-92 14 934-055 Overcap – Cap Base & Plating 93-96

Page 3: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

nov^TEST REPORT

NO. 4002R12050740-1R02 Daie: May. 09, 2012

T€stino method:

I\l1QL

IEC 62321:2008, seclion I tcP-oEs 2mg/kg

cadmium (Cd) IEC 62321:2008, seclion 9 rcP-oEs 2 mg/kg

Mercury (Hs) IEC 62321 2008, s€ction 7 tcP-oEs 2 mSeS

chrcmium (Cr VI) IEC 62321i200E Ann€x B 0.02mg/kg'

Ieq

Cu8tomer: Suzhou FuHong Electrcnic IndustrialCo., Ltd.

AddT€€3: NO,69\ryEIDU ROAD, WANGTING TO\M{, XIANGCHENG OISTRICI SUZHOU. CHINA

R€pot on the submitt€d sample sald to b€

Sample nah€: Copp€r sh€ll

Supplier: /

Sample rocolv€d date: lvlay. 07, 2012

T6tf ng pedod: Frcm luay.07,29l2toMay.A9,2012

T€€tino R€ou€6tod

As specified by clienl, lo delermine the Lead, Cadmium, l\,telcury & Hexavalent Chrcmium mntent in the submitled sample in

.ccodance wilh Dircctive 200295/EC (RoHS).

r 0.02 mgl(g efers to the MQLofsampb enraction tiquid.

Concll|3ion:-When lested as specified lhe submitled sampl€ €omplied with the requircments of commission Decision of 18 Aug 2005

amending Direcnve 2002r95/Ec notified underdocument 2005/61E/Ec.

*'*FOR FURTHER DETAILS. PLEASE REFERTOTHE FOLLOWING PAGE{S).*'"

Sigmd ior and on behalfof

Shenzhen AOV Tesling Technology Co., Lld, Kunshan Branch

,.r.ou.o.,, /uI?'Li nngtng, lMaggie

Ch€mical Test Di€ctor

oro.'n,44.

S}I€I\IZIIEN AOV TESTING TECHNOLOGY CO.,ITD.(UI{SHAN ERANCH ol:9Jllis,.*""

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nov'NO. A002R12050740-1R02

Cooling, filter;washed and fjll€d

lo lhe mark with Dl water.

-------------l --________' r€st€d by

l__rl nupo,r IInstumenl | | |

Add lhe digeslion €olution; lhe

vessel is heal€d unlil the sample

TEST REPORT

T6st€d by tCP-OEs

f*--* -j.-

d, C4lmium and Mercury Conbnt (Plating)

f*;;1.,-

Chromium Content (boiting- warer- ext€crion)r {Mstat subsrrare)

SHENZHEI\I AOV T€STII{O TECHI{OLOGY CO.,!TO.XUNSTIA BNA CH

Cooling lhe vessel, fiteri washed and

filled to the man( with dislilled water

Th8sample is digesred in the

micrcwave ov€n iollowing a specific

decomposition program

Test lhe sample solution and lhe 0.02

mg/kg standard solution by W-VIS.

Hotllne

Coolinglhe vessol, filtsr; wasi€d and

filled lo lhe markwilh distilled water.

Remove tne sample, snd cool

lhe beaker to rcom temp€€turc,

and do the color r€action

Heal 50 mL ofDlwalerin the

beaker to boiling for 'l 0 min

To Dsbmine

Page 5: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

nov'To Detemine H€xavalent Ch.omium

",ffii'Q*a*

NO

5.

TEST REPORTDats: iray 09,2012

Contenl in colorless and colored chromate

Page3ot4

coaling on metals: (Plaling)

lf lh€ tast r€sult is positive,

lhe sample ls considered lo

hav€ hexavalenl chromium

and lhe 0.0? mg/kg

Boiling- waler- enraclion

proc€dure shall be used tolfthe l€st tesull

lfthe|e is interierence oritis hard lodecidewhether

the sample have lhe ho(avalent chromium

5.2 Boiling- waleF exlraclion

Take the (5015) cm'z

SHENZHEN AOV TISTII{G IECHNOfOGY CO.,!TO.XUNSIIAT INA CH Hotline36.512-55100000

Remov€ lhe sample, and cool

the b€akor lo room tsmp€ralute,

and do the color reaction

Heat s0 mlof orwaler in lhebeaker !o boiling for 10 min

Tesl the samplesolution and the 0.02

mg/kg slandarit solution by UV-VIS.

Pl€ring

Unil RoHS Limil

Lead (Pb) mg/xg 1000 N.D. N.D.cadmium (cd) mg/Kg 100 N.D. N.D.

Mercury (Hg) mg/xg 1000 N.D. N.D.

chromium (Cr\,I) mg/xg 1000 Negalive Negalive

Page 6: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

nov-NO.: 4002R12050740-1R02

TEST REPORT

Photograph of Sample

-Tne n€w RoHS di€ctive 201 1/65/EU, on Jul. 21 , 201 1 com€ inlo iorce, on Jan 03, 201 3 the fomat imptemenlaton, Dircctrve2002/95/EC sh.ll be rcp€aled simultaneousty.

-Specimens, which requesred to detemine Lead, Cadmium and MercuryConrent, have boen dissotved compt€r€ty.

-N.D.=not detecGd(<rUaL)

]\,lQL=lvlethod Quantilation Limit-Negative=Absene or cr (VI):'Positive=Presence of Cr (VI)l

Uncedain= can nol v€dfy whether the sample hav€ Hexavalent Chromium by spot-test.(The lerled sample should be tunher veified by boiting,wal€r+xtraclion method if lhe spot test resutt is uncedain ol

single layer and each pa( is unifom The test resultsThe tesl is based on the followi.g assumplion: The sampte ptaring is a

maybe cannot srand ior lh€ physicalttuth ofsampte ptating.

SHINZIIENAOVTESIINGTFCHNOLOGYCO.,LTO-KUNSHA BRAI{CH

Ollo.tll.?,.""""

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Signature plidForQueslionPlease Qltwith SGSwww.tw.sal-om

rtlt[tll][]|lt

Test Report No.: CE/20't3l/13191 Dale 2013101121 Page: 1 of 29

CERAMTEC GMBHGESCHAFTSBEREICH IJULTIFUNKTIONSKEMMIK,LUITPOLDSTRABE'I5. 91207 LAUF

The following sample(s) was/werc submitted and identified by/on behatf of the client as:

Sample DesoriptionStyle/ltem No.Sample Receiving DateTesting Period

CERAMICc6102013t1tl42013t1tl4 10 2013tO1n1

Test Re3ult(s)

Conclusion

: Please lefer to next page(s).

: Based on the pedomed test6 on 6ubmitted 6amples, the test results of Cadmium, Lead,I\rercury, Hexavalent Chromium Cr(Vl), PBBS and PBDES comply with tho limits as set byRoHS Dircctive 201'1/65/EU Annex ll; recasting 2002/95/EC.

Efnrd fr. aod

Chqdcd frbot bry-Trlgd

tHl5";vtr^:,)n*$i"d h8 T.u:lM

I d!'€'' ledn'"Jg onr oi.-i"oiji.--," **o o n"c.ru rcele o1r{ o'd.r'"€.o*or

f';;il*-fl9#'i"15;; d;hd,"...bndd;cmsns. E-i '.r ' i ' 'r s.rd bndid roE. .1Yand{o1ouon! (

; -to;;'; ;;:' de. rdd a- i {d d s'***d $;i-.h'';l:*l;-*.":*:;;*|'!6;, .,1;TtydT PJ.;1ii:;;T*.iiift i;;5#;i"'":1'"p,;ilbe tme or E fleiEdm onry ad s

t";!i;y1;;*"*#:;;lim:r"r"*li:;.::ir*"'r;fff";ffij'i"""ffi'13il*:#ift'r-"-".ff'""1;",1#,;1""H{i;:i""'ri"rl,1;ii , : : : n r . l l i r i l l i

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Test Report No. : CE/2013/13191 DaIe :2013101121 Page: 2ol 29

CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNfiIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF

l[]t tt][ttttlt

Test Result(s)

PART I{AME No.1 : CREAM CERAirlC

Test ltem(s) Unit Method MDLReault

LimitNo.t

Cadmium (Cd) mg/Kg with reference to lEc 62321: 2008 andperformed by ICP-AES.

2 n.d. '100

Lead (Pb) mdkg With reference to IEC 62321: 2008 andperformed by lCPiEs.

2 204 1000

Mercury (Hg) mg/Kg With reference to IEC 6232 1 : 2008 andperformed by ICP-AES.

2 n.d. 1000

Hexavalent Chromium cr(Vl) msyKg With reference to IEC 62321: 2008 andperfonned by UV-VIS.

2 n.d. 1000

BBP (Benzyl butyl phthalate) (CASNo. : 85-68-7)

With reference to EN 14372. Analysis,ras performed by GC/MS.

0.003 n.d.

DEHP (Di- (2-ethylhexyl)phthalate) (CAS No.: 117-81-7)

o/. With reference to EN 14372. Analysiswas perfomed by GC/MS.

0.003 n.d.

DIDP (Di-i6odecyl phthalate) (CASNo. : 26761 -4O0)

% With reference to EN 14372. Analysis,,,€s p€rformed by GC/|\4S.

0.01 n.d.

DINP (Di-isononyl phthalate) (CASNo.:28553-12-0)

o/o With reference to EN 14372. AnalysiswEs perfomed by GC/MS.

0.01 n.d.

DNOP (Di-n-octyl phthalate) (CASNo.: 117-84-0)

o/o With reference to EN 14372. Analysisw€s perfomed by Gc/Ms.

0.003 n.d.

DBP (Dibutyl phthalate) (CAS No.u-7+2\

% With feference to EN 14372. Analysiswas performed by GC/MS.

0.003 n.o.

Perf luotooctane sulf onates(PFOS-Acid, Metal Salt, Amide)

mg/kg With reference to US EPA 3550C;2007. Analysis was performed byLC/MS.

1 0 n_o.

PFOA (CAS No.; 33S7-1) mg/Kg With reference to Us EPA 355ocl2007. Analysi6 was pedomed byLC/MS.

1 0 n.d,

Polychlorinated Biphenyls (PCBS)(CAS No.r '133,S36-3)

mg/kg with referenc€ to us EPA 3540cmethod. Analysis was perfomed byGC/MS.

0.5 n.d.

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Test Report No. I CE/2013/13191Oate | 2013101121Page :3o f29

CERAI,ITEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERA[/|IK,LUITPOLDSTMBE 15. 9'1207 LAUF

tl|||tt lttlul

Test ltem(s) Unit Method MDLR€6ult

LimitNo.'l

Polychlorinat€d Terphenyls(PCTs)

mS/kg With reference to US EPA 3540Cmethod. Analysis\ ras perfomed byGC/MS.

0.5 n . d .

Polychlorinat€d Naphthalene(PCNs)

mgKg Wth reference to US EPA 3540Cmethod. Analysis\ ras performed byGC/MS.

5 n.d.

Alkanes, C10-13, chloro (ShortChain Chlorinated Paraffins) (CASNo. : 85535-84-8)

mg/Kg With reference to US EPA 3540Cmethod. Analysis was performed byGC/l\rs.

'100 n.d.

PVC Analysis was performed by FTIR andFLAME Te6t.

Negative

Formaldehyde (CAS No.: 50{0-0) mg/Kg With reference to ISO 17226-1(2008).Analysis was performed by HPLC/DAD.

3 n.d.

Monomethyl dibromodiphenylmethane (DBBT)

mg/Kg With reference to uS EPA 8270Dmethod. Analysis was performed byGC/MS.

0.5 n.d.

Monomethyl dichlorodiphenylmethane (Ugilec121)

mg/Kg With refefence to US EPA 8270Dmethod. Analysis was performed byGC/MS.

0.5 n.d.

[4onomethyl tetrachlorodiphenylmethane (Ugilec141)

mg/kg With reference to US EPA 8270Dmethod. Analysis was performed byGC/rlts.

0.5 n.d.

HalogenHalogen-Fluodne (F) (CAs No.:14762444\

mg/Kg

Wilh €fe.ence to BS EN USA2:20O7.Analysis was p€rfomed by lC.

50 n.d.

Halogen-Chlorine (Cl) (CAS No.:22537-15-1)

mg/Kg 50 n . d .

Halogen-Bromine (Br) (CAS No.:1OO97-32-2)

mg/Kg 50 n.d.

Halogenlodine (l) (CAS No.:1436244-8)

mg/Kg 50 n.d.

Oryanic.tin compoundaTdbuvl Tin (TBT) mg/Kg With reference to DIN 38407-13.

Analysis was pertormed bY GC/FPD.0.03 n .d .

rriphenylTin (TphT) me/Kg 0.03 n.d.

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TestReport No.:CE/201:r/13191 Date:2013t01t21 pase:4of2s

CERAI,TEC GI,BH |I]|||tt][tt rlGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF

Test ltem(s) Unit method MDLResult

LimitNo.l

AabestosActinolite (CAS No.: 77536-66-4)

Wilh reference to EPA 600/R-93'/1 I 6method. Analysis was performed byStereo l\Iicroscope (SM), DispersionStaining Polarized Light Microscope(DS-PLlr) and X-ray DiffractionSpectrometef (XFID).

NegativeAmosite (CAS No.: 12172-73-5) o/o NegativeAnthophyllite (CAS No.: 77536-67-5)

% Negative

Chrysotjle (CAS No.: 12001-29-5) NegativeCrocidolite (CAS No.: 12OU-2a4\ ok NegaliveTremolile (CAS No.: 7753e68$) % Negative,zo1): 4-AMINODIPHENYL (CAS No.:92-67-1)

mg/Kg With reference to LFGB 82.02-2.Analysis uras performed by cC/lVS.

3 n.d,

BENZIDINE (CAS No.: 92-87- mg/Kg With feference to LFGB 82.02-2.Analysis was performed by GC/IVIS.

3 n.d.

3): 4.cHLORO-O-TOLUIDINE(CAS No.: 9569-2)

mg/Kg With reference to LFGB 82.02-2.Analysis u/as performed by GC/MS.

3 n.d.

4)r 2-NAPHTHYLAMINE (cASNo.r91-59-8)

mg/Kg With reference to LFGB 82.02-2.Analysis w€s performed by GC/MS.

3 n.d.

5): O-AMINOAZOTOLUENE (CASNo.:97-56-3)

mg/kg With reference to LFGB 82.02-2.Analysis was performed by GC/tu|S.

3 n .d .

6): 2-AMlNO.4-NITROTOLUENE(CAS No.: 99-55-8)

mgikg With reference to LFGB 82.02-2.Analysis was performed by GC/MS.

n.o.

7): P-CHLOROANILINE (CAS No.:10647-8)

mg/Kg With referenc€ to LFGB 82.02-2.Analysis wEs performed by GC/MS.

n.d.

8): 2,4-DIAMINOANISOLE (CASNo.:6'15-05-4)

m9Kg With reference to LFGB 82.02-2.Analysis was performed by GC/[,!S.

3 n.d.

9'):4,4-DIAMINODIPHENYLI\4ETHANE(CAS No.: 101-77-9)

mg/Kg With reference to LFGB 82.02-2.Analysis was performed by Gc/Ms.

3 n.d.

10): 3,3'-DICHLOROBENZIDINE(CAS No.: 91-9+1)

mg/Kg with reference to LFGB 82.02-2.Analysis was performed by GC/MS.

3 n.d.

1 1)r 3,3'-DIMETHOXYBENzIDINE(cAS No.r 11$9&)

mgftg With roference to LFGB 82.02-2.Analysis w€s perfomed by GC/MS.

3 n.o,

'1 2): 3,3'-DII,iIETHYLBENZIDINE(CAS No.: 119-93-7)

m9Kg With reference to LFGB 82.02-2.Analy6is was performed by GC/lltS.

3 n.d.

fi ' ' !,"l;*'"*.;*.-".:;". ' ' ' ,.""""...].,";..":"'.s"*"...*"-':.."'"."."-, i l ; , .n i ' jn . i , .n t tomaroi - . "* . -d€o6|er ,ardcotro|3|oLeiii, iil.-niiniiv-iiiiiinnn-in,ii^?,aitd;*uBdlin6dthe;;^i i i i i i i"i,i ir,i*o' -ry-"*ri tr. -'borc ctihqrudm' Ir'l -tcomdars ea s!oo!oi,.i"*.i- m * os no a i r.' q*

" o o'qa'o* -0.'- nino;r'doe-44 n s do' -d -moin. ?erc!L("d P e0

li;fiii rii;" r;;a; tao: b's;t "abi"r.d*

oJ rhe @;;;;;i;;;;;i $ n@*i' "

*h*tu sa otundds mai be prcsdcd b '

, " , . , , , . : i l i i ; i l . r , qno*' t r"aFt i r i . l i . { rrr * f : rr}L s d ..::i-:-1' 9P !.ll!!.r.1

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Test Report No. : CE/2013/13191 Dale:2013101121 Paqe | 5 of 29

CERAI\4TEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERA[IIK,LUITPOLDSTMBE 15, 91207 LAUF

Il]mttfittltl

Test ltem(s) Unit lrethod MDLR€ult

LimitNo.l

1 3): 3,3!DIMETFIYL-4,4-DIAIJINODIPHENYLMETHANE(CAS No.: 838-88-0)

mg/Kg With reference to LFGB 82.m-2.Analysis was performed by GC/lrS.

3 n.ct.

14)r P-CRESIDINE (2-IUETHOXY-s-METHYLANILINE) (CAS No. I120-71-8)

msasWith reference to LFGB 82.02-2.Analysis was performed by GC/MS.

3 n.d.

'1 5): 4,4.-METI-IYLENE-BIS- (2-CHLOROANILINE) (CAS No.:101-144)

m!/(g With reference to LFGB 82.02-2.Analysis was performed by GC/MS_

3 n.d.

16): 4,4'-OXYDIANILINE (CASNo.r 101-80-4)

mg/Kg With reference to LFGB 82.02-2.Analysjs wEs p€rfomed by GC/MS-

3 n.d.

17): 4,4'-THIODIANILINE (CASNo.: 139€5-1)

mg/Kg With reference to LFGB 82.02-2.Analysis w€s perfomed by GC/MS.

3 n.d.

1E): O-TOLUIDINE (CAS No : 95-s34)

mg/Kg With reference to LFGB 82.02-2.Analysis was performed by GC/MS.

3 n.d.

'1 9): 2,4-TOLUYLENEDIAMINE(CAS No.: 95-80-7)

mg/Kg With reference to LFGB 82.02-2.Analysis wa6 performed by GC/MS.

3 n . d .

20): 2,4,5-TRIMETHYLANILINE(CAS No.: 137-17-7)

mdkg With reference to LFGB 82.02-2.Analysis\ ras performed by co/l\rs.

3 n.d.

21): O-ANISIDINE (CAS No.:90-04-0)

mg/Kg With reference to LFGB 82.02-2.Analysis was performed by GC/MS.

3 n.d.

22): P-AMINOAZOBENZENE(CAS No.r 6M9-3)

mg/Kg With reference to LFGB 82.02-2.Analysis was perfomed by GC/MS.

3 n.d.

23): 2,4-XYLIDINE (CAS No.r95-68-1)

mg/kg With reference to LFGB 82.02-2.Analysis was performed by GC/IVS.

3 n.d.

24): 2,6-XYLIDINE (CAS No.: 87-62-7)

mg/Kg With reference to LFGB 82.02-2.Analysis was performed by GC/MS.

3 n.d.

CFC's (Chlorofl uorocarbons)Group IChlorofluorocabon-1 1 (CAS No.l75€9-4)

mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

n .d .

Chlorof luorocarbon-1 2 (CAS No. :75-714]

mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

n-d.

;ii; i;i;;; ; ,!,.i .d '; ri. c.-,;;' ',ti; b iL; &ne'ar condi om d;; ;;;;i i;; d;-tu:^a 3uh;ed b rem! ano co.o @ns h' rrqd. b;{.I d{w.{s.o- e.i ; ; d ; l a ' ' h " i j . ' i - * ' ; . d i $a fnn ' 3 . "dddh .F 'ha rme or i! 'meilerton onrv and -; ; ; ; - ; ; h : ; . ; n . d J , ' i . i ' . c ' o i d 0 a f ; i " ' d f u r 1 a " .

Nev tdiFi .ir r.iws / I -: .'. qi i ni {li3rrL

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Test Report No. : CE/2013/13191 Date: 2013t01t21 Paoe : 6of 29

CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTMBE 15. 91207 LAUF

rlfll tlt! ttt]l

lest ltem(s) Unit Me{hod MDL R€6ultLimitNo.1

Chlorof luorocarbon-1 13 (CAS No.:76-13-1)

mg/Kg With reference to US EPA 502 1method. Analysis was performed byGC/t S.

1 n.d.

Chlorcfluorocarbon-1 14 (CAS No.l7efi-2)

mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

1 n.o.

Chlorotluorocarbon-l 15 (CAS No.:76-15-3)

msasWith reference to US EPA 5021method. Analysis was performed byGC/MS,

1 n . d .

Group lllChlorof luoroca6on-1 3 (CAS No.:75-72-9)

mg/kg With reference to US EPA 502 1method. Analysis wEs perfomed byGC/MS.

1 n.d-

Chlorof luoroca6on-'1 1 1 (CAS No.:354-56-3)

mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

1 n.d-

Chlorofluoroc€rbon-'112 (CAS No.:76-12-O)

mlyKg With reference to US EPA 5021method. Analysis was performed byGC/MS.

'I n . d .

Chlorof luorocarbon-2l 1 (CAS No.:422-78-8)

mgikg With reference to US EPA 5021method. Analysis was pertormed byGC/MS.

'I n.d.

Chlorof luorocarbon-21 2 (CAS No. :3182-%-1)

mg/Kg With refefence to US EPA 5021method. Analysis wEs performed byGC/MS.

1 n.d.

Chlorof luoocarbon-21 3 (CAS No.:2354{6-5)

mg/kg With reference to US EPA 5021method- Analysis was performed byGC/[rS.

1 n.d.

Chlorof luoroca6on-214 (CAS No.:29255-31-0)

mgKg With reference to US EPA 5021method. Analysis was performed byGC/MS.

n.d.

Chlorof luorocarbon-215 (CAS No.:425943-2)

mgi Kg With reference to US EPA 5021method. Analysis w€s performed byGC/MS.

n .d .

. ! . .;

"'.i;-.. ; *d b' h6 cmou

,no b' e€dM c romar dnoments rd pd 6 hr3 and cot ions b' Lrecl;;;;tmh ;A;ii-6; md :.$-r,sr3ne . reo rE 'n r . ne f l ono -vdFowt i n ' h . 'mbo rca -s iF taon< 3 l ponqb f t v ' r o c iP "d t r sdo* *o , j " t ' o . i * - " " 0 a i r

" mo l imdmb- i 5doo - t ' a t b pno ' l de roo t l a o . i c

( omod i Mv r s ! o zao arasrca o's.ry o' r;sfr-ton ol I e d+n d

.-""'.,ii::lliiillr: r l Y"!:1t]:rt"pjrtrg:.11':11j'-

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Test Report No.: CE/201313191 DaIe 2013101121 Paoe 7 of 29

CERAMTEC GMBHGESCHAFTSBEREICH MULIIFUNKTIONSKERA[TIK,LUITPOLDSTMBE 15, 91207 LAUF

r[|||tt]llttI|

Test ltem(e) unit Method I'DLResult

LimitNo.l

Chlorof luoroc€6on-216 (CAS No.l661-97-2)

mg/Kg With reference to US EPA 5021method. Analysis was perfomed byGC/tUS.

1 n.d.

Chlorof luoroca6on-217 (CAS No.:422-E&6)

mg/kg With referenc€ to US EPA 5021method. Analysis was performed byGC/t S.

1 n.d.

HCFCa(Hydrochlorofl uorocalbons)HCFC-21 (CAS No.: 75434) mg/Kg With reference to US EPA 5021

method. Analy6is was performed byGC/MS.

I n.o,

HCFC-22 (CAS No.: 75-45$) mg/Kg Wilh reference to US EPA 502'1method. Analysis was pertormed byGC/MS.

'I n.d.

HCFC-31 (CAS No.: 593-70-4) mg/Kg With reference to US EPA 5021method. Analysis u/as performed byGC/MS.

'I n.d.

HCFC-121 (CAS No.: 354-14-3) mg/Kg With refefence to US EPA 5021method. Analysis was performed byGC/MS.

'I n.d.

HCFC-122 (CAS No.: 354-21-2) m!/Kg With reference to uS EPA 5021method. Analysi6 was pedormed byGC/MS.

1 n.d.

HCFC-123 {CAS No.: 306-83-2) mg/Kg With refere.ce to US EPA 502 1method. Analysis was performed byGC/rVlS.

1 n.d.

HCFC-124 (CAS No.: 2837-89-0) mg/Kg With reference to US EPA 5021method. Analysis rvas performed byGC/tVS.

n.d.

HCFC-13'1 (CAS No.r 359-28.4) mg/Kg With reference to US EPA 5021method. Analysis was pedormed byGC/tVS.

n.d.

HCFC-132b (CAS No.: 1649-08-7)mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

n.d.

-nn.'"iJ'""r

" **o

"iuie coma;";b,*

"iGa*eft codod'"s"1eor'sode' .s5i-ier-'-,nd rtro 5b

i J6 i i " oJ . i t i j a ' . i ' . n " , ' " ' , qa i 6 re - , ddod id ' b 'F3ad i , { do ' *La€ - . d t ?n &

rhermed b deiudio onl! d{sh F. aborc ens'n{rdo'' ' l;;;;" b; ;;-ii!i;,;. ilis i; ;'q;,r"";, iir" r*a;m;ry ay lmdb';d *sdon. ro@ery o, disddoi dr he 6n,ent o

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Test Report No.: CE/2013/13191 Date:2013101121 Page: 8 of 29

CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF

rll |ltt][ttllll

Test liem(s) Unit Method MDLResult

LimitNo.'l

HCFC-133a (CAS No.: 75-88-7) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/t S.

n.cl.

HCFCI4lb (CAS No.: 1717-00€) mgKg With reference to US EPA 5021method. Anaiysis was performed byGC/MS.

I n.d.

HCFC-142b (CAS No.: 75-68-3) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

1 n-d.

HCFC-221 (CAS No.: 422-264) mg/kg With reference to US EPA 502 1method. Analysis was performed byGC/l\rs.

1 n.d.

HCFC-222 (CAS No.r 422-49-1) mg/Kg With reference to US EPA 5021melhod. Analysis was performed byGC/MS.

1 n.d-

HCFC-223 (cAs No.: 422-526) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

'I n.d.

HCFC-224 (CAS No.: 422-54-8) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

1 n.d.

HCFC-22sca (CAS No.: 422-56-0) mg/Kg With reference to US EPA 502'lmethod. Analysis u/as performed byGC/MS.

1 n.d.

HCFC-22scb (CAS No.i 507-55-1) mg/Kg With reference to US EPA 5021method. Analysis was perfomed byGC/MS.

n.d.

HCFC-226 (CAS No.: 431-87-8) mg/Kg With reference to US EPA 502'1method. Analysis wes performed byGC/MS.

n.d.

HCFC-231 (CAS No.r 421-94-3) m9Kg With reference to tJS EPA 502'1method. Analysis was Performed bYGC/[iS.

't n.d.

HCFC-232 (CAS No.: 460-89-9) mg/Kg With reference to US EPA 502 1method. Analysis was Performed bYGC/MS.

1 n.d.

ow. m h's 3s B@. FF ul b ne 3

.;;.";;-", is ,rd b, h c-ps y sD.eq,o 6 Gr6rcdoj:i.,.*,pffii;F"1;f;*&,;:,#"r,,!;ri:\t,itr,:xi{.y;%1"iffT"1_i;j ?;:jli:i:",Sblecl lo rems and @ndhons ftr.,m. o. ar .* dstrnra,o, nd.inedd 'nu*"- "t:lll.lj;;1.;:t*"*;,f;:::*i;;fjl,,". if;ti* ilf,;'"-;le:'i:";i;; -?":ig:";',?lli0,:"ii

* * " " "a - , * ' - " - , - . J i i - a ; l ,mom.EF .do - -a ' 6 fdc r e . , & y l 1 a n 1 o n z e d " s d d , . - ' # i ; ; ; ; : ; ; i ; ; * : l i " ^ r ' r o b r o - d i b ' r e * d b r r l l e ' " ' { r o L h e b n

r\eift peicivft rs/:r";iii i ) i il i i 4firb

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Test Report No- : CE/201313191 Date:2013101121 Paoe i gof 29

CERAMTEC GMBHGESCHAFTSBEREICH

rllllllat][ ttltMULTIFUNKTIONSKERAMIK,LUITPOLDSTRAEE 15. 91207 LAUF

Te6t ltem(a) Unit method MDL Re€ultLimit

No.1HCFC-233 (CAS No.: 7125-84-0) mg/Kg With reference to US EPA 5021

method. Analysis wa6 performed byGC/MS.

'I n.d.

HCFC-234 (CAS No.: 425-94-5) mg/Kg With reference to US EPA 5021method. Analysis was perlormed byGC/MS.

1 n.d.

HCFC-235 (CAS No.: 450-92-4) rnglkg With reference to US EPA 5021method. Analysis wEs perfomed byGC/MS.

1 n . d .

HCFC-241 (CAS No.: 666-27-3) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

1 n . d .

HCFC-242 (CAS No.r 46063-9) mgag With reference to US EPA 5021method. Analysi6 was performed byGC/MS.

1 n .d .

HCFC-243 (CAS No.: 460$9-5) mgKg With reference to US EPA 502 1melhod. Analysis was perfomed byGC/MS.

1 n.d-

HCFC-244 mg/Kg With reference to US EPA 5021method. Analysis w€s performed byGC/MS.

1 n .d .

HCFC-251 (CAS No.: 421-41-0) mg/Kg With reference to US EPA 502 1method. Analysis was pertormed byGC/MS.

1 n.d.

HCFC-252 {CAS No.: 819-00-1) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

'I n.d.

HCFC-253 (CAS No.: 460-35-5) mdkg With reference to US EPA 5021method. Analysis was performed byGC/MS.

n.d.

HCFC-261 (CAS No.: 420-97-3) mg/Kg With reference to US EPA 5021method. Analysis w€s perfomed byGC/MS.

n.d.

HCFC-262 (CAS No.: 421-m-03) mdkg With reference to IJS EPA 5021method. Analysis was performed byGC/MS.

n.d.

I i B . I I l !anv5ub ] . db tGE la | cond lonso ' sed@prn iedowdca i ' ava iab |eon r€

qedb ams sr co-o m\!o' ehdd rinsdidon 'sEs ddd rhere n 6y io &r of b s eumd ; adv 3ad Lh be company s {indino! ar

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Test Report No. : CE/201313191 Dale 2013t01t21 paoe | 10 of 29

CERAIVTEC G[/lBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15. 91207 LAUF

rtrr lrt][ttt||l

Tegt ltem(s) unit Method MDL ResultLimitNo.1

HCFC-271 (CAS No.r 430-55-7) mg/Kg With reference to US EPA 5021method. Analysis was perfomed byGC/MS.

1 n .d .

HalonsHalon-1211 (CAS No.: 353-59-3) mg/Kg With reference to US EPA 5021

method. Analysis wEs performed byGC/MS.

1 n.d.Halon-1301 (CAS No.: 75-63-8) mg/Kg 1 n.d.Halon-2402 (CAS No.: 124-73-2) mg/Kg 1 n.d.CHCs (Chlorinate hydrocarbon)1, 1, 1,2-Tetrachloroelhane (CASNo.:630-206)

mg/Kg With reference to US EPA 5021melhod. Analysi6 w€s performed byGC/MS.

1 n.d.

'1 , 1 ,'1 -Trichloroethane (CAS No. :71-55€)

mdkg With reference to US EPA 5021method. Analysis w€s performed byGC/MS.

1 n . d .

'1, 1,2,2-Tetrachloroethane (CASNo.:79-34-5)

mgKg With reference to US EPA 5021method. Analysis wa6 perforned byGC/MS.

1 n . d .

1,1,2-Trichloroethane (CAS No.:79-00-s)

mg/Kg With reference to US EPA 5021method. Analysis $/as performed byGC/t\rs.

I n.d.

1,1-Dichloroethane (CAS No.: 7$34-3)

mgKg With reference to US EPA 5021method. Analysis was performed byGC/MS,

,| n .d .

't ,1-Dichloroethene (CAS No.: 75-354)

mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

1 n.d.

1,1-Dichloropropene (CAS No.:5695&6)

mg/Kg With reference to US EPA 5021method- Analysis was performed byGC/tVS.

n.d.

1,2,3-Tichloropropane (CAS No.:96-184)

mdks With reference to US EPA 5021method. Analysis was pedormed byGC/tVlS.

n.d.

'1,2-Dichloroethane (CAS No.:107-06-2)

mgftg With reference to US EPA 5021method. Analysis was performed byGC/l\,!S.

n.d.

LN4r : i F (V r r iw in rn 1 . 1 ' n i l r i i f r : t { J

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Test Report No. : CE/201 3/1 3 1 91 Dale : 2013t01t21 page : .l .1 of 29

CERAMTEC GMBHGESCTIAFTSBEREICH MULTIFUNKTIONSKERAI\4IK,LUITPOLDSTMBE .l 5, 91 207 LAUF

lfl tl|[ tllttl

Test lt€m(s) Unit Method i,DLRegult

LimitNo.l

1,2-Dichloroprcpane (CAS No.:78-87-5)

mg/kg With reference to US EPA 5021method. Analysis wEs perfomed byGC/MS.

1 n.d.

'l,}Dichloropropane (CAS No. :142-2&9)-

mg/Kg With referenc€ to US EPA 5021method. Analysis was performed byGC/MS.

1 n.o.

z,2-Dichloropropane (CAS No.:53+20-7',)

mg/Kg with reference to us EPA 5021method. Analysis wa6 performed byGC/MS.

I n.d.

Carbon tetrachloride (CAS No.i56-23-5)

mgikg Wath reference to US EPA 5021method. Analysis was pertormed byGC/MS.

1 n . d .

Chloroethane (CAS No.: 7$00-3) mg/Kg With reference to US EPA 502 1method. Analysis was porformed byGC/MS.

1 n.d.

Chlorofom {CAS No.: 67-66-3) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/[rS.

1 n.o.

Chloromethane (CAS No.: 74-87-3)

mg/Kg With reference to US EPA 5021method. Analysis wEs performed byGC/MS.

1 n.d.

cis-1,2-Dichloroethene (CAS No.:15G59-2)

mdkg With reference to uS EPA 5021method. Analysis\ ras pertormed byGC/MS.

1 n . d .

ci6-l,3-Dichloropropene (CAS No.l10061-01-5)

mg/Kg with reference to us EPA 502 1method. Analysis was performed byGC/MS,

1 n.d.

Hexachlorobutadiene (CAS No.i8768-3)

mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

'I n-d.

Methylene Chloride (CAS No.: 75-09-2)

mg/kg With referenc€ to US EPA 5021method. Analysis was performed byGC/MS.

n.d.

Tetrachloroethene (CAS No.: 127-184)

mgI(g With reference to uS EPA 5021method. Analysis was performed byGC/MS,

n.d.

s r lEk t repo ld - r t bs ' s

i ;T f t :k" ' ' ' , . " " " "* - , " . " . " " . " - ; - . " ' " " ' " : . . i " , ' i ' . "s . . *p**"" . i .a 'a-uu"" ' l .osdo!esbA-"e!o 'o 'i * i i " i

" an ' i n t ma r ; i e r c i . r i d . db -em, ' bco r ' . " r ' ' edonLOo@f t1Rd"ms { ' , o -

a1 eas , dco ,d tuo s r8Tseooai ; ; ; ; j b ; i i ; # ; i i " ; ; i ; ; . i " " " ; . ^ d ' * h . * , e ' ' d o . t r | ' 0 r ' a ' ' a d . gh " | - . d k FE ; \ ed on odv and w ,h i d he im so c rems nsMros ' L r v i b i s r r . l a d lF tum"d6;;;(-;;;;;;-;;;;6;i;;oi:a ;; ;;J;, . ;. :ie r,..obidd-.-d -n, oo@r1 d "o 0- re o! @o "oo;#ffi;:p;;;;,-,i;;;:d i;i,;: i;a;t ;iai,n-i;";i h" -"bd

"; r . : r i r ! r ' i ' i t - l r .

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Test Report No.:CE/2013/13191 Dale 201310121 Paoe:12 ot 29

CERAMTEC GMBHGESCI-I,AFTSBEREICH

tl| |l lrtl]lIVULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF

T€6r ltem(s) Unii method MDLResult

LimitNo.1

trans-1,2-Dichloroethene (CASNo. : 1 56-60-5)

mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

'I n.d.

trans-1,3-Dichloropropene (CASNo.: 10061-02€)

mg/Kg With reference to US EPA 502'method. Analysis was performed byGC/MS.

1 n.d.

Trichloroethylene (CAS No.: 7$.01€)

mg/Kg With refefence to US EPA 5021method. Analysis was performed byGC/US.

'I n.o,

Sum of PBBS mg/Kg

With reference to lEc 62321: 2008 andoertormed bv GC/I\IS.

n.d. 1000lMonobromobiphenyl mg,iKg 5 n.d.Dibromobiphenyl mdkg 5 n .d .Tribromobiphenyl mg/kg 5 n.d.Tetrabromobiphenyl mg/Kg n.o,Pentabromobiphenyl mg/Kg n.d.Hexabromobiphenyl mg/Kg 5 n.d.

Heptabromobiphenyl mgKg 5 n .d .Octabromobiphenyl mg/kg 5 n.d.Nonabomobiphenyl mg/Kg n.d.Decabromobiphenyl mg/Kg 5 n . d .

Sum of PBOE5 mg/Kg n.d. 1000Monobromodiphenyl ether mg/Kg 5 n.d.

Dibromodiphenyl ether mgikg 5 n.d.

Tribromodiphenyl ether mg/Kg 5 n.d.Tetrabromodiphenyl ether mg/Kg 5 n.d.

Pentabromodiphenyl ether mg/Kg 5 n.d.

Hexabromodiphenyl ether mg/kg 5 n.d.

Heptabromodiphenyl ether mg/Kg 5 n.d.

Octabromodiphenyl ether mgKg 5 n.d.

Nonabromodiphenyl ether mg/Kg 5 n.o.

oecabromodiphenyl ether mg/Kg 5 n.d.

i . , ; j i t r : l e t . r \ i

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Test Report No. I CE/2013/13191Dale | 2013101121Page : 13 ot 29

CERAMTEC GMBHGESCI-I,AFTSBEREICH iNULTIFUNKTIONSKERAMIK,LUITPOLDSTMBE 15, 9.1207 LAUF

lm[llt rt]I

Not. :'1. mg/kg = ppm | 0.1wt% = loooppm2. n.d. = Not Detecled3. MDL = Method Detection Limit4. "-"= Not Regulated5. - = Qualitative analysis (No Unit)6. N€gative = Undet€ctable / Positive = DetectableT Testing range of asbestos qualitative analysis is from less than 0.1% to 1OO%. The judgment crjterion: asbestos fibers

being found is shown as "Positive'; asbeslos fibers not being found is shown as,'Negative..

PFOS Refe.ence Intormetion : POPS - (EU) 757m10Outlawing PFOS as substances or preparations in concentrations above O.OOl% (lOppm), in s€mi-finished products ofarticle6 or parts at a level above 0.1%(1000ppm), in textiles or other coated materials above 1pg/m,.

3liffJ*:"iT,:'?jil\"ri+iTi:?i,iii)i:;::ii:?i"T::i:rl'!{i'iili:r!':ti,li;'rflf'l"1-'e@rcd@d eed rtur Mhdrp

ii":l"H*;:;rls,:iixs'.9"r;i"'t*;:ffagfi"u;::"^'J:rffis#j:r,x*ir5'Lri!tr:"i3;xlf;,i:;-x'#;%1:"#il";: rd,rll,l'Ti"'4ri,:"-..r-o'in|;n,*..neo,-d .<-'.*"a,doids";, ti;o; tr: dMm{ F;dre 'edsI e (omLnr\ihdin$''iiiiilni.l *'r"i'*ro" on" a"o *ti".m rns or ce.' +.*"i ';q Fe.d",p".v"d"."po"'blv ' 'o r! LrPl' . t r ' ood ̂ " diliil;a; i."- d*o.ri+e

"e;fi;;l!;;;'.;-*o;;&;1.;i;;: 6;s;t ;iaianai,* .r h. -dei, (

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Test Report No.:CEl2013l13191 DaIe:2013101121 Page: 14 of 29

CERA['TEC GI,lBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK.LUITPOLDSTRABE'15, 9'1207 LAUF

1 ) These samples were dissolved toblly by pretonditioning method according to belolt/ flow chart.( Cf' te€t method excluded )

Name of the person who made measurement Climbgleat YangName of the person in charge of measurement: Troy Chang

2)3)

SamDle Mderial DioestionAcid

S'teel, copper, aluminum, solder Aqua reqia, HNOr, HCl, HE HzO:

Glass HNOy'HF

Gold, platinum, palladium, ce€mic Aqua regia

Silver HN03

Plastic H,SO., H,O,, HNO3, HCI

Others Added appropriate reagent to totaldiOe6tion

Note- : (1) For non{netallic material, add alkaline digestion reagent and heat to 90'95f(2) For metallic material, add pure water and heat to bdling.

r ! { e * h p e . 4 f t t $ / i i : l i i i r d r i r : l i i 4 3 \ 1

Cutting / Preparation

Sample Measurement

Add appropriate amountof digestion reagent

Acid dige6tion by suitable aciddeoended on different samolematedal (as below table)

Microv/ave digestion withHN03/HCI/HF

Heat to appropriatetemperatuae to erdr€ct

1) Alkal iFusion2) HClto dissolve

Add d iphenyltarbazidefor color development

measute the absotbanceat 540 nm by UV-VIS

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Test Report No. ICE/2013i/13191Dele :2013101121Page : 15 of 29

CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK.LUITPOLDSTMBE 1 5. 91 207 LAUF

]tI|tt][tttutl

PFOA/PFOS analytical flow chart of Ultrasonic extraction (LC/MS) procedure

r Name of the person who made me€surement: Roman WongI Name ofthe person in chaqe of measurement Troy Chang

ffi um*m,1*ffit*'r,*ffi*#iHl*gl+rsirti*ffikNdrripd.tvlriw:i/li: ' n ] ': Iiriti33li

r+elo2)r4rD ||e6Orlr??1 ?1

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Test Report No. : CE2013l'13'191 Date 201?,10121 Paoe: 16of 29

CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK.LUITPOLDSTRABE 15, 91207 LAUF

lm[tr|| ||tt]t

Data

PCTS analytical flow chert

t Name ofthe petson who made measurement Barry T6engr Name ofthe per6on in charge of measurement: Troy Chang

. i r i { r i c f n r \ i

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Test Report No. : CE/2013/13191 Dale : 2013101121 Page : 17 of 29

CEMMTEC GMBHGESCFI,AFTSBEREICH MULTIFUNKTIONSKERA[/lIK,LUITPOLDSTMBE 1 5, 91 207 LAUF

ll] ttJflllafll

PBB/PBDE analytical FLOW CHART

I Name ofthe person who made measurement Roman Wongr Name of the person in charge of measurement Troy Chang

First testing process -----'

Optional screen proce6s ....

Confirmation procegs -.>

[J-"'d;---l--------r-------[s-"-lrj--jr"t""t.-tl-T-

Screen analysis

Sample e)draction/Soxhlet method

Concentrate./DiluteExtEcted solution

Filter

Analysis by GC/lvlS

lssue Report

" " " " " " ' f " " " " " "

a;; . : : ' ' . <we p" 'ed owtd ars dbir oll, :T i ;e1d; : - . ;F ; l ;u . ; " ;o€ ; '6hr 'mdcordb4u i ;n rc : .oo . - . ' l dMa ' jdq |

" ' , , . . - ' * * . . " ' , , " , , " ;r i , i j t i i o is ; ; l *m, - rv - " - ' . ,n " . ,uo |cs '+n ' .d ;n i; a ; i i i i ' . i # a j g . * , g , ' r - ' g t : T o o ] g ! j l o B J n d e l ' 9 ? n % d f ' @ o - 4 k T i 3 d o (

u ' { i;:;; ;;;;r;;: : 'oeft | s 5d|" oo'arc"a -dib'

l i i i ,: r !l I {lii:rri

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Test Report No. : CE/2013/13191 Dale:20131O1n1Page : 18 of 29

CERAI,TTEC GI,/lBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15. 91207 LAUF

PCBe analytical flow chart

r Name ofthe person who made measurement Bafiy Tsengr Nameoftheperson incharge of measurcment: Troy Chang

Data

lll |ltt][ttlllt

M ti rhlsresr €Don rerer ont ro be tpdorMtbpembsondrE

rhsiftinmr'a €sid b! lh€ cmoanv eubEci ro 'ls Gne'arcndiions orseruie or ed o6'ldat a$ abeonie ms .M,@iditons lrhand ror € adrof, c romd dntum.nb e 6 e d 6 re' ms and C.d ton s lo' Ered msad.Cond( ons/rerm* Dotuft

d u'is. dion isues derned bere i tuv s Ihe companvs nnd'nqs ari heheo ib i n l e iwn1ono i vandw id i n l he ] im$o l c i e i 1sns1 rc i ons f ; nyTheco Inpas$ |e Iespon3b |ftnsdon rrom err"vnq ri h., adFioftJml' hEoodm"lrConprnJ diy iaLtdzeo arleu on

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Test Report No. : CE/2013i13191Dale:2013101121Page : 19 of 29

CERAMTEC GMBHGESCHAFTSBEREICH [/|ULTIFUNKTIONSKERAMIK,LUITPOLDSTMBE 1 5, 91 207 LAUF

Chlorinated Paraffins analytical flow chart

r Name oflhe person who made measurement: Bary Tsengr Nam€ of the person in charge of measuremenl Troy Chang

Data

tl][ || t|:ll]I

a m o € ' : e e e d I i ' 6 r ? o o ' € o' , t . - I . t i ,

i i i i i . i . * . " * . * o " o e c o . o a ; ' ' o d b ' i c s t . | L d d ' o ' ' d . o l , o ' 3 e e * o A d e 3 s 9 J - l;; ;i; ;.;;; ;;;' ;r;. ;;;B &;ed b rems rm cdiGmb 0 Eranrcn( ooom.{ . ar "B {- "o_ .innn;iiri,h ,omnta;.; d :1d'do sr! d,,rd h.r,he ru or r 'n,ei!en, on oi v dnd dbinher+aorcrcn \'ran01"; ; ; ; ; ; ; ; ' ; " ^ n ; ; i ; ; i o i " * o o t a " . ' ' c . * . u " ' * . ' o , ' o o J m ' 6 i I o o J - e { o ' '( dmoa., hr ,rd bo zen ,n4no'

N€r tdFi.[r ri iwri / i i-: ' !: ]. ' i : . r {iLli! l i

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Test Report No. : CE/2013/13191D?[e:2013101121Page:20 ol 29

CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAIV]IK,LUITPOLDSTMBE 1 5. 91 207 LAUF

Analysis flow cha.t for determination of Asbe6tos

I Name ofthe person who made measuremenl: Victor KaoI Name of the person in charge of measurementt Wendy Wei

( Reie.ence method: EPA 600/R-93/l 16l

Sampling

Contai ning AsbestovPositive Not conhining Asbesto6/ N€gative

!]l[ttt ltt]l

" i t , 1rh6 do.irm.m E Lsusd s rha com"nd b . l . {on . r .mar o@merb . . ' iF - d re- 'dndco ld ro 's ro Fsa vdm(odor - " -3€Dor_ena

ndemnrca( on and 'LlNd d6 6su6rheriftdl6 d.iwi{on otrlv a qsi r;nrTh?com0anyssercspoi5br'ry'' 'o Lsc'en and'hsdocum.ndt r sdo hma . G ro a r i t e nConpaiy ay unauhdzad a lsrdion

k { 4 r t P ( r y r . e d / i . l : i . i 1 1 i t * j : t j r

Continue when probl€rnsarc encournefed withDS-PLM and/or for quality assurance pufposes

Asbestos identifc€lion by dispetsion stainingpola zed light micrcscope (DS-PLM)

Asbe€tos idenlifcation by X-faydiff raclion speclrometer (XRD)

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Test Report No. : CEl2013i/13191 Date : 2013101121 Paae : 21 of 29

CERAI,iITEC GMBHGESCHAFTSBEREICH

!

I

Analytical flow chan of Organic-Tin content

Name ofthe person who made measurement: Ginny ChenName ofthe person in charge of measuremenl Troy Chang

It] tttI[ltr tMULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF

ui4s dheNs sbcd hs e$ 6 s,o!.n ,n h'' '6d rcpoi erer o'u.bri€ 3aT?fFr,!".i:i .iii:iif...;r':pd

**d b

"K1 i l ; "1 . , . " ; , , " . * . *# ; " , " . * ' " " ; ' * , . J , * * . '9 {ep ' ' coo ' " l "a ] ' .€ ,bPo1 'a;;.rii;etu .-d oie.- ',oFc6 krsmd hthE,o L] . i i i ' i " ' i n * l "nd6mnid lo ,a t '1 r$oo '9ae ' *nare6 ' : , i , i i "nnn.s i io ; { ' , i .Nsddd'r. t-n:

"i s l;* m. -rv,

" w

3'Ji;::i:,m^'tf:3.'illli'i*:?fJliP','€*":ii#l;iik"," '""doneid-" *vbfi;;;;ih;i6.1eiii"brih" ""

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Test Report No.:CE201?'13191 Date:2013101121 Page: 22 of 29

CEMMTEC GIVBHGESCHAFTSBEREICH

rtl ltrt ttlllllMULTIFUNKTIONSKERAI/|IK,LUITPOLDSTRABE 15, 91207 LAUF

PCNS analytical flow chart

r Name ofthe person who made measurement: BarryTsengI Name of the person in charge of measurement; Troy Chang

Data

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Test Report No.: CE/201313191 DaIe 2013101121 Paqe: 23 of 29

CERAMTEC GMBHGESCHAFTSBEREICH IVULTIFUNKTIONSKERAMIK.LUITPOLDSTMBE 15. 91207 LAUF

tn[lnl|l l|l]t]

Analytical flow chad of phthalate content

I Name of the person who made measufementr Roman Wongr Name of the pe6on in charge of measurement: Troy Chang

Data

' ' r i n l ! r i r r f t i3 r l ' i

Concentrate./Dilute Extracted solution

An€lysis was perfomed by GC/MS

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Test Report No. : CE/2013/13191 Dale : 2013101121

CERAMTEC GMBHGESCIIAFTSBEREICH

Page:24 ol 29

91207 LAUFll| |l!] |lttl

I,IULTIFUNKTIONSKERAMIK,LUITPOLDSTMBE 1 5,

I

I

Formaldehyde analytical flow chart

Name of the pe6on who made measurement: Scott KuN€me of the person in charge of measurement: Troy Chang

I Test Method : US EPA 83154 ' ISO 17226-1 ]

Dala

Derived by DNPH ConcentrateJDilute Extractedsolution

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Test Report No. :CE/2013 /13191Dale'.2013101121Page : 25 of 29

Analyais flow chart for determination of PVC In material

CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAI,!IK.LUITPOLDSTMBE 1 5. 9'1 207 LAUF

||]tIltt][t [Il

I

I

Name ofthe person who made measurement: Ginny ChenName of the person in charge of measurement: Troy Chang

Sample analyzed by FTIR

Check wave-number of c-cl bonding

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Test Report No. CE2013,/13191 Dale:2O1AO1121 Page : 26 of 29

CERAMTEC GMBHGESCHAFTSBEREICH

|ln[ t][tll]rMULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF

II

DBBT analytical flow chart

Name ofthe pe6on who made me€surement Roman WongName ofthe person in charge of measurement: Troy Chang

Dala

. i : r , i l r 1 i l i t - l j

Sample pretreatmenvseparation

Sample extraction by 6oxhlet method

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Test Report No.:CEl2013/13191Dale: 2o13lo1nl Page 27 ot 29

CERAI.TTEC GI,/IBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAI/|IK,LUITPOLDSTRABE'1 5, 9'1 207 LAUF

Analytical flow chart of halogen content'1) Name of the oerson vt/t|o made measurement: Rita Chen2) Name of the person in charge of measurement: Troy Chang

||l ||tt]tI|tttll

9fj] iH*"", ';:* ' ' ,*.- '"], ' ' , ;;"...""*.l"i"".-".n.*,." ' '-"*"'.n-.*'."1' ; ; t i ; d f u .bmddmmmE' *oFdhh rsmdcodbn 'b ; ; i . nn . cDo6m{ | J# { , od 'ri,:"luri6'in

'rn,r Ardbs; ;jlnri'n dhatu-.in in i

" l " d* . " - , , " * i ' r . . , so - t "n .c i " . , ; ' ; ' : ;a ; . ; ; ; ' - ; - "F*br ' rv rb c* r id ' '<dc ' -c

r i in i i , " j r . * lo i rua i r " monoodm. . ' i ' doo .ne1rcomoanv try unau,tu'z& abad.,-q.ry * I'kh*- drb-tu;it;iFt€ne or th sdturud smawtu

i. ., + i _ri;\l

lFli33!1

Sample pretreatment / separation

Wdghting and putting sample in cell

Oxygen Bomb Cornbustion / Absorption

Dilution to fixed volume

Analysis was performed by lC

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Test Report No. : CE/20'13/13191Dai'e : 2O13101n1 Page : 28 of 29

CERAMTEC GMBHGESCHAFTSBEREICH l/TULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 1 5, 91207 LAUF

Analytical flow chart ofvolatile organic compounds (VOCS)

I Name ofthe oe6on who made measurement : Chun WuI Name of the person in charge of measurernent : Shinjyh Chen

(Reference method : US EPA 5021)

lfl||tt][ttl||ll

Sample pretreatment

Take sample and put it intoheadspace glassware.

Analy6is was per{ormed by GCYlrs

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Test Report No. : CE2013/13191D e: 2013101121Page : 29 of 29

cERAlilTEC GIVBHGESCHAFTSBEREICH MULTIFUNKTIONSKERA[/|IK,LUITPOLDSTRABE 15, 91207 LAUF

'The tested sample/ part is ma*ed by an arrow if ifs shown on lhe photo.'

'* End of Repod "

ll]t ttflll0llll

kNewr i t s i . i vL {$ i , : - : ' . ! r , d r i i i l i l f n r \ i

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Test Report Number: SHAH00361401

Authorized by: For intertek testing services Ltd., Shanghai

Jacob Lin General Manager

Page 1 Of 4 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

Applicant: LITTELFUSE,INC. Date: JAN 16, 2013 800 E. NORTHWEST HWY Attn: A.DIVIETRO/D.UNTIEDT

Sample Description: One (1) submitted sample said to be Grey Wire. Item Name : Wire Tin Plated Cu. Part No. : Element.

************************************************************************************************************************************************************ Tests Conducted:

As requested by the applicant, for details refer to attached page(s). ************************************************************************************************************************************************************

To be continued

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Test Report Number: SHAH00361401

Tests Conducted

Page 2 Of 4 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

(Ⅰ) Test Result Summary: Testing Item Result (ppm)

(1) Heavy Metal Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content (mg/kg With 50cm2) Negative (< 0.02)

Testing Item Result (ppm)

(2) Heavy Metal Cadmium (Cd) content / Plating ND Lead (Pb) content / Plating 60 Mercury (Hg) content / Plating ND Chromium VI (Cr6+) content (mg/kg With 50cm2) / Plating Negative (< 0.02)

Remarks: ppm = parts per million = mg/kg

ND = not detected @ = Due to the insufficient sample area, reduced total sample surface of 10 cm2 was used and the dilution factor

was adjusted accordingly. mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre

Tested components:

(1)Substrate. (2)Plating. Responsibility of Chemist: Dent Fang / Ken He

(Ⅱ) RoHS Requirement:

Restricted substances Limits Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ethers (PBDEs) 0.1% (1000ppm)

The above limits were quoted from RoHS Directive 2011/65/EU for homogeneous material.

(Ⅲ) Test Method:

Testing item Testing method Reporting limit

Cadmium (Cd) content With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content With reference to IEC 62321 edition 1.0:2008 in Annex B, by boiling water extraction and determined by UV-VIS Spectrophotometer.

0.02 mg/kg with 50cm2

Remark:Reporting limit = Quantitation limit of analyze in sample Date Sample Received:Jan.9, 2013 Testing Period:Jan.9, 2013 to Jan.14, 2013

************************************************************************************************************************************************************ To be continued

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Test Report Number: SHAH00361401

Tests Conducted

Page 3 Of 4 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

(Ⅳ) MEASUREMENT FLOWCHART: Test for Cd/ Pb/ Hg/Cr (VI)/ PBBs/PBDEs contents Reference standard: IEC 62321 edition 1.0:2008 REMARKS: *1: LIST OF APPROPRIATE ACID:

MATERIAL ACID ADDED FOR DIGESTION Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCL,HF Electronics HNO3,HCL,H2O2,HBF4

*2: IF THE RESULT OF SPOT TEST IS POSITIVE, CHROMIUM (VI) WOULD BE DETERMINED AS DETECTED. ************************************************************************************************************************************************************

To be continued

Sampling/grinding or cutting

Weigh sample and for different material,

digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline

solution

Definite temp. Extraction

Make up with deionized water and add Diphenyl-

carbazide solution

Cr6+

Weigh sample andadd organic

solvent

Soxhlet extractionor

Solvent extraction

Concentrate the extract and make up with organic

solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

Spot test

Get 50cm2 samples

Boiling water extraction

Metal Polymers / electronics

Negative*2

Confirm the tested samples are totally

dissolved

No

Cool and filter the extract

Yes

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Test Report Number: SHAH00361401

Tests Conducted

Page 4 Of 4 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

***********************************************************************************************************************************************************

End of report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

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SGqT€st Report

Testing Period :

Test Requested :

T€st Method :

Test Result6 :

Conclusion :

No. SHAECl215842621 Date: 13 Sep 2012 Page 1 of4

CHINALO LUOYANG COPPER CO., LTD.

NO,50.JIANSHE ROAD,LUOYANG.HENAN PROVINCE

The following sample(s) was6^/ere submitted and identfred on behalf of the clienb as : C10100(Tul)

SGS Job No. : sP12-027024 - SH

Date of Samole Received : 1 0 SeD 201 2

10 Seo 2012 - 13 SeD 2012

Selected tast(s) as requested by client.

Please refer to next page(s).

Plea66 refer to next page(s).

Bas€d on the performed tesb on 6ubmitted samples, the resulb of Lead,I\rercury, Cadmium, Hexavalent chromium comply wth the limits as set by RoHSDiredive 2011/65/EU Annex ll; recasting 200295/EC.

Signed for and on behalf ofscs-csrc Ltd.

,zQr"-Fan Jingjie, JJApproved Signatory

ryr{xrbrro-n'cFddd.ors{ "d *dn'bh rrbdsrh {r'@'f!qqrird-:miEr-

^. -q* r'o. -" *^ n 6.Eio,. eerir9! q!4+qgg-31@!!!l!o- --; l9li,l'^.q*Lll'.ig1li1ili*'f "aHfl .1ffi liiHl';d'#ff ;;,;;i;r;;'e-;-"i.?iEi@4araE@!dd_-*;il:?$tF-n9s'j*,H*"- *'"oor. -" -iiii'i'ri T !'r!i 119!!1'-.911rgl33il"lg::':.*':31'J"'.11:3g$iffi ffi :tff'ffili*;lil#{'tr#'#:#.1i1;'ftrsiii}i#rd',dilrrimrtrlo-;;;Bmti6"iib.fu,-

t'in!|n,olt iod)qrlffii4li.Ciror! 20@3{t.til.ltraldll$e+391 lr:2M3

IEIE{6-g1)0L660 lE{E(6-il)610536D ffi 6.!..d

NrlE-21)614@4 HL(F21)t$qS3 .llidtEe.S@

Menb6. oi rh€ scs grouD lSGs s.{)

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T€6t Report No. SHAEC1215842621 Date: 13 Sep 2012 Page2d4

Test R€sults :

Test Part Descaiption :

Sp€dmonNo. SGSS€mPlolD D6qiDdon1 SHA'12-158426 015 Copper metalsheet

Rema*s :(1) 1 mg/kg= 1 PPm=00001%(2) MDL = Method Detec{ion Limit

(3) ND = Not o€teded ( < MoL )(4) "'' = Not Regulated

Rolls Oil€ ive 201 1r85/EU

Test Method: With reference to IEC 6232'1:2008(1) Determination of Cadmium by ICP-OES(2) Determination of Lead bv ICP-OES'(3) Determination of Mercury by ICP-OES'(4) Determination of Hexavaler{ Chromium by Spot t€€t / Colodmetric lvelhod using Uv-vis

Te6t ltem{s)

Cadmium (Cd)

Lead (Pb)

Merdry (Hg)

Hexavalent Chrornium (Cr(Vl))

Notes :(1) The maximum permissible limit is quoted from direciive 2011/65/EU Annex ll

(2) osPot-test:N;gative = Absence of Cr(Vl) coating, Positive = Presenc€ of Cr(Vl) coating;.

Oh-e tested sample should be fufte; verified by boiling-wateFertrac'tion method if the spot test resuft

is Negative or cannot be confmed )o goiling-water-extraction:Negative = Absence of Cr(Vl) coatingpositive = presence of Cr(vt) coating; the detected conc€ntration in boiling-water-extraction solution is

equal or greater than O.O2 mg/kg with 50 cm" sample surface area

For conilon proteclion coating; on metals: Information on storage @nditions and prcducton date of

the tested sample is unavailable and thus results of Cr(Vl) rspres€nt status of the sample at the time

of testing-

t!nj! Ud! MpL pE

10O mSikS 2 ND1OOO msftg 2 ND1O0O mS/kS 2 ND

Negative

rhtddmdi]hndb'|i.

c!f,ffiffiffiffi'#fl*fiffi]ffiffiH'3dffi *fi ffi*fl l#trv;rm'ffi ndti;s.t**r,* ;*u.rn*s;sn"-f,$:ii

6l'ri.3r:ql|tll€a0*|}1 ll@!il.nD€rol$eSG8GtuP |SGSSA)

t r&&&r|!torap$0.|qi||rcn| 20(,3 IaE&aFlssf,g mci..cronfr[t-a)6{dcadt .{Fn'no.aro

r ElE {*-er)etoanrr j (i-a!1614s04

Page 42: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

Test Report No. SHAEC121584262'1 Date: 13 Sep 2012 Page 3 of 4

ATTACHMENTS

RoHs Testing Flow chart

1) Name of the p€rson who made testing: Jan Shi^/oyo Wangy'Allen xiao2t Name oI the person in charge of testing: Jeff Zhang/George Xusiil;;;;;;;;; tisioiilo totarrv o'v pr*conditionrng methoo accordrng ro oero/ now chart (cf*

test method excluded)

Sample Preparation

Heating to g0-95cfor extraction

1) Alkali Fusion /DryAshing

2) Acid to dissolve

Adding'1,5-diphenylcarbazide

for colordevelopment

A red color indicatesthe presence of cf'lf nec€ssary, confirm

PbrcdrHg

Positive

Negative

i'r4db rqshd g:dt:l. o' *rij91l#;Ygl'3'liii"lii-riifii"ir.r$a ;r;r u. c-1*.g cil!gTi.*3::::|.:: ;ac'@ri i"rhe. .thfrdi;;:;id1i;;.r,'d-"'d. @ih'k 4idllrr

ur tltrcolrytr d. ntdsrEfi [ffiiHffi #ffi ":ffi i##;?s'"r'f s&s*$ili:rm'""n'r'*m*.6i14t6mrHff #ffi.:ffiff H##ff**#rfficlms#^i:*""i';l**rhlrr'x;try'i'f,$:igiii io lim s * ta -la rt' -rr b tu.str.(.) r6bd

f a-flt&Yrrib.a&nc|l4ar9tcnE 5@+t.tt.*iEEi|llt$e!3r}l l*2@3

rE!€6-erF6Il w.i,.at.mdj{&a)5l@3 . rsdh€4@

r EtE (*-?1)6r1@5tH!o-er)€ @e4

M.mDd ol6e sGs goup (sGss )

Page 43: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

Test Report

Sample photo:

No. SHAEo1215842621 Date: 13 Sep 2012 Page 4 of 4

SGS adhenticate the photo on odginal repod only

"' End of Report *'

yg&rt&Lrbrt&irrfal|ldlctrs 2m3+l.It.tiE8lfi ft.ort39l al: ?@l

r ElF i6-2r)611G63HU (6-21t61{6el

tEtE {E+r)0KI9{:(e-aF|e3

M.nb.r ot tr scs Grouo lsGs &r)

Page 44: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

Vali

Please sGs

n

x{-d,+E+Test Report+4€+r*nDtr &2'4TY-OEIt ELECIRONIC NORKS I]0., LTD.

atEi #* &frrF*-1i4eti,NO. 49, DINGFU ISt STREET, CUEISS,{N TONNSHIP, TAOYIJAN @INTY 333, TAII'AN

; i ' i , T - E t P l e a s € r e r e r t o n e x r p a s e s )

f tq4(No.) : cE/20r2141404 A $ ( D a i e ) , ? 0 1 2 / o 4 l t 3 F j R ( P , r . ) , I o f 6

iultt|:l[ i||| ||t

t Tr l t l&.s. i i 6:F '*{ t , s6*P 4*j ! ,E*P*lsioT (rh. rol toeirs sarpres ras/sere subbit ted andi d e ! t i f i e d b y l o ! b e h a l f o f t h € c l i e n t a s ) :

{*.S?*B(s,'ple D€scripiion) : cAlBoN FILM REstsToRs

i* .S4f f (s iy le/ I i€ ' N" . ) : RD sERIEs

4t ' i fEs(s:hple R€ceiy ins Dat€) | 2ot2/04/07j r j : t *H( l€st ins Per iod) . 2012/04/07 " io 2ar2/n4/ f i

; r l t {glF.(Test Results)

Comodnr. ! I i^ i .1

"nd d atuir bm,r dd.JmenE soR i, rems aio ondroEbEdrcn-o;men.Erl/v',o.,ncnttr; € o;Lrad Ad;imn- 3 d.atr 'd heiLldsndmrsuesdernedherc'n avhorde,orbsd(umemdadvsedbai

se ime or iE '.reirehon onry 5nd wuiin fie rimiB oi c rsfs iisrtudioi3, ir ldy The compaiy! ele reEooi3b rirr s ro iB c ed.id rhr. do@me doer no, e.ne.aie patoeth 5

{rtwr-'s

99t|Cd ftr.id

ClEntcd fabodb.t - Trip.i

Page 45: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

l'fla.+R+t f , 6 ( N . . ) , c E / 2 0 1 2 / 4 t 4 a 4 a * ( D a r e ) . 2 0 L 2 / o a / L 3 Fl( (Pase): 2 of 6

Test Report+ ftg-+ t-Xak hA r&'r aTY-O[\I ELECTRONIC N'ORKS CO., LTD.

'E E ,ia ,I hrF U -6 1ett,NO. 49, DINGFU lST STREET, GUEISIIAN TOII']'{SHIP, TAOII]AN COUI\'TY 333, TAIWAN

' r l i l ** .(rest Results)

flASy'i(PART NAME)NO.1

'JJt' E(T.3t I t€rs)

+{q(U' i t )

',tarrl( l rerhod)

t*,lirlf ll{t(rDL)

S;F(ResuI t )

N o . lji / cadniri (cd) bg/kg ++w 62321. ?008ri i , t lS,G}*A€

*,F+6+jrt r$d,i*,r|. / lvitrr rere.enceto IEC 62321: 2008 and pe i fo rned by

ICP-AES.

2

,E / Lead ( Pb) \a/ka 2

i / x e r c u , y ( H s ) 2

' i 1 !J& / Eexava len t chron iunc r (v r )

+* lEc 6232r, 2oo8t;*, 4w-vrsiht,l./ I [ i t h r e f e . e n c e r o I F r - 6 2 3 2 L : 2 a a 8

and Der fo rned 6v UV-VIS.

t*t*13+ / srE of PBB3

++rEc 623211 2ra9t)L, ,^fr"taE ft /g, *d , * i l l . / l { i th re fe rence to M

6232r : 2008 a .d per fo rned 6y @/MS.

- i4## / lonobronob ipheny l 5: i ! t tX . / D ib ro ioh ipheny l

: l#* / T . ib ronob ip l .ny l 5€ iA#* / Te t !ab .onob iphenyL 5

i i * # j F / Pen tab io f r ab iphe . y l 5

n;*#* / lexab.onob ipheny l

+*d f / Bep iahroDoh iphenr l

^ i {#X / Ocrab.onoh iphentL

i-&4x' / Nonabronobiphenyl

+A#f / D€cahronobiph€!y1 rE/kg

a " ; ; - , " - ,

r " t oo I i a s i I i ! "i h ' sd ; c i nn in " . sLe ' t r i - o rd i ' ' 0 "db6k ' aE | coo$n .and b, eleftn'- rodobdre^u *rtrr16 6r\and.o dionst_Lrd-fii-.^-.-;";;',;;:;i;;;;

;;.6;;i;;;;dd";aia;iM6e me o, c 'm€i$don on v ard - fin m. 'm € or c ie'ranedodtom eFL,nd d;msn n -L eu6 r oror fldl aoproviL o' r€cr@rv { v - Eltdr'.n rF?..i o4€ y o' 'tsfi@tdr d '?ode" o

. . . ! , ! , x ,w .G" " " k ,N . r i i _n i r . , : , . , r r . i r ' ] : r f :

' i :-;;';"::---e' )F ^":\' ;

ll| l||l ltl]ll

!A'I,EiT] OIIXED ALL PARTS)

Page 46: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

,r1ff,+E+Test Report+q€+!*&l,)trlE?] 61TY-OHM ELECIRONIC II'ORI{S CO., LTD.

'rfr *t,! *TF#-{54e!tNO. 49, DINGFU lst STREET, GUEISIIAN TOSIISHIP, TAOWAIi COUI-TY 333, TAIIIAN

f t d q ( N . . ) , c B / 2 0 r 2 / 4 t 4 A 4 q S ( D a t € l : 2 0 r 2 l n 4 l r 3 q&(Page): 3 of 6

tlfi[]l]t |l[]ll

nrl{t E +&(Uri t )

riatrt t;*.nrtEII{t(uDL)

s*(ResuI t

N o . 1

t*t*nll+ / su! ot PBDE3

++rrr 6zszL, zoo9 *, "

ala&fr/X: *d,&i l l . / $ ' i th .eference to IEc62321t 2008 and lerforned by CCIYS.

- *$ rFe / Monobrohod iph€ny l e th€r 5-&d* l i / D ib lonod iphen l l e ther 5: * # *6 { / T r i b romod iFheny l e the . rg/kg 5

€)*# f ,6€ / rebabro f rad ip [enr l e ihe ! 5

tt*|f, F6t / P€ntabronodiph€nyl erh€r 5

*)Ald*at / liexahronodirhenyl etler 5

+i ! * le t / Hep lahrohod iphery l e ther

\ *$ iSA4 / o . rabrorod ' phefy l € tber na/kar 'L * i *A t / No.abronod iphenyt e ther

+ t l$Xq{ / Decabronod ipneny l e !her

f i t i (Note) :r . mAlks - ppn ; 0 .1wt% : 1000p!n

2 . n . d . : N o t D e t € c t e d ( : i . + A * )

3. . \ lDL = I te thod Detect ion L in i t ( t * . lA i l i i !FR4n)

4. - ' : Not R.s" l , t .d (*4, i4 ld)

5- *.s6tr1a.€AAq;t^.*+a+x,l?t , +E*f {l, lEaxls{,ex4.Ra* q'€tl+-*ttr6i }9. (r!e sanpresv a s / v € r e a n a l y 2 c d o n b e h a l f o f t i e a p p l i c a n t a s n i x i n a s a n p l e i n o n e t e s t i n g . T l e a b o v c . e s u l t s

w a s / w e r e o n l y s i v e n a s t h e i i f o . n a l i t y v a l u e . )

ahpLEG) @ed lrc 'en Bpon €dno, , ! t r ' d : :

" " ' - d ' - * ' sg ,eoon . . " . p ' y sLqe losceaa ' cond ioao : sPa@p ' | 6oo 'e ' i " s sdso "o11;; ;,;d;.i- 6;; A;n;b "Iiied; rems ad cmo rcmo re * a.o.cot'rr'-cmt' Dotu; ; ; ; ; ; ; i " : ; d ' i i ; , ; ;m ; i ; ; ; ; ;@- ; s i , a ' dv rd dh t sdoc . -d ; s ' * o | s r r comp '1s rnd re5a l;;';;

"i J;k;;dm o^i; ;;d *ihin r" r-

". cr€ds Etlno$, !

-- comoaa e s e

r6d$dm 'm e$E! no alr pr r.omDanr ArvL?Jrhorr.nab€roj bqeryo kir\16brd$€oae,ro

Page 47: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

x{fi,*E+Test Report+,!r€+r-*Etla rRa 4TY-OHM ELECTRONIC S'ORKS @., LTD.

ttF *ra,r. fi18fr-64eftNO. 49, DINGFU lst STREET, GUEISMN TO{NSHIP, TAOllJtl\l COUNTY 333, TAIIAN

t f , 4 ( N " . ) , C E / 2 0 1 2 / 4 1 4 0 4A l , ! ( D a t e ) : 2 0 1 2 l 0 . 1 / 1 3 Flt(Pase): 4 or 6

Il] tI| ]||t ]

r )

2)3)

l8*ttrT.tfi,tenzt*+ ' f.xge*8Jll. ( ifir&irlilt*r*rf ) / Thse samdas reredissolved totally by pMdirioning method according to berownow charl. ( cf't€€t ftEthod exduded );r!31,/- l : $+l* / Name of it€ peBon wt\o wde m€surmenlr crrmbgreal Yangtlr,t { lr'- : #8+ / Name or the person in charge or measu€m€.t Troy Chang

* rlL+t n.,i + *4tit,'*{|. / lcP AEs

lls}}{ / SamDle Ma|enal ,iilb&&lttr / oiq€slion rdd

slel. @DD€r. aluminun. 6oldera+. 4&, ld, n,ne, tt,l. /Aoua€oia. HNO.. HCl. HF. H,O

Gold. .latinum. €lladlum. eEmlc

,i,*, !tr+, rr|.n, f& / H,sor, H,o,, HNoi, Hcl,, \EE*re!84 / arry acid ro roral digElion

'mpp ! t s {eo f t ' e$cpd€ToL d m d r i \ , , , , . 1 r i t E F 1

" l - U t

r nEnMmen ,D E l Jeds rn . co i€, r oo ' e€dT . . , o f a l ddomen .9 ' JdF 'de -sJ t conono ' " , o lE ' ei ; , . d t n ;N l d i i ; d ; " ; n i i i n$do t sdoomsn r t . o , r d t ' do ru l o ' e ' d ' n . ohoeo r t . . , ' 1 " co rpd ' / s r r d ssa ri n . i n ; ' d € i w n D n o n " m o d . . r y F . ! o @ a . s c . A 9 r \ o '

na .d - . no tuT L F5 oo - . 6 i r 6 fd rbc5pmrodcoaoan'{rydrafu?eaF'dto|

r .New laF i . e tu 'wo i r , ; ; ;X . i i r ' : i : n l i

t{ . tftite /Cdling P€ps,gtion

id r'\,i*.sl! /sample Mesu€ment

ii.f 4 lq *.s 6ltt f ,rn trnt* at *'tli )X lE(+Ti.,in) /Acid digeslon by suiiable add depen@d dditrerent sample mabrial (as bdowtable)

4*/t&/&.n&6i&*fiiL /Microwave dEeslion wilh HNOTHCI/IIF

,"*antf ,aA4,iti'lb+{( / Heat lo appropdale

&16#ti /AlkaliFusionl*6* / HCr to dissor\€

+trii'E'dfs /Cool,filter digEslate lhrowh filter

nf,f)L-Tf,ararf& !jrl+is,5*E 540 nm al4

absooane at 540 nm bYUV,VIS

Page 48: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

,fla#+i i , 6 ( N o . ) , c ! / ? o r 2 l 4 1 4 0 4 E S ( D a t e ) : 2 0 1 2 l 0 a l 1 3 F*. (Pase): 5 or 6

,iA#S'/ t**$*+&*,AIi / PBB/PBDE anatyticat FLOW CHARTr,FIA,].F : ti!4# / Name of lhe peBonwho made measurement Romsn Wongr idt{Q I ,]. : f,*-R / Name ofthe person in draQe ol measurement Troy Changiq,^,4{t3F / Fi6r testing proces ------------t**ti&iltte,4 / oDlional sc€:i;Si:4 / Cmfmalion roes -. -.>

Test Report+q€+!*rtDArF?i.1TY-OI!,I ELECTRONIC WORKS co., LTD.

dr, Ei tr 1, ,! ftrF r, -?r4 efiNO. 49. DINGFU ISt STREET, GUEISHIX TOI'NSHIP, TAOI'IJI]{ COUNTY 333, TAII'AN

lllr || ]||[ll

fJ-"-jE pr"r"rt*"ti l*s;6,r _l

J

Screen analysis / t? 6 r|fi

I Concenlrale/Dilute ExtEcted solulion I| +*ri;ts/ft* |

sample erlraction #'&+41Soxhlel method *!\,+4.t*

Analysis by GC/[,IS / nfi{fif :*C..itr

lssue Repod l*lr*&+

c o - p a a f i l , l r . - irhis dnmr rs isu.d br the c.mpany o6td rd ns Gs.dr cond I on

rimrlar od or riabiliry rddemnficd on and iarisdidion is&ss d8fi.d seEri. tuy ho &r or rh6 doomem s adyhed rh s rhe company s fnd nos aran,Tlieco'F.dy3$eresps3ibiily

., 1l::Li!! |: l l l i lr-t99193t::::-:z: b,3i.1gt:5::31 !!!,rt,.!!

Page 49: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

,flH,+E+Test Report+.[€+r*ItAa Ba 4TI-OHtrI ELECTRONIC \{ORKS CO., LTD.

*rEl tf* l'l] srF4 -fi 4e*NO. 49, DINGFU 1st STREm, GUEIS|IAN TOINSHIP, TAOI'ItA\ COIJNTY 3i3, TAIn,All

! E € ( u . . ) , c E / 2 0 1 2 / 4 r 1 a 1 S ( D a t e ) : 2 0 1 2 / 0 4 / 1 3 F * . ( P a s e ) : 6 o r 6

rl| u ru t

+ F.4 f5trfrt*a ' tli+&lhttrlzt{.s/*.fr. .(Tbe tes ted saop le / par r i s Da lked by ad ar rox i f i t , s sho , r oo rhe Dhoto . )

. . 4+tEE (End of RePorr) **

eG) Frbd rhG Br e@d 6nior be IL d m o . n ! l l t ' t ' l t : : r R e A ' l i l i

_ n . 1ny ibjed ro i6 cdnsa cdndiroi3 o

nd iLltudidon suo, d€rnod rh.cin av h.@orb s dmmed aadusadbr " rm"o ,E t r - ; . . ond rand { ; ! f r e . d " . p .13$eF .p0 .3 " , oc (nd ' o ; 6 ;paaeahs

& " p i 1 . | 1 { l t . l p r o

4L404

Page 50: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

,E{-d,+E+Test Report+lE€+a*xt{r}t rFa ;lTY'OHM ELECTRONIC SOIIKS @. , LTD.+tE t&a,r. sr!H-{54ettNo. 49, DINGFU lsr STREEI, GLEISHAN To$NsHIp, TAowAti COI'NTI 333, TAI{A}I

f f6(No. ) : cEl2012141405 E l q ( D a t e ) : 2 0 r 2 l 0 4 l 1 3 F t t ( p a 8 e ) : I o f 4

Validit nownFor QueSIlPlease Co ith scs

tl][t[I| ||l

, r (T g,&.Arf &*P,*8, AA *F +* -rE+F *gje-F (rhe rorrovi ls 5aEpr€s va./eere subnit ted andi d e n t i f i e d b y l o n b e h . l f o f t h e c r i € n t a 6 ) :

l * "%Z*l (s . rp l " Desoi pt i on)

&&4l t t (s ty l€/ I tem No. )] l t4 t E S (sanrre Receiv ins Date)tF ldS Fl ( r "s t i ns Per i od)

j d A S * ( T e s t R e s u l t s )

Cl|gIicC L*ordo|y -TQd

sa@els) re,ed rh 5 res repon ann1 l - - . [ : ,

rhs documd s 'ssud by rhe comn c Dmumenis d M es @nren/rentu*nd.cdd riom,rems e D_odme

inidion0Jabry.indsmnir€Lionadru'$don,su!sderiedhd6inAryhorderorrisdocurudifadvedhahil ,'" i- s oi Cier", ,1,.atun. d \ 5 ro \ C er I ar mb dtufred oo

he ru estene orrhe.w

. CARmN FII,M mSISTORS: Rn SERIES, 2 0 1 2 / 0 4 / 0 7| 2 A l 2 / 4 1 / A 7 T O 2 0 1 2 / 0 4 / 1 3

: #- tT-F (p le,se refer to neyt pases) .

{NwaE

Sgmdior

Page 51: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

,F{a#+Test Report+.8€+a*xtr)tr R?r;1TY-OHII ELECTRONIC I'ORI{S @. , LTD.

tt E Ff i, Jl frtG rf -64e&NO. 49, DINGFU 1st STREET, GUEISHAIi mfi{slllP. TAOToAN @ll\Ifi 333, TAI\IAN

idgl** . ( r€st R€3u1!s)

f i 4 ( N o . ) : c E / 2 0 1 2 l 4 r 4 0 5 a S ( D a t € ) : 2 0 1 2 l 0 4 / 1 3 F * ( p a 8 e ) : 2 o r a

rtl|[]ll I

rq{ d,$/n (PART NAME) No.r !8fin9 jr,j (MIED AIr PARTS)

rl*,{ c +{i(Uni t )

,ng,tit(Metbod)

,i*.firdEIEIT(UDL)

S;F

N o . 1

E* / Ha I oscr

A i ( f , ) / H a r o s e n - F r u o r i n e ( F )(Cr ' 's No. : 14?62- 9a-8)

4+Bs EN 11582:2ooi, , l lF+,Ef r&"+]8. / l { i th r€ ie.ence toB S E N 1 4 5 8 2 : 2 0 0 7 . A n a l y s i s w a s

5 0

6*- (S.) i Haloren-chlor ine(cr) (c/'s No.: 22537 - r5-r)

5 0

6* ( ; l ) / Halosen-Brooine (Br)(CAS No. : 10097 -32-2 )

5 0

6 i ( 4 * ) / H a l o g e n - l o d i n e ( I )

(cAS No. : 14362-44-8)

5 0

_ ' r r r : t l i , r t i , l ] r r i

f i t i ( N o t e ) :1 . E g l k g = p p n i 0 . 1 n r % = 1 0 0 0 P P n2 . n . d . = N o t D e t e c t e d ( , t * S g )3. MDL = rdethod Detect io! LiEir ( t l i lAiXlEf&{6)4. *."%itx!:taA,if f ;6^**,Ea,Flii, ' #.+f 6rrE +;rli{,r* Rrf\** f l@fl +-*tf atl}8. (rhe sanpres

v a s / w e r e a . a l y z e d o r b e h a l f o i t h e a p F L j c a r r a s n i x i n g s a n p l e i n o n e t e s t i n S , T h € a b o v e r e s ! l r s

w a s / v e r € o n L y s i v e n a s t h e i n f o . n a l i t y v a l u e . )

r / t - l : li;sidmeft s,,:eod' ia-aiioJi,;-od b ,c".urco o m oord ! d"don' 1rdoao - b abed6 remsaldcro 'orb Fr.4i.*i."i,i n

". 'oii"'i'er"in; J iiti-"i' ,*,* d._* b". .A.vnode o i6doi -- ;ad.*oh

co -Dary +v ' adnd.'Pd d'"?'. i

Page 52: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

,flaa+Test Report+4€+a*xirla rE? '1TY-OHI{ ELECTRONIC {ORKS CO., LTD.

&m tia &ftrF!x-61efiNO. 49, DINGFU lst SIREET, cUEIsllAN TOr'lrSHIP. TAOI'IIAN COlllTY 333, TAlll'AN

f r ,&<N..) . cE/20t2/4r405 A*(Date) | 2or2/04/r3 F*.(pa8e) : 3 of a

flltN tlttt][]t!tl

I

I

**+ttti,An / Analytical flow chart of halogen contenl

xl*\,^ F : ft.g* / Name of the pe6on who made measurement Rita Chenirl:{,EI l' : ti.B* / Name of the person in charge of measurement: Troy Chang

&+E )tt&.'5fr tAnalysis was performed by lC

empiels)rased thstnrcponain' r i , t i - : t t I r : ;i h s d ; ; l nan ,

" ' * - n t ' d ; c , i D , : ; s ;F :o s - "Da o o10 '>

"nd b, e{fttu romardocJm.+ ad& rd er'drd.oldio aro L*a;'l;;;',;, ..;;;fti"* "-;.-d..,s'esoaneorrc,.'n at j . i . i " i . t n i i i l i " i i ' . ; : J ; ; ' " ; ' n i ' i ; , n i c ' c - r . sndd . ,

I 4{ d r ord d_Fn aDprov?r orraro-@a A v i.Lllo zen aF%m' !'ero' iis'r6ro o t@nre1ro

i . r : . c ; i , l i i 5 r :

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,flff.#+Test Report

! t16(Nd- ) i cE/ 2012 / 414 O 5 A r [ < D a r . ) : 2 0 7 2 / 0 4 / 7 3 q * ( P a s e ) : a o f a

+E€+r*xcSA].Ea5lTY-OH}I ELECTTONIC WORKS CO., LTD.

dt 6 tf *' & 8rA r8 -ai4 efiNO. 49, DINGFU lst STREEI, CUEISEAI'TOWNSHIP. TAOI'IJAN COIJNTY 333, TAIX'AN

. mttrrttt*i ' Fl*'i&f Ft*jd.iisi ${-n. .(The tes ted sa ip le / par t i s oark€d by an a ! .o r i f i t , . .hor ! o ! tbe pboto . )

. - t r + e . € ( E . d o l R e p o r t ) . .

smp sG) L6n.d rh Ekd6ponannc o m 6 d l T L t l l : ; , 1 { : l : . , 1 1 : l r l l \ f l i l a l '

dd |o ' . | . f t n ' ' | o f t l d ' o f uP rs * ' d6 - r r ' andc .1d f t o | s | o 'Egh1DFJp "SJM*5@ne |d r5 " t ' o ' d0oF ' | "T ' " on fuT rArim,krion ot r:biriM ind8mmdion and lfisnrdron isues d.fned rE€in tu

.nyThecomp.iysso|eregoorcrbiiy

t tI|[ l[I.]l

41405

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Page 58: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

Test Report No. SHAECl216714748 Date: 25 Sep 20 1 2 Page 1 of 5

ZHEJIANG ASIA GENERAL SOLDERING&BRAZING MATERIAL CO'' LTD

XIHU INDUSTRIAL PARK, SANDUN, HANGZHOU CITY, ZHEJIANG, PROVINCE' CHINA

The follorving sample(s) wasl/verc submitted and identified on behalf of the clienb as : LEAD'FREE SOLOER

WIRE

sGS Job No. :

Part No. (P/N) :

Composition :

Date ol Sample Received :

Testing Period :

Test Reqlested :

Test Method :

Test Resulb :

Condusion :

sP12-028285 - SH

YTW1o8 (692535-001' 692535-003 )

Sn3.0CuRE21 gep 2012

21 Sep 2012 - 25 seq 20 12

Seleded test(s) as requested by client.

Please refer to next page(s).

Ple€se refer to next Page(s)Based on the perfrcrmed tests on submitted samples, the results of Lead'

Mercury, cadmium, Hexavalent chromium, Polybrominated biphenyls (PBB)' -Polybrominatecl diphenylethe6 (PBDE) comply with the limits as set by RoHS

Direciive 2011/6tEu Annex lli recasting 200295/EC.

Signed for and on behalf ofsc$csrc Ltd.

,zQv"-Fan Jingjie, JJApproved Signatory

rhb@drb &.d tt tu cqryry aDld b b-

r4rg,.giffi:iii; ftH,#'ffiffiffiffffififfii';:i;c*;ivi ;f -d.urb-r-brbcld-n

tltrridtarblnlud.'i.groh 2@+t.rt.lE6lufte+eet al:4

iElE6-?1Fa€m9 wd{rm*.oeagms . *!|h.e4(!ii

108{S.?r)61{!!anL(d-21nl4@a

ri.rnb.lol0|. Sos oollP (8oS S )

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Teet Report

Test Resufts :

No. SHAEC1216714748 Date; 25 Sep 2012 Page 2 of 5

Test Part Desc.iption :

SpodmqrNo. SGSSandolD D*qiptlon1 SHA'12167147.041 Silvery wire

Rema*€ :(1 ) I mg /kg= 1 PPm=00001%(2) MDL = Method Detedion Limit

(3) ND = Not Detected ( < NIDL )(4)

"" = Not Regulated

RoHS Diradv€ 201 1/65/EU

Test Method : with reference to lEc 62321i2008(1) Determination of Cadmium by ICP-OES.(2) Oetemination of Lead by ICP-oES(3) Determination of Merdiry bv ICP'OES(4) Determination of Hexavalent Chromium by Spot test / Colorimetric Method using UV-Vis

(5) Determination of PBBS / PBDES by GC-MS'

Test ltem(s)

Cadmium (Cd)

Lead (Pb)

Mercury (Hs)

Hexavalent Chromium (Cr(Vl))

Sum ol PBBSMonobrcmobiphenylDibrcmobiphenylTribromobiphenylTetrabromobiPhenylPentabromobiphenYlHexabromobtphenylHeptabromobiPhenylOctabromobiphenylNonabromobiphonylDecabromobiPhenylSum of PBDESMonobromodiphenyl ether

Limit ud! M0!100 mg/kS 2

1000 mSftS 2

1000 mS/kg 2o

1000 mgkg- mSikS 5- mdkS 5- mS/kS 5- ms/ks 5- mdkS 5- mg/kg 5- mg/kg 5- mgftS 5

mdkg 5- mS/kg 5

1000 mS/kg- mdkg 5

@1ND55ND

NegativeNDNDNDNDNDNDNDNDNDNDNONDND

;i;a' ir*&{.d n dnl.,.d/bb 6rr.{.tt.d '

tlrr'ttafi$bDd|rddna.{rofr !93{l -I*.*trBlt!l8aea3+l aI: 2@

rE E6+r)B1a@ IEE€GA)6|€Sdrgnj{c-2rtauozg $i6GA)4|d063

M.n&r ot fi. Soa or.r0 (8Gs sA)

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sGqTest Report

Test ltem{s)

Dibromodiphenyl etherTribromodiphenyl etherTelrabromodiphenyl elherPentabrcmodiphenyl etherHexabromodiphenyl etherHeptabromodiphenyl elherOctabromodiphenyl elherNonabromodiphenyl ethetDecabromodiphenyl ether

Notes :(1) The maximum permissible limit is quoted ffom direclive 2011/65/EU' Annex ll(2) ospoltest:

Negative = Absence of Cr(Vl) coating, Positive = Presence of Cr(Vl) coating;

Ohe tested sample should be further vedfied by boiling-wateFexlraction method if the spot test result

is Negative or cannot be confimed-)oBoiling-wateFextraction:Negative = Absence of Cr(Vl) coatingpositive = Presence of Cr(Vl) coating; the detected concentration in boiling-wateFextraction solution is

equal or greater than O.O2 mg/kg with 50 crn" sample surface areaForcorosionprotectioncoatingsonmeta|s:|nformationonstorageconditionsandproducliondateofthe tested sample is unavailable and thus results of Cr(Vl) represent status of the sample at the time

of testing.

No. SHAEC1216714748 Date: 25 Sep 2012

ud! Mot @1mg/kS 5 NDmS/kS 5 NDmdks 5 NDmSikS 5 NDmg/kS 5 NDmSftS 5 NDmdkS 5 NDmS/kS 5 NDmdkS 5 ND

Page 3 of 5

tird!

iiiiir-r'ud-poa-t.ovbrk.md(.rrrd'

ttlEttlFYErto d!| |lqsrflddctrr 2@ rE E64r)6la{!54rii('-zl5r4&t4

ra€6+1F*n19f{! (6-er)6,La6t+l -ll.*tr6lurlftaer+gttl l|: 2a@

€mD.r ot !h. sGE GrcuP (8GS SA)

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Test R€port No. SHAECl216714748 Date: 25 Sep 2012 Pag€ 4 of 5

ATTACHMENTS

RoHS Testing Flow Chart

1) Name of the person who made testing: Jan Shi/Yoyo Wangr'Allen XiaolGaryXu2) Name of the person in charge of testing: Jeff Zhanglceorge Xu/ Linda Li3) These sampleswere dissolved lotally by pre-conditioning method according to betow flow chart. (Cf'

and PBB!,/PBDES test method excluded)

Sample PrepaEtion

1) Alkali Fusion /DryAshing

2) Acid to dissolve

Heating to 90-957for extraction

Adding 1,5-diphenylcalbaAde

for colordevelopment

Adding 1,5-diphenylcarbaade

for colordevelopment

A rcd colorindicatesthe

presence of cr8t.necessary,

Pb/CdHg PBBs/PBDES

t6&tttY|laf{dpdtrd,st{iatr @'Fr.-*.ltrEtdttidotsr+l lr:2@3

r ErE F2!) 8r@53rll Fzl6lil&5aa

I€EF{|FMDrij F€i)i6063

lLint r ot th.sos Gro{p (8GS s,l)

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Teet Report

Sample photo:

No. SHAEC1216714748 Oate: 25 Sep 2012 Page 5 of 5

sHA12-167147.041

SGS authenticate the photo on odginal report only

". End of Report '_

tu&.{drbdnrtbtu d..{d I bd rr h orFry ndd b rr oodr c.ddr o, sdi- rtu orr..r. hrlbd .rrh i!ra..!...* t'd @r'oqtuqd n rmr d c.du| @ Edmr o.eid d tlndrsso&E sEs4!ll4.r-ril_kr.rllnddb end r. dn-d b.k*r'd!. dnfu i.d| dr6 i. ct'e6r'.bffimidror. h.&,dr.dr4ffiFLb.tur&ldFcu&..rdLl&lr rd.&k, .bglfuoi.lb..oo&qan6pihtun,riMt st'ff..'|erEdctuc.ir4d|n-tu|i-.hAnrdrrrd

't6.h.nril*dnN..rnhidrtb6 |hpr.Gl6H.

fbtlnsll||lto dftnrada.cfirr ?w rEl.Fa)flroe5a r€.EFtl6&9 w.o.!.ch-tl'*,EEldJlsaol€tl i*@ u!9Fa)6l.aa!Da t{jF46ea .{.d*reg.@

[.tn!.rolfr. scaGr.{, {8GSA )

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Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338

TEST REPORT NUMBER: SH AH00334352

AUTHORIZED BY: FOR INTERTEK TESTING SERVICES LTD., SHANGHAI

JACOB LIN GENERAL MANAGER

PAGE 1 OF 8

APPLICANT: LITTELFUSE,INC. DATE: AUG 15, 2012 800 E. NORTHWEST HWY ATTN: A. CESISTA/ K. BACILA

SAMPLE DESCRIPTION: One (1) submitted sample said to be White Yarn. Part Description : Yarn. Part Number : 648102.

***************************************************************************************************************************************************** TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S) *****************************************************************************************************************************************************

TO BE CONTINUED

Page 64: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338

TEST REPORT NUMBER: SH AH00334352

TESTS CONDUCTED

PAGE 2 OF 8

1 ( Ⅰ) Test Result Summary:

TESTING ITEM R ESULT (ppm)

HEAVY METAL CADMIUM (Cd) CONTENT ND LEAD (Pb) CONTENT ND MERCURY (Hg) CONTENT ND CHROMIUM VI (Cr6+) CONTENT ND POLYBROMINATED BIPHENYLS (PBBs) MONOBROMINATED BIPHENYLS (MonoBB) ND DIBROMINATED BIPHENYLS (DiBB) ND TRIBROMINATED BIPHENYLS (TriBB) ND TETRABROMINATED BIPHENYLS (TetraBB) ND PENTABROMINATED BIPHENYLS (PentaBB) ND HEXABROMINATED BIPHENYLS (HexaBB) ND HEPTABROMINATED BIPHENYLS (HeptaBB) ND OCTABROMINATED BIPHENYLS (OctaBB) ND NONABROMINATED BIPHENYLS (NonaBB) ND DECABROMINATED BIPHENYL (DecaBB) ND POLYBROMINATED DIPHENYL ETHERS (PBDEs) MONOBROMINATED DIPHENYL ETHERS (MonoBDE) ND DIBROMINATED DIPHENYL ETHERS (DiBDE) ND TRIBROMINATED DIPHENYL ETHERS (TriBDE) ND TETRABROMINATED DIPHENYL ETHERS (TetraBDE) ND PENTABROMINATED DIPHENYL ETHERS (PentaBDE) ND HEXABROMINATED DIPHENYL ETHERS (HexaBDE) ND HEPTABROMINATED DIPHENYL ETHERS (HeptaBDE) ND OCTABROMINATED DIPHENYL ETHERS (OctaBDE) ND NONABROMINATED DIPHENYL ETHERS (NonaBDE) ND DECABROMINATED DIPHENYL ETHER (DecaBDE) ND HALOGEN CONTENT FLUORINE (F) ND CHLORINE (Cl) ND BROMINE (Br) ND IODINE (I) ND

REMARKS: ppm = PARTS PER MILLION = mg/kg

ND = NOT DETECTED

RESPONSIBILITY OF CHEMIST: DENT FANG / KEN HE *****************************************************************************************************************************************************

TO BE CONTINUED

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Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338

TEST REPORT NUMBER: SH AH00334352

TESTS CONDUCTED

PAGE 3 OF 8

(Ⅱ) ROHS REQUIREMENT:

RESTRICTED SUBSTANCES LIM ITS

CADMIUM (Cd) CONTENT 0.01% (100ppm) LEAD (Pb) CONTENT 0.1% (1000ppm) MERCURY (Hg) CONTENT 0.1% (1000ppm) CHROMIUM VI (Cr6+) CONTENT 0.1% (1000ppm) POLYBROMINATED BIPHENYLS (PBBs) 0.1% (1000ppm) POLYBROMINATED DIPHENYL ETHERS (PBDEs) 0.1% (1000ppm)

THE ABOVE LIMITS WERE QUOTED FROM ROHS DIRECTIVE 2002/95/EC AND AMENDMENT 2005/618/EC FOR HOMOGENEOUS MATERIAL.

(Ⅲ) TEST METHOD:

TESTING ITEM TE STING METHOD REPORTING LIMIT

CADMIUM (Cd) CONTENT

WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN CLAUSE 8/9/10, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES.

2 ppm

LEAD (Pb) CONTENT

WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN CLAUSE 8/9/10, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES.

2 ppm

MERCURY (Hg) CONTENT WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN CLAUSE 7, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES.

2 ppm

CHROMIUM VI (CR6+) CONTENT

WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN ANNEX C, BY ALKALINE DIGESTION AND DETERMINED BY UV-VIS SPECTROPHOTOMETER.

1 ppm

POLYBROMINATED BIPHENYLS (PBBs)

WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN ANNEX A, BY SOLVENT EXTRACTION AND DETERMINED BY GC-MSD AND FURTHER HPLC CONFIRMATION WHEN NECESSARY.

5 ppm

POLYBROMINATED DIPHENYL ETHERS (PBDEs)

WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN ANNEX A, BY SOLVENT EXTRACTION AND DETERMINED BY GC-MSD AND FURTHER HPLC CONFIRMATION WHEN NECESSARY.

5 ppm

REMARK:REPORTING LIMIT = QUANTITATION LIMIT OF ANALYZE IN SAMPLE

Date Sample Receive:AUG.9, 2012 Test Period: AUG.9, 2012 To AUG.15, 2012 RESPONSIBILITY OF CHEMIST: KEN HE

***************************************************************************************************************************************************** TO BE CONTINUED

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Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338

TEST REPORT NUMBER: SH AH00334352

TESTS CONDUCTED

PAGE 4 OF 8

(Ⅳ) MEASUREMENT FLOWCHART: TEST FOR Cd/ Pb/ Hg/Cr (VI)/ PBBS/PBDES CONTENTS REFERENCE STANDARD: IEC 62321 EDITION 1.0:2008

***************************************************************************************************************************************************** TO BE CONTINUED

Sampling/grinding or cutting

Weigh sample and for different material,

digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline

solution

Definite temp. Extraction

Make up with deionized water and add Diphenyl-

carbazide solution

Cr6+

Weigh sample and add organic

solvent

Soxhlet extractionor

Solvent extraction

Concentrate the extract and make up with organic

solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

Spot test

Get 50cm2 samples

Boiling water extraction

Metal Polymers / electronics

Positive*2

Confirm the tested samples are totally

dissolved

No

Cool and filter the extract

Yes

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Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338

TEST REPORT NUMBER: SH AH00334352

TESTS CONDUCTED

PAGE 5 OF 8

REMARKS: *1: LIST OF APPROPRIATE ACID: MATERIAL ACID ADDED FOR DIGESTION POLYMERS HNO 3,HCL,HF,H2O2,H3BO3 METALS HNO 3,HCL,HF ELECTRONICS HNO 3,HCL,H2O2,HBF4

*2: IF THE RESULT OF SPOT TEST IS POSITIVE, CHROMIUM (VI) WOULD BE DETERMINED AS DETECTED.

***************************************************************************************************************************************************** TO BE CONTINUED

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Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338

TEST REPORT NUMBER: SH AH00334352

TESTS CONDUCTED

PAGE 6 OF 8

2 ( ) Ⅰ Test Result Summary :

Testing Item Result (ppm)

Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND

Remarks: ppm = Parts per million = mg/kg ND = Not detected

(Ⅲ) Test Method:

Testing Item T esting Method R eporting Limit

Halogen Content With reference to EN 14582:2007 by combustion flask with oxygen and determined by ion chromatography 50 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

***************************************************************************************************************************************************** TO BE CONTINUED

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Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338

TEST REPORT NUMBER: SH AH00334352

TESTS CONDUCTED

PAGE 7 OF 8

(Ⅳ) Measurement Flowchart:

Test For Halogen Content Reference Standard: EN 14582

*****************************************************************************************************************************************************

TO BE CONTINUED

add absorbent in a combustion flask & place weighed sample in equipment

fill the combustion flask with oxygen

ignite then leave the flask at room temperature

transfer the absorbent into a volumetric flask

make up with deionized water

sampling/grinding or cutting

analyzed by ion chromatography

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Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338

TEST REPORT NUMBER: SH AH00334352

TESTS CONDUCTED

PAGE 8 OF 8

*****************************************************************************************************************************************************

END OF REPORT

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

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TEST REPORT NUMBER: SH AH00355828

AUTHORIZED BY: FOR INTERTEK TESTING SERVICES LTD., SHANGHAI

JACOB LIN GENERAL MANAGER

PAGE 1 OF 7 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

APPLICANT: LITTELFUSE,INC. DATE: DEC 13, 2012 800 E. NORTHWEST HWY AT TN: A.DIVIETRO/D.UNTIEDT

SAMPLE DESCRIPTION: ONE (1) SUBMITTED SAMPLE SAID TO BE WHITE POWDER. ITEM NAME : FILLER. PART NO. : 090187.

***************************************************************************************************************************************************** TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S) *****************************************************************************************************************************************************

TO BE CONTINUED

Page 72: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

TEST REPORT NUMBER: SH AH00355828

TESTS CONDUCTED

PAGE 2 OF 7 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

1 (Ⅰ) Test Result Summary:

TESTING ITEM R ESULT (ppm)

HEAVY METAL CADMIUM (Cd) CONTENT ND LEAD (Pb) CONTENT ND MERCURY (Hg) CONTENT ND CHROMIUM VI (Cr6+) CONTENT ND POLYBROMINATED BIPHENYLS (PBBs) MONOBROMINATED BIPHENYLS (MonoBB) ND DIBROMINATED BIPHENYLS (DiBB) ND TRIBROMINATED BIPHENYLS (TriBB) ND TETRABROMINATED BIPHENYLS (TetraBB) ND PENTABROMINATED BIPHENYLS (PentaBB) ND HEXABROMINATED BIPHENYLS (HexaBB) ND HEPTABROMINATED BIPHENYLS (HeptaBB) ND OCTABROMINATED BIPHENYLS (OctaBB) ND NONABROMINATED BIPHENYLS (NonaBB) ND DECABROMINATED BIPHENYL (DecaBB) ND POLYBROMINATED DIPHENYL ETHERS (PBDEs) MONOBROMINATED DIPHENYL ETHERS (MonoBDE) ND DIBROMINATED DIPHENYL ETHERS (DiBDE) ND TRIBROMINATED DIPHENYL ETHERS (TriBDE) ND TETRABROMINATED DIPHENYL ETHERS (TetraBDE) ND PENTABROMINATED DIPHENYL ETHERS (PentaBDE) ND HEXABROMINATED DIPHENYL ETHERS (HexaBDE) ND HEPTABROMINATED DIPHENYL ETHERS (HeptaBDE) ND OCTABROMINATED DIPHENYL ETHERS (OctaBDE) ND NONABROMINATED DIPHENYL ETHERS (NonaBDE) ND DECABROMINATED DIPHENYL ETHER (DecaBDE) ND

REMARKS: ppm = PARTS PER MILLION = mg/kg

ND = NOT DETECTED

(Ⅱ) ROHS REQUIREMENT: RESTRICTED SUBSTANCES LIM ITS

CADMIUM (Cd) CONTENT 0.01% (100ppm) LEAD (Pb) CONTENT 0.1% (1000ppm) MERCURY (Hg) CONTENT 0.1% (1000ppm) CHROMIUM VI (Cr6+) CONTENT 0.1% (1000ppm) POLYBROMINATED BIPHENYLS (PBBs) 0.1% (1000ppm) POLYBROMINATED DIPHENYL ETHERS (PBDEs) 0.1% (1000ppm)

THE ABOVE LIMITS WERE QUOTED FROM ROHS DIRECTIVE 2002/95/EC AND AMENDMENT 2005/618/EC FOR HOMOGENEOUS MATERIAL.

***************************************************************************************************************************************************** TO BE CONTINUED

Page 73: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

TEST REPORT NUMBER: SH AH00355828

TESTS CONDUCTED

PAGE 3 OF 7 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

2 (Ⅰ) Test Result Summary:

TESTING ITEM R ESULT (ppm)

HALOGEN CONTENT FLUORINE (F) ND CHLORINE (Cl) ND BROMINE (Br) ND IODINE (I) ND

REMARKS: ppm = PARTS PER MILLION = mg/kg

ND = NOT DETECTED

(Ⅲ) TEST METHOD:

TESTING ITEM T ESTING METHOD REPORTING LIMIT

HALOGEN CONTENT WITH REFERENCE TO EN 14582:2007 BY COMBUSTION FLASK WITH OXYGEN AND DETERMINED BY ION CHROMATOGRAPHY 50 ppm

***************************************************************************************************************************************************** TO BE CONTINUED

Page 74: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

TEST REPORT NUMBER: SH AH00355828

TESTS CONDUCTED

PAGE 4 OF 7 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

(Ⅲ) TEST METHOD:

TESTING ITEM T ESTING METHOD REPORTING LIMIT

CADMIUM (Cd) CONTENT

WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN CLAUSE 8/9/10, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES.

2 ppm

LEAD (Pb) CONTENT

WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN CLAUSE 8/9/10, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES.

2 ppm

MERCURY (Hg) CONTENT WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN CLAUSE 7, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES.

2 ppm

CHROMIUM VI (CR6+) CONTENT

WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN ANNEX C, BY ALKALINE DIGESTION AND DETERMINED BY UV-VIS SPECTROPHOTOMETER.

1 ppm

POLYBROMINATED BIPHENYLS (PBBs)

WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN ANNEX A, BY SOLVENT EXTRACTION AND DETERMINED BY GC-MSD AND FURTHER HPLC CONFIRMATION WHEN NECESSARY.

5 ppm

POLYBROMINATED DIPHENYL ETHERS (PBDEs)

WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN ANNEX A, BY SOLVENT EXTRACTION AND DETERMINED BY GC-MSD AND FURTHER HPLC CONFIRMATION WHEN NECESSARY.

5 ppm

REMARK:REPORTING LIMIT = QUANTITATION LIMIT OF ANALYZE IN SAMPLE

***************************************************************************************************************************************************** TO BE CONTINUED

Page 75: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

TEST REPORT NUMBER: SH AH00355828

TESTS CONDUCTED

PAGE 5 OF 7 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

(Ⅳ) MEASUREMENT FLOWCHART: TEST FOR Cd/ Pb/ Hg/Cr (VI)/ PBBS/PBDES CONTENTS REFERENCE STANDARD: IEC 62321 EDITION 1.0:2008

REMARKS: *1: LIST OF APPROPRIATE ACID: MATERIAL ACID ADDED FOR DIGESTION POLYMERS HNO 3,HCL,HF,H2O2,H3BO3 METALS HNO 3,HCL,HF ELECTRONICS HNO 3,HCL,H2O2,HBF4

*2: IF THE RESULT OF SPOT TEST IS POSITIVE, CHROMIUM (VI) WOULD BE DETERMINED AS DETECTED.

***************************************************************************************************************************************************** TO BE CONTINUED

Sampling/grinding or cutting

Weigh sample and for different material,

digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline

solution

Definite temp. Extraction

Make up with deionized water and add Diphenyl-

carbazide solution

Cr6+

Weigh sample andadd organic

solvent

Soxhlet extractionor

Solvent extraction

Concentrate the extract and make up with organic

solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

Spot test

Get 50cm2 samples

Boiling water extraction

Metal Polymers / electronics

Positive*2

Confirm the tested samples are totally

dissolved

No

Cool and filter the extract

Yes

Page 76: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

TEST REPORT NUMBER: SH AH00355828

TESTS CONDUCTED

PAGE 6 OF 7 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

(Ⅴ) MEASUREMENT FLOWCHART: TEST FOR HALOGEN CONTENT REFERENCE STANDARD: EN 14582

*****************************************************************************************************************************************************

TO BE CONTINUED

Add absorbent in a combustion flask & place weighted sample in equipment

Fill the combustion flask with Oxygen

Ignite then leave the flask at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by Ion Chromatography

Page 77: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

TEST REPORT NUMBER: SH AH00355828

TESTS CONDUCTED

PAGE 7 OF 7 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

*****************************************************************************************************************************************************

END OF REPORT

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Page 78: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

TEST REPORT NUMBER: SH AH00355836

AUTHORIZED BY: FOR INTERTEK TESTING SERVICES LTD., SHANGHAI

JACOB LIN GENERAL MANAGER

PAGE 1 OF 8 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

APPLICANT: LITTELFUSE,INC. DATE: DEC 13, 2012 800 E. NORTHWEST HWY AT TN: A.DIVIETRO/D.UNTIEDT

SAMPLE DESCRIPTION: ONE(1) SUBMITTED SAMPLE SAID TO BE BEIGE POWDER. ITEM NAME : FILLER. PART NO. : 090184. ******************************************************************************************************************************************************

TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)

****************************************************************************************************************************************************** TO BE CONTINUED

Page 79: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

TEST REPORT NUMBER: SH AH00355836

TESTS CONDUCTED

PAGE 2 OF 8 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

1 ( Ⅰ) Test Result Summary:

TESTING ITEM R ESULT (ppm)

HEAVY METAL CADMIUM (Cd) CONTENT ND LEAD (Pb) CONTENT ND MERCURY (Hg) CONTENT ND CHROMIUM VI (Cr6+) CONTENT ND POLYBROMINATED BIPHENYLS (PBBs) MONOBROMINATED BIPHENYLS (MonoBB) ND DIBROMINATED BIPHENYLS (DiBB) ND TRIBROMINATED BIPHENYLS (TriBB) ND TETRABROMINATED BIPHENYLS (TetraBB) ND PENTABROMINATED BIPHENYLS (PentaBB) ND HEXABROMINATED BIPHENYLS (HexaBB) ND HEPTABROMINATED BIPHENYLS (HeptaBB) ND OCTABROMINATED BIPHENYLS (OctaBB) ND NONABROMINATED BIPHENYLS (NonaBB) ND DECABROMINATED BIPHENYL (DecaBB) ND POLYBROMINATED DIPHENYL ETHERS (PBDEs) MONOBROMINATED DIPHENYL ETHERS (MonoBDE) ND DIBROMINATED DIPHENYL ETHERS (DiBDE) ND TRIBROMINATED DIPHENYL ETHERS (TriBDE) ND TETRABROMINATED DIPHENYL ETHERS (TetraBDE) ND PENTABROMINATED DIPHENYL ETHERS (PentaBDE) ND HEXABROMINATED DIPHENYL ETHERS (HexaBDE) ND HEPTABROMINATED DIPHENYL ETHERS (HeptaBDE) ND OCTABROMINATED DIPHENYL ETHERS (OctaBDE) ND NONABROMINATED DIPHENYL ETHERS (NonaBDE) ND DECABROMINATED DIPHENYL ETHER (DecaBDE) ND

REMARKS:ppm = PARTS PER MILLION = mg/kg

ND = NOT DETECTED

RESPONSIBILITY OF CHEMIST: DENT FANG / LEAF LIU (Ⅱ) ROHS REQUIREMENT:

RESTRICTED SUBSTANCES LIM ITS

CADMIUM (Cd) CONTENT 0.01% (100ppm) LEAD (Pb) CONTENT 0.1% (1000ppm) MERCURY (Hg) CONTENT 0.1% (1000ppm) CHROMIUM VI (Cr6+) CONTENT 0.1% (1000ppm) POLYBROMINATED BIPHENYLS (PBBs) 0.1% (1000ppm) POLYBROMINATED DIPHENYL ETHERS (PBDEs) 0.1% (1000ppm)

THE ABOVE LIMITS WERE QUOTED FROM ROHS DIRECTIVE 2002/95/EC AND AMENDMENT 2005/618/EC FOR HOMOGENEOUS MATERIAL.

****************************************************************************************************************************************************** TO BE CONTINUED

Page 80: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

TEST REPORT NUMBER: SH AH00355836

TESTS CONDUCTED

PAGE 3 OF 8 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

(Ⅲ) TEST METHOD:

TESTING ITEM T ESTING METHOD REPORTING LIMIT

CADMIUM (Cd) CONTENT

WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN CLAUSE 8/9/10, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES.

2 ppm

LEAD (Pb) CONTENT

WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN CLAUSE 8/9/10, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES.

2 ppm

MERCURY (Hg) CONTENT WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN CLAUSE 7, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES.

2 ppm

CHROMIUM VI (CR6+) CONTENT

WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN ANNEX C, BY ALKALINE DIGESTION AND DETERMINED BY UV-VIS SPECTROPHOTOMETER.

1 ppm

POLYBROMINATED BIPHENYLS (PBBs)

WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN ANNEX A, BY SOLVENT EXTRACTION AND DETERMINED BY GC-MSD AND FURTHER HPLC CONFIRMATION WHEN NECESSARY.

5 ppm

POLYBROMINATED DIPHENYL ETHERS (PBDEs)

WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN ANNEX A, BY SOLVENT EXTRACTION AND DETERMINED BY GC-MSD AND FURTHER HPLC CONFIRMATION WHEN NECESSARY.

5 ppm

REMARK:REPORTING LIMIT = QUANTITATION LIMIT OF ANALYZE IN SAMPLE

****************************************************************************************************************************************************** TO BE CONTINUED

Page 81: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

TEST REPORT NUMBER: SH AH00355836

TESTS CONDUCTED

PAGE 4 OF 8 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

(Ⅳ) MEASUREMENT FLOWCHART: TEST FOR Cd/ Pb/ Hg/Cr (VI)/ PBBS/PBDES CONTENTS REFERENCE STANDARD: IEC 62321 EDITION 1.0:2008

REMARKS: *1: LIST OF APPROPRIATE ACID: MATERIAL ACID ADDED FOR DIGESTION POLYMERS HNO 3,HCL,HF,H2O2,H3BO3 METALS HNO 3,HCL,HF ELECTRONICS HNO 3,HCL,H2O2,HBF4

*2: IF THE RESULT OF SPOT TEST IS POSITIVE, CHROMIUM (VI) WOULD BE DETERMINED AS DETECTED.

****************************************************************************************************************************************************** TO BE CONTINUED

Sampling/grinding or cutting

Weigh sample and for different material,

digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline

solution

Definite temp. Extraction

Make up with deionized water and add Diphenyl-

carbazide solution

Cr6+

Weigh sample andadd organic

solvent

Soxhlet extractionor

Solvent extraction

Concentrate the extract and make up with organic

solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

Spot test

Get 50cm2 samples

Boiling water extraction

Metal Polymers / electronics

Positive*2

Confirm the tested samples are totally

dissolved

No

Cool and filter the extract

Yes

Page 82: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

TEST REPORT NUMBER: SH AH00355836

TESTS CONDUCTED

PAGE 5 OF 8 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

(Ⅴ) MEASUREMENT FLOWCHART: TEST FOR HALOGEN CONTENT REFERENCE STANDARD: EN 14582

****************************************************************************************************************************************************** TO BE CONTINUED

Add absorbent in a combustion flask & place weighted sample in equipment

Fill the combustion flask with Oxygen

Ignite then leave the flask at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by Ion Chromatography

Page 83: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

TEST REPORT NUMBER: SH AH00355836

TESTS CONDUCTED

PAGE 6 OF 8 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

2 ( ) Ⅰ Test Result Summary :

Testing Item Result (ppm)

Halogen Content Fluorine (F) ND Chlorine (Cl) 100 Bromine (Br) ND Iodine (I) ND

Remarks: ppm = Parts per million = mg/kg N D = Not detected

Responsibility Of Chemist : Grace Wang

(Ⅲ) Test Method:

Testing Item T esting Method R eporting Limit

Halogen Content With reference to EN 14582:2007 by combustion flask with oxygen and determined by ion chromatography 50 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

Date Sample Received : Dec.5, 2012 Testing Period : Dec.5, 2012 To Dec.11, 2012

****************************************************************************************************************************************************** TO BE CONTINUED

Page 84: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

TEST REPORT NUMBER: SH AH00355836

TESTS CONDUCTED

PAGE 7 OF 8 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

(Ⅳ) Measurement Flowchart:

Test For Halogen Content Reference Standard: EN 14582

****************************************************************************************************************************************************** TO BE CONTINUED

add absorbent in a combustion flask & place weighed sample in equipment

fill the combustion flask with oxygen

ignite then leave the flask at room temperature

transfer the absorbent into a volumetric flask

make up with deionized water

sampling/grinding or cutting

analyzed by ion chromatography

Page 85: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

TEST REPORT NUMBER: SH AH00355836

TESTS CONDUCTED

PAGE 8 OF 8 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

******************************************************************************************************************************************************

END OF REPORT This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Page 86: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

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Page 93: ICP Test Report Certification Packet - Littelfuse/media/files/... · nov^ TEST REPORT NO. 4002R12050740-1R02 Daie: May. 09, 2012 T€stino method: I\l1QL IEC 62321:2008, seclion I

Cuslomer: Suzhou FuHong Electronic IndustriatCo., 16.

Addr6s: NO.89 \/ElDU ROAD, WANGTING TOVIN, XTANGCHENG DISTR|CI SUZHOU. CHINARepod on the submltted samrl€ said to be

sample name: Lead wife coppershell

Modol:/

Itefi/Lot Io.: /Matonal:/Buyen/ :S u p p l i e r : / ,

l i lanufacturE:/- . _ - i

- fSample recelved date: Gq _08, 2012 :t*,tn o"n.o, t.. o".;;,,013

"."r.-,.,,613, 1 ,]

&glirs-Bgsccsgq i

As specifed by dienl, to determine the L€ad, Cadrium, l,tercury & tiexayabntChrcmium conle in the 6ubmitted sampte inaccodance with Directive 2OO2I95/EC {RoHS). j

l\OV'BF.F.q,A

TEST REPORTNO.: 4002R121008024-2R02 Oate: Oct.1 0, 2012

Testing ltem Measufing instrument ,MQL

Lead (Pb) IEC 62321:2008. section I rcP-oEs a!gagcadmium (Cd) IEC 62321:2008, s€ction 9 tcP-oEs 2 mg/kg

[,lercury (Hg) IEC 62321r2008, s€ction 7 rcP-oEs 2 mg/kg

Chromium (CrM) IEC 62321: 2008, Annex B 0.02mg/kg*

Testino method:

lsqj 0.02 mg/tg rcturs to the MQL olsample exlraction liquid.

Conclu3ion:-\ryhen tested as specified lhe submilied sample compried with th€ requircments of commission D€cision of 18 Aug 2005

amending Dircctive 2002/95/EC notilied under docum€nt 2005/618/EC.

LiTingting, Maggie

Chemical Test Direclor

Yuan Qi, l,lickey

LabManager

Sign€d ior and on behallol

Shenzhen AOV Testing Technology Co., Ltd, Kunshan 8ran6h

ea"arc"a"r, A?1 W a l b n OrO."*0r44

."*FOR FURTHER DETAILS, PLEASE REFERTOT

Technical Di€clor

STIENZIIEN AOVTE$Tl'{G I€CHI!OLOGY CO,.I.TD,KUNSHAN BRANCI]

(,10",'ll,,u*

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l\ov"BF,?sn

NO.: A0O2R12100802+2R02

T63l Flow:

Cooling the vessel, fiitei washed and

fllled lo the mafK with distilled waler.

Add the digestion solulionj thevess€l is heated until the sample

TEST REPORTDate Oci .10,2012

L To Detemine/lead, Cldmium Content (Metal substrale)lestedbY

L7.^otq,

-*".irl,"*J "r,to,"t|,

Add lhe digestion soluUon, closelhe microwave vessel.

f---- -].-

(Plating)

The sample is digested in the

micrcwave oven tollowing a specinc

deoomposilion progrcm.

Test the sample solulion and ihe 0.02

mg/kg slandard solution by uv-vls.

' H o t l r n e40a 700 8600

Cooling the vessel, frller;washed and

filled to the maft wilh dislilled waler.

Remove lhe sample, and cool

the beak€r lo room temperature,

and do the color reaclion

______-l "*rn nrte,.washedand l_____*p;-r, f;;-1

I rilled lo$e mark with Dlwaler I

ShENZH€N AOV I6STII {G T 'C NOIOGY CO.. ITD.XUNSHAN OEANCH

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/\OV"BF#,HN

NO.i A002R121008024-2R02

Sample Doscripilon:

TEST REPORTOate :Oc l10 2012

5. To Deiermine Hexavalent Chromium Content in colorless and colorcd chromate coaling on metals: (Plating)

r e s t e d b v : l ) ^ ,' L/A^U,4.

5.1 Spotlesl (

f l;"')l;**SN€$ZHEN AOVI :STING T€C NOIOGY CO' ' ITD.XUNSI lAN BBANCI I

lf the lest result is posiiive,

ihe sample is considered lo

have hexavalenl chromium

Place 1-5

and the 0.02 mg/kg

Boiling- water- extracton

procedurc shall be us€d tolf the test reslrlt

lltherc is intederence or it is had to decide

whetherlhe sample have the hexavalent

5.2 Boilin9- water- enractronRemove the sample, and cool

the beaker to rcom temperalu€,

and do the color rcaolion

Take the (50i5)cm2

sample in the beaker.Heat 50 ml ol Dl waler in the

beak€r to boiling lof 10 min

Code Sample Desc{iplion Code

copper shell subslfate

Lead wire Plating 24 Copper shell Platng

Unit RoHS Limit Result

2-3

Lead {Pb) mg/l(g 1000 N.D. N.D. N.D. N.O

Cadmium (Cd) mg/k9 100 N.D. N.D. N.D, N.D.

Meroury (Hg) mg/kg 1000 N.D. N.D. N.D, N D .

Chromum (Crl'I) mg/K9 1000 Negalive Negalrve Negaliv€ Negative

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TEST REPORToare: oct.10,2012

-:fh€ new RoHS di€ctive 2011/65/EU, on Jul. 21,2011 come inlo force, on Jan. 03, 2013 ths formal implementation, Direcliv€

200295/EC ahall be repeal€d simultaneously-

Sp€cimens, which ggqeted to d€temine Lead, Cadmium and Mercury conient have been dissolved completelv.

NO.: A0O2R12100802+2R02

-mg/Kg=ppm

--The iest is bas€d on the following

ce of C_rl\,I)lif"veiry/y6hetp ttef.limere sr{.q!.be/rurTr v ii'iffyiT-''

*'q:*lhe spot test result is uncertain or

each pad is unifom. The tesl rcsult

maybe cannot stand for the physical truth-Photo is included

Lead wir€ copper shell

"'End of Repod""

sHEI\tZH:ir AOVrlsrr'tc IECNl'lO!OeY CO.,ITD KUNSHAN SRANCIi

r.r i35.1J:55i0eo0o Fd.3F1t?55roEr$ hrr ,w.d{.di' Fodrdo 1r.r00/ , Hot l rne

I , 400 700 8600