icp test report certification packet/media/electronics_technical/icp_test_reports/fuses/...directive...

1

ICP Test Report Certification Packet

Company name : Littelfuse, Inc. Product Series: 5x20 Fuse Product #: 477P Issue Date: October 15, 2012 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (2011/65/EU – recast of EU Directive 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components.

Issued by:

<Global EHS Engineer>

(1) Parts, sub-materials and unit parts This document covers the 477P Fuse RoHS-Compliant series products manufactured by Littelfuse, Inc. ＜ Raw Materials Used

Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1

Remarks：.

Form 585-047 Rev. A 2/21/06

2

Table 1: List of Raw Materials covered by this report

Total Parts Raw Material Part

Number Raw Material Description Page(s) 1 C910510/ C910541 Cap base & plating 3-6 2 C610 (909532/909-499) Body Ceramic tube 7-30 3 DRAGxxx Silver Plated Wires 31-35 4 687xxx-001 Wire – Tin Silver Plated Copper wire 36-41 5 004xxx Wire - Copper Clad CuNi44 Sn 40% 42-48 6 11-0010 Wire - Ag1000 49-55 7 11-0595 Wire - Cu99.9MSn 56-62

8 YTW206

(C692527- 692529) Solder 63-67

9 YTW102

(692539-002) Solder 68-72 10 311.7374.5000 Filler (Cornsilk Sand) 73-81 11 EP308 (087355) Glue 82-93 12 648901 Yarn 94-102

13 C030204/ 934-077/ 934-071/ 934-078 Overcap - Cap Base & Plating 102-106

14 C030204/ 934-077/ 934-071/ 934-078 Overcap - Wire Base & Palting 102-106

nov'TEST REPORT

NO.jA002E11121307'1R02 DaG:Dec.t5,2Oi1 page 1 of4Custom6i Suzhou FuHong Eteclronic IndustialCo., L6.AddT€sg: NO.89 WEIDU ROAD, WANGTINGTOWN. XIANGCHENG oIsTRIcT. sUzHoU. CHINAReport on tie subnitied samptes.id to beSample name: Copper shellModsl: /

Materlal: /D€cripiion: /Buyer: /Supplier: /

SamPle rcceiwd date: Elec.'13,2011T€dng poriod: From Dec.13,2011 lo Dec.15,2o.l1

T€lino Reou6tedAs sp€cified by client, to detemine the L€ad, Cadmium, Mercury & Hexavat€nt Chromilm content an the slbmified sampte inaccordance wilh Dircctive 200295/EC (RoHS).

Te.Uno method:

T€sling liem Measuring instrument MQL

Lead (Pb) IEC 62321:2008, section I rcP-oEs 2mg/kgcadmium (cd) IEC 62321:20t,3, s€clion 9 tcPoEs 2 mg/kgllercury (Hg) IEC 62321:2008, section 7 lcPoEs 2 mg/kg

Chromrum (Cr l'1) IEC 62321:2008, Annex B 0 o2mgkg'

---FOR FURTHER DETAILS, PLEASE REFERTOTHE FOLLOWNG PAGE(ST**'

leg-' 0.02 mg/kg reGrc lo the MQL of sampte extraction tiquid.

99!9!cis!i-When tesled as specined the submi(ed sample compli€d wilh the rcquirements of commission Decision of 18 Aug 2005amending Directive 2002/95/EC notilied undef document 2005/618/EC.

Pro,ect Leader /{bjA-L(Engine€r) J 4

lnsoected bv

,**'*''*,n-, [,[rlg-,i ti-Y\

,ffi:::j:,,44

SHENZHEnl AOVTESTINC TECHNO!OGY CO..L.TD,KUI\ISIIAI\I BRANCIi Holline86.512.5510 8000

nov.NO,: A002E11121307-1 R02

TEST REPORT

Tesled by ICP-OES

Add the digestion sotutioni thevessel is healed until the sampl€has b€€n dissolved

Weigh the sample into

F*_-l-Content (Melal substEle)

Add the digeslion solutjon, ctose

the micfowave ves:€|.

F;;1.-and l\Iercury Content (Plaling)

To Detenn exavalenl Chromium Content (bojting- wateF extraction): (Metat substrate)

The sample is digesred in the

mrcrowave oven iollowing a sp€citic

decomposilion program.

Tesl lh€ s€mple solution and the 0.02mg/kg standard solution by UV-VIS.

Hotline86-512-5510 8000

To

+Cooling the vessel, fltet washed and

filled to the ma* with distilled wat€r.

Remove the sample, and coolthe beaker to room lemperature,and do the color leadion

sample in the beaker.Heat 50 mL of Dl waler in the

beaker to boiling ior 10 min

To Delemine

___+l coorins. rirtei washed and lilled l_-_----|l resteo oy l+fl_*l

I t o t he ma*w i th D twa te r .

I l r n " r ,u rn "n , I l " * ' I

SHENZHsN AOV TG6TING ICCHITOI"OGY CO.,L'O.KUNAHAN BRANCH a

nov'NO.i 4002E11121307-rR02

5. To O€temine Hexavalent Chromium

,':"j":::i v^02

Place 1-5

TEST REPORToste:oec15,2011

Contentin colorless and cotorcd cnromaE coating on metats(Plaljng)

5 2 Eoiling- wat6F extraction

Tako the (50+5) cm'?

sample in the beaker.

S!IENZHEN AOV'CSTING IECIINOIOGY CO..ITD,KUNSHAN gNANCH Hotlinea6-512-5510 8000

lf the tesl rcsult is posilive,

the sample is considercd tohave hexavalenl chromilm

Compare the

and lhe 0.02 mg/(qstanda.d solution

Eoiling- wateF ext€ctjonprccedurc shall be used to

lfthere is int€rference or it is hard to decide whetherthe sampl€ have tie h€xavatent chromium

Remove tie sample, and cool

lhe beaksr to room tempeEture,

and do the color reaolion

Heat 50 mlof Dlwaier in the

beaker lo boiling for 10 min

Test the sample solution and the 0.02mg/kg standard solution by UV,VIS.

T€t Re6ult3:

Unit RoHS

Limil

Result

Substrate Plating'

Lead (Pb) mg/Kg 1000 N.O. N.O.Cadmium (cd) mg/Kg 100 N.D, N.D.lvercury (Hg) mgn(]s 1000 N.D. N.D.

chromium (Crl'I) mg/Kg 1000 Negalive Negative

nov-TEST REPORT

NO 4002E11121307.rR02

'The new RoHS directive 201 1/65/EU, on Jul. 21 , 201 1 come into lorce on Jan. 03, 20 1 3 the fomat imptementation. Direclive2002,95/EC shall be rcpeated simuttaneousty.

-specimens, which requested to determine Lead, cadmium and l,rercury conteni, have been dissorved comprererv

-N.D.=not detected(<tltoL)-MOL=ntethod Ouantitation Limit-Negative=Absence of Cr (VIir

PositivF Presence ofCr (\ll)i

Unc€rlain= can not verify whetlerthe sampte have Hexavatent Chromium by spoltest.(The test€d sample should be fufthet verified by boiling-waler-€nraction method if the spot test resutt |s uncertain ornegalive. )

-'The tesl is based on lhe following assumption:The sampte ptating is a singte tayefand each paft is uniform. The tesr resuttmaybe cannotsland br lhe physicaltruth ofsampte ptating.

Photograph ofSample

Coppershell

SHENZHEN AOVT€STING TECHNOLOGYCO.,IID,XUNSHAN ARANCTI e!:-"Jllls,.**

Validi ownFor QPlease SGS

tll||Ill ltltt]r

Test Report No. : CE/2012I14843A Dare .2O12J02104 Pagel.1o124

CERAIVTEC GIVBHMULTIFUNCTIONAL CERAI/IICS LUITPOLDSTMSSE 15 D.91207 LAUF, GERMANY

The following sample(s) was/u,€re submiltsd and identified by/on behalf of the client as:

Sample DescriptionStle/ltem No.Sample Receiving DateTesting Perjod

Te3t Re.ult(s)

Conclu6ion

CERAMICc6102012,01t30201 2J 01 | 30 T O 201 Z 02t 04

: Please refer lo next page(s).

: Bas€d on the performed tests on submitted samples, the test results of Cadmium, Lead,lvlercury, Hexavalent Ch.omium Cf(Vl), PBBS and PBDES comply with the limit6 as set byRoHS Direclive 2011/65/EU Annex ll; recasting 200295/EC.

Sg|rad for||d

Cltorlcd Lborlbry- T.Fd

comDafrAil B6;RE ,tRd-LXlAllHll lftlCt !IAIA| "SFiAE lq"1 )19{Th3dodm6dE6ebyfuconMy&bjedbi6Gengg|cddfooi3ds.s6pii6oveis43Eisb.on4wd

t'lnld d6 kru6 doinod droE i Ady ho der ot hB tuhed aadrsd tui i'noih6 r ft or rts iftmton mt and

"ih f sr rrE comp.nr'E E r.rspombrl'

comFry Atu sadoEs . rodon torcsry or rslff€ton d rhe 6ibd or sD nd ofl.id.6 m.y e p,@dk ro s. rd

.*n, ;S-:HJ'Y I iH::::gj;t.*t;:,$;; '-;*,t^-- "

r !6!a {Brts

***'*

Test ReportCERAI\,ITEC GMBHMULTIFUNCTIOML CERAITIICS

No.: CEJ2012/14843A Dale | 201Z0ZM Page:

LUITPOLDSTMSSE 15 D.91207 LAUF, GERIJANY

2 o f 2 4

t]r||lrrfl||fllllt

IeclBecc$GL

PART NAME No.l

Test ltem(s) lJnit Method MDLR€ult Limitl{o.t

Cadmium (Cd) mS/kS With reference to IEC 62321:2008 andperfomed by ICP-AES.

2 n,o, 100

Lead (Pb) mg/Kg With reference to IEC 62321:2008 andperformed by ICP-AES.

2 178 1000

lrercury (Hg) mg&g With reference to IEC 62321: 2008 andperformed by ICP-AES.

2 n.o. 1000

Hexavalent Chromium Cr(Vl) mgikg With reference to IEC 62321: 2008 andpedormed by UV-VIS.

2 n.d. 1000

Polychlorinated Biphenyls (PCBS)(cAS No.: 1336-3G3)

mgikg With reference to US EPA 3g0Cmethod. Analysis was performed byGC/rrs.

0.5 n.d.

Polychlodnated Terphenyls(PCTs)

mS/kS With feference to US EPA 3540Cmethod. Analysis was pedormed byGC/MS.

0.5 n.d.

Polychlofi nated Naphthalene(PCNs)

mg/Kg With reference to uS EPA 3540Cmethod. Analysis was performed byGC/|VS.

5 n.d.

Alkanes, C1Gl3, chloro (ShoftChain Chlodnated Paraffins) (CASNo.:8553t0a-8)

oa With referenc€ to US EPA 3540Cmethod. Analysis was performed byGC/MS.

0 . 0 1 n.d.

Pe|f luoroodane sulf onates(PFOS-Acid, Metal Salt, Amide)

mgKs With reference to US EPA 3540C:1 996 method for PFOS Content.Analysis was performed by LC/MS.

1 0 n.d.

PFOA (CAS No.: 335{7-1) m9Kg With reference to US EPA 3540C:1 996 method for PFOA Cont€nt.Analysis was performed by LC/MS-

1 0

Formaldehyde (CAS No.: 50{0-0) mg/kg With reference to ISO 17226-11200$.Analysis was perfomed by HPLC/DAD.

3 n.d.

Analysis was performed by FTIR andFLAME Test.

Negative

I WHITE CERAIVIC

cmEm6, REes t hE lE ie l i f i d i z l i Lbq .6 f i - { s6 - " ! . ? - " q r ' i E r , ] t&fttrerdEE$dbyTconp'

I ohF d r.rr'r, 'n&nre'r a{r]'d'do1's.! e -.d w's'1 ary -016' d dBderuddad!e hr .

tan*don ft6 a.B no ai h.r dod oodn.da Ti e oo@nofl @nd F sdcomEry ary un&ibai srbEr on bM or i'iB relon d b6 onbnr d.F

alnnr+nuunar-iI arapdciiv'rawd/firtd'rirr**Hmn:fiE G

q

Test Report No.:CE/2012I14843A D e:2012102104 Page: 3 of 24

CERAITTEC GltlBHMULTIFUNCTIONAL CERAI\/IICS LUITPOLDSTRASSE 15 D.91207 LAUF, GERMANY

|l]|||tllllll llll

Test ltem(s) Unit Melhod MDLResult LimltNo. l

BBP (Benzyl butyl phthalate) (CASNo-:85-68-7)

% With reference to EN 14372. Analygswas performed by GC/lVlS.

0.003 n.d.

DEHP (Di- (2-€thylhexyl)phthalate) (CAS No.: 1'17-81-7)

% With rofefence to EN 14372. AnalysiswBs pedormed by GC/lVlS.

0.003 n.d.

DIDP (Di-isodecyl phthalate) (CASNo.:26761-40-0)

oa With reference to EN 1 4372. AnalysiswBs pedormed by GC/IVS.

0.01 n.d.

DINP (Di-isononyl phthalate) (CASNo.:2855312-0)

With reference to EN 14372. Analysisrvas performed by GC/MS.

0.01 n.d.

DNOP (Di-n-ociyl phthalate) (CASNo.: 117"84-0)

With reference to EN 14372. Analysiswas perlomed by GC/MS.

0.003 n.d.

DBP (Dibutyl phthalate) (CAS No.:u-74-2)

y'Vith reference to EN 14372. Analysis/vas perfomed by GC/MS-

0.003 n.o.

l\Ionomethyl dibromodiphenylmethane (DBBT)

mg/Kg With reference to US EPA 8270Dmethod. Analysis was performed byGo/tlls.

0.5 n.d.

l\ronomethyl dichlorodiphenylmethane (Ugilec121)

mgikg With refefence to US EPA 8270Dmethod. Analysis w€s perfomed byGC/ttIS.

0.5 n.d.

Monomethyl tetrachlorodiphenylmethane (Ugilecl41)

mgikg With refefence to US EPA 8270Dmethod. Analysis w6s pefomed byGo/tlls.

0.5 n.d.

Organic-tin compoundsIributyl Tin (TBT) mgikg With refefence to DIN 38407-13.

Analysis was performed by GC/FPD.0.03 n-d.

Iriphenyl Tin (TphT) mgKs With reference to DIN 3840713.Analysis wEs performed by GC/FPD.

0.03 n.d.

HalonsHalon-12'11 (CAS No.: 353-59-3) mg/Kg with reference to US EPA 5021

melhod. Analysis was performed byGC/MS.

n.d.

Halon-13o1 (CAS No.: 75-63-8) mg/Kg With reference to US EPA 502 1method- Analysis was pertormed byGc/tlls.

Halon-2402 (CAS No.: 124-73-2) mg^g with refercnce to us EPA 5021method. Analysis was pedormed byGC/tis.

n.d.

redu€d..sdntur wLhdl rior k6 pomE! on d t6comEfr [}l l B E$3! nE-L1l{91:!l:dzttf la E l Hd- lH4 - l*lEii9 E i "I f, I ft{.

a3 ndmsa ! 6_sd 4 bs 'mEn

i-*f,r <Bd4€ h.rr !.r dd* d tE oodafl ;Bousd r.r 'dob r d or ib 'ftiwdo1 oits so {rhi'dnffioi tum ssEsm aii,ff i ' nohbaiodcrm! -ne b6rtuedoricomp.ny er mr6od& a radoi ta.ry o, tal6h6doi d rb 6ibd or s

a hrF. r Lbai /iurfi#JtE*$6nd4sct

Test Report No. : CE/2012/14843A Dale :2012102104 Pege : 4 d 24

CERAIVTEC GIVBHMULTIFUNCTIONAL CERAI\/IICS LUITPOLDSTRASSE 15 D-91207 LAUF, GERMANY

rt|| tt]l l]l

Test ltem(s) Unit Method MDLResult LimltNo. l

Halog€nHalogen-Fluorine (F) (CAS No.:14762-94-a)

mg/kS with ref€renc€ to BS EN 14582:2007-Analysis was performed by lC.

50

Halosen-chlorine (cl) (cAs No.:22537-15-1)

mS/kS With reference to BS EN 14582:2007.Analysis was performed by lc.

50 n.d.

Halogen-Bromine (Br) (CAS No.:10097-32-2)

mgKs With reference to BS EN 1 4582:2007.Analysis was pedormed by lC.

50 n,d.

Halogen-lodine (l) (CAS No.:14 24+81

mgKs r'Vith reference to BS EN 14582:2007.qnalysis was performed by lC.

50 n.o.

A3b€Bto3Aclinolite ICAS No.: 77536-664) With reference to EPA 600/R-93/116

method. Analysis was performed bySM, PLM and XRD.

Negatave

Amosite (CAS No.: 12172-73-5) % With reference to EPA 600/R-93/1 1 6method. Analysis was performed bySM, PLM and XRD.

Negative

Anthophyllite (CAS No.: 77536-67-5)

with refeence to EPA 600/R-93/1 1 6method. Analysis wEs performed byS[4, PL[4 and XRD.

Negative

Chry6otile (CAS No.: 12001-29-5) % With reference to EPA 600/R'93/116method. Analysis was performed byS[,], PL[,] and XRD.

Negative

Crocidolite (CAS No.: 12001-284) % With reference to EPA 600/R-93/116method. Analysis $ras pedormed bySM, PL[,] and XRD.

Negative

Tremolite {CAS No.: 7753&686) % With reference to EPA 600/R-93/116method. Analysis wEs perfomed bySNl, PLNI and XRD.

Negative

comD.fr KJ AF.fl8n d H:8Rl{6,! ^i-ttlg( t E-{R l_" rE/r: l"rJ n E{.M € ' r b q o d . a l ' . € . b . d 1 q u

'miirnon or I rii ly. knnnfr€ron end inld cds r$u6 dornd 6eF n Ad ho der or his dodmd tded that intod.lftdi! ' ft i@lonf|rad#iFnldonbm.^esnoaida' ndtr and od'G.tr3 ida, bs.6ieddi.mFry a1 ruuroda-d a Fdoi,o$ry o.Elserol d rhs @-6a o' I

effinr+Irror/rs|laa | ' q!!g1ryr!:: ! li ll!'l5!:l?! Nq rdF c ! r'E{ / rirlrnsirL**FErn}t'n%

Test Report No. : cE/2012/14843A Date-2o1zo2to4 Pase:5of 24

CEMMTEC GMBHI\4ULTIFUNCTIONAL CEMMICS LUITPOLDSTMSSE 15 D.gl207 LAUF, GERMANY

|ll |llt llllll

Test liem(s) Unit lllethod MDLR€sult

LimitNo.{

Sum of PBBs

mg/KgWith reference to IEC 6232112008 andperfofined by GC/MS.

n.d. 1000Monobromobiphenyl 5 n.d.Dibromobiphenyl n.d.Tribromobiphenyl 5 n.d.Tetrabromobiphenyl 5 n.d.Pentabromobiphenyl 5 n.d.Hexabromobiphenyl 5 n.d.Heptabromobiphenyl 5 n.d.Oclabromobiphenyl 5 n.d.Nonabromobiphenyl 5 n-d.

Decabromobiphenyl 5 n.d.

Sum of PBDE3'1000

Monobromodiphenyl ether 5 n.d.

Dibromodiphenyl ether 5 n,o,Tribromodiphenyl ether 5 n.d.

Tetrabromodiphenyl ether 5 n.d.

Pentabromodiphenyl ether 5 n.d.

Hexabromodiphenyl ether 5 n.d.

Heptabromodiphenyl ether 5 n.o.Octabromodiphenyl ether 5 n.d.

Nonabrcmodiphenyl ether 5 n.d.

Decabrcmodiphenyl ether 5 n.d.

AZO1): 4AIIINODIPHENYL (CAS No.l92-67-1)

mg/kg With reference to LFGB 82.02-2.Analysis was p€rfomed by GC/MS.

3 n.d.

2)i BENZIDINE (CAS No.: 92-87-5)

m9/K9 With reference to LFGB 82.02-2.Analysis was performed by GC/lvlS.

3

3): +CHLORO-O-TOLUIDINE(CAS No.:95692)

mg/Kg /Vith reference to LFGB 82.02-2.Analysis was performed by GC/MS.

3 n.d.

4): 2-MPHTHYLAIIINE (CASNo.:91-59-8)

msftg with reference to LFGB 82.02-2.Analysis was perfo.med by GC/l/lS.

3 n.d.

5): O-AIVINOMOToLUENE (CASNo.:97-5&3)

mg/kg with reference to LFGB 82.02-2.Analysis \ /as performed by GC/MS.

3 n.d,

a; ; ; ;h i r tErca D i ' - t+4r { .4 -6HEc (4d- r8 . . " . : ' - } ro r ) r l&"i n h e l ! l E I . ' * i . d * d . d n o ' - * " " d . " * * d c o t u r d ; s - 6 { 0 ' ' e s b 6 d * w 4 3 @ n | f ! - ! j ' d g l d g : : l lirii6iim-"j"in-inii*ij ' i i i lb''bnF.''. '[email protected]|fma.Doi!as1g{ws!sods4€i!g

]ii;;'6iifoidhnic!!aidiiirnidoili$@dmdMdn:ii;h;bl's];di{'md,i'ddmdii , i i , l i n d r , n i i " e - - - r * " " . i bs I n ! d c . a .n6 rc r ; i i i 6 cFa f , do .o ! * r cdd6 .dd;1;; ,;" ;-o d, r*' "qtu ro d, odotu Ln6 h. t'nsdoi ooer.ma ni s [email protected] @nr b' €.o.oan, ay ..arho-a ,! s d- baea d b 3'* * d ' r d;;:;;;';;;;l; doan"i4,"; ad a.o ot

Test Report No. ICE/2012114843A Daie:2O1Z0ZO4 Paoe:6 ot 24

CERAIVTEC GITIBHMULTIFUNCTIOML CERAIIIICS LUITPOLDSTMSSE 15 D-91207 LAUF, GERIVANY

tl]tI|tt ||ttll!t

Test ltem(s) Unit Method MDLResult

LimitNo.1

6)i 2'AMINO-4-NITROTOLUENE(CAS No.:99-55.8)

mgftg With refercnce to LFGB 82.02-2.Analysis was performed by GC/MS.

3

7): P-CHLOROANILINE (CAS No.:10647-8)

mdks With reference to LFGB 82.02-2.Analysis w€s perfomed by GC/lVlS.

3 n.d.

8): 2,4-DIAMINOANISOLE (cASNo.: 615-05-4)

m9Kg With reference to LFGB 82.02-2.Analysis was p€rformed by GC/|\IS.

3 n-d.

9): 4,4LDIAIIIINODIPHENYLMETHANE(CAS No.: 101-77-9)

mg/Kg With reference to LFGB 82.02-2.Analysis was performed by GC/I\IS.

3 n.d.

10)r 3,3'-DICHLOROBENZIDINE(CAS No.:91-9+1)

mg/kS With reference to LFGB 82.02-2.Analysis was performed by GC/MS.

3 n.d.

1 1): 3,3'-DIMETHOX/BENZIDINE(CAS No.: 11990-4)

mgikg With relerence to LFGB 82.02-2.Analysis \ /as performed by GC/MS.

3 n,o,

12): 3,3!DIMETHYLBENZIDINE(CAS No.: 11993-7)

mg/kg With reference to LFGB 82.02-2.Analy6is was perfomed by GC/MS.

3 n.o.

'| 3): 3,3-DlMETl-lYL-4,4'-DIAMINODIPHEI.IYLIIIETHANE(CAS No.: 838-8&0)

msfts With reference to LFGB 82.02-2.Analysis was pertormed by GC/lVlS.

3 n.d.

14): P-CRESIDINE (2]!IETHOXY-5-METHYLANILINE) (CAS No.:120-71-8)

mg/Kg A/ith reference to LFGB 82.02-2.Analysis was pedomed by GC/l\Is.

3 n.d.

15): 4,4'-[,IETHYLENE-BIS- (2-CHLOROANILINE) (CAS No.:101-14-4)

mg&g With reference to LFGB 82.02-2.Analysis was performed by GC/MS.

3 n.d.

16): 4,4LOXYDIANILINE (CASNo.:101-80-4)

mgftg With rcfercnce to LFGB 82.02-2.Analysis was performed by GC/MS-

3 n.d.

17): 4,4'-THIODIANILINE (CASNo.: 13965-1)

mgKg With reference to LFGB 82.02-2.Analysis was performed by Gc/lvls.

3 n.d.

18): O-TOLUIDINE (CAS No.: 9$5s)

mg/Kg With reference to LFGB 82.02-2.Analysis was perfomed by GC/IVS.

3 n.d.

19): 2,4-TOLUYLENEDIAMINE(CAS No.:95-80-7)

mg/kg With .eference to LFGB 82.02-2.Analysis was perfonned by GC/MS.

3 n.d.

20): 2,4,5-TRIItIETHYLANILINE(CAS No.: 137-17-7)

mg/Kg With reference to LFGB 82.02-2.Analysis was perfomed by GC/lVlS.

3 n.d.

2'l): O-ANISIDINE (CAs No.: 9G04-0)

mg/kg y]/ith .eference to LFGB 82.02-2.Analysis was performed by GC/MS.

3 n,d.

inALF,{rr!-i-Eeaa tdd- iMt, lg6"+_I T lil:' u?fi;6d,n;dB;;;'iti;@ind]li'ibd.o'i..fgeicsdnf.,*rn6qrbilode,'6|.d.o'Gqused io,asdtr'ctud6.r.n! *tidri,Tds.{cdmiomb-6d;i;bn;]ni'i;;.ii 'nd6'ilnijii 'nd;fusd.mn60DDnAilhdde.dFEoodnaa''.oIsdF,''fths m' d tr! 'nbii$ron 6k and *'rin h 'redlrsrtr -mdor ary -€conFnvt{ts@o13b"t' d3rcE 1.p.n6-bs

adb . cpdLdd rcp l | 1 t r |ii;i'inil;lii;dn;;a;G;;;1iiiriiry Jiii'i''neton a L* ontoni;ii,pp*Eme t 'h s [email protected] k mrdd sna or*dare mai bo prcedd !t ea tu

r$JrLfi*l[**l!6tfiflffi*tr];i1ira&eD6ri^;i I iiij;j;;:;;;t 'l;idD;;;t i;;J;

Test Report No. : CE/2012/14843A Dele : 201210204 Page | 7 of 24

CERAMTEC GI/lBHI\4ULTIFUNCTIONAL CERAMICS LUITPOLDSTRASSE 15 D.91207 LAUF, GERMANY

l]|||lll ll llll

T€st ltem(s) unit Method MDLReBult LimltNo.1

22): P-A[,IINOAZOBENZENE(CAS No.:60-09-3)

msfts With reference to LFGB 82.02-2.Analysis was performed by GC/lVlS.

3 n.d.

23): 2,4-XYLIDINE (CAS No.: 9$68-1)

mg/Kg /Vith reference to LFGB 82-02-2.Analysis was p€rformed by GC/MS.

3 n.d,

24): 2,6-XYLIDINE (CAS No.: 87-62-n

mdks With ref€rence to LFGB 82.02-2.Analysis was performed by GC/MS.

3

CFC's (Chlorofluorocarbons)Group IChlorof luorccabonl 1 (CAS No.:75-694)

mg/kg With reference to US EPA 502 1method. Analysis was performed byGC/MS,

Chlorof luorocarbon-12 (CAS No. :7171-8)

mg/Kg Wth reference to US EPA 5021method. Analysis was performed byGc/rlls.

n.d.

Chlorofluorocalbonl 13 (CAS No.:76-13-1)

MEKg with reference to uS EPA 5021method. Analysis was performed byGCi MS.

n.d.

Chlorof luoroca|bon-1 14 (CAS No.:76-14-2)

mgikg With reference to US EPA 502'1method. Analysis was pedormed bYGC/MS.

'| n.d.

Chlorofluorocarbon- 1 1 5 (CAS No.:7&'ts-3)

mg/Kg With reference to Us EPA 5021method. Analysis was Pertormed bY6C/MS.

1 n.d.

Group lllChlorof luorocarbon-l 3 (CAS No.:7U72-9)

mg/kg With .eference to US EPA 5021method. Analysis was performed bYGC/MS.

1 n.d.

Chlorofluorocarbon-1 I 1 (CAS No.:354-56-3)

m9Kg with reference to us EPA 5021method. Analysis vras performed byGC/|\,IS.

1 n.d.

Chlorofl uoroca6on-1 1 2 (CAS No.:7B-12-0)

mgKg With reference to IJS EPA 5021mehod. Analysis \o?s perfomed bYGC/tVlS.

1 n.d.

Chlorofluorocarbon-2l 1 (CAS No.422-784)

mg/kg Wilh feference to US EPA 5021method. Analysis was Performed bYGC/t\4S.

n,o.

;:li";iy*T B#; rftETtisi4u "f::Fri YisfPlT r5!E?;':r" ?':;'il*'Tl" il]lli*:::]]:il :"*'"-**-'"-"-"ffffi**;"lu*:ffir*"ieB,:.mr""*r*:[''*'inmv""r*irf#ilfi€sitr;:t$ijii"{s#xpa# ?ilrl",il

" "* ,c- ** .s 's*-" ' f rv-

i i ' i i innni i i l i iwt i t i " * r r - "*o: ' r * l ' "aL ' " r , * r . " - . i i ' ' i ' ; ; t ;dn. ! .€dsdro|dt rbt . . . u , g . . * " ' ' o ' r . r ' g . ; ; 6 ; ; dn ' " d * rgd * " ' b . 6

i;6;;:!,;uft d; r;,oi'" s",r "

ri'tdo' a * -'.j;:;;;;; r;;;"n;;id'ialia oird* ra b p6eo*d 6 n'

4riiFiciv,r TrtiJLinSl[&*6EE st!fi

Test Report No.: CE/201214843A Dale:2o1Z0AU Page: 8 or 24

CERAMTEC GIVBHItIULTIFUNCTIONAL CERAlrlcS LUITPOLDSTMSSE 't 5 D-91207 LAUF, GERMANY

l:] lrn tllllll

Test ltem(6) Unit ll/lethod MDLResult LimitNo. l

Chlorof luoroca6on-212 (CAS No. :3182- -1)

mdks With reference to uS EPA 5021method. Analysis was perfomed byGC/MS.

n,d,

Chlorof luorocarbon-21 3 (CAS No.:235,L0e5)

mg/Kg With reference to US EPA 5021method- Analysis was performed byGC/ttIS.

n.d.

Chlorofl uorocarbon-2'l4 (CAS No.:292sr31-0)

mgKg With reference to uS EPA 5021method. Analysis was performed byGC/MS.

n.d.

Chlorof luorocarbon-2l 5 (CAS No.:425943-2)

mgikg With reference to L,S EPA 502'lmethod. Analysis was pedormed bYGC/MS.

Chlorof luorocarbon-21 6 (CAS No.:661-97-2)

mg/Kg With reference to uS EPA 5021method. Analysis was p€rformed byGC/l\rs.

1 n.d.

Chlorofl uorocarbon-21 7 (CAS No.:422-86-6)

mgKs With reference to uS EPA 5021method. Analysis was perfomed byGC/MS.

1 n.d.

CHCa (Chlorinale hydroca.bon)1,1,1,2-Tetrachloro€thane (CASNo.r630-20-6)

mgKg With feference to uS EPA 5021method. Analysis wEs performed byGC/t\4S.

1 n.d.

1,1,1-Trichloro€thane (CAS No.:71-556)

mdks With refeence to US EPA 502 1method. Analysis was performed bYGC/MS,

1 n,o,

1 ,1 ,2,2-Tetrachloroethane (CASNo.: 79-3+5)

mg'ks with reference to us EPA 5021method. Analysis was pedormed bYGC/MS.

1 n.d.

1, 1,2-Trichlorcethane (CAS No. :7900-5)

mg/kg With reference to US EPA 5021method. Analysis was perfomed bYGC/MS.

1 n.d.

1 ,1-Diclloroethane (CAS No.:75-s+3)

mg/Kg With reference to US EPA 5021method. Analysis was Performed bYGC/|VS.

n.d.

1 ,1-Dichloroethene (CAS No.:75-3s)

mg/Kg With reference to IJS EPA 5021method. Analysis was Performed bYGC/|VS.

8"*affirli;sff r': !t'i?+riFs.t'li::E?'"iri:'13i: ?.gT+:ex;1:FdT6l.f ib::T::a:":1: ::,T" " "" *- *"*'*

r *bFbGq€E .mor r ;d t i'#.?n"i*inni#noi*i*t*b]66d'.tcodm!b,Ei.:i;;'d;;;6iw4.;'.''nil"i].i,i.ii"ni.ii'i.ini"ii'i&tona"ai"d@,$6dd"*b.1";.;;;;;b';mda'1'''e"9dFai-

i"i =n: j;nryt *r q-'r"r '

","0 ""'g*"o -"''-.*d;'a"'"j'iJ r"a"'#te-a *'pd'dsod n tr' do' oM r

r"' ", ". -'"'..' -.. ru;p"i":,il iir n'i;;; ;:'laa *6 n'@s rui € d@dd 't tra ikd 'asr db' &

drr F cehwd/ijll txirrc+Ffi f fi ki*

Test Report No. : CE/201214843A Date:2012,0i,M Paqe:9of24

CERAIVTEC GIlIBHMULTIFUNCTIONAL CERAIVICS LUITPOLDSTMSSE 15 D-91207 LAUF, GERMANY

rrrfirnl|| :]l

Test ltem(s) Unit ilethod MOLResult LimitNo.l

1 ,1-Dichloropropene (CAS No.:563-5&6)

mg/kg With reference to US EPA 5021method. Analysis was performed byGC/MS,

n.o.

'1,2,3-Tridlloropropane (CAS No.:961 8-4)

MEKq Wiih reference to uS EPA 5021method. Analysis was perfomed byGC/MS.

n.d.

1 ,2-Dichloroethane (CAS No.:1O7-06-2)

mg/Kg With reference to US EPA 5021method. Analysis \ ras perfomed byGc/ltlS.

n.d.

1,2-Dichloropropane (CAS No.:78-87-5)

msr'(g With refefence to US EPA 5021method. Analysis was performed byGC/MS.

n.d.

l,SDichtoropropane (CAS No.:142-28-3)

mg/Kg With reference to US EPA 5021method. Analysis \oas performed byGC/MS.

n.d-

2,2-Dichloropropane (CAS No.:594-20-7)

mg,Kg Wth reference to US EPA 5021method. Analysjs was performed byGC/MS.

n.d.

Carbon tetrachlonde (CAS No.:56-235)

mg/kg With reference to US EPA 5021method. Analysis $/as p€rformed byGC/ltlS.

n.d.

Chloroethane (CAS No-: 75-00-3) mgikg With .eference to US EPA 5021method. Analysis wEs performed byGC/|VS.

Chloroform (CAS No.: 67-66-3) m9K9 With reference to US EPA 5021method. Analysis was performed byGC/MS.

n.d.

Chloromethane (CAS No-: 74-87-3)

m9KS With reference to US EPA 5021method, Analysis was performecl byGCiMS.

n.d,

cis-1 ,2-Dichloroethene (CAS No.:15G59-2)

mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

n.d.

cis-1,3-Dichloropropene (CAS No.:10061-01-5)

mg/Kg With reference to US EPA 5021melhod. Analysis wes performed byGC/t\4S.

n.d.

p d u e d & € p l ' n f u j m h o d p n d d

i - h ' . o n B s d d h ? n * y d e d d r o o * r e a d l q { s t d o

cohpaa ^iy !i'6od;j o b,6r 6i toaery tr hrsheb d h6 trhr or apts

qrdF .M ta wd / ii:lld,|ilt**FmliEffitri

Test Report No.:CU2O1Z14U3A Dale 201210i,04 Page : 10 of 24

CERAI/ITEC GIlIBHMULTIFUNCTIONALCERAI\'ICS LUITPOLDSTMSSE 15 D-91207 LAUF, GERIJANY

t]|lrr |ll|rlr

Tost ltem(s) unit llethod MDLResult LimitNo.l

Hexachlorobutadiene (CAS No.:8748-3)

mgKg With refercnce to uS EPA 5021method. Analysis was perfo{med byGCiMS.

n.d.

lMethylene Chloride (CAS No.:7+0$.2)

mg/kg With reference to Lls EPA 5021method. Analysis was pertormed byGC/l\rs.

n.d.

Tetrachloroethene (CAS No.: 127-184)

mgKg With refercnce to US EPA 5021method. Analysis was perfomed byGC/MS.

n.d.

ttang1,2-Dichloro6thene {CASNo.:15G60-5)

msikg With reference to L,S EPA 5021method. Analysis was pedormed byGC/MS.

n,d.

trans-l,3-Dichloropropene (CASNo.: 10061-02-6)

mg/Kg With reference to US EPA 5021method. Analysis was performed bYGo/tlls.

n.d,

Trichloroethylene (CAS No.: 79-014)

mgKg With rcference to IJS EPA 5021method. Analysis was perfomed bYGC/rVlS.

1 n.d.

HCFcs(llydrochlorofi uorocarbom)HCFC-21 (CAS No.: 75-43-4) mg/Kg With reference to IJS EPA 5021

method- Analysis was performed bYGc/lrlS.

1 n.d.

HcFc-22 (cAs No. : 7545{) mg/Kg With rcference to uS EPA 5021melhod. Analysis was perfomed bYGo/tlls.

1 n.d.

HCFG3l (CAS No.: 593-7G4) mgKg with rcference to lJs EPA 5021melhod. Analysis was perfomed bYGC/l\,IS.

1 n.d.

HCFo12'1 (cAs No.: 35,4-14-3) msn(gWith rcfef€nc€ to US EPA 5021method. Analysis was performed bYGC/tus.

1 n.o,

HCFG122 (CAs No.: 3*21-2) mgrs With reference to US EPA 5021method. Analysis was Pedomed bYGC/MS.

n.d.

8ffintr8yq;HlErTftf stf,i"S"13::89';'.i:'rs,":g"r",F:'r'..i:iEr- *-"f ill1:-:1":: --':,::"' ""***'*'*' i , ? i ; d , r . a ! ; dbyb6hE y *b@bbk . . c -d * . d ;

";;:;;;;;;i;; iA;; i lti;it ds'bcorim!'0,e6ft:i,itn,iar'Jniii.innft-m"*oi"ao"-*"a"-to-.*"'i'nd;;'F,;-..-''*d*drd-

dn ; ; : ; ; ; ; i ; ; : ; ; a ;F ' i i i . , . 6dc | f l s 'Mdm. ,a " y€cdnsnY ' ! d . l . : po16b ' i t }i;sd m 'n o.€r,i tr. 8a...0 "o,s*"

. -".... "-*n

@;.;3 -ir err' 6-d b trpq"-ed "€er

n ir "h113fr. {;*'""".HT:iS X

a @n lDma . ,Ta ldbE to ' i bwd '5_a '6 ond t .@+{d r4

I lLmfrtE*FffinfiRtfi

Test Report No.: C9201214843A OaIe:201210204 Page:11of 24

CERAIVTEC GIlIBHMULTIFUNCTIONAL CERAIIIICS LUITPOLDSTMSSE 15 D-91207 LAUF, GERMANY

llfir l lllll

Te3t lt€m(s) Unit ilethod MDLResult

LimitNo.{

HCFG123 (CAS No.: 30G83-2) mgKg With reference to uS EPA 5021method. Analysis was performed byGC/tMS.

n.d.

HCFC-124 (CAS No.i 2837-89-0) mg/kg With reference to US EPA 502 1method. Analysis was performed byGC/MS.

n.d.

HCFG131 (CAS No.r 35$28-4) mgKg With reference to US EPA 5021method. Analysis was perfomed byGC/l\,1S.

n.d.

HCFC-132b (CAS No.: 1649-0&n mg/kg With refe.enc€ to US EPA 502 1method. Analysis was performed byGC/MS,

HCFC-133a (CAS No.: 75-88-7) mg/Kg With reference to US EPA 5021method. Analysis was p6rformed byGC/t S.

n.d.

HCFC-141b (CAS No.: 1717-006) mg/Kg with reference to US EPA 5021method. Analysis \Nas perfomod bYGC/MS.

n.d.

HCFG142b (CAS No.: 7568-3) mdts With reference to US EPA 5021method. Analysis wEs perfoamed byGC/MS.

1 n.d.

HcFc-221 (cAS No.: 422-26-4) mg/kg With reference to US EPA 502'lm€thod. Analysis was performed bYGC/t S.

'I n,d,

HCFC-222 (CAS No.r 42249-1) mg/Kg With reference to US EPA 5021melhod- Analysis was performed bYGc/rlls.

I n.d.

HCFC-223 (CAS No.r 422-526) mgKg With reference to IJS EPA 5021melhod. Analysis \ /as performed byGC/|\,IS.

1 n.d.

HCFG224 (CAS No.: 422-54-8) mgKg With feference to US EPA 5021method. Analysis was performed bYGC/tVlS.

1 n.d.

HCFG22sca (CAS No.: 422-56-0)msftg With reference to US EPA 502 1method. Analysis was performed bYGC/MS.

n.d.

iilit f&iFi#riE:ii:E8fdJrjie'€BlYs"'r,Fi:*r51':*dI'sEi':'or:nrF6::i-::1::l l"*^'*-*-"*asq .d regL6n .? !omsd . . 66e1ado ! . . ada I ' ! b€o lELg '

;;;;;H.;.;t-d"*..ft!'.idhr"-.-dc*d'6-b#;i;6;,n'i's*4!or,sf.m

"n r ' a - - - *e . . " * " , i ' i " . o6ddsdE td , i adso ' -; i ; ; d ; n ; i * d - - | v * " *h1 " " r . " ec . l . . * . - . i i ] r y i d ; coa ; ' ; ! d . €s fgo | , v l br" or s,r *' *s '"

". *;"iihr;tui ft'"*r'nrrc'b'Fru

- * -;:E;;;; ':;"@i':ri;in ldr md ftnds fuY b Pm

a rred. vr.dii / ttitirfiJ|x*mBndst6t

TeSt RepOft No.: cs201214843A Dare:2o1zozo4 Pasetl2ot24

CERAIIITEC GITIBHMULTIFUNCTIONAL CERAIVIICS LUITPOLDSTMSSE 15 D-91207 LAUF. GERITIANY

tl r mrrll|l

Test ltem(s) Unit Method MDLResull Limltt{o.'l

HCFC-22scb (CAS No.: 507"55-1)mgKg With reference to US EPA 5021method. Analysis \oas perfomed byGC/t\4S.

n.d.

HCFC-226 (CAS No.: 431 -87-8) mg/kg With reference to US EPA 5021method. Analysis was performed byGo/tlls.

n.d.

HCFG231 (CAS No.: 421-94-3) m(/kg With refercnce to uS EPA 5021method. Analysis was performed byGCiMS.

n,d.

HCFC-232 (CAS No.: 460-89-9) mg/Kg With reference to US EPA 5021melhod. Analysis was performed byGC/t\4S.

1 n.d-

HCFG233 (CAS No.: 7125-84-0) m9ks With refercnce to US EPA 5021method. Analysis was performed byGC/MS.

1 n.d.

HCFC-234 {CAS No.: 425-94-5) mg/Kg With reference to US EPA 5021method- Analysis was performed byGC/t S.

1 n.d.

HCFG235 (CAS No.: 46G92-4) mgKg With rcference to US EPA 5021method. Analysis was performed byGCA4S.

1 n,d.

HCFC-241 (CAS No.; 666-27-3) mg/kg With reference to US EPA 502 tmethod, Analysis was performed byGC/MS.

1 n,d,

HCFC-242 (CAS No.: 460-63-9) mgKg With rsfefence to US EPA 5021method. Analysis was perfomed bYGC/MS.

1 n.d.

HCFS243 (CAS No.: 46G69-5) mgfts With rcfefence to US EPA 5021method. Analysis was performed bYGC/tVrS.

1

HCFG244 msas With reference to uS EPA 5021method. Analysis was performed byGC/MS.

n.d.

HCFC-251 (CAS No.: 42141-0) mg/kg With reference to US EPA 5021method. Analysis was per{ormed bYGC/MS.

n.d.

H#n#Hyqgg1:iffdf +rsfi;T,.ffi8flq;i:"r."fi-tq"r' ":1::: - ll-:"'*-***""*jrj"er***:n*,f*njtru"rln*:."sltr,s:sr.".1x-rffrf*rrlgirsi"",Lrx$;"'trili:'#*tr"'r#ii**'".o*;lJ,ffiTli"iu'.,i,i mnrii

"i' i#i-m^ oo iiddr EUs o.rne t6c' 'i i; hod.'d rF .oor.a teied rar 'r'io

t i , i i i . ' . . g ' n ro - . * - ' - o . r i n ' h . ' n |Edc |51s ,ddoT : ; i ' ; i . i ' " " J i " d .gpo*b ' . ' o ' t s c | €nhd '1 - , . d 'moam4m.r ; ; ; ; n ' ; ; ou_od r s ns . €ma f f qoo .e_ '

- i ' oodn i ' 610 'B aad 'ed 6@pr na lcam;ry Ary-.dtu;.dEErm. bs'ry d dr ier m d b.6nbdi;;F-;;at bilru;ad 36rdu 4d on ideB rut b p@ork b he tuhd 'ns( d b' a*

ryrr+! crr ri wd / firlfisrlE+FmnERt*

TeSt RepOft No.rcE/201214843A Date.2o1zozo4 Pase:13or24

CEMMTEC GMBHIVIULTIFUNCTIONAL CERAMICS LUITPOLDSTMSSE 15 D-91207 LAUF. GERMANY

|l] ||ttl[Ilrt]r

Teet ltem(s) Unit Mothod MDLResull

LimitNo. l

HCFC-252 (CAS No.: 819-0t!1) mgikg with refefence to US EPA 5021method. Analysis was pedormed byGC/MS.

1 n.d.

HCFC-253 {CAS No.: 460-35-5) mgKg With reference to US EPA 5021method. Analysis was perfomed byGC/MS.

1 n.d.

HCFC-261 (CAS No.: 420-97-3) mg/kg With reference to US EPA 5021method. Analysis was pedormed byGC/|VS.

n.o.

HCFG262 (CAS No.: 421-02-03) m9Kg With reference to US EPA 5021method. Analysis was perfotmed byGCiMS.

n,d,

HCFC-271 (CAS No.: 430-55-7) mg/Kg With reference to US EPA 5021method. Analysis was perfomed byGC/MS.

n.d.

1. mg/kg = ppm : 0.1wro,6 = 1000ppm2. n.d. = Not Detected3. MDL = llethod Detection Limit4 . " - " = N o t R e g u l a t e d5- * = Qualitative analysis (No Unit)6. Negative = lJndeteclable / Positive = Detectable7. Asbestos : Negative = "< 1.0 %", Positive = "> 1.0 %"

PFOS Reterence Information : POPS - (EU) 757/20'10Outlawing PFOS as substances or preparations in conc€ntrations above 0.001% (10ppm), in s€mi-finished products oradicles or parts at a level above 0.1%(1000ppm), in textiles or other coated matedals above 1ug/m2

' n t rBb3 l€Fn t t ' 01y l o .h .qdcdmdi!kJr El *qs { HlElllltflr'l lH2Efi 61 " 4H& l Iti :)"lBd ldil l s _]ta'_i;;n.1

E d.d o d; cmFni aoF b tu crs6 coo'm; dlrc mrud oi.^tr *dbds r @am.ro.ortu brd dntr+b &d@ b-!-' {d c"-ft-, h' ii;;;; A;;;i#';€!s;;;'atii"d crdido-lr'T€ o-6trs abnb'306*roh'i;;ft;d; rbtilt'. hdanMata'iii"d i'iir;liai(n ''is ddlrei iDrein it; i'di* t h€ demi, 'isd{si ba iro ompaiv i ird ie3df t l ed 'B ' f umdmfx f l o *o :1 l € | f i . 3dL .d lB l1 f f g i ! nyD . !mpa1yss€ceo '3 ' b | i ,Gbmigoo. rt""*go"|*' ohb ro d{.r@ re h6 Endon @ritu ft6 d*rsd e..d ba F.mpanr tur d.dodd . i.dbi; hosry d h]!'idi or ih€ obi;i;iF,Ae or $h edm$r ts m r[{ur sd

4 hlts .lq,ra wd / FirLrrirrd*Erdrifrffirs

Test ReportCERAMTEC GMBHMULTIFUNCTIONAL CERAIJICS

No. : CE/201214843A Date :201i,02t}4 paoe: 14 of 24

LUITPOLDSTMSSE 15 D-91207 LAUF, GERIJANYt] tl| [ttttlrl

1 ) Thes€ sampies were dissolved totally by pre-conditioning meihod according to betow ttow chart.( Cf'lest method excluded )

Name oflhe person who made measuremenl: Climbgreat yangName oflhe person in charge of measurement Troy Chang

2)3)

ICP-AES

Sample IVaterial DigestionAcid

Steel, copper, aluminum, solder Aqua regia, HNOr, HCl, HF, H,O,

Glass HNO3/HF

Gold, platinum, palladium, ceramic Aqua rcgra

Silver HN03

Plastic HrSO4, HrOr, HNO3, HCI

Others Any acid lo total digestion

[email protected] du6d.6€0tintur wr$dpdoffrlGnpomsdndb.co.Dar t? / B l ;?!i .rlRA1l Rl6?ldlSt,&AlF? 4E- 1144- "i*EjAl T lS.nlb!

I d brsd ro 'b c3?d cfdrol d s.usd b rmE 'i cond' m3 tu - .tu

inturondrdrt idmnfieron,ndluddturrslsd.fn.dh.Dn.AdhfeyTh.comFrybe|'rs4odbity

cmFny tuy uiadoda abdoii '@dry d h]3fidoi orrh€ 6L*r or aoFadtu. or lh s dodn.d c ui.['ur.nd on€nds n.i b6 pGeMed b ib tu *id;ddb6rtu

Sample lvleasurement

Acid digestion by suitable acidclepended on differenl samplemateial (as below table)

Microwave digeslion with

HNO/HCI/HF

Heat lo appropriate

temperalure lo exiract

Cool, tilter digesiate

through filterAlkal iFusionHCllo dissolve

Add diphen9-carbazide for

measure the absorbance

at 540 nm by UV-VIS

*"un,,,i"&1,1ffii*,I il{,tliiilgtiffI1?lil' "T-

Test Report No.: C9201214843A D3l.e:201210?,04 Paoe:15 ol24

CERAIIITEC GITIBHMULTIFUNCTIOML CEMI\4lCS LUITPOLDSTMSSE 15 II91207 LAUF. cERltlANY

Analyticalflow chan of Soxhlet extracgon (LCIMS) procadure

t][Ilmfirllltl

Sample pretrcatmenuseparation

I

Data

comDafr [r ]l-d FdE nH-LxlAlrrl:L:EtAa " td;. {{r"Eifi"4l i A..bAand rq*ftntrmardidm*6 $68 6r6m3ed codhoGbrErtunc ooomsds.t trw $'@n/ddnE

l ; - { r r d n < i s d d @ ! r n a . y r r e d d ! d c m r d a d ! H h i -

.nd drsdon! une u. hns.dori [email protected], rh 3 ddmed ennor b Ep.de sopt n tu L ulM pnorsEp( n tu r. w1M pnor tu ,Ppdgr d ha'c, ' :trr '6n.r.or19 dir€' eft.ro d edon! Lnd b. [email protected] ri s odn.r endb €p.d!E. sopr r Jr. wrd md #,Posg d ha

a Name oflhe percon who made measurement Roman Wongr Name of lhe percon in chafge of measurement: Troy C hang

I Test lten3: PFOS/PFOA ' Benzotriazole )

TeSt RepOft No.: cEt2o12t14843A Date.2o12to2to4 Pase:16of 24

CERAMTEC GMBHI\4ULTIFUNCTIONAL CERAI/IICS LUITPOLDSTMSSE 15 D-91207 LAUF. GERMANY

Chlorinated Flamc retardant analytical flow chart

1) Name of the person who made measurcment: Bary Tseng2) Name ofthe person in chaee of measurenent: Troy C hang

I Refercnce method: US EPA8270D, US EPA 3540r Tesl ltems: PCBS, PCNS, PCTS, ltlkex, Ce MCCP

Data

ll|l|t [|rrlr|r

pr€13) '6bd rhk bn @on 6n6r ba rcComoanh l qFes r ' nE ;gF l {? , s : i z t s , rE ! . r n - I& ! " i l r " q : r ' I " r n E { .

nb rond16 rq 'T * rne lons rd irfy rh comFny 6 de 4o$ bi,v' r dbEpd l€d3cp l i 1 f u |

Test Report No. : cE/201214843A Date:2o1zo2!o4 PasetlT of 24

CERAMTEC GMBHItIULTIFUNCTIONAL CERAMICS LUITPOLDSTMSSE l5 D'91207 LAUF, GERMANY

|l][t t!l||r

Analysis flow chart for delerminalion of PVC in matorial

r Name oflhe person who made measuremenl: Ginny ChenI Name ofthe person in charce of m€asurcmentr Troy Chang

i n s s b { D F n ' $ e l o n ] y l o l h € & o p l @ d u d r e p t i f u | , d o d p i d " r i'nEryrilTEl,&sj ,{HAl"i*l49l1li"E.:&flAE lEd- kl,l1, \.13 til lq! llCSrnhd€um$ t l a i g .dby1h6c0np . r y ! ub ]6dbbGsmBcod lon6ds

bldd br.-..nd cf d !0.E b Er*n

-.*".;; i : i l : | :.*: i j ;*.)T.i." '"#',H.*-*;*i i "- ' " """- '* ', '

Sample analyzed by FTIR

Chec* wave-number of C-Clbonding

Test ReportCERAIVTEC GITIBHMULTIFUNCTIONAL CERAMICS

No. : CE/2012l148434 Dai€.2O1ZOZO4 Paoe : 18 of 24

LUITPOLDSTMSSE 15 D-91207 LAUF, GERIVANY

(TeEt ltems: Phthalate ' B€nzotriazole . HBCDD . NP . DBBT.

Oryanic phosphorus compoundrs)

trfllrI. tllllll

Analyticalflow cha of Soxhlet €xlraction (GC/MS) procedure

I Name of lhe person who made measurement Roman Wongr Name oflhe person in charge ofmeasuremenl Troy Chang

nrh.radGoodcrdontb{i.*nr€{e)l.sd.h6bn@od6nmLsrcpodu€d.€^6prrntur * ihdr Fiorwins p€m 3s on d h3co r raaBr . e e@ !BS4Fr * t d j ^+ -as t d& l : l d f - qEFdb ' " l J l - a t vTh E ood-md tr $&bh6comMand ror..dM( rffi dem.nr &t.di,-nr am codtms w ns4{4oT on/rsd*0oor.iimibr on d rdrt idmnneton l;d ':id doi i$u.s dsfind b.6 i Air io d.r ol rhi3 doonenl adu$d hlr 'ftu.lim.fi1!nEii€ntmd'ands.liin1i.imibo'c||€n|li9rudo6iai,rhconFnybd3r..ponEb''-@didouMts -b doLnfr 6cmFny Ary uruubodair abdon foasry or fsltr€ron or h' @i6d or ap

Test ReportCERAI/ITEC GI/tBHMULTIFUNCTIONAL CERAIVICS

I

I

No. : CE/201214843A Date:201i,02104 Page: 19of 24

lll|t|:: l]tLUITPOLDSTMSSE 15 D-91207 LAUF, GERMANY

Analytical flow chart of Organic-Tin content

Name ofthe person who made measurement GinnyChenName oflhe percon in chaee of measurement: T.oy Chang

Dala

o d u c d e e p l i f u l d b o d p ' o l dCmEi!hl EJ8! i E ,ERHtlr€ll2ll l A r " IE"{t{| "4h:n: i J.,b8l

,ond oftdSe1uDnftdoER *drrdr.rerdco.ono$6rEr.miandid on E6 dnd tudn An' h

rh rh6 dbideiadoi onrv snd * ihii h6 rh r d c iad3 insdons i iryhneo m rdm .rcEsm dl hq notu so dro.ron! und h. b.n*dod @compary Ary unadhoruA rE,!r n bqary q bls i€ln d hs trhr or ap

n"**.,ffiiu';tl.':j I i,;H.Jiil*iilI1n $ff ,991"**tr,i:1.""-,nu*'u***oon*.*

Concenbate/Dilute Exkacted solution

Analysis was perfomed by GC/FPD

Test Report No. : CE/201214e43A Dale : 201210?,04 Paoe :20 ot 24

CERAMTEC GMBHII,IULTIFUNCTIONAL CERAMICS

Analytical flow chart of halogen content

1) Name ofthe person who made measuremenl: Rita Chen2) Name ofthe person in chafge of measurement: Troy Chang

LUITPOLDSTMSSE 15 D.91207 LAUF, GERMANY

Sample prelreatment / Sepataiion

Weighting and putting sample in cell

Oxygen Bomb Combustion / Absorpiion

Dilutbn 10 fixed volume

Analysis was performed by lC

conFl[i]l teS3! -[HiL+liti]13 lliiAA. ldA f Ad .-FditE i " Eo\tqr'

rcddm. E s".d d u. cmEn3d ro dftnrbrddLnfb &drF16 sm E fd cortons to' Ebtu

i ' ln*idm s6 ddd badn. Anr fdt E r m . d 6 ' m i w m o n o n k a o w f t i h r m c r C a d s n $ t r o t r 3 i i nhiso m irem &sE,ft dl h.r iotu eo dr oar on! Lne h. hlnsdort ecmda ms odr6a 6nd ba Erucomp'a Any!m6o,ze dEErm'toEerydbsidbdhstrblorap

*"*'*ffilil]iio\'3;I l;k,ifig;|ff l"t*$$#gll"*.,lll:]"!k *-,nu"nuo*"*"oo"o

Test ReportCEMMTEC GIMBHMULTIFUNCTIONAL CERAIJICS

No. : CE|2O1Z14843A. Date : 2O1ZOZO4 Paae : 21 of 24

LUITPOLDSTMSSE 15 D-91207 LAUF, GERIVANY

Analysis flow chart for determination of Aabestos1 ) Name of the Derson who made mea6urcmenl: Victor Kao2) Name ofthe person in charge of measuremeni: Wendy Wei

I Refercnce mothod: EPA 600/R-93/l l6 )

Not conraining Asbesros/

@ d u d r e p l i f u l . d o d p i d f rcnFnyRJ BA&.8 {E: *lRl6flnld -AB Frt IEd-*l{4 \:ltffril r.JfllSp

nidhi d ri'driry. id.mn ieln 'id j

rE$don tm d.eno.i h., nod F hnEdon oodn.nri Tdeoo@rcdmFry Ary u@rb4n sbdon blw or raibf€ton d b. @ftdtr @

Conlinue wh€n problem€ a€ encounle€d with PLlvland/or for qualily assurance purpo€€s

Inleriercnce mahi\ removal

Asbeslos identification by dispersionstaining pobnzation light microscopy

A€bestos identitication by X-€y

** f,iFi$l' I ;i*,?1.;r,];'i[il::t;.,]-**u;]'*., r ar'eb.,.lr'**...*.

Test Report No. : CEi2012l14843A Date : 2O1Z0ZM Paoe : 22 ol 24

CERAITITEC GMBHIJULTIFUNCTIONAL CERAMICS

t]ttllll||Iltt]lLUITPOLDSTMSSE 15 I}91207 LAUF, GERITIANY

Analyticalflow chart

I Name of lhe person who made measurcment Roman WongI Name of lhe person in charge ofmeasurement Troy Chang

I Tesl llem3: PBB/PBDE, TBBP-A-bb)

Firsl lesting proc€ss -----+ Optionalscrcen pfoceEs ---. Confirmation proces€ -.>

Screen analysis

coFo. raJ FH&! i - { &d- E l lqUd ln IEEA{ . i€b f l4dr " -sa ,q . r " i id ! .bjd b rffir ad codi m3 tu E 6dm

irturondrdi t -d6rnh6dolends a . f t d n < i f u M o n f | y a ' o d

b a ' d d i s . f 3 ' r d e . ' 0 . ? 9 d o n p d L e d 4 e p l i l f u |

'Li-;iirn-rrn;i;;;i.ii .i;ii. . r

Sample extraclion method

Concentrale/Dilute Extracted solulion

Filter

Analysis by GC/lt/S

lssue Repod

Test Report No.: CE|2O1Z14A$A Dale:2012102104 Paoe:23 of 24

CERAMTEC GI\,iBHMULTIFUNCTIONAL CERAI\/IICS LUITPOLDSTMSSE 15 D,91207 LAUF. GERMANY

Analytical flow cha(otvolatils oryanic compounds (VOCS)

I Name of lhe person who made measuremenl : Chun WuI Name of the person in charge ofmeasurement : Shinjyh Chen

I Reference melhod : US EPA 502 1 )

nlfltm lm0trmt

Sample pretrealmenl

Take sample and put il intoheadspace glassware.

o rpanyuJ t l r ; t 8 r ' {F1 t :R@9 ld l t 4 & -AE lE l , - { l i l " : - " q . rE&"

Test ReportCEMMTEC G[/lBHMULTIFUNCTIONAL CERAIVICS

No.: CEI2O1Z14U3A, Date 201210?,A4 Page 24 ot 24

LUITPOLDSTMSSE 15 D-91207 LAUF, GERMANYr:|| tt]||ln|rr|l

* The tested sample / paft i6 marl(ed by an anow if if,s shown on the photo. .

** End of Report "

cmF.th/ tq$qS llmel .?l49jii];i -df{R&.,lE: llt li" *TA; I "! n dlJ.- t s f u913 ig .dbyso . f fF

|edhbdoUm'di3'sdtsdhatdoh t m d B d s ' e d i o i o n | , a n d d l h f t s c m F r y s s o € E s o i d b l i l y i s b

-_*-***-_*^_1 | rdF cie ri wd / fittir5:]ijf*Ld6n}f*r*

L4843

Test Report Number : TWNC00249179

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 5 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

Applicant: Littelfuse Philippines Inc. Date : Mar 28, 2012 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description:

One (1) group of submitted samples said to be : Part Description : Silver plated Wire Part Number : DRAGxxx Date Sample Received : Mar 22, 2012 Date Test Started : Mar 22, 2012

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Number : TWNC00249179

Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Submitted Samples

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content (mg/kg with 50cm2) Negative (< 0.02)

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation

was not found at the time of Test.

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Mar 22, 2012 Test Period : Mar 22, 2012 To Mar 27, 2012

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.


Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

(Ⅲ) Test Method: Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content


2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis Spectrophotometer.

0.02 mg/kg with 50cm2

Remark: Reporting limit = Quantitation limit of analyte in sample


Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

(Ⅳ) Measurement Flowchart:

Test For Cd/Pb/Hg/Chromium (VI) Reference Standard：IEC 62321 edition 1.0:2008

Remarks: *1: List Of Appropriate Acid：

Material Acid Added For Digestion

Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

End of Report

Sampling/grinding or cutting

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample

Boiling water extraction

Metal Polymers / Electronics

Negative*2 Confirm the tested samples are totally dissolved


Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

Photo

Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338

TEST REPORT NUMBER: SHAH00300757

PREPARED AND CHECKED BY: AUTHORIZED BY: FOR INTERTEK TESTING SERVICES FOR INTERTEK TESTING SERVICES LTD., SHANGHAI LTD., SHANGHAI

MYRA LV JACOB LIN CHEMICAL LAB SENIOR MANAGER GENERAL MANAGER

PAGE 1 OF 6

APPLICANT: LITTELFUSE,INC. DATE: FEB 02, 2012 800 E. NORTHWEST HWY

ATTN: A. CESISTA/ K. BACILA

SAMPLE DESCRIPTION: One(1) submitted sample said to be Wire with plating. Part Description : Wire(Polyil). Part Number : 687279-001. Date Sample Received : Jan.17, 2012. Date Test Started : Jan.17, 2012. ***********************************************************************

TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)

*********************************************************************** To Be Continued



TESTS CONDUCTED

PAGE 2 OF 6

(Ⅰ) Test Result Summary :

Result (ppm) Testing Item

(1)

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content (mg/kg with 50cm2) Negative (< 0.02)(#)

Result (ppm)

Testing Item (2)

Heavy Metal

Cadmium (Cd) content/Plating ND Lead (Pb) content/Plating 72 Mercury (Hg) content/Plating ND Chromium VI (Cr6+) content (mg/kg with 50cm2)/Plating

Negative (< 0.02)(#)

Tested components:

(1) Substrate (2) Plating

Remarks: ppm = Parts per million = mg/kg ND = Not detected # = Due to the insufficient sample area, reduced total

sample surface of 10 cm2 was used and the dilution factor was adjusted accordingly.

mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre

Negative = A negative test result indicated positive observation was not found at the time of testing.

Responsibility Of Chemist :Dent Fang / Ken He

Date Sample Received :Jan.17, 2012 Testing Period :Jan.21, 2012 ***********************************************************************

To Be Continued



TESTS CONDUCTED

PAGE 3 OF 6

(Ⅱ) RoHS Requirement: Restricted Substances Limits Cadmium (Cd) Content 0.01% (100ppm)Lead (Pb) Content 0.1% (1000ppm)Mercury (Hg) Content 0.1% (1000ppm)Chromium VI (Cr6+) Content 0.1% (1000ppm)Polybrominated Biphenyls (PBBs) 0.1% (1000ppm)Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

(Ⅲ) Test Method:

Testing Item Testing Method Reporting Limit



2 ppm

Lead (Pb) content


2 ppm



2 ppm


With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis spectrophotometer.

0.02 mg/kg with

50cm2

Remark: Reporting limit = Quantitation limit of analyte in sample ***********************************************************************

To Be Continued



TESTS CONDUCTED

PAGE 4 OF 6


Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents Reference Standard: IEC 62321 edition 1.0:2008

*********************************************************************** To Be Continued

sampling/grinding or cutting

weigh sample and for different

material, digest the sample with

make up with deionized water

Cd/Pb/Hg

analyzed by ICP-OES

weigh sample and add alkaline solution

definite temp.

make up with deionized water and add diphenyl-

carbazide solution

Cr6+

weigh sample and add organic

soxhlet extraction or

solvent extraction

concentrate the extract and make up with organic

PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples

boiling water extraction

metalpolymers / electronics

negative*2confirm the tested samples are totally

dissolved No

cool and filter the extract



TESTS CONDUCTED

PAGE 5 OF 6

REMARKS: *1: List of appropriate acid：

Material Acid added for digestion



*********************************************************************** To Be Continued



TESTS CONDUCTED

PAGE 6 OF 6

***********************************************************************

End Of Report




MYRA LV JACOB LIN CHEMICAL LAB SENIOR MANAGER GENERAL MANAGER

PAGE 1 OF 7

APPLICANT: LITTELFUSE,INC. DATE: FEB 02, 2012 800 E. NORTHWEST HWY ATTN: A. CESISTA/ K. BACILA

SAMPLE DESCRIPTION: One(1) submitted sample said to be Wire with plating. Part Description : Wire(Elschukon). Part Number : 004206. Date Sample Received : Jan.17, 2012. Date Test Started : Jan.17, 2012. ***********************************************************************


**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 2 OF 7

(Ⅰ) Test Result Summary :

Result (ppm) Testing Item

(1)

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content 20 Mercury (Hg) content ND Chromium VI (Cr6+) content (mg/kg with 50cm2)


Result (ppm)

Testing Item (2)

Heavy Metal

Cadmium (Cd) content/PLATING ND Lead (Pb) content/PLATING 238 Mercury (Hg) content/PLATING ND Chromium VI (Cr6+) content (mg/kg with 50cm2)/PLATING


Tested components:

(1) Substrate (2) Plating

Remarks: ppm = Parts per million = mg/kg ND = Not detected # = Due to the insufficient sample area, reduced total

sample surface of 10 cm2 was used and the dilution factor was adjusted accordingly.

mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre

Negative = A negative test result indicated positive observation was not found at the time of testing.

Responsibility Of Chemist :Dent Fang / Ken He **********************************************************************

TO BE CONTINUED



TESTS CONDUCTED

PAGE 3 OF 7

(Ⅱ) RoHS Requirement: Restricted Substances Limits Cadmium (Cd) Content 0.01% (100ppm)Lead (Pb) Content 0.1% (1000ppm)Mercury (Hg) Content 0.1% (1000ppm)Chromium VI (Cr6+) Content 0.1% (1000ppm)Polybrominated Biphenyls (PBBs) 0.1% (1000ppm)Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. **********************************************************************

TO BE CONTINUED



TESTS CONDUCTED

PAGE 4 OF 7

(Ⅲ) Test Method:




2 ppm

Lead (Pb) content


2 ppm



2 ppm


With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis spectrophotometer.

0.02 mg/kg with

50cm2


Date Sample Received :JAN.17, 2012 Testing Period :JAN.17, 2012 TO JAN.21, 2012 **********************************************************************

TO BE CONTINUED



TESTS CONDUCTED

PAGE 5 OF 7



**********************************************************************TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples




dissolved No




TESTS CONDUCTED

PAGE 6 OF 7

REMARKS:

*1: List of appropriate acid： Material Acid added for digestion



**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 7 OF 7

**********************************************************************

END OF REPORT

Validit nownFor OuestiPlease Co ith sGS

Test Report No. : CE20'11184940 Dale :2011h21o1

POLYFIL AGOBERALLMENDSTRASSE 2OA, CH$3OO ZUG / SWITZERLAND

Thefollowing sample(s) was/wero submitted and identified by/on behalf of the client as:

Pager '1 of 7

Ll|| lllllllll ll

Sample DescfiptionBuyer/Order No.Sample Receiving DateTesting Period

A9100011-00102011t11t25201I II1125 rO 201I l12to 1

Test Reault(s) Please refer to next page(s).

praG)radd hs@@d€nndb

c * * - , ,iiifji'iiiii;":;ovm'c";p,'iyi,bFatec*""rc*dioreas;"*Fi.l***"d*.abb-"ql i , ; i# , - . i . i ' *1 ' l t . j ' . *Jb , " i t i - . " "ac*a*o ,ea"o* ' : * " *e" - . ' " * . . l,il-.liiJ.ii.lru,".aa,*;**isr d"isdrt'"' rtmdff.mndhe@nciedssecnp5ir'srnd.qsdse

; ; ; ; f t " ; ' " . ' * ; . ; " ; ' * ' . ' e n o o . " e n ' j o " - . * . o r e - j - * a . e " " . ,' * . ; .Dk ie , ;o r .6 rs , r

1rn.r +!1iiE ti 1M 10r2o tD I i e6 iorrrs tt dw{<om

Ch..r{.{ lrbq.a..Y -Tdld

MeD&' or$e scsGldp l\6' 5A)

Test ReportPOLYFILAGOBERALLMENDSTMSSE

Test R6ult(s)

PART NAIVE No.1

No.: CE/2011/84940 Date | 2011112J01

2OA, CH€3OO ZUG / SWITZERLAND

Paga:2 ol7

r rIlt flttlt

SILVER COLORED IVETAL WIRE

Tost ltem(s) Unit ethod MDLRs6ultl.lo.l

Cadmium (Cd) mgKgWith reference to IEC 62321r 2008 andperfomed by ICP-AES.

n.d.Lead (Pb) mg/Kg 2 n.d.Mercury (Hg) mS/kS 2 n.o,Hexavalent Chromium Cr(Vl) With r€fefence to IEC 62321: 2008 and

perfomed by Boiling water ext€ctionMethod.#

Negative

Sum of PBB3

mg/Kg With reference to IEC 6232'1r 2008 and

n.o.Monobromobiphenyl 5 n.d-

Dibromobiphenyl 5 n.d.Tribromobiphenyl 5 n_o,Tetrabromobiphenyl n.d.

Pentabromobiphenyl 5 n . d .

Hexabromobiphenyl n.d.

Hoptabro.nobiphenyl 5 n.d.

Octabromobiphenyl 5 n.d.

Nonabromobiphenyl 5 n-o.Decabromobiphenyl 5 n.d.

Sum of PBDES perfomed by GC/MS. n.d.

Monobromodiphenyl ether 5 n.o.

Dibromodiphenyl ether 5 n.d.

Tribromodiphenyl ether n.d.

Tetrabromodiphenyl ether 5 n.d.

Pentabromodiphenyl ether 5 n .d .

Hexabromodiphenyl ether 5 n.d.

Heptabrornodiphenyl ether n.d.

Octabromodiphenyl ether 5 n.d.

Nonabromodiphenyl ether 5 n.d.

Decabromodiphenyl ether n . d .

sGrrsdd rhs rd @d €n@lb €

ni" i*i-.a;";;;ovdc"'mry ioi"ar r c*.a c"ar*" a sr -ogo i - t tau j 'o* '$ ;b i ' . ' "dc"d l - ' l . ,Ed- " * - . *ua*"g" . . ' t .l*i.'ii]*r-"rl*i;a."**ieiam"ryho6dat"a*,..n"a&i*dlsl"b,'d;^ffi"&hi*- , ' r * "u" i . "ac * , " . * p . i .b ivs ioBoam5d66@m

,ro* repua**p to t . .wm*-.

"w-'ia o"-^eno

l l r,: +i,!4i'r \t r 336 to2t22ee 3)7e | + & taa2a )t1 w 4"an

Test Report No. : CEl201'1/84940 Dale: 2O11112J01 Page: 3 of 7

rl [|||llt[l]tPOLYFIL AGOBERALLMENDSTMSSE 2OA, CH€3OO ZUG / SWITZERLAND

T€t lt.m(s) Unit Method [IDLResultNo.1

HalogenHalogen-Fluorine (F)(CAS No.: 14762-9+8)

mg/KgWith reference to BS EN ASAZ2007.Analysis was perfomed by lC.

50 n.o,

Halogen-Chlorin€ (Cl)(CAS No.: 22537-15-1)

50 n.d.

Halogen-Bromine (Br)(CAS No.:10097-32-2)

50 n-d.

Halogen-lodine (l)(CAS No.: 14362.44-8)

50 n.d.

Note :1. mg/kg = ppm i 0.1M% = 1000ppm2. n.d. = Not Det€cted3. MDL = Method Deteclion Limit4 . " - "=No tRegu la ted5. " = Qualitative analysis (No Unit)6. # = a. Positive means the presence of ClVl on the tested areas

b. Negative means the absence of OVI on the tested areasThe de'tected concent€tion in boiling-watea-extraction solution is equal or grcatef than 0.02 mg/kg with 50 cm'ztested areas.

'^lhsl6tts@1delm'Lo1bgamplel' igddft3l6drcpd€molbercpa**. ,n'ii i"il'ln i'' !i"a uyt;c".pry -bdb k c.€€rc-di *'; ssf u " . d - . 6 - d @ j . . d ' " d i g d b T m " ' d c m d € B 6 E | M " o " - . . a ' * * . e ' . . l " * ' "iilj'i'ii*i*

"ae;;a-,**; ed sad'edrhd tud;i€dad

*r,.* "'"^

'r i,.," o c,""* *', ; . , d L . M d . r f f i . n d a , o s t r a ; o r * _ p - ' * . @ " . ' ' , r o r

h - . ^ ' ' E E i d o n d n e @

Test Report No. : CE/2011/84940

POLYFILAGOBERALLMENDSTRASSE 2OA, CH63OO ZUG / SWTZERLAND

Dale .201111i,01 Page: 4 ol7

||t] tlt trlll

1) These samples were dissolved totally by pretonditioning method according to below flow chart.( Cr- test method excluded )

2) Name ofthe person who m€de measurernent: Climbgreat Yang3) Name of the person in charge of measu.ement: Troy Chang

ICP.AES

S€mple Material Dige*ionAcid

Steel, copper, aluminum, solder Aqua €gia, HNO3, HCl, HF, HrO,

Gla6s HNO3/HF

Gold, platinum, palladium, ceramic Aqua fegia

Silver HNOg

Plastic HrSO4, HrOr, HNq, HCI

Others Any acid to total digestion

ipsGlb{d rh s rd reD.d €nid bcmtsry alrrjllr!I. iri.if::l.r{iji;;i-\Jl*, i*"f.inF*}ri1'r:\, +j'an fn:/tE+'l."*.i,'.nggauymc"'pny3u$].dbAGm66|coidlonso'src

"e-" t"-a aoajmero.

";or; b i*.. ..d cddiom ro, E efu

,"M"if,*ld."d]@nd"" j**;

ory .r *u, rt'" i. e ot c iear etu;,ob"dd ods.6e,tuh

tr4!.1 lt rFrl |ri 14610r)re

Cutting / Preparation

Add appropiate amount of

digestion reagent

Acid digestion by suitable aciddepended on difierent samplematerial {a8 below table)

Heat to appropriate

t€rn perature to exttact

1) Alkal iFusion2) HClto di6solve

Add diphenyl-carbazide f or

color development

measure the absotbance

at 5,10 nm by W-VIS

Test ReportPOLYFILAGOBERALLMENDSTRASSE

No. : CE/2011/84940 Dale.2011hZO1

2OA, CH€3OO ZUG / SWITZERLAND

Page: 5 of 7

[fir |l lt]||]t

PBBIPBDE

1) l.lade of the person2) l{anE of the person

analytical FLow CHARTwho nEde rBasurerEnl Rornan Wongin charge of nEasurenEnt Troy Chang

Fi6t te6ting process ------'

Optional screen process ---.

Confinmtion proce6s - .>

Screen analysisi . . . . . . . . . . 1 . . . . . . . . . .

Sanple e)draction/So*rlet d€thod

ConcentratdDiluteExtracted softlion

vFilter

Analysis by GC/MS

nirhsl6itspdBlsrdvroibsamprqtbd€d fr s6nrcFd6ndecsF i ; : J re t4 i . . ! r i l ' j ! . ; ! 1 { t , ; j i i l n i : rE i , l - , 1 l l r i + t t r ^1 \ i = f l : ' ' r ! 11 t4 'riii i"ii'Ja i. 'i'i.a u.,r. c"'eny &brd ,o s c6€6 cmdib* or snr.LiL" r-J ir"",j'"ai

"or.i o ims -a c*4"* t". et*

,"is",r,*i- "ae*aa"" "*i*r-a*mnrci,.:s*cr"nt "sr

sponsbrt sb ccie^randrhsd@ei."oe"^o"lg"*"*o,u"t"**.'"d;.d.ri,do@.*l-ndbe.s$o!ucedeic€p1.fu[wihodr.a"t o' |aLs i€6" d 'h" @i1ad d

. , r l l , ,4 i i r r l ; ' r . : . i6 " . , - , r +Jr r+ i ' r ' ! i+M10r '$ ' r r+s

Test ReportPOLYFIL AGOBERALLMENDSTRASSE

No.:CE/2011/84940 Date:.2011h21j

2OA, CH-6300 ZUG / SWITZERLAND

Pagei 6 of 7

lm[r[ ttlltl|]

Analytical flow chart of halogen content'1) tlarne of the person who rEde rEasurerpnt: Rita Chen2) lLarE of the person in chaee of fiEa6urefl€nt: Troy Chang

comtsiy 3r;tlri."i4 ,r 4i+;: rlait;.ri!r,!iir.a! -i-it++if.l.1\. Jrrr+.. ^:i.- lul!11.ft s 6ummr s Gsu6d by s6 coipa

p . f u b l y 6 l o 8 c l 3 n | a d | h i s @ mrbrldceidob oar 63 undr rh3 ra

,:iit(:: +gt rr/di1i+er@rae

Sanple prekeatrent / Separatbn

Weigtrting and putting sarple in cell

Orygen Bomb Combustion / Ab6orption

Dilution to fixed volufl€

Analysis was perfonyEd by lC

Test Report No. : CE/2011/84940 Date:2011h2J01 Page:7 ol7

f][Ilrt]tlltttt!POLYFIL AGOBERALLMENDSTMSSE 2OA, CH-6300 ZUG / SWITZERLAND

' The tested sample / part ls marked by an anow if its shown on tho photo. '

'* End of Report "

n $6 ron repon dd on y b rhe smdaG)rad* Th. b! @on enid b.qodcmp.ny+I:rllirql.nrirf;tllrSii;;ilrliirEii 1-lli5*11t{llr -i;:4 f!l:$rrl!'Th€d&.d..dby1h"c.'Fny&q.db6Gs66lcmdioBdssruceFnl€de€d6al.*a|abem6qtu €ktrd bmd &imstu strl

hi.ohbadd od m6 uid., u,. r.

r-d,,;r +!r l{!lii irlas6 Dtre

scsI

Test ReportPOLYFIL AGOBERALLMENDSTMSSE 2OA,

was/w6re submitted and identified by/on behalfofthe client as:

Validit nownForQueStiPlease Co ith scs

No. : CE/2011/84950 D e | 2011112101

CH€3OO ZUG / SWITZERLAND

Cu99.9MSn'1'14595

2011t1lt25201 1t11/25 rO 201I |1',01

Page: 1 or 7

rr|| [ltt!|||tlt[t

The following sample(s)

S€mple DescriptionBuyer/Order No.Sample Receiving DateTesting Period

lest Result(a) Plea6eefer to next page(s).

prqt iadsd Ds Gn ,epd eind bComFiy -r ,: !;t lLr. . . i ; l :r l i l l{ i l rt lrd r qti ' r^rl l i9i: l+,11\- em+,i , -,:r. ift",rl.

.ysuq8d b b cs€rcond rbns d ssubrd lo Tems ad cd@ l.l:

o n L y a i d w l h L n h . t m B d c | € d l n !

E d ftr|tld

clsnH L.Do'|b.t - Trhd

Test ReportPOLYFILAGOBERALLI\4ENDSTRASSE

T66i R.6ultls)

PART t.lAME No.1

No.: CE/2011/84950 Dale :2O114ZO1

2OA, CH63OO ZUG / SWITZERLAND

Page'.2 of 7

t I] t l

SILVER COLORED METAL WIRE (INCLUDING THE PLATING LAYER)

Te3t lt6m(s) Unit Method MDLR.3ultNo,l

Cadmium (Cd) mg/KgWith reterence to IEC 62321r 2008 andperfomed by ICP-AES.

n.d.Lead (Pb) mgKg 24Mercury (Hg) mS/kS n.d.Hexavalent Chromium Cr(Vl) With reference to IEC 62321: 2008 and

pedormed by Boiling \r€ter ext€ctionMethod.#

Negative

Sum of PBBS

mgikS With reference to IEC 62321: 2008 andperfomed by GC/MS.

n.d.Monobromobiphenyl 5 n.d.Dibromobiphenyl 5 n.d.Tribromobiphenyl 5 n.d.Tetrabromobiphenyl 5 n.o.Pontabromobiphenyl n.d,Hexabrcmobiphenyl 5 n.o.Heptabromobiphenyl n.d.Octabromobiphenyl 5 n.d.Nonabrornobiphenyl 5 n.d.Dec€bromobiphenyl 5 n .d .Sum of PBOEa n.d.Monobromodiphenyl ether n.d.Dibromodiphenyl ether 5 n.o.Tribromodipheny! ethe. 5 n.d.Tetrabromodiphenyl ether n.d.Pentabromodiphenyl ether n.d.Hexabrcmodiohenvl ether 5 n.d.Heptabromodiphenyl ether 5 n.o,Octabromodiphenyl ether n.o,Nonabromodiphenyl ether 5 n.d.Decabromodiphenyl ether 5 n.d.

eGlG{d rh s ied @d €nrclb Bpdcn€ry 'l+ !r ! rlrl . .n 1!ts,:r1,rtilr. ;l'!l* rrn . imri+Al'r-\r jrl4.f4! 1r€11hsdocmdssdby'h€c.mpany&bldlobcffi6|codibGo's*to. e.d'mc romal dmstu suq

d ^ t ' n d w l h L n h r m B d c r . d ! n d p o B d r t s t o G c s r a n d r h 3 d Mldrrgh6add]Ed'on6un6lh6'm

t',i!r: :d, dri:_ 11rs6rorPre

Test Report No. : CE/2011/84950 Date | 2011h21O1 Page: 3 of 7

tl]tIlltltfltttltPOLYFILAGOBERALLMENDSTRASSE 2OA, CH€3OO ZUG / SWITZERLAND

Test ltem(s) Unit method MDLResultNo.1

HalogenHalogen-Fluorine (F)(CAS No.: 14762-94-8)

mg/Kg With reference to BS EN M5A2,2007.Analysis was perfomed by lC.

50 n,o,

HalogenChlodne (Cl)(CAS No.: 22537-1s1)

50 n.d.

Halogen-Brcmine (Br)(CAS No.r 10097-32-2)

50 n.d.

Halogen-lodine (l)(CAS No.i 14362-44-8)

50 n.d.

Note :1. mg/kg = ppm : 0.1wf/6 = 1o00ppm2. n.d. = Not Detected3. MDL = Method Detection Limit4 - " - "=No tRegu la led5. '" = Qualitative analysis (No unit)6. # = a. Positive means the presence of CrVl on the tested areas

b. Negative mgans the absence of C l on the tested areasThe dgteci€d concentration in boiling-lvater-ext€ction solution is equalor greaterthan 0.02 mg/kg with 50 cm,tested areas.

7. The sample(€) was/wer6 analyzed on behalfof the applicant as mixing sample in one testing. The above result(s)was^^/€re only giv€n as the informality value.

'nrhstar€Fnd€f ontrorbsmpq3)Idd rhEbd,etsn6ndbGComFny f l t r , l r i 9 ! r . , r l i ] l : r r ! l { : : l : : ; l i ' ! i : l j i A r i i F -5 ! , [ 1 ' e t r ; ' f ' , , ' l ] l t ) [ l i 1 'n3dumd ts6su6d ' l hscomtsny5u*db t csccond1 t r sds

sib iv 6 10 6 o er 5d b6 @mntft,ltrrsandd odd3undrth€ta mol & €pdud depr 'n ju r, ftd

+l r l *J l : r (+s610r ) re t7e f +sitlfuirL!{:,r rr ir: i - i.hsror

IlF

Test Report No. : CE201'1/84950 OaL .2011h2,01 Pager 4

according to belo\ / flo /

POLYFILAGOBERALLMENDSTRASSE 2OA, CH63OO ZUG / SWITZERLAND

1) These sample6were da66olved totally by pre-conditioning methoda Cf' test method excluded )

Name of the pe6on who made measurement: Climbg€at YangName ofthe pe6on in charge of measurement: Troy Chang3)

ICP-AES

Sample Material Dige€tion Acid

S1eel, copper, aluminum, sold€r Aqua regia, HNO3, HCl, HF, HrO,

Glass HNO3/HF

cold, platinum, palladium, ceramic Aqua regia

Silver HNO3

Plastic H2SO1, HrOr, HNq, HCI

Othe.s Any acid to totral digestion

ii. irei,.or if *q oy t . cop-r " ,g .oo-maa"J ' * .6b i " - ' *dco^d ' * "6 .Edrcn ico@isbdM!os@]bi.*ddb" -'d l,nsdd 6 *,* i5r

*l iq:i";* @"* -;d.." **o.ooissr,s.ry - r"

"rd;^ a * -nd .

rtf:r:: r1lirtii+ 1l i s6 io,t,e tTe t r s lo:)2e 'r7 ffiar(om

Acid digestion by suitable aciddepended on difierent samplemderial (as belo\ , iable)

Micro\rave digestion with

HNO/HCVHF

Heat to appropriat€

temperature to e,\tract

Cool, filter digestate

through filter1) Alkal iFusion2) HCltodissolve

at 540 nm by UV-VIS

Test ReportPOLYFILAGOBERALLI\4ENDSTRASSE 2OA,

No. : CE2011184950 Oale'. 201 lh2lo1

CH43OO ZUG / SWITZERLAND

Page: 5 of 7

t l | l [ ] | | I t t | l

PBB/PBDE1) lllanE of the person2) MnE of the person

analytical FLOW cHARTwho nEde npasurenEnt: Ronran Wongin charge of nEasurenent Troy Chang

Scrcen analysis

" " " " " 1 " " " " " "

Sanple extraction/So*rlet rEthod

ConcentratdDiluteE)dracbd solution

First testing process -----t

Optional screen process -.--

Confinmtion process - .>

-s."pb---_-]--------r-------[S-r-tp]-j-a"arn"-_l-----r----

Ft ler

Analysis by GC/liS

cm€ry r r ' r j l j r ) t r . : r i l i " . : . l ! i * i , ; i i l ' r l t : e l . t i l : i l r t / . 1 \ ' l r Fn . r ' j : 1 . ' t l 6+

to €sd'o'c ramd dm6tu suq

d^t ,nd vihin rb rmis ot cr€d s i3'lbr.ohbadd€donsu.ddsera od b. repdued eiceol itul wiher

! idsnrzorNe-tu!acirrrer/*l:r/f,!.r +!!4J1i:irlre 02)r!e

I

Test ReportPOLYFIL AGOBERALLMENDSTRASSE

No. : CE/2011/84950 Daie | 2011h21O1

2OA. CH-6300 ZUG / SWITZERLAND

Analytical flow chart of halogen content

1) Name of the p€rson who lmde rneasuredEntr Rita Chen2) llan€ of the person in charge of nEasurerEdt: Troy Chang

Page: 6 of 7

comoad N]r]F,j!:ir.. I tiir lt{!l; ;]]rltl.1!- . r. irtsih-{} I 11 FiT . f!l r19i!+l

fi"JHl"l;liiii',i!',i.iwi;c"ry"';ti"-"c*""tc"t.^a sriu*-t i*n d..",; ''jbl.n bi... .d c.d*" 6, €. a " ' ' i i a - - o e , " a a . ^ * * ' ; . n b a d " i s d l b d i b m a i o ; d k . d h ;

; ; ; q ; ; ; ; oo ,4a t ; . : 6 . ? .€6@- -hsd ; "db . - "b1 .

r L - I I i d l L a i

Sarple pretreatrnent / Separation

Weighting and putting safipte in cell

Orygen Bomb Cofibustion / Absorption

Dilution to fixed volurne

Analysisw€s perfornEd by lC

Test Report No. : CE/2011/84950 D€te 2011h2101 Paget 7 of 7

tl] tlt II][]lPOLYFILAGOBEMLLMENDSTRASSE 2OA, CH63OO ZUG / SWITZERLAND

* The teeted sample / pa is maaked by an arrow if ifs shown on ih€ pholo. '

" End of Report -

€(s) r6rd Th€ r6d rop.n @nd b rccomtsry rirl,,iirar.rr'ir,'r,:111!!1, iilrRj:itr r.il1' l:!11.!-em+iI, ra r';)n:ll 'Thsih{.d"**dbylh6c"np.nysub'db6G4€Ejcond1bngo{sld ,M6.6al &dmsfu' sub]rendir,e'@ d ru d dbn s€s ibrh€! n reieds rhe cmp8.r's t ndn$ 3r rhe-y .d fu " t h " i . 6dc " " c ' * dDc . {5ny r ' j e cdnF i ys9s . s$;nshisandobroa,o3@do,rbta mdsrepd@sxepr'nlu.wM,sio,MtenaFro!3 drhecompanv a

T€st Report No. SHAEC1216714738 Date: 25 Sep 201 2 Page 1 ol5

ZHEJIANG ASIA GENERAL SOLDERING&BRAZING MATERIAL CO., LTD

XIHU INDUSTRIAL PARK, SANDUN, HANGZHOU CIry' ZHEJIANG, PROVINCE' CHINA

The following 6ample(s) was/were submitted and identified on behalf of the clients as : LEAD-FREE SoLDER

WIRE

SGS Job No. :

Part No. (PN) :

Compositlon :

Date of Sampl€ Received :

Testing Period :

Test R€quested :

Test Method :

T€st Resulb :

Condusion :

Signed for and on b€half ofscs-csTc Ltd.

sP12-028285 - SH

YTW2O6

sno.3Ag0.7ouce

21 Sep 2012

21 s,ep 2012 - 25 SeP 2012

Selected test(s) as requested by client

Please refer to next Page(s)

Please refer to next Page(s).Baa€d on the perfomed tests on submitted samples' the results of Lead'I\rercury, Cadmium, Hexavalent chomium, Polybrorninated biphenyls (PBB)'

Polybrominated diphenyl ethe6 (PBDE) comply with the limits as set by RoHS

Di.ective 201 1/65/EU Annex ll; recasting 200295/EC

/Qv''Fan Jingiie, JJApproved Signatory

.n#ffiffiirmr r* u-ra -td *vot rmrr.t.t t*

tirtDafi$EE|ihtltrorr zxtaoil.t.|.*f,Ertr€€.lt$l ll@3

tErEl@llitldt6!E{ti"clt06t'9 ffior*ofrxr.c+rti el Kr(,-tt)Eaffi 1j!ltor-

iLnlirotllt SOS Otbt4 (aGS 8A)

T€6t Report

Test Results :

Test Pert De€criotion ;

S@rn6n No, SGS Sampl€ lD D6ctiptioi1 SHA12-167147.035 Silvery wire

Rgmarks :(1) 1 mg/kg= I PPm=00001%(2) MDL = Method Deteclion Limit

(3) ND = Not D€teded ( < lrDL )(4) '-' = Not Regulated

RoHS DllBdivs 201 l/85/EU

Test Llethod

No. SHAEC1216714734 Date: 25 Sep 2012 Page 2 o15

with reference to lEc 6232 1 :2008(1) Determination of cadmium by ICP-oEs.(2) Dete.mination of Lead by ICP-oEs(3) Determination of Mercrlry by ICP-OES.(4) Determination of Hexavalent Chromium by Spot test / Colorimetric l\,ethod using UV-Vis(5) Detemination of PBBS i PBoES by GC-[IS.

Test ltem{s)

Cadmium (Cd)

Lead (Pb)

Mercury fig)Hexavalent Chromium (Ci(VD)

Sum of PBBSMonobromobiphenylDibromobiphenylTribromobiph€nylTetrabrornobiphenylPentabromobiPhenYlHe/€bromobiphenylHeptabromobiPhenylOctabromobiphenylNonabromobiPhenylDecabromobiPhenYlSum oI PBDESMonobromodiphenyl ether

Limit UlE l\rDL

100 mdkg 2

1000 ms/kg 2

1000 ms/kS 2o

1000 mS.ftS- mS/kS 5- mdkg 5- mdkS s- mSikS 5- mdks 5- ms/kg 5- mg/kg 5- mdkS 5- msikg 5- mdks 5

1m0 mgftS- mg/KS 5

Ij*tffib D.r. na co{d6 *r I ffi*,Hffi !#,g;"EHT* ###f g"fff ffi Stift Ufiffiffi:ffi

Sffi *ff rffi #ffi*,rx*$'#'ffi *lvl*sm.1m*ts""nr*

ND50ND

N€gativeNDNDNDNDNDNDNDNDNDNDNDNDND

;;bii*hEni-.6fr d tbtk r6tr.{.)r-H

tt-ErrlFYasft.cxd|lt.9|dlcrn zfrlr3 rd€6+1)6r.@ tElEF{lF6tlHit!-2l164@raa it{&aFl@+l -l|.*tr[lt|fte||6+l lr:2@

lr.nD.t o1$.8Gg OrouP (8cgs )

Tes{ Report

Test ltem(s)Dibromodiphenyl etherTribromodiphenyl etherTetrabromodiphenyl etherPentabromodiphenyl elherHexabromodiphenyl etherHeptabromodiphenyl etherOc-tabromodiphenyl etherNonabro.nodiphenyl etherD€cabromodiphenyl ether

thi!

t'ilt,b.aYrbto drchrbrd,Swaon !e3a+1

No. SHAEC1216714738 Date: 25 Sep 2012

UdT MDt @mdkS 5 NDmdkS 5 NDmdkS 5 NDmdkg 5 NOmS/kg 5 NDmSikS 5 NDmg/kg 5 NDmS/kS 5 NDmgkg 5 ND

I ErE {O-Zr)OtrOO*FA)ala@!.a

Page 3 of 5

raEFaFffiTl|{j{l.?J)6r@

Notes :(1) The maximum permissible limit is quoted from diredive 2011/65/EU, Annex ll(2) ospot{est:

Negative = Absence of Cr(Vl) coating, Positive = Presence of Cr(Vl) coating;CIhe tested sample should be fudher verifed by boiling-waterextraction method if the spot test resultis Negative or cannot be confirmed.)oBoiling-wateFextraction:Negative = Ahsence of Cr(Vl) coatingPositive = Pesence of Cr(Vl) coating; the detected concentration in boiling-water-ext€ction solution isequal or greater than 0.02 mgl(q with 50 cm'z sample surtace area.For corrosion protection coatings on metals: Information on storage conditions and produclion date ofthe tested sample is unavailable and thus results of Cr(Vl) represent status of lhe sample at the timeof testing.

M.m!.rorh.scsGtuc(acgs )

Test Report No. SHAEC1216714734 Date: 25 S€p 2012 Page 4 of 5

' l ' ;-;Ltidbd$rffi '-d6.h*lhE.,nrdri*6

ATTACHMENTS

RoHS Te€ting Flow Chart

1) Name of the person who madetesting: Jan Shi/Yoyo Wang/Allen Xiao/Gary xu2i Name of the berson in charge of testing: Jeff Zhang/George Xu/ Linda Liiiiii,"i !!rir!!,i. aissoried totarry 6'y pre-condit-roningherhod accorcting to berowflow chart. (Cf '

and PBBdPBDES test method excluded)

tr

Sample Prcparation

Sample Measurement

Acid digestion withmicrow€ve/ hotplate

Concentration/Dilution of extraclion

solution

'1) Alkali Fusion /DryAshing

2) Acid to dissolve

Adding 1,sdiphenylcarbazide

for colordevelopment

A red colorindicatesthe

presence of cP'.neceas€ry,confirm with

Pbrcd,Hg PB86fPBDE8

tilairl$gYb.rto dErloat4ltrtracnr 20(43fl..tjt.*Iqldl|6els+l a|lM

rEtE Fzr)0tac53l+{a-a)dlqaa

rE&&4lrsartjF.?1)6@

$6nb.fol th.ao6 GlDlD {8oas )

Test Report

Sample photo:

No. SHAECl2'16714738 Date: 25 Sep 201 2 Page 5 of 5

sHA12-167147.035

SGS authenticato the photo on original report only'* End of Report ""

(d-l!r. .Dor d6.ccil-iibhihr.ldcn.h,

' | l ! !a|i!!{ l |ddbd',td.lwb|||d4ded

tLlliDl! Bftfiufition 2dEs rElE[6-eDdag6l lElfF2l!ffia *6r*.&rr{&a1}ara@a ttF+lFN .,9d'rt.l.-tr.tl.*tr6l||,|rF|6r+l ll: @3

l|.fiDcrolm. SOS Gtu,D |SOSS ]

Test R€port No. SHAEC1216714750 Date: 25 Sep 2012 Page 'l ofs

ZHEJIANG ASIA GENERAL SOLDERING&BRAZING MATERIAL CO., LTDXIHU INDUSTRIAL PARK, SANDUN, HANGZHOU CITY, ZHEJIANG, PROVINCE, CHINA

Thg following sample(s) was/were submitted and identifed on beharf of the dients as : LEAD-FREE soLDERWIRE

SGS Job No. :Part No. (P/N) :Composition :Date of Sample Received :Testing Period :Te6t Requested :

Test Method :

Test Results :Conclusion :

sP12-028285 - SHYTWl02 (692s39-002)

Sn2.0CuRE21 9ep 2012

21 Sep 2012 - 25 Sep 2012Selected test(s) as requested by dient.Please refer to next page(s).

Please ref€r to ne\4 page(s).

Based on the performed tests on submitted samples, lhe results of Lead,Mercury, Cadmium, Hexavalent cfiromium, polybrominated biphenyls (pBB),Polybrominated diphenylethe6 (PBDE) compty with the timib as set by RoHSDireclive 2011/6yEU Annex ll; recasting 2OO2|95/EC.

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Signed for and on b€half ofscs-cgTc Ltd.

,z?r"'-Fan Jinqjie, JJApproved Sign€tory

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Test Report No. SHAEC1216714750 Date: 25 Sep 201 2 Page 2 of 5

Test Results :

Test Part Desciiotion :

Sp€oim€n llo. SGS Sampl€ lD Dcc,ipdon1 SHA12-167147.043 Sitvery wire

RemarlG :(1) 1 mgftg= 1 PPm=0.0001%(2) IVDL = Method Detedion Limit(3) ND = Not Detected ( < l\4DL )(4) "-" = Not Regulated

RoHS Dir€divo 201 1/85/EU

Test l\rethod: With referenc€ to IEC 6232'1:2008(1) Determination ofCadmium by ICP-OES.(2) Determination of Lead by tCp-OES.(3) Determination of Mercury by |CP-OES.(4) Determination of Hexavalent Chromium by Spot test / Cotodmetric Method using UV-Vis.(5) Determination of PBBS / PBDES by GC-MS.

Te6t ltem(s)

Cadmium (Cd)

Lead (Pb)Mercury (Hg)Hexavalenl Chromium (Cr(Vl))Sum of PBBSMonobromobiphenylDibromobiphenylTribromobiphenylTetrabrcmobiphenylPentabromobiphenyl

HeptabromobiphenylOclabromobiphenylNonabromobiphenylDecabromobiphenylSum of PBDESMonobromodiphenyl ether

!!!it Ud!10O mS/kS1000 mSikg1To 'nT

1000 mdkg- mgKg

mgKg- mgKg- mgKg- mg/Kg

ms/Ksmg/Kgmg/KgmS/kS

- mgKs1000 mdkS

- meyKg

l\4DL @32 N D2 1682 N DO Negative- N D

5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D- N D

5 N D

rn .dothr,$rLbhdtuFl

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c!dr-/. ndhl. .rtrrhd

h dr hi rPd Dt' cir b,h. rm, .b, hro .

.mb.r ol rh. scs Goup {8Gs€ }

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Test ReportTest ltem(s)

Dibromodiphenyl etherTribromodiphenyl etherTetrabromodiphenyl etherPsntabromodiphenyl elherH€xabromodiphenyl etherHeptabromodiphenyl etherOctabomodiphenyl etherNonabromodiphenyl elherDecabromodiphenyl ether

No. SHAEC1216714750 Datei 25 Sep 2012 Page 3 of 5

Lldl udtms/Ksmg/Kgmg/rgmS/kgmg/Kgmg/Kgmg/Kgm9Kgmdkg

upt555555555

a3NDN DN DN DNDNDNDNDNO

Notes :(1) The maximum permissible limit is quoted from directive 201 1/65/EU, Annex ll(2) "spottest:

Negative = Abs€nce of Cr(Vl) coating, Positive = Presence of Cr(Vt) coating;Cfhe tested sample should be further vedfied by boiling-wateFextraction method if the spot test resultis Negative or cannot be confirmed,)o Boiling-wateFextraction:Negative = Absence of Cf(Vl) coatingPosilive = Presence of Cr(Vl) coating; the detected concenhation in boiling-water-extraclion solution isequal or greater than 0.02 mg/kg with 50 cm. sample surtac€ area.For@rosion protection coalings on metals: Infofmation on sto€ge conditions and production date ofthe tested sample is unavailable and thus results of Cr(Vl) represent status ofthe sample at the timeof testing.

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Test ReDort No. SHAEC1216714750 Date: 25 Sep 2012 Page 4 of 5

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ATTACHMENTS

RoHS Tesflng Ftow Chart1) Name of the person who made testing: Jan Shi^/oyo Wangr'A en Xao,cary Xuz) N€me or tne person in charge of testing: Jeff Zhang/ceorge Xu/ Linda Lir) Inese sampres w€re dissotved tota v bv ore-conditioning method according to belowflow chart. (Cr6'

and PBBS/PBDES test method exctudedi

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Pb/Cd/Hg PBBs/PBDEs

Acid digestion withmicrowave/ hotplate Nonmetallic

matedal

1) Alkali Fusion /DryAshing

2) Acid to dissolve Filtration and pHadjustment

Adding 1,5-diphenylc€rb€zide


Addang 1,5-diphenylcarbazide


A red colorindicatesthe

pre6ence of cr6*. lfnecess€ry,confirm with

rd.r[f,t Ddod@nFr!. Thb drsrud d!.r b.6rmdr..d *ror 6 nrr,$,l.d N.ris,.4jwr d tn.c.ffiv

Urmllr ol |h. AgA elou! (gGS SA)

Test Report

Sample photo:

No. SHAEC1216714750 Date:25 Sep 2012 Page 5 of 5

sHA12-167147.043

SGS authenticate the photo on original report only

"' End of Report "*

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tErEF.e0E @ rEtE16*r)af5rr9Hj{t-aldlML fU0SAl)64e0

lrom!.r ol rh.8og Group (8G€S )




MYRA LV STEPHEN TSANG CHEMICAL LAB SENIOR MANAGER GENERAL MANAGER

PAGE 1 OF 9

APPLICANT: LITTELFUSE,INC. DATE: DEC 20, 2011 800 E. NORTHWEST HWY


SAMPLE DESCRIPTION: One(1) submitted sample said to be Sand. Part Description : Sand. Part Number : 311.7374.5000. Date Sample Received : Dec.14, 2011. Date Test Started : Dec.14, 2011. ***********************************************************************


**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 2 OF 9

1 (I) Test Result Summary :

Testing Item Result (ppm)

Halogen Content Fluorine (F) ND Chlorine (Cl) 230 Bromine (Br) ND Iodine (I) ND

Remarks: ppm = Parts per million based on weight of tested sample =

mg/kg ND = Not detected

Responsibility Of Chemist :Ken He

(II) Test Method:


Halogen Content With reference to EN 14582:2007 by combustion flask with oxygen and determined by ion chromatography

50 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample **********************************************************************

TO BE CONTINUED



TESTS CONDUCTED

PAGE 3 OF 9

(III) Measurement Flowchart:

Test For Halogen Content Reference Standard： EN 14582

**********************************************************************TO BE CONTINUED

add absorbent in a combustion flask & place weighed sample in equipment

fill the combustion flask with oxygen

ignite then leave the flask at room temperature

transfer the absorbent into a volumetric flask



analyzed by ion chromatography



TESTS CONDUCTED

PAGE 4 OF 9



Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 5 OF 9

Remarks: ppm = Parts per million = mg/kg ND = Not detected


(II) RoHS Requirement:

Restricted Substances Limits Cadmium (Cd) Content 0.01% (100ppm)Lead (Pb) Content 0.1% (1000ppm)Mercury (Hg) Content 0.1% (1000ppm)Chromium VI (Cr6+) Content 0.1% (1000ppm)Polybrominated Biphenyls (PBBs) 0.1% (1000ppm)Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)


TO BE CONTINUED



TESTS CONDUCTED

PAGE 6 OF 9

(III) Test Method:




2 ppm

Lead (Pb) content


2 ppm



2 ppm


With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)


5 ppm


DATE SAMPLE RECEIVED : DEC.14, 2011 TESTING PERIOD : DEC.14, 2011 TO DEC.19, 2011

**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 7 OF 9

(IV) Measurement Flowchart:


**********************************************************************

TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples




dissolved No




TESTS CONDUCTED

PAGE 8 OF 9

REMARKS:

*1: List of appropriate acid： Material Acid added for digestion


*2: If the result of spot test is positive, Chromium VI would be determined as detected. **********************************************************************

TO BE CONTINUED



TESTS CONDUCTED

PAGE 9 OF 9

**********************************************************************

END OF REPORT

BEIJING HYSTIC NEW MATERIALS CO,, LTD.

5 SHUANGYUAN ROAD, BADACHU HIGH.TECH ZONE,BEIJING,100041, cHtNA

Test Report

l\rodel No. :

Date of Sample Received :Testing Period :Test Requested :

Test Method :

Test Results :

Conclusion i

O\ N6'(

The following sample(s) was^^/ere submitted and identified on behalf of the ctients as : EpOXy ADHESTVE

SGS Job No. : TP12-004950 - TJ

EP6O8

3l Mat 2012

31 Mat 2012 - 09 Apt 2012Selecled test(s) as requested by client.

Please refer to next page(s).


Based on the perfomed tesb on submitted samples, the resutts of Lead,Mercury, Cadmium, Hexavalent chromium, Polybrominated biphenyts (PBB),Polybrominated diphenyl ethers (PBDE) comply with the limits as set by RoHSDirective 2011/65/EU Annex ll; recasting 2002/95/EC.

Signed for and on behalf ofscs-csTc Ltd.

No. TSNEC1200272601 Date: 09 Apr 2012 Page 1 of I

r 13t2?66233000 I l|t2ri5e95?52 {r*cr !$.ohr 136 266233000 r 136-?a2546?52 e s!.c\ia@6!3@

Aimy WangApproved Signatory

rh!do.!n'lt6!.d5ylh.con!.iy

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Memberol rh. SGSGolp{SGS SAI

Te€t Report No. TSNEC1200272601 Date: 09 Apr 20 1 2 Page 2 ol8

Test Results :

Test Part Description :

Sp€d.n€n No. SGS Ssmple lD D€6criplion1 TSN12-002726.001 ivory-white paste

Remarks :(1) 1mg/kg= 1 ppm = 0.0001%(2) IIDL = Method Detection Limit(3) ND = Not Deteded ( < MDL )(4) "-' = 1o1 q"nu,","o

RoHS Dirodive 201 t/66/EU

Test Method : With reference to |EC62321:2008(1) Determination ofCadmium by tCP-OES.(2) Determination of Lead by ICP-OES.(3) Detemination of l,rercury by ICP-OES.(4) Determination of Hexavalent Chrcmium by Colo metric Method using UV-Vis(5) Detemination of PBBS / PBDES content by GC-MS.

Test ltem(s)Cadmium (Cd)Lead (Pb)lllercury (Hg)Hexavalent Chromium (Cr(Vl))Sum of PBBSIvlonobromobiphenylDibromobiphenylTribromobiphenylTetrabromobiphenylPentabromobiphenylHexabromobiphenylHeptabromobiphenylOclabromobiphenylNonabromobiphenyl

DecabromobiphenylSum of PBDESMonobromodiphenyl ether

tinit Ud!100 mg/kg1000 mS/kS1000 mS/KS1000 mS/kS1000 mdks

- mg/Kg- mg/Kg- mg/Kg- mg-fts' mgKg- mgKS- ms/Ks- mg/kg- mgKg- m9x9

1000 ms/ksmg/Kg

sG s Madsioi Nc.41 .Tho slh Avenue T EoA,llan in, chiM 1l}a57s F . *lriE*fitrtte8lit641Cscs*l ffll: 300457

MDt 0p12 N O2 N D2 N D2 N D- N D

5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D

ND5 N D

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h,q!aoit" rc'rdn dr s.iod.d'

I 136 2aBA80CC | 0G42529s29 f,nqc'i!9s@rI {3f2r66?8806 l1e2?26&12 s sss.f'[email protected]

Membero, rbe SGS Group (SGS SA)

Test Report

Tost ltem(s)Dibromodiphenyl elherTdbromodiphenyl elherTelrab.omodiphenyl etherPentabromodiphenyl elh€rHexabromodiphenyl etherHeptabromodiphenyl etherOctabromodiphenyl etherNonabromodiphenyl etherDecabromodiphenyl elher

Notes :

No. TSNEC1200272601 Date: 09 Apr 2012 Page 3 of 8

trd!

(1) The maximum permissibte limit is quoted from directive 2011/65/EU. Annex lt.

Horebrpmocrrdododecane THBCDD)

Test lvlethod : With reference to IEC 62321:2008, anatysis was p€rfomed by GC-N4S.

udtms/Kgmg/KgmS/kSms/Ksmg/kgmg/Kgm9KSmgKsmgKs

UlitmgKg

MDt555555555

@1N DN DNDNDNDNDNDNDND

pp1N D

T€st ltem(s)Hexabromocyclododecane (HBCDD)

Notes :

Test ltem(s)Dibutyl Phthalate (DBP)B€nzylbutyl Phthalate (BBP)Bis (2-elhylhexyD Phthalale (DEHP)

Notes :

!d! MDt 0p1% (w4,,/) 0.003 ND% (ww) 0.003 ND% (Ww) 0.003 ND

MDI1 0

(1) Reference Information: Diredive 201 1/6S/EU recasting RoHS directive 200?J9S/EC:Hexabromocydododec€ne (HBCDD) is considered as a priority for riskevaluation and substancerestriclion.

Phthalatss

Test l\Iethod: With reference to EN14372:2004, anatysis was performed by co-tvts.

(1) Reference Infomation: Directive 2011/65/EU recasting RoHS directive 200295/EC:Bis (2-ethylhexyl) phthaiate (DEHP), Butyl benzyt phthatate (BBP) and oibutyt phthatate (DBp) areconsidered as a pdority for riskevaluation and subslance restiction.

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Test ReportResult shown is

No. TSNEC1200272601

of the total weight of wet sample

Date: 09 Apr 201 2 Page 4 of I

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Test ReDort No. TSNEC1200272601 Date: 09 Apr 2012 Page 5 of 8

ATTACHMENTS

cd/Pb/Hg/Cf'lPBB5&PBOES Flow Chart

Name of lhe person who made tesl ing: Aer0n Wang/Jason Li /Angel l Yao

Name ofthe percon in charge oftest ing: Cindy Yin/Rel ZhuThsse samples wsrs dissolved tolal ly by pre-condi l ioning melhod according to

below l low chari . (C16* and PBBS/PBDES test melhod excluded)

ill;l,ffi;i;lii'#:;' i;;;;i'-,iiiliir ii'iiii;'";l;;n *a ro 1t:.,.trere1"l:,11e191191':ll1"l:11*:::::L:11.,1:1:":i:YlTi."ii i i; ;ii; ;'. ti;;:'ii.c"npi'ivt or..p*rurv "tid."di^, ; rn! dod@dca'mri . '#li*lr,:*r";*iitikl.*ri:ni*l:"ll*t:iim::,ttiil:r:r.""i?i"::::'ii,llii:::lligiirliii:?';"'tiiii'i:il*"'

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Sample Preparation

Sample lVeasuremenl

Acid digest ion wi lhmicrcwave/ holplale

Sample solvent Adding digest ion reagent

Heating io 9tF95'C forextractionConcentral ion/

Di lut ion ofextract ions0iuIt0n

ResiduBSolution Fi l t ral ion and pHadjustmenl

1) Akali Fusion IDry Ashin g2) Acid todissolve

Adding 1 ,5'diphenylcarbazide fo!

coloi development

Fb/Cd/Hg PEB'PEDE5

Membero , lne SCS Group (SGS SA)

Test Report

ATTACHMENTS

' l ) Name ofthe percon

2) Nams of lhe person

No. TSNEC1200272601 Date: 09 Apr 2012 Page 6 ofB

HECDD Tosting Flow Chaft

who made test ing: Marine Sunin charge oftest ingr Rex Zhu

h'iii d*,n'n.&ij'd b i.rrs

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Mebberol rh6 scs Grouo (SGS SAI

Sample cutt ing/preparation

Sample measurement

Solvenl exhaction

ConcBntral iodDilut ion

Test Report

ATTACHMENTS

Phthalde Testng Floli, chaft

1) Nams of lhe pelson who made lest ingi Maina Sun

2) Name ofthe person in charge oftesl ing: Rsx Zhu

i,ffi{{ftf#,fii#jja!:i;'}'.f:rir"" lirid+s6s Ma nsion, No 41 ,Th. 5lh Av.n u. T EDA,llr.jl., ChlM 3Xr457 I l€6 2?)65:4q10 r 1!t2)25295252 slcir93@tr

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Mbfrberoilh6 SGs 6roup {SGs 5A)

No. TSNEC1200272601 Date: 09 Apr 2012 Page 7 of I

Solvenl exhacl ion

Conc entralion/Dil ution

Fihralion

Test Report

Sample photo:

TSN12-002726.001

SGS authenticate the photo on original repoionly

'*. End of Report '-

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Mehboror $€ scs GbuP (SGS SA)

No. TSNEC1200272601 Date: 09 Apr 20 1 2 Page 8 of 8

scs Malior.No 4l,rno 5h aleFJ. rEDA qan 'n chrB 3m'5'

+!.xt6e;r*iteEtt16llCscs*! {|:30q9l

Test Report

BEIJING HYSTIC NEW IVATERIALS CO,, LTD,

5 SHUANGYUAN ROAD, BADACHU HIGH.TECH ZONE,BEIJING.100041, cHtNA


The following sample(6) wasirere submitted and identified on behalfof the clients as : EPOXY ADHESIVE

SGS Job No. :

lvodel No. :

Date of Sample Received

Testing Pedod :

Test Requested :

Test lvlethod :

Test Results :

TP12-004950 - TJ

EP6O8

31 Mat 2012

31 Mat 2012 - 0g Apt 2012

Selecled test(s) as requested by client.



Signed for and on behalf ofscs-csTc Ltd.

o*) N-(Aimy WangApproved Signatory

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- i i n . " " . s " knnF i . 6 . * y

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M€mb€rol ths sGS G.ooP (scs sA)

Test RemrtTest Results :

Test Part Descdption :

Spodm€i No.1

Remarks :

No. TSNEC1200272602 Date: 09 Apr 20'l 2 Page 2 of 4

SGS Sample lD D€6criptionTSN12-002726.002 ivorv-whiteDaste

0 )(2)(3)(4)

1 m g / k g = 1 p p m = 0 . 0 0 0 1 %

[,lDL = lllethod Detection Limit

ND = Not Detected ( < IVIDL )'!" = Not Regulated

Halogen

Test Method : With reference to EN 14582:

Test ltem(s)Fluorine (F)Chlorine (Cl)Bromine (Br)lodine (l)

2007, analysiswas performed by lon Chromatograph (lC).

u!j!mg/(9mgKsmg/Kgmg/kg

MDt O@50 5750 755750 ND50 NO

Result shown is of the total weight of wet sample

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Test Report

ATTACHMENTS

1) Name ofthe percon2) Name ofthe psrson

No. TSNEC1200272602 Dater09Apr2012 Page 3 of 4

Halogen Testing Flow Chad

who made tesl ing: Angell Yaoin charge oflesl ing: Rsx Zhu

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Sample cutt ing/preparat ion

Sample measuremsnl

Combusl ion in oxygen bomb

Dissolv€d in an absorption

Analyzed by ionchromatography. Do!ble

conlim by other inslruments, ifnacessaty

Test Report

Sample photo:


TSN l2-002726.002

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SGS authenticate the photo on odginal report only

'*" End of Report ""'

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MYRA LV STEPHEN TSANG CHEMICAL LAB SENIOR MANAGER GENERAL MANAGER

PAGE 1 OF 9

APPLICANT: LITTELFUSE,INC. DATE: JAN 18, 2012 800 E. NORTHWEST HWY


SAMPLE DESCRIPTION: One(1) submitted sample said to be White yarn. Part Description : YARN. Part Number : 648901. Date Sample Received : Jan.11, 2012. Date Test Started : Jan.11, 2012. ***********************************************************************


**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 2 OF 9



Halogen Content Fluorine (F) 820 Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND

Remarks: ppm = Parts per million based on weight of tested sample =

mg/kg ND = Not detected

Responsibility Of Chemist :Ken He

(II) Test Method:


Halogen Content With reference to EN 14582:2007 by combustion flask with oxygen and determined by ion chromatography

50 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample **********************************************************************

TO BE CONTINUED



TESTS CONDUCTED

PAGE 3 OF 9

(III) Measurement Flowchart:

Test For Halogen Content Reference Standard： EN 14582

**********************************************************************TO BE CONTINUED

add absorbent in a combustion flask & place weighed sample in equipment

fill the combustion flask with oxygen

ignite then leave the flask at room temperature

transfer the absorbent into a volumetric flask



analyzed by ion chromatography



TESTS CONDUCTED

PAGE 4 OF 9



Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 5 OF 9

Remarks: ppm = Parts per million = mg/kg ND = Not detected


(II) RoHS Requirement:

Restricted Substances Limits Cadmium (Cd) Content 0.01% (100ppm)Lead (Pb) Content 0.1% (1000ppm)Mercury (Hg) Content 0.1% (1000ppm)Chromium VI (Cr6+) Content 0.1% (1000ppm)Polybrominated Biphenyls (PBBs) 0.1% (1000ppm)Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)


TO BE CONTINUED



TESTS CONDUCTED

PAGE 6 OF 9

(III) Test Method:




2 ppm

Lead (Pb) content


2 ppm



2 ppm


With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)


5 ppm

Polybrominated Diphenyl Ethers (PBDEs)


5 ppm


DATE SAMPLE RECEIVED : JAN.11, 2012 TESTING PERIOD : JAN.11, 2012 TO JAN.13, 2012

**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 7 OF 9

(IV) Measurement Flowchart:


**********************************************************************

TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples




dissolved No




TESTS CONDUCTED

PAGE 8 OF 9

REMARKS:

*1: List of appropriate acid： Material Acid added for digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected. **********************************************************************

TO BE CONTINUED



TESTS CONDUCTED

PAGE 9 OF 9

**********************************************************************

END OF REPORT

nov'TEST REPORT

NO.:4002E11121307-2R02 Oa!aiDec15,2o11 page 1 of4

Customer: Suzhou FuHong Electrcnic IndustfialCo, Ltd.Addrgs8: NO.89WEl DU ROAD, WANGTING TOWN, XTANGCHENG D|STR|CT, SUZHOU, CHTNAReport on th6 3ubmitted ssmple said io beSample name: Fusos copper shellllodol: /

Material: /D$cription: /Buyea: /supplier: /

Sa|nple recelved date: Dec.13,2011Tcatlng p€riod: Frcm Dec.13,2011 to Dec.15,2011

T€tino Reau6tedAs specined by client, to delermine the L€ad, Cadmium, Mercrry & Hexavatent Chrcmium content in the submitted sampte inaccordance wilh Direclive 2002/95/EC (RoHS).

Tcstind method:

Testing llem [,leasudng inslrument MQL

Lead (Pb) EC 62321: 2008, seclion 9 ICP-OES 2mglkg

cadmium (Cd) EC 62321: 2008, section I ICP€ES 2 mg/kg

Mercury (Hg) EC 62321r 2008, section 7 rcP-oEs 2 mg/kg

Chrom'um (Cr l'I) EC 62321:2008, Annex I 0.02mg,a(g'

ILS, PLEASE REFER TOTHE FOLLOWING PAGE(S)'**'

lsg-'0.02 mg/kg returs 10 lhe MQLofsample extEction tiquid.

99!s!.c!i9!j-ffien tesied as specifred the submitted sample complied with the requircments of commission Decision of 18 Aug 2005amending Directive 2002l95/EC nolified lnderdocument 2005/618/EC

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S}'EI{ZN€N AOV TGSTING T€CHNOlOGY CO.,L'D.KUNSHAN EiANCH Hotllne86-512-5510 8000

6novNO.: 4002E11121307-2R02

TEST REPORT

Add the digestion solution; thevessel is heated Lrntil lhe sampl€ Add HrO, u nlil the sampl€ is clear

F;;1.-F;;,",..;-1.-{Melal subslrat€)

Add lhe digestion solution, clos€

the macrowave vess€|.

Cooling the vessel, fllleri washed and

filled to the mark with distilled water.

The sample is digested in the

micrcwave oven following a specific

decomposilion program.

and l\rercury Content: (Praring)

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I to the mark with Dtwater I I r*r.r*t | | -.- |

STIENZH€N AOV TESIING T€CIII{OLOGY CO.,lIO,KUII9HAN BFANCH

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Hotline86-512"s510 8oO0

Cooling the vessel, filter washed and

filled to the mark with distilled water.

Remove the sample, and coollhe beaker lo rcom tempefalure,and do 1ie color reaction

Heal 50 mL ofDlwaterin lhe

beakerto boiling for 10 min

Test the sample solution and lhe 0.02mg/kg standard solution by UV-VIS.

To Detemine

nov.NO.: 4002E11121 307-2R02

5. To Detemine Hexavalent Chromium- '' ',.'1re$eo ovr I r

s.t sw-resi (M&

TEST REPORTDate: Dec.15, 2011

Contentln colorless and colored ctlromate coaling on

Page 3 ol4

metals: (Plating)

lflhe lest resull is positive,

the sample is considered 1o

have hexavalenl chromium

and the 0.02 mg/kg

Boiling- waieF extractionprocedure shall be used to

lfthe€ isrnterference orI rs hard to decide *terhellhe sample have the hexavalent chrcmium

5 2 Boiling- wEter- en€ction

Take the (5015) cm'z

sample in the beaker.

Srmple d93cription:

SH!NZHEN AOV TESTING TCCTNOIqGY CO.,L}D,KUNSHAN BFANCH nHot l ine86'512^5510 8000

Remove he sample, and cool

lhe beaker 1o room temperature,

and do the color reaction

Heat 50 mlof Olwater in the

beaker lo boiling for 10 min

Test the sample solution and the 0.02

mg/kg standard solution by UV-VIS.

Copper shell subslrateLead wle Platrng 24 Copper shell Plaling

Unil RoHS

Limit 2-3 24"Lead (Pb) mg/Kg 1000 N.D. 2.5 40.0 N.D.Cadmium {Cd) mg/kg 100 N,D. N.D. N.D. N.D.Msrorry (Hs) mg/kg 1000 N.D, N.D, N.D. N.D.Chromium (Crvl) mg/Kg 1000 Negative Negative Negalive Negative

nov.TEST REPORT

NO.r A002E11121307-2R02 Dat€iOec15,2011

-The new RoHS di.ective 2011/65/EU, on Jul 21, 2011 come into force, on Jan. 03, 2013 the fomat imotementation. Dircctive

2002l95/EC shall be reoealed simultaneouslv.

Sp€cim€ns, wnicn requested to determine Lead, Cadmium and l4ercury Conlent, have been dissotved comptetety.-mg/kg=ppm

-N.D.=not detected(<tVoL)-MQL=l'rethod Ouaniilation Limit-Negalive=Abs€nce of Cr (VI);

Posilive=Prcs€nce of Cr (VI)i

Uncedain= c€n noi ve fy whether the sample have Hexavat€nt Chrcm ium by spoliesl.(The tested s€mple should be furlher venfed by boiling-waterextradion method if the spol test result is uncertain or

-'The test is based on the following assumption:The sampte ptating is a singte tayerand each pad is unifom. The test resuttmaybe cannol sland ior rhe physicartruth of sample plating.

Photog.aph ofSample

"'End of Repod"'

S'iE'!ZH€N AOVT€STING TECXNO!OGYCO..lIO,KUNSHAN ABANCH

Hh,:/fuloi6n nHotline86-512-5510 8000

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