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    Int. J. Rapid Manufacturing, Vol. x, No. x, xxxx 1

    Copyright 200x Inderscience Enterprises Ltd.

    Design development and functional validation of aninterchangeable head based on mini screw extrusionapplied in an experimental desktop 3-D printer

    Zilda de Castro Silveira*and Matheus Stoshy de Freitas

    Engineering School of Sao Carlos,

    Department of Mechanical Engineering,

    University of So Paulo,

    Trabalhador sancarlense Avenue,

    No. 400, Sao Carlos, S.P., 13566-590, Brazil

    E-mail: [email protected]

    E-mail: [email protected]

    *Corresponding author

    Paulo Inforatti Neto, Pedro Yoshito Noritomi,Jorge Vicente Lopes da Silva

    Renato Archer Center of Information Technology CTI,

    Campinas, Rodovia Dom Pedro I(SP 65),

    Km 143.6, 13069-901, Brazil

    E-mail: [email protected]

    E-mail: [email protected]

    E-mail: [email protected]

    Abstract: In this work is proposed the conceptual and preliminary design aswell functional validation of a head based on fused deposition modelling(FDM) technology using mini screw applied to experimental 3-D printer(Fab@CTI machine). The polymer Nylon 12 and the biopolymer -PCL(-policaprolactone) in powder form were used to design the barrel-screw anddrive system set-up. The proposed head demonstrated the functionality to carrythe powder material through the variable sections of the screw extrusion andhas generated Nylon filaments with diameter of approximately 0.7 mm withthe tip of 0.4 mm. The morphological characteristics of these filaments wereobserved in scanning electron microscopy (SEM) confirming the mixing of thepowder, generating continuous filaments and structured parts. SEM tests were

    made with -PCL using material generated from the feed to compression zonesof the screw extrusion head allowing the visualisation of the adhesion of thegrains in feed section and the complete mixing in the compression zone for the-PCL.

    Keywords:desktop 3-D printer; rapid manufacturing; FDM; fused depositionmodelling; design methodology; material reuse; polymer; process control.

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    2 Z.C. Silveira et al.

    Reference to this paper should be made as follows: Silveira, Z.C.,

    Freitas, M.S., Inforatti Neto, P., Noritomi, P.Y. and Silva, J.V.L. (xxxx)Design development and functional validation of an interchangeable headbased on mini screw extrusion applied in an experimental desktop 3-D printer,Int. J. Rapid Manufacturing, Vol. x, No. x, pp.xxxxxx.

    Biographical notes:Zilda de Castro Silveira is Professor of the Department ofMechanical Engineering of the Engineering School of Sao Carlos, Universityof Sao Paulo. She obtained DSc title in 2003 from Faculty of MechanicalEngineering, State University of Campinas (UNICAMP), Sao Paulo Brazil, inthe area of Mechanical Design and Solid Mechanics. She obtained the MSc titlein 1999 from Engineering School of Sao Carlos, University of Sao Paulo, in theMechanical Design area. Her researches areas included: design methodologyand numerical optimisation related to development of devices and machinesapplied to additive manufacturing and health area; theoretical and experimentalstudies of the aerostatic ceramic porous bearings applied to ultraprecision

    machines and development of the numerical models applied to bonere-modelling.

    Matheus Stoshy de Freitas is Masters degree (MSc) of the Department ofMechanical Engineering of the Engineering School of Sao Carlos, Universityof Sao Paulo (USP). He obtained a Bachelors degree in MechanicalEngineering at the same institution. He is a researcher in CTI acting thetheoretical and experimentally studies of mechanical solutions applied toadditive manufacturing.

    Paulo Inforatti Neto is graduated in Computer Engineering, has Masterin Mechanical Design at School of Engineering of So Carlos of the StateUniversity of So Paulo (EESC/USP), working with additive manufacturingresearch topics. Currently he is project manager by FACTI at the ThreeDimensional Technologies Division at the Renato Archer Information

    Technology Center (DT3D/CTI) coordinating applied researches indevelopment and using of additive manufacture technology to non-conventional applications, mainly in oil and gas research.

    Pedro Yoshito Noritomi is graduated in Mechanical Engineering, has Masterand PhD in Computational Mechanics at Campinas State University(UNICAMP) working with bioengineering research topics. Currently he isresearcher at the Three Dimensional Technologies Division at the RenatoArcher Information Technology Center (DT3D/CTI) coordinating thebioengineering initiative of the division and using his expertise incomputational modelling and simulation applied to other demand, mainly in oiland gas research.

    Jorge Vicente Lopes da Silva is a PhD in Chemical Engineering, MSc inElectrical Engineering and BSc in Electrical engineering. He created andcoordinates, since 1996, the Three-dimensional Division at CTI Renato Archer.Under his supervision this division develops application and research projectswith industry and universities in Brazil and abroad. He is member of manyscientific committees and invited speaker of the most relevant conferences inthe area of 3D printing.

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    Design development and functional validation 3

    1 Introduction

    Recently, there was an increasing development in rapid prototype technologies as well as

    a real perspective to use additive manufacturing in the area of health, with highly

    complex geometries, specifically the ones of tissue and bone engineering. The term rapid

    prototyping (RP) a.k.a additive manufacturing, is widely used in industry to describe the

    process to rapidly create a system or a component in a stage just before the final product

    or before commercialisation. The American Society for Testing and Materials (ASTM)

    define Additive Manufacturing (AM) as the process of joining materials to make objects

    from 3-D model data, usually layer-upon-layer, as opposed to subtractive manufacturing

    (ASTM, 2010) without the need of conventional process planning as used on machining

    or conformation processes. Commercial AM machines generally need a high quantity of

    material to start working and build parts; additionally there are operational constraints

    settings and they are configured to use proprietary materials from the suppliers andmanufacturers. These constraints hinder advances in research areas that include materials

    development and process. By these conditions, it becomes interesting the development of

    technologies in open source 3-D printers with reduced dimensions, due the small

    quantities of feedstock and more freedom towards the software and hardware

    development. Another motivation for this work is the increasing market related to

    desktop 3-D printers, with a crescent number of brands using different materials and

    techniques of deposition. The most common technologies used in desktop 3-D printer

    included: the fused deposition modelling (FDM) commercial processes consider the raw

    material as thermoplastic material fed in the form of a flexible filament rolled in a coil.

    The filament is guided into the head by a device controlled by integrated numerical

    command, where pulleys are responsible for feeding wired material and pushes it into a

    heated channel, causing it to melt and to be extruded through a nozzle in the opposite end

    of the channel. Other technique uses the extrusion by a syringe which occurs by the

    compression of the material within a deposition chamber and the subsequent extrusion of

    this material through a needle. Any of these processes, coupled to a (x,y,z) controlled

    displacement system enables prototyping 3-D models (Gibson et al., 2010). In the case in

    study, the development of a screw extrusion head, the material enters in a powder form in

    the superior part of the device, being carried to the lower parts getting melted in the way

    by the use of a tubular resistance acquiring a continuous and viscous consistence enabling

    its extrusion through a nozzle tip in the end of the process. The success or fail in this

    process rely in the capacity of producing continuous filaments that can be deposited in a

    3-D printing platform permitting the construction of parts. In the case of using

    biomaterials it permits the fabrication of scaffolds that can be defined as a temporary

    porous structure used to promote cells growth where its function is to allow a structural

    support to the formation of new biological tissues (Ikegami, 2007). The goal of thiswork is to present the design development and functional validation of an interchangeable

    screw extrusion head with variable section to be used in a desktop 3-D printer based on

    FDM approach. It was made a calculation methodology for the extrusion screw and

    transmission system. A validation of the conceptual design for industrial and biomaterials

    applications, respectively, were carried out using polyamide (Nylon 12) and -PCL

    producing continuous filaments and entire parts. The SEM analyses were made with

    these materials and the results presented morphological characteristics appropriated to

    polymer structure extrusion used in additive manufacture purposes.

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    4 Z.C. Silveira et al.

    2 Considerations about extrusion process

    The choice of the conformation method used in a specific polymer depends on

    some factors, as the choice of the polymer, geometry and size of the final part. In the case

    on a thermoplastic polymer, the rheological properties (flow curves, melting point),

    operational temperature, cooling time after the process should be considered, in the case

    of a thermofix, its considered the temperature and curing time. The temperature or

    melting point describes the phase transformation of a crystal solid for a liquid. According

    to Chung (2000) the melting point term is used only for crystalline polymers, because

    amorphous polymers without crystallisation do not present the same melting point

    (it can occur up to Glass Transition Temperature (Tg), for amorphous thermoplastics

    polymers). Chung (2000) describes the melting process as a change in solid/

    liquid behaviour in amorphous or semi-solid polymers. According Rauwendaal (2001),

    the polymer processing in extruders involves the use of any kind of solid material fed tothe extrusion screw, which is melted and carried by the screws rotation until the end of

    course. The designs of a single or double extrusion screw are the most common

    configurations in industrial polymer processing.

    There are many mechanisms used to pump liquids with low and high viscosity.

    According to White and Potente (2003) for highly viscous liquids usually two different

    principles are used:

    positive displacement pumps, where the fluid fills enclosed chambers and is moved

    forward by the mechanical movement of the parts of the machine (ram extruder in

    processing of thermoplastic)

    drag flow pumps, in this case the fluid fills a region between two surfaces, where one

    is in motion.

    The relative movement of the two surfaces drags the fluid along a channel, gradually

    pressurising and forcing it through a die. The second mechanism has some technical

    solutions developed along the years, but the simplest machine is the drum flow pump or

    drum extruder invented by Gabrielli (1952) apnd White and Potente (2003). In this

    machine, the material to be pumped is put on an annular space between the rotating drum

    and surrounding barrel. The rotation of the drum carries the liquid to a position where

    there is a wiper bar that diverts the liquid into the die. The die pressurises the liquid and a

    pressure gradient develops along the length of the channel between the drum and the

    barrel. A complete study about behaviour of extrusion processes involve an estimative on

    thermo-physical parameters, mainly related to screw, where its geometry, polymer

    rheology, and processing conditions must be considered. Breaux et al. (2009), Chung

    (2000) and White and Potente (2003) describe the extrusion process to a standard singlescrew extruder into three zones related with screw design. The performance of an

    extrusion process can be improved substantially by optimisation of the screw design.

    Summarising, the screw performs three basic functions:

    solid conveying function

    melting function

    metering or pumping function.

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    Design development and functional validation 5

    In most applications, these three functions occur simultaneously along screw length and

    they are strongly interdependent. The size of a screw is described by its diameter andlength or length-to-diameter (L/D) ratio. Chung (2000) used geometrical names to the

    three different sections:

    Feeding section at the hopper end with a constant, deep channel depth called

    feeding depth. In this region conveying of a solid bed from compacted pellets

    occurs. Pressure increases steeply along the screw but cannot reach high values in

    smooth barrel extruder without the phenomenon of melting of the superficial layer in

    contact with the barrel hence releasing any extra pressure.

    Metering section or pumping section at the die end with a constant, shallow channel

    depth called metering depth. Breaux et al. (2009) define this zone as delay

    where the molten film of polymer increases in thickness and possibly permeates the

    solid bed itself. This condition occurs at the end of the feed zone of the screw. A compression section (or transition section or melting section) between the feeding

    section and the metering section with a decreasing channel depth.

    In this region occurs the melting process, when the melt film has increased up to a point

    where it runs through the solid bed of ever decreasing width as presented in Figure 1.

    Breaux et al. (2009) identify a forth section in the direction of the end of the

    compression zone and in the metering zone the solid bed is completely melted and there

    is melt conveying only. Throughput in the conveying zone is the combination of screw

    rotation that provides the drag flow and the pressure gradient in the screw channel. When

    the pressure gradient is positive it blocks the drag flow, while it promotes the flow when

    it is negative. Throughput is constant along the channel, while pressure development start

    from atmospheric pressure and ends at back pressure imposed on the screw in the case of

    injection moulding, or at atmospheric pressure at the die exit in the case of extrusion. For

    the extrusion process, the level of back pressure is the result of the combination of die

    and screw.

    Figure 1 Processing zones to a single screw

    Source: Adapted from Manrich (2005)

    It is important to realise that conventional extruders have large dimensions compared

    with the device developed in this study. With the intention of built a functional device

    with the same capabilities of a conventional extruders, but with reduced dimensions,

    developed concepts and methods for these industrial extruders where used and based on

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    6 Z.C. Silveira et al.

    these, a calculation methodology was made. With this calculation methodology it was

    proposed the verification, dimensioning and choosing of the main components as screwextrusion, stepper motor, worm gear and barrel. The vertical configuration designed to

    the screw extrusion head allows better use of space design as well as the arrangement of

    the drive system.

    3 Case study

    For a desktop 3-D printer an alternative and interchangeable head design the users

    requirements and technical characteristics were defined:

    Raw materialrelated to the use of different forms (pellets, powder, solids) and

    in reduced amount. In bioengineering applications the use of powder material to

    generate prototypes is highly indicated due to commercial availability. The use ofpowder raw material is common in the polymer industry, especially in injection

    and extrusion moulding. In non-commercial AM machines, specifically desktop

    3-D printers, the solutions found are: syringe injection (Malone and Lipson, 2007),

    thermoplastic filament extruder (Inforatti Neto et al., 2012) and transport extrusion

    system for previously melted biopolymer (Almeida et al., 2008); all of them on open-

    source design.

    Operational performance, related to flexible platforms, reduced dimensions, again

    use of different raw materials and low cost. In commercial machines, technical

    solutions are protected by patents included control systems and combined

    mechanisms, making the purchase price of the machinery and raw material, as well

    as the cost of maintenance is too high and even unfeasible to non-industrial users.

    In this way, a new branch from Fab@Home, named Fab@CTI 3-D printer, showed

    in Figure 2(a) and (b), offer low cost, open platform to the assembly of a mini screw

    extrusion head based on FDM deposition technology.

    Figure 2 (a) Fab@CTI desktop 3-D printer and (b) syringe head extruder and fused depositionmodelling head (see online version for colours)

    (a) (b)

    Source: Inforatti Neto et al. (2012)

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    Design development and functional validation 7

    The Fab@CTI 3-D printer platform was designed from of the following demand:

    definition of the application demand: tissue engineering (production ofscaffolds)

    and small mechanical components

    utilisation environments:research laboratories including research centres and

    universities

    machine volume:460 410 470 mm

    mass: 2550 kg.

    Inforatti Neto (2013) presented a technical design feasibility of the mini screw with

    variable section head. The users requirements composed by users researcher were raised

    at design phase and obtained from quality function deployment (QFD) analysis described

    in Cheng and Melo Filho (2007). The list of users requirements was translated into

    technical characteristics which supports the constructive solutions choice to mechanical

    design of extrusion mini-head. The most important users requirements identified by

    QFD were:

    powder as raw material

    continuous feeding and process control

    low quantity of materials (adequated to the behaviour of the research demands)

    reuse of polymer power from commercial additive manufacturing machines

    filament modelling raw material to the use in FDM head (Fab@CTI)

    interchangeabale tip nozzles.

    The -PCL was the biomaterial chosen for the device trials and this material is related to

    other previous studies (Rezende et al., 2012; Inforatti Neto et al., 2012) in the health

    area. The choice of the polyamide is related to the reuse of material discarded

    from commercial machines. In this case, the availability of the material in the laboratory

    (CTI), in its non-degraded and degraded form, result of previous prototyping processes

    by selective laser sintering (SLS) and second, its wide use in industrial parts.

    4 Development of conceptual design

    The conceptual design uses the technical requirements which are identified as having

    greater importance in the phase before (informational design). There are some which

    have the objective to proportion a technical system to be understood as functions of thedesign subsequently related to technical items or components, and, on a higher abstract

    level, find innovative solutions or just improvements of technical solutions. The outcome

    of this step for the preliminary design is one or more sketches of technically viable

    solutions. For the development of the mini-head design of extrusion functions of

    technical developments of the head and of the structure material functions technical

    elements inside the 3-D printer system were extracted, which is presented in Figures 3

    and 4, using one of the engineering techniques of systems that relate Energy (E); Material

    (M) and Signal (S).

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    8 Z.C. Silveira et al.

    Figure 3 Material-energy-signal flows to a 3-D printer

    Figure 4 Material-energy-signal flow to the deposition mini-extrude head

    Inside the technical system 3-D printer, the production of the prototype piece is the

    principal function of the machines engineering design. In Figure 7(b) the production

    process of the piece is detailed, and for each described function, decisions of the design

    should be made based on conventional and alternative solutions which contemplate

    restrictions of this design, as there is the heads weight in relation to the machine,

    reduced spaces, and portability and low costs. Thus, starting from the information

    obtained with the QFD, a set of the designs parameters was chosen to find technical

    solutions. To organise the choice of solutions a morphologic picture was mounted,

    presented in Figure 5.The first option of technical solutions is presented by the arrows, to attend the

    designs restrictions described beforehand as shown by Table 1.

    The choice of the deposition material in the form of powder was made in function of

    its availability on the market and the possible mixtures with additives and other materials.

    The step motor to start the head was chosen for its control facilities and adjustment

    beforehand tested with the systems of injecting by syringe and filament.

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    Design development and functional validation 9

    Figure 5 Morphologic analysis

    Table 1 Partial value analysis to the extrusion head

    Components Design functions Partial cost (U$) Percentage

    Structure Support head set-up 363.10 16.6

    Barrel Extrusion screw housing 335.19 15.4

    Extrusion screw Transport, melting and homogenise thematerial

    837.98 38.5

    Stepper motor Supply energy/power to transmissionsystem

    90.50 4.14

    Gearbox Reduce the velocity and increase the

    screws torque

    335.19 15.3

    Microtubular resistance Heat the extrusions material 111.73 5.12

    Temperature sensor Measure the temperature 18.44 0.84

    Nozzle Deposit the material 16.75 0.77

    Mechanical coupling Join the shafts 33.52 1.54

    Thermal blanked Isolate thermally the head set-up 22.35 1.02

    Ball bearings Support shafts and friction minimisebetween elements

    22.351.02

    Total cost 2187.1 100

    The heads structure will be interchangeable to couple with other processes of deposition

    (Inforatti Neto, 2007; Inforatti Neto et al., 2012). A big part of the fixation done

    together with screws, mainly due to the easiness with which they can be bought,

    mounted, and subsystems can be maintained. In this first study, the extrusion will be

    made with a simple screw to test the concept of extrusion in the deposition process, so the

    polymers thermal effects in the cylinder part of the screwof the materials chosen, the

    easiness of assembly and manufacture can be studied. The die of extrusion is

    interchangeable to enable diverse diameters of the thread of material when exiting the

    machine. So, different resolutions and superficial finishings of the piece are possible.

    The feeding of the material is done by gravity using a mixer consisting of a rotating shaft

    coupled to the screw during the feeding phase to avoid the compression of the material.

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    10 Z.C. Silveira et al.

    The raw-material for the extrusion is made of polymers and was chosen because of it is

    so easily manipulated in the extrusion process. The mechanism of heating up will becarried out by electric resistances because they can be wrapped around the external

    cylinder in the extrusion process to guarantee controlled heating throughout the whole

    process of extrusion. On the basis of the data provided by the suppliers and our own data

    on estimates for the Fab@CTI printer an initial estimate for the costs of the extrusion

    head was made, presented in Table 1. The analysis of the value has the purpose to

    estimate the costs of each one of the components as well as their functions making it

    possible to analyse the economic impact of each part of the head more precisely. This is

    because of the choice of the material of the screw: titanium alloy (changed by stainless

    steel) for the extruder and the difficulty to find a commercially produced screw with the

    required dimensions (~150 mm long and 7 mm in diameter). With the procedures

    adopted, the conception design and the initial costs (based on Value Analysis Technique)

    of the head were estimated and are represented in Table 1, and an outline of the technicalsolution for the extrusion head is presented in Figure 6.

    Figure 6 Schematic view of extrusion head

    5 Calculation procedures

    With the aim to ensure strength and performance required, calculations to define the

    geometries of the extrusion screw and barrel were done. Calculation procedure was based

    on technical literature of standard industrial extrusion screw. A functional prototype was

    fabricated and assembled. From the theory described in item 4, were obtained the main

    design parameters of the barrel-screw and actuation system. Usually, the screws are not

    subjected to a high bending force because they run inside a strong rigid barrel and the

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    Design development and functional validation 11

    clearance between screw and barrel is small, around 0.00050.002 (White and Potente,

    2003). The small gap between screw and barrel prevents solidification by cooling of themelt. Leakage flow caused by the clearance between the inner barrel and screw flight

    reduces the melting efficiency also. Then, the manufacturing process of extrusion screw,

    in this case, must have high precision. The critical strength requirement is mechanical

    resistance to torque that is very dependent of polymerics material type. In this step, a

    pre-calculation was made considering some geometric and fluid characteristics to the

    mini screw as well as the head extruder. In this step, calculations were made considering

    some geometric and fluid characteristics to the extrusion screw as well as the head

    extruder in general. The flowchart presented in Figure 7(a) shows a simplified sequence

    of calculations applied in a single screw extrusion head to a portable 3-D printer

    (Fab@CTI). The procedure of the calculation was based on Rauwendaal (2001) and

    Chung (2000).

    The transmission system chosen was a gearbox (worm gear). This first choice hasconsidered the high transmission ratio as well as the space restrictions. The polymers

    viscosities were considered to selection of the stepper motor and those are directly related

    with power and torque characteristics represented in Figure 7(b).

    Figure 7 (a) Flowchart related to calculation procedure and (b) design parameters to choice of thegearbox (see online version for colours)

    (a)

    (b)

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    12 Z.C. Silveira et al.

    Nylon 12 was the first polymeric material used to obtain some important materials

    properties such as the relationship: shear rate and linear velocity. Polyamide (Nylon 12)is a semi-crystalline polymer which is highly hygroscopic and because of this

    characteristic it should be taken to a greenhouse with air ventilation, before being

    processed. Its processing temperature is higher than 240C, having a melting temperature

    in a narrow range and oxidises easily when exposed to hot air and it presents low

    viscosity after being fused. With these properties this material needs a dosage zone with a

    constant shallow canal, to avoid fluctuations due to its low viscosity. The control of

    polyamide viscosity in different extrusion velocities, rheometry analysis of virgin and

    degraded materials were considered and the objective was the determination of

    rheological curves of these samples at 225C. From the rheometry analysis it was

    possible to observe the shear strength of the non-degraded polyamide is significantly less

    than the degraded one, probably due to the thermal and mechanical solicitation, which are

    suffered in previous processing, this information are available in Inforatti Neto (2013).This means when leaking, through the extrusion process the non-degraded polymer offers

    less resistance to shearing, and therefore needs less energy in the activation of the

    extrusion screw to flow along the extruders body. However, the rheometry analysis

    indicated a higher resistance in the case of -PCL shearing and thus, calculation of the

    gearbox was based on the torque moment of -PCL. Figure 8 presents the input design

    data and calculated design parameters.

    Figure 8 (a) Main input and output design parameters and (b) AISI stainless steel 304for mini-screw (see online version for colours)

    (a)

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    Design development and functional validation 13

    Figure 8 (a) Main input and output design parameters and (b) AISI stainless steel 304

    for mini-screw (see online version for colours) (continued)

    (b)

    6 Detail design: mock-up and functional prototype

    The screw extrusion design presents three sections and it was developed considering

    mechanical strength to the torque caused by the turning into the viscous melted polymer

    material. The mixer in the feed section was proposed to avoid the caking of the powder

    material which would cause the locking of the screw and bubbles formation in the

    polymer material. Figure 9(a) presents a mock-up of the constructive solution for

    extrusion head and Figure 9(b) presents the functional head assembly stand alone for

    preliminary experimental tests.

    Figure 9 (a) Mock-up and (b) functional mini screw head (see online version for colours)

    (a) (b)

    7 Preliminary experimental tests: interchangeable mini screw headvalidation

    From the detailed design, it was generated a mock-up to verify the assembly system

    and kinematics aspects. The following step was the manufacturing of a functional

    prototype. Machining processes and additive manufacturing were used in the fabrication

    of this prototype. Finally, experimental tests were conducted to investigate the capacity

    of extrusion head to generate continuous filaments from powder raw material.

    The preliminary tests showed the generation of continuous filaments with no large

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    14 Z.C. Silveira et al.

    variations in diameter, where Nylon 12 was successfully extruded with diameter

    filaments of 0.75 mm (mean width value) according to Figure 10.

    Figure 10 Filaments generated from polyamide (Nylon 12) (see online version for colours)

    This initial test is important to demonstrate the capacity to transform the polymer powder

    in a melted polymer. The expected performance for the feed section is carrying the

    material to the downstream sections. The continuous filaments obtained reflect an

    adequate performance in the compression and metering section. In these sections, the

    rising pressure forces the melted polymer through the nozzle tip with the aim to produce

    continuous filaments demonstrating the conceptual design of create filaments from

    powder using polymers in a screw extruder of small proportions. This concept is based

    in an idea of using the known extrusions process in a small scale. In Figure 12, it is

    shown the nozzle tip of the extrusion head performing the manufacturing a PolyamideNylon 12 15 layers block, without air gap, and 0.8 nozzle tip, showing the capacity of

    generating parts extruding layer by layer as it is required in rapid prototype purposes. The

    morphological characteristics were analysed with scanning electron microscopy (SEM).

    The photomicrographs were obtained in the Instrumental Chemical Analysis Center of

    the So Carlos Chemical Institute (CAQI/IQSC/USP) in ZEISS LEO 440 (Cambridge,

    England) with detector OXFORD (model 7060) equipment, operating with electron beam

    of 15 kV. The samples were covered with 10 nm of gold in a sputter Coating System

    BAL-TEC MED 020 (BAL-TEC, Liechtenstein) and it was maintained in desiccators

    until the moment of the analysis.

    Figure 11 (a) Nylon 12 filaments and (b) photomicrographs

    (a) (b)

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    Design development and functional validation 15

    It is possible to observe in Figure 11(a) that the filament generated from Nylon 12

    powder is homogeneous. In Figure 11(b), it can be seen that the material has a solidsurface without any pore or surfaces discontinuities.

    For the -PCL material, SEM micrographs shows the total transformation of the

    grains in feed section to solid homogenous material in compression section, the scheme

    in Figure 13(a) and (b) shows the sections where the -PCL was collected and the

    micrographs also. Figures 12(a) and (b) present an experimental test generating a scaffold

    manufacturing with polyamide.

    Figure 12 (a) The extrusion head constructing a Scaffold; (b) detailed view on the nozzle tip and(c) Scaffold generate (see online version for colours)

    Figure 13 (a) SEM for -PCL showing the material state and (b) morphological aspects in feedand compression sections

    (a) (b)

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    16 Z.C. Silveira et al.

    8 Conclusions

    The innovative characteristics presented in this work are based on the fact that

    the feeding of material is in powder form, its extrusion into filament and transformation

    in the form of deposition layers occurs simultaneously. Control of process parameters

    such as temperature and extrusion output stream of material contributing to the quality

    of the material constituting the 3-D model obtained. The miniaturisation of the sub-

    assembly barrel-screw applied to AM machines is other important aspect of this design

    development. The preliminary tests of the head showed the capacity of extruding melted

    material producing continuous filaments demonstrating the performance of each section

    of the screw extrusion. The transmission system, including the stepper motor, presented a

    satisfactory performance, mainly related to driving control systems, once it was shown

    the screw extrusion head capability to fabricate a block composed by various layers

    characterising the application in additive manufacturing. The results present the potentialof this interchangeable screw extrusion head to provide new opportunities for desktop

    3-D printers in several applications using powder as feedstock with the aim to generate

    3-D models.

    The use of QFD support the identification of the more important design

    characteristics that lead the choices during design development. The use of mock-up and

    additive manufacturing are important to previously identify assembly failures reducing

    the design time. The preliminary tests of the head showed the capacity of extruding

    melted material (SEM photomicrographs), which showed homogeneous and continuous

    filaments, a necessary condition for layer deposition purposes demonstrating the

    performance of each section of the screw extrusion. The results present the potential of

    this interchangeable screw extrusion head to provide new opportunities for desktop 3-D

    printers in several applications using powder as feedstock with the aim to generate 3-D

    models. In direction of new additive manufacturing correlated areas as health, tissue

    engineering and biomaterial applications, this new device presents results using -PCL as

    powder material and has demonstrated its capacity to produce scaffolds. As future works,

    it is proposed the optimisation of the extrusion process using design of experiment (DOE)

    and RSM looking for the best mechanical settings coupling with material properties. The

    use of new materials, in specific thermoplastics, is a promising area towards the material

    sciences applications in additive manufacturing, more specifically, in desktop 3-D printer

    machines. The blend or mixture of two or more kinds of polymers in feed section and its

    respective study is another possibility of research.

    Acknowledgements

    The authors thank to the CNPq (Brazilian Counsel of Technological and Scientific

    Development) for the financial support.

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