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JOURNAL OF
C O MP O S I TE
MATER IALS Article
Study on static and fatigue behaviors of carbon fiber bundle and the statisticaldistribution by experiments
Jian Song, Weidong Wen, Haitao Cui and Sibo Zhao
Abstract
In this paper, the static, tension–tension fatigue, and residual strength behaviors of carbon fiber bundle have beeninvestigated using experimental methods. The corresponding mechanical models and statistical distribution regulationshave also been established based on the experimental data. The test results indicate that the test section length of fiberbundle had a marked effect on the static strength, which decreased with the increase of length. A two-parameter Weibulldistributional function was used to describe the distribution of static strength. Furthermore, the S-N curve was obtained
by a new segmented function to reflect the changing of fatigue life against stress levels. The experimental results of residual strength show that there was an abnormal tendency, which increased first and decreased later as the increase of cyclic number, for the residual strength of carbon fiber bundle in both tested stress levels 87% and 80%, respectively.Therefore, a new model for the residual strength was put forward and the good agreement between the fitting curvesand experimental was obtained.
Keywords
Carbon fiber bundle, static strength test and distribution law, fatigue life test and S-N, fatigue life distribution, residualstrength test and mechanical model
Introduction
Carbon fiber reinforced composites have been widely
used as reinforcement in polymer composites, owing to
their good mechanical properties and light weight. Most
of the early works focus on the certainty performance,1
such as the stiffness, strength, and fatigue characteristic
of composites, which causes that composites are often
overdesigned, such as heavier and more costly than
necessary. Therefore, probability design methods have
been gradually conducted into composites research.
Schaff and Davidson2 proposed a strength-based wear-
out model to predict the fatigue life and residual strength
of composite laminates and the related distributions
were investigated by a two parameter Weibull function.
Cheng and Hwu3 investigated the fatigue reliability of
composite laminates subjected to constant amplitude
loading and a residual analysis model was proposed to
predict the residual strength. Whitworth4–6 studied the
statistical distribution laws on graphite/epoxy compos-
ites based on a set of static and fatigue tests and put
forward to p-E-N and p-S-N models. Yang et al.7–9
proposed a three-parameter fatigue and residual
strength degradation model to predict the statistical fati-
gue behavior of angle-ply composites. Wu and Yao10
derived the fatigue life distribution of composite lamin-
ates based on their static strength distribution.
Although carbon fiber reinforced composites has
been studied in many aspects, the research on the per-
formance of carbon fiber bundle as main component is
quite limited. There are still some issues associated with
that left to be solved in the respects of non-uniform qual-
ityof filaments, length of limited fiber bundle and fatigue
characteristic, all of which have an impact on the static
and fatigue performance to some extent. Moreover, it is
inevitable to consider the statistical distribution
owing to the random question of self-defect and
College of Energy and Power Engineering, Nanjing University of
Aeronautics and Astronautics, China
Corresponding author:
Jian Song, College of Energy and Power Engineering, Nanjing University of
Aeronautics and Astronautics, No. 29 Street, Nanjing 210016, China.
Email: [email protected]
Journal of Composite Materials
2015, Vol. 49(25) 3157–3168
! The Author(s) 2014
Reprints and permissions:
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DOI: 10.1177/0021998314560385
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corresponding results are presented in Table 1, which
are also the residual strengths R(0) in the condition of
zero cycle.
U ¼ 4Pd 2 3000 ð1Þ
where P is the peak of static load; d is the nominaldiameter of carbon fiber bundle in which d is equal
to 7 mm.
From Table 1, we can see that the static strength of
fiber bundles was increased with the decrease of charac-
teristic lengths, which indicated a size effect on the static
strength of fiber bundles. In addition, the representative
load–displacement curves for different characteristic
lengths and the curve of influence of characteristic
length on average strength fitted by the model 2 were
shown in Figure 2, respectively. It is clearly found that
an obvious non-linear phenomenon happened as the
increase of load and also the average static strengths of
fiber bundle with different lengths were remarkable
reduced with the increase of characteristic length.
S 0 ¼ c0
L
1=mð2Þ
where S 0 is the average strength, L is the characteristiclength (30, 40, and 50 mm), c and m are the constants
determined by experimental data (m ¼ 1.632,c0 ¼ 3,625,272.57).
Damaged photographs subjected static loading are
given in Figure 3. From this figure, the location in
the surface of fiber bundles appears as the amountof fluffiness phenomena, which indicates that there
exists a certain quantity of monofilament taking
place failure gradually so that a de-bunching failure
mode finally happens in the middle of carbon fiber
bundle.
Statistical distribution of static strength. To research the
statistics distribution of fiber bundles, the two-para-
meter Weibull distribution function (3) is used to fit
the static strengths R(0) and thus we can plot the
related probability paper and distribution of static
strength in Figure 4.
F ðX Þ ¼ P U X f g ¼ 1 exp X
! ð3Þ
Table 1. Static strength test results of carbon fiber bundles.
Characteristiclength
Specimennumber
Peak load (N)
Strength(MPa)
Averagestrength (MPa)
Scaleparameter,
Shapeparameter,
50 mm L50-1 112.84 977.32 946.50 964.83 23.99L50-2 103.35 895.17
L50-3 104.05 901.23
L50-4 113.21 980.57
L50-5 106.95 926.31
L50-6 110.79 959.57
L50-7 113.81 985.73
40 mm L40-1 127.84 1107.29 1097.75 1111.23 37.61
L40-2 123.43 1069.05
L40-3 122.02 1056.91
L40-4 129.51 1121.73
L40-5 129.64 1122.84L40-6 128.00 1108.71
30 mm L30-1 130.72 1132.25 1172.73 1188.73 34.75
L30-2 131.74 1141.09
L30-3 132.65 1148.91
L30-4 133.48 1156.11
L30-5 134.92 1168.58
L30-6 137.84 1193.86
L30-7 140.68 1218.47
L30-8 141.15 1222.56
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Figure 3. Static tensile test of carbon fiber bundle: (a) pre-test; (b) during the test; (c) photograph of failure specimen.
0.0 0.2 0.4 0.6 0.8 1.0 1.2 1.4
0
20
40
60
80
100
120
140
160(a) (b) L30-1 : L=30mm
L40-3 : L=40mm
L50-4 : L=50mm
L o a d / N
displacement/%
25 30 35 40 45 50 55 60 65
800
900
1000
1100
1200
1300
1400
Fitting curve by Eq.(2)
Experimental data
A v e r a g e s t r e n g t h / M P a
Fiber length/mm
Figure 2. (a) Load–displacement curve of typical fiber bundle with different characteristic lengths; (b) influence of characteristic
length on average strength.
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where F (X ) represents the statistical distribution of
carbon fiber bundles; U means the static strength;
and are scale parameter and shape parameter,
respectively.
From Figure 4, several important findings about the
static strength statistical distribution of carbon fiber
bundles were given as follows: First of all, it is logicalto consider that the statistical distribution for fiber
bundle strength can be estimated by using a two-
parameter Weibull distribution function (3) according
to the correlation coefficients (R ¼ 0.903, 0.884, and0.865 for L ¼ 50, 40, and 30mm, respectively) inFigure 4(a) to (c). Furthermore, although the strength
of fiber bundles varies with different characteristic
length, the value of shape parameters has a no signifi-
cant change (refer to Figure 4(d)) and the general
change trend is that with the increase of length, the
curve slope of Weibll distribution function in view of
one type of length decreases gradually.
In addition, the Kolmogorov–Smirnov hypothesis
tests were applied to verify quantitatively whether the
proposed two-parameter Weibull distribution function
is suitable for the statistical distribution of carbon fiber
bundles. The hypothesis test results are listed in Table 2
and the method is introduced briefly in Appendix 1.
According to Table 2, the values for all of the teststatistics (sqrt(n)*D) are outside the reject domain,
therefore, it is reasonable to accept the hypothesis
that the statistical distribution for static strength of
fiber bundles follows the Weibull distribution law.
Fatigue life test
Testing results of fatigue life. A set of 22 specimens sub-
jected to nine various constant amplitude stress levels
are listed in Table 3. The S-N curve of carbon fiber
bundles referred to equations (4) to (6) was then plotted
in Figure 5 and the related parameters fitted by the
-2.0 -1.5 -1.0 -0.5 0.0 0.5 1.0
6.78
6.80
6.82
6.84
6.86
6.88
6.90
(a) (b)
(c) (d)
L50: Experimental data
L50: Fitting curving
l n X
ln[-ln(1-F(X))]
Equation y = a + b
Adj. R-Squ 0.90297
Value Standard Er
B Intercep 6.871 0.00551
B Slope 0.041 0.00553
-2.0 -1.5 -1.0 -0.5 0.0 0.5 1.0
6.96
6.97
6.98
6.99
7.00
7.01
7.02
7.03
7.04
Equation y = a + b Adj. R-Squa 0.88385
Value Standard Err
D Intercept 7.0132 0.00409
D Slope 0.0265 0.00426
L40: Experimental data
L40: Fitting curving
l n X
ln[-ln(1-F(X))]
-2.5 -2.0 -1.5 -1.0 -0.5 0.0 0.5 1.0
7.01
7.02
7.03
7.04
7.05
7.06
7.07
7.08
7.09
7.10
7.11
Equat ion y = a + b
Adj. R-Squa 0.86457
Value Standard Err
H Intercept 7.0806 0.00437
H Slope 0.0287 0.00426
l n X
L30: Experimental data
L30: Fitting curving
ln[-ln(1-F(X))]
800 900 1000 1100 1200 1300 1400
0.0
0.2
0.4
0.6
0.8
1.0
L30:Fitting curving
L40:Fitting curving
L50:Fitting curving
L30: Experimental data
L40: Experimental data
L50: Experimental data
F a i l u r e p r o b a b i l i t y
Static strength/MPa
Figure 4. Weibull distribution probability paper of static strength (a)–(c) and failure probability of carbon fiber bundles with different
characteristic lengths (d).
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fatigue test data was directly given in equations (4)
to (6).
From the experimental results in Figure 5(a) (open
triangle ‘‘4’’), it is concluded that the normalized stress
basically underwent a linear trend between 0.85 and
0.94, while there was an obvious decay trend in the
range of 0.73 to 0.85. When the normalized stress was
less than 0.73, all of the fatigue life of fiber bundles was
more than 1e6, which was defined as the infinite life.
Therefore, it can be used a linear function to describe
the variation trend between 0.85 and 0.94 and an expo-
nential model to describe the change regularity of
0.73–0.85, respectively. The determined relationshipsbetween fatigue life and normalized stress were
expressed in the following equations
1. 0:85 max U
0:94 max
U ¼ 0:0506l g N f þ 1:059 ð4Þ
2. 0:75 max U
0:85
max
U ¼1
0:310
lg N f 4:014
lg N f 1:469 0:182
ð5
Þ
3. max U
0:75
lg N f 4 6 ð6Þ
From Figure 5(a), it is clearly found that good coin-
cidence between experiment and theory was obtained
for the fatigue issue of carbon fiber bundles. Moreover,
failure photograph under the fatigue load was shown in
Figure 5(b) and it can be seen that the failure model
mainly manifested de-bunching failure, which was simi-lar with the mode as that in static strength.
Nevertheless, the difference was that the failure regions
were concentrated in the middle of specimens compared
to that in the static tests.
Statistical distribution of fatigue life. Furthermore, in order
to investigate the distribution law for the fatigue of
fiber bundles, we assume that the statistical distribution
of the fatigue life also follows a two-parameter Weibull
distribution with reference to composite laminates3,6,18
F ðnÞ ¼ P N f n ¼ 1 exp n
l ! ð7Þ
where F (n) denotes the fatigue life distribution of
carbon fiber bundles, N is the fatigue life, and l are
the scale and shape parameter, respectively both of
which can be calculated by the same method as the
static strength.
The calculated results are presented in Table 4 and
corresponding distributional curves are plotted in
Figure 6. As for these results, the statistical distribution
Table 3. Tension–tension fatigue test results of carbon fiber
bundles.
Stress
level
Specimen
number
Fatigue
life, Nf lgNf Average lgNf
94% U 1 185 2.267 2.372
2 243 2.386
3 291 2.464
92% U 4 629 2.799 2.721
5 500 2.699
6 450 2.653
87% U 7 6984 3.844 3.836
8 7949 3.900
9 5923 3.773
10 6550 3.816
85% U 11 10,881 4.037 4.064
12 12,363 4.092
80% U 13 14,544 4.163 4.248
14 20,883 4.320
15 15,869 4.201
16 19,486 4.290
75% 17 235,079 5.371 5.397
18 239,358 5.379
19 274,297 5.438
73% 20 >1e6 >6 >670% 21 >1e6 >6 >6
60% 22 >1e6 >6 >6
Table 2. Hypothesis test results for static strength distribution
function.
Characteristic lengths L ¼ 30mm L ¼ 40mm L ¼ 50mmNumber of specimens 8 6 7
Kolmogorov D 0.2388 0.2974 0.2438
sqrt(n)*D 0.6755 0.7285 0.6450Reject domain at
significant level 0.05
[1.36,1)
D ¼ supjF n( x ) F ( x )j, where F ( x ) and F n( x ) are the assumed distributionalfunction and distributional function of samples, respectively; sqrt(n)*D
represents test statistics.
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of fatigue life was fitted by the two-parameter Weibull
distribution fairly well, as shown in Figure 6(c).According to the statistical results mentioned above,
the excellent correlation implies that adoption of
Weibull distributional function in carbon fiber bundle
fatigue analysis is feasible. In addition, there was a
more discreteness in low stress level, which was also
reasonable because the lower stress level causes that
the fatigue damage takes place in more local positions
in the surface of fiber bundles and the propagation
paths are also more complex.
In addition, the similar approach as the static
strength was used to investigate whether the hypothesis
distribution regulation was reasonable for the fatigue
life of carbon fiber bundle at various stress levels. The
quantitative results are given in Table 5. It is clearly
seen that all the values of D were less than 1.36,
which was the lower limit of reject domain. Thus, the
hypothesis can be accepted.
Testing results for residual strength of carbon
fiber bundles
Testing results of residual strength. Fourteen specimens
were fatigued at two maximum stress levels 87% and
80%, respectively, up to 1/3 and 2/3 corresponding
average fatigue life, which were 7852 for 87% stress
level and 17696 for 80%. Their residual strength tests
were then performed and the results are listed in
Table 6. The failure photograph related to residual
strength tests is shown in Figure 7(a).
From Table 7, it is obviously found that the residual
strengths had a non-monotonic tendency with the
increase of cycle, which is similar to the notched
strength of woven composites.19,20 Figure 7(a) exhibits
several serious failure models with de-bunching and
fracture damages in the middle of fiber bundles. Thepossible reason for the phenomenon could be that the
monofilaments in the fiber bundle are gradually dis-
persed under the fatigue load, which may lead to
more uniform bearing in each of monofilaments.
Therefore, a higher load and further serious damage
are shown in the following static tensile test.
Meanwhile, a briefness ‘‘bang’’ sound could be listened
when the fracture occurred.
Furthermore, in order to investigate the difference
between static and residual strength, Figure 7(b) pre-
sents the load–displacement curves for three represen-
tative specimens used in static strength and residual
strength tests, respectively. It is found that the value
of residual strength experienced an increase firstly,
and then showed a decreased trend against cycle
number. The reasons of this abnormal phenomenon
may be that on the one hand, the stress state for each
of monofilaments is more uniform as mentioned above,
which could lead to the more bearing capacity for single
fiber bundle. On the other hand, the extent of accumu-
lative damage in monofilaments may increase subjected
cyclic loading, which could cause the decrease of the
mechanical performance to some degree. Therefore,
2 3 4 5 6
0.6
0.7
0.8
0.9
1.0
m a x
u l t
lgNf
(a) (b)
Figure 5. (a) The curve of fiber bundles normalized stress against lgNf ; (b) fatigue test specimen of carbon fiber bundle.
Table 4. Parameters in Weibull distributional function of fatiguelife.
Weibull distribution
parameters
87%
stress level
80%
stress level
G 7263.01 19,100.89
l 6.96 5.11
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the variation in residual strength versus cyclic number
may be the result of interaction of both factors
mentioned.
In order to describe the phenomenon quantitatively,
a new model was proposed. It is assumed that
dRðnÞdn
¼ gðS , rÞ f ðnÞ ð8Þ
-1.5 -1.0 -0.5 0.0 0.5
8.65
8.70
8.75
8.80
8.85
8.90
8.95
9.00
(a) (b)
(c)
Stress leve : 87% Ult Fitting curve
Equation y = a + b*
Adj. R-Squar 0.95498
Value Standard Erro
B Intercept 8.89055 0.01531
B Slope 0.14367 0.01787
ln[-ln(1-F(X))]
l n X
-1.5 -1.0 -0.5 0.0 0.5
9.55
9.60
9.65
9.70
9.75
9.80
9.85
9.90
9.95
10.00
Stress leve : 80% Ult Fitting curve
Equation y = a + b*
Adj. R-Squar 0.91796
Value Standard Err
H Intercept 9.8574 0.02849
H Slope 0.1955 0.03326
ln[-ln(1-F(X))]
l n X
4000 8000 12000 16000 20000 24000
0.0
0.2
0.4
0.6
0.8
1.0
Distribution function withmax
=80% U
Experimental data withmax
=80% U
Distribution function withmax
=87% U
Experimental data withmax
=87% U
Fatigue cycle Nf
F a i l u r e p r o b a b l i t y
Figure 6. Weibull distribution probability paper of fatigue life (a), (b) and failure probability (c).
Table 6. Residual strength tests results of carbon fiber bundles.
Stress
levels
Terminal
number
Peak
load (N)
Strength
(MPa)
Average
strength (MPa)
87% 1/3Nf * 169.41 1467.30 1391.34
150.69 1305.19
158.58 1373.58
163.86 1419.28
2/3Nf * 155.26 1344.81 1337.41
156.59 1356.34153.66 1330.93
152.12 1317.57
80% 1/3Nf ** 153.36 1328.33 1333.86
152.45 1320.43
156.19 1352.82
2/3Nf ** 110.35 955.81 1085.37
136.94 1186.06
128.64 1114.23
Nf * and Nf ** means the fatigue life of 87% and 80% stress levels,
respectively.
Table 5. Hypothesis test results for fatigue life distribution
function.
Stress levels 87% 80%
Number of specimens 4 4
Kolmogorov D 0.2465 0.2696
sqrt(n)*D 0.4931 0.5392
Reject domain at
significant level 0.05
[1.36,1)
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Indicating that R(n) (the rate of residual strength at
the nth stress cycles) is equal to the product of the
effect, g(S , r), of the stress range, S , of the stress ratio,
r and the effect, f (n), of the number of cycle. The stress
range S is defined as the difference between the max-
imum and minimum cycle stress. So, the simplest
approximation to the functional form of g(S , r) and
f (n) is expressed as
gðS Þ ¼ k1S b, S ¼ ð1 rÞ max, k14 0 f
ðn
Þ ¼ Qn
þv, Q4 0, v4 0
ð9Þ
where k1, b, Q, and v are constants. In equation (9), it is
assumed for simplicity that the stress ratio is fixed so
that g(S, r) is a function of S alone and f (n) is the linear
function to ensure the variation of R(n) is in accordance
with the experimental data.
Substituting equation (9) into equation (8) and car-
rying out the integration from n1 to n2 cycles, we have
Rðn2Þ Rðn1Þ ¼ k1S bQ
2 n22 n21 þ k1vS bðn2 n1Þ
ð10Þ
For n2¼ n, n1¼ 0, equation (10) reduces to
RðnÞ Rð0Þ ¼ k1S bQ
2 n2 þ k1vS bn ð11Þ
Let a ¼ k1Q/2, c ¼ k1v, then
RðnÞ ¼ Rð0Þ S bðan2 cnÞ ð12Þ
Equation (12) is a theoretical residual model of
carbon fiber bundle involving three parameters a, b,
and c, which will be determined by amount of residual
strength tests in the following section.Based on the data of residual strength tests, the par-
ameters involved in equation (12) can be obtained. The
results for residual strength tests at high and low stress
amplitudes are shown in Table 7 and the related curves
are plotted in Figure 8. Additionally, the corresponding
residual strength under 87% and 80% stress levels for
1/3N f and 2/3N f cycles calculated by the equation (12)
are listed in Table 8. According to the results, the max-
imum error was only 8.14%, which took place under
80% stress levels for 2/3N f , therefore, it is reasonable to
accept the theoretical formula (12) to predict the resi-
dual strength of fiber bundle.
Furthermore, as equation (12) reflects the relation-
ship between the static strength and residual strength, it
is necessary to further validate whether the converted
static strengths R(0) calculated by equation (13) are
suitable to the statistical distribution of static strength.
Therefore, the residual strength data listed in Table 6
can be converted into the equivalent static strength
using the model given by equation (13). And the cor-
responding results are plotted in Figure 9 where the set
of converted equivalent static strength, R(0), using the
values of a, b, and c given in Table 7 was plotted as
0.0 0.2 0.4 0.6 0.8 1.0 1.2 1.4
0
30
60
90
120
150
180(b)(a)
Residual strength at 1/3Nf
Residual strength at 2/3Nf
Ultimate strength
L o a d / N
displacement/%
Figure 7. Residual strength failure photograph of carbon fiber bundle.
Table 7. Parameters in residual strength model.
Parameters
Low stress
amplitudes (80% U)
High stress
amplitudes (87% U)
a 1.55e-3 3.86e-3
b 0.532 1.009c 10.016 59.454
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solid squares and the solid curve was the same Weibull
distribution of the static strength presented in
Figure 4(d) with the 50 mm characteristic length.
Rð0Þ ¼ RðnÞ þ S bðan2 cnÞ ð13Þ
where R(0) represents the converted equivalent
strength.
It can be observed from Figure 9 that the correlation
between the Weibull distribution obtained directly by
static strength and converted data from residual
strength was comparatively well despite of stress
levels. Thus, it is reasonable to describe the residual
strength at various stress levels by equation (12).
Conclusions
The performances of static strength, fatigue life, and
residual strength for carbon fiber bundles of T300
fibers have been tested and the corresponding mechan-
ical models have also been built based on the testing
results. The following conclusions can be made:
1. The inner original defects derived from manufactur-
ing process existing in each of monofilaments caused
that the static strength of fiber bundle was correlated
with test section length. Therefore, the specimen
with a longer characteristic length has generally
lower strength under static tests.
2. Under T-T cyclic loading, the de-bunching phenom-
ena are more obviously and mainly concentrated in
the middle of fiber bundle, and less in the root part.
A segmented function was proposed to describe the
S-N curve of carbon fiber bundles and the related
parameters were then obtained based on the fatigue
0 1000 2000 3000 4000 5000 6000 7000
0
200
400
600
800
1000
1200
1400
(a) (b)
Residual strength curve obtained by Eq (12)
of 87% stress level
Average value of 87% stress level
Experimental data of 87% stress level
R e s i d u a l s t r e n g t h R ( n )
Cycle number n
0 4000 8000 12000 16000 20000
0
200
400
600
800
1000
1200
1400
Residual strength curve obtained by Eq (12)
of 80% stress level
Average value of 80% stress level
Experimental data of 80% stress level
Cycle number n
R e s i d u a l s t r e n
g t h R ( n )
Figure 8. Residual strength curves of carbon fiber bundle at high stress level (a) and low stress level (b).
840 860 880 900 920 940 960 980 1000 1020 1040
0.0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
1.0
Convered ultimate strength using equation (13)
Weibull distribution obtained form equation (6)
D i s t r i b u t i o n f u n c t i o n
Convered ultimate strength
Figure 9. Theoretical prediction of static strength and residual
strength data converted to static strength for carbon fiber bundle
under both stress levels.
Table 8. Comparison between the predicted values of residual
strength based on equation (12) and test data.
Stress
levels
Terminal
number
Test
results
Predicted
results Error
87% 1/3Nf * 1391.34 1386.26 0.37%
2/3Nf * 1337.41 1345.20 0.58%
80% 1/3Nf ** 1333.86 1245.92 6.59%
2/3Nf ** 1085.37 1173.69 8.14%
Nf * and Nf ** means the fatigue life of 87% and 80% stress levels, respect-
ively. All of the test data are from Table 6.
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life data. In order to investigate the statistical distri-
bution of fatigue life, a two-parameter Weibull dis-
tribution function was well used to describe the
distribution.
3. In the end, the residual strength tests were conducted
and a theoretical model was derived based on the
assumption that the residual strength of fiber bun-dles is non-monotonic. Additionally, the failure
degree for residual strength tests was the most ser-
ious compared to others, which had not only obvi-
ous de-bunching damages, but also fracture
damages.
Funding
This work was supported by Jiangsu Innovation Program for
Graduate Education [grant number KYLX_0237].
Conflict of interest
None declared.
References
1. Degrieek J and Paepegem WV. Fatigue damage modeling
of fibre-reinforced composite materials: Review. Appl
Mech Rev 2001; 54(4): 279–300.
2. Schaff JR and Davidson BD. Life prediction method-
ology for composite structures, part I: Constant ampli-
tude and two-stress level fatigue. J Compos Mater 1997;
31(2): 128–157.
3. Cheng HC and Hwu FS. Fatigue reliability analysis of composites based on residual strength. Adv Compos
Mater 2006; 15(4): 385–402.
4. Whitworth HA. Modeling stiffness reduction of graphite/
epoxy composite laminates. J Compos Mater 1987; 21(6):
362–371.
5. Whitworth HA. A stiffness degradation model for com-
posite laminates under fatigue loading. Compos Struct
1998; 40(2): 95–101.
6. Whitworth HA. Evaluation of the residual strength deg-
radation in composite laminates under fatigue loading.
Compos Struct 2000; 48(5): 261–264.
7. Yang JN and Miller PK. Effect of high load on statistical
fatigue of unnotched graphite/epoxy laminates. J Compos
Mater 1980; 14(4): 82–94.
8. Yang JN and Liu MD. Residual strength degradation
model and theory of periodic proof tests for graphite/
epoxy laminates. J Compos Mater 1977; 11(2): 176–202.
9. Yang JN and Jones DL. Statistical fatigue of graphite/
epoxy angle-ply laminates in shear. J Compos Mater
1978; 12(4): 371–389.
10. Wu FQ and Yao WX. A model of the fatigue life distri-
bution of composite laminates based on their static
strength distribution. Chin J Aeronaut 2007; 21(6):
241–246.
11. Phani KK. Evaluation of single-fibre strength distribu-
tion from fibre bundle strength. J Mater Sci 1988;
23(3): 941–945.
12. Yu WD, Postle R and Gyan HJ. Evaluating single fiber
and fiber bundle tensile curves. Text Res J 2003; 73(8):
875–882.
13. Joffe R, Andersons J and Sparniņs ˇ E. Applicability of
Weibull strength distribution for cellulose fibers withhighly non-linear behaviour. In: Proceedings of the 17th
international conference on composite materials (ICCM-
17), Edinburg, UK, 27–31 July 2009.
14. Yuan H, Wen WD, Cui HT, et al. The random crack core
model for predicting the longitudinal tensile strengths of
unidirectional composites. J Mater Sci 2009; 44(12):
3026–3034.
15. Zhu YL, Cui HT, Wen WD, et al. Experiments on fatigue
damage failure test of carbon fiber yarn. Acta Mater
Compos Sin 2012; 29(5): 179–183.
16. ASTM. Standard test method for tensile strength and
Young’s modulus for high-modulus single filament mater-
ials. ASTM D3379-75. West Conshohocken, PA: ASTM,1989.
17. ASTM. Standard recommended practice for constant-
amplitude low-cycle fatigue testing. ASTM E606. West
Conshohocken, PA: ASTM, 1980.
18. Yang JN. Fatigue and residual strength degradation
for graphite/epoxy composites under tension-
compression cyclic loadings. J Compos Mater 1978;
12(19): 19–39.
19. Li JL, Yang HN and Kou CH. Fatigue properties of
three dimensional braiding composites. Acta Mater
Compos Sin 2005; 22(4): 172–176.
20. Ken G, Yu KF, Hiroshi H, et al. Fatigue behavior of 2D
laminate C/C composites at room temperature. Compos
Sci Technol 2005; 65(5): 1044–1051.21. Teng SZ and Feng JH. Mathematical statistics. Dalian:
Dalian University of Technology Press, 2005.
Appendix
The Kolmogorov–Smirnov test.
This method21 proposed by Kolmogorov was
used to test quantitatively the difference degree
between the assumed distributional function F (x)
and the distributional function of samples F n(x)
(plotted in Figure 10). From the following
Figure 10. Schematic diagram of Dn.
Song et al. 3167
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equation, it is defined as a distance Dn to describe
the difference
Dn ¼ sup F nðxÞ F ðxÞ ð14Þ
A reasonable test under a significant level is that if the hypothesis distribution is true, the value Dn men-
tioned above has a reduced trend, else the value
would be increased. Therefore, there exists a thresh-
old value k, i.e. when sqrt(n)*Dn< k, the hypothesis
could be accepted, else be rejected, where sqrt(n) is
used to reflect the effect of the number of test
specimens.
The limiting distribution of sqrt(n)*Dn was derived
by Kolmogorov as follows
limn!1
P ffiffiffi
np
Dn t ¼ F ðtÞ
F
ðt
Þ ¼1
2X
1
i ¼1 ð1
Þi 1e2i
2t2 ð15Þ
where F (t) was calculated and listed in the limiting dis-
tributional table of Dn.
Finally, the rejection domain can be obtained by
checking out the limiting distributional table under a
given significant levels , i.e. when ¼ 0.05, the rejectdomain U ¼ [1.36, 1).
3168 Journal of Composite Materials 49(25)
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