master thesis: characterization and optimization of an electron cyclotron resonance ion source
TRANSCRIPT
Characterization and Optimization of an Electron
Cyclotron Resonance Ion Source
J.Rabinder Henry
External: Dr. Stefhan Facsko(FZR Rossendorf)
Dip-Ing. Gerald Staats
Professor: Prof. Dr.-Ing. Christian Schäffer
Outlook
• Introduction
Electron Cyclotron Resonance Ion Source (ECRIS)
FZR 14.5 GHz source
• Characterization and Optimization
Plasma –X-ray Spectroscopy
Results
• Beam Emittance
Results
• Summary and outlook
RFcemeB ωω == /
Principle of ECRIS
●Electron Cyclotron Resonance Heating
●Electron impact ionization
●Magnetic confinement
Magnetic Field
FZR 14.5 GHz Supernanogan
RF Power
3
RF Power
ECR Zone
Gas Inlet
ECR Source Working PrincipleExtraction Electrode
Electron Cyclotron Emission
FC2
Microwave source
BL1
BL2
Target Chamber
BPM2
SL2
FZR 14.5 GHz ECR Source
and Beam Line
4
ECRISSL1BPM1FC1
MD
EL1
EBIT
Multielectrode
extraction
MS1
SL2
RF Power (x)
Pressure (y)
Biased disc (z)
I extracted (Iex)ECRIS
Characterization and Optimization
Max f (Iex) = min (x, y, z)
5
Gas mixing (a)
Plasma Characterization
X-ray Spectroscopy
Ion beam quality
Emittance
Electron Distribution
Charge State Distribution }Source Parameters
x, y, z, a
X-ray Spectroscopy
Electron –Bremsstrahlung Measurement
Ion charge state –Characteristics X-ray Measurement
Germanium Detector Attenuation of Radiation
Be window
Air column
Collimation
Extraction Voltage
6
Analyzing
Magnet
HPGe Detector
ECRIS
Faraday Cup
Beryllium
Window
4000
6000
Electronic Peak
Counts
No collimation
With collimation 1mm
2000
4000
Counts
US= 25KV
US=0V
Bremsstrahlung Measurement
Collimation Extraction Voltage
7
0 50 100 150 2000
2000
Energy (keV)
0 50 100 150 2000
2000
E (keV)
0 50 100 150 200
0
2000
4000
6000
8000
10000
25W
50W 75W
100W 125W
175W 200W
250W
Counts
E(keV)
0 50 100 150 2000
1000
2000
3000
0V
-100V
-200v
-300V
-400V
-600V
Coun
ts
E ( keV)
Photon Distribution Analysis
Power Bias
80 50 100 150 200
0
2000
4000
6000
8000
1x10-5mbar
2.5x10-5mbar
5X10-5mbar
4.210-5mbar
7.5x10-5mbar
1x10-4mbar
Counts
E (keV)
0 50 100 150 2000
2000
4000
6000
8000
Counts
E (keV)
Argon+Oxygen
Argon
Photon Distribution Analysis
PressureGas mixing
Bremsstrahlung Spectra for Varying Power
6000
8000
10000
25W 50W
75W
100W
125W
175W
200W
250W
Counts
Xenon Plasma
Pressure 9.8x10-5mbar
Bias voltage -200 V
9
0 50 100 150 200
0
2000
4000
Counts
E(keV)
4000
6000
8000
1x10-5mbar
2.5x10-5mbar
5X10-5mbar
4.210-5mbar
7.5x10-5mbar
1x10-4mbar
Counts
Bremsstrahlung Spectra for Varying Pressure
Argon Plasma
Power 100 W
Bias voltage -164 V
10
0 50 100 150 2000
2000
4000 1x10 mbar
Counts
E (keV)
2000
3000
0V
-100V
-200v
-300V
-400V
-600V
Co
un
ts
Bremsstrahlung Spectra for Varying Bias
Xenon Plasma
Pressure 9.8x10-5mbar
Power 100 W
11
0 50 100 150 2000
1000
Co
un
ts
E ( keV)
4000
6000
8000
Co
un
ts
Argon+Oxygen
Argon
Bremsstrahlung Spectra for Gas Mixing
Power 50 W
Pressure 3.9x 10-5 mbar
Bias voltage of -200V
12
0 50 100 150 2000
2000
4000Co
un
ts
E (keV)
0 50 100 150 2000
1
2
3
4
5
6
7
F(E
) (R
ea
ltiv
e C
ou
nts
)
Energy
50W
100W
200W
40 50 60 70 80 90 100 110 1200,0
0,2
0,4
0,6
0,8
1,0
F(E
) R
ela
tiv
e C
ou
nts
Energy (keV)
-200V
-300V
-400V
-500V
-600V
Electron Distribution Analysis
PowerBias
130 50 100 150 200 2500,0
0,2
0,4
0,6
0,8
1,0
1,2
1,4
1,6
F(E
) (R
ela
tive
Co
un
ts)
Energy (keV)
1x10-4
mbar
5x10-5
mbar
1X10-5
mbar
50 100 150 2000
1
2
F(E
) R
ela
tive
Co
un
ts
Energy (kev)
Argon
Argon+Oxygen
Electron Distribution Analysis
PressureGas mixing
10000
15000
20000
1 8
054ev
1 7
061ev
1 6
401ev
Xe L
α1 4
104ev
Counts
Characteristics X-ray Measurements
Xenon
Power 120 W
Pressure 9.7 x 10-5 mbar
Bias -200V
14
0 5000 10000 15000 20000 25000 30000 35000 400000
5000
Xe K
β1 3
3384ev
Xe K
α1 2
9779ev
Cu K
β1 8
904ev
Cu K
α1 8
054ev
Fe K
β1 7
061ev
Fe K
α1 6
401ev
Counts
E (eV)
0 10000 20000 30000 40000
0
5000
10000
15000
20000
60W
200W
20W
60W
80W
100W
120W
140W
160W
180W
200W
Co
un
ts
0 10000 20000 30000 400000
2000
4000
6000
8000
10000
12000
14000
2.7x10-6
mbar
1.03X-4
mbar
Ks
eri
es
Ls
eri
es
1.03x10-4
mbar
6.5x10-5
mbar
4.5x10-5
mbar
3.9x10-5
mbar
2.4x10-5
mbar
1.5x10-5
mbar
4.1x10-6
mbar
9.8x10-6
mbar
2.7x10-6
mbar
Co
un
ts
X-ray Spectra
Power Pressure
15
0 10000 20000 30000 40000
E (eV)
0 10000 20000 30000 40000
E(eV)
0 20 40 60 80 100 120 140 160 180 200
0,02
0,04
0,06
0,08
0,10
Inte
nsity R
atio
RF-Power(watts)0,0 2,0x10
-54,0x10
-56,0x10
-58,0x10
-51,0x10
-41,2x10
-40,00
0,01
0,02
0,03
0,04
0,05
0,06
Ik/IL Inte
nsity r
atio
Pressure mbar
10000
15000
20000
60W
200W
20W
60W
80W
100W
120W
140W
160W
180W
200W
Co
un
ts
X-ray Spectra For Varying Power
Xenon plasma
Pressure1.03 x 10-4 mbar
Bias voltage -200 V
16
0 10000 20000 30000 40000
0
5000
10000
Co
un
ts
E (eV)
8000
10000
12000
14000
Lse
ries
1.03x10-4
mbar
6.5x10-5
mbar
4.5x10-5
mbar
3.9x10-5
mbar
2.4x10-5
mbar
1.5x10-5
mbar
4.1x10-6
mbar
9.8x10-6
mbar
2.7x10-6
mbar
Co
un
ts
X-ray Spectra For Varying Pressure
Xenon plasma
Power 100 W
Bias voltage -200 V
17
0 10000 20000 30000 400000
2000
4000
60002.7x10
-6mbar
1.03X-4
mbar
Kse
ries
2.7x10 mbar
Co
un
ts
E(eV)
6000
8000
10000
Xe
L S
eri
es
Co
un
ts
-50V
-250V
-400V
-600V 2000
Fe K
α
Cu K
α 1
,2
Xe L
α 1
,2
Counts
Xe 27% /O 20%
Xe 27% /O 21.50%
Xe 27% /O 25.20%
X-ray Spectra
Bias Gas mixing
18
0 10000 20000 30000 400000
2000
4000X
e K
Se
rie
s
Co
un
ts
E(eV)0 10000 20000 30000 40000
0
1000
Xe K
β
Cu K
β
Fe K
β
Xe
Lβ
Counts
E (eV)
X-ray Spectra For Varying Bias
60 0 0
80 0 0
1 00 0 0
Xe L
Series
Counts
-50V
-250V
-400V
-600V
Xenon plasma
Pressure1.03 x 10-4 mbar
Power 100 W
19
0 10 0 00 20 0 00 30 00 0 4 0 00 00
20 0 0
40 0 0
Xe K
Series
Counts
E (e V )
2 0 0 0
Fe K
α
Cu K
α 1
,2
β
Xe L
α 1
,2
Counts
X e 2 7 % /O 2 0 %
X e 2 7 % /O 2 1 .5 0 %
X e 2 7 % /O 2 5 .2 0 %
X-ray Spectra For Gas Mixing
Xenon and Oxygen
Pressure 1.6x 10-6 mbar
Power 100 W
Bias voltage -200 V
20
0 1 0 0 0 0 2 0 0 0 0 3 0 0 0 0 4 0 0 0 00
1 0 0 0
Xe K
β
Cu K
β
Fe K
β
Xe L
β
Counts
E (e V )
60
80
Ar
2+
Ar
3+
Ar
4+
I e
xtr
acte
d u
A
40W
60W
80W
100W
Mass Spectra For Varying Power
Argon
Pressure 1x 10-4 mbar
Bias voltage -400 V
21
200 250 300 350 400 450 500
0
20
40
Ar
9+
Ar
8+
Ar
7+
Ar
5+
Ar
6+
I e
xtr
acte
d u
A
B mT
200 250 300 350 400 450 500
0
20
40
60
80
Ar 9+
Ar 8+
Ar 7+
Ar 6+
Ar 5+
Ar 4+
Ar 3+ Ar 2+
I extracted uA
B mT
1x10-5
mbar
1x10-4
mbar
5x10-5
mbarMass Spectra For Varying Pressure
Argon
Power 100 W
Bias voltage -400 V
22
B mT
2 3 4 5 6 7 8 9
0
20
40
60
80
I uA
Charge State
1x10-5
mbar
5x10-5
mbar
1x10-4
mbar
Charge State Distribution
200 250 300 350 400 450 500
0
10
20
30
40
50
60
70
80
Ar 2+
Ar 3+
Ar 4+
Ar 5+
Ar 6+
Ar 7+
Ar 8+
Ar 9+
I extracted uA
0V
-400V
-200V
Mass Spectra For Varying Bias
Argon
Power 100 W
Pressure 1x 10-4 mbar
23
B mT
1 2 3 4 5 6 7 8 9 100
10
20
30
40
50
60
70
80
I uA
Charge State
Ar
0V
-200V
-400V
Charge State Distribution
α
σ
z
y
x
Current
Profile
d
Emittance calculation
πε /xxA=
ασε .2 xx =
( )d/tan 1 σα −=
24
FC1
SL1ECRIS
z
d
Pin hole
Einzel lens
Steerer
Measurement Setup
0 2 4 6 80,0
0,2
0,4
0,6
0,8
1,0
1,2
FC
Curr
ent m
A
Slit Position mm
Slit +X
Slit -X
Slit +Y
Slit -Y
-x+x
Z
+y
-y
Emittance Measurement
250 2 4 6 8 10 12 14 16
0,00
0,05
0,10
0,15
0,20
0,25
Peak3
Peak 2
Peak1
M1S1
dI/dx
Current Profile
σ =0.24149
σ =0.40832
σ =0.35993
σ =0.4551
Re
lati
ve
In
ten
sit
y m
A
Slit position mm
Pea
ks
Peak width
2σ mm
Peak half width
σ mm
Divergenc
e Angle α
Phase
space
area
2σ* α
mmrad
1 0.72 0.36 0.147 0.001
2 0.92 0.46 0.188 0.003
3 0.80 0.40 0.163 0.002
Mea
n = 0.81 = 0.40
=0.166
0.002
Summary
Plasma
Two different population of electrons below 30 keV and 100 keV
Stable plasma at nominal power
Unstable plasma at very low pressure
Charge state distribution
Enhanced with bias voltage but no change in plasma characteristics
Ion current extracted depends on gas mixing ratio
Emittance
26
Emittance
Ion beam emittance depends on extraction and beam line elements
Outlook
Longmuir probe measurements
Better emittance with pin hole and CCD camera
Thank you !
27