materials discussion / integrated testing plan final optics transmissive - issues related to...

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Materials Discussion / Integrated Testing Plan Optics nsmissive issues related to absorption lective LIDT and effect of dust neutron-induced swelling in GIMM and substrate mitigate neutron induced dimensional change e Issues lic Thermomechanics - modeling - high cycle fatigue of engineering matl’s sed Neutron Effects sed X-ray - threshold and roughening Ablation Effects sed Ion Materials Specific Issues Graphite Composite - Lifetime under high temp. irradiation - Tritium retention during high temp. irrad - Radiation Enhanced Sublimation at high te Ceramic Composite System - development and properties including fa Refractory Armored System - development and properties including fat Alloy system - effects of environment on fatigue prope

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Page 1: Materials Discussion / Integrated Testing Plan Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced

Materials Discussion / Integrated Testing Plan

Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced swelling in GIMM and substrate - mitigate neutron induced dimensional change

Unique Issues Cyclic Thermomechanics - modeling - high cycle fatigue of engineering matl’s Pulsed Neutron Effects Pulsed X-ray - threshold and roughening He Ablation Effects Pulsed Ion

Materials Specific Issues Graphite Composite - Lifetime under high temp. irradiation - Tritium retention during high temp. irradiation - Radiation Enhanced Sublimation at high temp.

Ceramic Composite System - development and properties including fatigue

Refractory Armored System - development and properties including fatigue

Alloy system - effects of environment on fatigue properties

Page 2: Materials Discussion / Integrated Testing Plan Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced

Materials Discussion / Integrated Testing Plan

Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced swelling in GIMM and substrate - mitigate neutron induced dimensional change

Unique Issues Cyclic Thermomechanics - modeling - high cycle fatigue of engineering matl’s Pulsed Neutron Effects Pulsed X-ray - threshold and roughening He Ablation Effects Pulsed Ion

Materials Specific Issues Graphite Composite - Lifetime under high temp. irradiation - Tritium retention during high temp. irradiation - Radiation Enhanced Sublimation at high temp.

Ceramic Composite System - development and properties including fatigue

Refractory Armored System - development and properties including fatigue

Alloy system - effects of environment on fatigue properties

}Absorption studies indicated that loss would be unacceptable high in transmissive optics. Emphasis was shifted to reflectiveoptics

Page 3: Materials Discussion / Integrated Testing Plan Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced

Materials Discussion / Integrated Testing Plan

Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced swelling in GIMM and substrate - mitigate neutron induced dimensional change

Unique Issues Cyclic Thermomechanics - modeling - high cycle fatigue of engineering matl’s Pulsed Neutron Effects Pulsed X-ray - threshold and roughening He Ablation Effects Pulsed Ion

Materials Specific Issues Graphite Composite - Lifetime under high temp. irradiation - Tritium retention during high temp. irradiation - Radiation Enhanced Sublimation at high temp.

Ceramic Composite System - development and properties including fatigue

Refractory Armored System - development and properties including fatigue

Alloy system - effects of environment on fatigue properties

} Current Optics Program Plan

Page 4: Materials Discussion / Integrated Testing Plan Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced

Materials Discussion / Integrated Testing Plan

Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced swelling in GIMM and substrate - mitigate neutron induced dimensional change

Unique Issues Cyclic Thermomechanics - modeling - high cycle fatigue of engineering matl’s Pulsed Neutron Effects Pulsed X-ray - threshold and roughening He Ablation Effects Pulsed Ion

Materials Specific Issues Graphite Composite - Lifetime under high temp. irradiation - Tritium retention during high temp. irradiation - Radiation Enhanced Sublimation at high temp.

Ceramic Composite System - development and properties including fatigue

Refractory Armored System - development and properties including fatigue

Alloy system - effects of environment on fatigue properties

}

}pending

Page 5: Materials Discussion / Integrated Testing Plan Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced

Materials Discussion / Integrated Testing Plan

Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced swelling in GIMM and substrate - mitigate neutron induced dimensional change

Unique Issues Cyclic Thermomechanics - modeling - high cycle fatigue of engineering matl’s Pulsed Neutron Effects Pulsed X-ray - threshold and roughening He Ablation Effects Pulsed Ion

Materials Specific Issues Graphite Composite - Lifetime under high temp. irradiation - Tritium retention during high temp. irradiation - Radiation Enhanced Sublimation at high temp.

Ceramic Composite System - development and properties including fatigue

Refractory Armored System - development and properties including fatigue

Alloy system - effects of environment on fatigue properties

} Ghoniem work

Page 6: Materials Discussion / Integrated Testing Plan Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced

Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced swelling in GIMM and substrate - mitigate neutron induced dimensional change

Unique Issues Cyclic Thermomechanics - modeling - high cycle fatigue of engineering matl’s Pulsed Neutron Effects Pulsed X-ray - threshold and roughening He Ablation Effects Pulsed Ion

Materials Specific Issues Graphite Composite - Lifetime under high temp. irradiation - Tritium retention during high temp. irradiation - Radiation Enhanced Sublimation at high temp.

Ceramic Composite System - development and properties including fatigue

Refractory Armored System - development and properties including fatigue

Alloy system - effects of environment on fatigue properties}

Pending ~200 MPa at 108 cycles

Page 7: Materials Discussion / Integrated Testing Plan Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced

Materials Discussion / Integrated Testing Plan

Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced swelling in GIMM and substrate - mitigate neutron induced dimensional change

Unique Issues Cyclic Thermomechanics - modeling - high cycle fatigue of engineering matl’s Pulsed Neutron Effects Pulsed X-ray - threshold and roughening He Ablation Effects Pulsed Ion

Materials Specific Issues Graphite Composite - Lifetime under high temp. irradiation - Tritium retention during high temp. irradiation - Radiation Enhanced Sublimation at high temp.

Ceramic Composite System - development and properties including fatigue

Refractory Armored System - development and properties including fatigue

Alloy system - effects of environment on fatigue properties

} Limited ongoing work in modeling community

Page 8: Materials Discussion / Integrated Testing Plan Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced

Materials Discussion / Integrated Testing Plan

Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced swelling in GIMM and substrate - mitigate neutron induced dimensional change

Unique Issues Cyclic Thermomechanics - modeling - high cycle fatigue of engineering matl’s Pulsed Neutron Effects Pulsed X-ray - threshold and roughening He Ablation Effects Pulsed Ion

Materials Specific Issues Graphite Composite - Lifetime under high temp. irradiation - Tritium retention during high temp. irradiation - Radiation Enhanced Sublimation at high temp.

Ceramic Composite System - development and properties including fatigue

Refractory Armored System - development and properties including fatigue

Alloy system - effects of environment on fatigue properties

}}}

Planned XAPPER@LLNL and Z@SNL

Ongoing and Planned, ORNL,UNC,DELFT

Ongoing and Plannned, RHEPP@SNL

Page 9: Materials Discussion / Integrated Testing Plan Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced

Materials Discussion / Integrated Testing Plan

Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced swelling in GIMM and substrate - mitigate neutron induced dimensional change

Unique Issues Cyclic Thermomechanics - modeling - high cycle fatigue of engineering matl’s Pulsed Neutron Effects Pulsed X-ray - threshold and roughening He Ablation Effects Pulsed Ion

Materials Specific Issues Graphite Composite - Lifetime under high temp. irradiation - Tritium retention during high temp. irradiation - Radiation Enhanced Sublimation at high temp.

Ceramic Composite System - development and properties including fatigue

Refractory Armored System - development and properties including fatigue

Alloy system - effects of environment on fatigue properties

{Current OFES/HAPL work

HFIR Irradiation

Page 10: Materials Discussion / Integrated Testing Plan Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced
Page 11: Materials Discussion / Integrated Testing Plan Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced

Materials Discussion / Integrated Testing Plan

Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced swelling in GIMM and substrate - mitigate neutron induced dimensional change

Unique Issues Cyclic Thermomechanics - modeling - high cycle fatigue of engineering matl’s Pulsed Neutron Effects Pulsed X-ray - threshold and roughening He Ablation Effects Pulsed Ion

Materials Specific Issues Graphite Composite - Lifetime under high temp. irradiation - Tritium retention during high temp. irradiation - Radiation Enhanced Sublimation at high temp.

Ceramic Composite System - development and properties including fatigue

Refractory Armored System - development and properties including fatigue

Alloy system - effects of environment on fatigue properties

{Waiting for completion of thermalablation study

{Pending

Page 12: Materials Discussion / Integrated Testing Plan Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced

Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced swelling in GIMM and substrate - mitigate neutron induced dimensional change

Unique Issues Cyclic Thermomechanics - modeling - high cycle fatigue of engineering matl’s Pulsed Neutron Effects Pulsed X-ray - threshold and roughening He Ablation Effects Pulsed Ion

Materials Specific Issues Graphite Composite - Lifetime under high temp. irradiation - Tritium retention during high temp. irradiation - Radiation Enhanced Sublimation at high temp.

Ceramic Composite System - development and properties including fatigue

Refractory Armored System - development and properties including fatigue

Alloy system - effects of environment on fatigue properties

{Ongoing developmentFatigue Planned

{Proposed FY-03

Page 13: Materials Discussion / Integrated Testing Plan Final Optics Transmissive - issues related to absorption Reflective - LIDT and effect of dust - neutron-induced

Round-Robin Materials

• All “candidate” optical and structural materials under the HAPL program are being coordinated to ensure uniformity in materials chemistry, history and where appropriate the surface condition (eg polishing for surface studies.)

• Currently, the “candidate” materials being distributed are:

Tungsten: Zone refined single crystal (99.999%)Chemically Vapor Deposited (99.995%)Powder met. Polycrystalline (99.99%)

Graphite: FMI-222 balanced weave pitch fiber/matrix compositeSegri Great Lakes Near Isotropic Candidate Nuclear Graphite

Silicon Carbide: Rohm-Haas CVD Silicon Carbide

Aluminum: 1000 series, fully annealedothers tbd