metals analysis method ilm04 - united states …

e-Ckent: WESTON(Delran)SDG: 81956(8-1)

METALS ANALYSISMETHOD ILM04.0

A R I O O I 7 6

Table 1Organic Volatile Soil Data Summary Table for Krewatch Farm Drum Burial Site

Compound

acetone2-butanonebenzenetetrachloroethenetolueneethyl benzenexylene (total)m-xyleneo/p-xylenecarbon disulfideunknown hydrocarbonunknown hydrocarbonunknown hydrocarbonunknown hydrocarbonunknown hydrocarbon2-propyl-furan

S-1ppm0.180.0360.020.0251674940490440ND7339362572

QJJ

J

JJJJJ

S-2ppm0.078NDNDND0.0220.0120.0270.0140.013ND0.0020.0170.0050.038

Q

JJJJ

S-3ppm0.2720NDND0.180.070.340.160.15ND2

0.130.050.4

0.04

Q

J

JJJJ

NJ

S-4ppmNDNDNDNDNDNDNDNDND0.010.040.2

QS-5

ppm0.028NDNDNDNDNDNDNDND0.0070.025

QJ

JJ

Risk Based Concentrationsfor Residential Soil, ppm

780NA2212

1600780160001600016000780

NAQ = Data QualifierNJ= Tentative ConfirmationJ = ApproximateND = Non-DetectNA=Not Available

f l R I O O I 7 7

Table 2Inorganic Soil Analysis Data Summary Table for Krewatch Farm Drum Burial Site

Compound

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLead

MagnesiumManganeseMercuryNickel

PotassiumSeleniumSilverSodiumThalliumVanadium

Zinc

S-1ppm4400ND0.5717.5NDND1689.31.339.9209019.112311.40.1214.878.6NDND99.1ND5.294.7

Q

L

B

U

B

S-2ppm3680ND0.499.7NDNDND3.6ND3.517803.665.44.10.232.167.4NDND77.3ND5.48.3

Q

L

B

ULBB

B

S-3ppm2840ND0.474.9NDNDND3.1NDND14403.226.54.50.12ND47.2NDND67.6ND5.93.7

Q

UL

B

UL

B

B

B

S-4ppm1160ND0.043.4NDNDND1.5NDND8111.1ND3.60.11ND24.7NDND52.9ND2.1ND

Q

U

B

J

U

B

B

B

S-5ppm1260ND0.0443.6NDNDND1.7NDND8101ND3.20.12ND23.8NDND53.6ND2.22.7

Q

UB

B

J

U

B

B

BB

ERA RBCsfor Residential Soil, ppm

78003.10.435500.153.9NA394703102300NANA1802.3160NA3939NANA5502300

ND=Non-detectQ= Data QualifierU=Below Detection LimitUL= Detection Limit Biased LowJ= ApproximateB=Blank ContaminationL=Biased LowNA=Not Available

HRIOOI78

WESTON - DELRAN

COVER PAGE - INORGANIC ANALYSES DATA PACKAGE

Lab Name: SOUTHWEST_RESEARCH_INSTIT Contract: 01-6421-427

Lab Code: SWRI_ Case No.: ____ SAS No.: _____ SDG No.:81956_

SOW No.: ILHO4.0

WESTON Sample No. Lab Sample ID_S1_________ .81956________S2_________ _"S3_________ _81958__"S4_________ _81959_"S5_________ _81960_"SIS________ _81956S_"S1SD_______ _81956SD"SID 81956D "

Were ICP interelement corrections applied 7 Yes/No YES

Were ICP background corrections applied ? Yes/No YESIf yes - were raw data generated beforeapplication of background corrections ? . Yes/No N0_

Comments:

I certify that this data package is in compliance with the terms andconditions of the contract, both technically and for completeness, forother than the conditions detailed above. Release of the data containedin this hardcopy data package and in the computer-readable data submittedon floppy diskette has been authorized by the Laboratory Manager or theManager's designee, as verified by the following signature.

Signature: ^ TV CLAju ToHLoC-lA Afl'V. Name: CTo

Date: 1^1 tX3 ) TC__________ Title:

COVER PAGE - IN ILM03.C

Client: WESTON(Delran)SDG: 81956(8-1)

RESULTS

f l R I O O I S O

WESTON - DELRAN 040001

1 WESTON SAMPLEINORGANIC ANALYSES DATA SHEET

SILab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427

Lab Code: SWRI_ Case No.: _____ SAS No.: _____ SDG No.: 81956,

Matrix (soil/water): SOIL_ Lab Sample IDx 81956

Level (low/med): LOW_ Date Received: 12/05/96

% Solids: _83.1

Concentration Units (ug/L or mg/kg dry weight): MG/KG

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-274*3-66-6

'- •

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

Concentration

44001.20.5717.51.20.951689.31.339.9209019.112311.40.1214.878.60.711.299.10.485.294.7

C

UB

UU

B

U

BUUBU

Q

NN

N

*

M

PPFPPPPPPPPFPPCVPPFPPFPP

Color Before: _______ Clarity Before: _____ Texture:

Color After: _______ Clarity After: _____ Artifacts:

Comments:

FORM I - IN ILM03.0

A R I O O I 8 I


1 WESTON SAMPLE NO.INORGANIC ANALYSES DATA SHEET

S2Lab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427


Matrix (soil/water): SOIL_ Lab Sample ID: 81957


% Solids: _85.9

Concentration Units (ug/L or ing/kg dry weight): KG/KG

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte


Concentration

36801.10.499.71.10.8911.13.61.13.517803.665.44.10.232.167.40.671.177.30.445.48.3

C

UB

UUU

U

B

UBBUUBU

Q

NN

N

*

M



Color After: _______ Clarity After: ____ Artifacts:

Comments:

FORM I - IN ILM03.0

f l R I O O I 8 2

WESTON - DELRAN 0400031 WESTON SAMPLE NO

INORGANIC ANALYSES DATA SHEET


Lab Code: SWRI_ Case No.: _____ SAS No,: _____ SDG No.: 81956.


Level (low/med): LOW__ Date Received: 12/05/96

% Solids: _85.5


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

"•'t

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel .PotassiumSeleniumSilverSodiumThalliumVanadiumZinc

Concentration

28401.20.474.91.20.9411.73.11.21.214403.226.54.50.121.247.20.701.267.60.475.93.7

C

UU

UUU

UU

B

UUBUUBU

B

Q

NN

N

*

M


Color Before: _______ Clarity Before: ____ Texture:


Comments:

FORM I - IN ILM03.0

A R I O O I 8 3

WESTON - DELRAN 0400041 WESTON SAMPLE NO.

INORGANIC ANALYSES DATA SHEET


Lab Code: SWRI_ Case No.: _____ SAS No.: _____ SDG No.: 81956.



% Solids: _85.2


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte


Concentration

11601.10.443.41.10.8811.01.51.11.18111.111.03.60.111.124.70.661.152.90.442.19.2

C

UUBUUUBUU

U

UUBUUBUB

Q

NN

N

*

M


Color Before: _______ Clarity Before: ____ Texture:


Comments:

FORM I - IN ILM03.0

A R I O O I 8 U


1 WESTON SAMPLE NOINORGANIC ANALYSES DATA SHEET


Lab Code: SWRI_ Case No.: _____ SAS No.: _____ SDG No.: 81956_



% Solid*: _87.4

Concentration Units (ug/L or rag/kg dry weight): MG/KG

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte


Concentration

12601.1

0.443.61.1

0.8911.11*71.11.18101.0

11.13.20.121.1

23.80.671.1

53.60.442.22.7

C

UuBUUuBUu

uuuBUuBUBB

Q

NN

N

*

M

PPPPPPPPPPPFPPCVPPFPPFFP


Color After: _______ Clarity After: ____ Artifacts:

Comments:

FORM I - IN ILM03.0

S R I Q O I 8 5

WSSTON -

2AINITIAL AND CONTINUING CALIBRATION VERIFICATION

Lab Name: SOUTHWEST_RESEARCH_INSTIT Contract:01-6421-427

Lab Code: SWRI_ Case No.: _____ SAS No.: _____ SDG No.: 81956

Initial Calibration Source: INORGVEN/SPE

Continuing Calibration Source: INORGVEN/SPE

Concentration Units: ug/L

Analyte

Aluminum^Antimony_Araenic _BariumBerylliumCadmiumCalciumChromiumCobalt __CopperIron ____LeadMagnesiumManganeseMercuryNickel^ __PotassiumSelenium_Silver __SodiumThallium—Vanadium_Zinc

Initial CalibrationTrue Found %R(1)

8000.04000.040.0

8000.0800.0800.0

16000.01600.04000.01600.08000.040.0

16000.0800.03.0

4000.016000.0

40.0— §00.016000.0

40.0— 4 00.0

800.0

7970.004103.3942.30

8189.78843.27817.60

16630.171639.244124.471639.848196.6041.00

16548.79821.533.03

3965.6415115.96

42.90840.31

15004.9242.30

4061.90809.22

99.6102.6105.8102.4105.4102.2103.9102.5103.1102.5102.5102.5103.4102.7101.099.194.5107.2105.093.8105.8101.5101.2

Continuing CalibrationTrue Found %R ( 1 ) Found %R ( 1 )

10000.05000.050.0

10000.01000.01000.020000.02000.05000.02000.010000.0

50.020000.01000.0

5.05000.020000.0

50.01000.020000.0

50.05000.01000.0

10197.695196.9650.20

10282.611066.971037.4221148.312076.235224.472077.0010396.91

51.702X093.771038.68

5.125022.8119889.73

49.901065.1119201.05

54.305145.661028.10

102.0103.9100.4102.8106.7103.7105.7103.8104.5103.8104.0103.4105.5103.9102.4100.599.499.8106.596.0108.6102.9102.8

10383.215214.2150.70

10294.171069.671035.7221165.612075.015222.132082.5810450.55

52.5021155.421038.82

5.055021.9819986.83

49.001066.2119427.07

52.50"5T44.871024.70

103.8104.3101.4102.9107.0103.6105.8103.8104.4104.1104.5105.0105.8103.9101.0100.499.998.0106.697.1105.0102.9102.5

M


(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115

FORM II (PART 1) - IN ILM03.0

f l R I O O I 8 6








Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSelenium_SilverSodiumThalliumVanadiumZinc


___ 40.0 __ 42.80

————

107.0

Continuing CalibrationTrue Found %R( 1 ) Found %R( 1 )

10000.05000.0

50.010000.01000.01000.020000.02000.05000.02000.010000.0

50.020000.01000.0

5.05000.020000.0

50.01000.020000.0

50.05000.01000.0

10210.645221.5750.00

10309.461072.211038.6021084.872076.995220.952081.6010405.77

52.9021135.581040.01

5.165026.7920071.72

51.401066.8619303.75

52.205152.321027.94

102.1104.4100.0103.1107.2103.9105.4103.8104.4104.1104.1105.8105.7104.0103.2100.5100.4102.8106.796.5104.4103.0102.8

10385.515240.0950.70

10297.081071.071041.2221185.682078.595232.122082.3410474.86

21257.84_1040.57

5028.0820061.83

52.401067.2919337.76

52.805148.691026.74

103.9104.8101.4103.0107.1104.1105.9103.9104.6104.1104.7

106.3104.1

100.6100.3104.8106.796.7105.6103.0102.7

**

H

PPPPPT>

P

P

P

P

FPPCVPPFPPFPP



f l R I O O I 8 7




Lab Codes SWRI_ Case No.: _____ SAS No.: _____ SDG No.: 81956_

Initial Calibration Source: INORGVEN/SFE



Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel^ _PotassiumSeleniumSilverSodiumThalliumVanadiumZinc


40.0

40.0

38.80

39.10

97.0

97.8

Continuing CalibrationTrue Found %R(1) Found %R(1)

50.0

50.0

50.0

47.60

46.60

52.40

95.2

93.2

104.8

47.60

49.90

95.2

99.8

M

NRNRNRNRNRNRNRNRNRNRNRFNRNRNRNRNRFNRNRFNRNR



f l R I O O I 8 8

WESTON - DELRAN

2A 0400onINITIAL AND CONTINUING CALIBRATION VERIFICATION





Concentration Unit*: ug/L

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel_j __PotassiumSeleniumSilverSodiumThalliumVanadiumZinc


40.0 41.10 102.8

Continuing CalibrationTrue Found %R(1) Found %R(1)

50.0 51.90————103.8 51.30

,,

102.6

•

M

NRNRNRNRNRR-urnNRNRNRNRFNRNRNRNRNRNRNRNRNRNRNR

(1) Control Limit*: Mercury 80-120; Other Metals 90-110; Cyanide 85-115


A R I O O I 8 9








Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel __PotassiumSeleniumSilverSodiumThalliumVanadiumZinc


--

Continuing CalibrationTrue Found %R ( 1 ) Found %R ( 1 )

50.0 53.00 106.0

2~•>-

H

NRNRNRNRNRNRNRNRNRNRNRFNRNRNRNRNRNRNRNRNRNRNR

(1) Control Limits: Mercury 80-120; Other Metal* 90-110; Cyanide 85-115


A R I O O I 9 0

WESTON - DELRAN

2B 040011CRDL STANDARD FOR AA AND TCP



AA CRDL Standard Source: SPEX______

ICP CRDL Standard Source: SPEX______


Analyte


CRDL £

True

10.0

3.0

0.2

5.0

10.0.

Standard fc

Found

8.90

3.70

0.17

5.30

11.30

>r AA

%R

89.0

123.3

85.0

106.0

113.0

True

120.0

10.010.0

20.0100.050.0

30.0

80.0

20.0

100.040.0

CRDL StaxInitialFound

119.65

10.139.96

20.02100.9950.10

30.20

77.92

20.19

98.4139.79

idard J

%R

99.7

101.399.6

100.1101.0100.2

100.7

97.4

101.0

98.499.5

Eor ICPFina]

Found

118.58

9.979.83

19.61100.4949.59

30.10

77.42

20.30

97.7240.37

L%R

98.8

99.7r".3

98.0100.599.2

100.3

96.8

101.5

97.7100.9

FORM II (PART 2) - IN ILM03

f l R I Q Q I 9 l

WESTON - DELRAN

2BCRDL STANDARD FOR AA AND XCP

040012




ICP CRDL Standard Source: SPEX______


Analyte


CRDL J

True

3.0

5.0

10.0

Standard ft

Found

2.00

4.90

9.30

ar AA

%R

66.7

98.0

93.0

True

CRDL StaiInitialFound

idard i

%R

Eor ICPFinaJ

FoundL%R

*


f l R I O O I 9 2


2BCRDL STANDARD FOR AA AMD ICP


Lab Code: SWRI_ Case No. I _____ SAS No.: _____ SDG No.: 81956


ICP CRDL Standard Source: _________


Analyte


CRDL S

True

3.0

- *•_ —— .— i—— *s

Standard fc

Found

2.50

>r AA

%R

83.3

True

CRDL StaiInitialFound

idard \

%R

Eor ICPFinal

FoundL%R

-

^

FORM II (FART 2) - IN ILM03

f l R I O O I 9 3

WESTON - DELRAN

0400143BLANKS


Lab Code: SWRI_ Caae No.: _____ SAS No.: _____ SDG No.: 81956

Preparation Blank Matrix (soil/water): SOIL__

Preparation Blank Concentration Units (ug/L or ing/kg): MG/KG

Analyte

Aluminum_AntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel^ __PotassiumSeleniumSilverSodiumThalliumVanadiumZinc

InitialCalib.Blank(ug/L) C

50.05.02.05.05.04.050.05.05.05.0

20.02.0

50.05.00.25.0

100.03.05*0

200.02.05.05.0

UUUUUUUUUUUUUUUUUUUUUUU

Continuing CalibrationBlank (ug/L)

1 C 2 C 3 C

50.05.02.05.05.04.050.05.05.05.0

20.02.0

50.05.00.25.0

100.03.05.0

200.02.05.05.0


50.05.02.05.05.04.0

50.05.05.05.0

20.02.0

50.05.00.25.0

100.03.05.0

200.02.05.05.0


50.05.02.05.05.04.050.05.05.05.020.02.050.05.00.25.0

__ 100. 0_

5.0200.02.05.05.0

UUUUUUUUUUUUUUUUU

UUUUU

Prepa-ration 7Blank - C

-25.7801.0000.4001.0001.0000.800

-30.0721.0001.0001.000-9.7180.400

-29.5121.0000.1001.00020.0000.6001.00041.4640.4001.0001.000

UUUUUBUUUBUBUUUUUUBUUU

M


FORM III - IN ILM03.0

WESTON - DELRAN _ .^ 040015

3BLANKS


Lab Codes SWRI_ Case No.: _____ SAS No.: _____ SDG No.i 81956

Preparation Blank Matrix (soil/water): ____

Preparation Blank Concentration Unit* (ug/L or rag/kg);

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel^ __PotassiumSeleniumSilverSodiumThalliumVanadiumZinc


2.0

3.0'•'

U

u


1 C . 2 C 3 C

50.05.02.05.05.04.0

52.35.05.05.0

22.52.0

50.45.0

5.0100.03.05.0

200.02.05.05.0

UUUUUUBUUUBUBU

Uuuuuuuu

2.0

3.0

U

U 3.0

*.

U

Prepa-ration tBlank | C

i_

-•

M

PPF?r*ppppppFPPNRPPFPPFPP

FORM III - IN ILM03

A R I O O I 9 5

WESTON - DELRAN

3BLANKS

04001G



Preparation Blank Matrix (soil/water): ____

Preparation Blank Concentration Units (ug/L or mg/kg):

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel^ __PotassiumSeleniumSilverSodiumThalliumVanadiumZinc


2.0

2.0

U

U


1 C 2 C 3 C

2.0

2.0

U

U

2.0

2.0

U

U

2.0

—

—

—

U

-

-

—

Prepa-.ration*Blank * C

•vM

NRNRNRNRNRNRNRNRNRNRNRFNRNRNRNRNRNRNRNRFNRNR

FORM III - IN ILM03.0

flR!OOI96

WESTON - DELRAN 04QQ17

4ICF INTERFERENCE CHECK SAMPLE

Lab Name: SOUTHWEST_RESEARCH_JNSTIT Contract: 01-6421-427

Lab Code: SWRI_ Case No.: _____ SAS No: _____ SDG No.: 81956,

ICP ID Number: TJA TRACE__ ICS Source: INORGVEN___


TrueSol. Sol.

Analyte A AB

Aluminum_AntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel^ _PotassiumSeleniumSilverSodiumThalliumVanadiumZinc

5000000

000

400000000

200000

5000000

0

0

00

500000600

500500

1000400000

500500500

200000

500000500

1000

200

5001000

Initial FoundSol. Sol.A AB %R

5044913

002

4472532802

181820

5325796

5

____ -1

-313

502881.0618.7

516.3492.0933.2

443770.2498.6481.1551.6

181346.3

529390.0489.5

937.4

___ 210.5

485.8884.1

100.6103.1

103.398.493.3

110.999.796.2

TlO.390.7

105.997.9

93.7

105.2

97.288.4

Final FoundSol. Sol.A AB %R

5041675

-102

4455012802

181818

5336716

5

____ -1

-313

503066.8624.5

517.3492.9935.3

"441098.6498.4480.6551.8

T8T281.8

530270.8490.1

939.5

___ 210.6

486.4881.1

100.6104.1

163.598.6"93.5TlO.89996

110.490.6

106.198.0

94.0

105.3

97.388.1

FORM IV - IN ILM03.0

A R I Q Q I 9 7


5A WESTON SAMPLE NOSPIKE SAMPLE RECOVERY

SISLab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427"


Matrix (soil/water): SOIL_ Level (low/med): LOW

% Solids for Sample: _83.1


Analyte


ControlLimit%R

75-12575-12575-12575-12575-125

75-12575-12575-125

75-12575-12575-125

75-12575-125

75-12575-125-75-125"*

*?.

Spiked SampleResult (SSR)

7176.218710.69647.2429

480.909611.69770.9945

54.2038115.382797.2095

2711.527436.5552

124.54420.5087

126.5014

2.157011.5047

11.4434120.1462197.7318

CSample

Result (SR)

4404.28691.19150.571917.47631.19150.9532

9.26481.322539.8732

2092.352119.0633

11.43080.120314.7574

0.71491.1915

0.47665.240094.7111

C

UB

UU

B

U

UU

U

SpikeAdded (SA)

454.1022.719.08

454.1011.351.14

45.41113.5356.76227.054.54

113.530.55

113.53

2.2711.35

11.35113.53113.53

%R

610.447.173.5102.1103.187.2

99.0100.5101.0272.7385.3

99.692.598.4

95.0101.4

100.8101.290.7

Q

NN

M

PPPPPPNRPPPPFNRPCVPNRFPNRFPP

Comments:

FORM V (Part 1) - IN ILM03.0

A R I O O I 9 8

WESTON - DELRAN

5A WESTON SAMPLE NOSPIKE SAMPLE RECOVERY

S1SDLab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427'


Matrix (soil/water): SOIL_ Level (low/med): LOW_

% Solids for Sample: _83.1


Analyte


ControlLimit%R

75-12575-12575-12575-12575-125

75-12575-12575-125

75-12575-12575-125

75-12575-125

75-12575-12575-125


7042.072910.71797.0251

479.348211.75480.9559

53.7940115.2963122.41303040.966339.2450

126.31560,5776

143.1042

1.691211.5209

10.8845118.7265232.7676

CSample

Result (SR)

4404.28691.19150.571917.47631.19150.9532

9.26481.322539.8732

2092.352119.0633

11.43080.120314.7574

0.71491.1915

0.47665.240094.7111

C

UB

UU

B

U

UU

U

SpikeAdded (SA)

449.8622.498.67

449.8611.251.12

44.99112.4656.23224.934.34

112.460.60

112.46

2.1711.25

10.84112.46112.46

%R

586.447.774.4102;7104.585; 399.0101.3146.8421.7465.0

102.296.3114.1

77.9102.4

100.4100.9122.8

Q

NN

M

PPPPPPNRPP.PPFNRPCVPNRFPNRFPP

Comments:



SB WESTON SAMPLE NO,POST DIGEST SPIKE SAMPLE RECOVERY

S1ALab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427


Matrix (soil/water) : SOIL_ Level (low/med): LOW


Analyte

AluminumAntimonyAraenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

ControlLimit%R

-•

•"


96.27

473.03

CSample

Result (SR)

5.00

167.33

C

U

Added (SA)

100.0

300.0

%R

96.3

•-

101.9

Q M

NRPNRNRNRNRNRNRNRPNRNRNRNRNRNRNRNRNRNRNRNRNR

Commentsi


SRIU0200


6 WESTON SAMPLE NO.DUPLICATES

S1DLab Name: SOUTHWEST RESEARCH INSTIT Contract;01-6421-427



% Solids for Sample: _83.1 % Solid* for Duplicate: _84.3

Concentration Units (ug/L or ing/kg dry weight): MG/KG

Analyte


ControlLimit

4.7660

119.14502.3830

119.14502.3830

4.7660

2.3830

Sample (S)

4404.28691.19150.571917.47631.19150.9532

167.51629.26481.322539.8732

2092.352119.0633123.332311.43080.120314.757478.55740.71491.191599.10050.47665.240094.7111

C

UB

UU

B

U

BUUBU

Duplicate (D)

4612.59301.14611.628118.46541.14610.9169

181.56217.83911.389039.9977

2178.928435.1573135.036411.79300.120316.164191.67150.70791.146193.08580.47195.604391.2039

C

UB

UU

B

U

BUUBU

RPD

4.6

96.05.5

8.016.74.90.34.159.49.13.1

9.115.4

6.3

6.73.8

Q

1£Jr

*

M

PPPPPPPPPP^-fPFPPCVPPFPPFPP

FORM VI - IN ILM03.0

flRI0020l

WESTON - DELRAN 0400°2

7LABORATORY CONTROL SAMPLE



Solid LCS Source: ERA 223

Aqueous LCS Source: ____

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel __PotassiumSeleniumSilverSodiumThalliumVanadiumZinc

Aqueous (ug/L)True Found %R

Solid (mg/kg)True Found C Limits %R

6030.053.8178.088.6102.0180.04110.0250.063.962.4

8550.094.8

2820.0155.010.0171.03470.0185.0202.0391.073.5135.0630.0

5512.150.3162.989.1104.6178.64003.9230.661.862.4

7640.189.6

2737.7154.510.4166.52841.4199.6220.2375.768.0134.5612.6

^

—

—

—

3000.010.887.461.964.6101.02790.0134.038.435.6

JI80.049.8

1680.0108.05.293.1

2150.097.0101.0220.036.772.8341.0

8620*096.8265,0116,0142.0259.05590.0352.090.890.4

14100.0135.04060.0209.015.6249.04580.0276.0295.0566.0110.0196.0938.0

91.493.591.5100.6102.599.297.492.296.7100.089.494.597.199.7104.097.481.9107.9109.096.192.599.697.2

FORM VII - IN ILM03.0

ARI00202


8STANDARD ADDITION RESULTS


Lab Code: SWRI_ Case No.: _____ SAS No.:_____ SDG No.:81956


WESTONSampleNo.

1An

10 ADDABS

f

„

11 ADD

CON ABS

12 ADD

CON ABS

13 ADD

CON ABS

1FinalCone.

1r Q

•*m

FORM VIII - IN ILM03.0

flRIQ0203

WESTON - DELRAN G 4 0024

9 WESTON SAMPLE MOICP SERIAL DILUTION

S1LLab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427




Analyte

Aluminum_AntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

Initial SampleResult (I)

18482.815.00

73.345.004.00

702.9938.885.55

167.338780.66

517.5747.97

61.93329.67

5.00415.88

21.99397.46

C

U

UU

B

B

UB

SerialDilutionResult (S)

17423.6025.00

61.6025.0020.00250.0034.5525.00159.008352.35

250.0045.35

54.00500.00

25.001000.00

25.00390.50

C

U

BUUUBU

UB

BU

UU

U

%Differ-ence

__ 5.7_

16.0

100.011.1100.05.04.9

100.05.5

12.8100.0

100.0

100.0~ 1.8

Q

—

M

FPNRPPPPPPPPNRPPNRPPNRPPNRPP

FORM IX - IN ILM03.0

flRI0020U

WESTON - DELRAN

10 040025Instrument Detection Limits (Quarterly)

--—Lab Name: SOUTHWEST_RESEARCH_INSTIT Contract:01-6421-427


ICP ID Number: TJAJTRACE__ Date: 06/28/96

Flame AA ID Number : __________

Furnace AA ID Number :

Comments:

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadimZinc

Wave-length(nm)

396.80206.83

493.40313.04228.80317.93267.71228.61324.75259.94

279.07257.61

231.60766.40

328.06588.99

292.40213.85

Back-ground

-

CRDL(ug/L)

1005102011

5001010101003

500100.220750510500101020

IDL(ug/L)

50.05.0

5.05.04.050.05.05.05.020.0

50.05.0

5.0100.0

5.0200.0

5.05.0

M

PPNRPPPPPPPPNRPPNRPPNRPPNRPP

FORM X - IN ILM03.0

ftR!QQ205

WESTON - DELRAN10 G4002G

Instrument Detection Limits (Quarterly)

Lab Name: SOUTHWBST_RESEARCH_INSTIT Contract:01-6421-427

Lab Code: SWRI_ Case No.: ____ SAS No.: _____ SDG No.: 81956

ICP ID Number: _________ Date: 06/28/96

Flame AA ID Number : _________

Furnace AA ID Number : PE Z5100

Comments:

Analyte

AluminumAntimonyArsenic _BariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadimZinc

Wave-length(nm)

_193.70_

283.30

196.00

276.80

Back-ground

__ BZ __

BZ

BZ

BZ

CRDL(ug/L)

1005102011

5001010101003

500100.220750510

500101020

IDL(ug/L)

____ 2.0

2.0

3.0

2.0

M

NRNRFNRNRNRNRNRNRNRNRFNRNRNRNRNRFNRNRFNRNR

FORM X - IN ILM03.0

RRI00206


10Instrument Detection Limits (Quarterly)

Lab Name: SOUTHWEST_RESEARCH_INSTIT Contract:01-6421-427 *~

Lab Code: SWRI_ Case No.: ____ SAS No.: _____ SDG No.: 81956_

ICP ID Number: _________ Date: 06/28/96

Flame AA ID Number : PE_4100ZL__

Furnace AA ID Number :

Comments:

Analyte


Wave-length(nm)

253.30

Back-ground

CRDL(ug/L)

1005102011

5001010101003

500100.220750510

500101020

IDL(ug/L)

0.2

M

NRNRNRNRNRNRNRNRNRNRNRNRNRNRCVNRNRNRNRNRNRNRNR

FORM X - IN ILM03.0

RRI00207


11AICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)


Lab Code: SWRI_ Case No.: ____ SAS No.: _____ SDG No.: 81956,

ICP ID Number: TJA TRACE Date: 04/17/96

Analyte

Aluminum_Antimony_Arsenic _BariumBerylliumCadmiumCalciumChromiumCobalt __Copper __IronLeadMagnesiumManganeseMercuryNickelPotassiumSelenium_SilverSodiumThallium_Vanadium^Zinc

Wave-length(nm)

396.80206.83193.69493.40313.04228.80317.93267.71228.61324.75259.94

279.07_257.61 _

231.60766.40196.02328.06588.99190.86292.40213.85

*

Ii

Al

0.00000000.00000000.00399200.00000000.00000000.00000000.00000000.0000000•0.00002800.00000000.0000000

0.0000000_0. 0000000

0.00000000.00000000.00012000.00000000.00000000.00010200.00000000.0000000

iterelement (

Ca

0.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0000000

0.0000000_0.0000000_

0.00000000.0000000

""0.00010500.00000000.00000000.00010600.0000000o.ooooooo"

Correction 1

Fe

0.00000000.00000000.00000000.00000000.00000000.00025300.00000000.00003800.00002500.00000000.0000000

0.0002180-0.0000140

0.00000000.00000000.00010600.00000000.00000000.00011200.00000000.0000870

factors for

Mg

0.00000000.00000000.00000000.00000000.00000000.00000000.00014900.00000000.00000000.0000000"0.0000000

0.0000000J). 0000380

0.0000000"0.00000000.0000000"0.00000000.00000000.00000000.00000000.0000650

••

CR_

-0.00013200.00871100.00121000.0000000-0.00002500.0000000"0.00041100.00012500.00000000.00000000.0002480

0.0000000_0. 0000000

0.00000000.00000000.00010400.00000000.00006300.00011400.00007300.0000000

Comments:

FORM XI (Part 1) - IN ILH03.0

ARI00208

WESTON - DELRAN

11BICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)

G4002f)



ICP ID Number: TJA TRACE Date: 04/17/96

Analyte

Aluminum^Antimony_Arsenic _BariumBerylliumCadmiumCalciumChromiumCobaltCopper __IronLeadMagnesiumManganeseMercuryNickel^ __PotassiumSelenium_SilverSodiumThallium_Vanadium_Zinc

Wave-length(nm)

396.80206.83193.69493.40313.04228.80317.93267.71228.61324.75259.94

279.07_257.61 _

231.60766.40196.02328.06588.99190.86292.40213.85

Ii

CU_

0.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0000000

0.0000000_0. 0000000

0.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0026530

iterelement C

MN_

0.00000000.00000000.0000000"0.00000000.00000000.00000000.00015400.0000000"0.00000000.0000000-0.0003880

-0.0051890_0.0000000_

0.00000000.00000000.00000000.00006800.00000000.00000000.00030000.0000580

Correction I

NI_

0.0000000-0.00017100.00024900.00000000.00000000.00000000.00000000.00000000.00025900.00000000.0000000

0.0000000_0. 0000000

0.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0033320

7actors for

TI_

0.00000000.0007520"0.0000000-0.00027500.00000000.0000000"0. 0000000"0.00004900.00143800.00008100.0000000

-0.0002350_0. 0000000

0.00000000.00000000.00000000.00000000.00000000.0000000"0.0071490-0.0001980

••

V _

0.0000000-0.00837500.0039920"0.0000450"0.00000000.00000000.00019600.0002650~0. 00000000.0000*000.000 0

•*-~s

-0.0000870_0. 0000000

-0.00021500.00000000.00000000.00005400.00000000.00000000.00000000.0001140

Comments:

FORM XI (Part 2) - IN ILH03.0

RRI00209


12ICF LINEAR RANGES (QUARTERLY)

Lab Name: SOUTHWEST_RESEARCH_INSTIT Contract: 01-6421-427

Lab Code: SWRI_ Case No.: ____ SAS No.: _____ SDG No,: 81956

ICF ID Number: TJA TRACE Date: 06/28/96

Comments:

Analyte


Integ.Time(sec.)

5.005.005.005.005.005.005.005.005.005.005.00

5.005.00

5.005.005.005.005.005.005.005.00

Concentration(ug/L)

600000.0100000.0100000.0100000.010000.050000.0600000.0100000.0100000.040000.0300000.0

625000.020000.0

100000.0500000.0100000.010000.0

1000000.0100000.0250000.050000.0

M

PPPPPPPPPPPNRPPNRPPPPPPPP

FORM XII - IN ILM03.0

ARI 002 10

040031WESTON - DELRAN

13PREPARATION LOG

•i


Lab Code: SWRI_ Case No.:_____ SAS No.: _____ SDG No.:81956_

Method: P

WESTONSampleNo.

LCSSPBSSIS1DSISS1SDS2S334S5

PreparationDate

12/13/9612/13/9612/13/9612/13/9612/13/9612/13/9612/13/9612/13/9612/13/9612/13/96

Weight(gram)

1.021.001.011.051.061.071.051.001.071.03

Volume(mL)

200200200200200200200200200200

FORM XIII - IN ILM03.0

A R I 0 0 2 I I

WESTON - DELRANn 040032

PREPARATION LOG


Lab Code: SWRI_ Case No.:_____ SAS No.: _____ SDG No.:81956_

Method: F

WESTONSampleNo.

LCSSPBSSIS1DSISS1SDS2S3S4S5

PreparationDate

12/13/9612/13/9612/13/9612/13/9612/13/9612/13/9612/13/9612/13/9612/13/9612/13/96

Weight(gram)

1.021.001.011.021.061.111.051.001.071.03

Volume(mL)

200200200200200200200200200200

FORM XIII - IN ILM03.0

SRI002I2


13PREPARATION LOG

Lab Name: SOUTHHEST_RZSEARCH_INSTIT Contract:01-6421-427

Lab Code: SWRI_ Case No.:_____ SAS No.: _____ SDG No.:81956a

Method: CV

WESTONSampleNo.

LCSSPBSSIS1DSISS1SD32S3S4S5

9 —————————

PreparationDate

12/18/9612/18/9612/18/9612/18/9612/18/9612/18/9612/18/9612/18/9612/18/9612/18/96

Weight(gram)

0.200.200.200.200.220.200.100.200.220.19

Volume(mL)

100100100100100100100100100100

FORM XIII - IN ILH03.0

flRI002!3


14ANALYSIS RUN LOG


Lab Code: SWRI_ Case No.: _____ SAS No.: _____ SDG No.:81956

Instrument ID Number: TJA TRACE___ Method: P_

Start Date: 12/23/96 End Date: 12/23/96

WESTONSampleNo.

SOS4SIS5S2S3S6ICVICBCCVCCBCRIICSAICSABCCVCCBFBSLCSSSIS1DS1LSISS1SDSISS1SDS2CCVCCBS3S435S1A

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.001.001.00

Time

10011003100510071009101110131015101910231028103310371042104710511056110011051110111411191124112811331137114211471151115612011238

% R AL

X

X

XXXX

XXXXXXXXXXX

XXXXXXX

sB

XX

XXXXXXXXXXXXXX

XXXXXXXXX

AsBA

X

X

XXXX

XXXXXXXXXXX

XXXXXXX

BE

X

X

XXXXXXXXXXXXXXXX

XXXXXXX

cD

X

X

XXXXXXXXXXXXXX

XXXXXXXXX

cA

X

X

XXXX

XXXXXXXXX

XXXXXXX

cR

X

X

XXXXXXXXXXXXXXXX

XXXXXXX

c0

X

X

XXXXXXXXXXXXXXXX

XXXXXXX

Ai

cuX

X

XXXXXXXXXXXXXXXX

XXXXXXX

laJ

FE

X

X

XXXX

XXXXXXXXXXX

XXXXXXX

Ly1

pB

:ei

MG

X

X

XXXX

XXXXXXXXX

XXXXXXX

1

MN

X

X

XXXXXXXXXXXXXXXX

XXXXXXX

H6NIX

X

XXXXXXXXXXXXXXXX

XXXXXXX

K

X

X

XXXX

XXXXXXXXX

XXXXXXX

sEAG

XX

XXXXXXXXXXXXXXXX

XXXXXXX

NA

X

X

XXXX

XXXXXXXXX

XXXXXXX

TLV

X

X

XXXXXXXXXXXXXXXX

XXXXXXX

zN

X

X

XXXXXXXXXXXXXXXX

XXXXXXX

FORM XIV - IN ILM03.(

A R I 0 0 2 I U

WESTON - DELRAN

u 040035ANALYSIS RUN LOG ^

Lab Name: SOUTHWEST_RESEARCH_INSTIT ContractiOl-6421-427

Lab Code: SWRI_ Case No.: _____ SAS No.: _____ SDG No. :81956_

Instrument ID Number: TJA TRACE___ Method: P_


WESTONSampleNo.

CRIICSAICSABCCVCCB

D/F

1.001.001.001.001.00

Time

12431247125212571301

% R

Analytes

AL

XXXX

sB

XXXXX

AS

-

BA

XXXX

BE

XXXXX

cD

XXXXX

cA

XXXX

cR

XXXXX

c0

XXXXX

cuXXXXX

FE

XXXX

pB

—

HG

XXXX

MN

XXXXX

HGNI

XXXXX

K

XXXX

sE

-

AG

XXXXX

NA

XXXX

TLV

XXXXX

•*•

zN

XXXXX

—

FORM XIV - IN ILM03

S R I Q Q 2 I 5

WESTON - DELRAN

14 G4003GANALYSIS RUM LOG


Lab Code: SWRI_ Case No.: _____ SAS No.: _____ SDG No.:81956_

Instrument ID Number: PE Z5100____ Method: F_


WESTONSampleNo.

SOS10S25S50S100ICVICBCCVCCBCRAPBSPBSALCSSLCSSASIS1AS1DS1DACCVCCBSISS1SAS1SDS1SDAS2S2AS3S3AS4S4ACCVCCB

D/F

1.001.001.001.001.001.001.001.001.001.001.001.00

10.0010.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

15531558160216071612163716411646165016551659170417081713171717221726173117351740174417491754175818031807181218161821182518301834

% R

__ 99.5

__ 79.0

99.5

__ 98.5

__ 88.5

__ 94.0

_ 108.0

107.5

112.0

Ana ly tea

ALSBAS

XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX

BABECDCACRC0CUFEPBNGHNHGNIK SEAGNATLV Z

N

FORM XIV - IN ILM03.(

flRl002(6


14ANALYSIS RUN LOG

•"•


Lab Code: SWRI_ Cave No.: _____ SAS No.: _____ SDG No.:81956,



WESTONSampleNo.

S5S5ACCVCCB

D/F

1.001.001.001.00

Time

1839184318481850

% R

107.5

Analytes

ALSBAS

XXXX

BABECDCACRC0CuFBPBMGHN

HGNIK SEAGNA

i

TL

-

V

~s

zN

FORM XIV - IN ILM03

A R I 0 0 2 I 7

WBSTON - DELRA*

14ANALYSIS RUN LOG

Lab Name: SOUTHWEST_RESEARCH_INSTIT Contract;01-6421-427




WESTONSampleNo.

SOS3S25S50S100ICVICBCCVCCBCRAPBSPBSALCSSLCSSASIS1AS1DS1DS1DACCVCCBSISSISS1SAS1SDS1SDS1SDAS2S2AS3S3ACCV

D/F

1.001.001.001.001.001.001.001.001.001.001.001.00

10.0010.001.001.001.001.001.001.001.001.00i.oa1.00i.oa1.001.001.001.001.001.001.00

Time

16441648165316581702170717111716172017251729173417381743174817521755175918041809181318151820182518271832183718421846185118551900

% R

104.0

89.0

81.0

292.5

_ 225.5

_ 248.5

103.5

101.5

Analytes

ALSBASBABECDCACRC0CUFEPB

XXXXXXXXXXXXXX

XX

XXXXX

HGHNHGNIK SEAGNA

-

TLV ZN

FORM XIV - IN ILM03.C

flRI002!8

WHSTOH -

14ANALYSIS RUN LOG '•-—>





WESTONSampleNo.

CCB

D/F

1.00

Time

1904

% R ALSBASBABECDCACRC0

Ai

CU

laJ

FE

Lyl

FB

X

:ei

M6

i

MNHGNIK SEAGNA

•-

TLV

— '

ZN

FORM XIV - IN ILM03

flRIQ02!9

WESTON - DELRAN

14ANALYSIS RUN LOG

040040


Lab Code: SWRI_ Case No.: _____ SAS No.: _____ SDG.No. S81956.



WESTONSampleNo.

SOS5S25S50S100ICVICBCCVCCBCRAPBSPBSALCSSLCSSASIS1AS1DS1DACCVCCB

D/F

1.001.001.001.001.001.001.001.001.001.001.001.0020.0020.001.001.001.001.001.001.00

*

Time

08450850085408590904091009140919092309280932093709410945095009540959100310081012

% R

112.0

109.0

106.0

109.0

ALSBAS

-

BABECDCACRC0

Al

CU

laJ

FE

Ly1

PB

:ei

MG

1

MNHGNIK SE

XXXXXXXXXXXXXXXXXXXX

AGNATLV ZN

FORM XIV - IN ILM03.0

ARI00220

WESTON - DELRAN

14 C40041ANALYSIS RUM LOG

•4_,


Lab Code: SWRI_ Case No.: _____ SAS No.: _____ SDG No.:81956.



WESTONSampleNo.

SOS10S25S50S100ICVICBCCVCCBCRAPBSPBSALCSSLCSSASIS1AS1DS1DACCVCCBSISS1SAS1SDS1SDAS2S2AS3S3AS4S4ACCVCCB

D/F

1.001.001.001.001.001.001.001.001.001.001.001.0010.0010.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

13431348135313571402140714111416142114251430143414391444144814531457150215071511151615201525152915341539154315481553155716021606

% R

__ 96.5

74.0

102.0

116.0

__ 90.5

__ 88.5

99.5

106.5

104.0

Analytes

ALSBASBABECDCACRC0CuFEPBM6MNHGNIK SEAGNA

f'"t

TL

XXXXXXXXXXxlXXXXXXXXXXXXXXX

XXXX

V

r*1

zN

FORM XIV - IN

3RI0022

WESTON - DELRAN

14ANALYSIS RUN LOG

L40042





WESTONSampleNo.

S5S5ACCVCCB

D/F

1.001.001.001.00

Time

1611161516201625

% R

112.5

Analytes

ALSBASBABECDCACRC0CUFEFBMGHNHGNIK SEAGNATL

XXXX

V zN

-

-

-

FORM XIV - IN ILM03.C

SRI00222

WSSTON - DELRAN

14ANALYSIS RUN LOG

•»«•


Lab Code: SWRI_ Cave No.: _____ SAS No.: _____ SDG No.:81956_



WESTONSampleNo.

SOS3S25S50S100ICVICBCCVCCBCRAS4S4AS5S5ACCVCCB

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

w

••<-

Time

2213221822222227223222422246225122552300230423092314231823232327

———

% R

95.5

96.5

Analytes

ALSBASBABECDCACRC0CUFBPB

XXXXXXXXXXXXXXXX

MGHNHGNIK SEAGNA

•*-*

,

TL

-H.

V

~*

zN

FORM XIV - IN ILM03

ARI00223


14ANALYSIS RUM LOG





WESTONSampleNo.

S5S25S50S100S100ICVICBCCVCCBCRAZZZZZZZZZZZZASISS1SAS1SDS1SDAS2S2ACCVCCBS3S3AS4S4AS5S5AZZZZZZZZZZZZZZZZZZCCVCCB

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

1116112011251130113611421146115111551200120412091215121912241228123312371246125012551259130413081313131813321337134213501354

% R

_ 118.0

__ 87.0

84.0

101.0

__ 95.0

85.0

107.0

__ 91.0

Analytei

ALSBASBABECDCACRC0CuFEPBHGMNHGNIK SE

XXXXXXXXXX

XXXXXXXXXXXXXX

XX

AGNA

£

f«

.-

'_"

TLV ZN

^

-


WESTON - DELRAN G40045

14ANALYSIS RUN LOG

•-—





WESTONSampleNo.

SOS10S25S50S100ZZZZZZS25ICVICBCCVCCBCRAS3S3ACCVCCB

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

•

Time

1936194019451950195419592006201620202025203020342039204320482052

% R

__ 96.5

Analytes

AL

-

SBAS

•

BABECDCACRC0CuFEPBMGMNHGNIK SEAGNA

*r•St

TL

XXXXX

XXXXXXXXXX

V zN

FORM XIV - IN ILM03

ftR!00225

C4004CWESTON - DELRAN

14ANALYSIS RUN LOG





WESTONSampleNo.

SOS3S25S50S100ICVICBCCVCCBCRASICCVCCBSIS1AS1DS1DASISS1SAS1SDS1SDACCVCCB

D/F

1.001.001.001.001.001.001.001.001.001.005.001.001.005.005.005.005.005.005.005.005.001.001.09-'*

Time

16421648165517011708173317401746175317591806181318191830183718431850185719031910191719231930

% R

__ 99.0

_ 101.0

__ 98.0

_ 102.0

Analytea

ALSBASBABECDCACRC0CuFBPB

XXXXXXXXXX

XXXXXXXXXXXX

MGHNHGNIK SEAGNA

I•*v•M•V?.+

TLV ZN

-


ARI00226

WESTON - DELRAN G40047

14ANALYSIS RUN LOG



Instrument ID Number: PE 4100ZL___ Method: CV


WESTONSampleNo.

SOSO. 5SIS2S5S10ICVICBCCVCCBCRAZZZZZZPBSZZZZZZLCSSSIS1DSISS1SDS2CCVCCBS3S4S5CCVCCB

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

012401270130013201350138014001430146014901510153015902010204020602090212021402170221022402260229023202350237

% R ALSBASBABECDCACRC0

Ar

CU

laJ

FE

Lyt

PB

:ec

H6

I

HNHG

XXXXXXXXXXX

X

XXXXXXXXXXXXX

NIK SEAGNATLV

***!

ZN

FORM XIV - IN ILM03

flRI00227

metals analysis method ilm04 - united states …

Documents